#------------------------------------------------------------------------------
#$Date: 2016-03-26 12:56:19 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180217 $
#$URL: svn://www.crystallography.net/cod/cif/7/11/03/7110360.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided the Crystal Eye server at
# http://wwmm.ch.cam.ac.uk/crystaleye/, created by Nick Day at the
# Peter Murray-Rust laboratory.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_7110360
loop_
_publ_author_name
'McBurnett, Brian G.'
'Cowley, Alan H.'
_publ_section_title
;
 Binuclear tin and germanium calix[4]arenes
;
_journal_issue                   1
_journal_name_full               'Chemical Communications'
_journal_page_first              17
_journal_paper_doi               10.1039/a807167e
_journal_year                    1999
_chemical_formula_sum            'C46 H56 Cl4 O4 Sn2'
_chemical_formula_weight         1052.09
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL
_cell_angle_alpha                91.720(10)
_cell_angle_beta                 109.350(10)
_cell_angle_gamma                111.120(10)
_cell_formula_units_Z            2
_cell_length_a                   12.903(2)
_cell_length_b                   14.1920(10)
_cell_length_c                   14.236(2)
_cell_measurement_reflns_used    67
_cell_measurement_temperature    163(2)
_cell_measurement_theta_max      12.52
_cell_measurement_theta_min      4.74
_cell_volume                     2261.1(6)
_computing_cell_refinement       'Siemens XSCANS'
_computing_data_collection       'Siemens XSCANS'
_computing_data_reduction        'Siemens SHELXTL'
_computing_molecular_graphics    'Siemens SHELXTL'
_computing_publication_material  'Siemens SHELXTL'
_computing_structure_refinement  'SHELXL-93 (Sheldrick, 1993)'
_computing_structure_solution    'SHELXS-86 (Sheldrick, 1990)'
_diffrn_ambient_temperature      163(2)
_diffrn_measurement_device       'Siemens P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0546
_diffrn_reflns_av_sigmaI/netI    0.0498
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -1
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            10707
_diffrn_reflns_theta_max         27.50
_diffrn_reflns_theta_min         1.54
_diffrn_standards_decay_%        0.00
_diffrn_standards_interval_count 97
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    1.382
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.545
_exptl_crystal_description       parellelipiped
_exptl_crystal_F_000             1064
_exptl_crystal_size_max          0.50
_exptl_crystal_size_mid          0.24
_exptl_crystal_size_min          0.24
_refine_diff_density_max         0.904
_refine_diff_density_min         -1.211
_refine_diff_density_rms         0.185
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_all   0.964
_refine_ls_goodness_of_fit_obs   1.001
_refine_ls_matrix_type           full
_refine_ls_number_parameters     513
_refine_ls_number_reflns         8997
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.964
_refine_ls_restrained_S_obs      1.001
_refine_ls_R_factor_all          0.0466
_refine_ls_R_factor_obs          0.0351
_refine_ls_shift/esd_max         0.007
_refine_ls_shift/esd_mean        0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0637P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.0983
_refine_ls_wR_factor_obs         0.0908
_reflns_number_observed          7217
_reflns_number_total             8997
_reflns_observed_criterion       >2sigma(I)
_cod_data_source_file            807167Esup1.cif
_cod_data_source_block           bmcb13
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 

The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'calc
w=1/[\s^2^(Fo^2^)+(0.0637P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to
'w=1/[\s^2^(Fo^2^)+(0.0637P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        2261.1(5)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7110360
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_thermal_displace_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
Sn1 Sn 0.48059(2) 0.60134(2) 0.43163(2) 0.01869(7) Uani 1 d .
Sn2 Sn 0.43176(2) 0.88055(2) 0.53580(2) 0.01896(7) Uani 1 d .
O1 O 0.4861(2) 0.4488(2) 0.4228(2) 0.0172(5) Uani 1 d .
O2 O 0.6625(2) 0.6573(2) 0.4700(2) 0.0211(5) Uani 1 d .
O3 O 0.5729(2) 1.0299(2) 0.5850(2) 0.0182(5) Uani 1 d .
O4 O 0.4573(2) 1.1686(2) 0.5104(2) 0.0204(5) Uani 1 d .
Cl1 Cl 0.36328(9) 1.27892(8) 0.76705(8) 0.0356(2) Uani 1 d .
Cl2 Cl 0.10627(10) 1.20043(12) 0.71789(11) 0.0537(3) Uani 1 d .
Cl3 Cl 0.6824(2) 1.4418(2) 0.8786(2) 0.0810(5) Uani 1 d .
Cl4 Cl 0.67720(13) 1.54617(12) 1.05379(12) 0.0650(4) Uani 1 d .
C1 C 0.7373(3) 0.5246(3) 0.4760(3) 0.0196(7) Uani 1 d .
C2 C 0.6878(3) 0.4983(3) 0.3616(3) 0.0228(7) Uani 1 d .
H2A H 0.7488(3) 0.4862(3) 0.3411(3) 0.044(14) Uiso 1 calc R
H2B H 0.6786(3) 0.5595(3) 0.3346(3) 0.016(9) Uiso 1 calc R
C3 C 0.5694(3) 0.4067(3) 0.3095(3) 0.0190(7) Uani 1 d .
C4 C 0.5544(3) 0.3418(3) 0.2268(3) 0.0221(7) Uani 1 d .
H4B H 0.6205(3) 0.3528(3) 0.2067(3) 0.026 Uiso 1 calc R
C5 C 0.4457(3) 0.2609(2) 0.1721(3) 0.0212(7) Uani 1 d .
C6 C 0.3495(3) 0.2487(3) 0.2029(3) 0.0206(7) Uani 1 d .
H6A H 0.2742(3) 0.1951(3) 0.1659(3) 0.025 Uiso 1 calc R
C7 C 0.3592(3) 0.3112(2) 0.2850(3) 0.0182(7) Uani 1 d .
C8 C 0.7484(3) 0.7099(2) 0.6832(3) 0.0214(7) Uani 1 d .
H8A H 0.7474(3) 0.7611(2) 0.6376(3) 0.046(14) Uiso 1 calc R
H8B H 0.8210(3) 0.7433(2) 0.7446(3) 0.046(14) Uiso 1 calc R
C9 C 0.7643(3) 0.6243(2) 0.6319(3) 0.0184(7) Uani 1 d .
C10 C 0.8283(3) 0.5698(2) 0.6867(3) 0.0202(7) Uani 1 d .
H10A H 0.8583(3) 0.5846(2) 0.7584(3) 0.024 Uiso 1 calc R
C11 C 0.8497(3) 0.4949(3) 0.6403(3) 0.0223(7) Uani 1 d .
C12 C 0.8020(3) 0.4728(3) 0.5344(3) 0.0229(7) Uani 1 d .
H12A H 0.8141(3) 0.4208(3) 0.5013(3) 0.027 Uiso 1 calc R
C13 C 0.4711(3) 0.3893(2) 0.3393(3) 0.0171(6) Uani 1 d .
C14 C 0.7223(3) 0.6038(2) 0.5256(3) 0.0184(7) Uani 1 d .
C15 C 0.4316(3) 0.1870(3) 0.0839(3) 0.0262(8) Uani 1 d .
C16 C 0.5334(4) 0.2276(4) 0.0436(4) 0.0415(11) Uani 1 d .
H16A H 0.5195(4) 0.1771(4) -0.0125(4) 0.062 Uiso 1 calc R
H16B H 0.6096(4) 0.2393(4) 0.0977(4) 0.062 Uiso 1 calc R
H16C H 0.5360(4) 0.2922(4) 0.0198(4) 0.062 Uiso 1 calc R
C17 C 0.4288(4) 0.0859(3) 0.1205(4) 0.0394(10) Uani 1 d .
H17A H 0.4198(4) 0.0373(3) 0.0651(4) 0.059 Uiso 1 calc R
H17B H 0.3613(4) 0.0572(3) 0.1428(4) 0.059 Uiso 1 calc R
H17C H 0.5034(4) 0.0986(3) 0.1771(4) 0.059 Uiso 1 calc R
C18 C 0.3151(4) 0.1652(4) -0.0052(3) 0.0405(10) Uani 1 d .
H18A H 0.3084(4) 0.1178(4) -0.0605(3) 0.061 Uiso 1 calc R
H18B H 0.3151(4) 0.2295(4) -0.0285(3) 0.061 Uiso 1 calc R
H18C H 0.2472(4) 0.1345(4) 0.0162(3) 0.061 Uiso 1 calc R
C19 C 0.9237(3) 0.4376(3) 0.6990(3) 0.0278(8) Uani 1 d .
C20 C 1.0352(4) 0.4623(4) 0.6737(5) 0.053(2) Uani 1 d .
H20A H 1.0824(4) 0.5363(4) 0.6911(5) 0.079 Uiso 1 calc R
H20B H 1.0121(4) 0.4400(4) 0.6013(5) 0.079 Uiso 1 calc R
H20C H 1.0830(4) 0.4264(4) 0.7123(5) 0.079 Uiso 1 calc R
C21 C 0.9620(6) 0.4662(5) 0.8143(4) 0.064(2) Uani 1 d .
H21A H 0.8909(6) 0.4507(5) 0.8318(4) 0.096 Uiso 1 calc R
H21B H 1.0123(6) 0.5395(5) 0.8356(4) 0.096 Uiso 1 calc R
H21C H 1.0072(6) 0.4266(5) 0.8488(4) 0.096 Uiso 1 calc R
C22 C 0.8507(4) 0.3219(3) 0.6715(4) 0.0459(13) Uani 1 d .
H22A H 0.7786(4) 0.3054(3) 0.6876(4) 0.069 Uiso 1 calc R
H22B H 0.8988(4) 0.2862(3) 0.7101(4) 0.069 Uiso 1 calc R
H22C H 0.8279(4) 0.2999(3) 0.5991(4) 0.069 Uiso 1 calc R
C23 C 0.7673(3) 0.9655(3) 0.6399(3) 0.0214(7) Uani 1 d .
H23A H 0.7174(3) 0.8962(3) 0.6466(3) 0.024(10) Uiso 1 calc R
H23B H 0.8512(3) 0.9716(3) 0.6657(3) 0.038(13) Uiso 1 calc R
C24 C 0.7575(3) 1.0425(2) 0.7082(2) 0.0178(7) Uani 1 d .
C25 C 0.8440(3) 1.0849(3) 0.8050(3) 0.0208(7) Uani 1 d .
H25A H 0.9136(3) 1.0700(3) 0.8243(3) 0.025 Uiso 1 calc R
C26 C 0.8327(3) 1.1477(2) 0.8740(3) 0.0204(7) Uani 1 d .
C27 C 0.7294(3) 1.1679(2) 0.8448(3) 0.0194(7) Uani 1 d .
H27A H 0.7192(3) 1.2095(2) 0.8917(3) 0.023 Uiso 1 calc R
C28 C 0.6399(3) 1.1286(2) 0.7479(2) 0.0164(6) Uani 1 d .
C29 C 0.5332(3) 1.1596(3) 0.7219(3) 0.0213(7) Uani 1 d .
H29A H 0.5216(3) 1.1727(3) 0.7857(3) 0.034(12) Uiso 1 calc R
H29B H 0.5555(3) 1.2256(3) 0.6970(3) 0.029(11) Uiso 1 calc R
C30 C 0.4126(3) 1.0867(2) 0.6452(3) 0.0174(6) Uani 1 d .
C31 C 0.3319(3) 1.0122(3) 0.6765(3) 0.0211(7) Uani 1 d .
H31A H 0.3538(3) 1.0067(3) 0.7461(3) 0.025 Uiso 1 calc R
C32 C 0.2200(3) 0.9453(3) 0.6090(3) 0.0222(7) Uani 1 d .
C33 C 0.1911(3) 0.9546(3) 0.5078(3) 0.0206(7) Uani 1 d .
H33A H 0.1159(3) 0.9089(3) 0.4606(3) 0.025 Uiso 1 calc R
C34 C 0.2681(3) 1.0283(3) 0.4726(3) 0.0188(7) Uani 1 d .
C35 C 0.6572(3) 1.0681(2) 0.6822(2) 0.0164(6) Uani 1 d .
C36 C 0.3792(3) 1.0968(2) 0.5432(3) 0.0178(7) Uani 1 d .
C37 C 0.9302(3) 1.1908(3) 0.9803(3) 0.0260(8) Uani 1 d .
C38 C 0.9066(5) 1.2640(4) 1.0403(4) 0.0542(15) Uani 1 d .
H38A H 0.9027(5) 1.3213(4) 1.0044(4) 0.081 Uiso 1 calc R
H38B H 0.9711(5) 1.2902(4) 1.1067(4) 0.081 Uiso 1 calc R
H38C H 0.8304(5) 1.2284(4) 1.0488(4) 0.081 Uiso 1 calc R
C39 C 1.0527(4) 1.2465(4) 0.9712(4) 0.054(2) Uani 1 d .
H39A H 1.0688(4) 1.1991(4) 0.9321(4) 0.081 Uiso 1 calc R
H39B H 1.1151(4) 1.2706(4) 1.0388(4) 0.081 Uiso 1 calc R
H39C H 1.0518(4) 1.3052(4) 0.9368(4) 0.081 Uiso 1 calc R
C40 C 0.9362(5) 1.1019(4) 1.0362(3) 0.0469(13) Uani 1 d .
H40A H 0.9516(5) 1.0540(4) 0.9972(3) 0.070 Uiso 1 calc R
H40B H 0.8600(5) 1.0664(4) 1.0448(3) 0.070 Uiso 1 calc R
H40C H 1.0007(5) 1.1283(4) 1.1027(3) 0.070 Uiso 1 calc R
C41 C 0.1312(3) 0.8638(3) 0.6450(3) 0.0334(9) Uani 1 d .
C42 C 0.1838(8) 0.8454(10) 0.7455(7) 0.190(8) Uani 1 d .
H42A H 0.2496(8) 0.8248(10) 0.7489(7) 0.285 Uiso 1 calc R
H42B H 0.1231(8) 0.7907(10) 0.7617(7) 0.285 Uiso 1 calc R
H42C H 0.2144(8) 0.9083(10) 0.7943(7) 0.285 Uiso 1 calc R
C43 C 0.0794(8) 0.7606(5) 0.5765(6) 0.102(3) Uani 1 d .
H43A H 0.0419(8) 0.7677(5) 0.5064(6) 0.153 Uiso 1 calc R
H43B H 0.0195(8) 0.7105(5) 0.5973(6) 0.153 Uiso 1 calc R
H43C H 0.1435(8) 0.7371(5) 0.5816(6) 0.153 Uiso 1 calc R
C44 C 0.0330(10) 0.8946(7) 0.6383(13) 0.228(10) Uani 1 d .
H44A H -0.0018(10) 0.9068(7) 0.5697(13) 0.341 Uiso 1 calc R
H44B H 0.0630(10) 0.9577(7) 0.6866(13) 0.341 Uiso 1 calc R
H44D H -0.0282(10) 0.8401(7) 0.6540(13) 0.341 Uiso 1 calc R
C45 C 0.2214(3) 1.2116(3) 0.6721(3) 0.0288(8) Uani 1 d .
H45A H 0.2144(3) 1.1424(3) 0.6488(3) 0.035 Uiso 1 calc R
H45C H 0.2126(3) 1.2482(3) 0.6137(3) 0.035 Uiso 1 calc R
C46 C 0.6236(5) 1.5193(4) 0.9222(4) 0.0507(13) Uani 1 d .
H46C H 0.6444(5) 1.5845(4) 0.8956(4) 0.061 Uiso 1 calc R
H46A H 0.5354(5) 1.4845(4) 0.8962(4) 0.061 Uiso 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O2 Sn1 O1 85.78(9) . 2_666
O2 Sn1 O1 86.02(9) . .
O1 Sn1 O1 68.22(11) 2_666 .
O4 Sn2 O3 88.02(9) 2_676 .
O4 Sn2 O3 86.44(9) 2_676 2_676
O3 Sn2 O3 68.17(10) . 2_676
C13 O1 Sn1 121.5(2) . 2_666
C13 O1 Sn1 126.7(2) . .
Sn1 O1 Sn1 111.78(11) 2_666 .
C14 O2 Sn1 117.7(2) . .
C35 O3 Sn2 125.5(2) . .
C35 O3 Sn2 122.7(2) . 2_676
Sn2 O3 Sn2 111.83(9) . 2_676
C36 O4 Sn2 115.4(2) . 2_676
C12 C1 C14 118.6(3) . .
C12 C1 C2 120.3(3) . .
C14 C1 C2 121.0(3) . .
C1 C2 C3 118.7(3) . .
C4 C3 C13 118.3(3) . .
C4 C3 C2 120.0(3) . .
C13 C3 C2 121.6(3) . .
C3 C4 C5 122.5(3) . .
C4 C5 C6 117.0(3) . .
C4 C5 C15 122.0(3) . .
C6 C5 C15 121.0(3) . .
C7 C6 C5 123.1(3) . .
C6 C7 C13 117.7(3) . .
C6 C7 C8 120.0(3) . 2_666
C13 C7 C8 122.2(3) . 2_666
C9 C8 C7 121.1(3) . 2_666
C10 C9 C14 118.5(3) . .
C10 C9 C8 122.0(3) . .
C14 C9 C8 119.3(3) . .
C11 C10 C9 122.6(3) . .
C10 C11 C12 117.6(3) . .
C10 C11 C19 123.2(3) . .
C12 C11 C19 119.2(4) . .
C1 C12 C11 122.2(4) . .
O1 C13 C7 119.6(3) . .
O1 C13 C3 119.0(3) . .
C7 C13 C3 121.4(3) . .
O2 C14 C9 120.1(3) . .
O2 C14 C1 119.5(3) . .
C9 C14 C1 120.3(3) . .
C5 C15 C18 111.2(3) . .
C5 C15 C17 108.1(3) . .
C18 C15 C17 108.7(3) . .
C5 C15 C16 113.2(3) . .
C18 C15 C16 106.9(4) . .
C17 C15 C16 108.7(4) . .
C20 C19 C22 109.0(4) . .
C20 C19 C11 109.8(3) . .
C22 C19 C11 110.3(3) . .
C20 C19 C21 108.6(4) . .
C22 C19 C21 106.8(4) . .
C11 C19 C21 112.2(4) . .
C24 C23 C34 118.2(3) . 2_676
C25 C24 C35 116.7(3) . .
C25 C24 C23 120.8(3) . .
C35 C24 C23 122.2(3) . .
C26 C25 C24 122.8(3) . .
C25 C26 C27 117.8(3) . .
C25 C26 C37 120.4(3) . .
C27 C26 C37 121.8(4) . .
C26 C27 C28 122.0(4) . .
C35 C28 C27 117.5(3) . .
C35 C28 C29 124.7(3) . .
C27 C28 C29 117.8(3) . .
C30 C29 C28 119.2(3) . .
C31 C30 C36 119.0(3) . .
C31 C30 C29 120.4(3) . .
C36 C30 C29 120.5(3) . .
C30 C31 C32 122.2(3) . .
C33 C32 C31 117.5(3) . .
C33 C32 C41 120.9(3) . .
C31 C32 C41 121.6(3) . .
C32 C33 C34 122.6(3) . .
C33 C34 C36 118.5(3) . .
C33 C34 C23 120.6(3) . 2_676
C36 C34 C23 120.9(3) . 2_676
C28 C35 O3 119.5(3) . .
C28 C35 C24 123.2(3) . .
O3 C35 C24 117.4(3) . .
O4 C36 C30 120.1(3) . .
O4 C36 C34 119.7(3) . .
C30 C36 C34 120.1(3) . .
C38 C37 C40 109.3(4) . .
C38 C37 C26 112.2(3) . .
C40 C37 C26 108.8(3) . .
C38 C37 C39 109.0(4) . .
C40 C37 C39 107.9(4) . .
C26 C37 C39 109.6(3) . .
C42 C41 C44 110.4(9) . .
C42 C41 C43 105.3(7) . .
C44 C41 C43 108.0(8) . .
C42 C41 C32 114.2(4) . .
C44 C41 C32 108.6(4) . .
C43 C41 C32 110.1(4) . .
Cl1 C45 Cl2 110.9(2) . .
Cl4 C46 Cl3 112.1(3) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Sn1 O2 2.054(2) .
Sn1 O1 2.169(2) 2_666
Sn1 O1 2.193(2) .
Sn2 O4 2.070(3) 2_676
Sn2 O3 2.141(2) .
Sn2 O3 2.167(2) 2_676
O1 C13 1.354(4) .
O1 Sn1 2.169(2) 2_666
O2 C14 1.361(4) .
O3 C35 1.387(4) .
O3 Sn2 2.167(2) 2_676
O4 C36 1.369(4) .
O4 Sn2 2.070(3) 2_676
Cl1 C45 1.765(4) .
Cl2 C45 1.770(4) .
Cl3 C46 1.746(6) .
Cl4 C46 1.743(6) .
C1 C12 1.396(5) .
C1 C14 1.414(5) .
C1 C2 1.517(5) .
C2 C3 1.527(4) .
C3 C4 1.388(5) .
C3 C13 1.409(5) .
C4 C5 1.398(5) .
C5 C6 1.406(5) .
C5 C15 1.530(5) .
C6 C7 1.388(5) .
C7 C13 1.403(4) .
C7 C8 1.532(5) 2_666
C8 C9 1.509(5) .
C8 C7 1.532(5) 2_666
C9 C10 1.399(4) .
C9 C14 1.409(5) .
C10 C11 1.390(5) .
C11 C12 1.403(5) .
C11 C19 1.531(5) .
C15 C18 1.531(5) .
C15 C17 1.533(5) .
C15 C16 1.537(6) .
C19 C20 1.521(6) .
C19 C22 1.530(5) .
C19 C21 1.543(7) .
C23 C24 1.508(5) .
C23 C34 1.528(5) 2_676
C24 C25 1.398(4) .
C24 C35 1.404(4) .
C25 C26 1.384(5) .
C26 C27 1.395(5) .
C26 C37 1.541(4) .
C27 C28 1.408(4) .
C28 C35 1.375(5) .
C28 C29 1.528(5) .
C29 C30 1.526(4) .
C30 C31 1.395(5) .
C30 C36 1.398(5) .
C31 C32 1.395(5) .
C32 C33 1.386(5) .
C32 C41 1.543(5) .
C33 C34 1.394(5) .
C34 C36 1.412(4) .
C34 C23 1.528(5) 2_676
C37 C38 1.501(7) .
C37 C40 1.523(5) .
C37 C39 1.543(6) .
C41 C42 1.444(8) .
C41 C44 1.458(8) .
C41 C43 1.523(8) .
