#------------------------------------------------------------------------------
#$Date: 2019-11-06 17:26:41 +0200 (Wed, 06 Nov 2019) $
#$Revision: 223416 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/05/89/7058990.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7058990
loop_
_publ_author_name
'Sukhikh, Taisiya S.'
'Kolybalov, Dmitry S.'
'Pylova, Ekaterina K.'
'Bashirov, Denis A.'
'Komarov, Vladislav Y.'
'Kuratieva, Natalia V.'
'Smolentsev, Anton I.'
'Fitch, Andrew N.'
'Konchenko, Sergey N.'
_publ_section_title
;
 A fresh look at the structural diversity of dibenzoylmethanide complexes
 of lanthanides
;
_journal_issue                   25
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              9934
_journal_paper_doi               10.1039/C9NJ02059D
_journal_volume                  43
_journal_year                    2019
_chemical_formula_moiety         '2(C63 H50 Dy K O9)'
_chemical_formula_sum            'C126 H100 Dy2 K2 O18'
_chemical_formula_weight         2305.25
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_audit_creation_date             2018-11-27
_audit_creation_method
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_audit_update_record
;
2019-04-18 deposited with the CCDC.	2019-05-30 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 104.6080(10)
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   28.8124(5)
_cell_length_b                   28.9292(5)
_cell_length_c                   26.2157(5)
_cell_measurement_reflns_used    9285
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      28.74
_cell_measurement_theta_min      2.23
_cell_volume                     21144.9(7)
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'XS (Sheldrick, 2008)'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0394
_diffrn_reflns_av_unetI/netI     0.0335
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.997
_diffrn_reflns_limit_h_max       38
_diffrn_reflns_limit_h_min       -37
_diffrn_reflns_limit_k_max       36
_diffrn_reflns_limit_k_min       -39
_diffrn_reflns_limit_l_max       35
_diffrn_reflns_limit_l_min       -35
_diffrn_reflns_number            136904
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.997
_diffrn_reflns_theta_full        26.000
_diffrn_reflns_theta_max         28.762
_diffrn_reflns_theta_min         1.014
_exptl_absorpt_coefficient_mu    1.551
_exptl_absorpt_correction_T_max  0.7458
_exptl_absorpt_correction_T_min  0.5374
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
'SADABS-2012/1 (Bruker,2012) was used for absorption correction. wR2(int) was 0.0753 before and 0.0529 after correction. The Ratio of minimum to maximum transmission is 0.7206. The λ/2 correction factor is 0.0015.'
_exptl_crystal_colour            yellow
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    1.448
_exptl_crystal_description       prism
_exptl_crystal_F_000             9360
_exptl_crystal_size_max          0.3
_exptl_crystal_size_mid          0.2
_exptl_crystal_size_min          0.08
_refine_diff_density_max         1.304
_refine_diff_density_min         -1.201
_refine_diff_density_rms         0.089
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.033
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1341
_refine_ls_number_reflns         27414
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.033
_refine_ls_R_factor_all          0.0376
_refine_ls_R_factor_gt           0.0274
_refine_ls_shift/su_max          0.006
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0194P)²+46.7923P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0598
_refine_ls_wR_factor_ref         0.0654
_reflns_Friedel_coverage         0.000
_reflns_number_gt                23488
_reflns_number_total             27414
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c9nj02059d2.cif
_cod_data_source_block           ts209_3b_2
_cod_database_code               7058990
_shelx_shelxl_version_number     2017/1
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_max   0.886
_shelx_estimated_absorpt_t_min   0.653
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2.a Aromatic/amide H refined with riding coordinates:
 C12(H12), C22(H22), C32(H32), C42(H42), C112(H112), C113(H113), C114(H114),
 C115(H115), C116(H116), C122(H122), C123(H123), C124(H124), C125(H125),
 C126(H126), C212(H212), C213(H213), C214(H214), C215(H215), C216(H216),
 C222(H222), C223(H223), C224(H224), C225(H225), C226(H226), C312(H312),
 C313(H313), C314(H314), C315(H315), C316(H316), C322(H322), C323(H323),
 C324(H324), C325(H325), C326(H326), C412(H412), C413(H413), C414(H414),
 C415(H415), C416(H416), C422(H422), C423(H423), C424(H424), C425(H425),
 C426(H426), C52(H52), C62(H62), C72(H72), C82(H82), C512(H512), C513(H513),
 C514(H514), C515(H515), C516(H516), C522(H522), C523(H523), C524(H524),
 C525(H525), C526(H526), C612(H612), C613(H613), C614(H614), C615(H615),
 C616(H616), C622(H622), C623(H623), C624(H624), C625(H625), C626(H626),
 C712(H712), C713(H713), C714(H714), C715(H715), C716(H716), C722(H722),
 C723(H723), C724(H724), C725(H725), C726(H726), C812(H812), C813(H813),
 C814(H814), C815(H815), C816(H816), C822(H822), C823(H823), C824(H824),
 C825(H825), C826(H826)
2.b Idealised Me refined as rotating group:
 C92(H92A,H92B,H92C), C94(H94A,H94B,H94C), C96(H96A,H96B,H96C), C97(H97A,H97B,
 H97C)
;
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
Dy1 Dy 0.62364(2) 0.55843(2) 0.76143(2) 0.01555(3) Uani 1 1 d . . .
K1 K 0.500000 0.48223(2) 0.750000 0.02191(13) Uani 1 2 d S T P
K2 K 0.500000 0.62833(2) 0.750000 0.02281(13) Uani 1 2 d S T P
O1 O 0.68696(5) 0.57499(5) 0.83223(6) 0.0222(3) Uani 1 1 d . . .
O2 O 0.66447(5) 0.49024(5) 0.79122(6) 0.0259(3) Uani 1 1 d . . .
O3 O 0.66152(5) 0.54536(5) 0.69414(6) 0.0217(3) Uani 1 1 d . . .
O4 O 0.65097(5) 0.63012(5) 0.73690(6) 0.0230(3) Uani 1 1 d . . .
O5 O 0.57645(5) 0.49912(5) 0.70767(5) 0.0204(3) Uani 1 1 d . . .
O6 O 0.55777(5) 0.58926(5) 0.70053(6) 0.0224(3) Uani 1 1 d . . .
O7 O 0.57716(6) 0.52226(5) 0.81243(6) 0.0234(3) Uani 1 1 d . . .
O8 O 0.59264(5) 0.61470(5) 0.81228(6) 0.0217(3) Uani 1 1 d . . .
O9 O 0.500000 0.71546(8) 0.750000 0.0495(7) Uani 1 2 d S T P
O10 O 0.500000 0.39361(9) 0.750000 0.0633(9) Uani 1 2 d S T P
C11 C 0.71232(7) 0.55352(7) 0.87162(8) 0.0198(4) Uani 1 1 d . . .
C12 C 0.71475(8) 0.50522(7) 0.87561(9) 0.0240(4) Uani 1 1 d . . .
H12 H 0.733046 0.491659 0.907341 0.029 Uiso 1 1 calc R . .
C13 C 0.69100(7) 0.47613(7) 0.83422(8) 0.0213(4) Uani 1 1 d . . .
C21 C 0.65901(7) 0.64543(7) 0.69486(8) 0.0216(4) Uani 1 1 d . . .
C22 C 0.66477(8) 0.61755(7) 0.65308(8) 0.0237(4) Uani 1 1 d . . .
H22 H 0.668353 0.632329 0.621937 0.028 Uiso 1 1 calc R . .
C23 C 0.66551(7) 0.56929(8) 0.65472(8) 0.0220(4) Uani 1 1 d . . .
C31 C 0.56845(7) 0.50001(7) 0.65781(8) 0.0176(4) Uani 1 1 d . . .
C32 C 0.55340(7) 0.54023(7) 0.62756(8) 0.0192(4) Uani 1 1 d . . .
H32 H 0.547221 0.538355 0.590268 0.023 Uiso 1 1 calc R . .
C33 C 0.54727(7) 0.58262(7) 0.65047(8) 0.0182(4) Uani 1 1 d . . .
C41 C 0.58140(7) 0.52808(7) 0.86158(8) 0.0182(4) Uani 1 1 d . . .
C42 C 0.59548(8) 0.56972(7) 0.88820(8) 0.0208(4) Uani 1 1 d . . .
H42 H 0.602314 0.569926 0.925593 0.025 Uiso 1 1 calc R . .
C43 C 0.59995(7) 0.61128(7) 0.86194(8) 0.0194(4) Uani 1 1 d . . .
C91 C 0.500000 0.75703(11) 0.750000 0.0307(7) Uani 1 2 d S T P
C92 C 0.45556(10) 0.78340(9) 0.75013(12) 0.0411(6) Uani 1 1 d . . .
H92A H 0.442020 0.796435 0.715019 0.062 Uiso 1 1 calc GR . .
H92B H 0.463346 0.808464 0.776029 0.062 Uiso 1 1 calc GR . .
H92C H 0.432097 0.762624 0.759418 0.062 Uiso 1 1 calc GR . .
C93 C 0.500000 0.35212(12) 0.750000 0.0469(11) Uani 1 2 d S T P
C94 C 0.54601(15) 0.32584(11) 0.76090(15) 0.0675(10) Uani 1 1 d . . .
H94A H 0.547775 0.308393 0.729400 0.101 Uiso 1 1 calc GR . .
H94B H 0.547484 0.304393 0.790203 0.101 Uiso 1 1 calc GR . .
H94C H 0.573008 0.347469 0.770259 0.101 Uiso 1 1 calc GR . .
C111 C 0.74136(7) 0.58366(7) 0.91484(8) 0.0227(4) Uani 1 1 d . . .
C112 C 0.73940(10) 0.63121(8) 0.90688(10) 0.0350(6) Uani 1 1 d . . .
H112 H 0.720826 0.643545 0.874566 0.042 Uiso 1 1 calc R . .
C113 C 0.76442(12) 0.66071(10) 0.94589(11) 0.0488(8) Uani 1 1 d . . .
H113 H 0.762876 0.693170 0.940237 0.059 Uiso 1 1 calc R . .
C114 C 0.79160(11) 0.64308(10) 0.99297(11) 0.0491(8) Uani 1 1 d . . .
H114 H 0.808777 0.663421 1.019532 0.059 Uiso 1 1 calc R . .
C115 C 0.79381(10) 0.59618(10) 1.00141(10) 0.0429(7) Uani 1 1 d . . .
H115 H 0.812430 0.584109 1.033844 0.051 Uiso 1 1 calc R . .
C116 C 0.76884(9) 0.56646(9) 0.96256(9) 0.0319(5) Uani 1 1 d . . .
H116 H 0.770509 0.534048 0.968559 0.038 Uiso 1 1 calc R . .
C121 C 0.69808(8) 0.42461(7) 0.83858(9) 0.0244(4) Uani 1 1 d . . .
C122 C 0.71799(11) 0.40215(9) 0.88563(12) 0.0470(7) Uani 1 1 d . . .
H122 H 0.728274 0.419456 0.917270 0.056 Uiso 1 1 calc R . .
C123 C 0.72298(13) 0.35420(10) 0.88674(15) 0.0678(11) Uani 1 1 d . . .
H123 H 0.736363 0.338976 0.919234 0.081 Uiso 1 1 calc R . .
C124 C 0.70870(11) 0.32882(9) 0.84122(14) 0.0515(8) Uani 1 1 d . . .
H124 H 0.713099 0.296256 0.842073 0.062 Uiso 1 1 calc R . .
C125 C 0.68819(11) 0.35046(9) 0.79476(12) 0.0458(7) Uani 1 1 d . . .
H125 H 0.677618 0.332888 0.763350 0.055 Uiso 1 1 calc R . .
C126 C 0.68277(10) 0.39827(8) 0.79341(10) 0.0366(6) Uani 1 1 d . . .
H126 H 0.668311 0.413065 0.760940 0.044 Uiso 1 1 calc R . .
C211 C 0.66301(8) 0.69719(7) 0.69078(9) 0.0249(4) Uani 1 1 d . . .
C212 C 0.66360(9) 0.72386(8) 0.73485(10) 0.0326(5) Uani 1 1 d . . .
H212 H 0.661642 0.709277 0.766710 0.039 Uiso 1 1 calc R . .
C213 C 0.66703(10) 0.77180(9) 0.73293(12) 0.0423(6) Uani 1 1 d . . .
H213 H 0.667802 0.789660 0.763539 0.051 Uiso 1 1 calc R . .
C214 C 0.66932(11) 0.79346(9) 0.68675(13) 0.0486(7) Uani 1 1 d . . .
H214 H 0.671694 0.826169 0.685456 0.058 Uiso 1 1 calc R . .
C215 C 0.66814(14) 0.76752(10) 0.64289(14) 0.0615(9) Uani 1 1 d . . .
H215 H 0.669185 0.782345 0.610865 0.074 Uiso 1 1 calc R . .
C216 C 0.66543(12) 0.71950(10) 0.64477(12) 0.0497(8) Uani 1 1 d . . .
H216 H 0.665241 0.701857 0.614151 0.060 Uiso 1 1 calc R . .
C221 C 0.67214(7) 0.54286(8) 0.60761(9) 0.0250(4) Uani 1 1 d . . .
C222 C 0.65927(9) 0.56118(9) 0.55692(10) 0.0327(5) Uani 1 1 d . . .
H222 H 0.647129 0.591812 0.551663 0.039 Uiso 1 1 calc R . .
C223 C 0.66396(9) 0.53524(11) 0.51390(10) 0.0412(7) Uani 1 1 d . . .
H223 H 0.654882 0.548058 0.479453 0.049 Uiso 1 1 calc R . .
C224 C 0.68187(9) 0.49071(11) 0.52133(11) 0.0448(7) Uani 1 1 d . . .
H224 H 0.685078 0.472897 0.491964 0.054 Uiso 1 1 calc R . .
C225 C 0.69504(9) 0.47220(10) 0.57131(12) 0.0412(6) Uani 1 1 d . . .
H225 H 0.707719 0.441750 0.576368 0.049 Uiso 1 1 calc R . .
C226 C 0.68989(8) 0.49785(9) 0.61440(10) 0.0329(5) Uani 1 1 d . . .
H226 H 0.698525 0.484622 0.648668 0.039 Uiso 1 1 calc R . .
C311 C 0.57557(7) 0.45534(7) 0.63191(8) 0.0202(4) Uani 1 1 d . . .
C312 C 0.58081(10) 0.41498(8) 0.66189(9) 0.0331(5) Uani 1 1 d . . .
H312 H 0.577435 0.416039 0.696998 0.040 Uiso 1 1 calc R . .
C313 C 0.59092(11) 0.37326(8) 0.64085(11) 0.0419(7) Uani 1 1 d . . .
H313 H 0.594150 0.345926 0.661533 0.050 Uiso 1 1 calc R . .
C314 C 0.59628(9) 0.37127(8) 0.59017(10) 0.0350(6) Uani 1 1 d . . .
H314 H 0.603644 0.342743 0.576063 0.042 Uiso 1 1 calc R . .
C315 C 0.59090(8) 0.41096(8) 0.55994(9) 0.0292(5) Uani 1 1 d . . .
H315 H 0.594334 0.409606 0.524870 0.035 Uiso 1 1 calc R . .
C316 C 0.58049(8) 0.45282(7) 0.58050(8) 0.0230(4) Uani 1 1 d . . .
H316 H 0.576706 0.479907 0.559359 0.028 Uiso 1 1 calc R . .
C321 C 0.52869(7) 0.62435(7) 0.61795(8) 0.0187(4) Uani 1 1 d . . .
C322 C 0.53792(8) 0.66757(7) 0.64195(9) 0.0247(4) Uani 1 1 d . . .
H322 H 0.556101 0.669701 0.677545 0.030 Uiso 1 1 calc R . .
C323 C 0.52074(9) 0.70743(8) 0.61423(10) 0.0326(5) Uani 1 1 d . . .
H323 H 0.527243 0.736702 0.630942 0.039 Uiso 1 1 calc R . .
C324 C 0.49419(9) 0.70485(8) 0.56241(10) 0.0309(5) Uani 1 1 d . . .
H324 H 0.482130 0.732194 0.543634 0.037 Uiso 1 1 calc R . .
C325 C 0.48531(8) 0.66216(8) 0.53808(9) 0.0271(5) Uani 1 1 d . . .
H325 H 0.467277 0.660265 0.502412 0.032 Uiso 1 1 calc R . .
C326 C 0.50258(8) 0.62211(7) 0.56543(8) 0.0217(4) Uani 1 1 d . . .
H326 H 0.496567 0.592991 0.548283 0.026 Uiso 1 1 calc R . .
C411 C 0.57015(7) 0.48689(7) 0.89099(8) 0.0200(4) Uani 1 1 d . . .
C412 C 0.57584(9) 0.44283(7) 0.87201(9) 0.0283(5) Uani 1 1 d . . .
H412 H 0.587118 0.439312 0.841160 0.034 Uiso 1 1 calc R . .
C413 C 0.56509(10) 0.40400(8) 0.89808(11) 0.0375(6) Uani 1 1 d . . .
H413 H 0.569643 0.374017 0.885383 0.045 Uiso 1 1 calc R . .
C414 C 0.54780(10) 0.40884(8) 0.94236(10) 0.0358(6) Uani 1 1 d . . .
H414 H 0.539939 0.382237 0.959712 0.043 Uiso 1 1 calc R . .
C415 C 0.54193(9) 0.45246(8) 0.96142(9) 0.0288(5) Uani 1 1 d . . .
H415 H 0.529955 0.455764 0.991829 0.035 Uiso 1 1 calc R . .
C416 C 0.55345(8) 0.49128(7) 0.93634(8) 0.0227(4) Uani 1 1 d . . .
H416 H 0.549980 0.521117 0.950064 0.027 Uiso 1 1 calc R . .
C421 C 0.61237(8) 0.65475(7) 0.89368(9) 0.0242(4) Uani 1 1 d . . .
C422 C 0.63508(9) 0.65411(9) 0.94720(9) 0.0335(5) Uani 1 1 d . . .
H422 H 0.643290 0.625399 0.964734 0.040 Uiso 1 1 calc R . .
C423 C 0.64585(11) 0.69518(10) 0.97523(11) 0.0472(7) Uani 1 1 d . . .
H423 H 0.661775 0.694486 1.011675 0.057 Uiso 1 1 calc R . .
C424 C 0.63342(12) 0.73686(10) 0.95012(14) 0.0568(9) Uani 1 1 d . . .
H424 H 0.640066 0.764883 0.969475 0.068 Uiso 1 1 calc R . .
C425 C 0.61154(13) 0.73799(10) 0.89737(14) 0.0568(9) Uani 1 1 d . . .
H425 H 0.603089 0.766825 0.880200 0.068 Uiso 1 1 calc R . .
C426 C 0.60159(10) 0.69711(8) 0.86875(11) 0.0387(6) Uani 1 1 d . . .
H426 H 0.587334 0.698215 0.831909 0.046 Uiso 1 1 calc R . .
Dy2 Dy 0.500000 0.17304(2) 0.750000 0.01588(3) Uani 1 2 d S T P
Dy3 Dy 0.500000 -0.07053(2) 0.750000 0.01701(3) Uani 1 2 d S T P
K3 K 0.42652(2) 0.05155(2) 0.75039(2) 0.02304(9) Uani 1 1 d . . .
O11 O 0.56252(5) 0.20885(5) 0.72300(6) 0.0247(3) Uani 1 1 d . . .
O12 O 0.46754(5) 0.22170(5) 0.67980(6) 0.0231(3) Uani 1 1 d . . .
O13 O 0.47675(5) 0.11927(5) 0.80623(6) 0.0236(3) Uani 1 1 d . . .
O14 O 0.56872(5) 0.13331(5) 0.80298(6) 0.0219(3) Uani 1 1 d . . .
O15 O 0.45401(5) -0.03087(5) 0.80166(6) 0.0220(3) Uani 1 1 d . . .
O16 O 0.54558(6) -0.01475(5) 0.80528(6) 0.0255(3) Uani 1 1 d . . .
O17 O 0.57749(5) -0.10249(5) 0.77395(6) 0.0264(3) Uani 1 1 d . . .
O18 O 0.50424(5) -0.12129(5) 0.81971(6) 0.0235(3) Uani 1 1 d . . .
O19 O 0.33863(7) 0.06125(8) 0.75128(9) 0.0533(6) Uani 1 1 d . . .
C51 C 0.56722(8) 0.22741(7) 0.68118(8) 0.0208(4) Uani 1 1 d . . .
C52 C 0.52891(8) 0.24298(7) 0.64017(9) 0.0249(4) Uani 1 1 d . . .
H52 H 0.535998 0.256126 0.609792 0.030 Uiso 1 1 calc R . .
C53 C 0.48098(8) 0.24004(7) 0.64193(8) 0.0205(4) Uani 1 1 d . . .
C61 C 0.49489(8) 0.11251(7) 0.85533(8) 0.0201(4) Uani 1 1 d . . .
C62 C 0.54315(8) 0.12009(7) 0.88046(8) 0.0230(4) Uani 1 1 d . . .
H62 H 0.552909 0.118255 0.917831 0.028 Uiso 1 1 calc R . .
C63 C 0.57790(8) 0.13030(7) 0.85290(8) 0.0213(4) Uani 1 1 d . . .
C71 C 0.46779(8) -0.03388(7) 0.85154(8) 0.0198(4) Uani 1 1 d . . .
C72 C 0.51568(8) -0.02594(7) 0.88019(8) 0.0212(4) Uani 1 1 d . . .
H72 H 0.523613 -0.028404 0.917530 0.025 Uiso 1 1 calc R . .
C73 C 0.55177(7) -0.01458(7) 0.85527(8) 0.0196(4) Uani 1 1 d . . .
C81 C 0.60381(8) -0.11839(7) 0.81628(9) 0.0227(4) Uani 1 1 d . . .
C82 C 0.58678(8) -0.13205(7) 0.85970(9) 0.0257(5) Uani 1 1 d . . .
H82 H 0.609456 -0.140919 0.891210 0.031 Uiso 1 1 calc R . .
C83 C 0.53824(8) -0.13321(7) 0.85875(8) 0.0231(4) Uani 1 1 d . . .
C95 C 0.29987(9) 0.06291(9) 0.76080(10) 0.0342(6) Uani 1 1 d . . .
C96 C 0.27685(10) 0.10766(10) 0.76819(13) 0.0473(7) Uani 1 1 d . . .
H96A H 0.301014 0.132268 0.774597 0.071 Uiso 1 1 calc GR . .
H96B H 0.262768 0.105295 0.798434 0.071 Uiso 1 1 calc GR . .
H96C H 0.251638 0.114877 0.736404 0.071 Uiso 1 1 calc GR . .
C97 C 0.27294(10) 0.01985(10) 0.76537(13) 0.0471(7) Uani 1 1 d . . .
H97A H 0.288931 -0.006609 0.753811 0.071 Uiso 1 1 calc GR . .
H97B H 0.240131 0.022401 0.743147 0.071 Uiso 1 1 calc GR . .
H97C H 0.272009 0.015399 0.802157 0.071 Uiso 1 1 calc GR . .
C511 C 0.61795(8) 0.23416(7) 0.67734(9) 0.0241(4) Uani 1 1 d . . .
C512 C 0.62951(9) 0.24117(10) 0.62944(11) 0.0383(6) Uani 1 1 d . . .
H512 H 0.604842 0.242329 0.597639 0.046 Uiso 1 1 calc R . .
C513 C 0.67721(10) 0.24649(12) 0.62820(13) 0.0520(8) Uani 1 1 d . . .
H513 H 0.684981 0.251250 0.595469 0.062 Uiso 1 1 calc R . .
C514 C 0.71324(10) 0.24489(10) 0.67410(13) 0.0457(7) Uani 1 1 d . . .
H514 H 0.745721 0.248608 0.672955 0.055 Uiso 1 1 calc R . .
C515 C 0.70215(9) 0.23789(9) 0.72170(12) 0.0401(6) Uani 1 1 d . . .
H515 H 0.726967 0.236970 0.753386 0.048 Uiso 1 1 calc R . .
C516 C 0.65482(8) 0.23222(8) 0.72328(10) 0.0313(5) Uani 1 1 d . . .
H516 H 0.647419 0.226928 0.756122 0.038 Uiso 1 1 calc R . .
C521 C 0.44145(8) 0.25926(7) 0.59798(9) 0.0237(4) Uani 1 1 d . . .
C522 C 0.39485(9) 0.25760(10) 0.60364(10) 0.0387(6) Uani 1 1 d . . .
H522 H 0.388934 0.245727 0.635197 0.046 Uiso 1 1 calc R . .
C523 C 0.35699(10) 0.27310(12) 0.56367(12) 0.0534(8) Uani 1 1 d . . .
H523 H 0.325238 0.271888 0.567944 0.064 Uiso 1 1 calc R . .
C524 C 0.36518(11) 0.29041(11) 0.51739(11) 0.0476(7) Uani 1 1 d . . .
H524 H 0.339053 0.300833 0.489931 0.057 Uiso 1 1 calc R . .
C525 C 0.41107(10) 0.29246(9) 0.51131(10) 0.0381(6) Uani 1 1 d . . .
H525 H 0.416718 0.304282 0.479611 0.046 Uiso 1 1 calc R . .
C526 C 0.44923(9) 0.27727(8) 0.55148(9) 0.0291(5) Uani 1 1 d . . .
H526 H 0.480966 0.279150 0.547260 0.035 Uiso 1 1 calc R . .
C611 C 0.46087(8) 0.09540(7) 0.88592(8) 0.0213(4) Uani 1 1 d . . .
C612 C 0.47593(9) 0.06814(7) 0.93094(8) 0.0240(4) Uani 1 1 d . . .
H612 H 0.508981 0.060971 0.944004 0.029 Uiso 1 1 calc R . .
C613 C 0.44294(9) 0.05151(8) 0.95663(9) 0.0304(5) Uani 1 1 d . . .
H613 H 0.453414 0.032343 0.986772 0.037 Uiso 1 1 calc R . .
C614 C 0.39493(10) 0.06247(9) 0.93893(10) 0.0378(6) Uani 1 1 d . . .
H614 H 0.372489 0.051121 0.956928 0.045 Uiso 1 1 calc R . .
C615 C 0.37967(9) 0.09017(10) 0.89469(11) 0.0379(6) Uani 1 1 d . . .
H615 H 0.346748 0.098240 0.882758 0.045 Uiso 1 1 calc R . .
C616 C 0.41225(8) 0.10618(8) 0.86772(9) 0.0289(5) Uani 1 1 d . . .
H616 H 0.401451 0.124456 0.836905 0.035 Uiso 1 1 calc R . .
C621 C 0.62925(8) 0.13727(8) 0.88243(10) 0.0298(5) Uani 1 1 d . . .
C622 C 0.66433(10) 0.13617(12) 0.85520(14) 0.0553(9) Uani 1 1 d . . .
H622 H 0.655733 0.130904 0.818239 0.066 Uiso 1 1 calc R . .
C623 C 0.71203(12) 0.14269(17) 0.88124(19) 0.0875(15) Uani 1 1 d . . .
H623 H 0.735957 0.141558 0.862095 0.105 Uiso 1 1 calc R . .
C624 C 0.72490(12) 0.15074(15) 0.93433(18) 0.0806(13) Uani 1 1 d . . .
H624 H 0.757726 0.154725 0.952091 0.097 Uiso 1 1 calc R . .
C625 C 0.69070(13) 0.15304(13) 0.96169(14) 0.0674(11) Uani 1 1 d . . .
H625 H 0.699686 0.159247 0.998459 0.081 Uiso 1 1 calc R . .
C626 C 0.64268(10) 0.14639(11) 0.93629(11) 0.0474(7) Uani 1 1 d . . .
H626 H 0.618983 0.148059 0.955697 0.057 Uiso 1 1 calc R . .
C711 C 0.43006(8) -0.04712(7) 0.87885(8) 0.0219(4) Uani 1 1 d . . .
C712 C 0.44058(9) -0.06612(7) 0.92922(9) 0.0261(5) Uani 1 1 d . . .
H712 H 0.472922 -0.067702 0.949445 0.031 Uiso 1 1 calc R . .
C713 C 0.40425(9) -0.08269(8) 0.95001(10) 0.0324(5) Uani 1 1 d . . .
H713 H 0.411919 -0.095707 0.984384 0.039 Uiso 1 1 calc R . .
C714 C 0.35708(10) -0.08057(9) 0.92152(10) 0.0376(6) Uani 1 1 d . . .
H714 H 0.332418 -0.092845 0.935705 0.045 Uiso 1 1 calc R . .
C715 C 0.34590(10) -0.06037(10) 0.87197(11) 0.0414(6) Uani 1 1 d . . .
H715 H 0.313373 -0.057844 0.852518 0.050 Uiso 1 1 calc R . .
C716 C 0.38220(9) -0.04386(9) 0.85080(10) 0.0329(5) Uani 1 1 d . . .
H716 H 0.374336 -0.030158 0.816769 0.039 Uiso 1 1 calc R . .
C721 C 0.60128(8) -0.00197(7) 0.88595(8) 0.0214(4) Uani 1 1 d . . .
C722 C 0.61245(8) 0.01282(8) 0.93803(9) 0.0258(5) Uani 1 1 d . . .
H722 H 0.588178 0.013961 0.956700 0.031 Uiso 1 1 calc R . .
C723 C 0.65904(9) 0.02594(9) 0.96286(10) 0.0339(5) Uani 1 1 d . . .
H723 H 0.666450 0.036117 0.998456 0.041 Uiso 1 1 calc R . .
C724 C 0.69464(9) 0.02429(9) 0.93619(11) 0.0392(6) Uani 1 1 d . . .
H724 H 0.726302 0.033870 0.953171 0.047 Uiso 1 1 calc R . .
C725 C 0.68408(9) 0.00863(10) 0.88459(11) 0.0387(6) Uani 1 1 d . . .
H725 H 0.708631 0.006847 0.866348 0.046 Uiso 1 1 calc R . .
C726 C 0.63785(8) -0.00436(8) 0.85977(9) 0.0294(5) Uani 1 1 d . . .
H726 H 0.630777 -0.015072 0.824392 0.035 Uiso 1 1 calc R . .
C811 C 0.65651(8) -0.12249(7) 0.81897(9) 0.0269(5) Uani 1 1 d . . .
C812 C 0.68942(10) -0.14341(11) 0.86029(11) 0.0444(7) Uani 1 1 d . . .
H812 H 0.678837 -0.156694 0.888524 0.053 Uiso 1 1 calc R . .
C813 C 0.73772(11) -0.14517(13) 0.86085(13) 0.0582(9) Uani 1 1 d . . .
H813 H 0.759872 -0.159316 0.889670 0.070 Uiso 1 1 calc R . .
C814 C 0.75371(10) -0.12677(11) 0.82036(14) 0.0536(8) Uani 1 1 d . . .
H814 H 0.786829 -0.127732 0.821110 0.064 Uiso 1 1 calc R . .
C815 C 0.72130(11) -0.10686(11) 0.77858(15) 0.0575(9) Uani 1 1 d . . .
H815 H 0.732011 -0.094581 0.749931 0.069 Uiso 1 1 calc R . .
C816 C 0.67311(10) -0.10453(9) 0.77789(12) 0.0431(7) Uani 1 1 d . . .
H816 H 0.651163 -0.090433 0.748863 0.052 Uiso 1 1 calc R . .
C821 C 0.52345(9) -0.15096(7) 0.90631(9) 0.0265(5) Uani 1 1 d . . .
C822 C 0.47710(10) -0.16735(8) 0.90048(10) 0.0335(5) Uani 1 1 d . . .
H822 H 0.455484 -0.167996 0.866485 0.040 Uiso 1 1 calc R . .
C823 C 0.46195(12) -0.18286(8) 0.94396(12) 0.0438(7) Uani 1 1 d . . .
H823 H 0.430424 -0.194706 0.939488 0.053 Uiso 1 1 calc R . .
C824 C 0.49308(13) -0.18094(8) 0.99375(11) 0.0480(8) Uani 1 1 d . . .
H824 H 0.482678 -0.190939 1.023563 0.058 Uiso 1 1 calc R . .
C825 C 0.53892(12) -0.16460(8) 1.00006(10) 0.0428(7) Uani 1 1 d . . .
H825 H 0.560138 -0.163357 1.034268 0.051 Uiso 1 1 calc R . .
C826 C 0.55440(10) -0.14993(8) 0.95685(9) 0.0347(6) Uani 1 1 d . . .
H826 H 0.586318 -0.139062 0.961577 0.042 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
K2 Dy1 K1 62.240(11) . .
O1 Dy1 K1 131.51(4) . .
O1 Dy1 K2 117.42(4) . .
O1 Dy1 O2 71.04(5) . .
O1 Dy1 O3 102.54(5) . .
O1 Dy1 O4 77.65(5) . .
O1 Dy1 O5 146.64(5) . .
O1 Dy1 O6 144.78(5) . .
O1 Dy1 O7 94.77(5) . .
O1 Dy1 O8 75.09(5) . .
O2 Dy1 K1 85.74(4) . .
O2 Dy1 K2 144.11(4) . .
O2 Dy1 O4 131.27(5) . .
O2 Dy1 O5 75.87(5) . .
O2 Dy1 O7 75.26(6) . .
O2 Dy1 O8 127.75(5) . .
O3 Dy1 K1 114.74(4) . .
O3 Dy1 K2 126.74(4) . .
O3 Dy1 O2 79.79(5) . .
O3 Dy1 O4 71.60(5) . .
O3 Dy1 O5 75.19(5) . .
O3 Dy1 O7 142.96(5) . .
O3 Dy1 O8 146.91(5) . .
O4 Dy1 K1 141.98(4) . .
O4 Dy1 K2 83.62(4) . .
O4 Dy1 O5 129.99(5) . .
O4 Dy1 O8 75.74(5) . .
O5 Dy1 K1 39.62(3) . .
O5 Dy1 K2 87.49(4) . .
O5 Dy1 O8 124.77(5) . .
O6 Dy1 K1 67.43(4) . .
O6 Dy1 K2 37.48(4) . .
O6 Dy1 O2 144.11(5) . .
O6 Dy1 O3 89.97(5) . .
O6 Dy1 O4 75.36(5) . .
O6 Dy1 O5 68.26(5) . .
O6 Dy1 O7 94.44(5) . .
O6 Dy1 O8 76.66(5) . .
O7 Dy1 K1 37.23(3) . .
O7 Dy1 K2 69.42(4) . .
O7 Dy1 O4 144.87(5) . .
O7 Dy1 O5 72.48(5) . .
O7 Dy1 O8 69.18(5) . .
O8 Dy1 K1 88.14(4) . .
O8 Dy1 K2 42.39(3) . .
Dy1 K1 Dy1 115.569(14) . 2_656
Dy1 K1 K2 57.784(7) 2_656 .
Dy1 K1 K2 57.785(7) . .
O5 K1 Dy1 34.01(3) 2_656 2_656
O5 K1 Dy1 129.74(3) . 2_656
O5 K1 Dy1 129.74(3) 2_656 .
O5 K1 Dy1 34.02(3) . .
O5 K1 K2 79.76(3) 2_656 .
O5 K1 K2 79.76(3) . .
O5 K1 O5 159.52(6) 2_656 .
O5 K1 C31 153.60(5) . 2_656
O5 K1 C31 18.62(4) 2_656 2_656
O5 K1 C31 153.60(5) 2_656 .
O5 K1 C31 18.62(4) . .
O5 K1 C41 80.47(4) 2_656 2_656
O5 K1 C41 91.80(4) . 2_656
O5 K1 C41 80.47(4) . .
O5 K1 C41 91.80(4) 2_656 .
O7 K1 Dy1 32.37(3) 2_656 2_656
O7 K1 Dy1 32.37(3) . .
O7 K1 Dy1 112.46(4) 2_656 .
O7 K1 Dy1 112.46(4) . 2_656
O7 K1 K2 64.29(3) 2_656 .
O7 K1 K2 64.29(3) . .
O7 K1 O5 107.67(4) 2_656 .
O7 K1 O5 62.75(4) . .
O7 K1 O5 62.75(4) 2_656 2_656
O7 K1 O5 107.67(4) . 2_656
O7 K1 O7 128.57(7) . 2_656
O7 K1 C31 80.41(4) 2_656 2_656
O7 K1 C31 80.41(4) . .
O7 K1 C31 92.28(5) . 2_656
O7 K1 C31 92.28(5) 2_656 .
O7 K1 C41 128.62(5) 2_656 .
O7 K1 C41 17.91(4) . .
O7 K1 C41 128.62(5) . 2_656
O7 K1 C41 17.91(4) 2_656 2_656
O10 K1 Dy1 122.216(7) . 2_656
O10 K1 Dy1 122.215(7) . .
O10 K1 K2 180.0 . .
O10 K1 O5 100.24(3) . .
O10 K1 O5 100.24(3) . 2_656
O10 K1 O7 115.71(3) . 2_656
O10 K1 O7 115.71(3) . .
O10 K1 C31 98.40(3) . 2_656
O10 K1 C31 98.40(3) . .
O10 K1 C41 112.17(3) . 2_656
O10 K1 C41 112.17(3) . .
C31 K1 Dy1 49.50(3) . .
C31 K1 Dy1 49.50(3) 2_656 2_656
C31 K1 Dy1 119.58(3) . 2_656
C31 K1 Dy1 119.58(3) 2_656 .
C31 K1 K2 81.60(3) . .
C31 K1 K2 81.60(3) 2_656 .
C31 K1 C31 163.20(7) . 2_656
C41 K1 Dy1 49.97(3) . .
C41 K1 Dy1 103.94(3) 2_656 .
C41 K1 Dy1 49.97(3) 2_656 2_656
C41 K1 Dy1 103.94(3) . 2_656
C41 K1 K2 67.83(3) 2_656 .
C41 K1 K2 67.83(3) . .
C41 K1 C31 75.25(5) 2_656 .
C41 K1 C31 98.30(5) 2_656 2_656
C41 K1 C31 98.30(5) . .
C41 K1 C31 75.25(5) . 2_656
C41 K1 C41 135.66(7) 2_656 .
Dy1 K2 Dy1 119.952(15) . 2_656
Dy1 K2 K1 59.977(8) 2_656 .
Dy1 K2 K1 59.975(8) . .
O6 K2 Dy1 32.84(3) 2_656 2_656
O6 K2 Dy1 32.84(3) . .
O6 K2 Dy1 114.02(4) . 2_656
O6 K2 Dy1 114.02(4) 2_656 .
O6 K2 K1 64.35(4) 2_656 .
O6 K2 K1 64.35(4) . .
O6 K2 O6 128.71(7) 2_656 .
O6 K2 O8 65.98(4) 2_656 2_656
O6 K2 O8 65.98(4) . .
O6 K2 O8 106.53(4) 2_656 .
O6 K2 O8 106.53(4) . 2_656
O6 K2 C33 128.65(5) . 2_656
O6 K2 C33 17.79(4) 2_656 2_656
O6 K2 C33 128.65(5) 2_656 .
O6 K2 C33 17.79(4) . .
O6 K2 C322 156.55(5) . 2_656
O6 K2 C322 50.62(5) . .
O6 K2 C322 156.55(5) 2_656 .
O6 K2 C322 50.62(5) 2_656 2_656
O8 K2 Dy1 132.04(3) . 2_656
O8 K2 Dy1 35.77(3) 2_656 2_656
O8 K2 Dy1 35.77(3) . .
O8 K2 Dy1 132.04(3) 2_656 .
O8 K2 K1 81.86(3) . .
O8 K2 K1 81.86(3) 2_656 .
O8 K2 O8 163.72(6) 2_656 .
O8 K2 C33 83.55(4) 2_656 2_656
O8 K2 C33 90.29(4) 2_656 .
O8 K2 C33 90.29(4) . 2_656
O8 K2 C33 83.55(4) . .
O8 K2 C322 91.16(5) . 2_656
O8 K2 C322 94.15(5) . .
O8 K2 C322 94.15(5) 2_656 2_656
O8 K2 C322 91.16(5) 2_656 .
O9 K2 Dy1 120.025(8) . .
O9 K2 Dy1 120.023(8) . 2_656
O9 K2 K1 180.0 . .
O9 K2 O6 115.65(4) . 2_656
O9 K2 O6 115.65(4) . .
O9 K2 O8 98.14(3) . .
O9 K2 O8 98.14(3) . 2_656
O9 K2 C33 112.24(3) . 2_656
O9 K2 C33 112.24(3) . .
O9 K2 C322 70.93(4) . 2_656
O9 K2 C322 70.93(4) . .
C33 K2 Dy1 104.93(3) . 2_656
C33 K2 Dy1 50.47(3) 2_656 2_656
C33 K2 Dy1 104.93(3) 2_656 .
C33 K2 Dy1 50.47(3) . .
C33 K2 K1 67.76(3) . .
C33 K2 K1 67.76(3) 2_656 .
C33 K2 C33 135.52(7) . 2_656
C322 K2 Dy1 76.78(4) . .
C322 K2 Dy1 123.76(4) 2_656 .
C322 K2 Dy1 76.78(4) 2_656 2_656
C322 K2 Dy1 123.76(4) . 2_656
C322 K2 K1 109.07(4) 2_656 .
C322 K2 K1 109.07(4) . .
C322 K2 C33 174.14(5) 2_656 .
C322 K2 C33 174.14(5) . 2_656
C322 K2 C33 41.64(5) . .
C322 K2 C33 41.64(5) 2_656 2_656
C322 K2 C322 141.85(7) . 2_656
C11 O1 Dy1 137.08(13) . .
C13 O2 Dy1 135.71(14) . .
C23 O3 Dy1 133.04(14) . .
C21 O4 Dy1 133.81(13) . .
Dy1 O5 K1 106.36(5) . .
C31 O5 Dy1 121.12(12) . .
C31 O5 K1 117.62(12) . .
Dy1 O6 K2 109.68(5) . .
C33 O6 Dy1 125.78(13) . .
C33 O6 K2 123.82(12) . .
Dy1 O7 K1 110.40(5) . .
C41 O7 Dy1 126.18(13) . .
C41 O7 K1 121.99(13) . .
Dy1 O8 K2 101.84(5) . .
C43 O8 Dy1 121.68(12) . .
C43 O8 K2 119.95(13) . .
C91 O9 K2 180.0 . .
C93 O10 K1 180.0 . .
O1 C11 C12 123.85(19) . .
O1 C11 C111 115.24(18) . .
C12 C11 C111 120.90(19) . .
C11 C12 H12 118.9 . .
C11 C12 C13 122.23(19) . .
C13 C12 H12 118.9 . .
O2 C13 C12 124.32(19) . .
O2 C13 C121 115.40(19) . .
C12 C13 C121 120.23(19) . .
O4 C21 C22 124.32(19) . .
O4 C21 C211 116.39(19) . .
C22 C21 C211 119.29(19) . .
C21 C22 H22 118.2 . .
C23 C22 C21 123.7(2) . .
C23 C22 H22 118.2 . .
O3 C23 C22 124.4(2) . .
O3 C23 C221 116.48(19) . .
C22 C23 C221 119.1(2) . .
O5 C31 K1 43.76(10) . .
O5 C31 C32 123.03(18) . .
O5 C31 C311 116.06(17) . .
C32 C31 K1 111.08(13) . .
C32 C31 C311 120.90(18) . .
C311 C31 K1 110.47(12) . .
C31 C32 H32 118.8 . .
C33 C32 C31 122.40(18) . .
C33 C32 H32 118.8 . .
O6 C33 K2 38.39(9) . .
O6 C33 C32 123.23(18) . .
O6 C33 C321 114.80(17) . .
C32 C33 K2 140.28(14) . .
C32 C33 C321 121.96(18) . .
C321 C33 K2 88.24(11) . .
O7 C41 K1 40.10(10) . .
O7 C41 C42 124.01(18) . .
O7 C41 C411 115.94(17) . .
C42 C41 K1 142.02(14) . .
C42 C41 C411 120.05(18) . .
C411 C41 K1 86.71(11) . .
C41 C42 H42 118.6 . .
C41 C42 C43 122.82(19) . .
C43 C42 H42 118.6 . .
O8 C43 C42 123.81(19) . .
O8 C43 C421 117.26(18) . .
C42 C43 C421 118.89(18) . .
O9 C91 C92 120.77(15) . .
O9 C91 C92 120.76(15) . 2_656
C92 C91 C92 118.5(3) . 2_656
C91 C92 H92A 109.5 . .
C91 C92 H92B 109.5 . .
C91 C92 H92C 109.5 . .
H92A C92 H92B 109.5 . .
H92A C92 H92C 109.5 . .
H92B C92 H92C 109.5 . .
O10 C93 C94 120.63(18) . 2_656
O10 C93 C94 120.63(18) . .
C94 C93 C94 118.7(4) 2_656 .
C93 C94 H94A 109.5 . .
C93 C94 H94B 109.5 . .
C93 C94 H94C 109.5 . .
H94A C94 H94B 109.5 . .
H94A C94 H94C 109.5 . .
H94B C94 H94C 109.5 . .
C112 C111 C11 117.79(19) . .
C112 C111 C116 118.7(2) . .
C116 C111 C11 123.5(2) . .
C111 C112 H112 119.9 . .
C113 C112 C111 120.3(2) . .
C113 C112 H112 119.9 . .
C112 C113 H113 119.9 . .
C114 C113 C112 120.3(3) . .
C114 C113 H113 119.9 . .
C113 C114 H114 120.0 . .
C115 C114 C113 120.1(2) . .
C115 C114 H114 120.0 . .
C114 C115 H115 120.0 . .
C114 C115 C116 120.0(2) . .
C116 C115 H115 120.0 . .
C111 C116 H116 119.7 . .
C115 C116 C111 120.7(2) . .
C115 C116 H116 119.7 . .
C122 C121 C13 123.4(2) . .
C126 C121 C13 118.2(2) . .
C126 C121 C122 118.4(2) . .
C121 C122 H122 119.9 . .
C121 C122 C123 120.2(3) . .
C123 C122 H122 119.9 . .
C122 C123 H123 119.8 . .
C124 C123 C122 120.5(3) . .
C124 C123 H123 119.8 . .
C123 C124 H124 120.1 . .
C125 C124 C123 119.9(3) . .
C125 C124 H124 120.1 . .
C124 C125 H125 120.0 . .
C124 C125 C126 120.0(3) . .
C126 C125 H125 120.0 . .
C121 C126 C125 121.1(2) . .
C121 C126 H126 119.5 . .
C125 C126 H126 119.5 . .
C212 C211 C21 118.6(2) . .
C216 C211 C21 123.1(2) . .
C216 C211 C212 118.3(2) . .
C211 C212 H212 119.7 . .
C211 C212 C213 120.7(2) . .
C213 C212 H212 119.7 . .
C212 C213 H213 119.9 . .
C214 C213 C212 120.3(3) . .
C214 C213 H213 119.9 . .
C213 C214 H214 120.2 . .
C215 C214 C213 119.5(3) . .
C215 C214 H214 120.2 . .
C214 C215 H215 119.7 . .
C214 C215 C216 120.5(3) . .
C216 C215 H215 119.7 . .
C211 C216 C215 120.7(3) . .
C211 C216 H216 119.6 . .
C215 C216 H216 119.6 . .
C222 C221 C23 122.1(2) . .
C222 C221 C226 118.6(2) . .
C226 C221 C23 119.2(2) . .
C221 C222 H222 119.6 . .
C223 C222 C221 120.8(3) . .
C223 C222 H222 119.6 . .
C222 C223 H223 120.1 . .
C224 C223 C222 119.9(3) . .
C224 C223 H223 120.1 . .
C223 C224 H224 120.0 . .
C225 C224 C223 120.0(2) . .
C225 C224 H224 120.0 . .
C224 C225 H225 119.8 . .
C224 C225 C226 120.3(3) . .
C226 C225 H225 119.8 . .
C221 C226 H226 119.8 . .
C225 C226 C221 120.4(3) . .
C225 C226 H226 119.8 . .
C312 C311 C31 118.33(19) . .
C316 C311 C31 122.89(19) . .
C316 C311 C312 118.6(2) . .
C311 C312 H312 119.7 . .
C313 C312 C311 120.5(2) . .
C313 C312 H312 119.7 . .
C312 C313 H313 119.8 . .
C314 C313 C312 120.4(2) . .
C314 C313 H313 119.8 . .
C313 C314 H314 120.2 . .
C313 C314 C315 119.7(2) . .
C315 C314 H314 120.2 . .
C314 C315 H315 119.8 . .
C314 C315 C316 120.4(2) . .
C316 C315 H315 119.8 . .
C311 C316 H316 119.8 . .
C315 C316 C311 120.4(2) . .
C315 C316 H316 119.8 . .
C322 C321 C33 117.78(18) . .
C326 C321 C33 123.46(18) . .
C326 C321 C322 118.76(19) . .
K2 C322 H322 55.2 . .
C321 C322 K2 90.66(13) . .
C321 C322 H322 119.8 . .
C323 C322 K2 123.72(16) . .
C323 C322 C321 120.5(2) . .
C323 C322 H322 119.8 . .
C322 C323 H323 119.8 . .
C324 C323 C322 120.4(2) . .
C324 C323 H323 119.8 . .
C323 C324 H324 120.2 . .
C323 C324 C325 119.5(2) . .
C325 C324 H324 120.2 . .
C324 C325 H325 119.8 . .
C324 C325 C326 120.4(2) . .
C326 C325 H325 119.8 . .
C321 C326 H326 119.8 . .
C325 C326 C321 120.4(2) . .
C325 C326 H326 119.8 . .
C412 C411 C41 118.91(19) . .
C412 C411 C416 118.98(19) . .
C416 C411 C41 122.11(19) . .
C411 C412 H412 119.9 . .
C413 C412 C411 120.2(2) . .
C413 C412 H412 119.9 . .
C412 C413 H413 119.9 . .
C414 C413 C412 120.3(2) . .
C414 C413 H413 119.9 . .
C413 C414 H414 120.0 . .
C413 C414 C415 119.9(2) . .
C415 C414 H414 120.0 . .
C414 C415 H415 119.9 . .
C414 C415 C416 120.2(2) . .
C416 C415 H415 119.9 . .
C411 C416 H416 119.8 . .
C415 C416 C411 120.4(2) . .
C415 C416 H416 119.8 . .
C422 C421 C43 122.3(2) . .
C426 C421 C43 119.0(2) . .
C426 C421 C422 118.7(2) . .
C421 C422 H422 119.7 . .
C423 C422 C421 120.5(2) . .
C423 C422 H422 119.7 . .
C422 C423 H423 120.0 . .
C424 C423 C422 119.9(3) . .
C424 C423 H423 120.0 . .
C423 C424 H424 119.9 . .
C425 C424 C423 120.1(3) . .
C425 C424 H424 119.9 . .
C424 C425 H425 119.8 . .
C424 C425 C426 120.3(3) . .
C426 C425 H425 119.8 . .
C421 C426 C425 120.4(3) . .
C421 C426 H426 119.8 . .
C425 C426 H426 119.8 . .
K3 Dy2 K3 62.183(13) 2_656 .
O11 Dy2 K3 144.86(4) . .
O11 Dy2 K3 86.64(4) . 2_656
O11 Dy2 K3 86.64(4) 2_656 .
O11 Dy2 K3 144.85(4) 2_656 2_656
O11 Dy2 O11 127.38(7) . 2_656
O11 Dy2 O13 74.96(5) . 2_656
O11 Dy2 O13 147.72(5) . .
O11 Dy2 O13 147.72(5) 2_656 2_656
O11 Dy2 O13 74.95(5) 2_656 .
O11 Dy2 O14 78.56(5) 2_656 2_656
O11 Dy2 O14 128.47(5) 2_656 .
O11 Dy2 O14 128.47(5) . 2_656
O11 Dy2 O14 78.56(5) . .
O12 Dy2 K3 128.54(4) . 2_656
O12 Dy2 K3 114.64(4) 2_656 2_656
O12 Dy2 K3 114.64(4) . .
O12 Dy2 K3 128.54(4) 2_656 .
O12 Dy2 O11 71.21(5) 2_656 2_656
O12 Dy2 O11 77.52(5) 2_656 .
O12 Dy2 O11 77.52(5) . 2_656
O12 Dy2 O11 71.21(5) . .
O12 Dy2 O12 105.22(7) . 2_656
O12 Dy2 O13 91.48(5) . 2_656
O12 Dy2 O13 140.98(5) 2_656 2_656
O12 Dy2 O13 140.98(5) . .
O12 Dy2 O13 91.48(5) 2_656 .
O12 Dy2 O14 149.01(5) 2_656 2_656
O12 Dy2 O14 149.00(5) . .
O12 Dy2 O14 73.94(5) . 2_656
O12 Dy2 O14 73.93(5) 2_656 .
O13 Dy2 K3 37.25(4) 2_656 2_656
O13 Dy2 K3 37.25(4) . .
O13 Dy2 K3 70.36(4) . 2_656
O13 Dy2 K3 70.36(4) 2_656 .
O13 Dy2 O13 97.25(8) 2_656 .
O13 Dy2 O14 69.22(5) 2_656 2_656
O13 Dy2 O14 69.22(5) . .
O13 Dy2 O14 73.91(5) 2_656 .
O13 Dy2 O14 73.91(5) . 2_656
O14 Dy2 K3 40.72(3) 2_656 .
O14 Dy2 K3 86.52(4) 2_656 2_656
O14 Dy2 K3 40.72(3) . 2_656
O14 Dy2 K3 86.52(4) . .
O14 Dy2 O14 122.89(7) 2_656 .
K3 Dy3 K3 61.941(13) . 2_656
O15 Dy3 K3 87.07(4) . 2_656
O15 Dy3 K3 87.08(4) 2_656 .
O15 Dy3 K3 40.08(3) . .
O15 Dy3 K3 40.08(3) 2_656 2_656
O15 Dy3 O15 123.16(7) 2_656 .
O16 Dy3 K3 36.99(4) 2_656 .
O16 Dy3 K3 67.38(4) . .
O16 Dy3 K3 36.99(4) . 2_656
O16 Dy3 K3 67.38(4) 2_656 2_656
O16 Dy3 O15 68.02(5) . .
O16 Dy3 O15 68.02(5) 2_656 2_656
O16 Dy3 O15 73.59(5) 2_656 .
O16 Dy3 O15 73.59(5) . 2_656
O16 Dy3 O16 92.73(8) . 2_656
O16 Dy3 O17 76.05(6) 2_656 2_656
O16 Dy3 O17 141.62(5) 2_656 .
O16 Dy3 O17 76.04(6) . .
O16 Dy3 O17 141.62(5) . 2_656
O17 Dy3 K3 142.24(4) . .
O17 Dy3 K3 83.32(4) 2_656 .
O17 Dy3 K3 83.32(4) . 2_656
O17 Dy3 K3 142.24(4) 2_656 2_656
O17 Dy3 O15 131.05(5) . .
O17 Dy3 O15 73.60(5) 2_656 .
O17 Dy3 O15 73.60(5) . 2_656
O17 Dy3 O15 131.05(5) 2_656 2_656
O17 Dy3 O17 133.69(8) . 2_656
O18 Dy3 K3 117.72(4) 2_656 2_656
O18 Dy3 K3 128.23(4) 2_656 .
O18 Dy3 K3 117.72(4) . .
O18 Dy3 K3 128.23(4) . 2_656
O18 Dy3 O15 144.62(5) 2_656 .
O18 Dy3 O15 77.66(5) 2_656 2_656
O18 Dy3 O15 77.66(5) . .
O18 Dy3 O15 144.62(5) . 2_656
O18 Dy3 O16 92.22(5) 2_656 2_656
O18 Dy3 O16 146.46(5) . 2_656
O18 Dy3 O16 92.22(5) . .
O18 Dy3 O16 146.46(5) 2_656 .
O18 Dy3 O17 79.60(5) 2_656 .
O18 Dy3 O17 79.60(5) . 2_656
O18 Dy3 O17 71.54(5) 2_656 2_656
O18 Dy3 O17 71.54(5) . .
O18 Dy3 O18 101.60(7) . 2_656
Dy2 K3 Dy3 117.938(11) . .
Dy2 K3 K3 58.908(6) . 2_656
Dy3 K3 K3 59.030(6) . 2_656
O13 K3 Dy2 32.56(3) . .
O13 K3 Dy3 115.23(4) . .
O13 K3 K3 66.12(4) . 2_656
O13 K3 O14 63.73(4) . 2_656
O13 K3 O15 108.73(5) . .
O13 K3 O16 129.77(5) . 2_656
O13 K3 C61 19.10(4) . .
O13 K3 C63 81.66(5) . 2_656
O13 K3 C726 157.15(5) . 2_656
O14 K3 Dy2 34.51(3) 2_656 .
O14 K3 Dy3 129.80(3) 2_656 .
O14 K3 K3 79.68(3) 2_656 2_656
O14 K3 C61 82.81(5) 2_656 .
O14 K3 C63 18.96(4) 2_656 2_656
O14 K3 C726 93.60(5) 2_656 2_656
O15 K3 Dy2 131.13(3) . .
O15 K3 Dy3 34.31(3) . .
O15 K3 K3 80.66(3) . 2_656
O15 K3 O14 160.30(5) . 2_656
O15 K3 C61 91.00(5) . .
O15 K3 C63 152.50(5) . 2_656
O15 K3 C726 91.75(5) . 2_656
O16 K3 Dy2 112.92(4) 2_656 .
O16 K3 Dy3 32.01(3) 2_656 .
O16 K3 K3 63.64(4) 2_656 2_656
O16 K3 O14 106.19(5) 2_656 2_656
O16 K3 O15 63.45(4) 2_656 .
O16 K3 C61 128.22(5) 2_656 .
O16 K3 C63 90.11(5) 2_656 2_656
O16 K3 C726 50.87(5) 2_656 2_656
O19 K3 Dy2 114.78(5) . .
O19 K3 Dy3 127.28(5) . .
O19 K3 K3 173.68(5) . 2_656
O19 K3 O13 108.58(7) . .
O19 K3 O14 94.95(6) . 2_656
O19 K3 O15 104.75(6) . .
O19 K3 O16 121.53(7) . 2_656
O19 K3 C61 107.79(7) . .
O19 K3 C63 95.30(6) . 2_656
O19 K3 C726 74.45(7) . 2_656
C61 K3 Dy2 51.03(3) . .
C61 K3 Dy3 104.52(3) . .
C61 K3 K3 68.44(4) . 2_656
C61 K3 C63 100.72(5) . 2_656
C63 K3 Dy2 50.34(3) 2_656 .
C63 K3 Dy3 118.20(4) 2_656 .
C63 K3 K3 80.71(4) 2_656 2_656
C726 K3 Dy2 124.97(4) 2_656 .
C726 K3 Dy3 76.23(4) 2_656 .
C726 K3 K3 109.00(4) 2_656 2_656
C726 K3 C61 175.88(6) 2_656 .
C726 K3 C63 75.50(5) 2_656 2_656
C51 O11 Dy2 135.53(14) . .
C53 O12 Dy2 137.15(13) . .
Dy2 O13 K3 110.19(6) . .
C61 O13 Dy2 128.61(13) . .
C61 O13 K3 118.17(12) . .
Dy2 O14 K3 104.77(5) . 2_656
C63 O14 Dy2 123.69(13) . .
C63 O14 K3 115.96(12) . 2_656
Dy3 O15 K3 105.61(5) . .
C71 O15 Dy3 118.19(12) . .
C71 O15 K3 122.58(12) . .
Dy3 O16 K3 111.00(6) . 2_656
C73 O16 Dy3 123.36(13) . .
C73 O16 K3 125.31(12) . 2_656
C81 O17 Dy3 134.23(15) . .
C83 O18 Dy3 132.91(14) . .
C95 O19 K3 168.3(2) . .
O11 C51 C52 124.49(19) . .
O11 C51 C511 115.74(19) . .
C52 C51 C511 119.74(19) . .
C51 C52 H52 118.4 . .
C53 C52 C51 123.2(2) . .
C53 C52 H52 118.4 . .
O12 C53 C52 123.4(2) . .
O12 C53 C521 115.55(19) . .
C52 C53 C521 121.03(19) . .
O13 C61 K3 42.73(10) . .
O13 C61 C62 123.85(19) . .
O13 C61 C611 115.70(18) . .
C62 C61 K3 139.34(14) . .
C62 C61 C611 120.45(18) . .
C611 C61 K3 86.48(12) . .
C61 C62 H62 118.5 . .
C61 C62 C63 122.91(19) . .
C63 C62 H62 118.5 . .
O14 C63 K3 45.07(10) . 2_656
O14 C63 C62 123.59(19) . .
O14 C63 C621 116.4(2) . .
C62 C63 K3 111.56(13) . 2_656
C62 C63 C621 120.03(19) . .
C621 C63 K3 108.90(14) . 2_656
O15 C71 C72 123.08(19) . .
O15 C71 C711 115.75(19) . .
C72 C71 C711 121.17(18) . .
C71 C72 H72 119.0 . .
C73 C72 C71 122.05(19) . .
C73 C72 H72 119.0 . .
O16 C73 C72 123.37(19) . .
O16 C73 C721 114.85(18) . .
C72 C73 C721 121.78(19) . .
O17 C81 C82 124.0(2) . .
O17 C81 C811 116.4(2) . .
C82 C81 C811 119.58(19) . .
C81 C82 H82 118.4 . .
C83 C82 C81 123.1(2) . .
C83 C82 H82 118.4 . .
O18 C83 C82 125.0(2) . .
O18 C83 C821 115.9(2) . .
C82 C83 C821 119.1(2) . .
O19 C95 C96 121.9(3) . .
O19 C95 C97 120.8(3) . .
C97 C95 C96 117.3(2) . .
C95 C96 H96A 109.5 . .
C95 C96 H96B 109.5 . .
C95 C96 H96C 109.5 . .
H96A C96 H96B 109.5 . .
H96A C96 H96C 109.5 . .
H96B C96 H96C 109.5 . .
C95 C97 H97A 109.5 . .
C95 C97 H97B 109.5 . .
C95 C97 H97C 109.5 . .
H97A C97 H97B 109.5 . .
H97A C97 H97C 109.5 . .
H97B C97 H97C 109.5 . .
C512 C511 C51 122.5(2) . .
C516 C511 C51 118.7(2) . .
C516 C511 C512 118.8(2) . .
C511 C512 H512 120.0 . .
C513 C512 C511 120.0(3) . .
C513 C512 H512 120.0 . .
C512 C513 H513 119.8 . .
C514 C513 C512 120.5(3) . .
C514 C513 H513 119.8 . .
C513 C514 H514 120.0 . .
C513 C514 C515 120.0(3) . .
C515 C514 H514 120.0 . .
C514 C515 H515 120.0 . .
C514 C515 C516 120.0(3) . .
C516 C515 H515 120.0 . .
C511 C516 H516 119.6 . .
C515 C516 C511 120.8(2) . .
C515 C516 H516 119.6 . .
C522 C521 C53 118.0(2) . .
C522 C521 C526 118.6(2) . .
C526 C521 C53 123.3(2) . .
C521 C522 H522 119.8 . .
C523 C522 C521 120.5(2) . .
C523 C522 H522 119.8 . .
C522 C523 H523 119.9 . .
C522 C523 C524 120.3(3) . .
C524 C523 H523 119.9 . .
C523 C524 H524 120.0 . .
C525 C524 C523 119.9(3) . .
C525 C524 H524 120.0 . .
C524 C525 H525 120.0 . .
C524 C525 C526 120.0(2) . .
C526 C525 H525 120.0 . .
C521 C526 H526 119.7 . .
C525 C526 C521 120.7(2) . .
C525 C526 H526 119.7 . .
C612 C611 C61 122.3(2) . .
C612 C611 C616 119.1(2) . .
C616 C611 C61 118.60(19) . .
C611 C612 H612 119.9 . .
C613 C612 C611 120.2(2) . .
C613 C612 H612 119.9 . .
C612 C613 H613 119.7 . .
C614 C613 C612 120.7(2) . .
C614 C613 H613 119.7 . .
C613 C614 H614 120.2 . .
C613 C614 C615 119.6(2) . .
C615 C614 H614 120.2 . .
C614 C615 H615 119.8 . .
C614 C615 C616 120.4(2) . .
C616 C615 H615 119.8 . .
C611 C616 H616 120.0 . .
C615 C616 C611 120.0(2) . .
C615 C616 H616 120.0 . .
C622 C621 C63 119.1(2) . .
C622 C621 C626 118.5(2) . .
C626 C621 C63 122.3(2) . .
C621 C622 H622 119.7 . .
C621 C622 C623 120.6(3) . .
C623 C622 H622 119.7 . .
C622 C623 H623 119.8 . .
C624 C623 C622 120.4(4) . .
C624 C623 H623 119.8 . .
C623 C624 H624 120.0 . .
C625 C624 C623 119.9(3) . .
C625 C624 H624 120.0 . .
C624 C625 H625 119.8 . .
C624 C625 C626 120.5(3) . .
C626 C625 H625 119.8 . .
C621 C626 H626 120.0 . .
C625 C626 C621 120.1(3) . .
C625 C626 H626 120.0 . .
C712 C711 C71 123.0(2) . .
C712 C711 C716 118.5(2) . .
C716 C711 C71 118.21(19) . .
C711 C712 H712 119.8 . .
C713 C712 C711 120.4(2) . .
C713 C712 H712 119.8 . .
C712 C713 H713 119.6 . .
C714 C713 C712 120.8(2) . .
C714 C713 H713 119.6 . .
C713 C714 H714 120.3 . .
C713 C714 C715 119.4(2) . .
C715 C714 H714 120.3 . .
C714 C715 H715 120.0 . .
C714 C715 C716 120.0(2) . .
C716 C715 H715 120.0 . .
C711 C716 H716 119.6 . .
C715 C716 C711 120.8(2) . .
C715 C716 H716 119.6 . .
C722 C721 C73 123.8(2) . .
C722 C721 C726 118.8(2) . .
C726 C721 C73 117.34(19) . .
C721 C722 H722 119.9 . .
C723 C722 C721 120.1(2) . .
C723 C722 H722 119.9 . .
C722 C723 H723 119.8 . .
C724 C723 C722 120.5(2) . .
C724 C723 H723 119.8 . .
C723 C724 H724 120.1 . .
C723 C724 C725 119.8(2) . .
C725 C724 H724 120.1 . .
C724 C725 H725 120.1 . .
C726 C725 C724 119.9(2) . .
C726 C725 H725 120.1 . .
K3 C726 H726 52.6 2_656 .
C721 C726 K3 94.35(13) . 2_656
C721 C726 H726 119.6 . .
C725 C726 K3 121.55(17) . 2_656
C725 C726 C721 120.9(2) . .
C725 C726 H726 119.6 . .
C812 C811 C81 123.6(2) . .
C816 C811 C81 118.4(2) . .
C816 C811 C812 118.0(2) . .
C811 C812 H812 119.6 . .
C811 C812 C813 120.7(3) . .
C813 C812 H812 119.6 . .
C812 C813 H813 119.7 . .
C814 C813 C812 120.7(3) . .
C814 C813 H813 119.7 . .
C813 C814 H814 120.4 . .
C813 C814 C815 119.2(3) . .
C815 C814 H814 120.4 . .
C814 C815 H815 119.7 . .
C814 C815 C816 120.5(3) . .
C816 C815 H815 119.7 . .
C811 C816 C815 120.9(3) . .
C811 C816 H816 119.6 . .
C815 C816 H816 119.6 . .
C822 C821 C83 119.4(2) . .
C822 C821 C826 118.5(2) . .
C826 C821 C83 122.1(2) . .
C821 C822 H822 119.6 . .
C821 C822 C823 120.7(3) . .
C823 C822 H822 119.6 . .
C822 C823 H823 120.1 . .
C824 C823 C822 119.7(3) . .
C824 C823 H823 120.1 . .
C823 C824 H824 119.9 . .
C825 C824 C823 120.1(3) . .
C825 C824 H824 119.9 . .
C824 C825 H825 119.8 . .
C824 C825 C826 120.4(3) . .
C826 C825 H825 119.8 . .
C821 C826 H826 119.7 . .
C825 C826 C821 120.6(3) . .
C825 C826 H826 119.7 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Dy1 K1 4.1354(3) .
Dy1 K2 4.0411(3) .
Dy1 O1 2.3010(14) .
Dy1 O2 2.3284(14) .
Dy1 O3 2.3277(15) .
Dy1 O4 2.3644(14) .
Dy1 O5 2.4110(14) .
Dy1 O6 2.3276(14) .
Dy1 O7 2.3620(14) .
Dy1 O8 2.4136(14) .
K1 K2 4.2267(9) .
K1 O5 2.7487(14) .
K1 O5 2.7486(14) 2_656
K1 O7 2.6696(15) .
K1 O7 2.6697(15) 2_656
K1 O10 2.564(3) .
K1 C31 3.521(2) 2_656
K1 C31 3.521(2) .
K1 C41 3.515(2) 2_656
K1 C41 3.515(2) .
K2 O6 2.6113(15) 2_656
K2 O6 2.6114(15) .
K2 O8 2.7834(15) 2_656
K2 O8 2.7835(15) .
K2 O9 2.520(2) .
K2 C33 3.493(2) .
K2 C33 3.494(2) 2_656
K2 C322 3.474(2) .
K2 C322 3.474(2) 2_656
O1 C11 1.267(2) .
O2 C13 1.260(3) .
O3 C23 1.273(3) .
O4 C21 1.262(3) .
O5 C31 1.269(2) .
O6 C33 1.285(2) .
O7 C41 1.274(2) .
O8 C43 1.269(2) .
O9 C91 1.203(4) .
O10 C93 1.200(4) .
C11 C12 1.402(3) .
C11 C111 1.505(3) .
C12 H12 0.9500 .
C12 C13 1.407(3) .
C13 C121 1.505(3) .
C21 C22 1.403(3) .
C21 C211 1.508(3) .
C22 H22 0.9500 .
C22 C23 1.397(3) .
C23 C221 1.505(3) .
C31 C32 1.413(3) .
C31 C311 1.498(3) .
C32 H32 0.9500 .
C32 C33 1.396(3) .
C33 C321 1.497(3) .
C41 C42 1.400(3) .
C41 C411 1.499(3) .
C42 H42 0.9500 .
C42 C43 1.407(3) .
C43 C421 1.501(3) .
C91 C92 1.491(3) .
C91 C92 1.491(3) 2_656
C92 H92A 0.9800 .
C92 H92B 0.9800 .
C92 H92C 0.9800 .
C93 C94 1.492(4) .
C93 C94 1.492(4) 2_656
C94 H94A 0.9800 .
C94 H94B 0.9800 .
C94 H94C 0.9800 .
C111 C112 1.390(3) .
C111 C116 1.393(3) .
C112 H112 0.9500 .
C112 C113 1.386(3) .
C113 H113 0.9500 .
C113 C114 1.382(4) .
C114 H114 0.9500 .
C114 C115 1.373(4) .
C115 H115 0.9500 .
C115 C116 1.387(3) .
C116 H116 0.9500 .
C121 C122 1.384(3) .
C121 C126 1.384(3) .
C122 H122 0.9500 .
C122 C123 1.394(4) .
C123 H123 0.9500 .
C123 C124 1.373(5) .
C124 H124 0.9500 .
C124 C125 1.364(4) .
C125 H125 0.9500 .
C125 C126 1.391(3) .
C126 H126 0.9500 .
C211 C212 1.386(3) .
C211 C216 1.385(3) .
C212 H212 0.9500 .
C212 C213 1.392(3) .
C213 H213 0.9500 .
C213 C214 1.379(4) .
C214 H214 0.9500 .
C214 C215 1.366(5) .
C215 H215 0.9500 .
C215 C216 1.393(4) .
C216 H216 0.9500 .
C221 C222 1.391(3) .
C221 C226 1.394(3) .
C222 H222 0.9500 .
C222 C223 1.389(3) .
C223 H223 0.9500 .
C223 C224 1.383(4) .
C224 H224 0.9500 .
C224 C225 1.377(4) .
C225 H225 0.9500 .
C225 C226 1.391(3) .
C226 H226 0.9500 .
C311 C312 1.394(3) .
C311 C316 1.392(3) .
C312 H312 0.9500 .
C312 C313 1.388(3) .
C313 H313 0.9500 .
C313 C314 1.377(4) .
C314 H314 0.9500 .
C314 C315 1.381(3) .
C315 H315 0.9500 .
C315 C316 1.389(3) .
C316 H316 0.9500 .
C321 C322 1.395(3) .
C321 C326 1.394(3) .
C322 H322 0.9500 .
C322 C323 1.386(3) .
C323 H323 0.9500 .
C323 C324 1.383(3) .
C324 H324 0.9500 .
C324 C325 1.384(3) .
C325 H325 0.9500 .
C325 C326 1.387(3) .
C326 H326 0.9500 .
C411 C412 1.393(3) .
C411 C416 1.396(3) .
C412 H412 0.9500 .
C412 C413 1.390(3) .
C413 H413 0.9500 .
C413 C414 1.381(4) .
C414 H414 0.9500 .
C414 C415 1.383(3) .
C415 H415 0.9500 .
C415 C416 1.383(3) .
C416 H416 0.9500 .
C421 C422 1.391(3) .
C421 C426 1.387(3) .
C422 H422 0.9500 .
C422 C423 1.390(3) .
C423 H423 0.9500 .
C423 C424 1.377(4) .
C424 H424 0.9500 .
C424 C425 1.368(5) .
C425 H425 0.9500 .
C425 C426 1.391(4) .
C426 H426 0.9500 .
Dy2 K3 4.1045(5) .
Dy2 K3 4.1044(5) 2_656
Dy2 O11 2.3370(14) 2_656
Dy2 O11 2.3369(15) .
Dy2 O12 2.3184(14) .
Dy2 O12 2.3184(14) 2_656
Dy2 O13 2.3537(14) .
Dy2 O13 2.3536(14) 2_656
Dy2 O14 2.4049(14) .
Dy2 O14 2.4049(14) 2_656
Dy3 K3 4.1189(5) .
Dy3 K3 4.1189(5) 2_656
Dy3 O15 2.4106(14) .
Dy3 O15 2.4106(14) 2_656
Dy3 O16 2.3387(14) 2_656
Dy3 O16 2.3387(14) .
Dy3 O17 2.3510(15) .
Dy3 O17 2.3511(15) 2_656
Dy3 O18 2.3233(14) .
Dy3 O18 2.3234(14) 2_656
K3 K3 4.2391(9) 2_656
K3 O13 2.6470(15) .
K3 O14 2.7690(15) 2_656
K3 O15 2.7535(15) .
K3 O16 2.6544(15) 2_656
K3 O19 2.554(2) .
K3 C61 3.439(2) .
K3 C63 3.516(2) 2_656
K3 C726 3.420(2) 2_656
O11 C51 1.258(2) .
O12 C53 1.269(2) .
O13 C61 1.276(2) .
O14 C63 1.271(2) .
O15 C71 1.270(2) .
O16 C73 1.277(2) .
O17 C81 1.262(3) .
O18 C83 1.273(3) .
O19 C95 1.205(3) .
C51 C52 1.407(3) .
C51 C511 1.503(3) .
C52 H52 0.9500 .
C52 C53 1.396(3) .
C53 C521 1.507(3) .
C61 C62 1.398(3) .
C61 C611 1.498(3) .
C62 H62 0.9500 .
C62 C63 1.406(3) .
C63 C621 1.500(3) .
C71 C72 1.413(3) .
C71 C711 1.495(3) .
C72 H72 0.9500 .
C72 C73 1.400(3) .
C73 C721 1.495(3) .
C81 C82 1.405(3) .
C81 C811 1.507(3) .
C82 H82 0.9500 .
C82 C83 1.393(3) .
C83 C821 1.506(3) .
C95 C96 1.489(4) .
C95 C97 1.488(4) .
C96 H96A 0.9800 .
C96 H96B 0.9800 .
C96 H96C 0.9800 .
C97 H97A 0.9800 .
C97 H97B 0.9800 .
C97 H97C 0.9800 .
C511 C512 1.393(3) .
C511 C516 1.392(3) .
C512 H512 0.9500 .
C512 C513 1.391(4) .
C513 H513 0.9500 .
C513 C514 1.377(4) .
C514 H514 0.9500 .
C514 C515 1.379(4) .
C515 H515 0.9500 .
C515 C516 1.385(3) .
C516 H516 0.9500 .
C521 C522 1.388(3) .
C521 C526 1.395(3) .
C522 H522 0.9500 .
C522 C523 1.383(4) .
C523 H523 0.9500 .
C523 C524 1.387(4) .
C524 H524 0.9500 .
C524 C525 1.372(4) .
C525 H525 0.9500 .
C525 C526 1.388(3) .
C526 H526 0.9500 .
C611 C612 1.395(3) .
C611 C616 1.396(3) .
C612 H612 0.9500 .
C612 C613 1.383(3) .
C613 H613 0.9500 .
C613 C614 1.381(4) .
C614 H614 0.9500 .
C614 C615 1.387(4) .
C615 H615 0.9500 .
C615 C616 1.389(3) .
C616 H616 0.9500 .
C621 C622 1.377(4) .
C621 C626 1.392(4) .
C622 H622 0.9500 .
C622 C623 1.385(4) .
C623 H623 0.9500 .
C623 C624 1.367(6) .
C624 H624 0.9500 .
C624 C625 1.359(6) .
C625 H625 0.9500 .
C625 C626 1.389(4) .
C626 H626 0.9500 .
C711 C712 1.391(3) .
C711 C716 1.393(3) .
C712 H712 0.9500 .
C712 C713 1.382(3) .
C713 H713 0.9500 .
C713 C714 1.377(4) .
C714 H714 0.9500 .
C714 C715 1.386(4) .
C715 H715 0.9500 .
C715 C716 1.387(4) .
C716 H716 0.9500 .
C721 C722 1.389(3) .
C721 C726 1.396(3) .
C722 H722 0.9500 .
C722 C723 1.389(3) .
C723 H723 0.9500 .
C723 C724 1.380(4) .
C724 H724 0.9500 .
C724 C725 1.386(4) .
C725 H725 0.9500 .
C725 C726 1.379(3) .
C726 H726 0.9500 .
C811 C812 1.386(3) .
C811 C816 1.385(4) .
C812 H812 0.9500 .
C812 C813 1.389(4) .
C813 H813 0.9500 .
C813 C814 1.367(5) .
C814 H814 0.9500 .
C814 C815 1.374(5) .
C815 H815 0.9500 .
C815 C816 1.386(4) .
C816 H816 0.9500 .
C821 C822 1.389(4) .
C821 C826 1.398(3) .
C822 H822 0.9500 .
C822 C823 1.394(3) .
C823 H823 0.9500 .
C823 C824 1.386(4) .
C824 H824 0.9500 .
C824 C825 1.373(4) .
C825 H825 0.9500 .
C825 C826 1.385(4) .
C826 H826 0.9500 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
Dy1 O1 C11 C12 17.0(3) . .
Dy1 O1 C11 C111 -164.16(14) . .
Dy1 O2 C13 C12 -19.0(3) . .
Dy1 O2 C13 C121 163.53(14) . .
Dy1 O3 C23 C22 28.3(3) . .
Dy1 O3 C23 C221 -152.62(14) . .
Dy1 O4 C21 C22 -17.3(3) . .
Dy1 O4 C21 C211 163.37(14) . .
Dy1 O5 C31 K1 -133.41(16) . .
Dy1 O5 C31 C32 -46.8(2) . .
Dy1 O5 C31 C311 133.61(14) . .
Dy1 O6 C33 K2 169.3(2) . .
Dy1 O6 C33 C32 38.4(3) . .
Dy1 O6 C33 C321 -140.35(14) . .
Dy1 O7 C41 K1 165.0(2) . .
Dy1 O7 C41 C42 32.6(3) . .
Dy1 O7 C41 C411 -147.54(14) . .
Dy1 O8 C43 C42 -44.3(3) . .
Dy1 O8 C43 C421 137.90(15) . .
K1 O5 C31 C32 86.6(2) . .
K1 O5 C31 C311 -92.98(18) . .
K1 O7 C41 C42 -132.44(18) . .
K1 O7 C41 C411 47.4(2) . .
K1 C31 C32 C33 49.3(2) . .
K1 C31 C311 C312 -35.0(2) . .
K1 C31 C311 C316 149.57(17) . .
K1 C41 C42 C43 -41.4(3) . .
K1 C41 C411 C412 55.03(19) . .
K1 C41 C411 C416 -123.97(19) . .
K2 O6 C33 C32 -130.84(17) . .
K2 O6 C33 C321 50.4(2) . .
K2 O8 C43 C42 85.0(2) . .
K2 O8 C43 C421 -92.77(19) . .
K2 C33 C321 C322 47.62(18) . .
K2 C33 C321 C326 -131.93(19) . .
K2 C322 C323 C324 -114.1(2) . .
O1 C11 C12 C13 3.8(3) . .
O1 C11 C111 C112 -2.6(3) . .
O1 C11 C111 C116 175.6(2) . .
O2 C13 C121 C122 -167.0(2) . .
O2 C13 C121 C126 11.3(3) . .
O3 C23 C221 C222 155.3(2) . .
O3 C23 C221 C226 -22.0(3) . .
O4 C21 C22 C23 -4.6(3) . .
O4 C21 C211 C212 7.8(3) . .
O4 C21 C211 C216 -171.3(2) . .
O5 C31 C32 C33 1.6(3) . .
O5 C31 C311 C312 12.5(3) . .
O5 C31 C311 C316 -162.94(19) . .
O6 C33 C321 C322 19.0(3) . .
O6 C33 C321 C326 -160.52(19) . .
O7 C41 C42 C43 9.1(3) . .
O7 C41 C411 C412 26.7(3) . .
O7 C41 C411 C416 -152.3(2) . .
O8 C43 C421 C422 -159.8(2) . .
O8 C43 C421 C426 19.1(3) . .
C11 C12 C13 O2 -2.6(4) . .
C11 C12 C13 C121 174.8(2) . .
C11 C111 C112 C113 178.3(3) . .
C11 C111 C116 C115 -178.3(2) . .
C12 C11 C111 C112 176.3(2) . .
C12 C11 C111 C116 -5.5(3) . .
C12 C13 C121 C122 15.4(3) . .
C12 C13 C121 C126 -166.3(2) . .
C13 C121 C122 C123 179.3(3) . .
C13 C121 C126 C125 -179.9(2) . .
C21 C22 C23 O3 -0.7(3) . .
C21 C22 C23 C221 -179.72(19) . .
C21 C211 C212 C213 -179.7(2) . .
C21 C211 C216 C215 178.7(3) . .
C22 C21 C211 C212 -171.6(2) . .
C22 C21 C211 C216 9.4(3) . .
C22 C23 C221 C222 -25.6(3) . .
C22 C23 C221 C226 157.1(2) . .
C23 C221 C222 C223 -177.3(2) . .
C23 C221 C226 C225 178.1(2) . .
C31 C32 C33 K2 -42.5(3) . .
C31 C32 C33 O6 4.8(3) . .
C31 C32 C33 C321 -176.52(19) . .
C31 C311 C312 C313 -175.4(2) . .
C31 C311 C316 C315 174.8(2) . .
C32 C31 C311 C312 -167.1(2) . .
C32 C31 C311 C316 17.4(3) . .
C32 C33 C321 C322 -159.8(2) . .
C32 C33 C321 C326 20.7(3) . .
C33 C321 C322 K2 -47.95(18) . .
C33 C321 C322 C323 -178.6(2) . .
C33 C321 C326 C325 178.2(2) . .
C41 C42 C43 O8 -1.4(3) . .
C41 C42 C43 C421 176.32(19) . .
C41 C411 C412 C413 -179.2(2) . .
C41 C411 C416 C415 177.8(2) . .
C42 C41 C411 C412 -153.5(2) . .
C42 C41 C411 C416 27.5(3) . .
C42 C43 C421 C422 22.3(3) . .
C42 C43 C421 C426 -158.8(2) . .
C43 C421 C422 C423 -179.8(2) . .
C43 C421 C426 C425 178.3(3) . .
C111 C11 C12 C13 -174.9(2) . .
C111 C112 C113 C114 0.1(5) . .
C112 C111 C116 C115 0.0(4) . .
C112 C113 C114 C115 -0.2(5) . .
C113 C114 C115 C116 0.2(5) . .
C114 C115 C116 C111 -0.1(4) . .
C116 C111 C112 C113 0.0(4) . .
C121 C122 C123 C124 0.7(6) . .
C122 C121 C126 C125 -1.5(4) . .
C122 C123 C124 C125 -1.9(6) . .
C123 C124 C125 C126 1.4(5) . .
C124 C125 C126 C121 0.3(5) . .
C126 C121 C122 C123 1.0(4) . .
C211 C21 C22 C23 174.7(2) . .
C211 C212 C213 C214 0.8(4) . .
C212 C211 C216 C215 -0.3(4) . .
C212 C213 C214 C215 0.1(5) . .
C213 C214 C215 C216 -1.0(5) . .
C214 C215 C216 C211 1.2(5) . .
C216 C211 C212 C213 -0.6(4) . .
C221 C222 C223 C224 -0.4(4) . .
C222 C221 C226 C225 0.7(3) . .
C222 C223 C224 C225 -0.1(4) . .
C223 C224 C225 C226 0.8(4) . .
C224 C225 C226 C221 -1.1(4) . .
C226 C221 C222 C223 0.0(3) . .
C311 C31 C32 C33 -178.78(19) . .
C311 C312 C313 C314 0.5(4) . .
C312 C311 C316 C315 -0.7(3) . .
C312 C313 C314 C315 -0.9(4) . .
C313 C314 C315 C316 0.5(4) . .
C314 C315 C316 C311 0.3(4) . .
C316 C311 C312 C313 0.3(4) . .
C321 C322 C323 C324 0.0(4) . .
C322 C321 C326 C325 -1.3(3) . .
C322 C323 C324 C325 -0.8(4) . .
C323 C324 C325 C326 0.4(4) . .
C324 C325 C326 C321 0.6(3) . .
C326 C321 C322 K2 131.61(18) . .
C326 C321 C322 C323 1.0(3) . .
C411 C41 C42 C43 -170.73(19) . .
C411 C412 C413 C414 1.3(4) . .
C412 C411 C416 C415 -1.2(3) . .
C412 C413 C414 C415 -1.1(4) . .
C413 C414 C415 C416 -0.2(4) . .
C414 C415 C416 C411 1.3(3) . .
C416 C411 C412 C413 -0.1(3) . .
C421 C422 C423 C424 0.9(4) . .
C422 C421 C426 C425 -2.7(4) . .
C422 C423 C424 C425 -1.6(5) . .
C423 C424 C425 C426 0.1(5) . .
C424 C425 C426 C421 2.0(5) . .
C426 C421 C422 C423 1.3(4) . .
Dy2 O11 C51 C52 18.7(3) . .
Dy2 O11 C51 C511 -163.46(14) . .
Dy2 O12 C53 C52 -16.2(3) . .
Dy2 O12 C53 C521 164.17(14) . .
Dy2 O13 C61 K3 -158.2(2) . .
Dy2 O13 C61 C62 -29.9(3) . .
Dy2 O13 C61 C611 150.17(14) . .
Dy2 O14 C63 K3 131.71(17) . 2_656
Dy2 O14 C63 C62 44.0(3) . .
Dy2 O14 C63 C621 -137.37(15) . .
Dy3 O15 C71 C72 49.1(2) . .
Dy3 O15 C71 C711 -130.08(15) . .
Dy3 O16 C73 C72 -39.0(3) . .
Dy3 O16 C73 C721 140.03(14) . .
Dy3 O17 C81 C82 17.8(3) . .
Dy3 O17 C81 C811 -162.24(14) . .
Dy3 O18 C83 C82 -26.3(3) . .
Dy3 O18 C83 C821 155.49(14) . .
K3 O13 C61 C62 128.32(18) . .
K3 O13 C61 C611 -51.6(2) . .
K3 O14 C63 C62 -87.7(2) 2_656 .
K3 O14 C63 C621 90.92(19) 2_656 .
K3 O15 C71 C72 -85.7(2) . .
K3 O15 C71 C711 95.09(18) . .
K3 O16 C73 C72 133.85(17) 2_656 .
K3 O16 C73 C721 -47.2(2) 2_656 .
K3 O19 C95 C96 108.6(10) . .
K3 O19 C95 C97 -71.7(11) . .
K3 C61 C62 C63 46.4(3) . .
K3 C61 C611 C612 119.30(19) . .
K3 C61 C611 C616 -58.93(18) . .
K3 C63 C621 C622 34.3(3) 2_656 .
K3 C63 C621 C626 -147.9(2) 2_656 .
O11 C51 C52 C53 1.0(3) . .
O11 C51 C511 C512 160.7(2) . .
O11 C51 C511 C516 -17.7(3) . .
O12 C53 C521 C522 3.3(3) . .
O12 C53 C521 C526 -174.7(2) . .
O13 C61 C62 C63 -8.4(3) . .
O13 C61 C611 C612 151.5(2) . .
O13 C61 C611 C616 -26.7(3) . .
O14 C63 C621 C622 -14.2(3) . .
O14 C63 C621 C626 163.6(2) . .
O15 C71 C72 C73 -0.7(3) . .
O15 C71 C711 C712 158.82(19) . .
O15 C71 C711 C716 -15.6(3) . .
O16 C73 C721 C722 161.2(2) . .
O16 C73 C721 C726 -17.2(3) . .
O17 C81 C82 C83 5.8(3) . .
O17 C81 C811 C812 -173.4(2) . .
O17 C81 C811 C816 6.4(3) . .
O18 C83 C821 C822 20.6(3) . .
O18 C83 C821 C826 -157.0(2) . .
C51 C52 C53 O12 -2.5(3) . .
C51 C52 C53 C521 177.14(19) . .
C51 C511 C512 C513 -179.0(2) . .
C51 C511 C516 C515 179.5(2) . .
C52 C51 C511 C512 -21.3(3) . .
C52 C51 C511 C516 160.2(2) . .
C52 C53 C521 C522 -176.3(2) . .
C52 C53 C521 C526 5.6(3) . .
C53 C521 C522 C523 -177.5(3) . .
C53 C521 C526 C525 176.9(2) . .
C61 C62 C63 K3 -49.9(2) . 2_656
C61 C62 C63 O14 -0.4(3) . .
C61 C62 C63 C621 -179.00(19) . .
C61 C611 C612 C613 -177.26(19) . .
C61 C611 C616 C615 178.9(2) . .
C62 C61 C611 C612 -28.4(3) . .
C62 C61 C611 C616 153.3(2) . .
C62 C63 C621 C622 164.6(2) . .
C62 C63 C621 C626 -17.7(3) . .
C63 C621 C622 C623 179.7(3) . .
C63 C621 C626 C625 -179.3(3) . .
C71 C72 C73 O16 -6.8(3) . .
C71 C72 C73 C721 174.27(18) . .
C71 C711 C712 C713 -172.3(2) . .
C71 C711 C716 C715 172.9(2) . .
C72 C71 C711 C712 -20.4(3) . .
C72 C71 C711 C716 165.1(2) . .
C72 C73 C721 C722 -19.8(3) . .
C72 C73 C721 C726 161.8(2) . .
C73 C721 C722 C723 -177.0(2) . .
C73 C721 C726 K3 46.08(18) . 2_656
C73 C721 C726 C725 177.1(2) . .
C81 C82 C83 O18 -1.7(3) . .
C81 C82 C83 C821 176.53(19) . .
C81 C811 C812 C813 -178.6(3) . .
C81 C811 C816 C815 179.3(3) . .
C82 C81 C811 C812 6.6(3) . .
C82 C81 C811 C816 -173.6(2) . .
C82 C83 C821 C822 -157.8(2) . .
C82 C83 C821 C826 24.7(3) . .
C83 C821 C822 C823 -178.3(2) . .
C83 C821 C826 C825 177.1(2) . .
C511 C51 C52 C53 -176.77(19) . .
C511 C512 C513 C514 0.0(5) . .
C512 C511 C516 C515 1.1(4) . .
C512 C513 C514 C515 0.1(5) . .
C513 C514 C515 C516 0.4(4) . .
C514 C515 C516 C511 -1.0(4) . .
C516 C511 C512 C513 -0.6(4) . .
C521 C522 C523 C524 0.1(5) . .
C522 C521 C526 C525 -1.1(4) . .
C522 C523 C524 C525 -0.4(5) . .
C523 C524 C525 C526 -0.1(5) . .
C524 C525 C526 C521 0.8(4) . .
C526 C521 C522 C523 0.6(4) . .
C611 C61 C62 C63 171.53(19) . .
C611 C612 C613 C614 -1.5(3) . .
C612 C611 C616 C615 0.6(3) . .
C612 C613 C614 C615 0.5(4) . .
C613 C614 C615 C616 1.1(4) . .
C614 C615 C616 C611 -1.7(4) . .
C616 C611 C612 C613 1.0(3) . .
C621 C622 C623 C624 -0.6(7) . .
C622 C621 C626 C625 -1.5(4) . .
C622 C623 C624 C625 -0.9(7) . .
C623 C624 C625 C626 1.2(7) . .
C624 C625 C626 C621 0.0(5) . .
C626 C621 C622 C623 1.8(5) . .
C711 C71 C72 C73 178.48(18) . .
C711 C712 C713 C714 -0.3(4) . .
C712 C711 C716 C715 -1.8(4) . .
C712 C713 C714 C715 -1.8(4) . .
C713 C714 C715 C716 2.1(4) . .
C714 C715 C716 C711 -0.2(4) . .
C716 C711 C712 C713 2.1(3) . .
C721 C722 C723 C724 -0.2(4) . .
C722 C721 C726 K3 -132.45(17) . 2_656
C722 C721 C726 C725 -1.4(3) . .
C722 C723 C724 C725 -1.2(4) . .
C723 C724 C725 C726 1.3(4) . .
C724 C725 C726 K3 118.1(2) . 2_656
C724 C725 C726 C721 0.0(4) . .
C726 C721 C722 C723 1.5(3) . .
C811 C81 C82 C83 -174.17(19) . .
C811 C812 C813 C814 -0.8(5) . .
C812 C811 C816 C815 -0.9(4) . .
C812 C813 C814 C815 -0.7(5) . .
C813 C814 C815 C816 1.4(5) . .
C814 C815 C816 C811 -0.5(5) . .
C816 C811 C812 C813 1.6(4) . .
C821 C822 C823 C824 1.5(4) . .
C822 C821 C826 C825 -0.5(3) . .
C822 C823 C824 C825 -1.2(4) . .
C823 C824 C825 C826 0.0(4) . .
C824 C825 C826 C821 0.8(4) . .
C826 C821 C822 C823 -0.7(3) . .
