#------------------------------------------------------------------------------
#$Date: 2016-02-16 03:10:39 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176453 $
#$URL: svn://www.crystallography.net/cod/cif/7/10/44/7104439.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7104439
loop_
_publ_author_name
'Koshevoy, Igor O'
'Lin, Yi-Chih'
'Karttunen, Antti J'
'Haukka, Matti'
'Chou, Pi-Tai'
'Tunik, Sergey P'
'Pakkanen, Tapani A'
_publ_section_title
;
 An intensely and oxygen independent phosphorescent gold(I)-silver(I)
 complex: "trapping" an Au8Ag10 oligomer by two
 gold-alkynyl-diphosphine molecules.
;
_journal_issue                   20
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              2860
_journal_page_last               2862
_journal_paper_doi               10.1039/b901893j
_journal_volume                  34
_journal_year                    2009
_chemical_formula_moiety
'C244 H164 Ag10 Au12 P4, 2(P F6), 2(C3 H6 O), 2.5(C H2 Cl2), 2(C H4 O)'
_chemical_formula_sum            'C254.5 H189 Ag10 Au12 Cl5 F12 O4 P6'
_chemical_formula_weight         7344.43
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 99.6710(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   25.1281(2)
_cell_length_b                   23.4103(2)
_cell_length_c                   39.8036(3)
_cell_measurement_reflns_used    63483
_cell_measurement_temperature    90(2)
_cell_measurement_theta_max      27.48
_cell_measurement_theta_min      1.00
_cell_volume                     23082.0(3)
_computing_cell_refinement       'Denzo/Scalepack (Otwinowski & Minor, 1997)'
_computing_data_collection       'Collect (Bruker AXS BV, 1997-2004)'
_computing_data_reduction        'Denzo/Scalepack (Otwinowski & Minor, 1997)'
_computing_molecular_graphics    'Diamond v.3.1e (Brandenburg, 2007)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      90(2)
_diffrn_detector_area_resol_mean 9
_diffrn_measured_fraction_theta_full 0.983
_diffrn_measured_fraction_theta_max 0.983
_diffrn_measurement_device       '95mm CCD camera on κ-goniostat'
_diffrn_measurement_device_type  'Nonius KappaCCD'
_diffrn_measurement_method       'φ scans and ω scans with κ offset'
_diffrn_radiation_monochromator  'horizontally mounted graphite crystal'
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0488
_diffrn_reflns_av_sigmaI/netI    0.0566
_diffrn_reflns_limit_h_max       30
_diffrn_reflns_limit_h_min       -30
_diffrn_reflns_limit_k_max       28
_diffrn_reflns_limit_k_min       -28
_diffrn_reflns_limit_l_max       49
_diffrn_reflns_limit_l_min       -48
_diffrn_reflns_number            231392
_diffrn_reflns_theta_full        26.00
_diffrn_reflns_theta_max         26.00
_diffrn_reflns_theta_min         1.86
_exptl_absorpt_coefficient_mu    8.582
_exptl_absorpt_correction_T_max  0.3891
_exptl_absorpt_correction_T_min  0.0901
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS v.2.10 (Sheldrick, 2003)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    2.113
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             13796
_exptl_crystal_size_max          0.47
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.11
_refine_diff_density_max         2.808
_refine_diff_density_min         -1.729
_refine_diff_density_rms         0.173
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.008
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2813
_refine_ls_number_reflns         44603
_refine_ls_number_restraints     65
_refine_ls_restrained_S_all      1.012
_refine_ls_R_factor_all          0.0716
_refine_ls_R_factor_gt           0.0387
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0264P)²+147.7680P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0718
_refine_ls_wR_factor_ref         0.0799
_reflns_number_gt                32359
_reflns_number_total             44603
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b901893j.txt
_cod_data_source_block           1
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_original_formula_sum        'C254.50 H189 Ag10 Au12 Cl5 F12 O4 P6'
_cod_database_code               7104439
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Au1 Au 0.193333(12) 0.739950(13) 0.141533(8) 0.02930(8) Uani 1 1 d . . .
Au2 Au 0.312573(11) 0.778042(12) 0.139467(8) 0.02407(7) Uani 1 1 d . . .
Au3 Au 0.451341(11) 0.724474(12) 0.126061(7) 0.02233(7) Uani 1 1 d . . .
Au4 Au 0.590018(11) 0.669568(12) 0.111510(8) 0.02322(7) Uani 1 1 d . . .
Au5 Au 0.720781(11) 0.633767(12) 0.085006(7) 0.02224(7) Uani 1 1 d . . .
Au6 Au 0.795578(11) 0.602306(12) 0.032495(8) 0.02304(7) Uani 1 1 d . . .
Au7 Au 0.908774(11) 0.679038(12) 0.186635(8) 0.02512(7) Uani 1 1 d . . .
Au8 Au 0.787640(12) 0.712896(13) 0.154479(8) 0.02839(7) Uani 1 1 d . . .
Au9 Au 0.646385(12) 0.737361(13) 0.182778(8) 0.02645(7) Uani 1 1 d . . .
Au10 Au 0.515200(12) 0.807683(12) 0.192215(8) 0.02630(7) Uani 1 1 d . . .
Au11 Au 0.376950(11) 0.852530(12) 0.208204(8) 0.02362(7) Uani 1 1 d . . .
Au12 Au 0.307613(11) 0.939897(12) 0.241682(8) 0.02494(7) Uani 1 1 d . . .
Ag1 Ag 0.27948(2) 0.77340(3) 0.207836(16) 0.03130(14) Uani 1 1 d . . .
Ag2 Ag 0.41134(2) 0.73033(2) 0.191393(16) 0.02852(14) Uani 1 1 d . . .
Ag3 Ag 0.54653(2) 0.66978(3) 0.180271(16) 0.03311(15) Uani 1 1 d . . .
Ag4 Ag 0.69180(2) 0.62769(2) 0.159355(17) 0.03189(15) Uani 1 1 d . . .
Ag5 Ag 0.81803(2) 0.59315(2) 0.137913(17) 0.03183(15) Uani 1 1 d . . .
Ag6 Ag 0.81095(2) 0.71364(2) 0.082540(16) 0.03009(14) Uani 1 1 d . . .
Ag7 Ag 0.68243(2) 0.74273(2) 0.108594(15) 0.02652(13) Uani 1 1 d . . .
Ag8 Ag 0.55687(2) 0.80377(3) 0.129848(16) 0.03262(15) Uani 1 1 d . . .
Ag9 Ag 0.41892(2) 0.85302(2) 0.145905(15) 0.02823(14) Uani 1 1 d . . .
Ag10 Ag 0.27892(2) 0.89593(2) 0.160467(16) 0.02906(14) Uani 1 1 d . . .
Cl1 Cl 0.24891(19) 0.24415(19) 0.09903(11) 0.1313(17) Uani 1 1 d . . .
Cl2 Cl 0.22605(18) 0.31190(15) 0.03850(10) 0.1132(13) Uani 1 1 d . . .
Cl3 Cl 0.6331(2) 0.1903(2) 0.15994(12) 0.1405(16) Uani 1 1 d . . .
Cl4 Cl 0.7426(2) 0.1892(4) 0.15489(19) 0.237(4) Uani 1 1 d . . .
P1 P 0.19014(8) 0.70297(9) 0.08804(6) 0.0289(5) Uani 1 1 d . . .
P2 P 0.73354(7) 0.53658(8) 0.00835(5) 0.0217(4) Uani 1 1 d . . .
P3 P 0.92051(8) 0.75486(8) 0.22283(5) 0.0245(4) Uani 1 1 d . . .
P4 P 0.37671(8) 0.95427(8) 0.28597(5) 0.0255(5) Uani 1 1 d . . .
P5 P 1.06337(13) 0.79361(17) 0.41916(8) 0.0831(12) Uani 1 1 d . . .
F1 F 1.0848(3) 0.7977(4) 0.3848(2) 0.133(4) Uani 1 1 d . . .
F2 F 1.0401(4) 0.7901(3) 0.45393(15) 0.121(3) Uani 1 1 d . . .
F3 F 1.0100(3) 0.8207(3) 0.40042(15) 0.0801(19) Uani 1 1 d . . .
F4 F 1.0854(6) 0.8542(5) 0.4283(2) 0.272(9) Uani 1 1 d . . .
F5 F 1.1145(4) 0.7666(9) 0.4379(4) 0.362(14) Uani 1 1 d . . .
F6 F 1.0376(4) 0.7332(3) 0.4100(2) 0.130(3) Uani 1 1 d . . .
O1 O 0.6215(3) 0.2666(3) 0.0191(2) 0.089(3) Uani 1 1 d . . .
C1 C 0.1456(3) 0.6409(3) 0.0809(2) 0.0301(19) Uani 1 1 d . . .
C2 C 0.1474(3) 0.6045(3) 0.0537(2) 0.041(2) Uani 1 1 d . . .
H2 H 0.1743 0.6096 0.0397 0.050 Uiso 1 1 calc R . .
C3 C 0.1101(3) 0.5607(4) 0.0467(3) 0.049(3) Uani 1 1 d . . .
H3 H 0.1111 0.5362 0.0278 0.058 Uiso 1 1 calc R . .
C4 C 0.0715(4) 0.5526(4) 0.0672(3) 0.049(3) Uani 1 1 d . . .
H4 H 0.0459 0.5226 0.0624 0.059 Uiso 1 1 calc R . .
C5 C 0.0703(3) 0.5882(4) 0.0947(2) 0.044(2) Uani 1 1 d . . .
H5 H 0.0439 0.5829 0.1089 0.053 Uiso 1 1 calc R . .
C6 C 0.1080(3) 0.6321(3) 0.1014(2) 0.038(2) Uani 1 1 d . . .
H6 H 0.1075 0.6561 0.1206 0.045 Uiso 1 1 calc R . .
C7 C 0.1630(3) 0.7539(3) 0.0551(2) 0.034(2) Uani 1 1 d . . .
C8 C 0.1453(4) 0.7370(4) 0.0218(3) 0.057(3) Uani 1 1 d . . .
H8 H 0.1478 0.6982 0.0155 0.069 Uiso 1 1 calc R . .
C9 C 0.1238(4) 0.7769(5) -0.0020(3) 0.063(3) Uani 1 1 d . . .
H9 H 0.1116 0.7649 -0.0248 0.076 Uiso 1 1 calc R . .
C10 C 0.1196(4) 0.8330(5) 0.0061(3) 0.063(3) Uani 1 1 d . . .
H10 H 0.1040 0.8598 -0.0107 0.076 Uiso 1 1 calc R . .
C11 C 0.1383(4) 0.8500(4) 0.0390(3) 0.056(3) Uani 1 1 d . . .
H11 H 0.1365 0.8891 0.0449 0.067 Uiso 1 1 calc R . .
C12 C 0.1594(3) 0.8111(3) 0.0635(3) 0.038(2) Uani 1 1 d . . .
H12 H 0.1715 0.8234 0.0862 0.046 Uiso 1 1 calc R . .
C13 C 0.2547(3) 0.6799(3) 0.0782(2) 0.0269(18) Uani 1 1 d . . .
C14 C 0.2853(3) 0.7163(3) 0.06066(19) 0.0251(18) Uani 1 1 d . . .
H14 H 0.2718 0.7531 0.0536 0.030 Uiso 1 1 calc R . .
C15 C 0.3348(3) 0.6986(3) 0.0537(2) 0.0286(19) Uani 1 1 d . . .
H15 H 0.3551 0.7234 0.0417 0.034 Uiso 1 1 calc R . .
C16 C 0.3555(3) 0.6449(3) 0.06398(19) 0.0269(18) Uani 1 1 d . . .
C17 C 0.3254(3) 0.6097(3) 0.08229(19) 0.0255(18) Uani 1 1 d . . .
H17 H 0.3391 0.5733 0.0900 0.031 Uiso 1 1 calc R . .
C18 C 0.2765(3) 0.6274(3) 0.08918(19) 0.0275(18) Uani 1 1 d . . .
H18 H 0.2569 0.6030 0.1018 0.033 Uiso 1 1 calc R . .
C19 C 0.4076(3) 0.6257(3) 0.05449(18) 0.0213(16) Uani 1 1 d . . .
C20 C 0.4468(3) 0.6652(3) 0.04904(19) 0.0267(18) Uani 1 1 d . . .
H20 H 0.4402 0.7048 0.0513 0.032 Uiso 1 1 calc R . .
C21 C 0.4950(3) 0.6474(3) 0.04042(18) 0.0256(17) Uani 1 1 d . . .
H21 H 0.5202 0.6755 0.0361 0.031 Uiso 1 1 calc R . .
C22 C 0.5083(3) 0.5901(3) 0.03782(19) 0.0242(17) Uani 1 1 d . . .
C23 C 0.4685(3) 0.5506(3) 0.04265(19) 0.0265(18) Uani 1 1 d . . .
H23 H 0.4753 0.5110 0.0403 0.032 Uiso 1 1 calc R . .
C24 C 0.4195(3) 0.5679(3) 0.05082(19) 0.0281(18) Uani 1 1 d . . .
H24 H 0.3934 0.5399 0.0540 0.034 Uiso 1 1 calc R . .
C25 C 0.5615(3) 0.5737(3) 0.02982(18) 0.0215(16) Uani 1 1 d . . .
C26 C 0.5899(3) 0.6119(3) 0.0125(2) 0.032(2) Uani 1 1 d . . .
H26 H 0.5734 0.6471 0.0047 0.039 Uiso 1 1 calc R . .
C27 C 0.6415(3) 0.6001(3) 0.0065(2) 0.0282(18) Uani 1 1 d . . .
H27 H 0.6604 0.6275 -0.0046 0.034 Uiso 1 1 calc R . .
C28 C 0.6656(3) 0.5476(3) 0.01661(19) 0.0224(17) Uani 1 1 d . . .
C29 C 0.6378(3) 0.5097(3) 0.03415(18) 0.0236(17) Uani 1 1 d . . .
H29 H 0.6541 0.4743 0.0417 0.028 Uiso 1 1 calc R . .
C30 C 0.5872(3) 0.5223(3) 0.04081(18) 0.0239(17) Uani 1 1 d . . .
H30 H 0.5693 0.4957 0.0531 0.029 Uiso 1 1 calc R . .
C31 C 0.7548(3) 0.4647(3) 0.02143(18) 0.0211(16) Uani 1 1 d . . .
C32 C 0.8021(3) 0.4570(3) 0.0447(2) 0.032(2) Uani 1 1 d . . .
H32 H 0.8222 0.4894 0.0540 0.038 Uiso 1 1 calc R . .
C33 C 0.8201(3) 0.4029(3) 0.0546(2) 0.036(2) Uani 1 1 d . . .
H33 H 0.8528 0.3981 0.0701 0.043 Uiso 1 1 calc R . .
C34 C 0.7906(3) 0.3558(3) 0.0419(2) 0.033(2) Uani 1 1 d . . .
H34 H 0.8026 0.3186 0.0491 0.039 Uiso 1 1 calc R . .
C35 C 0.7429(3) 0.3628(3) 0.0185(2) 0.0306(19) Uani 1 1 d . . .
H35 H 0.7230 0.3302 0.0094 0.037 Uiso 1 1 calc R . .
C36 C 0.7248(3) 0.4166(3) 0.00838(19) 0.0273(18) Uani 1 1 d . . .
H36 H 0.6921 0.4212 -0.0073 0.033 Uiso 1 1 calc R . .
C37 C 0.7283(3) 0.5360(3) -0.03795(19) 0.0237(17) Uani 1 1 d . . .
C38 C 0.7755(3) 0.5208(3) -0.0501(2) 0.036(2) Uani 1 1 d . . .
H38 H 0.8068 0.5104 -0.0345 0.043 Uiso 1 1 calc R . .
C39 C 0.7767(4) 0.5206(4) -0.0844(2) 0.041(2) Uani 1 1 d . . .
H39 H 0.8086 0.5093 -0.0925 0.049 Uiso 1 1 calc R . .
C40 C 0.7319(4) 0.5370(4) -0.1071(2) 0.043(2) Uani 1 1 d . . .
H40 H 0.7332 0.5376 -0.1308 0.051 Uiso 1 1 calc R . .
C41 C 0.6850(4) 0.5524(4) -0.0957(2) 0.044(2) Uani 1 1 d . . .
H41 H 0.6540 0.5632 -0.1115 0.052 Uiso 1 1 calc R . .
C42 C 0.6834(3) 0.5521(3) -0.0606(2) 0.0327(19) Uani 1 1 d . . .
H42 H 0.6514 0.5629 -0.0525 0.039 Uiso 1 1 calc R . .
C43 C 0.8566(3) 0.6548(3) 0.0516(2) 0.0271(18) Uani 1 1 d . . .
C44 C 0.8956(3) 0.6836(3) 0.06410(19) 0.0267(18) Uani 1 1 d . . .
C45 C 0.9462(3) 0.7127(3) 0.0762(2) 0.0283(18) Uani 1 1 d . . .
C46 C 0.9761(4) 0.7348(4) 0.0532(3) 0.053(3) Uani 1 1 d . . .
H46 H 0.9638 0.7303 0.0294 0.063 Uiso 1 1 calc R . .
C47 C 1.0243(4) 0.7638(4) 0.0648(3) 0.061(3) Uani 1 1 d . . .
H47 H 1.0443 0.7799 0.0489 0.074 Uiso 1 1 calc R . .
C48 C 1.0423(3) 0.7688(4) 0.0986(3) 0.042(2) Uani 1 1 d . . .
H48 H 1.0752 0.7883 0.1065 0.050 Uiso 1 1 calc R . .
C49 C 1.0141(4) 0.7463(4) 0.1212(2) 0.048(2) Uani 1 1 d . . .
H49 H 1.0277 0.7496 0.1448 0.058 Uiso 1 1 calc R . .
C50 C 0.9658(4) 0.7186(4) 0.1108(2) 0.049(2) Uani 1 1 d . . .
H50 H 0.9460 0.7036 0.1272 0.059 Uiso 1 1 calc R . .
C51 C 0.9076(3) 0.6090(3) 0.1579(2) 0.0281(19) Uani 1 1 d . . .
C52 C 0.9141(3) 0.5665(3) 0.1408(2) 0.0261(18) Uani 1 1 d . . .
C53 C 0.9306(3) 0.5186(3) 0.1222(2) 0.0262(18) Uani 1 1 d . . .
C54 C 0.9474(3) 0.4679(3) 0.1388(2) 0.034(2) Uani 1 1 d . . .
H54 H 0.9470 0.4644 0.1625 0.041 Uiso 1 1 calc R . .
C55 C 0.9646(3) 0.4227(4) 0.1213(2) 0.042(2) Uani 1 1 d . . .
H55 H 0.9765 0.3884 0.1330 0.051 Uiso 1 1 calc R . .
C56 C 0.9644(3) 0.4277(3) 0.0868(2) 0.040(2) Uani 1 1 d . . .
H56 H 0.9764 0.3965 0.0747 0.048 Uiso 1 1 calc R . .
C57 C 0.9472(3) 0.4772(3) 0.0696(2) 0.034(2) Uani 1 1 d . . .
H57 H 0.9468 0.4799 0.0458 0.040 Uiso 1 1 calc R . .
C58 C 0.9305(3) 0.5228(3) 0.0872(2) 0.0304(19) Uani 1 1 d . . .
H58 H 0.9189 0.5571 0.0755 0.037 Uiso 1 1 calc R . .
C59 C 0.9547(3) 0.7346(3) 0.2647(2) 0.0277(18) Uani 1 1 d . . .
C60 C 0.9818(3) 0.6825(3) 0.2696(2) 0.034(2) Uani 1 1 d . . .
H60 H 0.9830 0.6580 0.2507 0.041 Uiso 1 1 calc R . .
C61 C 1.0070(3) 0.6662(4) 0.3019(2) 0.038(2) Uani 1 1 d . . .
H61 H 1.0244 0.6301 0.3051 0.046 Uiso 1 1 calc R . .
C62 C 1.0069(3) 0.7015(4) 0.3292(2) 0.041(2) Uani 1 1 d . . .
H62 H 1.0250 0.6906 0.3511 0.049 Uiso 1 1 calc R . .
C63 C 0.9799(3) 0.7539(4) 0.3245(2) 0.037(2) Uani 1 1 d . . .
H63 H 0.9794 0.7784 0.3435 0.045 Uiso 1 1 calc R . .
C64 C 0.9544(3) 0.7701(3) 0.2928(2) 0.0303(19) Uani 1 1 d . . .
H64 H 0.9362 0.8058 0.2900 0.036 Uiso 1 1 calc R . .
C65 C 0.9591(3) 0.8138(3) 0.2091(2) 0.0264(18) Uani 1 1 d . . .
C66 C 1.0028(3) 0.8383(4) 0.2307(3) 0.048(2) Uani 1 1 d . . .
H66 H 1.0126 0.8251 0.2535 0.057 Uiso 1 1 calc R . .
C67 C 1.0317(4) 0.8822(4) 0.2186(3) 0.058(3) Uani 1 1 d . . .
H67 H 1.0622 0.8980 0.2330 0.070 Uiso 1 1 calc R . .
C68 C 1.0175(4) 0.9026(4) 0.1871(3) 0.047(3) Uani 1 1 d . . .
H68 H 1.0379 0.9329 0.1797 0.057 Uiso 1 1 calc R . .
C69 C 0.9736(4) 0.8805(4) 0.1649(3) 0.050(3) Uani 1 1 d . . .
H69 H 0.9636 0.8959 0.1426 0.060 Uiso 1 1 calc R . .
C70 C 0.9441(4) 0.8348(4) 0.1761(3) 0.049(2) Uani 1 1 d . . .
H70 H 0.9144 0.8186 0.1612 0.059 Uiso 1 1 calc R . .
C71 C 0.8561(3) 0.7829(3) 0.23076(19) 0.0243(17) Uani 1 1 d . . .
C72 C 0.8321(3) 0.8319(3) 0.2153(2) 0.0286(18) Uani 1 1 d . . .
H72 H 0.8504 0.8542 0.2009 0.034 Uiso 1 1 calc R . .
C73 C 0.7816(3) 0.8480(3) 0.22123(19) 0.0273(18) Uani 1 1 d . . .
H73 H 0.7654 0.8813 0.2103 0.033 Uiso 1 1 calc R . .
C74 C 0.7538(3) 0.8172(3) 0.24255(18) 0.0217(17) Uani 1 1 d . . .
C75 C 0.7786(3) 0.7683(3) 0.2581(2) 0.0288(19) Uani 1 1 d . . .
H75 H 0.7608 0.7465 0.2731 0.035 Uiso 1 1 calc R . .
C76 C 0.8283(3) 0.7514(3) 0.2520(2) 0.0278(18) Uani 1 1 d . . .
H76 H 0.8441 0.7175 0.2624 0.033 Uiso 1 1 calc R . .
C77 C 0.6998(3) 0.8356(3) 0.24911(19) 0.0252(18) Uani 1 1 d . . .
C78 C 0.6833(3) 0.8920(3) 0.2449(2) 0.0298(19) Uani 1 1 d . . .
H78 H 0.7074 0.9193 0.2382 0.036 Uiso 1 1 calc R . .
C79 C 0.6329(3) 0.9098(3) 0.2502(2) 0.0312(19) Uani 1 1 d . . .
H79 H 0.6231 0.9489 0.2472 0.037 Uiso 1 1 calc R . .
C80 C 0.5962(3) 0.8706(3) 0.25982(19) 0.0236(17) Uani 1 1 d . . .
C81 C 0.6127(3) 0.8136(3) 0.26408(19) 0.0257(18) Uani 1 1 d . . .
H81 H 0.5885 0.7860 0.2705 0.031 Uiso 1 1 calc R . .
C82 C 0.6635(3) 0.7965(3) 0.25908(19) 0.0268(18) Uani 1 1 d . . .
H82 H 0.6739 0.7576 0.2625 0.032 Uiso 1 1 calc R . .
C83 C 0.5422(3) 0.8895(3) 0.26579(19) 0.0260(18) Uani 1 1 d . . .
C84 C 0.5159(3) 0.9352(3) 0.2475(2) 0.0282(18) Uani 1 1 d . . .
H84 H 0.5321 0.9533 0.2304 0.034 Uiso 1 1 calc R . .
C85 C 0.4670(3) 0.9545(3) 0.25388(19) 0.0268(18) Uani 1 1 d . . .
H85 H 0.4500 0.9860 0.2414 0.032 Uiso 1 1 calc R . .
C86 C 0.4420(3) 0.9279(3) 0.27871(19) 0.0225(17) Uani 1 1 d . . .
C87 C 0.4664(3) 0.8810(3) 0.2959(2) 0.0261(18) Uani 1 1 d . . .
H87 H 0.4492 0.8618 0.3122 0.031 Uiso 1 1 calc R . .
C88 C 0.5162(3) 0.8619(3) 0.2895(2) 0.0263(18) Uani 1 1 d . . .
H88 H 0.5327 0.8297 0.3014 0.032 Uiso 1 1 calc R . .
C89 C 0.3670(3) 0.9202(3) 0.3254(2) 0.0255(18) Uani 1 1 d . . .
C90 C 0.3374(3) 0.8700(3) 0.3241(2) 0.040(2) Uani 1 1 d . . .
H90 H 0.3201 0.8559 0.3026 0.047 Uiso 1 1 calc R . .
C91 C 0.3326(4) 0.8405(4) 0.3530(2) 0.048(2) Uani 1 1 d . . .
H91 H 0.3131 0.8056 0.3516 0.057 Uiso 1 1 calc R . .
C92 C 0.3563(4) 0.8616(4) 0.3842(3) 0.050(3) Uani 1 1 d . . .
H92 H 0.3521 0.8418 0.4045 0.060 Uiso 1 1 calc R . .
C93 C 0.3862(4) 0.9117(4) 0.3863(2) 0.045(2) Uani 1 1 d . . .
H93 H 0.4030 0.9258 0.4078 0.054 Uiso 1 1 calc R . .
C94 C 0.3916(3) 0.9405(3) 0.3572(2) 0.035(2) Uani 1 1 d . . .
H94 H 0.4122 0.9747 0.3587 0.041 Uiso 1 1 calc R . .
C95 C 0.3871(3) 1.0302(3) 0.29496(19) 0.0256(18) Uani 1 1 d . . .
C96 C 0.4369(3) 1.0543(3) 0.30632(19) 0.0267(18) Uani 1 1 d . . .
H96 H 0.4683 1.0309 0.3098 0.032 Uiso 1 1 calc R . .
C97 C 0.4416(3) 1.1122(3) 0.3127(2) 0.0308(19) Uani 1 1 d . . .
H97 H 0.4761 1.1284 0.3206 0.037 Uiso 1 1 calc R . .
C98 C 0.3966(3) 1.1465(3) 0.3076(2) 0.035(2) Uani 1 1 d . . .
H98 H 0.4000 1.1864 0.3117 0.042 Uiso 1 1 calc R . .
C99 C 0.3465(3) 1.1227(3) 0.2964(2) 0.043(2) Uani 1 1 d . . .
H99 H 0.3154 1.1464 0.2933 0.052 Uiso 1 1 calc R . .
C100 C 0.3411(3) 1.0652(3) 0.2897(2) 0.037(2) Uani 1 1 d . . .
H100 H 0.3065 1.0493 0.2817 0.044 Uiso 1 1 calc R . .
C101 C 0.2430(3) 0.9370(3) 0.2039(2) 0.0285(19) Uani 1 1 d . . .
C102 C 0.2031(3) 0.9390(3) 0.1817(2) 0.0284(19) Uani 1 1 d . . .
C103 C 0.1550(3) 0.9505(3) 0.1574(2) 0.0313(19) Uani 1 1 d . . .
C104 C 0.1359(3) 1.0064(4) 0.1534(2) 0.042(2) Uani 1 1 d . . .
H104 H 0.1538 1.0363 0.1670 0.051 Uiso 1 1 calc R . .
C105 C 0.0911(4) 1.0182(4) 0.1294(3) 0.052(3) Uani 1 1 d . . .
H105 H 0.0787 1.0564 0.1262 0.062 Uiso 1 1 calc R . .
C106 C 0.0639(4) 0.9754(4) 0.1100(3) 0.052(3) Uani 1 1 d . . .
H106 H 0.0329 0.9839 0.0936 0.062 Uiso 1 1 calc R . .
C107 C 0.0820(3) 0.9200(4) 0.1146(2) 0.045(2) Uani 1 1 d . . .
H107 H 0.0632 0.8902 0.1015 0.054 Uiso 1 1 calc R . .
C108 C 0.1268(3) 0.9075(4) 0.1380(2) 0.038(2) Uani 1 1 d . . .
H108 H 0.1387 0.8690 0.1410 0.046 Uiso 1 1 calc R . .
C109 C 0.1889(3) 0.7687(3) 0.1890(2) 0.0273(19) Uani 1 1 d . . .
C110 C 0.1848(3) 0.7829(3) 0.2175(2) 0.0277(19) Uani 1 1 d . . .
C111 C 0.1721(3) 0.7969(3) 0.2506(2) 0.0281(19) Uani 1 1 d . . .
C112 C 0.2021(3) 0.8367(3) 0.2721(2) 0.036(2) Uani 1 1 d . . .
H112 H 0.2314 0.8560 0.2647 0.043 Uiso 1 1 calc R . .
C113 C 0.1896(3) 0.8485(4) 0.3039(2) 0.041(2) Uani 1 1 d . . .
H113 H 0.2101 0.8762 0.3179 0.049 Uiso 1 1 calc R . .
C114 C 0.1483(3) 0.8212(3) 0.3154(2) 0.038(2) Uani 1 1 d . . .
H114 H 0.1405 0.8291 0.3374 0.045 Uiso 1 1 calc R . .
C115 C 0.1180(3) 0.7817(4) 0.2945(2) 0.043(2) Uani 1 1 d . . .
H115 H 0.0886 0.7629 0.3020 0.052 Uiso 1 1 calc R . .
C116 C 0.1300(3) 0.7696(3) 0.2630(2) 0.038(2) Uani 1 1 d . . .
H116 H 0.1092 0.7418 0.2491 0.045 Uiso 1 1 calc R . .
C117 C 0.2927(3) 0.8489(3) 0.1120(2) 0.0288(19) Uani 1 1 d . . .
C118 C 0.2741(3) 0.8904(3) 0.0951(2) 0.0306(19) Uani 1 1 d . . .
C119 C 0.2490(3) 0.9315(3) 0.0707(2) 0.038(2) Uani 1 1 d . . .
C120 C 0.2561(4) 0.9271(4) 0.0368(2) 0.047(2) Uani 1 1 d . . .
H120 H 0.2812 0.9005 0.0305 0.056 Uiso 1 1 calc R . .
C121 C 0.2266(4) 0.9613(5) 0.0127(3) 0.063(3) Uani 1 1 d . . .
H121 H 0.2310 0.9579 -0.0105 0.076 Uiso 1 1 calc R . .
C122 C 0.1907(5) 1.0004(5) 0.0217(3) 0.075(4) Uani 1 1 d . . .
H122 H 0.1703 1.0237 0.0046 0.090 Uiso 1 1 calc R . .
C123 C 0.1842(4) 1.0060(4) 0.0547(3) 0.067(3) Uani 1 1 d . . .
H123 H 0.1597 1.0335 0.0608 0.081 Uiso 1 1 calc R . .
C124 C 0.2131(4) 0.9720(4) 0.0792(3) 0.053(3) Uani 1 1 d . . .
H124 H 0.2085 0.9760 0.1023 0.063 Uiso 1 1 calc R . .
C125 C 0.3255(3) 0.7053(3) 0.1662(2) 0.0242(17) Uani 1 1 d . . .
C126 C 0.3268(3) 0.6601(3) 0.18134(19) 0.0256(18) Uani 1 1 d . . .
C127 C 0.3256(3) 0.6052(3) 0.1974(2) 0.0285(18) Uani 1 1 d . . .
C128 C 0.3447(3) 0.5564(3) 0.1824(2) 0.035(2) Uani 1 1 d . . .
H128 H 0.3573 0.5594 0.1612 0.042 Uiso 1 1 calc R . .
C129 C 0.3452(3) 0.5039(3) 0.1986(2) 0.043(2) Uani 1 1 d . . .
H129 H 0.3588 0.4711 0.1888 0.052 Uiso 1 1 calc R . .
C130 C 0.3256(3) 0.4991(4) 0.2294(2) 0.040(2) Uani 1 1 d . . .
H130 H 0.3243 0.4628 0.2399 0.048 Uiso 1 1 calc R . .
C131 C 0.3085(3) 0.5462(4) 0.2441(2) 0.038(2) Uani 1 1 d . . .
H131 H 0.2962 0.5430 0.2653 0.046 Uiso 1 1 calc R . .
C132 C 0.3087(3) 0.5995(4) 0.2285(2) 0.037(2) Uani 1 1 d . . .
H132 H 0.2971 0.6323 0.2394 0.045 Uiso 1 1 calc R . .
C133 C 0.4333(3) 0.7971(3) 0.10038(19) 0.0211(16) Uani 1 1 d . . .
C134 C 0.4214(3) 0.8389(3) 0.08300(19) 0.0240(17) Uani 1 1 d . . .
C135 C 0.4072(3) 0.8843(3) 0.0582(2) 0.0284(18) Uani 1 1 d . . .
C136 C 0.3931(3) 0.8715(4) 0.0241(2) 0.034(2) Uani 1 1 d . . .
H136 H 0.3914 0.8328 0.0169 0.041 Uiso 1 1 calc R . .
C137 C 0.3814(3) 0.9145(4) 0.0002(2) 0.044(2) Uani 1 1 d . . .
H137 H 0.3722 0.9051 -0.0233 0.052 Uiso 1 1 calc R . .
C138 C 0.3830(3) 0.9712(4) 0.0103(3) 0.048(3) Uani 1 1 d . . .
H138 H 0.3743 1.0007 -0.0060 0.057 Uiso 1 1 calc R . .
C139 C 0.3972(3) 0.9842(4) 0.0445(3) 0.046(2) Uani 1 1 d . . .
H139 H 0.3989 1.0229 0.0516 0.055 Uiso 1 1 calc R . .
C140 C 0.4091(3) 0.9414(3) 0.0683(2) 0.036(2) Uani 1 1 d . . .
H140 H 0.4186 0.9508 0.0917 0.043 Uiso 1 1 calc R . .
C141 C 0.4659(3) 0.6469(3) 0.1472(2) 0.0261(18) Uani 1 1 d . . .
C142 C 0.4724(3) 0.5979(3) 0.15652(19) 0.0260(18) Uani 1 1 d . . .
C143 C 0.4746(3) 0.5380(3) 0.1638(2) 0.0302(19) Uani 1 1 d . . .
C144 C 0.4559(3) 0.4994(4) 0.1384(2) 0.042(2) Uani 1 1 d . . .
H144 H 0.4424 0.5124 0.1160 0.051 Uiso 1 1 calc R . .
C145 C 0.4569(4) 0.4409(4) 0.1457(3) 0.051(3) Uani 1 1 d . . .
H145 H 0.4442 0.4145 0.1280 0.062 Uiso 1 1 calc R . .
C146 C 0.4757(4) 0.4210(4) 0.1775(3) 0.058(3) Uani 1 1 d . . .
H146 H 0.4747 0.3813 0.1822 0.069 Uiso 1 1 calc R . .
C147 C 0.4962(4) 0.4590(4) 0.2028(3) 0.060(3) Uani 1 1 d . . .
H147 H 0.5105 0.4455 0.2250 0.072 Uiso 1 1 calc R . .
C148 C 0.4960(4) 0.5174(4) 0.1959(2) 0.045(2) Uani 1 1 d . . .
H148 H 0.5107 0.5434 0.2133 0.054 Uiso 1 1 calc R . .
C149 C 0.5712(3) 0.7432(3) 0.0864(2) 0.0249(17) Uani 1 1 d . . .
C150 C 0.5578(3) 0.7844(3) 0.06837(19) 0.0231(17) Uani 1 1 d . . .
C151 C 0.5420(3) 0.8261(3) 0.0421(2) 0.0233(17) Uani 1 1 d . . .
C152 C 0.5268(3) 0.8080(3) 0.0084(2) 0.033(2) Uani 1 1 d . . .
H152 H 0.5251 0.7683 0.0033 0.039 Uiso 1 1 calc R . .
C153 C 0.5141(4) 0.8477(4) -0.0175(2) 0.042(2) Uani 1 1 d . . .
H153 H 0.5040 0.8350 -0.0404 0.050 Uiso 1 1 calc R . .
C154 C 0.5159(3) 0.9056(3) -0.0104(2) 0.035(2) Uani 1 1 d . . .
H154 H 0.5084 0.9327 -0.0283 0.042 Uiso 1 1 calc R . .
C155 C 0.5289(3) 0.9236(3) 0.0230(2) 0.036(2) Uani 1 1 d . . .
H155 H 0.5287 0.9632 0.0280 0.043 Uiso 1 1 calc R . .
C156 C 0.5420(3) 0.8847(3) 0.0492(2) 0.0295(19) Uani 1 1 d . . .
H156 H 0.5510 0.8978 0.0720 0.035 Uiso 1 1 calc R . .
C157 C 0.6089(3) 0.5936(3) 0.13300(19) 0.0242(17) Uani 1 1 d . . .
C158 C 0.6220(3) 0.5469(3) 0.14429(19) 0.0270(18) Uani 1 1 d . . .
C159 C 0.6317(3) 0.4887(3) 0.1551(2) 0.033(2) Uani 1 1 d . . .
C160 C 0.6759(3) 0.4729(4) 0.1803(2) 0.037(2) Uani 1 1 d . . .
H160 H 0.7004 0.5013 0.1906 0.044 Uiso 1 1 calc R . .
C161 C 0.6837(4) 0.4166(4) 0.1900(2) 0.048(3) Uani 1 1 d . . .
H161 H 0.7134 0.4066 0.2071 0.057 Uiso 1 1 calc R . .
C162 C 0.6486(4) 0.3744(4) 0.1751(3) 0.053(3) Uani 1 1 d . . .
H162 H 0.6542 0.3357 0.1821 0.064 Uiso 1 1 calc R . .
C163 C 0.6052(4) 0.3889(4) 0.1500(3) 0.047(2) Uani 1 1 d . . .
H163 H 0.5816 0.3600 0.1394 0.057 Uiso 1 1 calc R . .
C164 C 0.5966(3) 0.4454(3) 0.1406(2) 0.039(2) Uani 1 1 d . . .
H164 H 0.5663 0.4551 0.1240 0.046 Uiso 1 1 calc R . .
C165 C 0.7086(3) 0.7080(3) 0.0595(2) 0.0273(18) Uani 1 1 d . . .
C166 C 0.7094(3) 0.7483(3) 0.0403(2) 0.0280(18) Uani 1 1 d . . .
C167 C 0.7095(3) 0.7953(3) 0.0167(2) 0.0320(19) Uani 1 1 d . . .
C168 C 0.7575(4) 0.8227(5) 0.0145(3) 0.077(4) Uani 1 1 d . . .
H168 H 0.7903 0.8105 0.0279 0.092 Uiso 1 1 calc R . .
C169 C 0.7567(5) 0.8690(5) -0.0081(4) 0.102(5) Uani 1 1 d . . .
H169 H 0.7895 0.8880 -0.0099 0.123 Uiso 1 1 calc R . .
C170 C 0.7100(5) 0.8869(4) -0.0271(3) 0.062(3) Uani 1 1 d . . .
H170 H 0.7103 0.9185 -0.0420 0.075 Uiso 1 1 calc R . .
C171 C 0.6629(4) 0.8599(4) -0.0250(2) 0.046(2) Uani 1 1 d . . .
H171 H 0.6302 0.8724 -0.0385 0.055 Uiso 1 1 calc R . .
C172 C 0.6630(3) 0.8142(3) -0.0030(2) 0.038(2) Uani 1 1 d . . .
H172 H 0.6299 0.7954 -0.0016 0.045 Uiso 1 1 calc R . .
C173 C 0.7390(3) 0.5576(3) 0.10728(19) 0.0250(17) Uani 1 1 d . . .
C174 C 0.7542(3) 0.5109(3) 0.11758(19) 0.0239(17) Uani 1 1 d . . .
C175 C 0.7661(3) 0.4523(3) 0.1267(2) 0.0281(18) Uani 1 1 d . . .
C176 C 0.8125(3) 0.4369(4) 0.1486(2) 0.040(2) Uani 1 1 d . . .
H176 H 0.8364 0.4657 0.1589 0.048 Uiso 1 1 calc R . .
C177 C 0.8246(4) 0.3803(4) 0.1556(3) 0.055(3) Uani 1 1 d . . .
H177 H 0.8569 0.3704 0.1704 0.066 Uiso 1 1 calc R . .
C178 C 0.7902(4) 0.3382(4) 0.1413(3) 0.054(3) Uani 1 1 d . . .
H178 H 0.7989 0.2992 0.1460 0.064 Uiso 1 1 calc R . .
C179 C 0.7425(4) 0.3529(3) 0.1198(2) 0.042(2) Uani 1 1 d . . .
H179 H 0.7183 0.3238 0.1101 0.051 Uiso 1 1 calc R . .
C180 C 0.7301(3) 0.4097(3) 0.1126(2) 0.036(2) Uani 1 1 d . . .
H180 H 0.6974 0.4196 0.0981 0.043 Uiso 1 1 calc R . .
C181 C 0.8096(3) 0.7771(3) 0.1271(2) 0.0321(19) Uani 1 1 d . . .
C182 C 0.8289(3) 0.8142(3) 0.1117(2) 0.034(2) Uani 1 1 d . . .
C183 C 0.8524(3) 0.8631(4) 0.0970(2) 0.040(2) Uani 1 1 d . . .
C184 C 0.8901(5) 0.8552(5) 0.0761(3) 0.086(4) Uani 1 1 d . . .
H184 H 0.8994 0.8177 0.0702 0.103 Uiso 1 1 calc R . .
C185 C 0.9140(6) 0.9012(7) 0.0639(3) 0.100(5) Uani 1 1 d . . .
H185 H 0.9405 0.8953 0.0498 0.120 Uiso 1 1 calc R . .
C186 C 0.9004(5) 0.9561(6) 0.0717(4) 0.094(5) Uani 1 1 d . . .
H186 H 0.9175 0.9881 0.0633 0.112 Uiso 1 1 calc R . .
C187 C 0.8635(5) 0.9630(5) 0.0909(4) 0.081(4) Uani 1 1 d . . .
H187 H 0.8529 1.0005 0.0960 0.097 Uiso 1 1 calc R . .
C188 C 0.8396(4) 0.9166(4) 0.1040(3) 0.069(3) Uani 1 1 d . . .
H188 H 0.8134 0.9231 0.1182 0.083 Uiso 1 1 calc R . .
C189 C 0.7764(3) 0.6496(3) 0.1864(2) 0.0280(18) Uani 1 1 d . . .
C190 C 0.7841(3) 0.6174(3) 0.2100(2) 0.0294(19) Uani 1 1 d . . .
C191 C 0.8016(3) 0.5853(3) 0.2416(2) 0.0273(18) Uani 1 1 d . . .
C192 C 0.8569(3) 0.5847(3) 0.2556(2) 0.037(2) Uani 1 1 d . . .
H192 H 0.8824 0.6028 0.2440 0.045 Uiso 1 1 calc R . .
C193 C 0.8737(4) 0.5573(4) 0.2865(2) 0.043(2) Uani 1 1 d . . .
H193 H 0.9109 0.5569 0.2964 0.051 Uiso 1 1 calc R . .
C194 C 0.8365(4) 0.5309(4) 0.3027(2) 0.047(2) Uani 1 1 d . . .
H194 H 0.8483 0.5116 0.3237 0.056 Uiso 1 1 calc R . .
C195 C 0.7826(4) 0.5318(4) 0.2893(2) 0.046(2) Uani 1 1 d . . .
H195 H 0.7574 0.5140 0.3013 0.055 Uiso 1 1 calc R . .
C196 C 0.7648(3) 0.5582(3) 0.2587(2) 0.035(2) Uani 1 1 d . . .
H196 H 0.7274 0.5580 0.2493 0.042 Uiso 1 1 calc R . .
C197 C 0.6665(3) 0.8011(3) 0.1543(2) 0.0283(18) Uani 1 1 d . . .
C198 C 0.6797(3) 0.8389(3) 0.1366(2) 0.0304(19) Uani 1 1 d . . .
C199 C 0.6930(3) 0.8892(3) 0.1182(2) 0.0305(19) Uani 1 1 d . . .
C200 C 0.6853(3) 0.8897(4) 0.0828(2) 0.040(2) Uani 1 1 d . . .
H200 H 0.6727 0.8563 0.0705 0.048 Uiso 1 1 calc R . .
C201 C 0.6959(4) 0.9384(4) 0.0654(2) 0.050(2) Uani 1 1 d . . .
H201 H 0.6915 0.9381 0.0412 0.060 Uiso 1 1 calc R . .
C202 C 0.7130(4) 0.9874(4) 0.0833(3) 0.052(3) Uani 1 1 d . . .
H202 H 0.7189 1.0213 0.0713 0.063 Uiso 1 1 calc R . .
C203 C 0.7215(4) 0.9874(4) 0.1186(3) 0.048(2) Uani 1 1 d . . .
H203 H 0.7347 1.0208 0.1308 0.057 Uiso 1 1 calc R . .
C204 C 0.7108(3) 0.9383(3) 0.1362(2) 0.039(2) Uani 1 1 d . . .
H204 H 0.7156 0.9385 0.1604 0.047 Uiso 1 1 calc R . .
C205 C 0.6306(3) 0.6730(3) 0.2134(2) 0.0298(19) Uani 1 1 d . . .
C206 C 0.6267(3) 0.6347(3) 0.2332(2) 0.0303(19) Uani 1 1 d . . .
C207 C 0.6274(3) 0.5905(4) 0.2589(2) 0.038(2) Uani 1 1 d . . .
C208 C 0.6185(3) 0.5343(4) 0.2489(3) 0.051(3) Uani 1 1 d . . .
H208 H 0.6108 0.5252 0.2253 0.061 Uiso 1 1 calc R . .
C209 C 0.6206(4) 0.4910(5) 0.2729(3) 0.062(3) Uani 1 1 d . . .
H209 H 0.6142 0.4525 0.2658 0.075 Uiso 1 1 calc R . .
C210 C 0.6321(4) 0.5041(6) 0.3067(4) 0.075(4) Uani 1 1 d . . .
H210 H 0.6336 0.4745 0.3232 0.090 Uiso 1 1 calc R . .
C211 C 0.6413(5) 0.5591(6) 0.3172(3) 0.081(4) Uani 1 1 d . . .
H211 H 0.6492 0.5678 0.3408 0.098 Uiso 1 1 calc R . .
C212 C 0.6391(4) 0.6025(5) 0.2931(3) 0.061(3) Uani 1 1 d . . .
H212 H 0.6458 0.6409 0.3004 0.073 Uiso 1 1 calc R . .
C213 C 0.5311(3) 0.8752(3) 0.1639(2) 0.0294(19) Uani 1 1 d . . .
C214 C 0.5363(3) 0.9191(3) 0.1492(2) 0.0283(19) Uani 1 1 d . . .
C215 C 0.5379(3) 0.9751(3) 0.1344(2) 0.0282(18) Uani 1 1 d . . .
C216 C 0.5765(3) 0.9910(3) 0.1147(2) 0.036(2) Uani 1 1 d . . .
H216 H 0.6033 0.9643 0.1107 0.043 Uiso 1 1 calc R . .
C217 C 0.5761(4) 1.0449(4) 0.1009(2) 0.049(2) Uani 1 1 d . . .
H217 H 0.6033 1.0554 0.0880 0.059 Uiso 1 1 calc R . .
C218 C 0.5365(4) 1.0841(4) 0.1055(2) 0.052(3) Uani 1 1 d . . .
H218 H 0.5360 1.1210 0.0956 0.063 Uiso 1 1 calc R . .
C219 C 0.4975(4) 1.0685(4) 0.1249(3) 0.049(3) Uani 1 1 d . . .
H219 H 0.4704 1.0951 0.1284 0.058 Uiso 1 1 calc R . .
C220 C 0.4981(3) 1.0151(3) 0.1388(2) 0.040(2) Uani 1 1 d . . .
H220 H 0.4711 1.0048 0.1517 0.048 Uiso 1 1 calc R . .
C221 C 0.4977(3) 0.7431(3) 0.2216(2) 0.0269(18) Uani 1 1 d . . .
C222 C 0.4887(3) 0.7040(3) 0.2397(2) 0.0259(18) Uani 1 1 d . . .
C223 C 0.4856(3) 0.6588(3) 0.2635(2) 0.0308(19) Uani 1 1 d . . .
C224 C 0.5150(4) 0.6631(4) 0.2956(3) 0.052(3) Uani 1 1 d . . .
H224 H 0.5352 0.6968 0.3022 0.063 Uiso 1 1 calc R . .
C225 C 0.5157(4) 0.6185(5) 0.3188(3) 0.067(3) Uani 1 1 d . . .
H225 H 0.5371 0.6215 0.3408 0.080 Uiso 1 1 calc R . .
C226 C 0.4856(4) 0.5703(4) 0.3101(3) 0.056(3) Uani 1 1 d . . .
H226 H 0.4853 0.5401 0.3261 0.067 Uiso 1 1 calc R . .
C227 C 0.4562(4) 0.5663(4) 0.2783(3) 0.065(3) Uani 1 1 d . . .
H227 H 0.4357 0.5327 0.2720 0.078 Uiso 1 1 calc R . .
C228 C 0.4556(4) 0.6098(4) 0.2547(3) 0.051(3) Uani 1 1 d . . .
H228 H 0.4346 0.6062 0.2326 0.061 Uiso 1 1 calc R . .
C229 C 0.3850(3) 0.9199(3) 0.17800(19) 0.0231(17) Uani 1 1 d . . .
C230 C 0.3748(3) 0.9692(3) 0.1686(2) 0.0251(18) Uani 1 1 d . . .
C231 C 0.3642(3) 1.0286(3) 0.1614(2) 0.0310(19) Uani 1 1 d . . .
C232 C 0.3519(4) 1.0502(4) 0.1289(3) 0.054(3) Uani 1 1 d . . .
H232 H 0.3488 1.0253 0.1098 0.065 Uiso 1 1 calc R . .
C233 C 0.3441(5) 1.1088(5) 0.1239(3) 0.070(3) Uani 1 1 d . . .
H233 H 0.3362 1.1234 0.1013 0.084 Uiso 1 1 calc R . .
C234 C 0.3475(4) 1.1451(4) 0.1506(4) 0.061(3) Uani 1 1 d . . .
H234 H 0.3424 1.1850 0.1467 0.073 Uiso 1 1 calc R . .
C235 C 0.3582(4) 1.1244(4) 0.1829(3) 0.054(3) Uani 1 1 d . . .
H235 H 0.3596 1.1497 0.2017 0.065 Uiso 1 1 calc R . .
C236 C 0.3671(3) 1.0664(3) 0.1886(2) 0.039(2) Uani 1 1 d . . .
H236 H 0.3751 1.0524 0.2113 0.047 Uiso 1 1 calc R . .
C237 C 0.3625(3) 0.7930(3) 0.2416(2) 0.0239(17) Uani 1 1 d . . .
C238 C 0.3495(3) 0.7616(3) 0.2629(2) 0.0310(19) Uani 1 1 d . . .
C239 C 0.3417(4) 0.7264(3) 0.2914(2) 0.037(2) Uani 1 1 d . . .
C240 C 0.3862(4) 0.7114(5) 0.3146(3) 0.065(3) Uani 1 1 d . . .
H240 H 0.4209 0.7240 0.3112 0.078 Uiso 1 1 calc R . .
C241 C 0.3816(5) 0.6780(5) 0.3430(3) 0.088(4) Uani 1 1 d . . .
H241 H 0.4129 0.6668 0.3585 0.106 Uiso 1 1 calc R . .
C242 C 0.3312(6) 0.6618(4) 0.3482(3) 0.075(4) Uani 1 1 d . . .
H242 H 0.3274 0.6410 0.3682 0.090 Uiso 1 1 calc R . .
C243 C 0.2869(5) 0.6750(4) 0.3252(3) 0.063(3) Uani 1 1 d . . .
H243 H 0.2524 0.6623 0.3286 0.076 Uiso 1 1 calc R . .
C244 C 0.2917(4) 0.7073(4) 0.2963(2) 0.047(2) Uani 1 1 d . . .
H244 H 0.2606 0.7160 0.2801 0.056 Uiso 1 1 calc R . .
C245 C 0.6031(5) 0.2509(5) 0.0730(3) 0.084(4) Uani 1 1 d . . .
H24A H 0.6110 0.2112 0.0679 0.127 Uiso 1 1 calc R . .
H24B H 0.5667 0.2534 0.0786 0.127 Uiso 1 1 calc R . .
H24C H 0.6294 0.2642 0.0925 0.127 Uiso 1 1 calc R . .
C246 C 0.6066(4) 0.2866(5) 0.0434(3) 0.058(3) Uani 1 1 d . . .
C247 C 0.5937(4) 0.3500(4) 0.0465(3) 0.056(3) Uani 1 1 d . . .
H24D H 0.5985 0.3699 0.0255 0.084 Uiso 1 1 calc R . .
H24E H 0.6180 0.3665 0.0659 0.084 Uiso 1 1 calc R . .
H24F H 0.5562 0.3543 0.0500 0.084 Uiso 1 1 calc R . .
C248 C 0.2691(9) 0.2760(7) 0.0669(4) 0.184(10) Uani 1 1 d . . .
H24G H 0.2860 0.2465 0.0543 0.221 Uiso 1 1 calc R . .
H24H H 0.2981 0.3030 0.0765 0.221 Uiso 1 1 calc R . .
C249 C 0.6842(6) 0.1537(6) 0.1444(6) 0.168(9) Uani 1 1 d . . .
H24I H 0.6879 0.1148 0.1542 0.202 Uiso 1 1 calc R . .
H24J H 0.6750 0.1503 0.1193 0.202 Uiso 1 1 calc R . .
P6 P 0.9227(2) 1.2448(2) 0.11304(14) 0.0792(18) Uani 0.609(4) 1 d PD A 1
F7 F 0.9213(5) 1.2891(4) 0.1393(3) 0.138(6) Uani 0.609(4) 1 d PD A 1
F8 F 0.9238(4) 1.1927(5) 0.0873(3) 0.108(4) Uani 0.609(4) 1 d PD A 1
F9 F 0.9812(4) 1.2338(7) 0.1304(3) 0.173(8) Uani 0.609(4) 1 d PD A 1
F10 F 0.8986(4) 1.2045(5) 0.1380(3) 0.113(5) Uani 0.609(4) 1 d PD A 1
F11 F 0.8655(5) 1.2603(5) 0.0953(3) 0.166(8) Uani 0.609(4) 1 d PD A 1
F12 F 0.9435(5) 1.2844(4) 0.0883(2) 0.122(6) Uani 0.609(4) 1 d PD A 1
P7 P 0.9566(3) 1.1063(3) 0.08271(18) 0.053(2) Uani 0.391(4) 1 d P A 2
F13 F 0.9526(6) 1.0554(6) 0.1079(3) 0.067(5) Uani 0.391(4) 1 d P A 2
F14 F 0.9586(7) 1.1590(6) 0.0574(4) 0.084(6) Uani 0.391(4) 1 d P A 2
F15 F 1.0088(6) 1.1292(5) 0.1056(4) 0.063(4) Uani 0.391(4) 1 d P A 2
F16 F 0.9192(6) 1.1434(6) 0.1042(4) 0.074(5) Uani 0.391(4) 1 d P A 2
F17 F 0.9013(6) 1.0852(5) 0.0592(3) 0.065(4) Uani 0.391(4) 1 d P A 2
F18 F 0.9865(7) 1.0720(7) 0.0651(6) 0.115(9) Uani 0.391(4) 1 d P A 2
O5 O 0.7172(8) 0.1355(6) 0.0698(3) 0.242(11) Uani 1 1 d D . .
C250 C 0.7439(6) 0.1941(6) 0.0335(5) 0.152(9) Uani 1 1 d D . .
H25D H 0.7271 0.1634 0.0187 0.229 Uiso 1 1 calc R . .
H25E H 0.7770 0.2067 0.0258 0.229 Uiso 1 1 calc R . .
H25F H 0.7187 0.2263 0.0326 0.229 Uiso 1 1 calc R . .
C251 C 0.7579(9) 0.1714(12) 0.0714(5) 0.46(4) Uani 1 1 d D . .
C252 C 0.8008(6) 0.1283(8) 0.0810(5) 0.157(8) Uani 1 1 d D . .
H25G H 0.8210 0.1375 0.1036 0.236 Uiso 1 1 calc R . .
H25H H 0.8253 0.1285 0.0643 0.236 Uiso 1 1 calc R . .
H25I H 0.7844 0.0904 0.0816 0.236 Uiso 1 1 calc R . .
C256 C 1.0234(6) 0.4104(8) 0.0064(7) 0.063(7) Uani 0.50 1 d PDU B 3
H25J H 1.0198 0.4225 -0.0178 0.076 Uiso 0.50 1 calc PR B 3
H25K H 1.0123 0.4430 0.0195 0.076 Uiso 0.50 1 calc PR B 3
Cl5 Cl 0.9802(2) 0.3529(3) 0.00920(16) 0.0785(18) Uani 0.50 1 d PD B 3
Cl6 Cl 1.0875(3) 0.3952(4) 0.02092(18) 0.113(3) Uani 0.50 1 d PD B 3
C257 C 1.0424(16) 0.3956(11) 0.0069(12) 0.132(16) Uani 0.50 1 d PDU C 4
H25L H 1.0170 0.3746 -0.0100 0.198 Uiso 0.50 1 calc PR C 4
H25M H 1.0439 0.3778 0.0293 0.198 Uiso 0.50 1 calc PR C 4
H25N H 1.0783 0.3948 0.0005 0.198 Uiso 0.50 1 calc PR C 4
O6 O 1.0254(8) 0.4515(7) 0.0083(3) 0.121(9) Uani 0.50 1 d PD C 4
H6O H 1.0362 0.4862 -0.0026 0.181 Uiso 0.50 1 d PR C 4
O4 O 0.0000 1.0000 0.0000 0.171(7) Uani 1 2 d SU . .
H4O H 0.0000 1.0000 -0.0239 0.256 Uiso 0.50 1 d PR . .
C255 C 0.0312(15) 0.9625(16) 0.0162(10) 0.171(7) Uani 0.50 1 d PU . .
H25O H 0.0302 0.9656 0.0406 0.256 Uiso 0.50 1 calc PR . .
H25P H 0.0682 0.9687 0.0122 0.256 Uiso 0.50 1 calc PR . .
H25Q H 0.0191 0.9243 0.0082 0.256 Uiso 0.50 1 calc PR . .
O3 O 0.0810(11) 0.1491(11) 0.0491(8) 0.397(14) Uani 1 1 d D . .
H3O H 0.0485 0.1267 0.0504 0.596 Uiso 1 1 d R . .
C254 C 0.1080(16) 0.1930(15) 0.0407(10) 0.397(14) Uani 1 1 d D . .
H25X H 0.0831 0.2201 0.0275 0.596 Uiso 1 1 calc R . .
H25Z H 0.1346 0.1801 0.0270 0.596 Uiso 1 1 calc R . .
H25R H 0.1267 0.2118 0.0614 0.596 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C109 Au1 P1 174.17(19) . . ?
C109 Au1 Au2 97.60(19) . . ?
P1 Au1 Au2 88.14(5) . . ?
C109 Au1 Ag1 44.66(19) . . ?
P1 Au1 Ag1 140.31(5) . . ?
Au2 Au1 Ag1 55.858(13) . . ?
C117 Au2 C125 174.9(3) . . ?
C117 Au2 Ag1 116.5(2) . . ?
C125 Au2 Ag1 61.9(2) . . ?
C117 Au2 Ag10 49.0(2) . . ?
C125 Au2 Ag10 130.7(2) . . ?
Ag1 Au2 Ag10 69.458(17) . . ?
C117 Au2 Au1 95.6(2) . . ?
C125 Au2 Au1 79.3(2) . . ?
Ag1 Au2 Au1 63.361(14) . . ?
Ag10 Au2 Au1 86.559(14) . . ?
C117 Au2 Ag2 138.3(2) . . ?
C125 Au2 Ag2 46.6(2) . . ?
Ag1 Au2 Ag2 72.432(17) . . ?
Ag10 Au2 Ag2 111.422(18) . . ?
Au1 Au2 Ag2 122.092(15) . . ?
C117 Au2 Ag9 73.5(2) . . ?
C125 Au2 Ag9 111.6(2) . . ?
Ag1 Au2 Ag9 107.890(18) . . ?
Ag10 Au2 Ag9 75.238(16) . . ?
Au1 Au2 Ag9 161.757(15) . . ?
Ag2 Au2 Ag9 65.392(16) . . ?
C133 Au3 C141 173.7(3) . . ?
C133 Au3 Ag2 109.3(2) . . ?
C141 Au3 Ag2 74.8(2) . . ?
C133 Au3 Ag3 139.9(2) . . ?
C141 Au3 Ag3 45.1(2) . . ?
Ag2 Au3 Ag3 75.584(17) . . ?
C133 Au3 Ag8 69.4(2) . . ?
C141 Au3 Ag8 114.2(2) . . ?
Ag2 Au3 Ag8 109.417(18) . . ?
Ag3 Au3 Ag8 71.538(17) . . ?
C133 Au3 Ag9 44.8(2) . . ?
C141 Au3 Ag9 140.4(2) . . ?
Ag2 Au3 Ag9 66.763(16) . . ?
Ag3 Au3 Ag9 113.289(18) . . ?
Ag8 Au3 Ag9 72.112(16) . . ?
C157 Au4 C149 175.6(3) . . ?
C157 Au4 Ag7 114.09(19) . . ?
C149 Au4 Ag7 66.2(2) . . ?
C157 Au4 Ag4 48.6(2) . . ?
C149 Au4 Ag4 133.0(2) . . ?
Ag7 Au4 Ag4 68.034(17) . . ?
C157 Au4 Ag3 73.6(2) . . ?
C149 Au4 Ag3 110.4(2) . . ?
Ag7 Au4 Ag3 115.815(18) . . ?
Ag4 Au4 Ag3 80.479(18) . . ?
C157 Au4 Au9 91.3(2) . . ?
C149 Au4 Au9 92.6(2) . . ?
Ag7 Au4 Au9 61.781(14) . . ?
Ag4 Au4 Au9 55.829(13) . . ?
Ag3 Au4 Au9 54.242(13) . . ?
C157 Au4 Ag8 142.1(2) . . ?
C149 Au4 Ag8 42.3(2) . . ?
Ag7 Au4 Ag8 71.726(16) . . ?
Ag4 Au4 Ag8 111.926(18) . . ?
Ag3 Au4 Ag8 70.805(17) . . ?
Au9 Au4 Ag8 57.203(13) . . ?
C173 Au5 C165 173.7(3) . . ?
C173 Au5 Ag7 133.8(2) . . ?
C165 Au5 Ag7 51.7(2) . . ?
C173 Au5 Ag6 117.2(2) . . ?
C165 Au5 Ag6 59.2(2) . . ?
Ag7 Au5 Ag6 75.835(17) . . ?
C173 Au5 Ag5 48.1(2) . . ?
C165 Au5 Ag5 130.2(2) . . ?
Ag7 Au5 Ag5 108.258(18) . . ?
Ag6 Au5 Ag5 72.215(18) . . ?
C173 Au5 Au6 88.1(2) . . ?
C165 Au5 Au6 85.6(2) . . ?
Ag7 Au5 Au6 133.257(16) . . ?
Ag6 Au5 Au6 64.898(14) . . ?
Ag5 Au5 Au6 83.560(15) . . ?
C173 Au5 Ag4 67.6(2) . . ?
C165 Au5 Ag4 118.1(2) . . ?
Ag7 Au5 Ag4 66.480(17) . . ?
Ag6 Au5 Ag4 110.960(18) . . ?
Ag5 Au5 Ag4 68.266(17) . . ?
Au6 Au5 Ag4 150.801(16) . . ?
C43 Au6 P2 173.4(2) . . ?
C43 Au6 Au5 96.3(2) . . ?
P2 Au6 Au5 89.74(5) . . ?
C43 Au6 Ag6 43.7(2) . . ?
P2 Au6 Ag6 142.86(5) . . ?
Au5 Au6 Ag6 54.995(12) . . ?
C51 Au7 P3 172.7(2) . . ?
C51 Au7 Au8 93.0(2) . . ?
P3 Au7 Au8 94.22(5) . . ?
C181 Au8 C189 171.4(3) . . ?
C181 Au8 Ag5 118.7(2) . . ?
C189 Au8 Ag5 61.2(2) . . ?
C181 Au8 Ag6 50.2(2) . . ?
C189 Au8 Ag6 132.6(2) . . ?
Ag5 Au8 Ag6 72.569(18) . . ?
C181 Au8 Ag7 77.9(2) . . ?
C189 Au8 Ag7 110.5(2) . . ?
Ag5 Au8 Ag7 108.089(18) . . ?
Ag6 Au8 Ag7 73.480(17) . . ?
C181 Au8 Ag4 142.7(2) . . ?
C189 Au8 Ag4 45.8(2) . . ?
Ag5 Au8 Ag4 69.458(17) . . ?
Ag6 Au8 Ag4 109.487(18) . . ?
Ag7 Au8 Ag4 65.525(17) . . ?
C181 Au8 Au7 94.2(2) . . ?
C189 Au8 Au7 77.8(2) . . ?
Ag5 Au8 Au7 66.233(13) . . ?
Ag6 Au8 Au7 93.312(15) . . ?
Ag7 Au8 Au7 166.780(17) . . ?
Ag4 Au8 Au7 120.222(15) . . ?
C197 Au9 C205 176.5(3) . . ?
C197 Au9 Ag3 132.7(2) . . ?
C205 Au9 Ag3 50.8(2) . . ?
C197 Au9 Ag4 108.5(2) . . ?
C205 Au9 Ag4 71.0(2) . . ?
Ag3 Au9 Ag4 84.095(18) . . ?
C197 Au9 Ag8 58.7(2) . . ?
C205 Au9 Ag8 124.7(2) . . ?
Ag3 Au9 Ag8 74.920(18) . . ?
Ag4 Au9 Ag8 117.914(19) . . ?
C197 Au9 Ag7 46.7(2) . . ?
C205 Au9 Ag7 133.9(2) . . ?
Ag3 Au9 Ag7 110.897(18) . . ?
Ag4 Au9 Ag7 64.706(17) . . ?
Ag8 Au9 Ag7 69.821(16) . . ?
C197 Au9 Au4 89.1(2) . . ?
C205 Au9 Au4 93.4(2) . . ?
Ag3 Au9 Au4 58.782(14) . . ?
Ag4 Au9 Au4 57.573(14) . . ?
Ag8 Au9 Au4 61.582(13) . . ?
Ag7 Au9 Au4 52.305(12) . . ?
C221 Au10 C213 177.3(3) . . ?
C221 Au10 Ag8 129.2(2) . . ?
C213 Au10 Ag8 53.4(2) . . ?
C221 Au10 Ag9 113.2(2) . . ?
C213 Au10 Ag9 65.9(2) . . ?
Ag8 Au10 Ag9 81.472(19) . . ?
C221 Au10 Ag2 46.7(2) . . ?
C213 Au10 Ag2 132.9(2) . . ?
Ag8 Au10 Ag2 113.217(19) . . ?
Ag9 Au10 Ag2 67.409(17) . . ?
C221 Au10 Ag3 56.0(2) . . ?
C213 Au10 Ag3 126.7(2) . . ?
Ag8 Au10 Ag3 73.641(17) . . ?
Ag9 Au10 Ag3 115.969(18) . . ?
Ag2 Au10 Ag3 70.339(15) . . ?
C237 Au11 C229 171.8(3) . . ?
C237 Au11 Ag9 135.7(2) . . ?
C229 Au11 Ag9 52.3(2) . . ?
C237 Au11 Ag10 115.6(2) . . ?
C229 Au11 Ag10 61.0(2) . . ?
Ag9 Au11 Ag10 80.414(18) . . ?
C237 Au11 Ag1 49.3(2) . . ?
C229 Au11 Ag1 129.1(2) . . ?
Ag9 Au11 Ag1 114.173(19) . . ?
Ag10 Au11 Ag1 68.560(17) . . ?
C237 Au11 Ag2 65.7(2) . . ?
C229 Au11 Ag2 122.4(2) . . ?
Ag9 Au11 Ag2 70.019(17) . . ?
Ag10 Au11 Ag2 113.737(18) . . ?
Ag1 Au11 Ag2 72.095(16) . . ?
C237 Au11 Au12 89.8(2) . . ?
C229 Au11 Au12 82.0(2) . . ?
Ag9 Au11 Au12 132.971(16) . . ?
Ag10 Au11 Au12 66.072(14) . . ?
Ag1 Au11 Au12 84.000(14) . . ?
Ag2 Au11 Au12 153.248(16) . . ?
C101 Au12 P4 172.8(2) . . ?
C101 Au12 Au11 95.5(2) . . ?
P4 Au12 Au11 91.12(5) . . ?
C101 Au12 Ag10 42.0(2) . . ?
P4 Au12 Ag10 143.36(5) . . ?
Au11 Au12 Ag10 55.481(12) . . ?
C109 Ag1 C237 161.5(3) . . ?
C109 Ag1 C110 28.9(3) . . ?
C237 Ag1 C110 132.9(3) . . ?
C109 Ag1 C238 140.8(3) . . ?
C237 Ag1 C238 27.9(2) . . ?
C110 Ag1 C238 114.3(3) . . ?
C109 Ag1 C125 106.1(3) . . ?
C237 Ag1 C125 92.1(2) . . ?
C110 Ag1 C125 132.0(2) . . ?
C238 Ag1 C125 99.0(2) . . ?
C109 Ag1 Au2 96.8(2) . . ?
C237 Ag1 Au2 99.17(19) . . ?
C110 Ag1 Au2 124.1(2) . . ?
C238 Ag1 Au2 121.58(17) . . ?
C125 Ag1 Au2 41.00(16) . . ?
C109 Ag1 Au11 141.65(18) . . ?
C237 Ag1 Au11 40.67(19) . . ?
C110 Ag1 Au11 136.90(16) . . ?
C238 Ag1 Au11 68.37(18) . . ?
C125 Ag1 Au11 86.32(15) . . ?
Au2 Ag1 Au11 68.729(14) . . ?
C109 Ag1 Au1 38.8(2) . . ?
C237 Ag1 Au1 159.29(18) . . ?
C110 Ag1 Au1 67.6(2) . . ?
C238 Ag1 Au1 159.75(17) . . ?
C125 Ag1 Au1 69.53(15) . . ?
Au2 Ag1 Au1 60.781(14) . . ?
Au11 Ag1 Au1 125.27(2) . . ?
C125 Ag2 C221 171.4(3) . . ?
C125 Ag2 C222 143.4(3) . . ?
C221 Ag2 C222 28.1(2) . . ?
C125 Ag2 C126 27.1(2) . . ?
C221 Ag2 C126 144.3(3) . . ?
C222 Ag2 C126 116.6(2) . . ?
C125 Ag2 Au3 92.1(2) . . ?
C221 Ag2 Au3 92.0(2) . . ?
C222 Ag2 Au3 108.80(16) . . ?
C126 Ag2 Au3 102.75(16) . . ?
C125 Ag2 Au11 93.12(18) . . ?
C221 Ag2 Au11 92.27(18) . . ?
C222 Ag2 Au11 105.29(16) . . ?
C126 Ag2 Au11 111.02(16) . . ?
Au3 Ag2 Au11 112.54(2) . . ?
C125 Ag2 Au2 39.33(19) . . ?
C221 Ag2 Au2 149.2(2) . . ?
C222 Ag2 Au2 171.19(16) . . ?
C126 Ag2 Au2 66.44(17) . . ?
Au3 Ag2 Au2 77.620(16) . . ?
Au11 Ag2 Au2 66.224(14) . . ?
C125 Ag2 Au10 149.40(19) . . ?
C221 Ag2 Au10 39.1(2) . . ?
C222 Ag2 Au10 67.14(18) . . ?
C126 Ag2 Au10 171.20(16) . . ?
Au3 Ag2 Au10 68.493(14) . . ?
Au11 Ag2 Au10 74.287(15) . . ?
Au2 Ag2 Au10 111.097(19) . . ?
C141 Ag3 C205 168.3(3) . . ?
C141 Ag3 C142 28.1(2) . . ?
C205 Ag3 C142 140.6(3) . . ?
C141 Ag3 Au9 144.1(2) . . ?
C205 Ag3 Au9 43.0(2) . . ?
C142 Ag3 Au9 157.26(17) . . ?
C141 Ag3 Au4 84.33(19) . . ?
C205 Ag3 Au4 94.6(2) . . ?
C142 Ag3 Au4 90.87(17) . . ?
Au9 Ag3 Au4 66.976(15) . . ?
C141 Ag3 Au3 38.5(2) . . ?
C205 Ag3 Au3 152.1(2) . . ?
C142 Ag3 Au3 66.50(17) . . ?
Au9 Ag3 Au3 110.01(2) . . ?
Au4 Ag3 Au3 75.009(16) . . ?
C141 Ag3 Au10 95.73(19) . . ?
C205 Ag3 Au10 95.8(2) . . ?
C142 Ag3 Au10 120.42(16) . . ?
Au9 Ag3 Au10 72.534(15) . . ?
Au4 Ag3 Au10 104.476(19) . . ?
Au3 Ag3 Au10 63.102(13) . . ?
C189 Ag4 C157 172.9(3) . . ?
C189 Ag4 C158 145.1(3) . . ?
C157 Ag4 C158 27.9(2) . . ?
C189 Ag4 Au9 91.92(19) . . ?
C157 Ag4 Au9 94.32(18) . . ?
C158 Ag4 Au9 114.68(18) . . ?
C189 Ag4 Au4 146.4(2) . . ?
C157 Ag4 Au4 40.37(19) . . ?
C158 Ag4 Au4 68.18(17) . . ?
Au9 Ag4 Au4 66.598(14) . . ?
C189 Ag4 Au8 39.1(2) . . ?
C157 Ag4 Au8 145.95(19) . . ?
C158 Ag4 Au8 160.76(17) . . ?
Au9 Ag4 Au8 79.260(16) . . ?
Au4 Ag4 Au8 108.87(2) . . ?
C189 Ag4 Au5 95.1(2) . . ?
C157 Ag4 Au5 85.55(19) . . ?
C158 Ag4 Au5 93.99(17) . . ?
Au9 Ag4 Au5 114.10(2) . . ?
Au4 Ag4 Au5 72.871(16) . . ?
Au8 Ag4 Au5 67.470(15) . . ?
C189 Ag4 Ag7 94.0(2) . . ?
C157 Ag4 Ag7 92.13(19) . . ?
C158 Ag4 Ag7 118.21(17) . . ?
Au9 Ag4 Ag7 60.728(16) . . ?
Au4 Ag4 Ag7 53.466(15) . . ?
Au8 Ag4 Ag7 55.418(15) . . ?
Au5 Ag4 Ag7 53.451(15) . . ?
C51 Ag5 C173 162.2(3) . . ?
C51 Ag5 C52 29.6(2) . . ?
C173 Ag5 C52 132.9(3) . . ?
C51 Ag5 C174 139.7(2) . . ?
C173 Ag5 C174 28.2(2) . . ?
C52 Ag5 C174 112.4(2) . . ?
C51 Ag5 C189 98.6(3) . . ?
C173 Ag5 C189 98.8(2) . . ?
C52 Ag5 C189 125.7(2) . . ?
C174 Ag5 C189 107.4(2) . . ?
C51 Ag5 Au8 92.54(19) . . ?
C173 Ag5 Au8 102.99(19) . . ?
C52 Ag5 Au8 120.38(18) . . ?
C174 Ag5 Au8 127.19(17) . . ?
C189 Ag5 Au8 40.64(18) . . ?
C51 Ag5 Au5 143.6(2) . . ?
C173 Ag5 Au5 40.47(19) . . ?
C52 Ag5 Au5 139.53(18) . . ?
C174 Ag5 Au5 68.50(17) . . ?
C189 Ag5 Au5 88.80(17) . . ?
Au8 Ag5 Au5 70.266(15) . . ?
C43 Ag6 C181 150.9(3) . . ?
C43 Ag6 C44 29.6(2) . . ?
C181 Ag6 C44 122.3(3) . . ?
C43 Ag6 C165 109.7(3) . . ?
C181 Ag6 C165 99.4(3) . . ?
C44 Ag6 C165 137.4(2) . . ?
C43 Ag6 C182 135.6(3) . . ?
C181 Ag6 C182 27.4(3) . . ?
C44 Ag6 C182 107.1(3) . . ?
C165 Ag6 C182 106.8(2) . . ?
C43 Ag6 Au5 95.38(19) . . ?
C181 Ag6 Au5 105.7(2) . . ?
C44 Ag6 Au5 122.33(17) . . ?
C165 Ag6 Au5 41.92(18) . . ?
C182 Ag6 Au5 128.90(19) . . ?
C43 Ag6 Au8 134.79(19) . . ?
C181 Ag6 Au8 41.2(2) . . ?
C44 Ag6 Au8 126.54(18) . . ?
C165 Ag6 Au8 89.78(17) . . ?
C182 Ag6 Au8 68.4(2) . . ?
Au5 Ag6 Au8 72.081(15) . . ?
C43 Ag6 Au6 37.52(19) . . ?
C181 Ag6 Au6 164.5(2) . . ?
C44 Ag6 Au6 67.08(18) . . ?
C165 Ag6 Au6 74.57(16) . . ?
C182 Ag6 Au6 168.0(2) . . ?
Au5 Ag6 Au6 60.107(13) . . ?
Au8 Ag6 Au6 123.54(2) . . ?
C165 Ag7 C197 164.5(3) . . ?
C165 Ag7 C198 136.2(3) . . ?
C197 Ag7 C198 28.5(2) . . ?
C165 Ag7 Au4 99.74(19) . . ?
C197 Ag7 Au4 94.03(19) . . ?
C198 Ag7 Au4 115.37(18) . . ?
C165 Ag7 Au5 43.0(2) . . ?
C197 Ag7 Au5 148.9(2) . . ?
C198 Ag7 Au5 162.36(17) . . ?
Au4 Ag7 Au5 78.927(16) . . ?
C165 Ag7 Au8 94.91(19) . . ?
C197 Ag7 Au8 84.99(18) . . ?
C198 Ag7 Au8 91.42(18) . . ?
Au4 Ag7 Au8 117.54(2) . . ?
Au5 Ag7 Au8 72.102(15) . . ?
C165 Ag7 Au9 157.1(2) . . ?
C197 Ag7 Au9 37.8(2) . . ?
C198 Ag7 Au9 66.3(2) . . ?
Au4 Ag7 Au9 65.914(14) . . ?
Au5 Ag7 Au9 114.56(2) . . ?
Au8 Ag7 Au9 77.912(16) . . ?
C165 Ag7 Ag4 103.1(2) . . ?
C197 Ag7 Ag4 90.2(2) . . ?
C198 Ag7 Ag4 117.1(2) . . ?
Au4 Ag7 Ag4 58.500(15) . . ?
Au5 Ag7 Ag4 60.069(16) . . ?
Au8 Ag7 Ag4 59.056(15) . . ?
Au9 Ag7 Ag4 54.566(15) . . ?
C149 Ag8 C213 167.6(3) . . ?
C149 Ag8 C150 29.0(2) . . ?
C213 Ag8 C150 139.2(3) . . ?
C149 Ag8 Au10 142.89(18) . . ?
C213 Ag8 Au10 44.5(2) . . ?
C150 Ag8 Au10 157.71(16) . . ?
C149 Ag8 Au9 90.81(19) . . ?
C213 Ag8 Au9 101.5(2) . . ?
C150 Ag8 Au9 115.78(17) . . ?
Au10 Ag8 Au9 76.340(17) . . ?
C149 Ag8 Au3 80.94(18) . . ?
C213 Ag8 Au3 97.73(19) . . ?
C150 Ag8 Au3 89.57(16) . . ?
Au10 Ag8 Au3 68.871(15) . . ?
Au9 Ag8 Au3 103.422(19) . . ?
C149 Ag8 Au4 35.81(19) . . ?
C213 Ag8 Au4 155.1(2) . . ?
C150 Ag8 Au4 64.75(17) . . ?
Au10 Ag8 Au4 111.07(2) . . ?
Au9 Ag8 Au4 61.215(13) . . ?
Au3 Ag8 Au4 71.531(14) . . ?
C229 Ag9 C133 162.2(3) . . ?
C229 Ag9 C134 135.9(3) . . ?
C133 Ag9 C134 28.3(2) . . ?
C229 Ag9 Au11 44.50(19) . . ?
C133 Ag9 Au11 143.90(18) . . ?
C134 Ag9 Au11 158.66(16) . . ?
C229 Ag9 Au10 103.85(19) . . ?
C133 Ag9 Au10 93.78(18) . . ?
C134 Ag9 Au10 114.33(16) . . ?
Au11 Ag9 Au10 80.860(18) . . ?
C229 Ag9 Au2 92.10(17) . . ?
C133 Ag9 Au2 82.16(17) . . ?
C134 Ag9 Au2 90.49(16) . . ?
Au11 Ag9 Au2 68.810(15) . . ?
Au10 Ag9 Au2 116.00(2) . . ?
C229 Ag9 Au3 155.06(19) . . ?
C133 Ag9 Au3 37.53(18) . . ?
C134 Ag9 Au3 65.84(17) . . ?
Au11 Ag9 Au3 110.604(19) . . ?
Au10 Ag9 Au3 67.036(14) . . ?
Au2 Ag9 Au3 73.146(14) . . ?
C101 Ag10 C117 165.6(3) . . ?
C101 Ag10 C102 29.8(3) . . ?
C117 Ag10 C102 136.8(3) . . ?
C101 Ag10 C118 145.3(3) . . ?
C117 Ag10 C118 28.4(2) . . ?
C102 Ag10 C118 117.6(3) . . ?
C101 Ag10 C229 102.4(3) . . ?
C117 Ag10 C229 92.0(2) . . ?
C102 Ag10 C229 128.5(2) . . ?
C118 Ag10 C229 98.5(2) . . ?
C101 Ag10 Au11 92.8(2) . . ?
C117 Ag10 Au11 98.3(2) . . ?
C102 Ag10 Au11 121.7(2) . . ?
C118 Ag10 Au11 120.72(17) . . ?
C229 Ag10 Au11 40.73(16) . . ?
C101 Ag10 Au2 138.60(19) . . ?
C117 Ag10 Au2 41.1(2) . . ?
C102 Ag10 Au2 137.90(18) . . ?
C118 Ag10 Au2 69.33(18) . . ?
C229 Ag10 Au2 87.23(16) . . ?
Au11 Ag10 Au2 68.487(14) . . ?
C101 Ag10 Au12 36.1(2) . . ?
C117 Ag10 Au12 156.6(2) . . ?
C102 Ag10 Au12 65.9(2) . . ?
C118 Ag10 Au12 161.94(17) . . ?
C229 Ag10 Au12 69.13(15) . . ?
Au11 Ag10 Au12 58.447(13) . . ?
Au2 Ag10 Au12 121.22(2) . . ?
C13 P1 C7 106.3(4) . . ?
C13 P1 C1 106.1(3) . . ?
C7 P1 C1 105.3(4) . . ?
C13 P1 Au1 114.9(3) . . ?
C7 P1 Au1 111.9(3) . . ?
C1 P1 Au1 111.7(3) . . ?
C28 P2 C31 108.8(3) . . ?
C28 P2 C37 105.9(3) . . ?
C31 P2 C37 104.5(3) . . ?
C28 P2 Au6 115.1(2) . . ?
C31 P2 Au6 110.9(2) . . ?
C37 P2 Au6 111.0(2) . . ?
C59 P3 C65 106.3(4) . . ?
C59 P3 C71 103.5(3) . . ?
C65 P3 C71 108.2(3) . . ?
C59 P3 Au7 111.8(3) . . ?
C65 P3 Au7 114.9(3) . . ?
C71 P3 Au7 111.5(2) . . ?
C89 P4 C86 104.2(3) . . ?
C89 P4 C95 107.1(3) . . ?
C86 P4 C95 105.0(3) . . ?
C89 P4 Au12 114.1(2) . . ?
C86 P4 Au12 114.6(2) . . ?
C95 P4 Au12 111.1(2) . . ?
F5 P5 F4 91.5(10) . . ?
F5 P5 F1 93.9(7) . . ?
F4 P5 F1 89.3(6) . . ?
F5 P5 F3 178.8(6) . . ?
F4 P5 F3 89.1(7) . . ?
F1 P5 F3 87.2(4) . . ?
F5 P5 F6 91.2(9) . . ?
F4 P5 F6 176.7(8) . . ?
F1 P5 F6 92.4(5) . . ?
F3 P5 F6 88.2(5) . . ?
F5 P5 F2 87.5(7) . . ?
F4 P5 F2 90.7(5) . . ?
F1 P5 F2 178.6(5) . . ?
F3 P5 F2 91.4(5) . . ?
F6 P5 F2 87.5(4) . . ?
C6 C1 C2 119.5(7) . . ?
C6 C1 P1 119.8(6) . . ?
C2 C1 P1 120.7(6) . . ?
C3 C2 C1 120.0(8) . . ?
C3 C2 H2 120.0 . . ?
C1 C2 H2 120.0 . . ?
C4 C3 C2 120.2(9) . . ?
C4 C3 H3 119.9 . . ?
C2 C3 H3 119.9 . . ?
C3 C4 C5 119.7(8) . . ?
C3 C4 H4 120.2 . . ?
C5 C4 H4 120.2 . . ?
C4 C5 C6 119.7(9) . . ?
C4 C5 H5 120.2 . . ?
C6 C5 H5 120.2 . . ?
C1 C6 C5 120.9(8) . . ?
C1 C6 H6 119.6 . . ?
C5 C6 H6 119.6 . . ?
C8 C7 C12 118.8(8) . . ?
C8 C7 P1 121.7(7) . . ?
C12 C7 P1 119.5(7) . . ?
C9 C8 C7 119.6(10) . . ?
C9 C8 H8 120.2 . . ?
C7 C8 H8 120.2 . . ?
C10 C9 C8 121.9(11) . . ?
C10 C9 H9 119.1 . . ?
C8 C9 H9 119.1 . . ?
C9 C10 C11 118.5(10) . . ?
C9 C10 H10 120.7 . . ?
C11 C10 H10 120.7 . . ?
C12 C11 C10 120.9(9) . . ?
C12 C11 H11 119.5 . . ?
C10 C11 H11 119.5 . . ?
C11 C12 C7 120.2(9) . . ?
C11 C12 H12 119.9 . . ?
C7 C12 H12 119.9 . . ?
C18 C13 C14 118.3(7) . . ?
C18 C13 P1 121.1(6) . . ?
C14 C13 P1 120.5(6) . . ?
C15 C14 C13 120.1(7) . . ?
C15 C14 H14 120.0 . . ?
C13 C14 H14 120.0 . . ?
C14 C15 C16 120.9(7) . . ?
C14 C15 H15 119.6 . . ?
C16 C15 H15 119.6 . . ?
C15 C16 C17 118.4(7) . . ?
C15 C16 C19 119.7(7) . . ?
C17 C16 C19 121.9(7) . . ?
C18 C17 C16 120.5(7) . . ?
C18 C17 H17 119.7 . . ?
C16 C17 H17 119.7 . . ?
C17 C18 C13 121.7(7) . . ?
C17 C18 H18 119.1 . . ?
C13 C18 H18 119.1 . . ?
C20 C19 C24 117.2(6) . . ?
C20 C19 C16 120.9(6) . . ?
C24 C19 C16 121.9(6) . . ?
C21 C20 C19 120.7(7) . . ?
C21 C20 H20 119.6 . . ?
C19 C20 H20 119.6 . . ?
C20 C21 C22 122.9(7) . . ?
C20 C21 H21 118.5 . . ?
C22 C21 H21 118.5 . . ?
C21 C22 C23 116.2(6) . . ?
C21 C22 C25 120.4(7) . . ?
C23 C22 C25 123.4(6) . . ?
C24 C23 C22 121.5(7) . . ?
C24 C23 H23 119.3 . . ?
C22 C23 H23 119.3 . . ?
C23 C24 C19 121.3(7) . . ?
C23 C24 H24 119.3 . . ?
C19 C24 H24 119.3 . . ?
C26 C25 C30 117.2(7) . . ?
C26 C25 C22 119.7(7) . . ?
C30 C25 C22 123.0(6) . . ?
C27 C26 C25 121.9(7) . . ?
C27 C26 H26 119.0 . . ?
C25 C26 H26 119.0 . . ?
C26 C27 C28 119.8(7) . . ?
C26 C27 H27 120.1 . . ?
C28 C27 H27 120.1 . . ?
C29 C28 C27 118.5(6) . . ?
C29 C28 P2 124.7(5) . . ?
C27 C28 P2 116.7(5) . . ?
C30 C29 C28 121.3(7) . . ?
C30 C29 H29 119.4 . . ?
C28 C29 H29 119.4 . . ?
C29 C30 C25 121.2(7) . . ?
C29 C30 H30 119.4 . . ?
C25 C30 H30 119.4 . . ?
C32 C31 C36 119.2(7) . . ?
C32 C31 P2 119.3(5) . . ?
C36 C31 P2 121.5(6) . . ?
C33 C32 C31 120.7(7) . . ?
C33 C32 H32 119.7 . . ?
C31 C32 H32 119.7 . . ?
C34 C33 C32 120.2(7) . . ?
C34 C33 H33 119.9 . . ?
C32 C33 H33 119.9 . . ?
C33 C34 C35 119.9(7) . . ?
C33 C34 H34 120.0 . . ?
C35 C34 H34 120.0 . . ?
C36 C35 C34 120.4(7) . . ?
C36 C35 H35 119.8 . . ?
C34 C35 H35 119.8 . . ?
C35 C36 C31 119.6(7) . . ?
C35 C36 H36 120.2 . . ?
C31 C36 H36 120.2 . . ?
C42 C37 C38 119.5(7) . . ?
C42 C37 P2 124.9(6) . . ?
C38 C37 P2 115.4(6) . . ?
C39 C38 C37 120.5(8) . . ?
C39 C38 H38 119.8 . . ?
C37 C38 H38 119.8 . . ?
C38 C39 C40 120.0(8) . . ?
C38 C39 H39 120.0 . . ?
C40 C39 H39 120.0 . . ?
C39 C40 C41 120.7(9) . . ?
C39 C40 H40 119.7 . . ?
C41 C40 H40 119.7 . . ?
C40 C41 C42 119.5(8) . . ?
C40 C41 H41 120.3 . . ?
C42 C41 H41 120.3 . . ?
C37 C42 C41 119.9(8) . . ?
C37 C42 H42 120.1 . . ?
C41 C42 H42 120.1 . . ?
C44 C43 Au6 175.7(7) . . ?
C44 C43 Ag6 83.6(5) . . ?
Au6 C43 Ag6 98.8(3) . . ?
C43 C44 C45 171.9(8) . . ?
C43 C44 Ag6 66.8(5) . . ?
C45 C44 Ag6 121.3(5) . . ?
C46 C45 C50 118.6(8) . . ?
C46 C45 C44 120.0(8) . . ?
C50 C45 C44 121.4(7) . . ?
C45 C46 C47 120.2(9) . . ?
C45 C46 H46 119.9 . . ?
C47 C46 H46 119.9 . . ?
C48 C47 C46 119.8(9) . . ?
C48 C47 H47 120.1 . . ?
C46 C47 H47 120.1 . . ?
C49 C48 C47 120.4(8) . . ?
C49 C48 H48 119.8 . . ?
C47 C48 H48 119.8 . . ?
C48 C49 C50 121.5(9) . . ?
C48 C49 H49 119.2 . . ?
C50 C49 H49 119.2 . . ?
C49 C50 C45 119.5(9) . . ?
C49 C50 H50 120.3 . . ?
C45 C50 H50 120.3 . . ?
C52 C51 Au7 171.7(6) . . ?
C52 C51 Ag5 83.8(5) . . ?
Au7 C51 Ag5 104.5(3) . . ?
C51 C52 C53 171.0(8) . . ?
C51 C52 Ag5 66.7(5) . . ?
C53 C52 Ag5 122.3(5) . . ?
C54 C53 C58 118.9(7) . . ?
C54 C53 C52 120.8(7) . . ?
C58 C53 C52 120.3(7) . . ?
C55 C54 C53 120.9(8) . . ?
C55 C54 H54 119.5 . . ?
C53 C54 H54 119.5 . . ?
C54 C55 C56 119.4(8) . . ?
C54 C55 H55 120.3 . . ?
C56 C55 H55 120.3 . . ?
C55 C56 C57 121.0(8) . . ?
C55 C56 H56 119.5 . . ?
C57 C56 H56 119.5 . . ?
C56 C57 C58 119.6(8) . . ?
C56 C57 H57 120.2 . . ?
C58 C57 H57 120.2 . . ?
C57 C58 C53 120.2(8) . . ?
C57 C58 H58 119.9 . . ?
C53 C58 H58 119.9 . . ?
C60 C59 C64 118.7(7) . . ?
C60 C59 P3 120.1(6) . . ?
C64 C59 P3 121.2(6) . . ?
C61 C60 C59 120.2(8) . . ?
C61 C60 H60 119.9 . . ?
C59 C60 H60 119.9 . . ?
C62 C61 C60 120.7(8) . . ?
C62 C61 H61 119.7 . . ?
C60 C61 H61 119.7 . . ?
C61 C62 C63 119.5(8) . . ?
C61 C62 H62 120.3 . . ?
C63 C62 H62 120.3 . . ?
C64 C63 C62 120.5(8) . . ?
C64 C63 H63 119.8 . . ?
C62 C63 H63 119.8 . . ?
C63 C64 C59 120.5(7) . . ?
C63 C64 H64 119.7 . . ?
C59 C64 H64 119.7 . . ?
C70 C65 C66 119.6(8) . . ?
C70 C65 P3 118.5(6) . . ?
C66 C65 P3 122.0(7) . . ?
C67 C66 C65 119.4(9) . . ?
C67 C66 H66 120.3 . . ?
C65 C66 H66 120.3 . . ?
C68 C67 C66 121.2(9) . . ?
C68 C67 H67 119.4 . . ?
C66 C67 H67 119.4 . . ?
C67 C68 C69 121.6(9) . . ?
C67 C68 H68 119.2 . . ?
C69 C68 H68 119.2 . . ?
C68 C69 C70 118.8(9) . . ?
C68 C69 H69 120.6 . . ?
C70 C69 H69 120.6 . . ?
C65 C70 C69 119.4(9) . . ?
C65 C70 H70 120.3 . . ?
C69 C70 H70 120.3 . . ?
C72 C71 C76 118.7(7) . . ?
C72 C71 P3 123.5(6) . . ?
C76 C71 P3 117.7(5) . . ?
C73 C72 C71 119.5(7) . . ?
C73 C72 H72 120.2 . . ?
C71 C72 H72 120.2 . . ?
C72 C73 C74 122.3(7) . . ?
C72 C73 H73 118.9 . . ?
C74 C73 H73 118.9 . . ?
C73 C74 C75 117.6(6) . . ?
C73 C74 C77 121.6(6) . . ?
C75 C74 C77 120.8(7) . . ?
C76 C75 C74 120.6(7) . . ?
C76 C75 H75 119.7 . . ?
C74 C75 H75 119.7 . . ?
C75 C76 C71 121.3(7) . . ?
C75 C76 H76 119.3 . . ?
C71 C76 H76 119.3 . . ?
C78 C77 C82 117.7(7) . . ?
C78 C77 C74 121.2(7) . . ?
C82 C77 C74 121.1(7) . . ?
C79 C78 C77 122.1(7) . . ?
C79 C78 H78 119.0 . . ?
C77 C78 H78 119.0 . . ?
C78 C79 C80 120.5(7) . . ?
C78 C79 H79 119.8 . . ?
C80 C79 H79 119.8 . . ?
C81 C80 C79 117.6(7) . . ?
C81 C80 C83 121.7(7) . . ?
C79 C80 C83 120.8(7) . . ?
C82 C81 C80 121.3(7) . . ?
C82 C81 H81 119.3 . . ?
C80 C81 H81 119.3 . . ?
C81 C82 C77 120.9(7) . . ?
C81 C82 H82 119.6 . . ?
C77 C82 H82 119.6 . . ?
C88 C83 C84 118.2(7) . . ?
C88 C83 C80 121.1(7) . . ?
C84 C83 C80 120.7(7) . . ?
C85 C84 C83 121.0(7) . . ?
C85 C84 H84 119.5 . . ?
C83 C84 H84 119.5 . . ?
C84 C85 C86 120.4(7) . . ?
C84 C85 H85 119.8 . . ?
C86 C85 H85 119.8 . . ?
C87 C86 C85 119.1(6) . . ?
C87 C86 P4 121.9(6) . . ?
C85 C86 P4 118.9(5) . . ?
C86 C87 C88 120.2(7) . . ?
C86 C87 H87 119.9 . . ?
C88 C87 H87 119.9 . . ?
C87 C88 C83 121.0(7) . . ?
C87 C88 H88 119.5 . . ?
C83 C88 H88 119.5 . . ?
C90 C89 C94 118.4(8) . . ?
C90 C89 P4 119.2(6) . . ?
C94 C89 P4 122.2(6) . . ?
C91 C90 C89 121.2(8) . . ?
C91 C90 H90 119.4 . . ?
C89 C90 H90 119.4 . . ?
C90 C91 C92 119.7(8) . . ?
C90 C91 H91 120.2 . . ?
C92 C91 H91 120.2 . . ?
C91 C92 C93 120.2(9) . . ?
C91 C92 H92 119.9 . . ?
C93 C92 H92 119.9 . . ?
C94 C93 C92 119.9(8) . . ?
C94 C93 H93 120.0 . . ?
C92 C93 H93 120.0 . . ?
C93 C94 C89 120.5(8) . . ?
C93 C94 H94 119.7 . . ?
C89 C94 H94 119.7 . . ?
C96 C95 C100 119.3(7) . . ?
C96 C95 P4 123.7(5) . . ?
C100 C95 P4 117.0(6) . . ?
C95 C96 C97 120.4(7) . . ?
C95 C96 H96 119.8 . . ?
C97 C96 H96 119.8 . . ?
C98 C97 C96 120.3(7) . . ?
C98 C97 H97 119.9 . . ?
C96 C97 H97 119.9 . . ?
C97 C98 C99 119.7(7) . . ?
C97 C98 H98 120.2 . . ?
C99 C98 H98 120.2 . . ?
C100 C99 C98 120.8(8) . . ?
C100 C99 H99 119.6 . . ?
C98 C99 H99 119.6 . . ?
C99 C100 C95 119.4(7) . . ?
C99 C100 H100 120.3 . . ?
C95 C100 H100 120.3 . . ?
C102 C101 Au12 175.6(6) . . ?
C102 C101 Ag10 81.2(5) . . ?
Au12 C101 Ag10 101.9(3) . . ?
C101 C102 C103 170.8(8) . . ?
C101 C102 Ag10 68.9(5) . . ?
C103 C102 Ag10 117.6(5) . . ?
C108 C103 C104 118.9(7) . . ?
C108 C103 C102 122.0(7) . . ?
C104 C103 C102 119.1(7) . . ?
C105 C104 C103 119.5(8) . . ?
C105 C104 H104 120.2 . . ?
C103 C104 H104 120.2 . . ?
C106 C105 C104 121.1(9) . . ?
C106 C105 H105 119.5 . . ?
C104 C105 H105 119.5 . . ?
C105 C106 C107 119.3(9) . . ?
C105 C106 H106 120.4 . . ?
C107 C106 H106 120.4 . . ?
C108 C107 C106 120.6(8) . . ?
C108 C107 H107 119.7 . . ?
C106 C107 H107 119.7 . . ?
C107 C108 C103 120.5(8) . . ?
C107 C108 H108 119.8 . . ?
C103 C108 H108 119.8 . . ?
C110 C109 Au1 176.3(6) . . ?
C110 C109 Ag1 85.2(5) . . ?
Au1 C109 Ag1 96.6(3) . . ?
C109 C110 C111 171.9(8) . . ?
C109 C110 Ag1 65.9(5) . . ?
C111 C110 Ag1 121.7(5) . . ?
C116 C111 C112 117.1(7) . . ?
C116 C111 C110 120.9(7) . . ?
C112 C111 C110 122.0(7) . . ?
C113 C112 C111 120.6(7) . . ?
C113 C112 H112 119.7 . . ?
C111 C112 H112 119.7 . . ?
C114 C113 C112 121.2(8) . . ?
C114 C113 H113 119.4 . . ?
C112 C113 H113 119.4 . . ?
C113 C114 C115 119.0(8) . . ?
C113 C114 H114 120.5 . . ?
C115 C114 H114 120.5 . . ?
C116 C115 C114 120.4(8) . . ?
C116 C115 H115 119.8 . . ?
C114 C115 H115 119.8 . . ?
C115 C116 C111 121.6(8) . . ?
C115 C116 H116 119.2 . . ?
C111 C116 H116 119.2 . . ?
C118 C117 Au2 172.3(6) . . ?
C118 C117 Ag10 89.0(5) . . ?
Au2 C117 Ag10 89.9(3) . . ?
C117 C118 C119 169.6(9) . . ?
C117 C118 Ag10 62.6(5) . . ?
C119 C118 Ag10 126.1(6) . . ?
C124 C119 C120 118.8(8) . . ?
C124 C119 C118 121.3(9) . . ?
C120 C119 C118 119.6(8) . . ?
C121 C120 C119 119.6(10) . . ?
C121 C120 H120 120.2 . . ?
C119 C120 H120 120.2 . . ?
C120 C121 C122 120.7(11) . . ?
C120 C121 H121 119.7 . . ?
C122 C121 H121 119.7 . . ?
C123 C122 C121 120.4(11) . . ?
C123 C122 H122 119.8 . . ?
C121 C122 H122 119.8 . . ?
C122 C123 C124 120.0(11) . . ?
C122 C123 H123 120.0 . . ?
C124 C123 H123 120.0 . . ?
C123 C124 C119 120.6(10) . . ?
C123 C124 H124 119.7 . . ?
C119 C124 H124 119.7 . . ?
C126 C125 Au2 172.3(6) . . ?
C126 C125 Ag2 93.5(5) . . ?
Au2 C125 Ag2 94.1(3) . . ?
C126 C125 Ag1 100.8(6) . . ?
Au2 C125 Ag1 77.1(2) . . ?
Ag2 C125 Ag1 92.8(2) . . ?
C125 C126 C127 176.1(8) . . ?
C125 C126 Ag2 59.4(4) . . ?
C127 C126 Ag2 124.0(5) . . ?
C132 C127 C128 118.8(7) . . ?
C132 C127 C126 121.1(7) . . ?
C128 C127 C126 120.1(7) . . ?
C129 C128 C127 119.7(8) . . ?
C129 C128 H128 120.2 . . ?
C127 C128 H128 120.2 . . ?
C128 C129 C130 120.2(8) . . ?
C128 C129 H129 119.9 . . ?
C130 C129 H129 119.9 . . ?
C131 C130 C129 119.9(8) . . ?
C131 C130 H130 120.1 . . ?
C129 C130 H130 120.1 . . ?
C130 C131 C132 120.7(8) . . ?
C130 C131 H131 119.6 . . ?
C132 C131 H131 119.6 . . ?
C127 C132 C131 120.7(8) . . ?
C127 C132 H132 119.7 . . ?
C131 C132 H132 119.7 . . ?
C134 C133 Au3 175.8(7) . . ?
C134 C133 Ag9 86.2(5) . . ?
Au3 C133 Ag9 97.6(3) . . ?
C133 C134 C135 172.4(8) . . ?
C133 C134 Ag9 65.4(5) . . ?
C135 C134 Ag9 122.0(5) . . ?
C136 C135 C140 118.7(8) . . ?
C136 C135 C134 120.3(7) . . ?
C140 C135 C134 121.0(7) . . ?
C135 C136 C137 120.7(8) . . ?
C135 C136 H136 119.6 . . ?
C137 C136 H136 119.6 . . ?
C136 C137 C138 120.3(9) . . ?
C136 C137 H137 119.8 . . ?
C138 C137 H137 119.8 . . ?
C139 C138 C137 119.2(8) . . ?
C139 C138 H138 120.4 . . ?
C137 C138 H138 120.4 . . ?
C140 C139 C138 120.5(9) . . ?
C140 C139 H139 119.8 . . ?
C138 C139 H139 119.8 . . ?
C139 C140 C135 120.6(9) . . ?
C139 C140 H140 119.7 . . ?
C135 C140 H140 119.7 . . ?
C142 C141 Au3 172.9(7) . . ?
C142 C141 Ag3 89.1(5) . . ?
Au3 C141 Ag3 96.4(3) . . ?
C141 C142 C143 172.3(8) . . ?
C141 C142 Ag3 62.8(5) . . ?
C143 C142 Ag3 124.5(5) . . ?
C144 C143 C148 118.6(8) . . ?
C144 C143 C142 119.9(7) . . ?
C148 C143 C142 121.5(8) . . ?
C143 C144 C145 119.8(9) . . ?
C143 C144 H144 120.1 . . ?
C145 C144 H144 120.1 . . ?
C146 C145 C144 121.4(9) . . ?
C146 C145 H145 119.3 . . ?
C144 C145 H145 119.3 . . ?
C145 C146 C147 119.3(9) . . ?
C145 C146 H146 120.3 . . ?
C147 C146 H146 120.3 . . ?
C146 C147 C148 120.0(10) . . ?
C146 C147 H147 120.0 . . ?
C148 C147 H147 120.0 . . ?
C143 C148 C147 120.7(9) . . ?
C143 C148 H148 119.7 . . ?
C147 C148 H148 119.7 . . ?
C150 C149 Au4 173.4(7) . . ?
C150 C149 Ag8 83.8(5) . . ?
Au4 C149 Ag8 101.9(3) . . ?
C149 C150 C151 169.7(8) . . ?
C149 C150 Ag8 67.2(5) . . ?
C151 C150 Ag8 123.0(5) . . ?
C152 C151 C156 118.9(7) . . ?
C152 C151 C150 119.3(6) . . ?
C156 C151 C150 121.8(7) . . ?
C153 C152 C151 120.2(7) . . ?
C153 C152 H152 119.9 . . ?
C151 C152 H152 119.9 . . ?
C154 C153 C152 120.5(8) . . ?
C154 C153 H153 119.7 . . ?
C152 C153 H153 119.7 . . ?
C155 C154 C153 119.4(8) . . ?
C155 C154 H154 120.3 . . ?
C153 C154 H154 120.3 . . ?
C154 C155 C156 121.0(8) . . ?
C154 C155 H155 119.5 . . ?
C156 C155 H155 119.5 . . ?
C155 C156 C151 120.0(8) . . ?
C155 C156 H156 120.0 . . ?
C151 C156 H156 120.0 . . ?
C158 C157 Au4 175.9(7) . . ?
C158 C157 Ag4 88.6(5) . . ?
Au4 C157 Ag4 91.1(3) . . ?
C157 C158 C159 172.9(8) . . ?
C157 C158 Ag4 63.6(5) . . ?
C159 C158 Ag4 123.4(5) . . ?
C164 C159 C160 117.8(7) . . ?
C164 C159 C158 119.9(7) . . ?
C160 C159 C158 122.2(7) . . ?
C161 C160 C159 120.4(8) . . ?
C161 C160 H160 119.8 . . ?
C159 C160 H160 119.8 . . ?
C160 C161 C162 120.8(8) . . ?
C160 C161 H161 119.6 . . ?
C162 C161 H161 119.6 . . ?
C161 C162 C163 119.7(8) . . ?
C161 C162 H162 120.1 . . ?
C163 C162 H162 120.1 . . ?
C164 C163 C162 119.8(9) . . ?
C164 C163 H163 120.1 . . ?
C162 C163 H163 120.1 . . ?
C163 C164 C159 121.4(8) . . ?
C163 C164 H164 119.3 . . ?
C159 C164 H164 119.3 . . ?
C166 C165 Au5 166.1(7) . . ?
C166 C165 Ag7 107.2(6) . . ?
Au5 C165 Ag7 85.3(3) . . ?
C166 C165 Ag6 93.6(5) . . ?
Au5 C165 Ag6 78.8(3) . . ?
Ag7 C165 Ag6 95.1(3) . . ?
C165 C166 C167 178.5(9) . . ?
C172 C167 C168 118.8(8) . . ?
C172 C167 C166 121.7(7) . . ?
C168 C167 C166 119.5(8) . . ?
C167 C168 C169 118.8(10) . . ?
C167 C168 H168 120.6 . . ?
C169 C168 H168 120.6 . . ?
C170 C169 C168 121.0(10) . . ?
C170 C169 H169 119.5 . . ?
C168 C169 H169 119.5 . . ?
C169 C170 C171 120.4(9) . . ?
C169 C170 H170 119.8 . . ?
C171 C170 H170 119.8 . . ?
C170 C171 C172 119.3(9) . . ?
C170 C171 H171 120.3 . . ?
C172 C171 H171 120.3 . . ?
C167 C172 C171 121.7(8) . . ?
C167 C172 H172 119.1 . . ?
C171 C172 H172 119.1 . . ?
C174 C173 Au5 171.6(7) . . ?
C174 C173 Ag5 87.3(5) . . ?
Au5 C173 Ag5 91.5(3) . . ?
C173 C174 C175 172.2(8) . . ?
C173 C174 Ag5 64.5(5) . . ?
C175 C174 Ag5 123.2(5) . . ?
C176 C175 C180 119.1(7) . . ?
C176 C175 C174 121.8(7) . . ?
C180 C175 C174 119.1(7) . . ?
C177 C176 C175 121.0(8) . . ?
C177 C176 H176 119.5 . . ?
C175 C176 H176 119.5 . . ?
C178 C177 C176 120.4(9) . . ?
C178 C177 H177 119.8 . . ?
C176 C177 H177 119.8 . . ?
C177 C178 C179 119.6(8) . . ?
C177 C178 H178 120.2 . . ?
C179 C178 H178 120.2 . . ?
C180 C179 C178 120.4(8) . . ?
C180 C179 H179 119.8 . . ?
C178 C179 H179 119.8 . . ?
C179 C180 C175 119.6(8) . . ?
C179 C180 H180 120.2 . . ?
C175 C180 H180 120.2 . . ?
C182 C181 Au8 172.5(7) . . ?
C182 C181 Ag6 90.8(6) . . ?
Au8 C181 Ag6 88.6(3) . . ?
C181 C182 C183 172.9(9) . . ?
C181 C182 Ag6 61.8(5) . . ?
C183 C182 Ag6 125.2(6) . . ?
C188 C183 C184 117.8(9) . . ?
C188 C183 C182 121.8(8) . . ?
C184 C183 C182 120.4(8) . . ?
C185 C184 C183 120.1(11) . . ?
C185 C184 H184 120.0 . . ?
C183 C184 H184 120.0 . . ?
C184 C185 C186 121.1(12) . . ?
C184 C185 H185 119.5 . . ?
C186 C185 H185 119.5 . . ?
C187 C186 C185 118.2(11) . . ?
C187 C186 H186 120.9 . . ?
C185 C186 H186 120.9 . . ?
C186 C187 C188 121.3(11) . . ?
C186 C187 H187 119.4 . . ?
C188 C187 H187 119.4 . . ?
C183 C188 C187 121.5(10) . . ?
C183 C188 H188 119.2 . . ?
C187 C188 H188 119.2 . . ?
C190 C189 Au8 160.8(7) . . ?
C190 C189 Ag4 104.2(6) . . ?
Au8 C189 Ag4 95.0(3) . . ?
C190 C189 Ag5 102.9(6) . . ?
Au8 C189 Ag5 78.2(3) . . ?
Ag4 C189 Ag5 89.7(3) . . ?
C189 C190 C191 169.3(8) . . ?
C196 C191 C192 119.7(8) . . ?
C196 C191 C190 121.7(7) . . ?
C192 C191 C190 118.6(7) . . ?
C193 C192 C191 119.3(8) . . ?
C193 C192 H192 120.3 . . ?
C191 C192 H192 120.3 . . ?
C194 C193 C192 119.6(8) . . ?
C194 C193 H193 120.2 . . ?
C192 C193 H193 120.2 . . ?
C195 C194 C193 121.2(9) . . ?
C195 C194 H194 119.4 . . ?
C193 C194 H194 119.4 . . ?
C194 C195 C196 120.5(8) . . ?
C194 C195 H195 119.8 . . ?
C196 C195 H195 119.8 . . ?
C195 C196 C191 119.6(8) . . ?
C195 C196 H196 120.2 . . ?
C191 C196 H196 120.2 . . ?
C198 C197 Au9 178.1(7) . . ?
C198 C197 Ag7 82.8(5) . . ?
Au9 C197 Ag7 95.5(3) . . ?
C197 C198 C199 172.8(8) . . ?
C197 C198 Ag7 68.6(5) . . ?
C199 C198 Ag7 118.4(5) . . ?
C200 C199 C204 119.6(8) . . ?
C200 C199 C198 120.9(7) . . ?
C204 C199 C198 119.4(8) . . ?
C201 C200 C199 120.7(8) . . ?
C201 C200 H200 119.7 . . ?
C199 C200 H200 119.7 . . ?
C202 C201 C200 119.7(9) . . ?
C202 C201 H201 120.2 . . ?
C200 C201 H201 120.2 . . ?
C201 C202 C203 120.4(9) . . ?
C201 C202 H202 119.8 . . ?
C203 C202 H202 119.8 . . ?
C202 C203 C204 120.0(9) . . ?
C202 C203 H203 120.0 . . ?
C204 C203 H203 120.0 . . ?
C199 C204 C203 119.6(8) . . ?
C199 C204 H204 120.2 . . ?
C203 C204 H204 120.2 . . ?
C206 C205 Au9 173.1(7) . . ?
C206 C205 Ag3 100.7(6) . . ?
Au9 C205 Ag3 86.2(3) . . ?
C205 C206 C207 174.2(9) . . ?
C212 C207 C208 118.6(9) . . ?
C212 C207 C206 121.9(8) . . ?
C208 C207 C206 119.5(8) . . ?
C207 C208 C209 120.7(11) . . ?
C207 C208 H208 119.6 . . ?
C209 C208 H208 119.6 . . ?
C210 C209 C208 119.5(11) . . ?
C210 C209 H209 120.2 . . ?
C208 C209 H209 120.2 . . ?
C211 C210 C209 120.8(11) . . ?
C211 C210 H210 119.6 . . ?
C209 C210 H210 119.6 . . ?
C210 C211 C212 119.7(11) . . ?
C210 C211 H211 120.2 . . ?
C212 C211 H211 120.2 . . ?
C207 C212 C211 120.7(10) . . ?
C207 C212 H212 119.6 . . ?
C211 C212 H212 119.6 . . ?
C214 C213 Au10 172.0(7) . . ?
C214 C213 Ag8 105.5(6) . . ?
Au10 C213 Ag8 82.1(3) . . ?
C213 C214 C215 172.2(8) . . ?
C216 C215 C220 118.0(7) . . ?
C216 C215 C214 122.8(7) . . ?
C220 C215 C214 119.1(7) . . ?
C217 C216 C215 120.6(8) . . ?
C217 C216 H216 119.7 . . ?
C215 C216 H216 119.7 . . ?
C216 C217 C218 120.7(9) . . ?
C216 C217 H217 119.7 . . ?
C218 C217 H217 119.7 . . ?
C217 C218 C219 119.2(9) . . ?
C217 C218 H218 120.4 . . ?
C219 C218 H218 120.4 . . ?
C220 C219 C218 120.1(9) . . ?
C220 C219 H219 120.0 . . ?
C218 C219 H219 120.0 . . ?
C219 C220 C215 121.4(9) . . ?
C219 C220 H220 119.3 . . ?
C215 C220 H220 119.3 . . ?
C222 C221 Au10 178.0(7) . . ?
C222 C221 Ag2 87.7(5) . . ?
Au10 C221 Ag2 94.2(3) . . ?
C221 C222 C223 172.1(8) . . ?
C221 C222 Ag2 64.2(5) . . ?
C223 C222 Ag2 123.7(5) . . ?
C224 C223 C228 118.9(8) . . ?
C224 C223 C222 118.9(7) . . ?
C228 C223 C222 122.1(8) . . ?
C223 C224 C225 120.6(9) . . ?
C223 C224 H224 119.7 . . ?
C225 C224 H224 119.7 . . ?
C226 C225 C224 120.3(10) . . ?
C226 C225 H225 119.8 . . ?
C224 C225 H225 119.8 . . ?
C227 C226 C225 118.9(10) . . ?
C227 C226 H226 120.5 . . ?
C225 C226 H226 120.5 . . ?
C226 C227 C228 121.6(9) . . ?
C226 C227 H227 119.2 . . ?
C228 C227 H227 119.2 . . ?
C227 C228 C223 119.6(9) . . ?
C227 C228 H228 120.2 . . ?
C223 C228 H228 120.2 . . ?
C230 C229 Au11 151.9(6) . . ?
C230 C229 Ag9 123.7(6) . . ?
Au11 C229 Ag9 83.2(3) . . ?
C230 C229 Ag10 88.3(5) . . ?
Au11 C229 Ag10 78.3(2) . . ?
Ag9 C229 Ag10 99.1(3) . . ?
C229 C230 C231 173.7(8) . . ?
C232 C231 C236 118.2(8) . . ?
C232 C231 C230 123.2(8) . . ?
C236 C231 C230 118.6(8) . . ?
C231 C232 C233 120.0(10) . . ?
C231 C232 H232 120.0 . . ?
C233 C232 H232 120.0 . . ?
C234 C233 C232 121.1(10) . . ?
C234 C233 H233 119.4 . . ?
C232 C233 H233 119.4 . . ?
C233 C234 C235 119.7(9) . . ?
C233 C234 H234 120.1 . . ?
C235 C234 H234 120.1 . . ?
C234 C235 C236 120.3(10) . . ?
C234 C235 H235 119.9 . . ?
C236 C235 H235 119.9 . . ?
C235 C236 C231 120.6(9) . . ?
C235 C236 H236 119.7 . . ?
C231 C236 H236 119.7 . . ?
C238 C237 Au11 172.4(7) . . ?
C238 C237 Ag1 87.9(5) . . ?
Au11 C237 Ag1 90.0(3) . . ?
C237 C238 C239 171.3(9) . . ?
C237 C238 Ag1 64.3(5) . . ?
C239 C238 Ag1 124.4(6) . . ?
C240 C239 C244 118.7(9) . . ?
C240 C239 C238 118.2(8) . . ?
C244 C239 C238 123.1(8) . . ?
C239 C240 C241 121.4(11) . . ?
C239 C240 H240 119.3 . . ?
C241 C240 H240 119.3 . . ?
C242 C241 C240 118.8(12) . . ?
C242 C241 H241 120.6 . . ?
C240 C241 H241 120.6 . . ?
C243 C242 C241 120.6(11) . . ?
C243 C242 H242 119.7 . . ?
C241 C242 H242 119.7 . . ?
C242 C243 C244 120.4(10) . . ?
C242 C243 H243 119.8 . . ?
C244 C243 H243 119.8 . . ?
C239 C244 C243 120.0(10) . . ?
C239 C244 H244 120.0 . . ?
C243 C244 H244 120.0 . . ?
C246 C245 H24A 109.5 . . ?
C246 C245 H24B 109.5 . . ?
H24A C245 H24B 109.5 . . ?
C246 C245 H24C 109.5 . . ?
H24A C245 H24C 109.5 . . ?
H24B C245 H24C 109.5 . . ?
O1 C246 C245 120.0(12) . . ?
O1 C246 C247 123.3(10) . . ?
C245 C246 C247 116.6(10) . . ?
C246 C247 H24D 109.5 . . ?
C246 C247 H24E 109.5 . . ?
H24D C247 H24E 109.5 . . ?
C246 C247 H24F 109.5 . . ?
H24D C247 H24F 109.5 . . ?
H24E C247 H24F 109.5 . . ?
Cl1 C248 Cl2 120.9(14) . . ?
Cl1 C248 H24G 107.1 . . ?
Cl2 C248 H24G 107.1 . . ?
Cl1 C248 H24H 107.1 . . ?
Cl2 C248 H24H 107.1 . . ?
H24G C248 H24H 106.8 . . ?
Cl4 C249 Cl3 109.5(11) . . ?
Cl4 C249 H24I 109.8 . . ?
Cl3 C249 H24I 109.8 . . ?
Cl4 C249 H24J 109.8 . . ?
Cl3 C249 H24J 109.8 . . ?
H24I C249 H24J 108.2 . . ?
F7 P6 F12 94.7(6) . . ?
F7 P6 F11 91.5(6) . . ?
F12 P6 F11 87.4(6) . . ?
F7 P6 F9 86.3(6) . . ?
F12 P6 F9 89.2(6) . . ?
F11 P6 F9 175.8(8) . . ?
F7 P6 F10 85.3(6) . . ?
F12 P6 F10 177.5(7) . . ?
F11 P6 F10 90.1(6) . . ?
F9 P6 F10 93.3(5) . . ?
F7 P6 F8 174.8(7) . . ?
F12 P6 F8 90.3(6) . . ?
F11 P6 F8 90.1(6) . . ?
F9 P6 F8 92.3(6) . . ?
F10 P6 F8 89.8(6) . . ?
F18 P7 F15 91.3(10) . . ?
F18 P7 F13 88.9(10) . . ?
F15 P7 F13 91.4(8) . . ?
F18 P7 F14 93.0(11) . . ?
F15 P7 F14 89.5(8) . . ?
F13 P7 F14 177.9(11) . . ?
F18 P7 F17 90.9(10) . . ?
F15 P7 F17 177.6(9) . . ?
F13 P7 F17 89.8(8) . . ?
F14 P7 F17 89.2(8) . . ?
F18 P7 F16 176.4(11) . . ?
F15 P7 F16 90.7(8) . . ?
F13 P7 F16 88.0(9) . . ?
F14 P7 F16 90.1(10) . . ?
F17 P7 F16 87.3(9) . . ?
C251 C250 H25D 109.5 . . ?
C251 C250 H25E 109.5 . . ?
H25D C250 H25E 109.5 . . ?
C251 C250 H25F 109.5 . . ?
H25D C250 H25F 109.5 . . ?
H25E C250 H25F 109.5 . . ?
O5 C251 C252 95.9(19) . . ?
O5 C251 C250 97.0(18) . . ?
C252 C251 C250 120.9(17) . . ?
C251 C252 H25G 109.5 . . ?
C251 C252 H25H 109.5 . . ?
H25G C252 H25H 109.5 . . ?
C251 C252 H25I 109.5 . . ?
H25G C252 H25I 109.5 . . ?
H25H C252 H25I 109.5 . . ?
Cl6 C256 Cl5 113.0(12) . . ?
Cl6 C256 H25J 109.0 . . ?
Cl5 C256 H25J 109.0 . . ?
Cl6 C256 H25K 109.0 . . ?
Cl5 C256 H25K 109.0 . . ?
H25J C256 H25K 107.8 . . ?
O6 C257 H25L 109.5 . . ?
O6 C257 H25M 109.5 . . ?
H25L C257 H25M 109.5 . . ?
O6 C257 H25N 109.5 . . ?
H25L C257 H25N 109.5 . . ?
H25M C257 H25N 109.5 . . ?
C257 O6 H6O 131.1 . . ?
C255 O4 C255 180(4) 3_575 . ?
C255 O4 H4O 66.3 3_575 . ?
C255 O4 H4O 113.7 . . ?
O4 C255 H25O 109.5 . . ?
O4 C255 H25P 109.5 . . ?
H25O C255 H25P 109.5 . . ?
O4 C255 H25Q 109.5 . . ?
H25O C255 H25Q 109.5 . . ?
H25P C255 H25Q 109.5 . . ?
C254 O3 H3O 155.4 . . ?
O3 C254 H25X 109.5 . . ?
O3 C254 H25Z 109.5 . . ?
H25X C254 H25Z 109.5 . . ?
O3 C254 H25R 109.5 . . ?
H25X C254 H25R 109.5 . . ?
H25Z C254 H25R 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au1 C109 2.027(9) . yes
Au1 P1 2.287(2) . yes
Au1 Au2 3.1404(4) . yes
Au1 Ag1 3.2163(7) . yes
Au2 C117 2.002(8) . yes
Au2 C125 2.005(7) . yes
Au2 Ag1 2.9781(7) . yes
Au2 Ag10 3.0443(6) . yes
Au2 Ag2 3.1552(7) . yes
Au2 Ag9 3.1713(6) . yes
Au3 C133 1.997(7) . yes
Au3 C141 2.009(8) . yes
Au3 Ag2 2.9444(7) . yes
Au3 Ag3 3.2067(7) . yes
Au3 Ag8 3.2195(7) . yes
Au3 Ag9 3.2496(6) . yes
Au4 C157 1.996(8) . yes
Au4 C149 2.010(7) . yes
Au4 Ag7 2.9035(6) . yes
Au4 Ag4 3.0810(7) . yes
Au4 Ag3 3.1128(7) . yes
Au4 Au9 3.3499(4) . yes
Au4 Ag8 3.3617(6) . yes
Au5 C173 2.010(8) . yes
Au5 C165 2.010(8) . yes
Au5 Ag7 2.9361(6) . yes
Au5 Ag6 2.9522(6) . yes
Au5 Ag5 3.0954(7) . yes
Au5 Au6 3.1247(4) . yes
Au5 Ag4 3.1674(7) . yes
Au6 C43 2.011(8) . yes
Au6 P2 2.2843(19) . yes
Au6 Ag6 3.2638(6) . yes
Au7 C51 1.998(8) . yes
Au7 P3 2.274(2) . yes
Au7 Au8 3.1973(4) . yes
Au8 C181 1.990(9) . yes
Au8 C189 2.001(9) . yes
Au8 Ag5 3.0075(6) . yes
Au8 Ag6 3.0177(7) . yes
Au8 Ag7 3.0315(7) . yes
Au8 Ag4 3.1580(7) . yes
Au9 C197 1.990(9) . yes
Au9 C205 2.019(9) . yes
Au9 Ag3 2.9537(6) . yes
Au9 Ag4 3.0200(7) . yes
Au9 Ag8 3.2129(7) . yes
Au9 Ag7 3.2333(6) . yes
Au10 C221 2.004(8) . yes
Au10 C213 2.019(9) . yes
Au10 Ag8 2.8531(7) . yes
Au10 Ag9 2.9798(7) . yes
Au10 Ag2 3.1721(6) . yes
Au10 Ag3 3.3755(7) . yes
Au11 C237 2.000(8) . yes
Au11 C229 2.014(7) . yes
Au11 Ag9 2.8530(6) . yes
Au11 Ag10 3.0229(7) . yes
Au11 Ag1 3.0689(6) . yes
Au11 Ag2 3.0939(6) . yes
Au11 Au12 3.1264(4) . yes
Au12 C101 2.019(9) . yes
Au12 P4 2.282(2) . yes
Au12 Ag10 3.3535(7) . yes
Ag1 C109 2.276(7) . yes
Ag1 C237 2.328(7) . yes
Ag1 C110 2.484(7) . yes
Ag1 C238 2.583(8) . yes
Ag1 C125 2.696(7) . yes
Ag2 C125 2.298(7) . yes
Ag2 C221 2.315(7) . yes
Ag2 C222 2.569(8) . yes
Ag2 C126 2.664(7) . yes
Ag3 C141 2.286(7) . yes
Ag3 C205 2.295(7) . yes
Ag3 C142 2.569(7) . yes
Ag4 C189 2.274(7) . yes
Ag4 C157 2.311(7) . yes
Ag4 C158 2.579(7) . yes
Ag4 Ag7 3.3512(8) . yes
Ag5 C51 2.288(7) . yes
Ag5 C173 2.303(7) . yes
Ag5 C52 2.477(7) . yes
Ag5 C174 2.549(7) . yes
Ag5 C189 2.691(8) . yes
Ag6 C43 2.282(7) . yes
Ag6 C181 2.318(8) . yes
Ag6 C44 2.466(7) . yes
Ag6 C165 2.586(7) . yes
Ag6 C182 2.630(8) . yes
Ag7 C165 2.312(7) . yes
Ag7 C197 2.364(7) . yes
Ag7 C198 2.518(7) . yes
Ag8 C149 2.312(7) . yes
Ag8 C213 2.314(7) . yes
Ag8 C150 2.493(7) . yes
Ag9 C229 2.275(7) . yes
Ag9 C133 2.312(7) . yes
Ag9 C134 2.537(7) . yes
Ag10 C101 2.292(7) . yes
Ag10 C117 2.297(8) . yes
Ag10 C102 2.428(7) . yes
Ag10 C118 2.587(8) . yes
Ag10 C229 2.699(7) . yes
Cl1 C248 1.634(17) . ?
Cl2 C248 1.656(16) . ?
Cl3 C249 1.741(14) . ?
Cl4 C249 1.676(15) . ?
P1 C13 1.814(7) . ?
P1 C7 1.817(9) . ?
P1 C1 1.827(8) . ?
P2 C28 1.811(7) . ?
P2 C31 1.815(7) . ?
P2 C37 1.826(8) . ?
P3 C59 1.807(8) . ?
P3 C65 1.821(7) . ?
P3 C71 1.822(7) . ?
P4 C89 1.814(8) . ?
P4 C86 1.821(7) . ?
P4 C95 1.823(7) . ?
P5 F5 1.512(10) . ?
P5 F4 1.544(10) . ?
P5 F1 1.555(8) . ?
P5 F3 1.557(7) . ?
P5 F6 1.573(8) . ?
P5 F2 1.593(8) . ?
O1 C246 1.188(12) . ?
C1 C6 1.364(11) . ?
C1 C2 1.388(11) . ?
C2 C3 1.385(11) . ?
C2 H2 0.9500 . ?
C3 C4 1.379(13) . ?
C3 H3 0.9500 . ?
C4 C5 1.381(12) . ?
C4 H4 0.9500 . ?
C5 C6 1.391(11) . ?
C5 H5 0.9500 . ?
C6 H6 0.9500 . ?
C7 C8 1.383(12) . ?
C7 C12 1.387(11) . ?
C8 C9 1.374(13) . ?
C8 H8 0.9500 . ?
C9 C10 1.360(14) . ?
C9 H9 0.9500 . ?
C10 C11 1.375(15) . ?
C10 H10 0.9500 . ?
C11 C12 1.373(13) . ?
C11 H11 0.9500 . ?
C12 H12 0.9500 . ?
C13 C18 1.386(10) . ?
C13 C14 1.410(10) . ?
C14 C15 1.384(10) . ?
C14 H14 0.9500 . ?
C15 C16 1.396(10) . ?
C15 H15 0.9500 . ?
C16 C17 1.402(10) . ?
C16 C19 1.494(10) . ?
C17 C18 1.368(10) . ?
C17 H17 0.9500 . ?
C18 H18 0.9500 . ?
C19 C20 1.393(10) . ?
C19 C24 1.399(10) . ?
C20 C21 1.377(10) . ?
C20 H20 0.9500 . ?
C21 C22 1.390(10) . ?
C21 H21 0.9500 . ?
C22 C23 1.399(10) . ?
C22 C25 1.475(10) . ?
C23 C24 1.387(10) . ?
C23 H23 0.9500 . ?
C24 H24 0.9500 . ?
C25 C26 1.397(10) . ?
C25 C30 1.400(10) . ?
C26 C27 1.386(10) . ?
C26 H26 0.9500 . ?
C27 C28 1.398(10) . ?
C27 H27 0.9500 . ?
C28 C29 1.389(10) . ?
C29 C30 1.374(10) . ?
C29 H29 0.9500 . ?
C30 H30 0.9500 . ?
C31 C32 1.391(10) . ?
C31 C36 1.406(10) . ?
C32 C33 1.379(10) . ?
C32 H32 0.9500 . ?
C33 C34 1.374(11) . ?
C33 H33 0.9500 . ?
C34 C35 1.400(11) . ?
C34 H34 0.9500 . ?
C35 C36 1.377(10) . ?
C35 H35 0.9500 . ?
C36 H36 0.9500 . ?
C37 C42 1.372(10) . ?
C37 C38 1.399(10) . ?
C38 C39 1.371(11) . ?
C38 H38 0.9500 . ?
C39 C40 1.374(12) . ?
C39 H39 0.9500 . ?
C40 C41 1.379(12) . ?
C40 H40 0.9500 . ?
C41 C42 1.406(11) . ?
C41 H41 0.9500 . ?
C42 H42 0.9500 . ?
C43 C44 1.226(10) . ?
C44 C45 1.450(10) . ?
C45 C46 1.379(11) . ?
C45 C50 1.390(11) . ?
C46 C47 1.398(12) . ?
C46 H46 0.9500 . ?
C47 C48 1.352(13) . ?
C47 H47 0.9500 . ?
C48 C49 1.342(12) . ?
C48 H48 0.9500 . ?
C49 C50 1.376(12) . ?
C49 H49 0.9500 . ?
C50 H50 0.9500 . ?
C51 C52 1.230(10) . ?
C52 C53 1.443(10) . ?
C53 C54 1.389(10) . ?
C53 C58 1.395(11) . ?
C54 C55 1.374(11) . ?
C54 H54 0.9500 . ?
C55 C56 1.377(12) . ?
C55 H55 0.9500 . ?
C56 C57 1.378(11) . ?
C56 H56 0.9500 . ?
C57 C58 1.380(10) . ?
C57 H57 0.9500 . ?
C58 H58 0.9500 . ?
C59 C60 1.395(10) . ?
C59 C64 1.395(10) . ?
C60 C61 1.390(11) . ?
C60 H60 0.9500 . ?
C61 C62 1.362(12) . ?
C61 H61 0.9500 . ?
C62 C63 1.398(11) . ?
C62 H62 0.9500 . ?
C63 C64 1.369(11) . ?
C63 H63 0.9500 . ?
C64 H64 0.9500 . ?
C65 C70 1.397(12) . ?
C65 C66 1.398(11) . ?
C66 C67 1.394(12) . ?
C66 H66 0.9500 . ?
C67 C68 1.330(13) . ?
C67 H67 0.9500 . ?
C68 C69 1.392(12) . ?
C68 H68 0.9500 . ?
C69 C70 1.415(12) . ?
C69 H69 0.9500 . ?
C70 H70 0.9500 . ?
C71 C72 1.391(10) . ?
C71 C76 1.394(10) . ?
C72 C73 1.381(10) . ?
C72 H72 0.9500 . ?
C73 C74 1.390(10) . ?
C73 H73 0.9500 . ?
C74 C75 1.397(10) . ?
C74 C77 1.487(9) . ?
C75 C76 1.371(10) . ?
C75 H75 0.9500 . ?
C76 H76 0.9500 . ?
C77 C78 1.386(10) . ?
C77 C82 1.396(10) . ?
C78 C79 1.381(10) . ?
C78 H78 0.9500 . ?
C79 C80 1.401(10) . ?
C79 H79 0.9500 . ?
C80 C81 1.400(10) . ?
C80 C83 1.484(10) . ?
C81 C82 1.385(10) . ?
C81 H81 0.9500 . ?
C82 H82 0.9500 . ?
C83 C88 1.392(10) . ?
C83 C84 1.398(10) . ?
C84 C85 1.372(10) . ?
C84 H84 0.9500 . ?
C85 C86 1.403(10) . ?
C85 H85 0.9500 . ?
C86 C87 1.381(10) . ?
C87 C88 1.392(10) . ?
C87 H87 0.9500 . ?
C88 H88 0.9500 . ?
C89 C90 1.387(10) . ?
C89 C94 1.396(11) . ?
C90 C91 1.366(12) . ?
C90 H90 0.9500 . ?
C91 C92 1.374(12) . ?
C91 H91 0.9500 . ?
C92 C93 1.388(12) . ?
C92 H92 0.9500 . ?
C93 C94 1.364(11) . ?
C93 H93 0.9500 . ?
C94 H94 0.9500 . ?
C95 C96 1.379(10) . ?
C95 C100 1.403(10) . ?
C96 C97 1.380(10) . ?
C96 H96 0.9500 . ?
C97 C98 1.373(10) . ?
C97 H97 0.9500 . ?
C98 C99 1.380(11) . ?
C98 H98 0.9500 . ?
C99 C100 1.374(11) . ?
C99 H99 0.9500 . ?
C100 H100 0.9500 . ?
C101 C102 1.222(11) . ?
C102 C103 1.441(11) . ?
C103 C108 1.389(11) . ?
C103 C104 1.395(11) . ?
C104 C105 1.376(12) . ?
C104 H104 0.9500 . ?
C105 C106 1.374(13) . ?
C105 H105 0.9500 . ?
C106 C107 1.376(12) . ?
C106 H106 0.9500 . ?
C107 C108 1.367(11) . ?
C107 H107 0.9500 . ?
C108 H108 0.9500 . ?
C109 C110 1.203(10) . ?
C110 C111 1.444(11) . ?
C111 C116 1.394(10) . ?
C111 C112 1.397(11) . ?
C112 C113 1.383(11) . ?
C112 H112 0.9500 . ?
C113 C114 1.361(11) . ?
C113 H113 0.9500 . ?
C114 C115 1.383(12) . ?
C114 H114 0.9500 . ?
C115 C116 1.368(11) . ?
C115 H115 0.9500 . ?
C116 H116 0.9500 . ?
C117 C118 1.230(10) . ?
C118 C119 1.437(11) . ?
C119 C124 1.390(12) . ?
C119 C120 1.392(12) . ?
C120 C121 1.368(13) . ?
C120 H120 0.9500 . ?
C121 C122 1.374(16) . ?
C121 H121 0.9500 . ?
C122 C123 1.357(16) . ?
C122 H122 0.9500 . ?
C123 C124 1.370(13) . ?
C123 H123 0.9500 . ?
C124 H124 0.9500 . ?
C125 C126 1.217(10) . ?
C126 C127 1.438(11) . ?
C127 C132 1.381(11) . ?
C127 C128 1.412(11) . ?
C128 C129 1.387(11) . ?
C128 H128 0.9500 . ?
C129 C130 1.399(12) . ?
C129 H129 0.9500 . ?
C130 C131 1.354(11) . ?
C130 H130 0.9500 . ?
C131 C132 1.394(11) . ?
C131 H131 0.9500 . ?
C132 H132 0.9500 . ?
C133 C134 1.206(10) . ?
C134 C135 1.452(10) . ?
C135 C136 1.379(11) . ?
C135 C140 1.393(11) . ?
C136 C137 1.381(11) . ?
C136 H136 0.9500 . ?
C137 C138 1.386(13) . ?
C137 H137 0.9500 . ?
C138 C139 1.380(13) . ?
C138 H138 0.9500 . ?
C139 C140 1.377(11) . ?
C139 H139 0.9500 . ?
C140 H140 0.9500 . ?
C141 C142 1.208(10) . ?
C142 C143 1.431(10) . ?
C143 C144 1.379(11) . ?
C143 C148 1.387(11) . ?
C144 C145 1.399(12) . ?
C144 H144 0.9500 . ?
C145 C146 1.355(14) . ?
C145 H145 0.9500 . ?
C146 C147 1.377(14) . ?
C146 H146 0.9500 . ?
C147 C148 1.395(12) . ?
C147 H147 0.9500 . ?
C148 H148 0.9500 . ?
C149 C150 1.214(10) . ?
C150 C151 1.437(10) . ?
C151 C152 1.395(10) . ?
C151 C156 1.401(10) . ?
C152 C153 1.386(11) . ?
C152 H152 0.9500 . ?
C153 C154 1.385(11) . ?
C153 H153 0.9500 . ?
C154 C155 1.378(11) . ?
C154 H154 0.9500 . ?
C155 C156 1.382(11) . ?
C155 H155 0.9500 . ?
C156 H156 0.9500 . ?
C157 C158 1.206(10) . ?
C158 C159 1.438(11) . ?
C159 C164 1.403(11) . ?
C159 C160 1.415(11) . ?
C160 C161 1.377(11) . ?
C160 H160 0.9500 . ?
C161 C162 1.390(13) . ?
C161 H161 0.9500 . ?
C162 C163 1.391(13) . ?
C162 H162 0.9500 . ?
C163 C164 1.382(11) . ?
C163 H163 0.9500 . ?
C164 H164 0.9500 . ?
C165 C166 1.217(10) . ?
C166 C167 1.444(11) . ?
C167 C172 1.368(11) . ?
C167 C168 1.382(12) . ?
C168 C169 1.404(14) . ?
C168 H168 0.9500 . ?
C169 C170 1.351(15) . ?
C169 H169 0.9500 . ?
C170 C171 1.356(13) . ?
C170 H170 0.9500 . ?
C171 C172 1.383(11) . ?
C171 H171 0.9500 . ?
C172 H172 0.9500 . ?
C173 C174 1.207(10) . ?
C174 C175 1.436(10) . ?
C175 C176 1.380(11) . ?
C175 C180 1.401(10) . ?
C176 C177 1.377(12) . ?
C176 H176 0.9500 . ?
C177 C178 1.369(13) . ?
C177 H177 0.9500 . ?
C178 C179 1.395(12) . ?
C178 H178 0.9500 . ?
C179 C180 1.384(11) . ?
C179 H179 0.9500 . ?
C180 H180 0.9500 . ?
C181 C182 1.209(11) . ?
C182 C183 1.454(12) . ?
C183 C188 1.335(12) . ?
C183 C184 1.373(13) . ?
C184 C185 1.361(16) . ?
C184 H184 0.9500 . ?
C185 C186 1.379(17) . ?
C185 H185 0.9500 . ?
C186 C187 1.308(16) . ?
C186 H186 0.9500 . ?
C187 C188 1.383(13) . ?
C187 H187 0.9500 . ?
C188 H188 0.9500 . ?
C189 C190 1.197(11) . ?
C190 C191 1.468(11) . ?
C191 C196 1.391(11) . ?
C191 C192 1.406(11) . ?
C192 C193 1.389(12) . ?
C192 H192 0.9500 . ?
C193 C194 1.370(12) . ?
C193 H193 0.9500 . ?
C194 C195 1.369(12) . ?
C194 H194 0.9500 . ?
C195 C196 1.372(11) . ?
C195 H195 0.9500 . ?
C196 H196 0.9500 . ?
C197 C198 1.212(11) . ?
C198 C199 1.455(11) . ?
C199 C200 1.388(11) . ?
C199 C204 1.389(11) . ?
C200 C201 1.383(12) . ?
C200 H200 0.9500 . ?
C201 C202 1.380(13) . ?
C201 H201 0.9500 . ?
C202 C203 1.385(13) . ?
C202 H202 0.9500 . ?
C203 C204 1.395(12) . ?
C203 H203 0.9500 . ?
C204 H204 0.9500 . ?
C205 C206 1.209(11) . ?
C206 C207 1.453(12) . ?
C207 C212 1.372(12) . ?
C207 C208 1.383(12) . ?
C208 C209 1.387(13) . ?
C208 H208 0.9500 . ?
C209 C210 1.363(15) . ?
C209 H209 0.9500 . ?
C210 C211 1.362(16) . ?
C210 H210 0.9500 . ?
C211 C212 1.391(14) . ?
C211 H211 0.9500 . ?
C212 H212 0.9500 . ?
C213 C214 1.203(11) . ?
C214 C215 1.440(11) . ?
C215 C216 1.397(11) . ?
C215 C220 1.402(11) . ?
C216 C217 1.375(11) . ?
C216 H216 0.9500 . ?
C217 C218 1.388(13) . ?
C217 H217 0.9500 . ?
C218 C219 1.395(13) . ?
C218 H218 0.9500 . ?
C219 C220 1.366(12) . ?
C219 H219 0.9500 . ?
C220 H220 0.9500 . ?
C221 C222 1.211(10) . ?
C222 C223 1.432(11) . ?
C223 C224 1.368(12) . ?
C223 C228 1.385(11) . ?
C224 C225 1.392(13) . ?
C224 H224 0.9500 . ?
C225 C226 1.370(14) . ?
C225 H225 0.9500 . ?
C226 C227 1.359(14) . ?
C226 H226 0.9500 . ?
C227 C228 1.384(13) . ?
C227 H227 0.9500 . ?
C228 H228 0.9500 . ?
C229 C230 1.227(10) . ?
C230 C231 1.434(10) . ?
C231 C232 1.377(12) . ?
C231 C236 1.391(11) . ?
C232 C233 1.395(13) . ?
C232 H232 0.9500 . ?
C233 C234 1.352(15) . ?
C233 H233 0.9500 . ?
C234 C235 1.361(14) . ?
C234 H234 0.9500 . ?
C235 C236 1.388(12) . ?
C235 H235 0.9500 . ?
C236 H236 0.9500 . ?
C237 C238 1.208(10) . ?
C238 C239 1.442(11) . ?
C239 C240 1.371(13) . ?
C239 C244 1.377(11) . ?
C240 C241 1.396(14) . ?
C240 H240 0.9500 . ?
C241 C242 1.370(16) . ?
C241 H241 0.9500 . ?
C242 C243 1.355(16) . ?
C242 H242 0.9500 . ?
C243 C244 1.397(13) . ?
C243 H243 0.9500 . ?
C244 H244 0.9500 . ?
C245 C246 1.461(14) . ?
C245 H24A 0.9800 . ?
C245 H24B 0.9800 . ?
C245 H24C 0.9800 . ?
C246 C247 1.529(14) . ?
C247 H24D 0.9800 . ?
C247 H24E 0.9800 . ?
C247 H24F 0.9800 . ?
C248 H24G 0.9900 . ?
C248 H24H 0.9900 . ?
C249 H24I 0.9900 . ?
C249 H24J 0.9900 . ?
P6 F7 1.477(10) . ?
P6 F12 1.508(9) . ?
P6 F11 1.534(10) . ?
P6 F9 1.539(9) . ?
P6 F10 1.564(10) . ?
P6 F8 1.596(10) . ?
P7 F18 1.37(2) . ?
P7 F15 1.561(15) . ?
P7 F13 1.571(16) . ?
P7 F14 1.597(16) . ?
P7 F17 1.619(15) . ?
P7 F16 1.625(17) . ?
O5 C251 1.32(3) . ?
C250 C251 1.58(3) . ?
C250 H25D 0.9800 . ?
C250 H25E 0.9800 . ?
C250 H25F 0.9800 . ?
C251 C252 1.479(19) . ?
C252 H25G 0.9800 . ?
C252 H25H 0.9800 . ?
C252 H25I 0.9800 . ?
C256 Cl6 1.656(17) . ?
C256 Cl5 1.747(9) . ?
C256 H25J 0.9900 . ?
C256 H25K 0.9900 . ?
C257 O6 1.379(10) . ?
C257 H25L 0.9800 . ?
C257 H25M 0.9800 . ?
C257 H25N 0.9800 . ?
O6 H6O 0.9800 . ?
O4 C255 1.28(4) 3_575 ?
O4 C255 1.28(4) . ?
O4 H4O 0.9501 . ?
C255 H25O 0.9800 . ?
C255 H25P 0.9800 . ?
C255 H25Q 0.9800 . ?
O3 C254 1.31(5) . ?
O3 H3O 0.9800 . ?
C254 H25X 0.9800 . ?
C254 H25Z 0.9800 . ?
C254 H25R 0.9800 . ?
