#------------------------------------------------------------------------------
#$Date: 2016-03-26 13:36:50 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180229 $
#$URL: svn://www.crystallography.net/cod/cif/7/11/15/7111599.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided the Crystal Eye server at
# http://wwmm.ch.cam.ac.uk/crystaleye/, created by Nick Day at the
# Peter Murray-Rust laboratory.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_7111599
loop_
_publ_author_name
'Ni, Chengbao'
'Stich, Troy A.'
'Long, Gary J.'
'Power, Philip P.'
_publ_section_title
;
 Unusual magnetic properties of a two-coordinate heteroleptic linear
 cobalt(ii) complex
;
_journal_issue                   25
_journal_name_full               'Chemical Communications'
_journal_page_first              4466
_journal_page_last               4468
_journal_paper_doi               10.1039/c001483d
_journal_volume                  46
_journal_year                    2010
_chemical_formula_moiety         'C60 H74 Co'
_chemical_formula_sum            'C60 H74 Co'
_chemical_formula_weight         854.12
_chemical_name_systematic
;
?
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 93.6750(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   15.6649(6)
_cell_length_b                   15.9068(6)
_cell_length_c                   19.7416(8)
_cell_measurement_reflns_used    9993
_cell_measurement_temperature    90(2)
_cell_measurement_theta_max      27.50
_cell_measurement_theta_min      2.56
_cell_volume                     4909.1(3)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      90(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0160
_diffrn_reflns_av_sigmaI/netI    0.0146
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -20
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       25
_diffrn_reflns_limit_l_min       -25
_diffrn_reflns_number            18454
_diffrn_reflns_theta_full        27.50
_diffrn_reflns_theta_max         27.50
_diffrn_reflns_theta_min         1.83
_exptl_absorpt_coefficient_mu    0.387
_exptl_absorpt_correction_T_max  0.9551
_exptl_absorpt_correction_T_min  0.8272
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS, 2008'
_exptl_crystal_colour            dark_green
_exptl_crystal_density_diffrn    1.156
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             1844
_exptl_crystal_size_max          0.51
_exptl_crystal_size_mid          0.24
_exptl_crystal_size_min          0.12
_refine_diff_density_max         0.812
_refine_diff_density_min         -0.298
_refine_diff_density_rms         0.054
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.060
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     284
_refine_ls_number_reflns         5641
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.060
_refine_ls_R_factor_all          0.0442
_refine_ls_R_factor_gt           0.0408
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0536P)²+6.4491P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1079
_refine_ls_wR_factor_ref         0.1099
_reflns_number_gt                5184
_reflns_number_total             5641
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            C001483Dsup1.cif
_cod_data_source_block           cbn264fmi
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7111599
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Co1 Co 0.5000 0.751141(17) 0.7500 0.02042(9) Uani 1 2 d S
C1 C 0.42575(9) 0.72843(9) 0.66488(7) 0.0182(3) Uani 1 1 d .
C2 C 0.43959(9) 0.67451(9) 0.60939(7) 0.0184(3) Uani 1 1 d .
C3 C 0.37095(9) 0.64679(10) 0.56605(7) 0.0232(3) Uani 1 1 d .
H3A H 0.3811 0.6078 0.5310 0.028 Uiso 1 1 calc R
C4 C 0.28826(10) 0.67538(11) 0.57347(8) 0.0266(3) Uani 1 1 d .
H4A H 0.2418 0.6542 0.5452 0.032 Uiso 1 1 calc R
C5 C 0.27447(10) 0.73476(10) 0.62238(8) 0.0247(3) Uani 1 1 d .
H5A H 0.2190 0.7582 0.6253 0.030 Uiso 1 1 calc R
C6 C 0.34177(9) 0.76090(9) 0.66782(7) 0.0202(3) Uani 1 1 d .
C7 C 0.52622(9) 0.65234(9) 0.58510(7) 0.0197(3) Uani 1 1 d .
C8 C 0.56078(9) 0.70696(10) 0.53738(7) 0.0226(3) Uani 1 1 d .
C9 C 0.63324(10) 0.68118(12) 0.50495(8) 0.0293(3) Uani 1 1 d .
H9A H 0.6580 0.7182 0.4739 0.035 Uiso 1 1 calc R
C10 C 0.66951(10) 0.60273(12) 0.51725(8) 0.0320(4) Uani 1 1 d .
H10A H 0.7169 0.5851 0.4931 0.038 Uiso 1 1 calc R
C11 C 0.63635(10) 0.55030(11) 0.56475(8) 0.0285(3) Uani 1 1 d .
H11A H 0.6621 0.4970 0.5738 0.034 Uiso 1 1 calc R
C12 C 0.56543(9) 0.57445(10) 0.59981(7) 0.0223(3) Uani 1 1 d .
C13 C 0.51914(10) 0.79076(10) 0.51821(8) 0.0249(3) Uani 1 1 d .
H13A H 0.4735 0.8012 0.5503 0.030 Uiso 1 1 calc R
C14 C 0.47594(11) 0.78789(11) 0.44635(9) 0.0327(4) Uani 1 1 d .
H14A H 0.4338 0.7423 0.4434 0.049 Uiso 1 1 calc R
H14B H 0.5192 0.7780 0.4135 0.049 Uiso 1 1 calc R
H14C H 0.4472 0.8415 0.4362 0.049 Uiso 1 1 calc R
C15 C 0.58241(13) 0.86379(12) 0.52545(10) 0.0379(4) Uani 1 1 d .
H15A H 0.6090 0.8647 0.5717 0.057 Uiso 1 1 calc R
H15B H 0.5521 0.9168 0.5162 0.057 Uiso 1 1 calc R
H15C H 0.6267 0.8566 0.4931 0.057 Uiso 1 1 calc R
C16 C 0.53272(10) 0.51522(10) 0.65236(8) 0.0252(3) Uani 1 1 d .
H16A H 0.4856 0.5442 0.6750 0.030 Uiso 1 1 calc R
C17 C 0.49645(19) 0.43573(14) 0.61918(12) 0.0568(6) Uani 1 1 d .
H17A H 0.4769 0.3979 0.6541 0.085 Uiso 1 1 calc R
H17B H 0.5409 0.4078 0.5947 0.085 Uiso 1 1 calc R
H17C H 0.4482 0.4502 0.5873 0.085 Uiso 1 1 calc R
C18 C 0.60341(12) 0.49386(14) 0.70685(10) 0.0417(5) Uani 1 1 d .
H18A H 0.5799 0.4584 0.7417 0.062 Uiso 1 1 calc R
H18B H 0.6261 0.5459 0.7277 0.062 Uiso 1 1 calc R
H18C H 0.6495 0.4636 0.6860 0.062 Uiso 1 1 calc R
C19 C 0.32395(9) 0.82929(9) 0.71751(7) 0.0217(3) Uani 1 1 d .
C20 C 0.26785(10) 0.81429(10) 0.76935(8) 0.0268(3) Uani 1 1 d .
C21 C 0.25191(11) 0.87945(11) 0.81435(8) 0.0305(3) Uani 1 1 d .
H21A H 0.2165 0.8692 0.8508 0.037 Uiso 1 1 calc R
C22 C 0.28692(11) 0.95877(11) 0.80677(9) 0.0311(3) Uani 1 1 d .
H22A H 0.2759 1.0022 0.8381 0.037 Uiso 1 1 calc R
C23 C 0.33816(11) 0.97449(10) 0.75316(9) 0.0294(3) Uani 1 1 d .
H23A H 0.3601 1.0295 0.7473 0.035 Uiso 1 1 calc R
C24 C 0.35790(10) 0.91121(10) 0.70796(8) 0.0240(3) Uani 1 1 d .
C25 C 0.22109(11) 0.73040(11) 0.77567(8) 0.0284(3) Uani 1 1 d .
H25 H 0.2441 0.6905 0.7422 0.034 Uiso 1 1 calc R
C26 C 0.12427(11) 0.73927(12) 0.75841(10) 0.0348(4) Uani 1 1 d .
H26A H 0.0972 0.6838 0.7598 0.052 Uiso 1 1 calc R
H26B H 0.1145 0.7633 0.7129 0.052 Uiso 1 1 calc R
H26C H 0.0995 0.7764 0.7916 0.052 Uiso 1 1 calc R
C27 C 0.23840(12) 0.69295(12) 0.84606(9) 0.0364(4) Uani 1 1 d .
H27A H 0.3003 0.6893 0.8566 0.055 Uiso 1 1 calc R
H27B H 0.2133 0.6366 0.8473 0.055 Uiso 1 1 calc R
H27C H 0.2128 0.7288 0.8796 0.055 Uiso 1 1 calc R
C28 C 0.40847(10) 0.93134(10) 0.64606(8) 0.0266(3) Uani 1 1 d .
H28A H 0.4479 0.8831 0.6393 0.032 Uiso 1 1 calc R
C29 C 0.46276(12) 1.01069(11) 0.65234(10) 0.0353(4) Uani 1 1 d .
H29A H 0.4988 1.0144 0.6137 0.053 Uiso 1 1 calc R
H29B H 0.4991 1.0087 0.6946 0.053 Uiso 1 1 calc R
H29C H 0.4253 1.0600 0.6528 0.053 Uiso 1 1 calc R
C30 C 0.34801(12) 0.93825(12) 0.58217(9) 0.0345(4) Uani 1 1 d .
H30A H 0.3142 0.8866 0.5766 0.052 Uiso 1 1 calc R
H30B H 0.3816 0.9463 0.5424 0.052 Uiso 1 1 calc R
H30C H 0.3096 0.9863 0.5866 0.052 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_3
C1 Co1 C1 159.34(8) 2_656
C6 C1 C2 116.10(13) .
C6 C1 Co1 112.84(10) .
C2 C1 Co1 130.09(10) .
C3 C2 C1 120.81(13) .
C3 C2 C7 113.74(12) .
C1 C2 C7 124.85(12) .
C4 C3 C2 121.10(14) .
C4 C3 H3A 119.5 .
C2 C3 H3A 119.5 .
C5 C4 C3 119.17(14) .
C5 C4 H4A 120.4 .
C3 C4 H4A 120.4 .
C4 C5 C6 120.42(14) .
C4 C5 H5A 119.8 .
C6 C5 H5A 119.8 .
C5 C6 C1 121.81(13) .
C5 C6 C19 117.94(13) .
C1 C6 C19 120.13(13) .
C12 C7 C8 119.89(13) .
C12 C7 C2 122.03(13) .
C8 C7 C2 117.28(13) .
C9 C8 C7 118.74(14) .
C9 C8 C13 119.36(13) .
C7 C8 C13 121.84(13) .
C10 C9 C8 121.25(15) .
C10 C9 H9A 119.4 .
C8 C9 H9A 119.4 .
C11 C10 C9 119.66(14) .
C11 C10 H10A 120.2 .
C9 C10 H10A 120.2 .
C10 C11 C12 121.00(15) .
C10 C11 H11A 119.5 .
C12 C11 H11A 119.5 .
C11 C12 C7 119.35(14) .
C11 C12 C16 118.82(14) .
C7 C12 C16 121.83(13) .
C8 C13 C15 112.20(14) .
C8 C13 C14 111.15(13) .
C15 C13 C14 110.76(13) .
C8 C13 H13A 107.5 .
C15 C13 H13A 107.5 .
C14 C13 H13A 107.5 .
C13 C14 H14A 109.5 .
C13 C14 H14B 109.5 .
H14A C14 H14B 109.5 .
C13 C14 H14C 109.5 .
H14A C14 H14C 109.5 .
H14B C14 H14C 109.5 .
C13 C15 H15A 109.5 .
C13 C15 H15B 109.5 .
H15A C15 H15B 109.5 .
C13 C15 H15C 109.5 .
H15A C15 H15C 109.5 .
H15B C15 H15C 109.5 .
C12 C16 C17 110.87(14) .
C12 C16 C18 110.97(14) .
C17 C16 C18 110.62(17) .
C12 C16 H16A 108.1 .
C17 C16 H16A 108.1 .
C18 C16 H16A 108.1 .
C16 C17 H17A 109.5 .
C16 C17 H17B 109.5 .
H17A C17 H17B 109.5 .
C16 C17 H17C 109.5 .
H17A C17 H17C 109.5 .
H17B C17 H17C 109.5 .
C16 C18 H18A 109.5 .
C16 C18 H18B 109.5 .
H18A C18 H18B 109.5 .
C16 C18 H18C 109.5 .
H18A C18 H18C 109.5 .
H18B C18 H18C 109.5 .
C20 C19 C24 120.38(14) .
C20 C19 C6 120.08(14) .
C24 C19 C6 119.29(13) .
C21 C20 C19 118.71(15) .
C21 C20 C25 119.24(14) .
C19 C20 C25 122.00(14) .
C22 C21 C20 121.18(15) .
C22 C21 H21A 119.4 .
C20 C21 H21A 119.4 .
C21 C22 C23 119.78(15) .
C21 C22 H22A 120.1 .
C23 C22 H22A 120.1 .
C22 C23 C24 121.34(16) .
C22 C23 H23A 119.3 .
C24 C23 H23A 119.3 .
C23 C24 C19 118.43(14) .
C23 C24 C28 120.48(14) .
C19 C24 C28 120.88(13) .
C27 C25 C20 110.97(15) .
C27 C25 C26 110.72(14) .
C20 C25 C26 111.82(14) .
C27 C25 H25 107.7 .
C20 C25 H25 107.7 .
C26 C25 H25 107.7 .
C25 C26 H26A 109.5 .
C25 C26 H26B 109.5 .
H26A C26 H26B 109.5 .
C25 C26 H26C 109.5 .
H26A C26 H26C 109.5 .
H26B C26 H26C 109.5 .
C25 C27 H27A 109.5 .
C25 C27 H27B 109.5 .
H27A C27 H27B 109.5 .
C25 C27 H27C 109.5 .
H27A C27 H27C 109.5 .
H27B C27 H27C 109.5 .
C29 C28 C30 108.68(14) .
C29 C28 C24 115.02(14) .
C30 C28 C24 110.34(13) .
C29 C28 H28A 107.5 .
C30 C28 H28A 107.5 .
C24 C28 H28A 107.5 .
C28 C29 H29A 109.5 .
C28 C29 H29B 109.5 .
H29A C29 H29B 109.5 .
C28 C29 H29C 109.5 .
H29A C29 H29C 109.5 .
H29B C29 H29C 109.5 .
C28 C30 H30A 109.5 .
C28 C30 H30B 109.5 .
H30A C30 H30B 109.5 .
C28 C30 H30C 109.5 .
H30A C30 H30C 109.5 .
H30B C30 H30C 109.5 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Co1 C1 2.0141(14) .
Co1 C1 2.0141(14) 2_656
C1 C6 1.418(2) .
C1 C2 1.4188(19) .
C2 C3 1.402(2) .
C2 C7 1.5097(19) .
C3 C4 1.389(2) .
C3 H3A 0.9500 .
C4 C5 1.378(2) .
C4 H4A 0.9500 .
C5 C6 1.403(2) .
C5 H5A 0.9500 .
C6 C19 1.503(2) .
C7 C12 1.405(2) .
C7 C8 1.415(2) .
C8 C9 1.400(2) .
C8 C13 1.521(2) .
C9 C10 1.386(3) .
C9 H9A 0.9500 .
C10 C11 1.381(2) .
C10 H10A 0.9500 .
C11 C12 1.400(2) .
C11 H11A 0.9500 .
C12 C16 1.515(2) .
C13 C15 1.528(2) .
C13 C14 1.533(2) .
C13 H13A 1.0000 .
C14 H14A 0.9800 .
C14 H14B 0.9800 .
C14 H14C 0.9800 .
C15 H15A 0.9800 .
C15 H15B 0.9800 .
C15 H15C 0.9800 .
C16 C17 1.518(3) .
C16 C18 1.532(2) .
C16 H16A 1.0000 .
C17 H17A 0.9800 .
C17 H17B 0.9800 .
C17 H17C 0.9800 .
C18 H18A 0.9800 .
C18 H18B 0.9800 .
C18 H18C 0.9800 .
C19 C20 1.411(2) .
C19 C24 1.425(2) .
C20 C21 1.398(2) .
C20 C25 1.531(2) .
C21 C22 1.388(3) .
C21 H21A 0.9500 .
C22 C23 1.391(2) .
C22 H22A 0.9500 .
C23 C24 1.393(2) .
C23 H23A 0.9500 .
C24 C28 1.532(2) .
C25 C27 1.520(2) .
C25 C26 1.539(2) .
C25 H25 1.0000 .
C26 H26A 0.9800 .
C26 H26B 0.9800 .
C26 H26C 0.9800 .
C27 H27A 0.9800 .
C27 H27B 0.9800 .
C27 H27C 0.9800 .
C28 C29 1.523(2) .
C28 C30 1.532(2) .
C28 H28A 1.0000 .
C29 H29A 0.9800 .
C29 H29B 0.9800 .
C29 H29C 0.9800 .
C30 H30A 0.9800 .
C30 H30B 0.9800 .
C30 H30C 0.9800 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
C1 Co1 C1 C6 118.59(10) 2_656
C1 Co1 C1 C2 -49.48(12) 2_656
C6 C1 C2 C3 -8.3(2) .
Co1 C1 C2 C3 159.44(11) .
C6 C1 C2 C7 162.25(13) .
Co1 C1 C2 C7 -30.0(2) .
C1 C2 C3 C4 4.1(2) .
C7 C2 C3 C4 -167.44(14) .
C2 C3 C4 C5 2.9(2) .
C3 C4 C5 C6 -5.3(2) .
C4 C5 C6 C1 0.7(2) .
C4 C5 C6 C19 176.68(14) .
C2 C1 C6 C5 6.0(2) .
Co1 C1 C6 C5 -163.84(12) .
C2 C1 C6 C19 -169.90(12) .
Co1 C1 C6 C19 20.25(16) .
C3 C2 C7 C12 -85.82(17) .
C1 C2 C7 C12 103.03(17) .
C3 C2 C7 C8 83.90(16) .
C1 C2 C7 C8 -87.25(17) .
C12 C7 C8 C9 0.9(2) .
C2 C7 C8 C9 -169.02(13) .
C12 C7 C8 C13 178.17(13) .
C2 C7 C8 C13 8.2(2) .
C7 C8 C9 C10 2.0(2) .
C13 C8 C9 C10 -175.28(15) .
C8 C9 C10 C11 -3.2(3) .
C9 C10 C11 C12 1.3(3) .
C10 C11 C12 C7 1.6(2) .
C10 C11 C12 C16 -178.82(15) .
C8 C7 C12 C11 -2.7(2) .
C2 C7 C12 C11 166.74(14) .
C8 C7 C12 C16 177.74(13) .
C2 C7 C12 C16 -12.8(2) .
C9 C8 C13 C15 -55.25(19) .
C7 C8 C13 C15 127.53(15) .
C9 C8 C13 C14 69.39(19) .
C7 C8 C13 C14 -107.83(16) .
C11 C12 C16 C17 -66.5(2) .
C7 C12 C16 C17 113.06(19) .
C11 C12 C16 C18 56.9(2) .
C7 C12 C16 C18 -123.59(16) .
C5 C6 C19 C20 67.00(19) .
C1 C6 C19 C20 -116.93(16) .
C5 C6 C19 C24 -107.28(16) .
C1 C6 C19 C24 68.79(18) .
C24 C19 C20 C21 -5.1(2) .
C6 C19 C20 C21 -179.35(14) .
C24 C19 C20 C25 172.06(14) .
C6 C19 C20 C25 -2.2(2) .
C19 C20 C21 C22 3.1(2) .
C25 C20 C21 C22 -174.21(15) .
C20 C21 C22 C23 0.7(3) .
C21 C22 C23 C24 -2.4(3) .
C22 C23 C24 C19 0.3(2) .
C22 C23 C24 C28 175.14(15) .
C20 C19 C24 C23 3.5(2) .
C6 C19 C24 C23 177.75(14) .
C20 C19 C24 C28 -171.32(14) .
C6 C19 C24 C28 2.9(2) .
C21 C20 C25 C27 -57.6(2) .
C19 C20 C25 C27 125.21(16) .
C21 C20 C25 C26 66.6(2) .
C19 C20 C25 C26 -110.63(17) .
C23 C24 C28 C29 22.8(2) .
C19 C24 C28 C29 -162.51(14) .
C23 C24 C28 C30 -100.58(17) .
C19 C24 C28 C30 74.12(18) .
