#------------------------------------------------------------------------------
#$Date: 2016-03-26 03:42:01 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180192 $
#$URL: svn://www.crystallography.net/cod/cif/7/10/88/7108825.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7108825
loop_
_publ_author_name
'Sheng-Chun Chen'
'Zhi-Hui Zhang'
'Qun Chen'
'Li-Qun Wang'
'Juan Xu'
'Ming-Yang He'
'Miao Du'
'Xiao-Ping Yang'
'Richard A.Jones'
_publ_section_title
;
 An efficient strategy to achieve hydrophilic polymeric silver(I)
 materials with exceptional antibacterial activity
;
_journal_name_full               Chem.Commun.
_journal_page_first              1270
_journal_paper_doi               10.1039/c2cc36538c
_journal_volume                  49
_journal_year                    2012
_chemical_formula_moiety         'C38 H14 Ag8 F16 N2 O18'
_chemical_formula_sum            'C38 H14 Ag8 F16 N2 O18'
_chemical_formula_weight         1953.47
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 120.181(5)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   17.9401(17)
_cell_length_b                   12.8038(11)
_cell_length_c                   23.0195(16)
_cell_measurement_reflns_used    9750
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      28.50
_cell_measurement_theta_min      2.38
_cell_volume                     4570.8(7)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.981
_diffrn_measured_fraction_theta_max 0.981
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0332
_diffrn_reflns_av_sigmaI/netI    0.0373
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            25557
_diffrn_reflns_theta_full        25.52
_diffrn_reflns_theta_max         25.52
_diffrn_reflns_theta_min         1.79
_exptl_absorpt_coefficient_mu    3.498
_exptl_absorpt_correction_T_max  0.465
_exptl_absorpt_correction_T_min  0.417
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.839
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             3680
_exptl_crystal_size_max          0.26
_exptl_crystal_size_mid          0.24
_exptl_crystal_size_min          0.22
_refine_diff_density_max         1.280
_refine_diff_density_min         -1.355
_refine_diff_density_rms         0.118
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.003
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     777
_refine_ls_number_reflns         8358
_refine_ls_number_restraints     38
_refine_ls_restrained_S_all      1.009
_refine_ls_R_factor_all          0.0603
_refine_ls_R_factor_gt           0.0412
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0334P)²+23.5503P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0895
_refine_ls_wR_factor_ref         0.0997
_reflns_number_gt                6406
_reflns_number_total             8358
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c2cc36538c.txt
_cod_data_source_block           1
_cod_original_sg_symbol_H-M      P2(1)/c
_cod_database_code               7108825
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_group
Ag1 Ag 0.55296(4) 0.96341(4) 0.97169(3) 0.05233(15) Uani 1 1 d . .
Ag2 Ag 0.41997(4) 0.72223(6) 0.92217(3) 0.0683(2) Uani 1 1 d . .
Ag3 Ag 0.54075(4) 0.83780(5) 0.80599(3) 0.05823(17) Uani 1 1 d . .
Ag4 Ag 0.41640(4) 0.80540(5) 0.65605(3) 0.05975(17) Uani 1 1 d . .
Ag5 Ag 0.53122(4) 0.57499(4) 0.70520(3) 0.04870(15) Uani 1 1 d . .
Ag6 Ag 0.40439(4) 0.57866(5) 0.76427(3) 0.05956(17) Uani 1 1 d . .
Ag7 Ag 0.55956(4) 0.46442(5) 0.97368(3) 0.0686(2) Uani 1 1 d . .
Ag8 Ag 0.52978(3) 0.79038(4) 1.05960(2) 0.04338(14) Uani 1 1 d . .
F1 F 0.8493(3) 1.1926(4) 1.1259(2) 0.0795(15) Uani 1 1 d . .
F2 F 0.9794(3) 1.0884(5) 1.1319(3) 0.109(2) Uani 1 1 d . .
F3 F 0.9547(4) 0.9567(5) 1.0313(3) 0.110(2) Uani 1 1 d . .
F4 F 0.7967(3) 0.9372(4) 0.9212(3) 0.0766(14) Uani 1 1 d . .
F5 F 0.2099(5) 1.0595(5) 0.8559(3) 0.112(2) Uani 1 1 d . .
F6 F 0.0543(4) 1.0078(7) 0.7568(5) 0.168(4) Uani 1 1 d . .
F7 F 0.0362(4) 0.8833(7) 0.6583(4) 0.163(3) Uani 1 1 d . .
F8 F 0.1708(6) 0.8078(5) 0.6572(3) 0.138(3) Uani 1 1 d . .
F9 F 0.7905(3) 0.8035(4) 1.0569(2) 0.0766(14) Uani 1 1 d . .
F10 F 0.9209(3) 0.7335(5) 1.0441(3) 0.0947(17) Uani 1 1 d . .
F11 F 0.8932(3) 0.5928(4) 0.9470(3) 0.0863(16) Uani 1 1 d . .
F12 F 0.7329(3) 0.5267(3) 0.8613(2) 0.0626(12) Uani 1 1 d . .
F13 F 0.7448(3) 0.7120(4) 0.8065(2) 0.0837(16) Uani 1 1 d . .
F14 F 0.9020(3) 0.6897(4) 0.8202(3) 0.0939(18) Uani 1 1 d . .
F15 F 0.9377(3) 0.7831(5) 0.7305(3) 0.0893(17) Uani 1 1 d . .
F16 F 0.8194(3) 0.8966(4) 0.6315(2) 0.0723(13) Uani 1 1 d . .
O1 O 0.6015(3) 1.1607(4) 0.9626(2) 0.0587(14) Uani 1 1 d . .
O2 O 0.6853(3) 1.2401(4) 1.0605(2) 0.0567(13) Uani 1 1 d . .
O3 O 0.6081(4) 0.9654(5) 0.8970(3) 0.0773(18) Uani 1 1 d . .
O4 O 0.6376(4) 1.1046(4) 0.8532(2) 0.0648(15) Uani 1 1 d U .
O5A O 0.4025(5) 0.9425(6) 0.9186(4) 0.067(2) Uani 0.715(5) 1 d PD 1
O6A O 0.3903(5) 1.0792(6) 0.8550(4) 0.062(2) Uani 0.715(5) 1 d PD 1
O7A O 0.3296(5) 0.7988(6) 0.7037(3) 0.0607(19) Uani 0.715(5) 1 d PD 1
O8A O 0.4145(5) 0.8934(7) 0.7962(5) 0.081(3) Uani 0.715(5) 1 d PD 1
O9A O 0.6233(9) 0.7915(6) 1.0193(3) 0.053(2) Uani 0.715(5) 1 d PD 1
O10A O 0.5416(5) 0.6910(9) 0.9312(5) 0.084(4) Uani 0.715(5) 1 d PD 1
O5B O 0.3516(13) 0.9994(17) 0.9200(7) 0.067(2) Uani 0.285(5) 1 d PD 2
O6B O 0.4328(9) 1.0249(17) 0.8786(10) 0.062(2) Uani 0.285(5) 1 d PD 2
O7B O 0.3977(11) 0.9052(14) 0.7413(9) 0.0607(19) Uani 0.285(5) 1 d PD 2
O8B O 0.4057(11) 0.8221(16) 0.8080(8) 0.081(3) Uani 0.285(5) 1 d PD 2
O9B O 0.635(3) 0.756(2) 1.0319(7) 0.053(2) Uani 0.285(5) 1 d PD 2
O10B O 0.5478(12) 0.759(2) 0.9185(8) 0.084(4) Uani 0.285(5) 1 d PD 2
O11 O 0.5541(4) 0.5148(5) 0.8663(3) 0.0783(17) Uani 1 1 d U .
O12 O 0.5531(3) 0.6488(4) 0.8060(2) 0.0521(12) Uani 1 1 d U .
O13 O 0.6146(3) 0.8888(4) 0.7526(2) 0.0523(12) Uani 1 1 d . .
O14 O 0.5524(3) 0.7623(4) 0.6769(2) 0.0478(11) Uani 1 1 d . .
O15 O 0.5710(3) 0.9088(4) 0.5962(3) 0.0646(15) Uani 1 1 d U .
O16 O 0.6635(3) 0.9786(4) 0.5703(2) 0.0556(13) Uani 1 1 d . .
O17 O 0.3219(3) 0.6339(5) 0.8116(2) 0.0637(15) Uani 1 1 d . .
N1 N 0.1785(4) 0.6086(5) 0.7421(3) 0.0539(15) Uani 1 1 d . .
C1 C 0.6730(4) 1.1811(5) 1.0135(3) 0.0432(16) Uani 1 1 d . .
C2 C 0.7483(4) 1.1238(5) 1.0170(3) 0.0424(15) Uani 1 1 d . .
C3 C 0.8313(5) 1.1316(6) 1.0728(3) 0.0548(19) Uani 1 1 d . .
C4 C 0.8992(5) 1.0774(7) 1.0770(4) 0.070(2) Uani 1 1 d . .
C5 C 0.8885(5) 1.0123(7) 1.0274(5) 0.069(2) Uani 1 1 d . .
C6 C 0.8078(5) 1.0032(6) 0.9712(4) 0.0559(19) Uani 1 1 d . .
C7 C 0.7382(4) 1.0579(5) 0.9649(3) 0.0415(15) Uani 1 1 d . .
C8 C 0.6535(5) 1.0423(6) 0.9001(4) 0.0509(18) Uani 1 1 d . .
C9 C 0.3616(5) 0.9983(6) 0.8672(4) 0.059(2) Uani 1 1 d D .
C10 C 0.2789(4) 0.9611(5) 0.8104(3) 0.0398(15) Uani 1 1 d . .
C11 C 0.2037(6) 0.9967(6) 0.8069(4) 0.060(2) Uani 1 1 d . .
C12 C 0.1251(6) 0.9710(8) 0.7577(6) 0.081(3) Uani 1 1 d . .
C13 C 0.1165(6) 0.9095(9) 0.7093(5) 0.087(3) Uani 1 1 d . .
C14 C 0.1859(7) 0.8708(7) 0.7077(4) 0.070(3) Uani 1 1 d . .
C15 C 0.2707(5) 0.8958(5) 0.7592(3) 0.0459(17) Uani 1 1 d . .
C16 C 0.3447(6) 0.8577(6) 0.7538(5) 0.067(2) Uani 1 1 d D .
C17 C 0.6140(5) 0.7333(6) 0.9735(3) 0.0491(17) Uani 1 1 d D .
C18 C 0.6883(4) 0.7004(5) 0.9649(3) 0.0385(14) Uani 1 1 d . .
C19 C 0.7732(5) 0.7345(6) 1.0078(3) 0.0498(18) Uani 1 1 d . .
C20 C 0.8408(5) 0.6991(6) 1.0020(4) 0.057(2) Uani 1 1 d . .
C21 C 0.8260(5) 0.6286(6) 0.9524(4) 0.0545(19) Uani 1 1 d . .
C22 C 0.7441(5) 0.5948(5) 0.9094(3) 0.0447(16) Uani 1 1 d . .
C23 C 0.6750(4) 0.6305(5) 0.9137(3) 0.0377(14) Uani 1 1 d . .
C24 C 0.5861(5) 0.5956(6) 0.8592(3) 0.0477(17) Uani 1 1 d . .
C25 C 0.6128(4) 0.8243(5) 0.7113(3) 0.0414(15) Uani 1 1 d . .
C26 C 0.6971(4) 0.8147(5) 0.7099(3) 0.0355(14) Uani 1 1 d . .
C27 C 0.7609(5) 0.7583(6) 0.7612(3) 0.0503(18) Uani 1 1 d . .
C28 C 0.8406(5) 0.7467(6) 0.7689(4) 0.060(2) Uani 1 1 d . .
C29 C 0.8590(5) 0.7938(6) 0.7243(4) 0.058(2) Uani 1 1 d . .
C30 C 0.7969(4) 0.8523(6) 0.6731(3) 0.0461(16) Uani 1 1 d . .
C31 C 0.7143(4) 0.8638(5) 0.6635(3) 0.0347(14) Uani 1 1 d . .
C32 C 0.6450(4) 0.9235(5) 0.6049(3) 0.0376(14) Uani 1 1 d . .
C33 C 0.2465(5) 0.6388(6) 0.7984(3) 0.0514(18) Uani 1 1 d . .
H33A H 0.2367 0.6666 0.8313 0.062 Uiso 1 1 calc R .
C34 C 0.1863(6) 0.5596(7) 0.6887(4) 0.074(3) Uani 1 1 d . .
H34A H 0.2452 0.5397 0.7054 0.111 Uiso 1 1 calc R .
H34B H 0.1688 0.6080 0.6522 0.111 Uiso 1 1 calc R .
H34C H 0.1502 0.4988 0.6731 0.111 Uiso 1 1 calc R .
C35 C 0.0931(6) 0.6197(10) 0.7323(5) 0.102(4) Uani 1 1 d . .
H35A H 0.0964 0.6530 0.7709 0.152 Uiso 1 1 calc R .
H35B H 0.0672 0.5520 0.7263 0.152 Uiso 1 1 calc R .
H35C H 0.0587 0.6615 0.6931 0.152 Uiso 1 1 calc R .
N2 N 0.1578(5) 0.8699(6) 0.4861(3) 0.072(2) Uani 1 1 d D .
O18A O 0.2909(17) 0.847(3) 0.5569(18) 0.084(7) Uani 0.409(8) 1 d PD 1
C36A C 0.2409(10) 0.8996(15) 0.4940(11) 0.066(3) Uani 0.409(8) 1 d PD 1
H36A H 0.2561 0.9388 0.4675 0.079 Uiso 0.409(8) 1 calc PR 1
C37A C 0.0915(14) 0.912(2) 0.4251(9) 0.092(5) Uani 0.409(8) 1 d PD 1
H37A H 0.0393 0.8733 0.4106 0.139 Uiso 0.409(8) 1 calc PR 1
H37B H 0.1080 0.9077 0.3914 0.139 Uiso 0.409(8) 1 calc PR 1
H37C H 0.0823 0.9839 0.4318 0.139 Uiso 0.409(8) 1 calc PR 1
C38A C 0.1568(19) 0.820(2) 0.5394(10) 0.094(5) Uani 0.409(8) 1 d PD 1
H38A H 0.1001 0.7927 0.5247 0.141 Uiso 0.409(8) 1 calc PR 1
H38B H 0.1722 0.8684 0.5754 0.141 Uiso 0.409(8) 1 calc PR 1
H38C H 0.1975 0.7631 0.5550 0.141 Uiso 0.409(8) 1 calc PR 1
O18B O 0.3131(9) 0.873(2) 0.5483(12) 0.084(7) Uani 0.591(8) 1 d PD 2
C36B C 0.2364(9) 0.8362(11) 0.5464(7) 0.066(3) Uani 0.591(8) 1 d PD 2
H36B H 0.2367 0.7953 0.5800 0.079 Uiso 0.591(8) 1 calc PR 2
C37B C 0.1557(14) 0.9290(14) 0.4345(8) 0.092(5) Uani 0.591(8) 1 d PD 2
H37D H 0.1082 0.9067 0.3921 0.139 Uiso 0.591(8) 1 calc PR 2
H37E H 0.2086 0.9196 0.4343 0.139 Uiso 0.591(8) 1 calc PR 2
H37F H 0.1487 1.0015 0.4414 0.139 Uiso 0.591(8) 1 calc PR 2
C38B C 0.0855(10) 0.8304(15) 0.4883(9) 0.094(5) Uani 0.591(8) 1 d PD 2
H38D H 0.0502 0.7902 0.4486 0.141 Uiso 0.591(8) 1 calc PR 2
H38E H 0.0524 0.8874 0.4908 0.141 Uiso 0.591(8) 1 calc PR 2
H38F H 0.1048 0.7867 0.5272 0.141 Uiso 0.591(8) 1 calc PR 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O5B Ag1 O6B 143.0(8) 3_677 .
O5B Ag1 O5A 129.3(4) 3_677 .
O6B Ag1 O5A 42.0(4) . .
O5B Ag1 O3 115.9(4) 3_677 .
O6B Ag1 O3 81.8(4) . .
O5A Ag1 O3 114.3(2) . .
O5B Ag1 O9A 76.5(6) 3_677 .
O6B Ag1 O9A 138.2(6) . .
O5A Ag1 O9A 108.8(4) . .
O3 Ag1 O9A 91.4(3) . .
O5B Ag1 O5A 27.7(5) 3_677 3_677
O6B Ag1 O5A 116.5(5) . 3_677
O5A Ag1 O5A 106.0(2) . 3_677
O3 Ag1 O5A 132.7(2) . 3_677
O9A Ag1 O5A 98.3(2) . 3_677
O5B Ag1 Ag1 75.1(5) 3_677 3_677
O6B Ag1 Ag1 77.9(4) . 3_677
O5A Ag1 Ag1 55.9(2) . 3_677
O3 Ag1 Ag1 155.87(18) . 3_677
O9A Ag1 Ag1 112.4(3) . 3_677
O5A Ag1 Ag1 50.12(19) 3_677 3_677
O5B Ag1 Ag8 73.2(5) 3_677 .
O6B Ag1 Ag8 118.4(4) . .
O5A Ag1 Ag8 76.54(17) . .
O3 Ag1 Ag8 134.93(17) . .
O9A Ag1 Ag8 45.8(3) . .
O5A Ag1 Ag8 76.87(16) 3_677 .
Ag1 Ag1 Ag8 67.57(2) 3_677 .
O10A Ag2 O2 165.8(3) . 3_677
O10A Ag2 O10B 23.2(6) . .
O2 Ag2 O10B 154.7(7) 3_677 .
O10A Ag2 O17 100.1(2) . .
O2 Ag2 O17 93.17(17) 3_677 .
O10B Ag2 O17 104.4(5) . .
O10A Ag2 Ag8 81.3(2) . .
O2 Ag2 Ag8 84.78(12) 3_677 .
O10B Ag2 Ag8 80.9(5) . .
O17 Ag2 Ag8 170.01(14) . .
O10A Ag2 Ag7 93.4(3) . 3_667
O2 Ag2 Ag7 79.32(15) 3_677 3_667
O10B Ag2 Ag7 114.5(5) . 3_667
O17 Ag2 Ag7 100.17(14) . 3_667
Ag8 Ag2 Ag7 69.85(2) . 3_667
O8A Ag3 O13 131.9(3) . .
O8A Ag3 O7B 28.5(4) . .
O13 Ag3 O7B 106.9(4) . .
O8A Ag3 O12 113.4(3) . .
O13 Ag3 O12 101.85(17) . .
O7B Ag3 O12 115.4(4) . .
O8A Ag3 O3 85.1(2) . .
O13 Ag3 O3 95.69(18) . .
O7B Ag3 O3 101.9(4) . .
O12 Ag3 O3 131.3(2) . .
O8A Ag3 O8B 23.7(4) . .
O13 Ag3 O8B 150.4(4) . .
O7B Ag3 O8B 44.0(5) . .
O12 Ag3 O8B 90.5(5) . .
O3 Ag3 O8B 96.0(5) . .
O8A Ag3 Ag4 78.8(2) . .
O13 Ag3 Ag4 74.05(12) . .
O7B Ag3 Ag4 53.0(4) . .
O12 Ag3 Ag4 83.09(11) . .
O3 Ag3 Ag4 145.64(17) . .
O8B Ag3 Ag4 81.0(4) . .
O8A Ag3 Ag5 50.6(3) . 2_656
O13 Ag3 Ag5 90.28(13) . 2_656
O7B Ag3 Ag5 49.9(4) . 2_656
O12 Ag3 Ag5 163.81(13) . 2_656
O3 Ag3 Ag5 56.66(17) . 2_656
O8B Ag3 Ag5 73.9(5) . 2_656
Ag4 Ag3 Ag5 90.11(2) . 2_656
O14 Ag4 O7A 141.9(2) . .
O14 Ag4 O18A 131.4(11) . .
O7A Ag4 O18A 85.6(10) . .
O14 Ag4 O18B 119.4(5) . .
O7A Ag4 O18B 98.6(6) . .
O18A Ag4 O18B 15.1(11) . .
O14 Ag4 O7B 120.3(4) . .
O7A Ag4 O7B 42.2(4) . .
O18A Ag4 O7B 102.0(13) . .
O18B Ag4 O7B 106.8(9) . .
O14 Ag4 Ag3 72.64(11) . .
O7A Ag4 Ag3 75.67(17) . .
O18A Ag4 Ag3 151.1(12) . .
O18B Ag4 Ag3 150.2(7) . .
O7B Ag4 Ag3 49.7(5) . .
O12 Ag5 O6B 156.9(5) . 2_646
O12 Ag5 O6A 134.4(2) . 2_646
O6B Ag5 O6A 23.2(5) 2_646 2_646
O12 Ag5 O7B 94.2(4) . 2_646
O6B Ag5 O7B 83.6(6) 2_646 2_646
O6A Ag5 O7B 90.1(4) 2_646 2_646
O12 Ag5 O8A 120.6(2) . 2_646
O6B Ag5 O8A 59.0(5) 2_646 2_646
O6A Ag5 O8A 71.0(3) 2_646 2_646
O7B Ag5 O8A 26.5(4) 2_646 2_646
O12 Ag5 O14 84.39(16) . .
O6B Ag5 O14 84.9(5) 2_646 .
O6A Ag5 O14 68.3(2) 2_646 .
O7B Ag5 O14 146.3(4) 2_646 .
O8A Ag5 O14 138.6(2) 2_646 .
O12 Ag5 Ag6 51.12(13) . .
O6B Ag5 Ag6 152.0(5) 2_646 .
O6A Ag5 Ag6 171.73(18) 2_646 .
O7B Ag5 Ag6 95.7(3) 2_646 .
O8A Ag5 Ag6 112.46(19) 2_646 .
O14 Ag5 Ag6 108.90(11) . .
O12 Ag5 Ag3 108.40(12) . 2_646
O6B Ag5 Ag3 86.8(5) 2_646 2_646
O6A Ag5 Ag3 107.25(19) 2_646 2_646
O7B Ag5 Ag3 46.7(5) 2_646 2_646
O8A Ag5 Ag3 44.10(19) 2_646 2_646
O14 Ag5 Ag3 162.80(10) . 2_646
Ag6 Ag5 Ag3 73.01(2) . 2_646
O17 Ag6 O4 123.99(19) . 2_646
O17 Ag6 O13 107.57(19) . 2_646
O4 Ag6 O13 91.07(17) 2_646 2_646
O17 Ag6 O12 120.83(17) . .
O4 Ag6 O12 93.02(17) 2_646 .
O13 Ag6 O12 116.86(16) 2_646 .
O17 Ag6 Ag5 162.97(15) . .
O4 Ag6 Ag5 54.35(14) 2_646 .
O13 Ag6 Ag5 89.44(11) 2_646 .
O12 Ag6 Ag5 46.93(10) . .
O16 Ag7 O15 154.93(19) 4_576 2_646
O16 Ag7 O11 120.48(19) 4_576 .
O15 Ag7 O11 82.08(19) 2_646 .
O16 Ag7 Ag7 84.67(13) 4_576 3_667
O15 Ag7 Ag7 71.78(13) 2_646 3_667
O11 Ag7 Ag7 128.39(16) . 3_667
O16 Ag7 Ag2 76.96(15) 4_576 3_667
O15 Ag7 Ag2 89.14(16) 2_646 3_667
O11 Ag7 Ag2 147.57(16) . 3_667
Ag7 Ag7 Ag2 76.83(3) 3_667 3_667
O1 Ag8 O9A 144.0(2) 3_677 .
O1 Ag8 O9B 154.3(5) 3_677 .
O9A Ag8 O9B 13.0(7) . .
O1 Ag8 O6A 96.8(2) 3_677 3_677
O9A Ag8 O6A 94.0(3) . 3_677
O9B Ag8 O6A 97.0(8) . 3_677
O1 Ag8 Ag2 76.98(11) 3_677 .
O9A Ag8 Ag2 78.1(2) . .
O9B Ag8 Ag2 81.0(6) . .
O6A Ag8 Ag2 153.36(19) 3_677 .
O1 Ag8 Ag1 96.88(15) 3_677 .
O9A Ag8 Ag1 51.55(19) . .
O9B Ag8 Ag1 64.5(7) . .
O6A Ag8 Ag1 79.75(17) 3_677 .
Ag2 Ag8 Ag1 75.42(2) . .
C1 O1 Ag8 128.3(4) . 3_677
C1 O2 Ag2 120.2(4) . 3_677
C8 O3 Ag1 117.5(4) . .
C8 O3 Ag3 126.7(5) . .
Ag1 O3 Ag3 114.1(2) . .
C8 O4 Ag6 132.7(5) . 2_656
C9 O5A Ag1 113.5(6) . .
C9 O5A Ag1 114.2(6) . 3_677
Ag1 O5A Ag1 74.0(2) . 3_677
C9 O6A Ag5 122.2(6) . 2_656
C9 O6A Ag8 122.1(6) . 3_677
Ag5 O6A Ag8 101.7(3) 2_656 3_677
C16 O7A Ag4 120.9(6) . .
C16 O8A Ag3 122.0(7) . .
C16 O8A Ag5 125.4(8) . 2_656
Ag3 O8A Ag5 85.3(3) . 2_656
C17 O9A Ag8 122.2(10) . .
C17 O9A Ag1 109.6(6) . .
Ag8 O9A Ag1 82.7(3) . .
C17 O10A Ag2 126.3(7) . .
C9 O5B Ag1 130.1(12) . 3_677
C9 O6B Ag1 120.0(14) . .
C9 O6B Ag5 125.2(13) . 2_656
Ag1 O6B Ag5 109.7(5) . 2_656
C16 O7B O8B 44.0(9) . .
C16 O7B Ag3 112.1(13) . .
O8B O7B Ag3 70.0(9) . .
C16 O7B Ag4 110.0(10) . .
O8B O7B Ag4 112.3(11) . .
Ag3 O7B Ag4 77.2(5) . .
C16 O7B Ag5 123.6(11) . 2_656
O8B O7B Ag5 106.8(10) . 2_656
Ag3 O7B Ag5 83.4(5) . 2_656
Ag4 O7B Ag5 126.3(5) . 2_656
C16 O8B O7B 44.8(9) . .
C16 O8B Ag3 109.0(14) . .
O7B O8B Ag3 66.1(9) . .
C17 O9B Ag8 120(3) . .
C17 O10B Ag2 110.4(16) . .
C24 O11 Ag7 123.8(5) . .
C24 O12 Ag5 120.4(4) . .
C24 O12 Ag3 122.5(4) . .
Ag5 O12 Ag3 115.50(19) . .
C24 O12 Ag6 94.0(4) . .
Ag5 O12 Ag6 81.95(14) . .
Ag3 O12 Ag6 106.14(18) . .
C25 O13 Ag3 114.6(4) . .
C25 O13 Ag6 125.9(4) . 2_656
Ag3 O13 Ag6 107.01(19) . 2_656
C25 O14 Ag4 118.0(4) . .
C25 O14 Ag5 128.6(4) . .
Ag4 O14 Ag5 90.00(15) . .
C32 O15 Ag7 136.5(4) . 2_656
C32 O16 Ag7 118.7(4) . 4_575
C33 O17 Ag6 140.5(5) . .
C33 O17 Ag2 110.5(4) . .
Ag6 O17 Ag2 108.8(2) . .
C33 N1 C35 120.9(7) . .
C33 N1 C34 121.7(7) . .
C35 N1 C34 117.4(7) . .
O2 C1 O1 126.1(7) . .
O2 C1 C2 119.1(6) . .
O1 C1 C2 114.7(6) . .
C3 C2 C7 116.7(7) . .
C3 C2 C1 121.9(6) . .
C7 C2 C1 121.4(6) . .
F1 C3 C4 115.6(7) . .
F1 C3 C2 122.3(7) . .
C4 C3 C2 122.0(7) . .
C5 C4 C3 120.9(7) . .
C5 C4 F2 118.8(9) . .
C3 C4 F2 120.3(9) . .
F3 C5 C4 121.7(8) . .
F3 C5 C6 119.5(9) . .
C4 C5 C6 118.8(8) . .
F4 C6 C7 119.3(7) . .
F4 C6 C5 118.9(7) . .
C7 C6 C5 121.8(8) . .
C6 C7 C2 119.8(6) . .
C6 C7 C8 116.5(6) . .
C2 C7 C8 123.8(6) . .
O4 C8 O3 126.2(7) . .
O4 C8 C7 116.4(7) . .
O3 C8 C7 117.4(7) . .
O6B C9 O6A 46.3(10) . .
O6B C9 O5A 84.4(12) . .
O6A C9 O5A 124.8(8) . .
O6B C9 O5B 114.5(14) . .
O6A C9 O5B 117.5(11) . .
O5A C9 O5B 54.6(10) . .
O6B C9 C10 139.4(12) . .
O6A C9 C10 114.4(7) . .
O5A C9 C10 120.1(7) . .
O5B C9 C10 106.1(11) . .
C11 C10 C15 117.6(7) . .
C11 C10 C9 117.4(7) . .
C15 C10 C9 125.0(7) . .
C12 C11 F5 117.9(9) . .
C12 C11 C10 123.4(8) . .
F5 C11 C10 118.7(8) . .
C13 C12 C11 119.7(9) . .
C13 C12 F6 119.4(10) . .
C11 C12 F6 120.9(11) . .
C12 C13 C14 121.7(9) . .
C12 C13 F7 120.1(11) . .
C14 C13 F7 118.1(11) . .
F8 C14 C13 117.4(10) . .
F8 C14 C15 122.0(9) . .
C13 C14 C15 120.6(7) . .
C10 C15 C14 117.1(7) . .
C10 C15 C16 123.6(7) . .
C14 C15 C16 119.3(7) . .
O8A C16 O8B 46.8(11) . .
O8A C16 O7B 54.8(9) . .
O8B C16 O7B 91.2(16) . .
O8A C16 O7A 127.1(9) . .
O8B C16 O7A 111.2(12) . .
O7B C16 O7A 85.6(10) . .
O8A C16 C15 114.3(8) . .
O8B C16 C15 114.0(13) . .
O7B C16 C15 131.6(11) . .
O7A C16 C15 118.3(8) . .
O9A C17 O9B 24.5(13) . .
O9A C17 O10B 110.7(14) . .
O9B C17 O10B 130(2) . .
O9A C17 O10A 123.5(10) . .
O9B C17 O10A 124(2) . .
O10B C17 O10A 43.2(13) . .
O9A C17 C18 122.3(9) . .
O9B C17 C18 114(2) . .
O10B C17 C18 112.9(13) . .
O10A C17 C18 114.1(7) . .
C23 C18 C19 117.2(6) . .
C23 C18 C17 120.1(6) . .
C19 C18 C17 122.7(6) . .
F9 C19 C20 117.4(7) . .
F9 C19 C18 120.4(7) . .
C20 C19 C18 122.1(7) . .
F10 C20 C19 120.3(8) . .
F10 C20 C21 120.3(7) . .
C19 C20 C21 119.4(7) . .
F11 C21 C22 120.7(7) . .
F11 C21 C20 119.4(7) . .
C22 C21 C20 119.9(7) . .
F12 C22 C21 117.6(6) . .
F12 C22 C23 120.6(6) . .
C21 C22 C23 121.7(6) . .
C22 C23 C18 119.6(6) . .
C22 C23 C24 117.0(6) . .
C18 C23 C24 123.3(6) . .
O11 C24 O12 124.0(7) . .
O11 C24 C23 120.1(7) . .
O12 C24 C23 115.6(6) . .
O13 C25 O14 125.7(6) . .
O13 C25 C26 114.8(6) . .
O14 C25 C26 119.1(6) . .
C27 C26 C31 119.1(6) . .
C27 C26 C25 115.5(6) . .
C31 C26 C25 125.2(5) . .
F13 C27 C28 118.1(6) . .
F13 C27 C26 119.2(7) . .
C28 C27 C26 122.6(7) . .
F14 C28 C27 120.9(7) . .
F14 C28 C29 119.7(7) . .
C27 C28 C29 119.4(7) . .
F15 C29 C28 120.7(7) . .
F15 C29 C30 120.0(7) . .
C28 C29 C30 119.3(7) . .
F16 C30 C29 116.2(6) . .
F16 C30 C31 121.5(6) . .
C29 C30 C31 122.3(6) . .
C30 C31 C26 117.3(5) . .
C30 C31 C32 121.9(5) . .
C26 C31 C32 120.8(6) . .
O16 C32 O15 126.3(6) . .
O16 C32 C31 120.2(6) . .
O15 C32 C31 113.5(6) . .
O17 C33 N1 126.2(7) . .
O17 C33 H33A 116.9 . .
N1 C33 H33A 116.9 . .
N1 C34 H34A 109.5 . .
N1 C34 H34B 109.5 . .
H34A C34 H34B 109.5 . .
N1 C34 H34C 109.5 . .
H34A C34 H34C 109.5 . .
H34B C34 H34C 109.5 . .
N1 C35 H35A 109.5 . .
N1 C35 H35B 109.5 . .
H35A C35 H35B 109.5 . .
N1 C35 H35C 109.5 . .
H35A C35 H35C 109.5 . .
H35B C35 H35C 109.5 . .
C37B N2 C38A 174.2(15) . .
C37B N2 C37A 45.3(12) . .
C38A N2 C37A 132.4(18) . .
C37B N2 C38B 126.3(13) . .
C38A N2 C38B 52.1(13) . .
C37A N2 C38B 81.1(14) . .
C37B N2 C36A 63.4(12) . .
C38A N2 C36A 118.4(16) . .
C37A N2 C36A 108.7(16) . .
C38B N2 C36A 170.1(14) . .
C37B N2 C36B 124.8(12) . .
C38A N2 C36B 57.3(13) . .
C37A N2 C36B 170.0(15) . .
C38B N2 C36B 108.9(11) . .
C36A N2 C36B 61.4(12) . .
C36A O18A Ag4 155(2) . .
O18A C36A N2 94.9(18) . .
O18A C36A H36A 132.6 . .
N2 C36A H36A 132.6 . .
N2 C37A H37A 109.5 . .
N2 C37A H37B 109.5 . .
N2 C37A H37C 109.5 . .
N2 C38A H38A 109.5 . .
N2 C38A H38B 109.5 . .
N2 C38A H38C 109.5 . .
C36B O18B Ag4 98.2(13) . .
O18B C36B N2 112.6(15) . .
O18B C36B H36B 123.7 . .
N2 C36B H36B 123.7 . .
N2 C37B H37D 109.5 . .
N2 C37B H37E 109.5 . .
H37D C37B H37E 109.5 . .
N2 C37B H37F 109.5 . .
H37D C37B H37F 109.5 . .
H37E C37B H37F 109.5 . .
N2 C38B H38D 109.5 . .
N2 C38B H38E 109.5 . .
H38D C38B H38E 109.5 . .
N2 C38B H38F 109.5 . .
H38D C38B H38F 109.5 . .
H38E C38B H38F 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 O5B 2.255(17) 3_677
Ag1 O6B 2.28(2) .
Ag1 O5A 2.352(8) .
Ag1 O3 2.375(5) .
Ag1 O9A 2.500(7) .
Ag1 O5A 2.537(8) 3_677
Ag1 Ag1 2.9458(11) 3_677
Ag1 Ag8 3.1659(8) .
Ag2 O10A 2.123(9) .
Ag2 O2 2.173(5) 3_677
Ag2 O10B 2.38(3) .
Ag2 O17 2.519(5) .
Ag2 Ag8 2.8956(8) .
Ag2 Ag7 3.2724(10) 3_667
Ag3 O8A 2.276(8) .
Ag3 O13 2.309(5) .
Ag3 O7B 2.39(2) .
Ag3 O12 2.430(5) .
Ag3 O3 2.444(5) .
Ag3 O8B 2.46(2) .
Ag3 Ag4 3.0529(9) .
Ag3 Ag5 3.2592(9) 2_656
Ag4 O14 2.305(5) .
Ag4 O7A 2.315(7) .
Ag4 O18A 2.32(3) .
Ag4 O18B 2.39(2) .
Ag4 O7B 2.502(16) .
Ag5 O12 2.349(4) .
Ag5 O6B 2.408(18) 2_646
Ag5 O6A 2.422(8) 2_646
Ag5 O7B 2.508(16) 2_646
Ag5 O8A 2.528(10) 2_646
Ag5 O14 2.564(5) .
Ag5 Ag6 3.1842(8) .
Ag5 Ag3 3.2592(9) 2_646
Ag6 O17 2.345(5) .
Ag6 O4 2.436(5) 2_646
Ag6 O13 2.458(5) 2_646
Ag6 O12 2.503(5) .
Ag7 O16 2.188(5) 4_576
Ag7 O15 2.189(5) 2_646
Ag7 O11 2.509(6) .
Ag7 Ag7 3.0771(15) 3_667
Ag7 Ag2 3.2724(11) 3_667
Ag8 O1 2.234(5) 3_677
Ag8 O9A 2.289(13) .
Ag8 O9B 2.32(4) .
Ag8 O6A 2.423(7) 3_677
F1 C3 1.345(9) .
F2 C4 1.363(9) .
F3 C5 1.348(9) .
F4 C6 1.360(9) .
F5 C11 1.343(9) .
F6 C12 1.346(11) .
F7 C13 1.367(11) .
F8 C14 1.327(9) .
F9 C19 1.344(8) .
F10 C20 1.341(9) .
F11 C21 1.352(8) .
F12 C22 1.343(7) .
F13 C27 1.350(8) .
F14 C28 1.354(8) .
F15 C29 1.352(9) .
F16 C30 1.335(8) .
O1 C1 1.255(8) .
O1 Ag8 2.234(5) 3_677
O2 C1 1.244(8) .
O2 Ag2 2.173(5) 3_677
O3 C8 1.257(9) .
O4 C8 1.255(9) .
O4 Ag6 2.436(5) 2_656
O5A C9 1.256(9) .
O5A Ag1 2.537(8) 3_677
O6A C9 1.250(9) .
O6A Ag5 2.422(8) 2_656
O6A Ag8 2.423(7) 3_677
O7A C16 1.288(10) .
O8A C16 1.224(11) .
O8A Ag5 2.528(10) 2_656
O9A C17 1.232(8) .
O10A C17 1.287(10) .
O5B C9 1.314(12) .
O5B Ag1 2.255(16) 3_677
O6B C9 1.217(12) .
O6B Ag5 2.408(18) 2_656
O7B C16 1.278(12) .
O7B O8B 1.81(3) .
O7B Ag5 2.508(16) 2_656
O8B C16 1.261(13) .
O9B C17 1.233(11) .
O10B C17 1.269(12) .
O11 C24 1.235(9) .
O12 C24 1.258(8) .
O13 C25 1.248(8) .
O13 Ag6 2.458(5) 2_656
O14 C25 1.252(8) .
O15 C32 1.253(8) .
O15 Ag7 2.189(5) 2_656
O16 C32 1.229(8) .
O16 Ag7 2.188(4) 4_575
O17 C33 1.229(9) .
N1 C33 1.315(9) .
N1 C35 1.439(11) .
N1 C34 1.448(9) .
C1 C2 1.504(10) .
C2 C3 1.397(9) .
C2 C7 1.403(9) .
C3 C4 1.362(12) .
C4 C5 1.349(12) .
C5 C6 1.379(11) .
C6 C7 1.373(10) .
C7 C8 1.515(10) .
C9 C10 1.478(10) .
C10 C11 1.388(10) .
C10 C15 1.393(9) .
C11 C12 1.332(12) .
C12 C13 1.307(14) .
C13 C14 1.357(14) .
C14 C15 1.417(12) .
C15 C16 1.476(11) .
C17 C18 1.504(10) .
C18 C23 1.400(8) .
C18 C19 1.404(10) .
C19 C20 1.362(11) .
C20 C21 1.373(11) .
C21 C22 1.364(10) .
C22 C23 1.372(9) .
C23 C24 1.518(9) .
C25 C26 1.532(9) .
C26 C27 1.366(9) .
C26 C31 1.401(8) .
C27 C28 1.359(11) .
C28 C29 1.367(11) .
C29 C30 1.368(10) .
C30 C31 1.393(9) .
C31 C32 1.504(8) .
C33 H33A 0.9300 .
C34 H34A 0.9600 .
C34 H34B 0.9600 .
C34 H34C 0.9600 .
C35 H35A 0.9600 .
C35 H35B 0.9600 .
C35 H35C 0.9600 .
N2 C37B 1.393(11) .
N2 C38A 1.395(12) .
N2 C37A 1.414(12) .
N2 C38B 1.418(11) .
N2 C36A 1.459(14) .
N2 C36B 1.462(14) .
O18A C36A 1.43(2) .
C36A H36A 0.9300 .
C37A H37A 0.9600 .
C37A H37B 0.9600 .
C37A H37C 0.9600 .
C38A H38A 0.9600 .
C38A H38B 0.9600 .
C38A H38C 0.9600 .
O18B C36B 1.44(2) .
C36B H36B 0.9300 .
C37B H37D 0.9600 .
C37B H37E 0.9600 .
C37B H37F 0.9600 .
C38B H38D 0.9600 .
C38B H38E 0.9600 .
C38B H38F 0.9600 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O8A Ag3 Ag4 O14 176.8(3) . .
O13 Ag3 Ag4 O14 36.85(18) . .
O7B Ag3 Ag4 O14 163.2(5) . .
O12 Ag3 Ag4 O14 -67.62(17) . .
O3 Ag3 Ag4 O14 113.2(3) . .
O8B Ag3 Ag4 O14 -159.2(5) . .
Ag5 Ag3 Ag4 O14 127.11(12) 2_656 .
O8A Ag3 Ag4 O7A -24.6(3) . .
O13 Ag3 Ag4 O7A -164.6(2) . .
O7B Ag3 Ag4 O7A -38.2(5) . .
O12 Ag3 Ag4 O7A 91.0(2) . .
O3 Ag3 Ag4 O7A -88.2(3) . .
O8B Ag3 Ag4 O7A -0.7(5) . .
Ag5 Ag3 Ag4 O7A -74.3(2) 2_656 .
O8A Ag3 Ag4 O18A 26.4(18) . .
O13 Ag3 Ag4 O18A -113.5(17) . .
O7B Ag3 Ag4 O18A 12.8(18) . .
O12 Ag3 Ag4 O18A 142.0(17) . .
O3 Ag3 Ag4 O18A -37.1(18) . .
O8B Ag3 Ag4 O18A 50.4(18) . .
Ag5 Ag3 Ag4 O18A -23.2(17) 2_656 .
O8A Ag3 Ag4 O18B 57.6(9) . .
O13 Ag3 Ag4 O18B -82.4(9) . .
O7B Ag3 Ag4 O18B 44.0(10) . .
O12 Ag3 Ag4 O18B 173.2(9) . .
O3 Ag3 Ag4 O18B -6.0(9) . .
O8B Ag3 Ag4 O18B 81.6(10) . .
Ag5 Ag3 Ag4 O18B 7.9(9) 2_656 .
O8A Ag3 Ag4 O7B 13.6(5) . .
O13 Ag3 Ag4 O7B -126.3(5) . .
O12 Ag3 Ag4 O7B 129.2(5) . .
O3 Ag3 Ag4 O7B -49.9(5) . .
O8B Ag3 Ag4 O7B 37.6(6) . .
Ag5 Ag3 Ag4 O7B -36.1(5) 2_656 .
O12 Ag5 Ag6 O17 49.0(5) . .
O6B Ag5 Ag6 O17 -133.3(10) 2_646 .
O6A Ag5 Ag6 O17 -85.9(14) 2_646 .
O7B Ag5 Ag6 O17 139.7(6) 2_646 .
O8A Ag5 Ag6 O17 161.0(5) 2_646 .
O14 Ag5 Ag6 O17 -16.9(4) . .
Ag3 Ag5 Ag6 O17 -178.9(4) 2_646 .
O12 Ag5 Ag6 O4 139.4(2) . 2_646
O6B Ag5 Ag6 O4 -42.9(10) 2_646 2_646
O6A Ag5 Ag6 O4 4.6(13) 2_646 2_646
O7B Ag5 Ag6 O4 -129.8(5) 2_646 2_646
O8A Ag5 Ag6 O4 -108.6(3) 2_646 2_646
O14 Ag5 Ag6 O4 73.5(2) . 2_646
Ag3 Ag5 Ag6 O4 -88.50(17) 2_646 2_646
O12 Ag5 Ag6 O13 -128.88(19) . 2_646
O6B Ag5 Ag6 O13 48.9(10) 2_646 2_646
O6A Ag5 Ag6 O13 96.3(13) 2_646 2_646
O7B Ag5 Ag6 O13 -38.1(5) 2_646 2_646
O8A Ag5 Ag6 O13 -16.9(3) 2_646 2_646
O14 Ag5 Ag6 O13 165.24(16) . 2_646
Ag3 Ag5 Ag6 O13 3.22(11) 2_646 2_646
O6B Ag5 Ag6 O12 177.7(10) 2_646 .
O6A Ag5 Ag6 O12 -134.8(13) 2_646 .
O7B Ag5 Ag6 O12 90.8(5) 2_646 .
O8A Ag5 Ag6 O12 112.0(3) 2_646 .
O14 Ag5 Ag6 O12 -65.87(18) . .
Ag3 Ag5 Ag6 O12 132.10(15) 2_646 .
O10A Ag2 Ag8 O1 172.3(4) . 3_677
O2 Ag2 Ag8 O1 -10.2(2) 3_677 3_677
O10B Ag2 Ag8 O1 148.9(6) . 3_677
O17 Ag2 Ag8 O1 -88.8(7) . 3_677
Ag7 Ag2 Ag8 O1 -90.74(16) 3_667 3_677
O10A Ag2 Ag8 O9A 18.6(4) . .
O2 Ag2 Ag8 O9A -164.0(2) 3_677 .
O10B Ag2 Ag8 O9A -4.9(6) . .
O17 Ag2 Ag8 O9A 117.5(8) . .
Ag7 Ag2 Ag8 O9A 115.47(19) 3_667 .
O10A Ag2 Ag8 O9B 5.7(8) . .
O2 Ag2 Ag8 O9B -176.9(7) 3_677 .
O10B Ag2 Ag8 O9B -17.8(9) . .
O17 Ag2 Ag8 O9B 104.6(10) . .
Ag7 Ag2 Ag8 O9B 102.6(7) 3_667 .
O10A Ag2 Ag8 O6A 93.4(5) . 3_677
O2 Ag2 Ag8 O6A -89.2(5) 3_677 3_677
O10B Ag2 Ag8 O6A 69.9(7) . 3_677
O17 Ag2 Ag8 O6A -167.7(9) . 3_677
Ag7 Ag2 Ag8 O6A -169.7(5) 3_667 3_677
O10A Ag2 Ag8 Ag1 71.5(3) . .
O2 Ag2 Ag8 Ag1 -111.01(14) 3_677 .
O10B Ag2 Ag8 Ag1 48.1(6) . .
O17 Ag2 Ag8 Ag1 170.5(7) . .
Ag7 Ag2 Ag8 Ag1 168.47(2) 3_667 .
O5B Ag1 Ag8 O1 111.9(5) 3_677 3_677
O6B Ag1 Ag8 O1 -29.8(6) . 3_677
O5A Ag1 Ag8 O1 -26.8(2) . 3_677
O3 Ag1 Ag8 O1 -137.9(2) . 3_677
O9A Ag1 Ag8 O1 -160.8(3) . 3_677
O5A Ag1 Ag8 O1 83.4(2) 3_677 3_677
Ag1 Ag1 Ag8 O1 31.47(12) 3_677 3_677
O5B Ag1 Ag8 O9A -87.2(6) 3_677 .
O6B Ag1 Ag8 O9A 131.0(7) . .
O5A Ag1 Ag8 O9A 134.0(4) . .
O3 Ag1 Ag8 O9A 22.9(4) . .
O5A Ag1 Ag8 O9A -115.7(4) 3_677 .
Ag1 Ag1 Ag8 O9A -167.7(3) 3_677 .
O5B Ag1 Ag8 O9B -86.6(9) 3_677 .
O6B Ag1 Ag8 O9B 131.6(9) . .
O5A Ag1 Ag8 O9B 134.6(8) . .
O3 Ag1 Ag8 O9B 23.5(8) . .
O9A Ag1 Ag8 O9B 0.6(10) . .
O5A Ag1 Ag8 O9B -115.1(8) 3_677 .
Ag1 Ag1 Ag8 O9B -167.1(7) 3_677 .
O5B Ag1 Ag8 O6A 16.3(6) 3_677 3_677
O6B Ag1 Ag8 O6A -125.5(6) . 3_677
O5A Ag1 Ag8 O6A -122.5(3) . 3_677
O3 Ag1 Ag8 O6A 126.4(3) . 3_677
O9A Ag1 Ag8 O6A 103.5(4) . 3_677
O5A Ag1 Ag8 O6A -12.2(3) 3_677 3_677
Ag1 Ag1 Ag8 O6A -64.2(2) 3_677 3_677
O5B Ag1 Ag8 Ag2 -173.5(5) 3_677 .
O6B Ag1 Ag8 Ag2 44.8(6) . .
O5A Ag1 Ag8 Ag2 47.7(2) . .
O3 Ag1 Ag8 Ag2 -63.32(19) . .
O9A Ag1 Ag8 Ag2 -86.2(3) . .
O5A Ag1 Ag8 Ag2 158.03(19) 3_677 .
Ag1 Ag1 Ag8 Ag2 106.05(3) 3_677 .
O5B Ag1 O3 C8 -47.4(9) 3_677 .
O6B Ag1 O3 C8 98.4(8) . .
O5A Ag1 O3 C8 125.6(6) . .
O9A Ag1 O3 C8 -123.1(7) . .
O5A Ag1 O3 C8 -20.4(8) 3_677 .
Ag1 Ag1 O3 C8 65.4(7) 3_677 .
Ag8 Ag1 O3 C8 -139.3(5) . .
O5B Ag1 O3 Ag3 146.5(6) 3_677 .
O6B Ag1 O3 Ag3 -67.7(6) . .
O5A Ag1 O3 Ag3 -40.5(4) . .
O9A Ag1 O3 Ag3 70.8(4) . .
O5A Ag1 O3 Ag3 173.5(3) 3_677 .
Ag1 Ag1 O3 Ag3 -100.7(4) 3_677 .
Ag8 Ag1 O3 Ag3 54.6(4) . .
O8A Ag3 O3 C8 -119.8(8) . .
O13 Ag3 O3 C8 11.9(7) . .
O7B Ag3 O3 C8 -96.7(8) . .
O12 Ag3 O3 C8 123.1(7) . .
O8B Ag3 O3 C8 -140.9(8) . .
Ag4 Ag3 O3 C8 -58.0(8) . .
Ag5 Ag3 O3 C8 -74.7(7) 2_656 .
O8A Ag3 O3 Ag1 44.7(4) . .
O13 Ag3 O3 Ag1 176.5(3) . .
O7B Ag3 O3 Ag1 67.9(5) . .
O12 Ag3 O3 Ag1 -72.3(4) . .
O8B Ag3 O3 Ag1 23.7(5) . .
Ag4 Ag3 O3 Ag1 106.6(3) . .
Ag5 Ag3 O3 Ag1 89.9(3) 2_656 .
O5B Ag1 O5A C9 127.2(10) 3_677 .
O6B Ag1 O5A C9 -2.1(9) . .
O3 Ag1 O5A C9 -44.7(7) . .
O9A Ag1 O5A C9 -145.2(6) . .
O5A Ag1 O5A C9 109.9(7) 3_677 .
Ag1 Ag1 O5A C9 109.9(7) 3_677 .
Ag8 Ag1 O5A C9 -178.2(7) . .
O5B Ag1 O5A Ag1 17.2(7) 3_677 3_677
O6B Ag1 O5A Ag1 -112.1(8) . 3_677
O3 Ag1 O5A Ag1 -154.63(19) . 3_677
O9A Ag1 O5A Ag1 104.9(2) . 3_677
O5A Ag1 O5A Ag1 0.0 3_677 3_677
Ag8 Ag1 O5A Ag1 71.84(11) . 3_677
O14 Ag4 O7A C16 70.7(8) . .
O18A Ag4 O7A C16 -121.6(13) . .
O18B Ag4 O7A C16 -113.9(10) . .
O7B Ag4 O7A C16 -8.4(9) . .
Ag3 Ag4 O7A C16 36.3(7) . .
O13 Ag3 O8A C16 86.1(10) . .
O7B Ag3 O8A C16 52.9(10) . .
O12 Ag3 O8A C16 -47.5(11) . .
O3 Ag3 O8A C16 179.3(10) . .
O8B Ag3 O8A C16 -63.3(10) . .
Ag4 Ag3 O8A C16 29.8(9) . .
Ag5 Ag3 O8A C16 129.3(11) 2_656 .
O13 Ag3 O8A Ag5 -43.2(4) . 2_656
O7B Ag3 O8A Ag5 -76.3(10) . 2_656
O12 Ag3 O8A Ag5 -176.83(15) . 2_656
O3 Ag3 O8A Ag5 50.0(2) . 2_656
O8B Ag3 O8A Ag5 167.4(13) . 2_656
Ag4 Ag3 O8A Ag5 -99.5(2) . 2_656
O1 Ag8 O9A C17 -74.9(8) 3_677 .
O9B Ag8 O9A C17 74(4) . .
O6A Ag8 O9A C17 177.8(7) 3_677 .
Ag2 Ag8 O9A C17 -27.9(7) . .
Ag1 Ag8 O9A C17 -108.6(8) . .
O1 Ag8 O9A Ag1 33.7(5) 3_677 .
O9B Ag8 O9A Ag1 -178(4) . .
O6A Ag8 O9A Ag1 -73.6(3) 3_677 .
Ag2 Ag8 O9A Ag1 80.74(19) . .
O5B Ag1 O9A C17 -158.8(11) 3_677 .
O6B Ag1 O9A C17 36.8(14) . .
O5A Ag1 O9A C17 73.9(10) . .
O3 Ag1 O9A C17 -42.4(10) . .
O5A Ag1 O9A C17 -176.0(9) 3_677 .
Ag1 Ag1 O9A C17 133.9(9) 3_677 .
Ag8 Ag1 O9A C17 121.6(11) . .
O5B Ag1 O9A Ag8 79.6(4) 3_677 .
O6B Ag1 O9A Ag8 -84.7(6) . .
O5A Ag1 O9A Ag8 -47.7(3) . .
O3 Ag1 O9A Ag8 -164.0(2) . .
O5A Ag1 O9A Ag8 62.4(3) 3_677 .
Ag1 Ag1 O9A Ag8 12.3(3) 3_677 .
O2 Ag2 O10A C17 -33(2) 3_677 .
O10B Ag2 O10A C17 64.8(13) . .
O17 Ag2 O10A C17 167.7(10) . .
Ag8 Ag2 O10A C17 -22.3(10) . .
Ag7 Ag2 O10A C17 -91.3(10) 3_667 .
O5B Ag1 O6B C9 -93.3(17) 3_677 .
O5A Ag1 O6B C9 2.3(10) . .
O3 Ag1 O6B C9 143.8(16) . .
O9A Ag1 O6B C9 60.9(18) . .
O5A Ag1 O6B C9 -82.3(16) 3_677 .
Ag1 Ag1 O6B C9 -49.3(14) 3_677 .
Ag8 Ag1 O6B C9 6.7(18) . .
O5B Ag1 O6B Ag5 110.7(10) 3_677 2_656
O5A Ag1 O6B Ag5 -153.6(13) . 2_656
O3 Ag1 O6B Ag5 -12.2(6) . 2_656
O9A Ag1 O6B Ag5 -95.0(8) . 2_656
O5A Ag1 O6B Ag5 121.8(6) 3_677 2_656
Ag1 Ag1 O6B Ag5 154.7(8) 3_677 2_656
Ag8 Ag1 O6B Ag5 -149.3(5) . 2_656
O8A Ag3 O7B C16 -44.4(9) . .
O13 Ag3 O7B C16 160.7(10) . .
O12 Ag3 O7B C16 48.3(12) . .
O3 Ag3 O7B C16 -99.5(11) . .
O8B Ag3 O7B C16 -13.1(10) . .
Ag4 Ag3 O7B C16 106.7(11) . .
Ag5 Ag3 O7B C16 -123.7(13) 2_656 .
O8A Ag3 O7B O8B -31.3(8) . .
O13 Ag3 O7B O8B 173.9(8) . .
O12 Ag3 O7B O8B 61.4(9) . .
O3 Ag3 O7B O8B -86.4(8) . .
Ag4 Ag3 O7B O8B 119.8(9) . .
Ag5 Ag3 O7B O8B -110.6(9) 2_656 .
O8A Ag3 O7B Ag4 -151.1(11) . .
O13 Ag3 O7B Ag4 54.0(4) . .
O12 Ag3 O7B Ag4 -58.4(4) . .
O3 Ag3 O7B Ag4 153.8(3) . .
O8B Ag3 O7B Ag4 -119.8(9) . .
Ag5 Ag3 O7B Ag4 129.6(5) 2_656 .
O8A Ag3 O7B Ag5 79.3(9) . 2_656
O13 Ag3 O7B Ag5 -75.6(4) . 2_656
O12 Ag3 O7B Ag5 171.99(18) . 2_656
O3 Ag3 O7B Ag5 24.2(4) . 2_656
O8B Ag3 O7B Ag5 110.6(9) . 2_656
Ag4 Ag3 O7B Ag5 -129.6(5) . 2_656
O14 Ag4 O7B C16 -127.8(11) . .
O7A Ag4 O7B C16 7.7(8) . .
O18A Ag4 O7B C16 77.2(16) . .
O18B Ag4 O7B C16 92.0(13) . .
Ag3 Ag4 O7B C16 -109.1(14) . .
O14 Ag4 O7B O8B -80.4(10) . .
O7A Ag4 O7B O8B 55.0(9) . .
O18A Ag4 O7B O8B 124.5(13) . .
O18B Ag4 O7B O8B 139.3(11) . .
Ag3 Ag4 O7B O8B -61.8(10) . .
O14 Ag4 O7B Ag3 -18.6(5) . .
O7A Ag4 O7B Ag3 116.8(8) . .
O18A Ag4 O7B Ag3 -173.7(9) . .
O18B Ag4 O7B Ag3 -158.9(5) . .
O14 Ag4 O7B Ag5 53.1(11) . 2_656
O7A Ag4 O7B Ag5 -171.4(15) . 2_656
O18A Ag4 O7B Ag5 -101.9(13) . 2_656
O18B Ag4 O7B Ag5 -87.1(10) . 2_656
Ag3 Ag4 O7B Ag5 71.8(8) . 2_656
Ag3 O7B O8B C16 -162.4(13) . .
Ag4 O7B O8B C16 -96.2(12) . .
Ag5 O7B O8B C16 121.4(14) 2_656 .
C16 O7B O8B Ag3 162.4(13) . .
Ag4 O7B O8B Ag3 66.2(7) . .
Ag5 O7B O8B Ag3 -76.3(7) 2_656 .
O8A Ag3 O8B C16 51.1(9) . .
O13 Ag3 O8B C16 1(2) . .
O7B Ag3 O8B C16 13.0(10) . .
O12 Ag3 O8B C16 -114.5(13) . .
O3 Ag3 O8B C16 113.9(13) . .
Ag4 Ag3 O8B C16 -31.5(12) . .
Ag5 Ag3 O8B C16 61.2(12) 2_656 .
O8A Ag3 O8B O7B 38.1(9) . .
O13 Ag3 O8B O7B -12.0(15) . .
O12 Ag3 O8B O7B -127.5(8) . .
O3 Ag3 O8B O7B 100.9(8) . .
Ag4 Ag3 O8B O7B -44.6(7) . .
Ag5 Ag3 O8B O7B 48.2(7) 2_656 .
O1 Ag8 O9B C17 -25(4) 3_677 .
O9A Ag8 O9B C17 -69(3) . .
O6A Ag8 O9B C17 -147(2) 3_677 .
Ag2 Ag8 O9B C17 7(2) . .
Ag1 Ag8 O9B C17 -71.4(19) . .
O10A Ag2 O10B C17 -52.1(10) . .
O2 Ag2 O10B C17 93.3(18) 3_677 .
O17 Ag2 O10B C17 -134.2(15) . .
Ag8 Ag2 O10B C17 37.1(15) . .
Ag7 Ag2 O10B C17 -25.8(19) 3_667 .
O16 Ag7 O11 C24 -26.2(7) 4_576 .
O15 Ag7 O11 C24 142.1(7) 2_646 .
Ag7 Ag7 O11 C24 83.0(7) 3_667 .
Ag2 Ag7 O11 C24 -142.2(5) 3_667 .
O6B Ag5 O12 C24 -87.4(13) 2_646 .
O6A Ag5 O12 C24 -98.3(6) 2_646 .
O7B Ag5 O12 C24 -4.0(7) 2_646 .
O8A Ag5 O12 C24 -5.4(6) 2_646 .
O14 Ag5 O12 C24 -150.3(5) . .
Ag6 Ag5 O12 C24 89.9(5) . .
Ag3 Ag5 O12 C24 41.5(5) 2_646 .
O6B Ag5 O12 Ag3 78.6(12) 2_646 .
O6A Ag5 O12 Ag3 67.7(3) 2_646 .
O7B Ag5 O12 Ag3 161.9(5) 2_646 .
O8A Ag5 O12 Ag3 160.5(3) 2_646 .
O14 Ag5 O12 Ag3 15.7(2) . .
Ag6 Ag5 O12 Ag3 -104.1(2) . .
Ag3 Ag5 O12 Ag3 -152.50(16) 2_646 .
O6B Ag5 O12 Ag6 -177.3(12) 2_646 .
O6A Ag5 O12 Ag6 171.8(2) 2_646 .
O7B Ag5 O12 Ag6 -94.0(4) 2_646 .
O8A Ag5 O12 Ag6 -95.4(2) 2_646 .
O14 Ag5 O12 Ag6 119.82(15) . .
Ag3 Ag5 O12 Ag6 -48.40(12) 2_646 .
O8A Ag3 O12 C24 -90.8(6) . .
O13 Ag3 O12 C24 122.6(5) . .
O7B Ag3 O12 C24 -122.1(6) . .
O3 Ag3 O12 C24 14.0(6) . .
O8B Ag3 O12 C24 -84.5(6) . .
Ag4 Ag3 O12 C24 -165.4(5) . .
Ag5 Ag3 O12 C24 -99.6(6) 2_656 .
O8A Ag3 O12 Ag5 103.5(3) . .
O13 Ag3 O12 Ag5 -43.1(2) . .
O7B Ag3 O12 Ag5 72.3(5) . .
O3 Ag3 O12 Ag5 -151.7(2) . .
O8B Ag3 O12 Ag5 109.8(4) . .
Ag4 Ag3 O12 Ag5 28.97(19) . .
Ag5 Ag3 O12 Ag5 94.7(4) 2_656 .
O8A Ag3 O12 Ag6 14.9(3) . .
O13 Ag3 O12 Ag6 -131.73(18) . .
O7B Ag3 O12 Ag6 -16.4(4) . .
O3 Ag3 O12 Ag6 119.7(2) . .
O8B Ag3 O12 Ag6 21.2(4) . .
Ag4 Ag3 O12 Ag6 -59.69(13) . .
Ag5 Ag3 O12 Ag6 6.1(5) 2_656 .
O17 Ag6 O12 C24 74.8(4) . .
O4 Ag6 O12 C24 -152.1(4) 2_646 .
O13 Ag6 O12 C24 -59.4(4) 2_646 .
Ag5 Ag6 O12 C24 -120.2(4) . .
O17 Ag6 O12 Ag5 -165.09(17) . .
O4 Ag6 O12 Ag5 -31.98(18) 2_646 .
O13 Ag6 O12 Ag5 60.76(18) 2_646 .
O17 Ag6 O12 Ag3 -50.8(2) . .
O4 Ag6 O12 Ag3 82.3(2) 2_646 .
O13 Ag6 O12 Ag3 175.07(14) 2_646 .
Ag5 Ag6 O12 Ag3 114.3(2) . .
O8A Ag3 O13 C25 -108.1(5) . .
O7B Ag3 O13 C25 -92.3(6) . .
O12 Ag3 O13 C25 29.1(5) . .
O3 Ag3 O13 C25 163.4(5) . .
O8B Ag3 O13 C25 -83.7(11) . .
Ag4 Ag3 O13 C25 -50.1(4) . .
Ag5 Ag3 O13 C25 -140.1(4) 2_656 .
O8A Ag3 O13 Ag6 36.4(4) . 2_656
O7B Ag3 O13 Ag6 52.2(4) . 2_656
O12 Ag3 O13 Ag6 173.65(17) . 2_656
O3 Ag3 O13 Ag6 -52.1(2) . 2_656
O8B Ag3 O13 Ag6 60.9(11) . 2_656
Ag4 Ag3 O13 Ag6 94.48(16) . 2_656
Ag5 Ag3 O13 Ag6 4.45(16) 2_656 2_656
O7A Ag4 O14 C25 -82.5(5) . .
O18A Ag4 O14 C25 113.9(15) . .
O18B Ag4 O14 C25 102.6(9) . .
O7B Ag4 O14 C25 -32.7(6) . .
Ag3 Ag4 O14 C25 -47.5(4) . .
O7A Ag4 O14 Ag5 52.4(4) . .
O18A Ag4 O14 Ag5 -111.1(14) . .
O18B Ag4 O14 Ag5 -122.4(8) . .
O7B Ag4 O14 Ag5 102.2(5) . .
Ag3 Ag4 O14 Ag5 87.43(10) . .
O12 Ag5 O14 C25 51.9(6) . .
O6B Ag5 O14 C25 -107.5(7) 2_646 .
O6A Ag5 O14 C25 -90.8(6) 2_646 .
O7B Ag5 O14 C25 -37.1(9) 2_646 .
O8A Ag5 O14 C25 -79.5(7) 2_646 .
Ag6 Ag5 O14 C25 97.5(5) . .
Ag3 Ag5 O14 C25 -169.0(4) 2_646 .
O12 Ag5 O14 Ag4 -75.02(17) . .
O6B Ag5 O14 Ag4 125.5(4) 2_646 .
O6A Ag5 O14 Ag4 142.2(3) 2_646 .
O7B Ag5 O14 Ag4 -164.1(7) 2_646 .
O8A Ag5 O14 Ag4 153.5(3) 2_646 .
Ag6 Ag5 O14 Ag4 -29.47(14) . .
Ag3 Ag5 O14 Ag4 64.0(4) 2_646 .
O4 Ag6 O17 C33 40.2(9) 2_646 .
O13 Ag6 O17 C33 -63.5(9) 2_646 .
O12 Ag6 O17 C33 158.7(8) . .
Ag5 Ag6 O17 C33 118.7(8) . .
O4 Ag6 O17 Ag2 -134.4(2) 2_646 .
O13 Ag6 O17 Ag2 121.9(2) 2_646 .
O12 Ag6 O17 Ag2 -15.9(3) . .
Ag5 Ag6 O17 Ag2 -55.8(5) . .
O10A Ag2 O17 C33 176.7(6) . .
O2 Ag2 O17 C33 1.7(5) 3_677 .
O10B Ag2 O17 C33 -159.9(7) . .
Ag8 Ag2 O17 C33 79.5(9) . .
Ag7 Ag2 O17 C33 81.4(5) 3_667 .
O10A Ag2 O17 Ag6 -6.9(4) . .
O2 Ag2 O17 Ag6 178.0(2) 3_677 .
O10B Ag2 O17 Ag6 16.4(6) . .
Ag8 Ag2 O17 Ag6 -104.2(7) . .
Ag7 Ag2 O17 Ag6 -102.3(2) 3_667 .
Ag2 O2 C1 O1 20.6(10) 3_677 .
Ag2 O2 C1 C2 -156.9(5) 3_677 .
Ag8 O1 C1 O2 -5.7(11) 3_677 .
Ag8 O1 C1 C2 172.0(4) 3_677 .
O2 C1 C2 C3 2.8(10) . .
O1 C1 C2 C3 -175.1(6) . .
O2 C1 C2 C7 -178.7(6) . .
O1 C1 C2 C7 3.5(9) . .
C7 C2 C3 F1 179.6(6) . .
C1 C2 C3 F1 -1.8(11) . .
C7 C2 C3 C4 -0.6(11) . .
C1 C2 C3 C4 178.0(7) . .
F1 C3 C4 C5 178.8(8) . .
C2 C3 C4 C5 -1.0(13) . .
F1 C3 C4 F2 -1.2(12) . .
C2 C3 C4 F2 179.0(7) . .
C3 C4 C5 F3 -178.7(8) . .
F2 C4 C5 F3 1.3(14) . .
C3 C4 C5 C6 1.5(14) . .
F2 C4 C5 C6 -178.5(8) . .
F3 C5 C6 F4 0.5(12) . .
C4 C5 C6 F4 -179.7(7) . .
F3 C5 C6 C7 179.8(7) . .
C4 C5 C6 C7 -0.4(13) . .
F4 C6 C7 C2 178.1(6) . .
C5 C6 C7 C2 -1.2(11) . .
F4 C6 C7 C8 -1.8(10) . .
C5 C6 C7 C8 178.9(7) . .
C3 C2 C7 C6 1.6(9) . .
C1 C2 C7 C6 -177.0(6) . .
C3 C2 C7 C8 -178.5(6) . .
C1 C2 C7 C8 2.9(10) . .
Ag6 O4 C8 O3 -47.8(11) 2_656 .
Ag6 O4 C8 C7 128.1(6) 2_656 .
Ag1 O3 C8 O4 -120.2(7) . .
Ag3 O3 C8 O4 43.9(11) . .
Ag1 O3 C8 C7 63.9(8) . .
Ag3 O3 C8 C7 -132.0(6) . .
C6 C7 C8 O4 -91.4(8) . .
C2 C7 C8 O4 88.7(8) . .
C6 C7 C8 O3 84.9(8) . .
C2 C7 C8 O3 -95.0(8) . .
Ag1 O6B C9 O6A 149(2) . .
Ag5 O6B C9 O6A -58.5(14) 2_656 .
Ag1 O6B C9 O5A -2.9(13) . .
Ag5 O6B C9 O5A 149.1(15) 2_656 .
Ag1 O6B C9 O5B 44(2) . .
Ag5 O6B C9 O5B -164.0(14) 2_656 .
Ag1 O6B C9 C10 -134.2(12) . .
Ag5 O6B C9 C10 18(3) 2_656 .
Ag5 O6A C9 O6B 55.0(14) 2_656 .
Ag8 O6A C9 O6B -77.8(15) 3_677 .
Ag5 O6A C9 O5A 89.1(10) 2_656 .
Ag8 O6A C9 O5A -43.6(13) 3_677 .
Ag5 O6A C9 O5B 153.5(12) 2_656 .
Ag8 O6A C9 O5B 20.8(15) 3_677 .
Ag5 O6A C9 C10 -81.1(9) 2_656 .
Ag8 O6A C9 C10 146.2(6) 3_677 .
Ag1 O5A C9 O6B 2.7(12) . .
Ag1 O5A C9 O6B 85.0(11) 3_677 .
Ag1 O5A C9 O6A -21.4(12) . .
Ag1 O5A C9 O6A 60.9(12) 3_677 .
Ag1 O5A C9 O5B -122.7(13) . .
Ag1 O5A C9 O5B -40.4(11) 3_677 .
Ag1 O5A C9 C10 148.3(6) . .
Ag1 O5A C9 C10 -129.4(6) 3_677 .
Ag1 O5B C9 O6B -3(2) 3_677 .
Ag1 O5B C9 O6A -55(2) 3_677 .
Ag1 O5B C9 O5A 60.3(14) 3_677 .
Ag1 O5B C9 C10 176.1(13) 3_677 .
O6B C9 C10 C11 -142.2(19) . .
O6A C9 C10 C11 -91.7(10) . .
O5A C9 C10 C11 97.6(10) . .
O5B C9 C10 C11 39.5(13) . .
O6B C9 C10 C15 36(2) . .
O6A C9 C10 C15 86.2(10) . .
O5A C9 C10 C15 -84.5(10) . .
O5B C9 C10 C15 -142.6(12) . .
C15 C10 C11 C12 0.6(12) . .
C9 C10 C11 C12 178.6(8) . .
C15 C10 C11 F5 179.8(6) . .
C9 C10 C11 F5 -2.2(10) . .
F5 C11 C12 C13 -179.6(9) . .
C10 C11 C12 C13 -0.4(15) . .
F5 C11 C12 F6 0.7(14) . .
C10 C11 C12 F6 180.0(8) . .
C11 C12 C13 C14 0.0(17) . .
F6 C12 C13 C14 179.7(9) . .
C11 C12 C13 F7 -179.5(9) . .
F6 C12 C13 F7 0.2(16) . .
C12 C13 C14 F8 179.1(9) . .
F7 C13 C14 F8 -1.5(14) . .
C12 C13 C14 C15 0.2(15) . .
F7 C13 C14 C15 179.7(8) . .
C11 C10 C15 C14 -0.3(9) . .
C9 C10 C15 C14 -178.2(7) . .
C11 C10 C15 C16 175.8(7) . .
C9 C10 C15 C16 -2.0(10) . .
F8 C14 C15 C10 -178.8(7) . .
C13 C14 C15 C10 0.0(12) . .
F8 C14 C15 C16 4.9(11) . .
C13 C14 C15 C16 -176.3(8) . .
Ag3 O8A C16 O8B 73.7(16) . .
Ag5 O8A C16 O8B -177.4(19) 2_656 .
Ag3 O8A C16 O7B -60.5(12) . .
Ag5 O8A C16 O7B 48.4(13) 2_656 .
Ag3 O8A C16 O7A -11.2(16) . .
Ag5 O8A C16 O7A 97.7(10) 2_656 .
Ag3 O8A C16 C15 174.5(6) . .
Ag5 O8A C16 C15 -76.6(10) 2_656 .
O7B O8B C16 O8A -35.9(15) . .
Ag3 O8B C16 O8A -52.9(12) . .
Ag3 O8B C16 O7B -17.0(13) . .
O7B O8B C16 O7A 85.7(12) . .
Ag3 O8B C16 O7A 68.7(13) . .
O7B O8B C16 C15 -137.4(13) . .
Ag3 O8B C16 C15 -154.5(7) . .
O8B O7B C16 O8A 31.5(13) . .
Ag3 O7B C16 O8A 49.4(9) . .
Ag4 O7B C16 O8A 133.3(15) . .
Ag5 O7B C16 O8A -47.6(11) 2_656 .
Ag3 O7B C16 O8B 17.9(14) . .
Ag4 O7B C16 O8B 101.8(13) . .
Ag5 O7B C16 O8B -79.1(16) 2_656 .
O8B O7B C16 O7A -111.2(12) . .
Ag3 O7B C16 O7A -93.3(9) . .
Ag4 O7B C16 O7A -9.3(10) . .
Ag5 O7B C16 O7A 169.8(13) 2_656 .
O8B O7B C16 C15 124.3(18) . .
Ag3 O7B C16 C15 142.2(10) . .
Ag4 O7B C16 C15 -133.9(10) . .
Ag5 O7B C16 C15 45(2) 2_656 .
Ag4 O7A C16 O8A -27.4(14) . .
Ag4 O7A C16 O8B -78.5(15) . .
Ag4 O7A C16 O7B 11.1(12) . .
Ag4 O7A C16 C15 146.7(5) . .
C10 C15 C16 O8A -4.2(12) . .
C14 C15 C16 O8A 171.8(9) . .
C10 C15 C16 O8B 47.4(15) . .
C14 C15 C16 O8B -136.6(14) . .
C10 C15 C16 O7B -67.9(17) . .
C14 C15 C16 O7B 108.2(15) . .
C10 C15 C16 O7A -179.1(7) . .
C14 C15 C16 O7A -3.0(11) . .
Ag8 O9A C17 O9B -79(6) . .
Ag1 O9A C17 O9B -173(7) . .
Ag8 O9A C17 O10B 68.4(17) . .
Ag1 O9A C17 O10B -25.2(18) . .
Ag8 O9A C17 O10A 21.6(12) . .
Ag1 O9A C17 O10A -72.0(12) . .
Ag8 O9A C17 C18 -154.6(6) . .
Ag1 O9A C17 C18 111.7(8) . .
Ag8 O9B C17 O9A 70(5) . .
Ag8 O9B C17 O10B 29(4) . .
Ag8 O9B C17 O10A -26(3) . .
Ag8 O9B C17 C18 -172.9(11) . .
Ag2 O10B C17 O9A -68.9(17) . .
Ag2 O10B C17 O9B -52(3) . .
Ag2 O10B C17 O10A 48.5(14) . .
Ag2 O10B C17 C18 149.9(9) . .
Ag2 O10A C17 O9A 7.1(15) . .
Ag2 O10A C17 O9B 37(2) . .
Ag2 O10A C17 O10B -78(2) . .
Ag2 O10A C17 C18 -176.3(6) . .
O9A C17 C18 C23 177.2(7) . .
O9B C17 C18 C23 151.2(17) . .
O10B C17 C18 C23 -46.7(17) . .
O10A C17 C18 C23 0.6(11) . .
O9A C17 C18 C19 -0.8(11) . .
O9B C17 C18 C19 -26.8(19) . .
O10B C17 C18 C19 135.3(16) . .
O10A C17 C18 C19 -177.3(8) . .
C23 C18 C19 F9 178.4(6) . .
C17 C18 C19 F9 -3.6(10) . .
C23 C18 C19 C20 -2.1(10) . .
C17 C18 C19 C20 175.9(7) . .
F9 C19 C20 F10 -0.4(11) . .
C18 C19 C20 F10 -179.9(7) . .
F9 C19 C20 C21 -179.9(6) . .
C18 C19 C20 C21 0.6(11) . .
F10 C20 C21 F11 1.0(11) . .
C19 C20 C21 F11 -179.4(7) . .
F10 C20 C21 C22 -179.4(7) . .
C19 C20 C21 C22 0.1(11) . .
F11 C21 C22 F12 -1.1(10) . .
C20 C21 C22 F12 179.3(6) . .
F11 C21 C22 C23 -179.7(6) . .
C20 C21 C22 C23 0.8(11) . .
F12 C22 C23 C18 179.1(5) . .
C21 C22 C23 C18 -2.4(10) . .
F12 C22 C23 C24 -4.3(9) . .
C21 C22 C23 C24 174.2(6) . .
C19 C18 C23 C22 3.0(9) . .
C17 C18 C23 C22 -175.1(6) . .
C19 C18 C23 C24 -173.4(6) . .
C17 C18 C23 C24 8.6(9) . .
Ag7 O11 C24 O12 -143.3(6) . .
Ag7 O11 C24 C23 43.2(9) . .
Ag5 O12 C24 O11 -60.9(9) . .
Ag3 O12 C24 O11 134.1(7) . .
Ag6 O12 C24 O11 22.1(8) . .
Ag5 O12 C24 C23 112.8(5) . .
Ag3 O12 C24 C23 -52.1(8) . .
Ag6 O12 C24 C23 -164.2(5) . .
C22 C23 C24 O11 90.1(8) . .
C18 C23 C24 O11 -93.5(9) . .
C22 C23 C24 O12 -84.0(8) . .
C18 C23 C24 O12 92.5(8) . .
Ag3 O13 C25 O14 31.1(8) . .
Ag6 O13 C25 O14 -105.6(7) 2_656 .
Ag3 O13 C25 C26 -141.9(4) . .
Ag6 O13 C25 C26 81.3(6) 2_656 .
Ag4 O14 C25 O13 24.0(8) . .
Ag5 O14 C25 O13 -91.1(8) . .
Ag4 O14 C25 C26 -163.2(4) . .
Ag5 O14 C25 C26 81.6(6) . .
O13 C25 C26 C27 77.4(8) . .
O14 C25 C26 C27 -96.1(7) . .
O13 C25 C26 C31 -98.6(7) . .
O14 C25 C26 C31 87.9(8) . .
C31 C26 C27 F13 179.2(6) . .
C25 C26 C27 F13 3.0(10) . .
C31 C26 C27 C28 -0.7(11) . .
C25 C26 C27 C28 -176.9(7) . .
F13 C27 C28 F14 0.5(12) . .
C26 C27 C28 F14 -179.6(7) . .
F13 C27 C28 C29 -179.3(7) . .
C26 C27 C28 C29 0.7(13) . .
F14 C28 C29 F15 0.6(13) . .
C27 C28 C29 F15 -179.6(7) . .
F14 C28 C29 C30 -179.2(7) . .
C27 C28 C29 C30 0.5(13) . .
F15 C29 C30 F16 -0.2(11) . .
C28 C29 C30 F16 179.6(7) . .
F15 C29 C30 C31 178.5(7) . .
C28 C29 C30 C31 -1.7(12) . .
F16 C30 C31 C26 -179.8(6) . .
C29 C30 C31 C26 1.6(10) . .
F16 C30 C31 C32 2.0(10) . .
C29 C30 C31 C32 -176.6(7) . .
C27 C26 C31 C30 -0.4(9) . .
C25 C26 C31 C30 175.4(6) . .
C27 C26 C31 C32 177.8(6) . .
C25 C26 C31 C32 -6.4(9) . .
Ag7 O16 C32 O15 -12.2(10) 4_575 .
Ag7 O16 C32 C31 166.5(4) 4_575 .
Ag7 O15 C32 O16 -2.1(12) 2_656 .
Ag7 O15 C32 C31 179.1(5) 2_656 .
C30 C31 C32 O16 -12.5(10) . .
C26 C31 C32 O16 169.3(6) . .
C30 C31 C32 O15 166.4(6) . .
C26 C31 C32 O15 -11.8(9) . .
Ag6 O17 C33 N1 -0.7(14) . .
Ag2 O17 C33 N1 173.8(6) . .
C35 N1 C33 O17 -179.2(9) . .
C34 N1 C33 O17 3.0(13) . .
O14 Ag4 O18A C36A -46(8) . .
O7A Ag4 O18A C36A 144(8) . .
O18B Ag4 O18A C36A -6(2) . .
O7B Ag4 O18A C36A 105(8) . .
Ag3 Ag4 O18A C36A 95(8) . .
Ag4 O18A C36A N2 -168(7) . .
C37B N2 C36A O18A -179(2) . .
C38A N2 C36A O18A 7(3) . .
C37A N2 C36A O18A -180(2) . .
C38B N2 C36A O18A -7(8) . .
C36B N2 C36A O18A 1(2) . .
O14 Ag4 O18B C36B 151.2(12) . .
O7A Ag4 O18B C36B -25.6(16) . .
O18A Ag4 O18B C36B 5(6) . .
O7B Ag4 O18B C36B -68.1(16) . .
Ag3 Ag4 O18B C36B -101.7(14) . .
Ag4 O18B C36B N2 177.1(8) . .
C37B N2 C36B O18B 2(2) . .
C38A N2 C36B O18B -172(2) . .
C37A N2 C36B O18B -3(8) . .
C38B N2 C36B O18B -179.9(17) . .
C36A N2 C36B O18B 1.5(17) . .
