#------------------------------------------------------------------------------
#$Date: 2016-03-26 01:55:57 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180115 $
#$URL: svn://www.crystallography.net/cod/cif/7/10/13/7101308.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7101308
loop_
_publ_author_name
'Robert Davies'
'M. Giovanna Martinelli'
'Andrew J. P. White'
_publ_section_title
;
Discrete copper(I) clusters with Cu6P6Se6 and Cu6P4Se6
cores
;
_journal_issue                   30
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b605191j
_journal_year                    2006
_chemical_formula_sum            'C98 H86 Cu6 P8 Se8'
_chemical_formula_weight         2524.35
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 106.850(7)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   13.1362(12)
_cell_length_b                   22.2016(14)
_cell_length_c                   17.6252(14)
_cell_measurement_reflns_used    20
_cell_measurement_temperature    203(2)
_cell_measurement_theta_max      24.89
_cell_measurement_theta_min      11.09
_cell_volume                     4919.6(7)
_computing_cell_refinement       'Bruker XSCANS'
_computing_data_collection       'Bruker XSCANS'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      203(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Bruker P4/RA'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54178
_diffrn_reflns_av_R_equivalents  0.0256
_diffrn_reflns_av_sigmaI/netI    0.0488
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            7626
_diffrn_reflns_theta_full        60.00
_diffrn_reflns_theta_max         60.00
_diffrn_reflns_theta_min         3.29
_diffrn_standards_interval_count 97
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    6.372
_exptl_absorpt_correction_T_max  0.6975
_exptl_absorpt_correction_T_min  0.2366
_exptl_absorpt_correction_type   Shelxa
_exptl_crystal_colour            Orange/yellow
_exptl_crystal_density_diffrn    1.704
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       blocks
_exptl_crystal_F_000             2480
_exptl_crystal_size_max          0.22
_exptl_crystal_size_mid          0.13
_exptl_crystal_size_min          0.13
_refine_diff_density_max         1.176
_refine_diff_density_min         -1.142
_refine_diff_density_rms         0.102
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.058
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     445
_refine_ls_number_reflns         7269
_refine_ls_number_restraints     60
_refine_ls_restrained_S_all      1.069
_refine_ls_R_factor_all          0.0837
_refine_ls_R_factor_gt           0.0604
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0599P)²+15.9858P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1350
_refine_ls_wR_factor_ref         0.1457
_reflns_number_gt                5605
_reflns_number_total             7269
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b605191j.txt
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P2(1)/n
_cod_database_code               7101308
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Cu1 Cu 0.35324(10) 0.51073(5) 0.99901(7) 0.0553(3) Uani 1 1 d .
Se2 Se 0.31104(8) 0.50197(4) 1.11914(6) 0.0581(2) Uani 1 1 d .
Cu3 Cu 0.50532(10) 0.51254(5) 1.14824(7) 0.0522(3) Uani 1 1 d .
P4 P 0.5721(2) 0.57403(11) 1.25353(13) 0.0630(6) Uani 1 1 d .
Se5 Se 0.57015(7) 0.57383(4) 1.04965(5) 0.0472(2) Uani 1 1 d .
Cu6 Cu 0.55937(10) 0.63548(5) 0.92723(7) 0.0512(3) Uani 1 1 d .
Se7 Se 0.40979(7) 0.58825(4) 0.83023(5) 0.0493(2) Uani 1 1 d .
P8 P 0.29865(16) 0.57863(9) 0.90406(12) 0.0476(5) Uani 1 1 d .
P9 P 0.31045(19) 0.40170(10) 1.12092(14) 0.0568(5) Uani 1 1 d .
Se10 Se 0.64509(12) 0.65382(5) 1.21194(7) 0.0856(4) Uani 1 1 d .
P11 P 0.5478(2) 0.73160(10) 0.96127(15) 0.0615(6) Uani 1 1 d .
H11 H 0.4700 0.7336 0.9930 0.074 Uiso 1 1 calc R
C1 C 0.6896(8) 0.6088(4) 1.1292(6) 0.070(3) Uani 1 1 d .
H1A H 0.7276 0.6362 1.1033 0.084 Uiso 1 1 calc R
H1B H 0.7388 0.5766 1.1545 0.084 Uiso 1 1 calc R
C2 C 0.4770(6) 0.6118(4) 1.2958(4) 0.072(3) Uani 1 1 d G
C3 C 0.3871(8) 0.6369(5) 1.2431(4) 0.125(5) Uani 1 1 d GU
H3A H 0.3792 0.6363 1.1884 0.150 Uiso 1 1 calc R
C4 C 0.3088(7) 0.6627(5) 1.2714(7) 0.169(8) Uani 1 1 d GU
H4A H 0.2479 0.6797 1.2357 0.203 Uiso 1 1 calc R
C5 C 0.3204(8) 0.6635(6) 1.3523(7) 0.157(8) Uani 1 1 d G
H5A H 0.2675 0.6810 1.3714 0.189 Uiso 1 1 calc R
C6 C 0.4104(10) 0.6384(6) 1.4050(5) 0.154(8) Uani 1 1 d G
H6A H 0.4182 0.6390 1.4597 0.184 Uiso 1 1 calc R
C7 C 0.4887(7) 0.6126(5) 1.3768(4) 0.118(5) Uani 1 1 d G
H7A H 0.5495 0.5956 1.4124 0.141 Uiso 1 1 calc R
C8 C 0.6712(6) 0.5448(3) 1.3405(4) 0.074(3) Uani 1 1 d G
C9 C 0.6460(7) 0.4910(3) 1.3713(4) 0.104(4) Uani 1 1 d G
H9A H 0.5819 0.4712 1.3460 0.125 Uiso 1 1 calc R
C10 C 0.7156(9) 0.4665(3) 1.4392(5) 0.126(5) Uani 1 1 d GU
H10A H 0.6985 0.4302 1.4600 0.151 Uiso 1 1 calc R
C11 C 0.8104(8) 0.4958(5) 1.4765(5) 0.137(6) Uani 1 1 d GU
H11A H 0.8575 0.4793 1.5225 0.164 Uiso 1 1 calc R
C12 C 0.8357(6) 0.5496(5) 1.4458(6) 0.146(7) Uani 1 1 d G
H12A H 0.8998 0.5694 1.4710 0.175 Uiso 1 1 calc R
C13 C 0.7661(7) 0.5741(3) 1.3778(5) 0.104(4) Uani 1 1 d G
H13A H 0.7831 0.6104 1.3571 0.124 Uiso 1 1 calc R
C14 C 0.2782(5) 0.65524(18) 0.9346(3) 0.0531(19) Uani 1 1 d G
C15 C 0.3100(5) 0.6680(2) 1.0153(3) 0.062(2) Uani 1 1 d G
H15A H 0.3387 0.6373 1.0521 0.074 Uiso 1 1 calc R
C16 C 0.2995(5) 0.7260(3) 1.0416(3) 0.072(3) Uani 1 1 d G
H16A H 0.3211 0.7346 1.0962 0.086 Uiso 1 1 calc R
C17 C 0.2572(6) 0.7714(2) 0.9872(4) 0.076(3) Uani 1 1 d G
H17A H 0.2501 0.8106 1.0050 0.091 Uiso 1 1 calc R
C18 C 0.2253(6) 0.7586(2) 0.9065(4) 0.083(3) Uani 1 1 d G
H18A H 0.1967 0.7893 0.8697 0.100 Uiso 1 1 calc R
C19 C 0.2359(5) 0.7006(3) 0.8802(3) 0.071(3) Uani 1 1 d G
H19A H 0.2143 0.6920 0.8257 0.086 Uiso 1 1 calc R
C20 C 0.1696(4) 0.5601(3) 0.8348(4) 0.061(2) Uani 1 1 d G
C21 C 0.1534(5) 0.5559(3) 0.7535(4) 0.082(3) Uani 1 1 d G
H21A H 0.2110 0.5606 0.7324 0.098 Uiso 1 1 calc R
C22 C 0.0521(7) 0.5448(4) 0.7034(4) 0.114(5) Uani 1 1 d G
H22A H 0.0411 0.5419 0.6484 0.136 Uiso 1 1 calc R
C23 C -0.0330(4) 0.5379(4) 0.7345(6) 0.118(5) Uani 1 1 d GU
H23A H -0.1016 0.5303 0.7006 0.142 Uiso 1 1 calc R
C24 C -0.0168(5) 0.5421(4) 0.8159(6) 0.122(5) Uani 1 1 d GU
H24A H -0.0744 0.5374 0.8369 0.146 Uiso 1 1 calc R
C25 C 0.0845(6) 0.5532(4) 0.8660(4) 0.102(5) Uani 1 1 d G
H25A H 0.0954 0.5560 0.9210 0.123 Uiso 1 1 calc R
C26 C 0.1713(4) 0.3810(3) 1.0714(4) 0.070(3) Uani 1 1 d G
C27 C 0.1223(6) 0.4084(4) 0.9990(5) 0.110(5) Uani 1 1 d G
H27A H 0.1578 0.4389 0.9798 0.132 Uiso 1 1 calc R
C28 C 0.0208(7) 0.3906(5) 0.9552(4) 0.134(6) Uani 1 1 d G
H28A H -0.0123 0.4091 0.9063 0.160 Uiso 1 1 calc R
C29 C -0.0317(5) 0.3455(5) 0.9837(6) 0.118(5) Uani 1 1 d GU
H29A H -0.1003 0.3335 0.9541 0.141 Uiso 1 1 calc R
C30 C 0.0173(6) 0.3181(4) 1.0560(7) 0.118(5) Uani 1 1 d GU
H30A H -0.0182 0.2876 1.0753 0.142 Uiso 1 1 calc R
C31 C 0.1188(6) 0.3359(3) 1.0998(5) 0.098(4) Uani 1 1 d G
H31A H 0.1519 0.3174 1.1487 0.118 Uiso 1 1 calc R
C32 C 0.3310(6) 0.3812(3) 1.2257(3) 0.075(3) Uani 1 1 d G
C33 C 0.3523(7) 0.3210(3) 1.2459(5) 0.100(4) Uani 1 1 d G
H33A H 0.3527 0.2926 1.2065 0.120 Uiso 1 1 calc R
C34 C 0.3730(8) 0.3030(4) 1.3244(6) 0.130(6) Uani 1 1 d G
H34A H 0.3874 0.2623 1.3382 0.156 Uiso 1 1 calc R
C35 C 0.3724(8) 0.3451(6) 1.3827(4) 0.139(6) Uani 1 1 d GU
H35A H 0.3864 0.3328 1.4358 0.166 Uiso 1 1 calc R
C36 C 0.3511(8) 0.4052(5) 1.3624(4) 0.130(6) Uani 1 1 d G
H36A H 0.3507 0.4337 1.4018 0.156 Uiso 1 1 calc R
C37 C 0.3304(7) 0.4233(3) 1.2839(5) 0.104(4) Uani 1 1 d G
H37A H 0.3160 0.4640 1.2702 0.125 Uiso 1 1 calc R
C38 C 0.6631(4) 0.7613(3) 1.0357(3) 0.064(2) Uani 1 1 d G
C39 C 0.6556(5) 0.7940(3) 1.1011(4) 0.085(3) Uani 1 1 d G
H39A H 0.5893 0.7987 1.1107 0.102 Uiso 1 1 calc R
C40 C 0.7461(7) 0.8197(3) 1.1523(3) 0.090(4) Uani 1 1 d G
H40A H 0.7411 0.8418 1.1966 0.107 Uiso 1 1 calc R
C41 C 0.8442(5) 0.8127(3) 1.1381(4) 0.089(3) Uani 1 1 d G
H41A H 0.9054 0.8300 1.1728 0.107 Uiso 1 1 calc R
C42 C 0.8517(4) 0.7800(3) 1.0727(4) 0.082(3) Uani 1 1 d G
H42A H 0.9179 0.7753 1.0631 0.098 Uiso 1 1 calc R
C43 C 0.7611(5) 0.7543(3) 1.0215(3) 0.072(3) Uani 1 1 d G
H43A H 0.7662 0.7322 0.9772 0.086 Uiso 1 1 calc R
C44 C 0.5193(6) 0.7897(3) 0.8856(4) 0.065(2) Uani 1 1 d G
C45 C 0.5569(7) 0.8482(3) 0.9027(4) 0.110(5) Uani 1 1 d G
H45A H 0.5962 0.8585 0.9546 0.132 Uiso 1 1 calc R
C46 C 0.5363(8) 0.8913(2) 0.8430(5) 0.132(6) Uani 1 1 d GU
H46A H 0.5617 0.9308 0.8545 0.158 Uiso 1 1 calc R
C47 C 0.4781(7) 0.8760(3) 0.7662(4) 0.096(4) Uani 1 1 d G
H47A H 0.4642 0.9052 0.7258 0.115 Uiso 1 1 calc R
C48 C 0.4406(7) 0.8176(3) 0.7491(3) 0.101(4) Uani 1 1 d G
H48A H 0.4012 0.8072 0.6971 0.122 Uiso 1 1 calc R
C49 C 0.4611(6) 0.7744(2) 0.8088(4) 0.089(4) Uani 1 1 d G
H49A H 0.4357 0.7349 0.7972 0.107 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu -1.9646 0.5888 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.7943 1.1372 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
P8 Cu1 Se2 129.01(8) . .
P8 Cu1 Se5 109.87(8) . 3_667
Se2 Cu1 Se5 119.36(6) . 3_667
P8 Cu1 Cu3 133.35(8) . .
Se2 Cu1 Cu3 56.32(4) . .
Se5 Cu1 Cu3 95.04(5) 3_667 .
P9 Se2 Cu1 95.63(7) . .
P9 Se2 Cu3 95.73(8) . .
Cu1 Se2 Cu3 71.25(5) . .
P4 Cu3 Se2 111.07(9) . .
P4 Cu3 Se7 111.61(8) . 3_667
Se2 Cu3 Se7 109.79(5) . 3_667
P4 Cu3 Se5 96.35(8) . .
Se2 Cu3 Se5 116.17(6) . .
Se7 Cu3 Se5 111.28(5) 3_667 .
P4 Cu3 Cu1 141.10(9) . .
Se2 Cu3 Cu1 52.43(4) . .
Se7 Cu3 Cu1 107.28(5) 3_667 .
Se5 Cu3 Cu1 69.83(4) . .
C8 P4 C2 103.1(4) . .
C8 P4 Se10 106.8(3) . .
C2 P4 Se10 100.3(3) . .
C8 P4 Cu3 119.2(3) . .
C2 P4 Cu3 117.5(3) . .
Se10 P4 Cu3 108.04(10) . .
C1 Se5 Cu1 103.7(3) . 3_667
C1 Se5 Cu6 103.6(3) . .
Cu1 Se5 Cu6 92.52(5) 3_667 .
C1 Se5 Cu3 94.7(3) . .
Cu1 Se5 Cu3 94.81(5) 3_667 .
Cu6 Se5 Cu3 158.15(6) . .
P11 Cu6 P9 124.37(10) . 3_667
P11 Cu6 Se7 119.71(9) . .
P9 Cu6 Se7 97.05(8) 3_667 .
P11 Cu6 Se5 106.24(8) . .
P9 Cu6 Se5 105.09(8) 3_667 .
Se7 Cu6 Se5 101.56(5) . .
P8 Se7 Cu6 99.39(7) . .
P8 Se7 Cu3 99.54(7) . 3_667
Cu6 Se7 Cu3 92.61(5) . 3_667
C20 P8 C14 102.7(3) . .
C20 P8 Cu1 112.8(2) . .
C14 P8 Cu1 117.0(2) . .
C20 P8 Se7 105.7(2) . .
C14 P8 Se7 105.1(2) . .
Cu1 P8 Se7 112.54(10) . .
C26 P9 C32 104.5(4) . .
C26 P9 Se2 104.5(3) . .
C32 P9 Se2 105.1(3) . .
C26 P9 Cu6 118.9(3) . 3_667
C32 P9 Cu6 112.1(3) . 3_667
Se2 P9 Cu6 110.60(10) . 3_667
C1 Se10 P4 95.0(3) . .
C44 P11 C38 102.9(3) . .
C44 P11 Cu6 119.8(2) . .
C38 P11 Cu6 115.7(2) . .
Se5 C1 Se10 112.5(5) . .
C3 C2 C7 120.0 . .
C3 C2 P4 117.3(5) . .
C7 C2 P4 122.5(5) . .
C2 C3 C4 120.0 . .
C5 C4 C3 120.0 . .
C4 C5 C6 120.0 . .
C5 C6 C7 120.0 . .
C6 C7 C2 120.0 . .
C9 C8 C13 120.0 . .
C9 C8 P4 116.2(5) . .
C13 C8 P4 123.8(5) . .
C10 C9 C8 120.0 . .
C9 C10 C11 120.0 . .
C12 C11 C10 120.0 . .
C11 C12 C13 120.0 . .
C12 C13 C8 120.0 . .
C15 C14 C19 120.0 . .
C15 C14 P8 117.7(3) . .
C19 C14 P8 122.3(3) . .
C14 C15 C16 120.0 . .
C15 C16 C17 120.0 . .
C18 C17 C16 120.0 . .
C17 C18 C19 120.0 . .
C18 C19 C14 120.0 . .
C21 C20 C25 120.0 . .
C21 C20 P8 122.6(4) . .
C25 C20 P8 117.3(4) . .
C22 C21 C20 120.0 . .
C21 C22 C23 120.0 . .
C24 C23 C22 120.0 . .
C23 C24 C25 120.0 . .
C24 C25 C20 120.0 . .
C27 C26 C31 120.0 . .
C27 C26 P9 117.3(4) . .
C31 C26 P9 122.5(4) . .
C26 C27 C28 120.0 . .
C27 C28 C29 120.0 . .
C28 C29 C30 120.0 . .
C31 C30 C29 120.0 . .
C30 C31 C26 120.0 . .
C33 C32 C37 120.0 . .
C33 C32 P9 117.1(5) . .
C37 C32 P9 122.9(5) . .
C32 C33 C34 120.0 . .
C35 C34 C33 120.0 . .
C36 C35 C34 120.0 . .
C37 C36 C35 120.0 . .
C36 C37 C32 120.0 . .
C39 C38 C43 120.0 . .
C39 C38 P11 122.9(4) . .
C43 C38 P11 116.9(4) . .
C38 C39 C40 120.0 . .
C39 C40 C41 120.0 . .
C42 C41 C40 120.0 . .
C41 C42 C43 120.0 . .
C42 C43 C38 120.0 . .
C45 C44 C49 120.0 . .
C45 C44 P11 121.3(4) . .
C49 C44 P11 118.7(4) . .
C46 C45 C44 120.0 . .
C45 C46 C47 120.0 . .
C46 C47 C48 120.0 . .
C49 C48 C47 120.0 . .
C48 C49 C44 120.0 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Cu1 P8 2.212(2) .
Cu1 Se2 2.3471(16) .
Cu1 Se5 2.4027(15) 3_667
Cu1 Cu3 2.8043(18) .
Se2 P9 2.226(3) .
Se2 Cu3 2.4643(16) .
Cu3 P4 2.266(3) .
Cu3 Se7 2.4799(15) 3_667
Cu3 Se5 2.5404(14) .
P4 C8 1.820(6) .
P4 C2 1.833(6) .
P4 Se10 2.236(3) .
Se5 C1 1.937(10) .
Se5 Cu1 2.4027(15) 3_667
Se5 Cu6 2.5244(14) .
Cu6 P11 2.234(3) .
Cu6 P9 2.273(3) 3_667
Cu6 Se7 2.4363(15) .
Se7 P8 2.230(2) .
Se7 Cu3 2.4799(15) 3_667
P8 C20 1.825(5) .
P8 C14 1.827(4) .
P9 C26 1.841(6) .
P9 C32 1.844(6) .
P9 Cu6 2.273(3) 3_667
Se10 C1 1.991(10) .
P11 C44 1.816(5) .
P11 C38 1.816(5) .
C2 C3 1.3900 .
C2 C7 1.3900 .
C3 C4 1.3900 .
C4 C5 1.3900 .
C5 C6 1.3900 .
C6 C7 1.3900 .
C8 C9 1.3900 .
C8 C13 1.3900 .
C9 C10 1.3900 .
C10 C11 1.3900 .
C11 C12 1.3900 .
C12 C13 1.3900 .
C14 C15 1.3900 .
C14 C19 1.3900 .
C15 C16 1.3900 .
C16 C17 1.3900 .
C17 C18 1.3900 .
C18 C19 1.3900 .
C20 C21 1.3900 .
C20 C25 1.3900 .
C21 C22 1.3900 .
C22 C23 1.3900 .
C23 C24 1.3900 .
C24 C25 1.3900 .
C26 C27 1.3900 .
C26 C31 1.3900 .
C27 C28 1.3900 .
C28 C29 1.3900 .
C29 C30 1.3900 .
C30 C31 1.3900 .
C32 C33 1.3900 .
C32 C37 1.3900 .
C33 C34 1.3900 .
C34 C35 1.3900 .
C35 C36 1.3900 .
C36 C37 1.3900 .
C38 C39 1.3900 .
C38 C43 1.3900 .
C39 C40 1.3900 .
C40 C41 1.3900 .
C41 C42 1.3900 .
C42 C43 1.3900 .
C44 C45 1.3900 .
C44 C49 1.3900 .
C45 C46 1.3900 .
C46 C47 1.3900 .
C47 C48 1.3900 .
C48 C49 1.3900 .
