#------------------------------------------------------------------------------
#$Date: 2016-03-26 13:39:38 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180231 $
#$URL: svn://www.crystallography.net/cod/cif/7/11/17/7111746.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided the Crystal Eye server at
# http://wwmm.ch.cam.ac.uk/crystaleye/, created by Nick Day at the
# Peter Murray-Rust laboratory.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_7111746
loop_
_publ_author_name
'Burrows, Andrew D.'
'Frost, Christopher G.'
'Mahon, Mary F.'
'Raithby, Paul R.'
'Richardson, Christopher'
'Stevenson, Anna J.'
_publ_section_title
;
 Solid state interconversion of cages and coordination networks via
 conformational change of a semi-rigid ligand
;
_journal_issue                   28
_journal_name_full               'Chemical Communications'
_journal_page_first              5064
_journal_page_last               5066
_journal_paper_doi               10.1039/c0cc00826e
_journal_volume                  46
_journal_year                    2010
_chemical_formula_sum            'C58 H70 Ag2 Cl2 N6 O15'
_chemical_formula_weight         1377.84
_chemical_name_systematic
;
?
;
_space_group_IT_number           176
_symmetry_cell_setting           hexagonal
_symmetry_space_group_name_Hall  '-P 6c'
_symmetry_space_group_name_H-M   'P 63/m'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            4
_cell_length_a                   14.4400(2)
_cell_length_b                   14.4400(2)
_cell_length_c                   35.3990(6)
_cell_measurement_reflns_used    52173
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      25.028
_cell_measurement_theta_min      2.910
_cell_volume                     6392.28(17)
_computing_cell_refinement       'HKL Scalepack (Otwinowski & Minor 1997)'
_computing_data_collection       'Collect (Bruker AXS BV, 1997-2004)'
_computing_data_reduction
'Denzo & Scalepack (Otwinowski & Minor, 1997)'
_computing_molecular_graphics    'ORTEX (P.McArdle, 1995)'
_computing_publication_material  'SHELXL-97/2 (Sheldrick,1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  '95mm CCD camera on κ-goniostat'
_diffrn_measurement_method       CCD
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1774
_diffrn_reflns_av_sigmaI/netI    0.0736
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       42
_diffrn_reflns_limit_l_min       -42
_diffrn_reflns_number            67463
_diffrn_reflns_theta_full        25.02
_diffrn_reflns_theta_max         25.02
_diffrn_reflns_theta_min         3.99
_exptl_absorpt_coefficient_mu    0.763
_exptl_absorpt_correction_T_max  0.88
_exptl_absorpt_correction_T_min  0.82
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
multi-scan from symmetry-related measurements
Sortav (Blessing 1995)
;
_exptl_crystal_colour            Colourless
_exptl_crystal_density_diffrn    1.432
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Parallelepiped
_exptl_crystal_F_000             2832
_exptl_crystal_size_max          0.22
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.13
_refine_diff_density_max         0.451
_refine_diff_density_min         -0.543
_refine_diff_density_rms         0.079
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.937
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     265
_refine_ls_number_reflns         3828
_refine_ls_number_restraints     26
_refine_ls_restrained_S_all      0.939
_refine_ls_R_factor_all          0.1196
_refine_ls_R_factor_gt           0.0455
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0729P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1075
_refine_ls_wR_factor_ref         0.1343
_reflns_number_gt                2001
_reflns_number_total             3828
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            C0CC00826Esup1.cif
_cod_data_source_block           h08adb04-(Compound_2)
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Hexagonal' changed to 'hexagonal'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from
2011-04-26.

'_exptl_absorpt_correction_type' value 'Multi-Scan'
changed to 'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_H-M      P63/m
_cod_database_code               7111746
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'x-y, x, z+1/2'
'-y, x-y, z'
'-x, -y, z+1/2'
'-x+y, -x, z'
'y, -x+y, z+1/2'
'-x, -y, -z'
'-x+y, -x, -z-1/2'
'y, -x+y, -z'
'x, y, -z-1/2'
'x-y, x, -z'
'-y, x-y, -z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 1.0000 0.0000 0.363061(17) 0.0396(2) Uani 1 3 d S
Ag2 Ag 1.0000 0.0000 0.456999(16) 0.0378(2) Uani 1 3 d S
Cl1 Cl 1.3333 0.6667 0.40077(6) 0.0404(6) Uani 1 3 d S
Cl2 Cl 1.6667 0.3333 0.35730(10) 0.0851(9) Uani 1 3 d S
O1 O 1.0695(3) 0.2395(3) 0.36451(9) 0.0461(9) Uani 1 1 d .
O2 O 1.2377(3) 0.0866(3) 0.44477(10) 0.0487(9) Uani 1 1 d .
O3 O 1.3333 0.6667 0.35989(14) 0.0409(14) Uani 1 3 d S
O4 O 1.2924(3) 0.5597(3) 0.41389(9) 0.0545(10) Uani 1 1 d .
O5 O 1.5838(5) 0.3516(5) 0.34589(15) 0.140(2) Uani 1 1 d .
O6 O 1.6667 0.3333 0.3975(2) 0.092(2) Uani 1 3 d S
N1 N 1.1167(3) 0.1753(3) 0.36054(11) 0.0454(11) Uani 1 1 d .
N2 N 1.1701(3) 0.1273(3) 0.45382(10) 0.0432(11) Uani 1 1 d .
C1 C 1.2862(4) 0.1948(4) 0.34003(14) 0.0526(15) Uani 1 1 d .
H1A H 1.2570 0.1233 0.3511 0.079 Uiso 1 1 calc R
H1B H 1.3570 0.2424 0.3508 0.079 Uiso 1 1 calc R
H1C H 1.2923 0.1905 0.3126 0.079 Uiso 1 1 calc R
C2 C 1.2140(4) 0.2373(4) 0.34860(13) 0.0387(13) Uani 1 1 d .
C3 C 1.2359(4) 0.3444(4) 0.34499(12) 0.0350(12) Uani 1 1 d .
C4 C 1.1436(4) 0.3402(4) 0.35463(14) 0.0418(13) Uani 1 1 d .
C5 C 1.1058(4) 0.4192(4) 0.35579(17) 0.0598(16) Uani 1 1 d .
H5A H 1.0865 0.4260 0.3818 0.090 Uiso 1 1 calc R
H5B H 1.0430 0.3946 0.3394 0.090 Uiso 1 1 calc R
H5C H 1.1629 0.4888 0.3469 0.090 Uiso 1 1 calc R
C6 C 1.3397(4) 0.4389(4) 0.33244(12) 0.0406(13) Uani 1 1 d .
H6A H 1.3999 0.4323 0.3427 0.049 Uiso 1 1 calc R
H6B H 1.3451 0.5051 0.3428 0.049 Uiso 1 1 calc R
C7 C 1.3491(4) 0.4478(4) 0.28945(13) 0.0369(12) Uani 1 1 d .
C8 C 1.4020(4) 0.4076(4) 0.26957(12) 0.0446(13) Uani 1 1 d .
H8 H 1.4395 0.3791 0.2828 0.054 Uiso 1 1 calc R
C9 C 1.2996(4) 0.4936(4) 0.26959(12) 0.0494(14) Uani 1 1 d .
H9 H 1.2654 0.5253 0.2829 0.059 Uiso 1 1 calc R
C10 C 1.4190(4) 0.1445(5) 0.42508(16) 0.0624(16) Uani 1 1 d .
H10A H 1.4882 0.2105 0.4227 0.094 Uiso 1 1 calc R
H10B H 1.4005 0.1060 0.4010 0.094 Uiso 1 1 calc R
H10C H 1.4234 0.0993 0.4448 0.094 Uiso 1 1 calc R
C11 C 1.3351(4) 0.1716(4) 0.43527(14) 0.0444(13) Uani 1 1 d .
C12 C 1.3317(4) 0.2624(4) 0.43785(13) 0.0385(12) Uani 1 1 d .
C13 C 1.2264(4) 0.2318(4) 0.44979(12) 0.0359(12) Uani 1 1 d .
C14 C 1.1796(4) 0.3006(4) 0.45756(13) 0.0463(14) Uani 1 1 d .
H14A H 1.1845 0.3416 0.4348 0.070 Uiso 1 1 calc R
H14B H 1.2188 0.3499 0.4782 0.070 Uiso 1 1 calc R
H14C H 1.1043 0.2558 0.4647 0.070 Uiso 1 1 calc R
C15 C 1.4200(4) 0.3753(4) 0.43067(13) 0.0447(13) Uani 1 1 d .
H15A H 1.3935 0.4109 0.4135 0.054 Uiso 1 1 calc R
H15B H 1.4801 0.3735 0.4180 0.054 Uiso 1 1 calc R
C16 C 1.4605(4) 0.4403(4) 0.46694(13) 0.0359(12) Uani 1 1 d .
C17 C 1.4979(4) 0.4041(4) 0.49643(13) 0.0424(13) Uani 1 1 d .
H17 H 1.4974 0.3384 0.4941 0.051 Uiso 1 1 calc R
C18 C 1.5354(3) 0.4633(4) 0.52895(14) 0.0415(13) Uani 1 1 d .
H18 H 1.5591 0.4368 0.5491 0.050 Uiso 1 1 calc R
O7 O 1.3074(3) 0.0741(4) 0.25008(14) 0.130(3) Uani 0.67 2 d SPRDU
C102 C 1.4914(3) 0.1927(4) 0.25008(14) 0.120(5) Uani 0.67 2 d SPRDU
H10D H 1.5572 0.1888 0.2500 0.180 Uiso 0.67 2 calc SPR
H10E H 1.4896 0.2307 0.2728 0.180 Uiso 0.33 1 calc PR
H10F H 1.4894 0.2311 0.2276 0.180 Uiso 0.33 1 calc PR
C101 C 1.4061(11) 0.0931(12) 0.2500 0.124(4) Uani 0.67 2 d SPDU
H10G H 1.4135 0.0566 0.2275 0.148 Uiso 0.33 1 calc PR
H10H H 1.4136 0.0561 0.2723 0.148 Uiso 0.33 1 calc PR
C104 C 1.1169(13) -0.0692(13) 0.2500 0.115(5) Uani 0.67 2 d SPDU
H10I H 1.0797 -0.1476 0.2500 0.173 Uiso 0.67 2 calc SPR
H10J H 1.0968 -0.0441 0.2274 0.173 Uiso 0.33 1 calc PR
H10K H 1.0968 -0.0442 0.2726 0.173 Uiso 0.33 1 calc PR
C103 C 1.2245(13) -0.0300(13) 0.2500 0.132(4) Uani 0.67 2 d SPDU
H10L H 1.2378 -0.0629 0.2277 0.158 Uiso 0.33 1 calc PR
H10M H 1.2377 -0.0633 0.2723 0.158 Uiso 0.33 1 calc PR
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N1 Ag1 N1 119.841(14) . 3_645
N1 Ag1 N1 119.841(15) . 5_765
N1 Ag1 N1 119.841(15) 3_645 5_765
N1 Ag1 Ag2 92.29(10) . .
N1 Ag1 Ag2 92.29(10) 3_645 .
N1 Ag1 Ag2 92.29(10) 5_765 .
N2 Ag2 N2 119.745(17) . 3_645
N2 Ag2 N2 119.744(17) . 5_765
N2 Ag2 N2 119.744(17) 3_645 5_765
N2 Ag2 Ag2 92.91(10) . 7_756
N2 Ag2 Ag2 92.91(10) 3_645 7_756
N2 Ag2 Ag2 92.91(10) 5_765 7_756
N2 Ag2 Ag1 87.09(10) . .
N2 Ag2 Ag1 87.09(10) 3_645 .
N2 Ag2 Ag1 87.09(10) 5_765 .
Ag2 Ag2 Ag1 180.0 7_756 .
O4 Cl1 O4 110.15(15) 5_775 .
O4 Cl1 O4 109.98(15) 5_775 3_755
O4 Cl1 O4 109.70(15) . 3_755
O4 Cl1 O3 109.19(15) 5_775 .
O4 Cl1 O3 108.97(15) . .
O4 Cl1 O3 108.80(15) 3_755 .
O5 Cl2 O5 112.4(2) 5_875 3_745
O5 Cl2 O5 112.0(2) 5_875 .
O5 Cl2 O5 111.9(2) 3_745 .
O5 Cl2 O6 106.8(3) 5_875 .
O5 Cl2 O6 106.5(3) 3_745 .
O5 Cl2 O6 106.8(3) . .
C4 O1 N1 107.4(4) . .
C11 O2 N2 107.3(4) . .
C2 N1 O1 107.0(4) . .
C2 N1 Ag1 137.3(4) . .
O1 N1 Ag1 113.8(3) . .
C13 N2 O2 107.2(4) . .
C13 N2 Ag2 138.5(4) . .
O2 N2 Ag2 112.2(3) . .
C2 C1 H1A 109.5 . .
C2 C1 H1B 109.5 . .
H1A C1 H1B 109.5 . .
C2 C1 H1C 109.5 . .
H1A C1 H1C 109.5 . .
H1B C1 H1C 109.5 . .
N1 C2 C3 110.7(5) . .
N1 C2 C1 121.5(5) . .
C3 C2 C1 127.8(5) . .
C4 C3 C2 104.6(4) . .
C4 C3 C6 129.1(5) . .
C2 C3 C6 126.4(5) . .
C3 C4 O1 110.4(5) . .
C3 C4 C5 134.8(5) . .
O1 C4 C5 114.8(5) . .
C4 C5 H5A 109.5 . .
C4 C5 H5B 109.5 . .
H5A C5 H5B 109.5 . .
C4 C5 H5C 109.5 . .
H5A C5 H5C 109.5 . .
H5B C5 H5C 109.5 . .
C3 C6 C7 112.2(4) . .
C3 C6 H6A 109.2 . .
C7 C6 H6A 109.2 . .
C3 C6 H6B 109.2 . .
C7 C6 H6B 109.2 . .
H6A C6 H6B 107.9 . .
C8 C7 C9 118.4(4) . .
C8 C7 C6 121.6(5) . .
C9 C7 C6 120.0(4) . .
C7 C8 C8 121.1(3) . 10_556
C7 C8 H8 119.5 . .
C8 C8 H8 119.5 10_556 .
C7 C9 C9 120.5(3) . 10_556
C7 C9 H9 119.7 . .
C9 C9 H9 119.7 10_556 .
C11 C10 H10A 109.5 . .
C11 C10 H10B 109.5 . .
H10A C10 H10B 109.5 . .
C11 C10 H10C 109.5 . .
H10A C10 H10C 109.5 . .
H10B C10 H10C 109.5 . .
C12 C11 O2 109.7(5) . .
C12 C11 C10 134.9(5) . .
O2 C11 C10 115.4(5) . .
C11 C12 C13 105.9(4) . .
C11 C12 C15 128.4(5) . .
C13 C12 C15 125.7(5) . .
N2 C13 C12 109.9(4) . .
N2 C13 C14 121.5(5) . .
C12 C13 C14 128.6(5) . .
C13 C14 H14A 109.5 . .
C13 C14 H14B 109.5 . .
H14A C14 H14B 109.5 . .
C13 C14 H14C 109.5 . .
H14A C14 H14C 109.5 . .
H14B C14 H14C 109.5 . .
C12 C15 C16 112.4(4) . .
C12 C15 H15A 109.1 . .
C16 C15 H15A 109.1 . .
C12 C15 H15B 109.1 . .
C16 C15 H15B 109.1 . .
H15A C15 H15B 107.9 . .
C18 C16 C17 118.3(4) 7_866 .
C18 C16 C15 121.5(4) 7_866 .
C17 C16 C15 120.2(5) . .
C18 C17 C16 120.1(5) . .
C18 C17 H17 119.9 . .
C16 C17 H17 119.9 . .
C17 C18 C16 121.6(4) . 7_866
C17 C18 H18 119.2 . .
C16 C18 H18 119.2 7_866 .
C101 O7 C103 119.3(12) . .
C101 C102 H10D 109.5 . .
C101 C102 H10E 109.5 . .
H10D C102 H10E 109.5 . .
C101 C102 H10F 109.5 . .
H10D C102 H10F 109.5 . .
H10E C102 H10F 109.5 . .
O7 C101 C102 122.8(13) . .
O7 C101 H10G 106.6 . .
C102 C101 H10G 106.6 . .
O7 C101 H10H 106.6 . .
C102 C101 H10H 106.6 . .
H10G C101 H10H 106.6 . .
C103 C104 H10I 109.5 . .
C103 C104 H10J 109.5 . .
H10I C104 H10J 109.5 . .
C103 C104 H10K 109.5 . .
H10I C104 H10K 109.5 . .
H10J C104 H10K 109.5 . .
C104 C103 O7 130.0(17) . .
C104 C103 H10L 104.8 . .
O7 C103 H10L 104.8 . .
C104 C103 H10M 104.8 . .
O7 C103 H10M 104.8 . .
H10L C103 H10M 105.8 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N1 2.234(4) .
Ag1 N1 2.234(4) 3_645
Ag1 N1 2.234(4) 5_765
Ag1 Ag2 3.3253(8) .
Ag2 N2 2.216(4) .
Ag2 N2 2.216(4) 3_645
Ag2 N2 2.216(4) 5_765
Ag2 Ag2 3.0444(11) 7_756
Cl1 O4 1.424(3) 5_775
Cl1 O4 1.429(3) .
Cl1 O4 1.432(3) 3_755
Cl1 O3 1.447(5) .
Cl2 O5 1.404(5) 5_875
Cl2 O5 1.405(5) 3_745
Cl2 O5 1.412(5) .
Cl2 O6 1.425(8) .
O1 C4 1.351(6) .
O1 N1 1.406(5) .
O2 C11 1.368(6) .
O2 N2 1.404(5) .
N1 C2 1.302(6) .
N2 C13 1.317(6) .
C1 C2 1.481(7) .
C1 H1A 0.9800 .
C1 H1B 0.9800 .
C1 H1C 0.9800 .
C2 C3 1.422(6) .
C3 C4 1.347(7) .
C3 C6 1.503(6) .
C4 C5 1.492(7) .
C5 H5A 0.9800 .
C5 H5B 0.9800 .
C5 H5C 0.9800 .
C6 C7 1.528(6) .
C6 H6A 0.9900 .
C6 H6B 0.9900 .
C7 C8 1.364(6) .
C7 C9 1.384(6) .
C8 C8 1.386(9) 10_556
C8 H8 0.9500 .
C9 C9 1.387(9) 10_556
C9 H9 0.9500 .
C10 C11 1.492(7) .
C10 H10A 0.9800 .
C10 H10B 0.9800 .
C10 H10C 0.9800 .
C11 C12 1.340(6) .
C12 C13 1.419(6) .
C12 C15 1.506(6) .
C13 C14 1.479(7) .
C14 H14A 0.9800 .
C14 H14B 0.9800 .
C14 H14C 0.9800 .
C15 C16 1.524(6) .
C15 H15A 0.9900 .
C15 H15B 0.9900 .
C16 C18 1.371(6) 7_866
C16 C17 1.391(6) .
C17 C18 1.373(6) .
C17 H17 0.9500 .
C18 C16 1.371(6) 7_866
C18 H18 0.9500 .
O7 C101 1.311(14) .
O7 C103 1.376(16) .
C102 C101 1.346(14) .
C102 H10D 0.9800 .
C102 H10E 0.9800 .
C102 H10F 0.9800 .
C101 H10G 0.9900 .
C101 H10H 0.9900 .
C104 C103 1.362(15) .
C104 H10I 0.9800 .
C104 H10J 0.9800 .
C104 H10K 0.9800 .
C103 H10L 0.9900 .
C103 H10M 0.9900 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
N1 Ag1 Ag2 N2 -33.18(16) . .
N1 Ag1 Ag2 N2 -153.18(16) 3_645 .
N1 Ag1 Ag2 N2 86.82(16) 5_765 .
N1 Ag1 Ag2 N2 86.82(17) . 3_645
N1 Ag1 Ag2 N2 -33.18(17) 3_645 3_645
N1 Ag1 Ag2 N2 -153.18(17) 5_765 3_645
N1 Ag1 Ag2 N2 -153.18(16) . 5_765
N1 Ag1 Ag2 N2 86.82(16) 3_645 5_765
N1 Ag1 Ag2 N2 -33.18(16) 5_765 5_765
N1 Ag1 Ag2 Ag2 -79(12) . 7_756
N1 Ag1 Ag2 Ag2 161(12) 3_645 7_756
N1 Ag1 Ag2 Ag2 41(4) 5_765 7_756
C4 O1 N1 C2 -0.4(5) . .
C4 O1 N1 Ag1 -167.4(3) . .
N1 Ag1 N1 C2 -150.2(4) 3_645 .
N1 Ag1 N1 C2 21.8(6) 5_765 .
Ag2 Ag1 N1 C2 115.8(5) . .
N1 Ag1 N1 O1 11.3(4) 3_645 .
N1 Ag1 N1 O1 -176.66(16) 5_765 .
Ag2 Ag1 N1 O1 -82.7(3) . .
C11 O2 N2 C13 -0.1(5) . .
C11 O2 N2 Ag2 166.7(3) . .
N2 Ag2 N2 C13 -1.1(6) 3_645 .
N2 Ag2 N2 C13 168.9(3) 5_765 .
Ag2 Ag2 N2 C13 -96.1(5) 7_756 .
Ag1 Ag2 N2 C13 83.9(5) . .
N2 Ag2 N2 O2 -161.92(16) 3_645 .
N2 Ag2 N2 O2 8.0(4) 5_765 .
Ag2 Ag2 N2 O2 103.1(3) 7_756 .
Ag1 Ag2 N2 O2 -76.9(3) . .
O1 N1 C2 C3 1.3(5) . .
Ag1 N1 C2 C3 163.6(3) . .
O1 N1 C2 C1 -177.8(4) . .
Ag1 N1 C2 C1 -15.5(8) . .
N1 C2 C3 C4 -1.7(5) . .
C1 C2 C3 C4 177.3(5) . .
N1 C2 C3 C6 179.3(4) . .
C1 C2 C3 C6 -1.7(8) . .
C2 C3 C4 O1 1.4(5) . .
C6 C3 C4 O1 -179.6(4) . .
C2 C3 C4 C5 -176.7(6) . .
C6 C3 C4 C5 2.3(9) . .
N1 O1 C4 C3 -0.7(5) . .
N1 O1 C4 C5 177.8(4) . .
C4 C3 C6 C7 -95.0(6) . .
C2 C3 C6 C7 83.8(6) . .
C3 C6 C7 C8 -96.1(6) . .
C3 C6 C7 C9 81.2(6) . .
C9 C7 C8 C8 -3.1(6) . 10_556
C6 C7 C8 C8 174.2(3) . 10_556
C8 C7 C9 C9 3.1(6) . 10_556
C6 C7 C9 C9 -174.3(3) . 10_556
N2 O2 C11 C12 -0.1(5) . .
N2 O2 C11 C10 179.3(4) . .
O2 C11 C12 C13 0.3(5) . .
C10 C11 C12 C13 -179.0(6) . .
O2 C11 C12 C15 179.1(4) . .
C10 C11 C12 C15 -0.2(9) . .
O2 N2 C13 C12 0.3(5) . .
Ag2 N2 C13 C12 -161.1(3) . .
O2 N2 C13 C14 -179.3(4) . .
Ag2 N2 C13 C14 19.3(7) . .
C11 C12 C13 N2 -0.4(5) . .
C15 C12 C13 N2 -179.2(4) . .
C11 C12 C13 C14 179.2(4) . .
C15 C12 C13 C14 0.4(8) . .
C11 C12 C15 C16 -108.8(6) . .
C13 C12 C15 C16 69.8(6) . .
C12 C15 C16 C18 -126.1(5) . 7_866
C12 C15 C16 C17 56.0(6) . .
C18 C16 C17 C18 1.4(7) 7_866 .
C15 C16 C17 C18 179.3(4) . .
C16 C17 C18 C16 -1.5(8) . 7_866
C103 O7 C101 C102 -179.98(3) . .
C101 O7 C103 C104 -179.89(19) . .
