#------------------------------------------------------------------------------
#$Date: 2015-01-27 21:58:39 +0200 (Tue, 27 Jan 2015) $
#$Revision: 130149 $
#$URL: svn://www.crystallography.net/cod/cif/7/10/00/7100040.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7100040
loop_
_publ_author_name
'Elena Fernandez'
'Rosa Corberan'
'Eduardo Peris'
'Jesus Ramirez'
'Mercedes Sanau'
_publ_section_title
;
Unprecedented use of silver(I) N-heterocyclic
carbene complexes for the catalytic preparation of 1,2-bis(boronate)esters
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b503239c
_journal_year                    2005
_chemical_formula_sum            'C60 H104 Ag4 Cl4 N8 O4'
_chemical_formula_weight         1574.79
_space_group_IT_number           1
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  'P 1'
_symmetry_space_group_name_H-M   'P 1'
_cell_angle_alpha                105.54(3)
_cell_angle_beta                 97.78(3)
_cell_angle_gamma                94.74(3)
_cell_formula_units_Z            1
_cell_length_a                   9.3318(19)
_cell_length_b                   11.080(2)
_cell_length_c                   18.816(4)
_cell_measurement_temperature    273(2)
_cell_volume                     1842.6(6)
_diffrn_ambient_temperature      273(2)
_exptl_crystal_density_diffrn    1.419
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               7100040
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.35012(11) 1.19148(8) 0.47397(6) 0.0553(4) Uani 1 1 d . . .
N1 N -0.307(3) 0.788(2) 0.2228(13) 0.094(7) Uani 1 1 d . . .
O1 O 0.0381(19) 0.8274(11) 0.0799(8) 0.090(5) Uani 1 1 d . . .
Cl1 Cl 0.4206(8) 1.1087(6) 0.2731(5) 0.094(2) Uani 1 1 d . . .
C1 C 0.481(4) 0.177(5) 0.099(2) 0.26(3) Uani 1 1 d . . .
H1A H 0.5757 0.1980 0.1294 0.389 Uiso 1 1 calc R . .
H1B H 0.4811 0.1020 0.0584 0.389 Uiso 1 1 calc R . .
H1C H 0.4093 0.1613 0.1283 0.389 Uiso 1 1 calc R . .
Ag2 Ag 0.27456(18) 0.98807(14) 0.33201(9) 0.0810(6) Uani 1 1 d . . .
N2 N -0.117(3) 0.843(2) 0.1779(11) 0.090(7) Uani 1 1 d . . .
O2 O 0.1854(19) 0.3884(15) 0.1200(10) 0.089(5) Uani 1 1 d . . .
Cl2 Cl 0.0265(6) 1.0296(4) 0.3798(3) 0.0626(15) Uani 1 1 d . . .
C2 C 0.444(7) 0.289(5) 0.066(2) 0.26(3) Uani 1 1 d . . .
H2 H 0.4368 0.3597 0.1089 0.308 Uiso 1 1 calc R . .
Ag3 Ag -0.01135(17) 0.79441(13) 0.36238(9) 0.0754(6) Uani 1 1 d . . .
N3 N -0.112(2) 0.3396(18) 0.2611(11) 0.087(7) Uani 1 1 d . . .
Cl3 Cl 0.2390(6) 0.7530(4) 0.3152(4) 0.0653(16) Uani 1 1 d . . .
O3 O 0.0712(15) 1.4046(10) 0.5664(9) 0.061(4) Uani 1 1 d . . .
C3 C 0.568(5) 0.348(5) 0.016(2) 0.23(2) Uani 1 1 d . . .
H3A H 0.5781 0.2821 -0.0274 0.347 Uiso 1 1 calc R . .
H3B H 0.6606 0.3764 0.0476 0.347 Uiso 1 1 calc R . .
H3C H 0.5309 0.4171 0.0008 0.347 Uiso 1 1 calc R . .
Ag4 Ag -0.08659(12) 0.59192(9) 0.22081(7) 0.0622(5) Uani 1 1 d . . .
N4 N 0.097(2) 0.3697(16) 0.2310(11) 0.070(5) Uani 1 1 d . . .
Cl4 Cl -0.1533(6) 0.6722(5) 0.4237(3) 0.0696(15) Uani 1 1 d . . .
C4 C 0.278(3) 0.229(2) 0.0281(12) 0.098(6) Uani 1 1 d . . .
H4 H 0.2486 0.2773 -0.0067 0.118 Uiso 1 1 calc R . .
O4 O 0.2446(14) 0.9165(10) 0.5972(7) 0.062(3) Uani 1 1 d . . .
N5 N 0.577(2) 1.009(2) 0.4792(11) 0.082(6) Uani 1 1 d . . .
C5 C 0.282(4) 0.110(2) -0.0163(16) 0.125(9) Uani 1 1 d . . .
H5A H 0.3096 0.0537 0.0137 0.149 Uiso 1 1 calc R . .
H5B H 0.3520 0.1106 -0.0502 0.149 Uiso 1 1 calc R . .
N6 N 0.386(2) 0.9281(13) 0.5060(10) 0.065(5) Uani 1 1 d . . .
C6 C 0.004(4) 0.065(3) -0.016(2) 0.136(12) Uani 1 1 d . . .
H6 H 0.0305 0.0105 0.0162 0.163 Uiso 1 1 calc R . .
N7 N 0.165(2) 1.4129(13) 0.4578(10) 0.060(5) Uani 1 1 d . . .
C7 C 0.141(4) 0.071(3) -0.0559(19) 0.140(11) Uiso 1 1 d . . .
H7A H 0.1416 -0.0127 -0.0890 0.168 Uiso 1 1 calc R . .
H7B H 0.1239 0.1263 -0.0875 0.168 Uiso 1 1 calc R . .
N8 N 0.365(2) 1.4324(14) 0.4257(11) 0.071(5) Uani 1 1 d . . .
C8 C -0.164(5) 0.034(4) -0.035(3) 0.25(3) Uani 1 1 d . . .
H8A H -0.2078 0.1111 -0.0268 0.379 Uiso 1 1 calc R . .
H8B H -0.1979 -0.0134 -0.0028 0.379 Uiso 1 1 calc R . .
H8C H -0.1919 -0.0150 -0.0859 0.379 Uiso 1 1 calc R . .
C9 C 0.041(3) 0.216(2) 0.0479(16) 0.111(8) Uani 1 1 d . . .
H9A H 0.0081 0.2766 0.0224 0.133 Uiso 1 1 calc R . .
H9B H -0.0159 0.2185 0.0878 0.133 Uiso 1 1 calc R . .
C10 C 0.185(3) 0.252(2) 0.0789(13) 0.067(6) Uani 1 1 d . . .
H10 H 0.2101 0.2059 0.1157 0.080 Uiso 1 1 calc R . .
C11 C 0.361(5) 0.660(4) 0.065(2) 0.23(2) Uani 1 1 d . . .
H11A H 0.4533 0.7050 0.0931 0.343 Uiso 1 1 calc R . .
H11B H 0.3774 0.5817 0.0323 0.343 Uiso 1 1 calc R . .
H11C H 0.2997 0.6437 0.0994 0.343 Uiso 1 1 calc R . .
C12 C 0.288(3) 0.741(2) 0.0192(13) 0.110(7) Uani 1 1 d . . .
H12 H 0.2876 0.8254 0.0532 0.132 Uiso 1 1 calc R . .
C13 C 0.389(4) 0.754(3) -0.0359(16) 0.145(10) Uani 1 1 d . . .
H13A H 0.3987 0.6722 -0.0670 0.218 Uiso 1 1 calc R . .
H13B H 0.4829 0.7951 -0.0089 0.218 Uiso 1 1 calc R . .
H13C H 0.3492 0.8042 -0.0666 0.218 Uiso 1 1 calc R . .
C14 C 0.138(3) 0.6930(19) -0.0147(11) 0.095(6) Uani 1 1 d . . .
H14 H 0.1083 0.7454 -0.0473 0.114 Uiso 1 1 calc R . .
C15 C 0.121(3) 0.562(3) -0.0640(19) 0.132(12) Uani 1 1 d . . .
H15A H 0.1550 0.5075 -0.0340 0.158 Uiso 1 1 calc R . .
H15B H 0.1842 0.5587 -0.1012 0.158 Uiso 1 1 calc R . .
C16 C -0.041(4) 0.504(4) -0.1065(17) 0.186(17) Uani 1 1 d . . .
H16A H -0.0648 0.5411 -0.1470 0.223 Uiso 1 1 calc R . .
H16B H -0.0430 0.4136 -0.1283 0.223 Uiso 1 1 calc R . .
C17 C -0.153(4) 0.526(3) -0.0563(16) 0.164(14) Uani 1 1 d . . .
H17 H -0.1436 0.4670 -0.0261 0.197 Uiso 1 1 calc R . .
C18 C -0.303(4) 0.498(4) -0.0992(19) 0.22(2) Uani 1 1 d . . .
H18A H -0.3657 0.5500 -0.0716 0.334 Uiso 1 1 calc R . .
H18B H -0.3380 0.4107 -0.1072 0.334 Uiso 1 1 calc R . .
H18C H -0.3027 0.5151 -0.1466 0.334 Uiso 1 1 calc R . .
C19 C -0.126(2) 0.662(2) -0.0006(11) 0.098(6) Uani 1 1 d . . .
H19A H -0.1527 0.7223 -0.0277 0.118 Uiso 1 1 calc R . .
H19B H -0.1881 0.6662 0.0370 0.118 Uiso 1 1 calc R . .
C20 C 0.025(3) 0.698(2) 0.0362(14) 0.092(8) Uani 1 1 d . . .
H20 H 0.0479 0.6453 0.0694 0.110 Uiso 1 1 calc R . .
C21 C 0.031(4) 0.851(3) 0.1637(15) 0.120(12) Uani 1 1 d . . .
H21A H 0.0815 0.7897 0.1821 0.144 Uiso 1 1 calc R . .
H21B H 0.0815 0.9345 0.1908 0.144 Uiso 1 1 calc R . .
C22 C -0.199(4) 0.937(2) 0.1718(17) 0.113(11) Uani 1 1 d . . .
H22 H -0.1798 1.0056 0.1529 0.136 Uiso 1 1 calc R . .
C23 C -0.326(3) 0.900(2) 0.2039(17) 0.098(9) Uani 1 1 d . . .
H23 H -0.4057 0.9444 0.2105 0.118 Uiso 1 1 calc R . .
C24 C -0.393(3) 0.741(3) 0.2553(19) 0.123(12) Uani 1 1 d . . .
H24A H -0.3448 0.7441 0.3043 0.185 Uiso 1 1 calc R . .
H24B H -0.4259 0.6552 0.2273 0.185 Uiso 1 1 calc R . .
H24C H -0.4748 0.7882 0.2597 0.185 Uiso 1 1 calc R . .
C04 C -0.166(3) 0.759(2) 0.2073(13) 0.071(6) Uani 1 1 d . . .
C03 C -0.023(3) 0.4163(15) 0.2335(11) 0.069(7) Uani 1 1 d . . .
C27 C 0.221(2) 0.424(2) 0.2021(17) 0.097(10) Uani 1 1 d . . .
H27A H 0.2360 0.5157 0.2220 0.117 Uiso 1 1 calc R . .
H27B H 0.3105 0.3920 0.2173 0.117 Uiso 1 1 calc R . .
C28 C 0.114(7) 0.268(4) 0.251(2) 0.15(2) Uani 1 1 d . . .
H28 H 0.1928 0.2221 0.2497 0.182 Uiso 1 1 calc R . .
C29 C 0.008(6) 0.250(2) 0.2717(15) 0.13(2) Uani 1 1 d . . .
H29 H -0.0079 0.1854 0.2937 0.158 Uiso 1 1 calc R . .
C30 C -0.2567(17) 0.3650(19) 0.2810(12) 0.091(7) Uani 1 1 d . . .
H30A H -0.2451 0.4173 0.3317 0.136 Uiso 1 1 calc R . .
H30B H -0.3146 0.2866 0.2763 0.136 Uiso 1 1 calc R . .
H30C H -0.3045 0.4074 0.2480 0.136 Uiso 1 1 calc R . .
C31 C 0.592(2) 1.092(2) 0.7158(16) 0.126(8) Uani 1 1 d . . .
H31A H 0.5878 1.1782 0.7430 0.189 Uiso 1 1 calc R . .
H31B H 0.5809 1.0848 0.6632 0.189 Uiso 1 1 calc R . .
H31C H 0.6844 1.0675 0.7318 0.189 Uiso 1 1 calc R . .
C32 C 0.470(2) 1.0068(18) 0.7306(11) 0.093(6) Uani 1 1 d . . .
H32 H 0.4632 0.9234 0.6946 0.112 Uiso 1 1 calc R . .
C33 C 0.515(3) 0.992(2) 0.8089(14) 0.121(8) Uani 1 1 d . . .
H33A H 0.6185 0.9902 0.8179 0.181 Uiso 1 1 calc R . .
H33B H 0.4655 0.9152 0.8124 0.181 Uiso 1 1 calc R . .
H33C H 0.4899 1.0625 0.8455 0.181 Uiso 1 1 calc R . .
C34 C 0.3152(17) 1.0511(14) 0.7246(9) 0.067(4) Uani 1 1 d . . .
H34 H 0.2507 0.9946 0.7418 0.080 Uiso 1 1 calc R . .
C35 C 0.312(3) 1.188(2) 0.7729(13) 0.112(8) Uani 1 1 d . . .
H35A H 0.3520 1.1942 0.8243 0.134 Uiso 1 1 calc R . .
H35B H 0.3742 1.2448 0.7559 0.134 Uiso 1 1 calc R . .
C36 C 0.176(4) 1.226(3) 0.7712(18) 0.123(12) Uani 1 1 d . . .
H36A H 0.1849 1.3131 0.8017 0.147 Uiso 1 1 calc R . .
H36B H 0.1165 1.1752 0.7936 0.147 Uiso 1 1 calc R . .
C37 C 0.096(2) 1.2169(15) 0.6915(12) 0.085(5) Uani 1 1 d . . .
H37 H 0.1532 1.2747 0.6717 0.102 Uiso 1 1 calc R . .
C38 C -0.066(3) 1.250(3) 0.684(2) 0.154(13) Uani 1 1 d . . .
H38A H -0.0669 1.3365 0.7118 0.232 Uiso 1 1 calc R . .
H38B H -0.1249 1.1959 0.7039 0.232 Uiso 1 1 calc R . .
H38C H -0.1043 1.2383 0.6325 0.232 Uiso 1 1 calc R . .
C39 C 0.0884(18) 1.0756(17) 0.6353(11) 0.080(5) Uani 1 1 d . . .
H39A H 0.0251 1.0151 0.6494 0.095 Uiso 1 1 calc R . .
H39B H 0.0538 1.0737 0.5840 0.095 Uiso 1 1 calc R . .
C40 C 0.247(2) 1.0485(16) 0.6455(11) 0.057(4) Uani 1 1 d . . .
H40 H 0.3075 1.1070 0.6275 0.068 Uiso 1 1 calc R . .
C41 C 0.504(3) 0.852(2) 0.5088(13) 0.076(7) Uani 1 1 d . . .
H41 H 0.4988 0.7746 0.5188 0.091 Uiso 1 1 calc R . .
C42 C 0.2424(18) 0.9091(17) 0.5306(12) 0.065(6) Uani 1 1 d . . .
H42A H 0.1834 0.9712 0.5185 0.078 Uiso 1 1 calc R . .
H42B H 0.1937 0.8265 0.5014 0.078 Uiso 1 1 calc R . .
C44 C 0.619(4) 0.910(4) 0.4952(16) 0.131(14) Uani 1 1 d . . .
H44 H 0.7124 0.8860 0.4967 0.157 Uiso 1 1 calc R . .
C45 C 0.686(2) 1.105(2) 0.4486(17) 0.098(8) Uani 1 1 d . . .
H45A H 0.6300 1.1635 0.4316 0.147 Uiso 1 1 calc R . .
H45B H 0.7268 1.0552 0.4080 0.147 Uiso 1 1 calc R . .
H45C H 0.7623 1.1497 0.4885 0.147 Uiso 1 1 calc R . .
C46 C 0.472(7) 1.415(3) 0.408(2) 0.24(3) Uani 1 1 d . . .
H46A H 0.4886 1.4594 0.3717 0.356 Uiso 1 1 calc R . .
H46B H 0.4724 1.3261 0.3858 0.356 Uiso 1 1 calc R . .
H46C H 0.5485 1.4443 0.4504 0.356 Uiso 1 1 calc R . .
C47 C 0.304(3) 1.5266(18) 0.4101(13) 0.078(6) Uani 1 1 d . . .
H47 H 0.3441 1.5893 0.3915 0.094 Uiso 1 1 calc R . .
C48 C 0.162(3) 1.510(2) 0.4284(15) 0.078(6) Uani 1 1 d . . .
H48 H 0.0854 1.5558 0.4215 0.094 Uiso 1 1 calc R . .
C02 C 0.2907(19) 1.3573(17) 0.4524(12) 0.056(5) Uani 1 1 d . . .
C50 C 0.045(2) 1.3741(19) 0.4916(12) 0.076(7) Uani 1 1 d . . .
H50A H -0.0395 1.4124 0.4764 0.091 Uiso 1 1 calc R . .
H50B H 0.0204 1.2833 0.4722 0.091 Uiso 1 1 calc R . .
C01 C 0.449(2) 1.0340(17) 0.4887(12) 0.059(5) Uani 1 1 d . . .
C52 C 0.086(2) 1.5355(17) 0.6006(12) 0.053(5) Uani 1 1 d . . .
H52 H 0.1294 1.5807 0.5690 0.064 Uiso 1 1 calc R . .
C53 C -0.0615(18) 1.5791(13) 0.6140(10) 0.067(4) Uani 1 1 d . . .
H53A H -0.1239 1.5626 0.5660 0.080 Uiso 1 1 calc R . .
H53B H -0.1060 1.5286 0.6420 0.080 Uiso 1 1 calc R . .
C54 C -0.0565(18) 1.7148(13) 0.6550(11) 0.077(5) Uani 1 1 d . . .
H54 H -0.0124 1.7652 0.6262 0.093 Uiso 1 1 calc R . .
C55 C -0.202(2) 1.759(2) 0.6687(16) 0.118(8) Uani 1 1 d . . .
H55A H -0.2230 1.7480 0.7152 0.177 Uiso 1 1 calc R . .
H55B H -0.2769 1.7114 0.6287 0.177 Uiso 1 1 calc R . .
H55C H -0.1979 1.8473 0.6710 0.177 Uiso 1 1 calc R . .
C56 C 0.039(2) 1.7387(16) 0.7266(11) 0.077(5) Uani 1 1 d . . .
H56A H -0.0079 1.6917 0.7558 0.093 Uiso 1 1 calc R . .
H56B H 0.0429 1.8276 0.7526 0.093 Uiso 1 1 calc R . .
C57 C 0.198(2) 1.7074(18) 0.7284(15) 0.086(6) Uani 1 1 d . . .
H57A H 0.2439 1.7165 0.7793 0.103 Uiso 1 1 calc R . .
H57B H 0.2544 1.7635 0.7080 0.103 Uiso 1 1 calc R . .
C58 C 0.188(2) 1.5660(15) 0.6791(9) 0.062(4) Uani 1 1 d . . .
H58 H 0.1438 1.5135 0.7068 0.075 Uiso 1 1 calc R . .
C59 C 0.3356(18) 1.5222(17) 0.6680(10) 0.080(5) Uani 1 1 d . . .
H59 H 0.3175 1.4329 0.6393 0.096 Uiso 1 1 calc R . .
C60 C 0.4225(18) 1.5917(18) 0.6241(13) 0.099(7) Uani 1 1 d . . .
H60A H 0.3628 1.5895 0.5779 0.148 Uiso 1 1 calc R . .
H60B H 0.5075 1.5513 0.6137 0.148 Uiso 1 1 calc R . .
H60C H 0.4517 1.6779 0.6531 0.148 Uiso 1 1 calc R . .
C61 C 0.438(3) 1.531(2) 0.7457(14) 0.130(9) Uani 1 1 d . . .
H61A H 0.5297 1.5030 0.7358 0.195 Uiso 1 1 calc R . .
H61B H 0.3910 1.4778 0.7709 0.195 Uiso 1 1 calc R . .
H61C H 0.4534 1.6165 0.7767 0.195 Uiso 1 1 calc R . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 C02 2.09(2) . ?
Ag1 C01 2.104(18) . ?
Ag1 Ag2 2.952(2) . ?
N1 C24 1.24(4) . ?
N1 C23 1.40(4) . ?
N1 C04 1.43(3) . ?
O1 C20 1.43(2) . ?
O1 C21 1.54(3) . ?
Cl1 Ag2 2.403(7) . ?
C1 C2 1.57(7) . ?
Ag2 Cl3 2.526(5) . ?
Ag2 Cl2 2.626(6) . ?
N2 C04 1.29(3) . ?
N2 C22 1.36(3) . ?
N2 C21 1.45(4) . ?
O2 C27 1.47(3) . ?
O2 C10 1.50(3) . ?
Cl2 Ag3 2.526(5) . ?
C2 C4 1.62(7) . ?
C2 C3 1.77(6) . ?
Ag3 Cl4 2.424(6) . ?
Ag3 Cl3 2.641(6) . ?
Ag3 Ag4 2.942(2) . ?
N3 C03 1.38(3) . ?
N3 C30 1.48(3) . ?
N3 C29 1.58(4) . ?
O3 C50 1.34(3) . ?
O3 C52 1.41(2) . ?
Ag4 C04 2.11(2) . ?
Ag4 C03 2.144(18) . ?
N4 C03 1.27(3) . ?
N4 C28 1.30(5) . ?
N4 C27 1.50(3) . ?
C4 C10 1.36(3) . ?
C4 C5 1.37(3) . ?
O4 C42 1.23(2) . ?
O4 C40 1.497(19) . ?
N5 C01 1.27(2) . ?
N5 C44 1.29(4) . ?
N5 C45 1.67(3) . ?
C5 C7 1.39(4) . ?
N6 C01 1.40(3) . ?
N6 C41 1.45(3) . ?
N6 C42 1.49(3) . ?
C6 C8 1.55(5) . ?
C6 C7 1.58(4) . ?
C6 C9 1.75(4) . ?
N7 C48 1.33(3) . ?
N7 C02 1.37(2) . ?
N7 C50 1.45(3) . ?
N8 C46 1.12(5) . ?
N8 C02 1.28(3) . ?
N8 C47 1.31(3) . ?
C9 C10 1.38(3) . ?
C11 C12 1.55(4) . ?
C12 C14 1.45(3) . ?
C12 C13 1.52(4) . ?
C14 C15 1.49(3) . ?
C14 C20 1.51(4) . ?
C15 C16 1.60(4) . ?
C16 C17 1.49(4) . ?
C17 C18 1.49(4) . ?
C17 C19 1.56(3) . ?
C19 C20 1.45(3) . ?
C22 C23 1.48(4) . ?
C28 C29 1.13(7) . ?
C31 C32 1.53(3) . ?
C32 C33 1.53(3) . ?
C32 C34 1.56(2) . ?
C34 C40 1.53(3) . ?
C34 C35 1.55(2) . ?
C35 C36 1.37(4) . ?
C36 C37 1.56(4) . ?
C37 C38 1.58(3) . ?
C37 C39 1.63(3) . ?
C39 C40 1.53(2) . ?
C41 C44 1.30(5) . ?
C47 C48 1.42(4) . ?
C52 C53 1.53(3) . ?
C52 C58 1.58(3) . ?
C53 C54 1.49(2) . ?
C54 C56 1.46(3) . ?
C54 C55 1.51(2) . ?
C56 C57 1.55(3) . ?
C57 C58 1.58(2) . ?
C58 C59 1.52(2) . ?
C59 C60 1.54(3) . ?
C59 C61 1.61(3) . ?
