#------------------------------------------------------------------------------
#$Date: 2018-08-16 01:09:46 +0300 (Thu, 16 Aug 2018) $
#$Revision: 209740 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/10/38/7103862.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7103862
loop_
_publ_author_name
'Wei, Qiao-Hua'
'Yin, Gang-Qiang'
'Ma, Zhen'
'Shi, Lin-Xi'
'Chen, Zhong-Ning'
_publ_section_title
;
 Luminescent heterohexanuclear complexes with platinum alkynyl and silver
 diphosphine as components
;
_journal_coden_ASTM              CHCOFS
_journal_issue                   17
_journal_name_full
;
 Chemical Communications (Cambridge, United Kingdom)
;
_journal_page_first              2188
_journal_page_last               2189
_journal_paper_doi               10.1039/b305284b
_journal_year                    2003
_chemical_formula_sum            'C129 H114 Ag4 N4 O6 P8 Pt2'
_chemical_formula_weight         2885.66
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 103.8360(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   18.5759(3)
_cell_length_b                   22.4019(3)
_cell_length_c                   29.97010(10)
_cell_measurement_reflns_used    7654
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      22.50
_cell_measurement_theta_min      1.15
_cell_volume                     12109.7(3)
_computing_cell_refinement       'Siemens SMART & SAINT'
_computing_data_collection       'Siemens SMART'
_computing_data_reduction        'Siemens XPREP'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'Siemens SHELXTL'
_computing_structure_solution    'Siemens SHELXTL'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Siemens SMART CCD'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0546
_diffrn_reflns_av_sigmaI/netI    0.0600
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_l_max       32
_diffrn_reflns_limit_l_min       -31
_diffrn_reflns_number            30665
_diffrn_reflns_theta_full        22.50
_diffrn_reflns_theta_max         22.50
_diffrn_reflns_theta_min         1.15
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  .
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    3.097
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  .6084
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   'SADABS (Sheldrick, 1996)'
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.583
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             5712
_exptl_crystal_size_max          .68
_exptl_crystal_size_mid          .60
_exptl_crystal_size_min          .36
_refine_diff_density_max         1.664
_refine_diff_density_min         -2.308
_refine_diff_density_rms         0.246
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.276
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1373
_refine_ls_number_reflns         15810
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.276
_refine_ls_R_factor_all          0.1116
_refine_ls_R_factor_gt           0.0681
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w==1/[σ²(Fo²)+(0.0514P)²+224.1118P] where P==(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1596
_refine_ls_wR_factor_ref         0.2030
_reflns_number_gt                11380
_reflns_number_total             15810
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b305284b.txt
_cod_data_source_block           1
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P2(1)/n
_cod_database_code               7103862
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 1.01129(3) 0.24901(3) 0.33646(2) 0.03706(19) Uani 1 1 d . . .
Pt2 Pt 1.08333(3) 0.27294(3) 0.25295(2) 0.03663(19) Uani 1 1 d . . .
Ag1 Ag 0.89981(8) 0.19345(7) 0.37591(5) 0.0586(4) Uani 1 1 d . . .
Ag2 Ag 1.03346(8) 0.26889(6) 0.43573(5) 0.0542(4) Uani 1 1 d . . .
Ag3 Ag 1.06796(8) 0.25121(7) 0.15456(5) 0.0596(4) Uani 1 1 d . . .
Ag4 Ag 1.20713(8) 0.33072(7) 0.22542(5) 0.0570(4) Uani 1 1 d . . .
P2 P 1.1478(2) 0.18309(19) 0.27264(15) 0.0402(10) Uani 1 1 d . . .
P1 P 1.1067(2) 0.17806(19) 0.36127(15) 0.0410(10) Uani 1 1 d . . .
P4 P 1.0140(2) 0.36124(19) 0.24108(15) 0.0410(10) Uani 1 1 d . . .
P3 P 0.9237(2) 0.32217(19) 0.30344(14) 0.0385(10) Uani 1 1 d . . .
P5 P 0.8557(3) 0.1940(2) 0.44423(17) 0.0547(13) Uani 1 1 d . . .
P6 P 0.9912(3) 0.2404(2) 0.50048(16) 0.0521(12) Uani 1 1 d . . .
P7 P 1.2432(3) 0.3488(2) 0.15631(18) 0.0565(13) Uani 1 1 d . . .
P8 P 1.1475(3) 0.2599(2) 0.10358(18) 0.0608(14) Uani 1 1 d . . .
O1 O 0.9412(13) 0.0841(19) 0.0537(15) 0.32(3) Uani 1 1 d D . .
O2 O 1.633(2) 0.4785(12) 0.3978(16) 0.44(4) Uani 1 1 d . . .
O3 O 1.6124(15) 0.3952(14) 0.3111(10) 0.204(13) Uani 1 1 d . . .
O4 O 0.5836(13) 0.1214(16) 0.3223(11) 0.209(14) Uani 1 1 d . . .
O5 O 0.5547(15) 0.1015(18) 0.250(2) 0.39(4) Uani 1 1 d . . .
O6 O 0.526(3) 0.063(2) 0.3647(17) 0.34(2) Uiso 1 1 d . . .
N1 N 1.1544(7) 0.1648(6) 0.3246(4) 0.040(3) Uani 1 1 d . . .
N2 N 0.9436(7) 0.3612(6) 0.2631(5) 0.045(3) Uani 1 1 d . . .
N3 N 0.9102(8) 0.2084(7) 0.4924(5) 0.060(4) Uani 1 1 d . . .
N4 N 1.2160(9) 0.3062(7) 0.1133(5) 0.064(5) Uani 1 1 d . . .
C01 C 0.9441(19) 0.0250(17) 0.0370(11) 0.30(4) Uani 1 1 d D . .
C11 C 0.9443(9) 0.1814(9) 0.3107(5) 0.049(5) Uani 1 1 d . . .
C12 C 0.8983(10) 0.1412(9) 0.3010(6) 0.051(5) Uani 1 1 d . . .
C13 C 0.8552(11) 0.0873(9) 0.2905(6) 0.056(5) Uani 1 1 d . . .
C14 C 0.7823(12) 0.0899(11) 0.2733(9) 0.090(8) Uani 1 1 d . . .
H14F H 0.7584 0.1265 0.2669 0.109 Uiso 1 1 calc R . .
C15 C 0.7417(15) 0.0359(15) 0.2648(11) 0.124(11) Uani 1 1 d . . .
H15F H 0.6906 0.0378 0.2533 0.149 Uiso 1 1 calc R . .
C16 C 0.7731(19) -0.0165(12) 0.2724(12) 0.125(12) Uani 1 1 d . . .
H16F H 0.7458 -0.0514 0.2649 0.150 Uiso 1 1 calc R . .
C17 C 0.845(2) -0.0180(14) 0.2913(11) 0.128(11) Uani 1 1 d . . .
H17F H 0.8683 -0.0548 0.2984 0.153 Uiso 1 1 calc R . .
C18 C 0.8869(14) 0.0336(11) 0.3006(10) 0.104(9) Uani 1 1 d . . .
H18F H 0.9374 0.0311 0.3139 0.124 Uiso 1 1 calc R . .
C21 C 1.0691(9) 0.3126(7) 0.3749(6) 0.043(4) Uani 1 1 d . . .
C22 C 1.0959(9) 0.3506(8) 0.4039(6) 0.047(4) Uani 1 1 d . . .
C23 C 1.1282(10) 0.3977(8) 0.4362(5) 0.048(4) Uani 1 1 d . . .
C24 C 1.1985(11) 0.3918(10) 0.4630(7) 0.074(6) Uani 1 1 d . . .
H23F H 1.2263 0.3578 0.4611 0.088 Uiso 1 1 calc R . .
C25 C 1.2271(14) 0.4373(12) 0.4927(7) 0.082(7) Uani 1 1 d . . .
H24F H 1.2737 0.4326 0.5123 0.099 Uiso 1 1 calc R . .
C26 C 1.1892(17) 0.4893(11) 0.4944(8) 0.087(8) Uani 1 1 d . . .
H25F H 1.2105 0.5208 0.5132 0.104 Uiso 1 1 calc R . .
C27 C 1.1200(15) 0.4929(9) 0.4678(8) 0.076(6) Uani 1 1 d . . .
H26F H 1.0921 0.5266 0.4702 0.091 Uiso 1 1 calc R . .
C28 C 1.0891(11) 0.4497(9) 0.4377(7) 0.062(5) Uani 1 1 d . . .
H27A H 1.0423 0.4550 0.4184 0.074 Uiso 1 1 calc R . .
C31 C 0.9970(11) 0.2353(7) 0.2055(6) 0.049(5) Uani 1 1 d . . .
C32 C 0.9505(9) 0.2130(8) 0.1778(6) 0.049(5) Uani 1 1 d . . .
C33 C 0.8839(10) 0.1869(9) 0.1511(6) 0.056(5) Uani 1 1 d . . .
C34 C 0.8523(12) 0.1375(10) 0.1686(7) 0.075(6) Uani 1 1 d . . .
H33A H 0.8748 0.1202 0.1966 0.089 Uiso 1 1 calc R . .
C35 C 0.7863(13) 0.1160(12) 0.1420(10) 0.095(8) Uani 1 1 d . . .
H34A H 0.7642 0.0838 0.1531 0.114 Uiso 1 1 calc R . .
C36 C 0.7524(15) 0.1386(15) 0.1015(10) 0.106(9) Uani 1 1 d . . .
H35A H 0.7083 0.1219 0.0849 0.127 Uiso 1 1 calc R . .
C37 C 0.7813(18) 0.1850(15) 0.0849(10) 0.118(10) Uani 1 1 d . . .
H36A H 0.7575 0.2003 0.0563 0.142 Uiso 1 1 calc R . .
C38 C 0.8465(14) 0.2114(12) 0.1091(8) 0.090(7) Uani 1 1 d . . .
H37A H 0.8651 0.2450 0.0975 0.108 Uiso 1 1 calc R . .
C41 C 1.1704(9) 0.3128(8) 0.2911(5) 0.042(4) Uani 1 1 d . . .
C42 C 1.2293(10) 0.3359(7) 0.3110(6) 0.042(4) Uani 1 1 d . . .
C43 C 1.2967(10) 0.3578(7) 0.3417(6) 0.046(4) Uani 1 1 d . . .
C44 C 1.3658(13) 0.3397(10) 0.3373(9) 0.084(7) Uani 1 1 d . . .
H43A H 1.3698 0.3160 0.3125 0.100 Uiso 1 1 calc R . .
C45 C 1.4305(13) 0.3570(14) 0.3704(11) 0.109(10) Uani 1 1 d . . .
H44A H 1.4771 0.3429 0.3691 0.131 Uiso 1 1 calc R . .
C46 C 1.4219(18) 0.3948(13) 0.4039(10) 0.107(10) Uani 1 1 d . . .
H45A H 1.4638 0.4079 0.4253 0.128 Uiso 1 1 calc R . .
C47 C 1.3553(17) 0.4142(11) 0.4073(9) 0.093(8) Uani 1 1 d . . .
H46A H 1.3511 0.4390 0.4314 0.111 Uiso 1 1 calc R . .
C48 C 1.2948(11) 0.3976(9) 0.3758(7) 0.063(5) Uani 1 1 d . . .
H47A H 1.2494 0.4140 0.3771 0.075 Uiso 1 1 calc R . .
C111 C 1.1142(11) 0.1158(8) 0.2384(7) 0.054(5) Uani 1 1 d . . .
C112 C 1.0451(12) 0.0966(9) 0.2384(6) 0.063(5) Uani 1 1 d . . .
H11A H 1.0148 0.1202 0.2518 0.075 Uiso 1 1 calc R . .
C113 C 1.0188(15) 0.0430(11) 0.2192(8) 0.091(8) Uani 1 1 d . . .
H11B H 0.9708 0.0314 0.2193 0.110 Uiso 1 1 calc R . .
C114 C 1.0604(19) 0.0073(12) 0.2003(10) 0.113(10) Uani 1 1 d . . .
H11C H 1.0417 -0.0285 0.1866 0.136 Uiso 1 1 calc R . .
C115 C 1.1305(18) 0.0242(11) 0.2016(10) 0.113(10) Uani 1 1 d . . .
H11D H 1.1615 -0.0012 0.1902 0.136 Uiso 1 1 calc R . .
C116 C 1.1568(16) 0.0789(11) 0.2196(10) 0.106(9) Uani 1 1 d . . .
H11E H 1.2044 0.0907 0.2187 0.128 Uiso 1 1 calc R . .
C121 C 1.2432(9) 0.1889(7) 0.2681(6) 0.043(4) Uani 1 1 d . . .
C122 C 1.3017(10) 0.1818(8) 0.3049(7) 0.057(5) Uani 1 1 d . . .
H12A H 1.2929 0.1739 0.3336 0.068 Uiso 1 1 calc R . .
C123 C 1.3724(12) 0.1860(10) 0.3007(9) 0.081(7) Uani 1 1 d . . .
H12B H 1.4116 0.1811 0.3263 0.097 Uiso 1 1 calc R . .
C124 C 1.3863(14) 0.1977(10) 0.2581(11) 0.093(9) Uani 1 1 d . . .
H12C H 1.4350 0.1996 0.2552 0.111 Uiso 1 1 calc R . .
C125 C 1.3315(13) 0.2061(9) 0.2218(9) 0.075(7) Uani 1 1 d . . .
H12D H 1.3418 0.2164 0.1939 0.090 Uiso 1 1 calc R . .
C126 C 1.2602(10) 0.1998(8) 0.2247(7) 0.058(5) Uani 1 1 d . . .
H12E H 1.2221 0.2025 0.1982 0.070 Uiso 1 1 calc R . .
C131 C 1.0756(10) 0.1054(8) 0.3770(7) 0.054(5) Uani 1 1 d . . .
C132 C 1.0329(10) 0.0988(8) 0.4085(6) 0.057(5) Uani 1 1 d . . .
H13A H 1.0173 0.1326 0.4217 0.068 Uiso 1 1 calc R . .
C133 C 1.0128(12) 0.0433(9) 0.4209(8) 0.075(7) Uani 1 1 d . . .
H13B H 0.9829 0.0398 0.4416 0.090 Uiso 1 1 calc R . .
C134 C 1.0366(13) -0.0065(10) 0.4029(8) 0.082(7) Uani 1 1 d . . .
H13C H 1.0237 -0.0440 0.4118 0.099 Uiso 1 1 calc R . .
C135 C 1.0801(13) -0.0015(9) 0.3712(8) 0.078(7) Uani 1 1 d . . .
H13D H 1.0969 -0.0354 0.3590 0.093 Uiso 1 1 calc R . .
C136 C 1.0980(11) 0.0541(8) 0.3583(7) 0.063(5) Uani 1 1 d . . .
H13E H 1.1258 0.0576 0.3364 0.075 Uiso 1 1 calc R . .
C141 C 1.1759(8) 0.1973(8) 0.4118(5) 0.042(4) Uani 1 1 d . . .
C142 C 1.2316(9) 0.2374(9) 0.4072(6) 0.058(5) Uani 1 1 d . . .
H14A H 1.2288 0.2556 0.3789 0.069 Uiso 1 1 calc R . .
C143 C 1.2901(11) 0.2504(10) 0.4434(7) 0.070(6) Uani 1 1 d . . .
H14B H 1.3263 0.2770 0.4389 0.083 Uiso 1 1 calc R . .
C144 C 1.2969(13) 0.2260(12) 0.4854(9) 0.086(7) Uani 1 1 d . . .
H14C H 1.3364 0.2357 0.5098 0.103 Uiso 1 1 calc R . .
C145 C 1.2424(16) 0.1853(13) 0.4909(7) 0.101(9) Uani 1 1 d . . .
H14D H 1.2464 0.1671 0.5192 0.122 Uiso 1 1 calc R . .
C146 C 1.1833(11) 0.1719(10) 0.4553(6) 0.067(6) Uani 1 1 d . . .
H14E H 1.1474 0.1453 0.4601 0.080 Uiso 1 1 calc R . .
C151 C 0.9750(10) 0.3746(8) 0.1797(6) 0.051(5) Uani 1 1 d . . .
C152 C 1.0197(11) 0.3793(8) 0.1486(6) 0.056(5) Uani 1 1 d . . .
H15A H 1.0710 0.3782 0.1592 0.067 Uiso 1 1 calc R . .
C153 C 0.9879(12) 0.3856(10) 0.1014(6) 0.070(6) Uani 1 1 d . . .
H15B H 1.0181 0.3869 0.0808 0.084 Uiso 1 1 calc R . .
C154 C 0.9145(13) 0.3897(12) 0.0861(8) 0.087(7) Uani 1 1 d . . .
H15C H 0.8937 0.3941 0.0548 0.105 Uiso 1 1 calc R . .
C155 C 0.8700(13) 0.3874(11) 0.1163(7) 0.080(7) Uani 1 1 d . . .
H15D H 0.8189 0.3899 0.1054 0.096 Uiso 1 1 calc R . .
C156 C 0.9006(11) 0.3812(9) 0.1640(7) 0.065(6) Uani 1 1 d . . .
H15E H 0.8700 0.3817 0.1844 0.078 Uiso 1 1 calc R . .
C161 C 1.0659(9) 0.4291(7) 0.2614(6) 0.047(4) Uani 1 1 d . . .
C162 C 1.0755(12) 0.4459(9) 0.3068(6) 0.067(6) Uani 1 1 d . . .
H16A H 1.0555 0.4219 0.3260 0.080 Uiso 1 1 calc R . .
C163 C 1.1125(12) 0.4954(9) 0.3243(7) 0.076(7) Uani 1 1 d . . .
H16B H 1.1164 0.5051 0.3550 0.091 Uiso 1 1 calc R . .
C164 C 1.1438(13) 0.5309(10) 0.2984(8) 0.080(7) Uani 1 1 d . . .
H16C H 1.1682 0.5657 0.3105 0.096 Uiso 1 1 calc R . .
C165 C 1.1391(15) 0.5151(11) 0.2534(9) 0.101(9) Uani 1 1 d . . .
H16D H 1.1616 0.5387 0.2351 0.121 Uiso 1 1 calc R . .
C166 C 1.1011(15) 0.4639(10) 0.2352(8) 0.095(8) Uani 1 1 d . . .
H16E H 1.0993 0.4530 0.2050 0.114 Uiso 1 1 calc R . .
C171 C 0.8307(9) 0.2930(7) 0.2770(6) 0.044(4) Uani 1 1 d . . .
C172 C 0.8156(10) 0.2699(9) 0.2328(7) 0.062(5) Uani 1 1 d . . .
H17A H 0.8533 0.2695 0.2172 0.074 Uiso 1 1 calc R . .
C173 C 0.7474(12) 0.2478(9) 0.2112(7) 0.070(6) Uani 1 1 d . . .
H17B H 0.7393 0.2324 0.1816 0.084 Uiso 1 1 calc R . .
C174 C 0.6927(13) 0.2484(11) 0.2330(9) 0.086(7) Uani 1 1 d . . .
H17C H 0.6457 0.2352 0.2180 0.103 Uiso 1 1 calc R . .
C175 C 0.7054(14) 0.2685(15) 0.2776(11) 0.127(12) Uani 1 1 d . . .
H17D H 0.6673 0.2684 0.2929 0.152 Uiso 1 1 calc R . .
C176 C 0.7756(13) 0.2890(14) 0.2997(9) 0.114(11) Uani 1 1 d . . .
H17E H 0.7850 0.3002 0.3305 0.137 Uiso 1 1 calc R . .
C181 C 0.9030(9) 0.3773(7) 0.3433(6) 0.047(4) Uani 1 1 d . . .
C182 C 0.8906(10) 0.4340(8) 0.3295(6) 0.054(5) Uani 1 1 d . . .
H18A H 0.8960 0.4456 0.3007 0.064 Uiso 1 1 calc R . .
C183 C 0.8696(13) 0.4756(9) 0.3586(8) 0.078(7) Uani 1 1 d . . .
H18B H 0.8634 0.5154 0.3495 0.094 Uiso 1 1 calc R . .
C184 C 0.8580(13) 0.4595(11) 0.3995(9) 0.089(8) Uani 1 1 d . . .
H18C H 0.8420 0.4876 0.4178 0.107 Uiso 1 1 calc R . .
C185 C 0.8700(13) 0.4008(10) 0.4146(7) 0.079(7) Uani 1 1 d . . .
H18D H 0.8640 0.3891 0.4433 0.095 Uiso 1 1 calc R . .
C186 C 0.8916(10) 0.3598(8) 0.3847(7) 0.060(5) Uani 1 1 d . . .
H18E H 0.8982 0.3199 0.3933 0.072 Uiso 1 1 calc R . .
C191 C 0.7732(12) 0.2423(9) 0.4366(7) 0.066(6) Uani 1 1 d . . .
C192 C 0.7699(13) 0.2839(12) 0.4703(8) 0.086(7) Uani 1 1 d . . .
H19A H 0.8086 0.2873 0.4964 0.104 Uiso 1 1 calc R . .
C193 C 0.7062(18) 0.3214(13) 0.4643(12) 0.113(10) Uani 1 1 d . . .
H19B H 0.7028 0.3497 0.4863 0.136 Uiso 1 1 calc R . .
C194 C 0.652(2) 0.3153(18) 0.4269(13) 0.132(13) Uani 1 1 d . . .
H19C H 0.6109 0.3402 0.4226 0.159 Uiso 1 1 calc R . .
C195 C 0.6554(16) 0.2734(19) 0.3948(12) 0.142(14) Uani 1 1 d . . .
H19D H 0.6157 0.2688 0.3694 0.170 Uiso 1 1 calc R . .
C196 C 0.7173(14) 0.2378(14) 0.3996(9) 0.105(9) Uani 1 1 d . . .
H19E H 0.7200 0.2104 0.3767 0.126 Uiso 1 1 calc R . .
C201 C 0.8179(10) 0.1195(8) 0.4518(7) 0.055(5) Uani 1 1 d . . .
C202 C 0.8232(13) 0.0971(10) 0.4942(8) 0.081(7) Uani 1 1 d . . .
H20A H 0.8457 0.1193 0.5200 0.097 Uiso 1 1 calc R . .
C203 C 0.7952(16) 0.0410(13) 0.4992(11) 0.114(10) Uani 1 1 d . . .
H20B H 0.8022 0.0240 0.5282 0.137 Uiso 1 1 calc R . .
C204 C 0.7566(18) 0.0104(12) 0.4607(14) 0.120(11) Uani 1 1 d . . .
H20C H 0.7339 -0.0259 0.4637 0.144 Uiso 1 1 calc R . .
C205 C 0.753(2) 0.0337(12) 0.4199(13) 0.134(12) Uani 1 1 d . . .
H20D H 0.7276 0.0128 0.3940 0.161 Uiso 1 1 calc R . .
C206 C 0.7845(14) 0.0882(10) 0.4142(8) 0.088(7) Uani 1 1 d . . .
H20E H 0.7829 0.1028 0.3849 0.105 Uiso 1 1 calc R . .
C211 C 0.9924(10) 0.3041(8) 0.5383(6) 0.055(5) Uani 1 1 d . . .
C212 C 1.0301(12) 0.3552(8) 0.5333(7) 0.067(6) Uani 1 1 d . . .
H21A H 1.0525 0.3590 0.5088 0.081 Uiso 1 1 calc R . .
C213 C 1.0348(14) 0.4004(12) 0.5644(10) 0.097(8) Uani 1 1 d . . .
H21B H 1.0592 0.4354 0.5601 0.117 Uiso 1 1 calc R . .
C215 C 0.9692(16) 0.3448(13) 0.6070(8) 0.098(8) Uani 1 1 d . . .
H21C H 0.9499 0.3405 0.6327 0.118 Uiso 1 1 calc R . .
C216 C 1.0051(16) 0.3961(12) 0.6011(10) 0.101(9) Uani 1 1 d . . .
H21D H 1.0092 0.4274 0.6220 0.122 Uiso 1 1 calc R . .
C217 C 0.9608(12) 0.2991(10) 0.5755(7) 0.072(6) Uani 1 1 d . . .
H21E H 0.9341 0.2651 0.5791 0.086 Uiso 1 1 calc R . .
C221 C 1.0569(11) 0.1905(8) 0.5396(6) 0.056(5) Uani 1 1 d . . .
C222 C 1.0471(13) 0.1304(10) 0.5325(9) 0.087(7) Uani 1 1 d . . .
H22A H 1.0068 0.1163 0.5103 0.104 Uiso 1 1 calc R . .
C223 C 1.0957(16) 0.0917(12) 0.5577(14) 0.116(11) Uani 1 1 d . . .
H22B H 1.0907 0.0511 0.5513 0.139 Uiso 1 1 calc R . .
C224 C 1.1521(19) 0.1113(14) 0.5925(11) 0.106(9) Uani 1 1 d . . .
H22C H 1.1829 0.0840 0.6113 0.127 Uiso 1 1 calc R . .
C225 C 1.1633(16) 0.1707(18) 0.5996(10) 0.123(11) Uani 1 1 d . . .
H22D H 1.2032 0.1844 0.6223 0.148 Uiso 1 1 calc R . .
C226 C 1.1145(14) 0.2110(13) 0.5727(9) 0.103(9) Uani 1 1 d . . .
H22E H 1.1215 0.2518 0.5774 0.124 Uiso 1 1 calc R . .
C231 C 1.3429(12) 0.3489(9) 0.1675(7) 0.064(5) Uani 1 1 d . . .
C232 C 1.3852(15) 0.3638(13) 0.2094(10) 0.105(9) Uani 1 1 d . . .
H23A H 1.3611 0.3746 0.2320 0.126 Uiso 1 1 calc R . .
C233 C 1.4647(18) 0.3639(15) 0.2213(13) 0.130(11) Uani 1 1 d . . .
H23B H 1.4917 0.3742 0.2505 0.156 Uiso 1 1 calc R . .
C234 C 1.4984(18) 0.3479(14) 0.1872(16) 0.126(12) Uani 1 1 d . . .
H23C H 1.5498 0.3452 0.1935 0.152 Uiso 1 1 calc R . .
C235 C 1.4570(16) 0.3358(12) 0.1440(13) 0.105(10) Uani 1 1 d . . .
H23D H 1.4808 0.3278 0.1207 0.126 Uiso 1 1 calc R . .
C236 C 1.3799(13) 0.3352(9) 0.1342(9) 0.084(7) Uani 1 1 d . . .
H23E H 1.3531 0.3254 0.1048 0.101 Uiso 1 1 calc R . .
C241 C 1.2209(11) 0.4248(8) 0.1353(7) 0.059(6) Uani 1 1 d . . .
C242 C 1.2380(14) 0.4720(10) 0.1668(9) 0.090(7) Uani 1 1 d . . .
H24A H 1.2595 0.4634 0.1974 0.108 Uiso 1 1 calc R . .
C243 C 1.2243(17) 0.5301(11) 0.1540(13) 0.106(10) Uani 1 1 d . . .
H24B H 1.2361 0.5608 0.1754 0.128 Uiso 1 1 calc R . .
C244 C 1.194(2) 0.5417(13) 0.1100(13) 0.117(11) Uani 1 1 d . . .
H24C H 1.1836 0.5811 0.1006 0.141 Uiso 1 1 calc R . .
C245 C 1.177(2) 0.4972(16) 0.0787(13) 0.156(15) Uani 1 1 d . . .
H24D H 1.1550 0.5055 0.0480 0.187 Uiso 1 1 calc R . .
C246 C 1.1916(19) 0.4402(12) 0.0931(10) 0.119(11) Uani 1 1 d . . .
H24E H 1.1802 0.4100 0.0712 0.143 Uiso 1 1 calc R . .
C251 C 1.1864(10) 0.1846(8) 0.0969(6) 0.053(5) Uani 1 1 d . . .
C252 C 1.2512(13) 0.1780(11) 0.0885(9) 0.090(8) Uani 1 1 d . . .
H25A H 1.2806 0.2110 0.0865 0.107 Uiso 1 1 calc R . .
C253 C 1.2753(15) 0.1218(13) 0.0826(10) 0.101(9) Uani 1 1 d . . .
H25B H 1.3218 0.1179 0.0764 0.122 Uiso 1 1 calc R . .
C254 C 1.2376(17) 0.0728(14) 0.0850(10) 0.104(9) Uani 1 1 d . . .
H25C H 1.2566 0.0351 0.0815 0.125 Uiso 1 1 calc R . .
C255 C 1.171(2) 0.0804(10) 0.0928(14) 0.151(15) Uani 1 1 d . . .
H25D H 1.1419 0.0472 0.0947 0.181 Uiso 1 1 calc R . .
C256 C 1.1440(17) 0.1369(12) 0.0981(14) 0.156(17) Uani 1 1 d . . .
H25E H 1.0964 0.1415 0.1025 0.187 Uiso 1 1 calc R . .
C261 C 1.0947(15) 0.2745(14) 0.0445(8) 0.098(9) Uani 1 1 d . . .
C262 C 1.0247(17) 0.257(3) 0.0277(12) 0.25(3) Uani 1 1 d . . .
H26A H 1.0001 0.2356 0.0463 0.297 Uiso 1 1 calc R . .
C263 C 0.990(3) 0.269(5) -0.0161(15) 0.42(8) Uani 1 1 d . . .
H26B H 0.9397 0.2601 -0.0260 0.500 Uiso 1 1 calc R . .
C264 C 1.018(3) 0.290(4) -0.0409(16) 0.32(6) Uani 1 1 d . . .
H26C H 0.9931 0.2902 -0.0717 0.381 Uiso 1 1 calc R . .
C265 C 1.088(3) 0.315(2) -0.0292(11) 0.20(3) Uani 1 1 d . . .
H26D H 1.1074 0.3377 -0.0496 0.239 Uiso 1 1 calc R . .
C266 C 1.126(2) 0.3045(13) 0.0157(10) 0.126(11) Uani 1 1 d . . .
H26E H 1.1745 0.3183 0.0259 0.152 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C21 Pt1 C11 166.7(6) . . ?
C21 Pt1 P3 88.2(5) . . ?
C11 Pt1 P3 93.5(5) . . ?
C21 Pt1 P1 92.3(5) . . ?
C11 Pt1 P1 87.9(5) . . ?
P3 Pt1 P1 172.28(14) . . ?
C21 Pt1 Ag1 114.4(5) . . ?
C11 Pt1 Ag1 52.5(4) . . ?
P3 Pt1 Ag1 88.90(11) . . ?
P1 Pt1 Ag1 97.94(11) . . ?
C21 Pt1 Ag2 51.4(5) . . ?
C11 Pt1 Ag2 115.5(4) . . ?
P3 Pt1 Ag2 103.62(11) . . ?
P1 Pt1 Ag2 82.56(11) . . ?
Ag1 Pt1 Ag2 65.98(4) . . ?
C21 Pt1 Pt2 93.8(5) . . ?
C11 Pt1 Pt2 99.5(4) . . ?
P3 Pt1 Pt2 85.99(10) . . ?
P1 Pt1 Pt2 86.29(10) . . ?
Ag1 Pt1 Pt2 151.24(4) . . ?
Ag2 Pt1 Pt2 142.61(4) . . ?
C41 Pt2 C31 172.3(6) . . ?
C41 Pt2 P4 92.9(5) . . ?
C31 Pt2 P4 86.1(4) . . ?
C41 Pt2 P2 86.8(5) . . ?
C31 Pt2 P2 95.1(4) . . ?
P4 Pt2 P2 173.32(15) . . ?
C41 Pt2 Ag4 50.8(4) . . ?
C31 Pt2 Ag4 121.6(5) . . ?
P4 Pt2 Ag4 91.39(11) . . ?
P2 Pt2 Ag4 93.57(11) . . ?
C41 Pt2 Ag3 122.1(4) . . ?
C31 Pt2 Ag3 50.5(5) . . ?
P4 Pt2 Ag3 94.00(11) . . ?
P2 Pt2 Ag3 91.81(11) . . ?
Ag4 Pt2 Ag3 71.58(4) . . ?
C41 Pt2 Pt1 93.5(4) . . ?
C31 Pt2 Pt1 94.0(5) . . ?
P4 Pt2 Pt1 86.66(10) . . ?
P2 Pt2 Pt1 86.70(10) . . ?
Ag4 Pt2 Pt1 144.17(4) . . ?
Ag3 Pt2 Pt1 144.25(4) . . ?
C11 Ag1 P5 173.5(5) . . ?
C11 Ag1 C12 28.9(6) . . ?
P5 Ag1 C12 146.5(5) . . ?
C11 Ag1 Pt1 43.2(5) . . ?
P5 Ag1 Pt1 140.81(14) . . ?
C12 Ag1 Pt1 72.1(4) . . ?
C11 Ag1 Ag2 98.6(5) . . ?
P5 Ag1 Ag2 84.00(13) . . ?
C12 Ag1 Ag2 126.0(4) . . ?
Pt1 Ag1 Ag2 57.59(4) . . ?
C21 Ag2 P6 170.4(4) . . ?
C21 Ag2 C22 29.7(5) . . ?
P6 Ag2 C22 143.0(5) . . ?
C21 Ag2 Pt1 42.2(4) . . ?
P6 Ag2 Pt1 143.30(13) . . ?
C22 Ag2 Pt1 71.8(4) . . ?
C21 Ag2 Ag1 96.5(4) . . ?
P6 Ag2 Ag1 87.20(13) . . ?
C22 Ag2 Ag1 123.4(4) . . ?
Pt1 Ag2 Ag1 56.42(4) . . ?
C31 Ag3 P8 175.0(4) . . ?
C31 Ag3 C32 26.6(6) . . ?
P8 Ag3 C32 153.4(4) . . ?
C31 Ag3 Pt2 44.2(5) . . ?
P8 Ag3 Pt2 135.02(14) . . ?
C32 Ag3 Pt2 70.8(4) . . ?
C41 Ag4 P7 179.0(5) . . ?
C41 Ag4 C42 29.3(5) . . ?
P7 Ag4 C42 151.7(4) . . ?
C41 Ag4 Pt2 42.0(4) . . ?
P7 Ag4 Pt2 136.97(14) . . ?
C42 Ag4 Pt2 71.3(4) . . ?
N1 P2 C121 104.1(8) . . ?
N1 P2 C111 105.7(8) . . ?
C121 P2 C111 103.0(8) . . ?
N1 P2 Pt2 112.6(5) . . ?
C121 P2 Pt2 111.6(5) . . ?
C111 P2 Pt2 118.5(7) . . ?
N1 P1 C141 102.9(7) . . ?
N1 P1 C131 105.9(7) . . ?
C141 P1 C131 101.7(9) . . ?
N1 P1 Pt1 114.0(5) . . ?
C141 P1 Pt1 115.9(5) . . ?
C131 P1 Pt1 114.9(6) . . ?
N2 P4 C161 106.4(7) . . ?
N2 P4 C151 104.4(8) . . ?
C161 P4 C151 104.4(8) . . ?
N2 P4 Pt2 114.3(5) . . ?
C161 P4 Pt2 115.2(6) . . ?
C151 P4 Pt2 111.2(6) . . ?
N2 P3 C181 104.3(7) . . ?
N2 P3 C171 103.3(8) . . ?
C181 P3 C171 101.6(8) . . ?
N2 P3 Pt1 115.8(5) . . ?
C181 P3 Pt1 115.4(6) . . ?
C171 P3 Pt1 114.7(5) . . ?
N3 P5 C201 104.5(9) . . ?
N3 P5 C191 108.9(10) . . ?
C201 P5 C191 102.5(9) . . ?
N3 P5 Ag1 120.5(5) . . ?
C201 P5 Ag1 108.7(6) . . ?
C191 P5 Ag1 110.1(7) . . ?
N3 P6 C211 108.1(8) . . ?
N3 P6 C221 105.8(9) . . ?
C211 P6 C221 99.8(9) . . ?
N3 P6 Ag2 118.4(6) . . ?
C211 P6 Ag2 110.2(6) . . ?
C221 P6 Ag2 112.7(6) . . ?
N4 P7 C231 105.4(9) . . ?
N4 P7 C241 106.2(10) . . ?
C231 P7 C241 101.5(9) . . ?
N4 P7 Ag4 120.6(6) . . ?
C231 P7 Ag4 109.4(7) . . ?
C241 P7 Ag4 111.9(6) . . ?
N4 P8 C261 106.0(12) . . ?
N4 P8 C251 106.9(9) . . ?
C261 P8 C251 100.9(10) . . ?
N4 P8 Ag3 121.5(6) . . ?
C261 P8 Ag3 111.4(8) . . ?
C251 P8 Ag3 108.2(7) . . ?
P2 N1 P1 134.6(9) . . ?
P4 N2 P3 132.0(9) . . ?
P5 N3 P6 126.2(9) . . ?
P7 N4 P8 128.0(9) . . ?
C12 C11 Pt1 169.5(14) . . ?
C12 C11 Ag1 85.3(11) . . ?
Pt1 C11 Ag1 84.3(6) . . ?
C11 C12 C13 170.2(19) . . ?
C11 C12 Ag1 65.8(11) . . ?
C13 C12 Ag1 118.0(12) . . ?
C14 C13 C18 119(2) . . ?
C14 C13 C12 120.6(19) . . ?
C18 C13 C12 120.7(19) . . ?
C13 C14 C15 119(2) . . ?
C16 C15 C14 123(3) . . ?
C15 C16 C17 117(3) . . ?
C16 C17 C18 122(3) . . ?
C13 C18 C17 121(2) . . ?
C22 C21 Pt1 168.1(14) . . ?
C22 C21 Ag2 83.1(12) . . ?
Pt1 C21 Ag2 86.3(6) . . ?
C21 C22 C23 176.9(18) . . ?
C21 C22 Ag2 67.2(11) . . ?
C23 C22 Ag2 115.8(11) . . ?
C24 C23 C28 120.0(18) . . ?
C24 C23 C22 120.2(18) . . ?
C28 C23 C22 119.7(17) . . ?
C23 C24 C25 118(2) . . ?
C26 C25 C24 122(2) . . ?
C27 C26 C25 117(2) . . ?
C26 C27 C28 123(2) . . ?
C27 C28 C23 119(2) . . ?
C32 C31 Pt2 177.0(15) . . ?
C32 C31 Ag3 92.1(13) . . ?
Pt2 C31 Ag3 85.3(7) . . ?
C31 C32 C33 167.3(19) . . ?
C31 C32 Ag3 61.3(11) . . ?
C33 C32 Ag3 131.2(12) . . ?
C38 C33 C34 118.8(19) . . ?
C38 C33 C32 121(2) . . ?
C34 C33 C32 119.7(19) . . ?
C35 C34 C33 117(2) . . ?
C36 C35 C34 124(2) . . ?
C37 C36 C35 120(3) . . ?
C36 C37 C38 122(3) . . ?
C37 C38 C33 119(2) . . ?
C42 C41 Pt2 172.3(14) . . ?
C42 C41 Ag4 86.0(11) . . ?
Pt2 C41 Ag4 87.2(6) . . ?
C41 C42 C43 169.8(17) . . ?
C41 C42 Ag4 64.7(10) . . ?
C43 C42 Ag4 124.8(11) . . ?
C48 C43 C44 117.0(18) . . ?
C48 C43 C42 121.6(17) . . ?
C44 C43 C42 121.4(18) . . ?
C43 C44 C45 120(2) . . ?
C46 C45 C44 117(3) . . ?
C47 C46 C45 122(2) . . ?
C48 C47 C46 120(3) . . ?
C47 C48 C43 123(2) . . ?
C112 C111 C116 117.0(19) . . ?
C112 C111 P2 117.0(13) . . ?
C116 C111 P2 125.1(17) . . ?
C111 C112 C113 121.4(19) . . ?
C114 C113 C112 121(2) . . ?
C113 C114 C115 118(2) . . ?
C114 C115 C116 121(3) . . ?
C111 C116 C115 121(3) . . ?
C122 C121 C126 116.7(15) . . ?
C122 C121 P2 122.5(13) . . ?
C126 C121 P2 120.8(13) . . ?
C123 C122 C121 121(2) . . ?
C122 C123 C124 120(2) . . ?
C125 C124 C123 121(2) . . ?
C124 C125 C126 121(2) . . ?
C125 C126 C121 120.4(19) . . ?
C132 C131 C136 117.8(17) . . ?
C132 C131 P1 122.8(14) . . ?
C136 C131 P1 119.3(13) . . ?
C133 C132 C131 121.3(17) . . ?
C134 C133 C132 120.1(19) . . ?
C133 C134 C135 120.2(19) . . ?
C136 C135 C134 119.1(19) . . ?
C135 C136 C131 121.5(18) . . ?
C146 C141 C142 116.3(17) . . ?
C146 C141 P1 125.5(15) . . ?
C142 C141 P1 117.9(13) . . ?
C143 C142 C141 121.4(18) . . ?
C144 C143 C142 122(2) . . ?
C143 C144 C145 118(2) . . ?
C146 C145 C144 121(2) . . ?
C145 C146 C141 121(2) . . ?
C156 C151 C152 118.7(18) . . ?
C156 C151 P4 119.4(13) . . ?
C152 C151 P4 121.8(15) . . ?
C151 C152 C153 120.4(18) . . ?
C154 C153 C152 120.3(19) . . ?
C153 C154 C155 120(2) . . ?
C154 C155 C156 121(2) . . ?
C151 C156 C155 119.4(18) . . ?
C166 C161 C162 116.1(18) . . ?
C166 C161 P4 124.5(15) . . ?
C162 C161 P4 119.2(13) . . ?
C163 C162 C161 122.9(19) . . ?
C164 C163 C162 121(2) . . ?
C163 C164 C165 118.7(19) . . ?
C164 C165 C166 120(2) . . ?
C161 C166 C165 121(2) . . ?
C176 C171 C172 116.7(17) . . ?
C176 C171 P3 123.2(16) . . ?
C172 C171 P3 119.9(12) . . ?
C173 C172 C171 122.5(18) . . ?
C174 C173 C172 119(2) . . ?
C173 C174 C175 120(2) . . ?
C174 C175 C176 120(2) . . ?
C171 C176 C175 121(2) . . ?
C182 C181 C186 120.1(16) . . ?
C182 C181 P3 119.2(13) . . ?
C186 C181 P3 120.3(13) . . ?
C181 C182 C183 119.6(17) . . ?
C184 C183 C182 121(2) . . ?
C183 C184 C185 120(2) . . ?
C184 C185 C186 117(2) . . ?
C181 C186 C185 121.5(18) . . ?
C196 C191 C192 120(2) . . ?
C196 C191 P5 121.1(19) . . ?
C192 C191 P5 119.0(18) . . ?
C191 C192 C193 119(2) . . ?
C194 C193 C192 119(3) . . ?
C193 C194 C195 121(3) . . ?
C194 C195 C196 120(3) . . ?
C191 C196 C195 120(3) . . ?
C202 C201 C206 121(2) . . ?
C202 C201 P5 120.6(16) . . ?
C206 C201 P5 118.8(17) . . ?
C201 C202 C203 120(2) . . ?
C202 C203 C204 120(3) . . ?
C205 C204 C203 119(3) . . ?
C204 C205 C206 122(3) . . ?
C201 C206 C205 119(3) . . ?
C212 C211 C217 119.0(18) . . ?
C212 C211 P6 121.1(15) . . ?
C217 C211 P6 119.6(14) . . ?
C213 C212 C211 120(2) . . ?
C216 C213 C212 122(3) . . ?
C216 C215 C217 121(2) . . ?
C213 C216 C215 118(2) . . ?
C215 C217 C211 120(2) . . ?
C226 C221 C222 120(2) . . ?
C226 C221 P6 123.0(18) . . ?
C222 C221 P6 116.9(18) . . ?
C223 C222 C221 120(3) . . ?
C222 C223 C224 121(3) . . ?
C225 C224 C223 120(3) . . ?
C224 C225 C226 119(3) . . ?
C221 C226 C225 120(3) . . ?
C232 C231 C236 117(2) . . ?
C232 C231 P7 121.0(17) . . ?
C236 C231 P7 122.4(19) . . ?
C231 C232 C233 124(3) . . ?
C234 C233 C232 116(3) . . ?
C235 C234 C233 120(3) . . ?
C234 C235 C236 121(3) . . ?
C231 C236 C235 121(3) . . ?
C246 C241 C242 115(2) . . ?
C246 C241 P7 126.1(18) . . ?
C242 C241 P7 118.4(19) . . ?
C243 C242 C241 122(3) . . ?
C244 C243 C242 118(3) . . ?
C243 C244 C245 121(3) . . ?
C244 C245 C246 119(3) . . ?
C241 C246 C245 124(3) . . ?
C252 C251 C256 120(2) . . ?
C252 C251 P8 121.8(16) . . ?
C256 C251 P8 118.4(17) . . ?
C251 C252 C253 119(2) . . ?
C254 C253 C252 125(3) . . ?
C253 C254 C255 116(3) . . ?
C254 C255 C256 121(3) . . ?
C251 C256 C255 120(2) . . ?
C266 C261 C262 116(3) . . ?
C266 C261 P8 120(2) . . ?
C262 C261 P8 124(3) . . ?
C261 C262 C263 120(5) . . ?
C264 C263 C262 123(6) . . ?
C263 C264 C265 125(5) . . ?
C266 C265 C264 114(5) . . ?
C261 C266 C265 121(4) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C21 1.979(17) . ?
Pt1 C11 1.995(19) . ?
Pt1 P3 2.355(4) . ?
Pt1 P1 2.365(4) . ?
Pt1 Ag1 2.8994(15) . ?
Pt1 Ag2 2.9381(15) . ?
Pt1 Pt2 3.1534(8) . ?
Pt2 C41 1.960(18) . ?
Pt2 C31 2.05(2) . ?
Pt2 P4 2.341(4) . ?
Pt2 P2 2.344(4) . ?
Pt2 Ag4 2.9245(14) . ?
Pt2 Ag3 2.9347(15) . ?
Ag1 C11 2.313(15) . ?
Ag1 P5 2.380(5) . ?
Ag1 C12 2.527(18) . ?
Ag1 Ag2 3.179(2) . ?
Ag2 C21 2.302(16) . ?
Ag2 P6 2.349(5) . ?
Ag2 C22 2.478(17) . ?
Ag3 C31 2.273(16) . ?
Ag3 P8 2.373(5) . ?
Ag3 C32 2.590(17) . ?
Ag4 C41 2.269(15) . ?
Ag4 P7 2.359(5) . ?
Ag4 C42 2.502(16) . ?
P2 N1 1.586(13) . ?
P2 C121 1.813(15) . ?
P2 C111 1.846(18) . ?
P1 N1 1.596(13) . ?
P1 C141 1.790(17) . ?
P1 C131 1.827(18) . ?
P4 N2 1.598(13) . ?
P4 C161 1.826(17) . ?
P4 C151 1.834(19) . ?
P3 N2 1.607(14) . ?
P3 C181 1.822(17) . ?
P3 C171 1.839(17) . ?
P5 N3 1.586(15) . ?
P5 C201 1.844(18) . ?
P5 C191 1.85(2) . ?
P6 N3 1.631(14) . ?
P6 C211 1.819(17) . ?
P6 C221 1.854(19) . ?
P7 N4 1.586(15) . ?
P7 C231 1.80(2) . ?
P7 C241 1.83(2) . ?
P8 N4 1.615(15) . ?
P8 C261 1.84(3) . ?
P8 C251 1.865(18) . ?
O1 C01 1.422(5) . ?
C11 C12 1.23(2) . ?
C12 C13 1.44(3) . ?
C13 C14 1.33(3) . ?
C13 C18 1.34(3) . ?
C14 C15 1.42(3) . ?
C15 C16 1.31(4) . ?
C16 C17 1.32(4) . ?
C17 C18 1.38(4) . ?
C21 C22 1.23(2) . ?
C22 C23 1.46(2) . ?
C23 C24 1.37(3) . ?
C23 C28 1.38(3) . ?
C24 C25 1.37(3) . ?
C25 C26 1.37(3) . ?
C26 C27 1.34(3) . ?
C27 C28 1.35(3) . ?
C31 C32 1.16(2) . ?
C32 C33 1.43(2) . ?
C33 C38 1.40(3) . ?
C33 C34 1.41(3) . ?
C34 C35 1.38(3) . ?
C35 C36 1.33(4) . ?
C36 C37 1.32(4) . ?
C37 C38 1.39(4) . ?
C41 C42 1.23(2) . ?
C42 C43 1.45(2) . ?
C43 C48 1.36(2) . ?
C43 C44 1.38(3) . ?
C44 C45 1.42(3) . ?
C45 C46 1.35(4) . ?
C46 C47 1.34(4) . ?
C47 C48 1.34(3) . ?
C111 C112 1.35(3) . ?
C111 C116 1.36(3) . ?
C112 C113 1.37(3) . ?
C113 C114 1.33(3) . ?
C114 C115 1.35(4) . ?
C115 C116 1.38(3) . ?
C121 C122 1.36(2) . ?
C121 C126 1.43(2) . ?
C122 C123 1.35(3) . ?
C123 C124 1.39(3) . ?
C124 C125 1.31(3) . ?
C125 C126 1.35(3) . ?
C131 C132 1.38(2) . ?
C131 C136 1.39(2) . ?
C132 C133 1.37(3) . ?
C133 C134 1.36(3) . ?
C134 C135 1.39(3) . ?
C135 C136 1.37(3) . ?
C141 C146 1.40(2) . ?
C141 C142 1.40(2) . ?
C142 C143 1.37(3) . ?
C143 C144 1.35(3) . ?
C144 C145 1.40(3) . ?
C145 C146 1.37(3) . ?
C151 C156 1.36(2) . ?
C151 C152 1.39(2) . ?
C152 C153 1.40(3) . ?
C153 C154 1.33(3) . ?
C154 C155 1.37(3) . ?
C155 C156 1.41(3) . ?
C161 C166 1.38(3) . ?
C161 C162 1.38(2) . ?
C162 C163 1.34(3) . ?
C163 C164 1.34(3) . ?
C164 C165 1.38(3) . ?
C165 C166 1.39(3) . ?
C171 C176 1.36(3) . ?
C171 C172 1.39(2) . ?
C172 C173 1.37(3) . ?
C173 C174 1.33(3) . ?
C174 C175 1.38(3) . ?
C175 C176 1.39(3) . ?
C181 C182 1.34(2) . ?
C181 C186 1.36(2) . ?
C182 C183 1.39(3) . ?
C183 C184 1.35(3) . ?
C184 C185 1.39(3) . ?
C185 C186 1.41(3) . ?
C191 C196 1.33(3) . ?
C191 C192 1.38(3) . ?
C192 C193 1.43(3) . ?
C193 C194 1.32(4) . ?
C194 C195 1.36(4) . ?
C195 C196 1.38(4) . ?
C201 C202 1.35(3) . ?
C201 C206 1.35(3) . ?
C202 C203 1.38(3) . ?
C203 C204 1.38(4) . ?
C204 C205 1.32(4) . ?
C205 C206 1.39(3) . ?
C211 C212 1.37(2) . ?
C211 C217 1.38(3) . ?
C212 C213 1.37(3) . ?
C213 C216 1.35(3) . ?
C215 C216 1.36(4) . ?
C215 C217 1.38(3) . ?
C221 C226 1.35(3) . ?
C221 C222 1.37(3) . ?
C222 C223 1.35(3) . ?
C223 C224 1.36(4) . ?
C224 C225 1.35(4) . ?
C225 C226 1.39(4) . ?
C231 C232 1.35(3) . ?
C231 C236 1.37(3) . ?
C232 C233 1.43(4) . ?
C233 C234 1.37(4) . ?
C234 C235 1.37(4) . ?
C235 C236 1.39(3) . ?
C241 C246 1.30(3) . ?
C241 C242 1.40(3) . ?
C242 C243 1.36(3) . ?
C243 C244 1.33(4) . ?
C244 C245 1.35(4) . ?
C245 C246 1.36(4) . ?
C251 C252 1.30(3) . ?
C251 C256 1.33(3) . ?
C252 C253 1.36(3) . ?
C253 C254 1.31(3) . ?
C254 C255 1.32(4) . ?
C255 C256 1.38(4) . ?
C261 C266 1.33(4) . ?
C261 C262 1.34(4) . ?
C262 C263 1.35(6) . ?
C263 C264 1.11(11) . ?
C264 C265 1.38(8) . ?
C265 C266 1.38(4) . ?
