#------------------------------------------------------------------------------
#$Date: 2016-03-26 02:49:11 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180156 $
#$URL: svn://www.crystallography.net/cod/cif/7/10/52/7105237.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7105237
loop_
_publ_author_name
'Fortman, George C'
'Scott, Natalie M'
'Linden, Anthony'
'Stevens, Edwin D'
'Dorta, Reto'
'Nolan, Steven P'
_publ_section_title
;
 Unusual reactivities of N-heterocyclic carbenes upon coordination to
 the platinum(II)-dimethyl moiety.
;
_journal_issue                   7
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              1050
_journal_page_last               1052
_journal_paper_doi               10.1039/b920482b
_journal_volume                  46
_journal_year                    2010
_chemical_formula_sum            'C44 H54 N4 Pt'
_chemical_formula_weight         834.00
_chemical_name_common            (Pt(IMes)2(Me2))
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 99.4110(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   16.7156(10)
_cell_length_b                   13.1785(8)
_cell_length_c                   17.6422(10)
_cell_measurement_reflns_used    49199
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      30.546
_cell_measurement_theta_min      2.195
_cell_volume                     3834.0(4)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0373
_diffrn_reflns_av_sigmaI/netI    0.0275
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_h_min       -23
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            56756
_diffrn_reflns_theta_full        30.00
_diffrn_reflns_theta_max         30.00
_diffrn_reflns_theta_min         2.34
_exptl_absorpt_coefficient_mu    3.695
_exptl_absorpt_correction_T_max  1.000000
_exptl_absorpt_correction_T_min  0.601619
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.445
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             1696
_exptl_crystal_size_max          0.7
_exptl_crystal_size_mid          0.6
_exptl_crystal_size_min          0.5
_refine_diff_density_max         1.559
_refine_diff_density_min         -1.791
_refine_diff_density_rms         0.131
_refine_ls_extinction_coef       0.00029(5)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.231
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     457
_refine_ls_number_reflns         11107
_refine_ls_number_restraints     438
_refine_ls_restrained_S_all      1.209
_refine_ls_R_factor_all          0.0420
_refine_ls_R_factor_gt           0.0312
_refine_ls_shift/su_max          0.035
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0001P)²+8.9816P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0588
_refine_ls_wR_factor_ref         0.0627
_reflns_number_gt                9591
_reflns_number_total             11107
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b920482b.txt
_cod_data_source_block           nol280m
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Empirical' changed to
'empirical' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P2(1)/n
_cod_database_code               7105237
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.287745(6) 0.356718(8) 0.040570(6) 0.01513(4) Uani 1 1 d U . .
N1 N 0.25240(15) 0.2059(2) 0.16826(14) 0.0200(5) Uani 1 1 d U . .
C1 C 0.30448(17) 0.2467(2) 0.12321(16) 0.0169(5) Uani 1 1 d U . .
N2 N 0.37933(15) 0.2235(2) 0.16436(14) 0.0203(5) Uani 1 1 d U . .
C2 C 0.29474(19) 0.1625(3) 0.23516(18) 0.0284(7) Uani 1 1 d U . .
H2 H 0.2718 0.1314 0.2752 0.034 Uiso 1 1 calc R . .
N3 N 0.18066(14) 0.30711(19) -0.10888(13) 0.0189(5) Uani 1 1 d U . .
C3 C 0.37383(19) 0.1729(3) 0.23225(18) 0.0279(7) Uani 1 1 d U . .
H3 H 0.4177 0.1501 0.2695 0.034 Uiso 1 1 calc R . .
N4 N 0.30411(15) 0.2872(2) -0.12517(14) 0.0207(5) Uani 1 1 d U . .
C4 C 0.16534(17) 0.1932(2) 0.15436(16) 0.0201(5) Uani 1 1 d U . .
C5 C 0.13607(19) 0.0933(2) 0.14530(17) 0.0218(6) Uani 1 1 d U . .
C6 C 0.05413(19) 0.0763(2) 0.14760(18) 0.0248(6) Uani 1 1 d U . .
H6 H 0.0334 0.0092 0.1409 0.030 Uiso 1 1 calc R . .
C7 C 0.00199(18) 0.1549(2) 0.15942(17) 0.0236(6) Uani 1 1 d U . .
C8 C 0.03201(18) 0.2529(2) 0.16417(17) 0.0229(6) Uani 1 1 d U . .
H8 H -0.0039 0.3073 0.1697 0.028 Uiso 1 1 calc R . .
C9 C 0.11351(18) 0.2747(2) 0.16117(16) 0.0202(5) Uani 1 1 d U . .
C10 C 0.1427(2) 0.3825(2) 0.1671(2) 0.0272(7) Uani 1 1 d U . .
H10A H 0.1932 0.3866 0.2040 0.041 Uiso 1 1 calc R . .
H10B H 0.1015 0.4256 0.1845 0.041 Uiso 1 1 calc R . .
H10C H 0.1524 0.4058 0.1166 0.041 Uiso 1 1 calc R . .
C11 C -0.0842(2) 0.1343(3) 0.1699(2) 0.0331(7) Uani 1 1 d U . .
H11A H -0.0848 0.1077 0.2216 0.050 Uiso 1 1 calc R . .
H11B H -0.1085 0.0843 0.1318 0.050 Uiso 1 1 calc R . .
H11C H -0.1155 0.1975 0.1630 0.050 Uiso 1 1 calc R . .
C12 C 0.1903(2) 0.0041(3) 0.1360(2) 0.0312(7) Uani 1 1 d U . .
H12A H 0.2174 -0.0184 0.1867 0.047 Uiso 1 1 calc R . .
H12B H 0.2311 0.0245 0.1049 0.047 Uiso 1 1 calc R . .
H12C H 0.1577 -0.0515 0.1104 0.047 Uiso 1 1 calc R . .
C13 C 0.45584(17) 0.2349(2) 0.13772(16) 0.0195(5) Uani 1 1 d U . .
C14 C 0.47240(18) 0.1685(2) 0.08046(17) 0.0199(6) Uani 1 1 d U . .
C15 C 0.54901(19) 0.1717(2) 0.05925(18) 0.0230(6) Uani 1 1 d U . .
H15 H 0.5610 0.1274 0.0201 0.028 Uiso 1 1 calc R . .
C16 C 0.60861(18) 0.2385(2) 0.09417(18) 0.0236(6) Uani 1 1 d U . .
C17 C 0.58972(18) 0.3033(2) 0.15027(18) 0.0234(6) Uani 1 1 d U . .
H17 H 0.6295 0.3503 0.1733 0.028 Uiso 1 1 calc R . .
C18 C 0.51399(18) 0.3021(2) 0.17432(17) 0.0216(6) Uani 1 1 d U . .
C19 C 0.5001(2) 0.3691(3) 0.2403(2) 0.0339(8) Uani 1 1 d U . .
H19A H 0.4417 0.3770 0.2398 0.051 Uiso 1 1 calc R . .
H19B H 0.5245 0.4358 0.2351 0.051 Uiso 1 1 calc R . .
H19C H 0.5250 0.3381 0.2889 0.051 Uiso 1 1 calc R . .
C20 C 0.6919(2) 0.2388(3) 0.0719(2) 0.0331(8) Uani 1 1 d U . .
H20A H 0.7283 0.2812 0.1079 0.050 Uiso 1 1 calc R . .
H20B H 0.6886 0.2662 0.0198 0.050 Uiso 1 1 calc R . .
H20C H 0.7130 0.1693 0.0733 0.050 Uiso 1 1 calc R . .
C21 C 0.4092(2) 0.0941(2) 0.0441(2) 0.0270(7) Uani 1 1 d U . .
H21A H 0.3905 0.0534 0.0842 0.040 Uiso 1 1 calc R . .
H21B H 0.4328 0.0494 0.0091 0.040 Uiso 1 1 calc R . .
H21C H 0.3633 0.1312 0.0151 0.040 Uiso 1 1 calc R . .
C22 C 0.25778(17) 0.2995(2) -0.06806(16) 0.0168(5) Uani 1 1 d U . .
C23 C 0.17979(19) 0.3035(3) -0.18779(17) 0.0266(7) Uani 1 1 d U . .
H23 H 0.1336 0.3089 -0.2269 0.032 Uiso 1 1 calc R . .
C24 C 0.25654(19) 0.2911(3) -0.19775(18) 0.0280(7) Uani 1 1 d U . .
H24 H 0.2754 0.2858 -0.2456 0.034 Uiso 1 1 calc R . .
C25 C 0.10551(17) 0.3029(2) -0.07903(15) 0.0193(5) Uani 1 1 d U . .
C26 C 0.08296(17) 0.2087(2) -0.05186(16) 0.0202(5) Uani 1 1 d U . .
C27 C 0.00546(18) 0.1993(2) -0.03290(17) 0.0231(6) Uani 1 1 d U . .
H27 H -0.0108 0.1360 -0.0147 0.028 Uiso 1 1 calc R . .
C28 C -0.04862(18) 0.2804(3) -0.03991(18) 0.0250(6) Uani 1 1 d U . .
C29 C -0.02399(19) 0.3724(3) -0.06664(18) 0.0264(6) Uani 1 1 d U . .
H29 H -0.0602 0.4285 -0.0707 0.032 Uiso 1 1 calc R . .
C30 C 0.05266(18) 0.3852(2) -0.08787(18) 0.0237(6) Uani 1 1 d U . .
C31 C 0.0729(2) 0.4847(3) -0.1219(2) 0.0338(8) Uani 1 1 d U . .
H31A H 0.0491 0.4866 -0.1765 0.051 Uiso 1 1 calc R . .
H31B H 0.1319 0.4918 -0.1166 0.051 Uiso 1 1 calc R . .
H31C H 0.0509 0.5405 -0.0950 0.051 Uiso 1 1 calc R . .
C32 C -0.1329(2) 0.2679(3) -0.0206(2) 0.0367(8) Uani 1 1 d U . .
H32A H -0.1422 0.1963 -0.0097 0.055 Uiso 1 1 calc R . .
H32B H -0.1730 0.2902 -0.0642 0.055 Uiso 1 1 calc R . .
H32C H -0.1381 0.3089 0.0247 0.055 Uiso 1 1 calc R . .
C33 C 0.13875(19) 0.1188(2) -0.04695(19) 0.0243(6) Uani 1 1 d U . .
H33A H 0.1120 0.0597 -0.0285 0.036 Uiso 1 1 calc R . .
H33B H 0.1887 0.1338 -0.0112 0.036 Uiso 1 1 calc R . .
H33C H 0.1520 0.1043 -0.0979 0.036 Uiso 1 1 calc R . .
C34 C 0.38801(18) 0.2561(3) -0.12056(17) 0.0227(6) Uani 1 1 d U . .
C35 C 0.4027(2) 0.1561(3) -0.14112(19) 0.0284(7) Uani 1 1 d U . .
C36 C 0.4819(2) 0.1277(3) -0.1473(2) 0.0327(7) Uani 1 1 d U . .
H36 H 0.4924 0.0599 -0.1612 0.039 Uiso 1 1 calc R . .
C37 C 0.5454(2) 0.1965(3) -0.1336(2) 0.0327(7) Uani 1 1 d U . .
C38 C 0.52916(19) 0.2947(3) -0.11363(19) 0.0300(7) Uani 1 1 d U . .
H38 H 0.5726 0.3419 -0.1042 0.036 Uiso 1 1 calc R . .
C39 C 0.45082(19) 0.3272(3) -0.10682(18) 0.0259(6) Uani 1 1 d U . .
C40 C 0.4363(2) 0.4350(3) -0.0868(2) 0.0378(8) Uani 1 1 d U . .
H40A H 0.3908 0.4623 -0.1232 0.057 Uiso 1 1 calc R . .
H40B H 0.4851 0.4752 -0.0896 0.057 Uiso 1 1 calc R . .
H40C H 0.4235 0.4384 -0.0346 0.057 Uiso 1 1 calc R . .
C41 C 0.6309(2) 0.1642(3) -0.1398(2) 0.0417(9) Uani 1 1 d U . .
H41A H 0.6593 0.2205 -0.1600 0.063 Uiso 1 1 calc R . .
H41B H 0.6291 0.1059 -0.1745 0.063 Uiso 1 1 calc R . .
H41C H 0.6596 0.1452 -0.0888 0.063 Uiso 1 1 calc R . .
C42 C 0.3356(2) 0.0780(3) -0.1573(2) 0.0377(8) Uani 1 1 d U . .
H42A H 0.2974 0.0873 -0.1212 0.057 Uiso 1 1 calc R . .
H42B H 0.3590 0.0097 -0.1512 0.057 Uiso 1 1 calc R . .
H42C H 0.3070 0.0864 -0.2100 0.057 Uiso 1 1 calc R . .
C43 C 0.2720(2) 0.4952(2) -0.01784(19) 0.0276(7) Uani 1 1 d U . .
H43A H 0.2233 0.5290 -0.0060 0.041 Uiso 1 1 calc R . .
H43B H 0.2660 0.4831 -0.0733 0.041 Uiso 1 1 calc R . .
H43C H 0.3194 0.5385 -0.0016 0.041 Uiso 1 1 calc R . .
C44 C 0.32005(19) 0.4546(2) 0.13394(18) 0.0245(6) Uani 1 1 d U . .
H44A H 0.3180 0.4179 0.1819 0.037 Uiso 1 1 calc R . .
H44B H 0.2821 0.5118 0.1297 0.037 Uiso 1 1 calc R . .
H44C H 0.3752 0.4800 0.1340 0.037 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Pt1 C22 113.03(11) . . ?
C1 Pt1 C43 164.28(12) . . ?
C22 Pt1 C43 82.44(12) . . ?
C1 Pt1 C44 83.58(12) . . ?
C22 Pt1 C44 163.27(12) . . ?
C43 Pt1 C44 81.09(13) . . ?
C1 N1 C2 111.5(2) . . ?
C1 N1 C4 131.3(2) . . ?
C2 N1 C4 116.9(2) . . ?
N2 C1 N1 102.4(2) . . ?
N2 C1 Pt1 122.8(2) . . ?
N1 C1 Pt1 131.4(2) . . ?
C1 N2 C3 112.3(2) . . ?
C1 N2 C13 125.8(2) . . ?
C3 N2 C13 121.3(2) . . ?
C3 C2 N1 107.0(3) . . ?
C22 N3 C23 112.2(2) . . ?
C22 N3 C25 127.3(2) . . ?
C23 N3 C25 119.9(2) . . ?
C2 C3 N2 106.7(3) . . ?
C22 N4 C24 111.3(2) . . ?
C22 N4 C34 130.3(2) . . ?
C24 N4 C34 117.6(3) . . ?
C9 C4 C5 121.4(3) . . ?
C9 C4 N1 121.1(3) . . ?
C5 C4 N1 116.8(3) . . ?
C6 C5 C4 118.3(3) . . ?
C6 C5 C12 119.2(3) . . ?
C4 C5 C12 122.5(3) . . ?
C7 C6 C5 121.8(3) . . ?
C8 C7 C6 118.3(3) . . ?
C8 C7 C11 120.3(3) . . ?
C6 C7 C11 121.3(3) . . ?
C7 C8 C9 122.3(3) . . ?
C4 C9 C8 117.7(3) . . ?
C4 C9 C10 122.3(3) . . ?
C8 C9 C10 119.9(3) . . ?
C18 C13 C14 121.8(3) . . ?
C18 C13 N2 120.3(3) . . ?
C14 C13 N2 117.5(3) . . ?
C15 C14 C13 118.3(3) . . ?
C15 C14 C21 121.2(3) . . ?
C13 C14 C21 120.5(3) . . ?
C14 C15 C16 121.5(3) . . ?
C17 C16 C15 118.4(3) . . ?
C17 C16 C20 120.9(3) . . ?
C15 C16 C20 120.7(3) . . ?
C16 C17 C18 122.3(3) . . ?
C13 C18 C17 117.7(3) . . ?
C13 C18 C19 123.1(3) . . ?
C17 C18 C19 119.2(3) . . ?
N3 C22 N4 102.5(2) . . ?
N3 C22 Pt1 122.0(2) . . ?
N4 C22 Pt1 130.4(2) . . ?
C24 C23 N3 106.5(3) . . ?
C23 C24 N4 107.5(3) . . ?
C30 C25 C26 121.8(3) . . ?
C30 C25 N3 120.3(3) . . ?
C26 C25 N3 117.2(3) . . ?
C27 C26 C25 118.1(3) . . ?
C27 C26 C33 120.6(3) . . ?
C25 C26 C33 121.2(3) . . ?
C28 C27 C26 121.7(3) . . ?
C29 C28 C27 118.5(3) . . ?
C29 C28 C32 120.8(3) . . ?
C27 C28 C32 120.8(3) . . ?
C28 C29 C30 122.0(3) . . ?
C25 C30 C29 117.9(3) . . ?
C25 C30 C31 122.9(3) . . ?
C29 C30 C31 119.1(3) . . ?
C39 C34 C35 121.1(3) . . ?
C39 C34 N4 120.8(3) . . ?
C35 C34 N4 117.4(3) . . ?
C36 C35 C34 118.8(3) . . ?
C36 C35 C42 119.0(3) . . ?
C34 C35 C42 122.2(3) . . ?
C37 C36 C35 121.3(3) . . ?
C38 C37 C36 118.7(3) . . ?
C38 C37 C41 120.7(3) . . ?
C36 C37 C41 120.6(4) . . ?
C37 C38 C39 122.3(3) . . ?
C34 C39 C38 117.8(3) . . ?
C34 C39 C40 122.1(3) . . ?
C38 C39 C40 120.1(3) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C1 2.043(3) . ?
Pt1 C22 2.044(3) . ?
Pt1 C43 2.091(3) . ?
Pt1 C44 2.093(3) . ?
N1 C1 1.380(4) . ?
N1 C2 1.396(4) . ?
N1 C4 1.445(4) . ?
C1 N2 1.375(4) . ?
N2 C3 1.387(4) . ?
N2 C13 1.441(4) . ?
C2 C3 1.339(4) . ?
N3 C22 1.374(3) . ?
N3 C23 1.391(4) . ?
N3 C25 1.440(4) . ?
N4 C22 1.377(4) . ?
N4 C24 1.393(4) . ?
N4 C34 1.450(4) . ?
C4 C9 1.398(4) . ?
C4 C5 1.404(4) . ?
C5 C6 1.395(4) . ?
C5 C12 1.510(4) . ?
C6 C7 1.391(4) . ?
C7 C8 1.384(4) . ?
C7 C11 1.507(4) . ?
C8 C9 1.402(4) . ?
C9 C10 1.500(4) . ?
C13 C18 1.393(4) . ?
C13 C14 1.398(4) . ?
C14 C15 1.392(4) . ?
C14 C21 1.505(4) . ?
C15 C16 1.395(4) . ?
C16 C17 1.382(4) . ?
C16 C20 1.508(4) . ?
C17 C18 1.400(4) . ?
C18 C19 1.510(4) . ?
C23 C24 1.333(5) . ?
C25 C30 1.391(4) . ?
C25 C26 1.405(4) . ?
C26 C27 1.395(4) . ?
C26 C33 1.501(4) . ?
C27 C28 1.392(4) . ?
C28 C29 1.388(5) . ?
C28 C32 1.512(4) . ?
C29 C30 1.402(4) . ?
C30 C31 1.504(5) . ?
C34 C39 1.398(4) . ?
C34 C35 1.400(5) . ?
C35 C36 1.397(5) . ?
C35 C42 1.515(5) . ?
C36 C37 1.388(5) . ?
C37 C38 1.379(5) . ?
C37 C41 1.512(5) . ?
C38 C39 1.401(5) . ?
C39 C40 1.494(5) . ?
