#------------------------------------------------------------------------------
#$Date: 2022-10-07 04:10:13 +0300 (Fri, 07 Oct 2022) $
#$Revision: 278455 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/06/16/7061683.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7061683
loop_
_publ_author_name
'Sulaiman, Adam A. A.'
'Ahmad, Saeed'
'Mujahid Hashimi, Saeed'
'Alqosaibi, Amany I.'
'Peedikakkal, Abdul Malik Puthan'
'Alhoshani, Ali'
'Alsaleh, Nasser B.'
'Isab, Anvarhusein A.'
_publ_section_title
;
 Novel dinuclear gold(i) complexes containing
 bis(diphenylphosphano)alkanes and
 (biphenyl-2-yl)(di-tert-butyl)phosphane: synthesis, structural
 characterization and anticancer activity
;
_journal_issue                   35
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              16821
_journal_page_last               16831
_journal_paper_doi               10.1039/D2NJ01680J
_journal_volume                  46
_journal_year                    2022
_chemical_formula_sum            'C67 H Au2 F12 P6'
_chemical_formula_weight         1613.43
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2016/6
_audit_update_record
;
2022-03-28 deposited with the CCDC.	2022-08-01 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 117.195(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   24.3842(11)
_cell_length_b                   11.8498(5)
_cell_length_c                   26.2952(16)
_cell_measurement_temperature    296(2)
_cell_volume                     6758.0(6)
_computing_structure_refinement  'SHELXL-2016/6 (Sheldrick, 2016)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.990
_diffrn_measured_fraction_theta_max 0.971
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0691
_diffrn_reflns_av_unetI/netI     0.0884
_diffrn_reflns_Laue_measured_fraction_full 0.990
_diffrn_reflns_Laue_measured_fraction_max 0.971
_diffrn_reflns_limit_h_max       30
_diffrn_reflns_limit_h_min       -36
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       39
_diffrn_reflns_limit_l_min       -35
_diffrn_reflns_number            31109
_diffrn_reflns_point_group_measured_fraction_full 0.990
_diffrn_reflns_point_group_measured_fraction_max 0.971
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         32.103
_diffrn_reflns_theta_min         2.892
_exptl_absorpt_coefficient_mu    4.549
_exptl_crystal_density_diffrn    1.586
_exptl_crystal_F_000             3036
_refine_diff_density_max         1.562
_refine_diff_density_min         -1.577
_refine_diff_density_rms         0.145
_refine_ls_extinction_coef       0.00017(4)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2016/6 (Sheldrick 2016)'
_refine_ls_goodness_of_fit_ref   1.023
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     400
_refine_ls_number_reflns         11489
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.023
_refine_ls_R_factor_all          0.0906
_refine_ls_R_factor_gt           0.0492
_refine_ls_shift/su_max          0.009
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0385P)²+15.3225P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1035
_refine_ls_wR_factor_ref         0.1179
_reflns_Friedel_coverage         0.000
_reflns_number_gt                7876
_reflns_number_total             11489
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d2nj01680j2.cif
_cod_data_source_block           AD2
_cod_depositor_comments
'Adding full bibliography for 7061681--7061683.cif.'
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               7061683
_shelx_shelxl_version_number     2016/6
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au1 Au 0.64860(2) 0.15428(2) 0.32142(2) 0.03134(7) Uani 1 1 d . . . . .
P2 P 0.61593(5) 0.29472(9) 0.25308(5) 0.0259(2) Uani 1 1 d . . . . .
P1 P 0.67805(5) 0.00152(9) 0.38442(5) 0.0276(2) Uani 1 1 d . . . . .
P3 P 0.54540(9) 0.69581(14) 0.11035(8) 0.0594(4) Uani 1 1 d . . . . .
C1 C 0.500000 0.3034(5) 0.250000 0.0306(13) Uani 1 2 d S T P . .
H1A H 0.483972 0.255303 0.216441 0.037 Uiso 0.5 1 calc R U P . .
H1B H 0.516028 0.255305 0.283559 0.037 Uiso 0.5 1 calc R U P . .
C21 C 0.6452(2) 0.2418(3) 0.43363(19) 0.0296(9) Uani 1 1 d . . . . .
C9 C 0.67727(19) 0.3948(4) 0.26718(19) 0.0286(9) Uani 1 1 d . . . . .
C3 C 0.5880(2) 0.2451(4) 0.1801(2) 0.0319(9) Uani 1 1 d . . . . .
C26 C 0.6958(2) 0.2881(4) 0.4298(2) 0.0371(11) Uani 1 1 d . . . . .
H26 H 0.731245 0.245213 0.439911 0.045 Uiso 1 1 calc R U . . .
C20 C 0.6490(2) 0.1309(4) 0.4613(2) 0.0310(9) Uani 1 1 d . . . . .
C10 C 0.7375(2) 0.3556(5) 0.2914(2) 0.0414(12) Uani 1 1 d . . . . .
H10 H 0.745339 0.278884 0.298443 0.050 Uiso 1 1 calc R U . . .
C28 C 0.6202(3) -0.1116(4) 0.3431(2) 0.0470(13) Uani 1 1 d . . . . .
C15 C 0.6681(2) 0.0269(4) 0.4479(2) 0.0310(9) Uani 1 1 d . . . . .
C14 C 0.6667(2) 0.5092(4) 0.2577(2) 0.0437(12) Uani 1 1 d . . . . .
H14 H 0.626541 0.536666 0.241044 0.052 Uiso 1 1 calc R U . . .
C4 C 0.5687(3) 0.1343(4) 0.1657(2) 0.0423(12) Uani 1 1 d . . . . .
H4 H 0.571516 0.084026 0.193971 0.051 Uiso 1 1 calc R U . . .
C22 C 0.5930(2) 0.3077(4) 0.4173(2) 0.0435(12) Uani 1 1 d . . . . .
H22 H 0.558246 0.277750 0.418388 0.052 Uiso 1 1 calc R U . . .
C25 C 0.6933(3) 0.3985(4) 0.4109(2) 0.0478(13) Uani 1 1 d . . . . .
H25 H 0.726934 0.428744 0.407926 0.057 Uiso 1 1 calc R U . . .
C23 C 0.5920(3) 0.4180(5) 0.3995(3) 0.0562(16) Uani 1 1 d . . . . .
H23 H 0.556916 0.462025 0.389205 0.067 Uiso 1 1 calc R U . . .
C24 C 0.6423(3) 0.4624(4) 0.3969(3) 0.0587(17) Uani 1 1 d . . . . .
H24 H 0.641636 0.536849 0.385424 0.070 Uiso 1 1 calc R U . . .
C8 C 0.5830(2) 0.3194(5) 0.1374(2) 0.0425(12) Uani 1 1 d . . . . .
H8 H 0.595247 0.394163 0.146396 0.051 Uiso 1 1 calc R U . . .
C19 C 0.6327(3) 0.1323(4) 0.5060(2) 0.0413(12) Uani 1 1 d . . . . .
H19 H 0.619030 0.199629 0.514501 0.050 Uiso 1 1 calc R U . . .
C16 C 0.6725(3) -0.0664(4) 0.4829(2) 0.0440(12) Uani 1 1 d . . . . .
H16 H 0.687155 -0.134377 0.476187 0.053 Uiso 1 1 calc R U . . .
C11 C 0.7862(2) 0.4299(6) 0.3052(3) 0.0584(17) Uani 1 1 d . . . . .
H11 H 0.826405 0.403069 0.320323 0.070 Uiso 1 1 calc R U . . .
C7 C 0.5595(3) 0.2824(6) 0.0811(3) 0.0561(15) Uani 1 1 d . . . . .
H7 H 0.556139 0.332184 0.052410 0.067 Uiso 1 1 calc R U . . .
C33 C 0.7994(3) 0.0673(5) 0.4338(3) 0.0619(17) Uani 1 1 d . . . . .
H33A H 0.841851 0.051695 0.444158 0.093 Uiso 1 1 calc R U . . .
H33B H 0.795623 0.088921 0.467217 0.093 Uiso 1 1 calc R U . . .
H33C H 0.785056 0.127687 0.406408 0.093 Uiso 1 1 calc R U . . .
C12 C 0.7743(3) 0.5442(6) 0.2963(3) 0.0639(18) Uani 1 1 d . . . . .
H12 H 0.806955 0.594476 0.306577 0.077 Uiso 1 1 calc R U . . .
C30 C 0.6157(4) -0.1214(5) 0.2830(3) 0.071(2) Uani 1 1 d . . . . .
H30A H 0.585635 -0.177584 0.261476 0.107 Uiso 1 1 calc R U . . .
H30B H 0.655134 -0.142836 0.286122 0.107 Uiso 1 1 calc R U . . .
H30C H 0.603642 -0.050000 0.263810 0.107 Uiso 1 1 calc R U . . .
C5 C 0.5453(3) 0.0981(5) 0.1094(3) 0.0526(15) Uani 1 1 d . . . . .
H5 H 0.532197 0.023891 0.099887 0.063 Uiso 1 1 calc R U . . .
C18 C 0.6361(3) 0.0389(5) 0.5374(3) 0.0527(14) Uani 1 1 d . . . . .
H18 H 0.624748 0.042979 0.566648 0.063 Uiso 1 1 calc R U . . .
C6 C 0.5414(3) 0.1718(6) 0.0680(3) 0.0562(16) Uani 1 1 d . . . . .
H6 H 0.526407 0.146827 0.030491 0.067 Uiso 1 1 calc R U . . .
C31 C 0.7678(3) -0.0767(8) 0.3559(3) 0.085(2) Uani 1 1 d . . . . .
H31A H 0.751220 -0.020128 0.326549 0.127 Uiso 1 1 calc R U . . .
H31B H 0.746103 -0.146404 0.341651 0.127 Uiso 1 1 calc R U . . .
H31C H 0.810755 -0.087484 0.366670 0.127 Uiso 1 1 calc R U . . .
C34 C 0.7855(3) -0.1316(6) 0.4536(3) 0.075(2) Uani 1 1 d . . . . .
H34A H 0.762286 -0.199752 0.438854 0.112 Uiso 1 1 calc R U . . .
H34B H 0.781711 -0.107440 0.486673 0.112 Uiso 1 1 calc R U . . .
H34C H 0.828122 -0.145497 0.463977 0.112 Uiso 1 1 calc R U . . .
C29 C 0.5586(3) -0.0677(6) 0.3370(3) 0.075(2) Uani 1 1 d . . . . .
H29A H 0.525988 -0.116950 0.312300 0.113 Uiso 1 1 calc R U . . .
H29B H 0.551351 0.006855 0.321051 0.113 Uiso 1 1 calc R U . . .
H29C H 0.559609 -0.065570 0.373975 0.113 Uiso 1 1 calc R U . . .
C2 C 0.55200(19) 0.3765(4) 0.2509(2) 0.0281(9) Uani 1 1 d . . . . .
H2A H 0.567069 0.425646 0.283993 0.034 Uiso 1 1 calc R U . . .
H2B H 0.535689 0.423828 0.217018 0.034 Uiso 1 1 calc R U . . .
C32 C 0.7605(2) -0.0389(4) 0.4074(2) 0.0401(11) Uani 1 1 d . . . . .
C17 C 0.6563(3) -0.0612(5) 0.5259(3) 0.0581(16) Uani 1 1 d . . . . .
H17 H 0.658903 -0.125204 0.547431 0.070 Uiso 1 1 calc R U . . .
C13 C 0.7160(3) 0.5836(5) 0.2729(3) 0.0621(17) Uani 1 1 d . . . . .
H13 H 0.708664 0.660631 0.266913 0.074 Uiso 1 1 calc R U . . .
C27 C 0.6323(4) -0.2303(5) 0.3696(3) 0.085(3) Uani 1 1 d . . . . .
H27A H 0.626252 -0.229794 0.403226 0.127 Uiso 1 1 calc R U . . .
H27B H 0.673955 -0.252211 0.379806 0.127 Uiso 1 1 calc R U . . .
H27C H 0.604310 -0.283025 0.342435 0.127 Uiso 1 1 calc R U . . .
F4 F 0.4768(3) 0.7129(9) 0.0740(3) 0.182(3) Uani 1 1 d . . . . .
F1 F 0.6153(3) 0.6798(8) 0.1461(4) 0.201(4) Uani 1 1 d . . . . .
F5 F 0.5599(4) 0.7445(10) 0.0659(4) 0.240(6) Uani 1 1 d . . . . .
F2 F 0.5293(4) 0.6448(9) 0.1559(4) 0.213(5) Uani 1 1 d . . . . .
F3 F 0.5420(6) 0.5826(7) 0.0902(7) 0.289(7) Uani 1 1 d . . . . .
F6 F 0.5536(5) 0.8019(7) 0.1401(5) 0.242(6) Uani 1 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
P2 Au1 P1 175.29(4) . . ?
C9 P2 C2 105.9(2) . . ?
C9 P2 C3 107.7(2) . . ?
C2 P2 C3 103.7(2) . . ?
C9 P2 Au1 110.75(14) . . ?
C2 P2 Au1 113.35(15) . . ?
C3 P2 Au1 114.74(16) . . ?
C15 P1 C32 108.6(2) . . ?
C15 P1 C28 105.5(2) . . ?
C32 P1 C28 114.4(2) . . ?
C15 P1 Au1 113.34(14) . . ?
C32 P1 Au1 111.29(17) . . ?
C28 P1 Au1 103.62(17) . . ?
F3 P3 F6 170.5(9) . . ?
F3 P3 F5 93.8(8) . . ?
F6 P3 F5 93.6(7) . . ?
F3 P3 F4 91.8(7) . . ?
F6 P3 F4 93.7(6) . . ?
F5 P3 F4 92.4(5) . . ?
F3 P3 F1 88.3(6) . . ?
F6 P3 F1 86.3(6) . . ?
F5 P3 F1 86.2(5) . . ?
F4 P3 F1 178.6(5) . . ?
F3 P3 F2 85.9(7) . . ?
F6 P3 F2 86.7(6) . . ?
F5 P3 F2 179.1(6) . . ?
F4 P3 F2 86.8(5) . . ?
F1 P3 F2 94.6(5) . . ?
C2 C1 C2 110.9(5) 2_655 . ?
C2 C1 H1A 109.5 2_655 . ?
C2 C1 H1A 109.5 . . ?
C2 C1 H1B 109.5 2_655 . ?
C2 C1 H1B 109.5 . . ?
H1A C1 H1B 108.0 . . ?
C22 C21 C26 118.3(4) . . ?
C22 C21 C20 119.6(4) . . ?
C26 C21 C20 121.6(4) . . ?
C14 C9 C10 118.9(4) . . ?
C14 C9 P2 122.5(3) . . ?
C10 C9 P2 118.5(4) . . ?
C4 C3 C8 119.1(5) . . ?
C4 C3 P2 120.7(4) . . ?
C8 C3 P2 120.1(4) . . ?
C25 C26 C21 120.0(5) . . ?
C25 C26 H26 120.0 . . ?
C21 C26 H26 120.0 . . ?
C19 C20 C15 118.0(4) . . ?
C19 C20 C21 114.9(4) . . ?
C15 C20 C21 127.1(4) . . ?
C11 C10 C9 120.5(5) . . ?
C11 C10 H10 119.7 . . ?
C9 C10 H10 119.7 . . ?
C29 C28 C27 109.5(6) . . ?
C29 C28 C30 108.3(5) . . ?
C27 C28 C30 107.8(5) . . ?
C29 C28 P1 105.0(4) . . ?
C27 C28 P1 116.7(4) . . ?
C30 C28 P1 109.2(4) . . ?
C16 C15 C20 117.2(4) . . ?
C16 C15 P1 117.7(3) . . ?
C20 C15 P1 124.6(3) . . ?
C9 C14 C13 120.2(5) . . ?
C9 C14 H14 119.9 . . ?
C13 C14 H14 119.9 . . ?
C3 C4 C5 120.4(5) . . ?
C3 C4 H4 119.8 . . ?
C5 C4 H4 119.8 . . ?
C23 C22 C21 120.5(5) . . ?
C23 C22 H22 119.7 . . ?
C21 C22 H22 119.7 . . ?
C24 C25 C26 120.5(6) . . ?
C24 C25 H25 119.7 . . ?
C26 C25 H25 119.7 . . ?
C24 C23 C22 120.2(5) . . ?
C24 C23 H23 119.9 . . ?
C22 C23 H23 119.9 . . ?
C25 C24 C23 120.4(5) . . ?
C25 C24 H24 119.8 . . ?
C23 C24 H24 119.8 . . ?
C3 C8 C7 120.1(5) . . ?
C3 C8 H8 119.9 . . ?
C7 C8 H8 119.9 . . ?
C18 C19 C20 122.4(5) . . ?
C18 C19 H19 118.8 . . ?
C20 C19 H19 118.8 . . ?
C17 C16 C15 122.8(5) . . ?
C17 C16 H16 118.6 . . ?
C15 C16 H16 118.6 . . ?
C12 C11 C10 119.4(5) . . ?
C12 C11 H11 120.3 . . ?
C10 C11 H11 120.3 . . ?
C6 C7 C8 119.6(6) . . ?
C6 C7 H7 120.2 . . ?
C8 C7 H7 120.2 . . ?
C32 C33 H33A 109.5 . . ?
C32 C33 H33B 109.5 . . ?
H33A C33 H33B 109.5 . . ?
C32 C33 H33C 109.5 . . ?
H33A C33 H33C 109.5 . . ?
H33B C33 H33C 109.5 . . ?
C13 C12 C11 120.8(5) . . ?
C13 C12 H12 119.6 . . ?
C11 C12 H12 119.6 . . ?
C28 C30 H30A 109.5 . . ?
C28 C30 H30B 109.5 . . ?
H30A C30 H30B 109.5 . . ?
C28 C30 H30C 109.5 . . ?
H30A C30 H30C 109.5 . . ?
H30B C30 H30C 109.5 . . ?
C6 C5 C4 119.8(5) . . ?
C6 C5 H5 120.1 . . ?
C4 C5 H5 120.1 . . ?
C19 C18 C17 120.0(5) . . ?
C19 C18 H18 120.0 . . ?
C17 C18 H18 120.0 . . ?
C5 C6 C7 120.9(6) . . ?
C5 C6 H6 119.5 . . ?
C7 C6 H6 119.5 . . ?
C32 C31 H31A 109.5 . . ?
C32 C31 H31B 109.5 . . ?
H31A C31 H31B 109.5 . . ?
C32 C31 H31C 109.5 . . ?
H31A C31 H31C 109.5 . . ?
H31B C31 H31C 109.5 . . ?
C32 C34 H34A 109.5 . . ?
C32 C34 H34B 109.5 . . ?
H34A C34 H34B 109.5 . . ?
C32 C34 H34C 109.5 . . ?
H34A C34 H34C 109.5 . . ?
H34B C34 H34C 109.5 . . ?
C28 C29 H29A 109.5 . . ?
C28 C29 H29B 109.5 . . ?
H29A C29 H29B 109.5 . . ?
C28 C29 H29C 109.5 . . ?
H29A C29 H29C 109.5 . . ?
H29B C29 H29C 109.5 . . ?
C1 C2 P2 113.1(3) . . ?
C1 C2 H2A 109.0 . . ?
P2 C2 H2A 109.0 . . ?
C1 C2 H2B 109.0 . . ?
P2 C2 H2B 109.0 . . ?
H2A C2 H2B 107.8 . . ?
C31 C32 C33 110.2(5) . . ?
C31 C32 C34 109.2(5) . . ?
C33 C32 C34 106.7(5) . . ?
C31 C32 P1 109.5(4) . . ?
C33 C32 P1 106.6(3) . . ?
C34 C32 P1 114.5(4) . . ?
C16 C17 C18 119.5(5) . . ?
C16 C17 H17 120.3 . . ?
C18 C17 H17 120.3 . . ?
C12 C13 C14 120.2(6) . . ?
C12 C13 H13 119.9 . . ?
C14 C13 H13 119.9 . . ?
C28 C27 H27A 109.5 . . ?
C28 C27 H27B 109.5 . . ?
H27A C27 H27B 109.5 . . ?
C28 C27 H27C 109.5 . . ?
H27A C27 H27C 109.5 . . ?
H27B C27 H27C 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au1 P2 2.3075(11) . ?
Au1 P1 2.3344(10) . ?
P2 C9 1.810(4) . ?
P2 C2 1.814(4) . ?
P2 C3 1.816(5) . ?
P1 C15 1.820(5) . ?
P1 C32 1.877(5) . ?
P1 C28 1.889(5) . ?
P3 F3 1.431(7) . ?
P3 F6 1.445(7) . ?
P3 F5 1.484(6) . ?
P3 F4 1.513(6) . ?
P3 F1 1.536(7) . ?
P3 F2 1.544(8) . ?
C1 C2 1.527(5) 2_655 ?
C1 C2 1.527(5) . ?
C1 H1A 0.9700 . ?
C1 H1B 0.9700 . ?
C21 C22 1.385(7) . ?
C21 C26 1.397(7) . ?
C21 C20 1.484(6) . ?
C9 C14 1.381(6) . ?
C9 C10 1.388(6) . ?
C3 C4 1.387(7) . ?
C3 C8 1.389(7) . ?
C26 C25 1.390(7) . ?
C26 H26 0.9300 . ?
C20 C19 1.403(7) . ?
C20 C15 1.416(6) . ?
C10 C11 1.385(8) . ?
C10 H10 0.9300 . ?
C28 C29 1.528(9) . ?
C28 C27 1.537(7) . ?
C28 C30 1.539(9) . ?
C15 C16 1.410(6) . ?
C14 C13 1.394(7) . ?
C14 H14 0.9300 . ?
C4 C5 1.391(8) . ?
C4 H4 0.9300 . ?
C22 C23 1.385(8) . ?
C22 H22 0.9300 . ?
C25 C24 1.355(9) . ?
C25 H25 0.9300 . ?
C23 C24 1.366(9) . ?
C23 H23 0.9300 . ?
C24 H24 0.9300 . ?
C8 C7 1.393(8) . ?
C8 H8 0.9300 . ?
C19 C18 1.361(7) . ?
C19 H19 0.9300 . ?
C16 C17 1.361(8) . ?
C16 H16 0.9300 . ?
C11 C12 1.382(9) . ?
C11 H11 0.9300 . ?
C7 C6 1.376(9) . ?
C7 H7 0.9300 . ?
C33 C32 1.538(8) . ?
C33 H33A 0.9600 . ?
C33 H33B 0.9600 . ?
C33 H33C 0.9600 . ?
C12 C13 1.349(9) . ?
C12 H12 0.9300 . ?
C30 H30A 0.9600 . ?
C30 H30B 0.9600 . ?
C30 H30C 0.9600 . ?
C5 C6 1.364(9) . ?
C5 H5 0.9300 . ?
C18 C17 1.370(8) . ?
C18 H18 0.9300 . ?
C6 H6 0.9300 . ?
C31 C32 1.514(8) . ?
C31 H31A 0.9600 . ?
C31 H31B 0.9600 . ?
C31 H31C 0.9600 . ?
C34 C32 1.542(8) . ?
C34 H34A 0.9600 . ?
C34 H34B 0.9600 . ?
C34 H34C 0.9600 . ?
C29 H29A 0.9600 . ?
C29 H29B 0.9600 . ?
C29 H29C 0.9600 . ?
C2 H2A 0.9700 . ?
C2 H2B 0.9700 . ?
C17 H17 0.9300 . ?
C13 H13 0.9300 . ?
C27 H27A 0.9600 . ?
C27 H27B 0.9600 . ?
C27 H27C 0.9600 . ?
