#------------------------------------------------------------------------------
#$Date: 2016-03-26 14:14:05 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180253 $
#$URL: svn://www.crystallography.net/cod/cif/7/11/39/7113918.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7113918
loop_
_publ_author_name
'Li Jia'
'Qi Chen'
'Yin-Shan Meng'
'Hao-Ling Sun'
'Song Gao'
_publ_section_title
;
 Elucidation of slow magnetic relaxation in a ferromagnetic 1D dysprosium
 chain through magnetic dilution
;
_journal_name_full               Chem.Commun.
_journal_page_first              6052
_journal_paper_doi               10.1039/C4CC01368A
_journal_volume                  50
_journal_year                    2014
_chemical_formula_sum            'C33 H31 Dy N6 O11'
_chemical_formula_weight         850.14
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 108.4240(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   10.1030(9)
_cell_length_b                   23.756(2)
_cell_length_c                   14.7387(13)
_cell_measurement_reflns_used    5347
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      27.47
_cell_measurement_theta_min      2.29
_cell_volume                     3356.1(5)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'Bruker SHELXTL'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.988
_diffrn_measured_fraction_theta_max 0.988
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0350
_diffrn_reflns_av_sigmaI/netI    0.0448
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       30
_diffrn_reflns_limit_k_min       -26
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            20234
_diffrn_reflns_theta_full        27.60
_diffrn_reflns_theta_max         27.60
_diffrn_reflns_theta_min         1.69
_exptl_absorpt_coefficient_mu    2.297
_exptl_absorpt_correction_T_max  0.9137
_exptl_absorpt_correction_T_min  0.6694
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.683
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       columnar
_exptl_crystal_F_000             1700
_exptl_crystal_size_max          0.19
_exptl_crystal_size_mid          0.07
_exptl_crystal_size_min          0.04
_refine_diff_density_max         1.452
_refine_diff_density_min         -0.744
_refine_diff_density_rms         0.184
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.275
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     491
_refine_ls_number_reflns         7700
_refine_ls_number_restraints     15
_refine_ls_restrained_S_all      1.274
_refine_ls_R_factor_all          0.0747
_refine_ls_R_factor_gt           0.0492
_refine_ls_shift/su_max          0.005
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0452P)²+7.1805P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1164
_refine_ls_wR_factor_ref         0.1322
_reflns_number_gt                5462
_reflns_number_total             7700
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c4cc01368a2.cif
_cod_data_source_block           110403e_0m
_cod_original_cell_volume        3356.0(5)
_cod_original_sg_symbol_H-M      P2(1)/c
_cod_database_code               7113918
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C 0.5669(6) 0.9817(2) 0.6630(4) 0.0230(11) Uani 1 1 d .
C2 C 0.6539(6) 0.9635(2) 0.7628(4) 0.0245(12) Uani 1 1 d .
C3 C 0.5914(7) 0.9483(3) 0.8306(5) 0.0378(16) Uani 1 1 d .
H3A H 0.4955 0.9508 0.8182 0.045 Uiso 1 1 calc R
C4 C 0.6787(8) 0.9293(3) 0.9172(5) 0.0471(19) Uani 1 1 d .
H4A H 0.6388 0.9172 0.9627 0.057 Uiso 1 1 calc R
C5 C 0.8687(6) 0.9449(3) 0.8711(4) 0.0326(14) Uani 1 1 d .
C6 C 1.0220(7) 0.9460(3) 0.8952(4) 0.0360(15) Uani 1 1 d .
C7 C 1.1032(8) 0.9150(4) 0.9716(6) 0.069(3) Uani 1 1 d .
H7A H 1.0616 0.8940 1.0084 0.083 Uiso 1 1 calc R
C8 C 1.2474(9) 0.9152(5) 0.9934(7) 0.086(4) Uani 1 1 d .
H8A H 1.3017 0.8934 1.0439 0.103 Uiso 1 1 calc R
C9 C 1.3110(8) 0.9472(4) 0.9413(6) 0.064(3) Uani 1 1 d .
H9A H 1.4077 0.9487 0.9584 0.077 Uiso 1 1 calc R
C10 C 1.2303(8) 0.9767(4) 0.8644(6) 0.061(2) Uani 1 1 d .
H10A H 1.2720 0.9970 0.8269 0.073 Uiso 1 1 calc R
C11 C 1.0866(7) 0.9765(3) 0.8420(5) 0.0446(17) Uani 1 1 d .
H11A H 1.0327 0.9973 0.7900 0.054 Uiso 1 1 calc R
C12 C 0.9488(6) 0.9375(2) 0.3760(4) 0.0224(11) Uani 1 1 d .
C13 C 0.8621(6) 0.9002(2) 0.2938(4) 0.0263(12) Uani 1 1 d .
C14 C 0.9159(7) 0.8804(3) 0.2246(5) 0.0399(16) Uani 1 1 d .
H14A H 1.0067 0.8889 0.2267 0.048 Uiso 1 1 calc R
C15 C 0.8318(8) 0.8482(4) 0.1537(5) 0.052(2) Uani 1 1 d .
H15A H 0.8680 0.8334 0.1080 0.063 Uiso 1 1 calc R
C16 C 0.6548(6) 0.8579(3) 0.2146(4) 0.0300(13) Uani 1 1 d .
C17 C 0.5073(6) 0.8462(3) 0.2073(4) 0.0286(13) Uani 1 1 d .
C18 C 0.4398(8) 0.7993(3) 0.1569(5) 0.0403(17) Uani 1 1 d .
H18A H 0.4875 0.7750 0.1285 0.048 Uiso 1 1 calc R
C19 C 0.3028(7) 0.7887(3) 0.1490(5) 0.0443(18) Uani 1 1 d .
H19A H 0.2588 0.7571 0.1157 0.053 Uiso 1 1 calc R
C20 C 0.2302(7) 0.8240(3) 0.1894(5) 0.0449(18) Uani 1 1 d .
H20A H 0.1374 0.8164 0.1832 0.054 Uiso 1 1 calc R
C21 C 0.2949(8) 0.8711(4) 0.2396(6) 0.053(2) Uani 1 1 d .
H21A H 0.2460 0.8951 0.2674 0.064 Uiso 1 1 calc R
C22 C 0.4326(7) 0.8822(3) 0.2481(5) 0.0400(16) Uani 1 1 d .
H22A H 0.4759 0.9140 0.2813 0.048 Uiso 1 1 calc R
Dy1 Dy 0.75077(3) 1.005868(10) 0.49874(2) 0.02215(9) Uani 1 1 d .
N1 N 0.7928(5) 0.9619(2) 0.7822(3) 0.0259(11) Uani 1 1 d .
N2 N 0.8162(6) 0.9273(3) 0.9391(4) 0.0426(14) Uani 1 1 d .
N3 N 0.7304(5) 0.8891(2) 0.2893(3) 0.0249(10) Uani 1 1 d .
N4 N 0.7002(6) 0.8369(3) 0.1464(4) 0.0474(16) Uani 1 1 d .
O1 O 0.6293(5) 0.99225(18) 0.6045(3) 0.0332(10) Uani 1 1 d .
O2 O 0.4382(4) 0.98469(18) 0.6472(3) 0.0290(9) Uani 1 1 d .
O3 O 0.8911(4) 0.95577(19) 0.4325(3) 0.0330(10) Uani 1 1 d .
O4 O 1.0714(4) 0.94603(17) 0.3805(3) 0.0279(9) Uani 1 1 d .
O7 O 0.6375(4) 1.09268(18) 0.5126(3) 0.0307(9) Uani 1 1 d D
O8 O 0.8298(4) 1.0705(2) 0.4052(3) 0.0369(11) Uani 1 1 d D
O9 O 0.8892(4) 0.93746(18) 0.6225(3) 0.0306(9) Uani 1 1 d D
O10 O 0.6404(4) 0.91323(17) 0.4554(3) 0.0299(9) Uani 1 1 d D
O11 O 0.7438(5) 0.83492(19) 0.5984(4) 0.0432(12) Uani 1 1 d D
C23 C 0.5529(7) 0.1594(3) 0.2944(5) 0.0394(16) Uani 1 1 d .
C24 C 0.4649(7) 0.1912(3) 0.2060(5) 0.0364(15) Uani 1 1 d .
C25 C 0.5205(8) 0.2060(3) 0.1355(6) 0.0479(19) Uani 1 1 d .
H25A H 0.6101 0.1952 0.1380 0.058 Uiso 1 1 calc R
C26 C 0.4362(9) 0.2377(4) 0.0606(6) 0.056(2) Uani 1 1 d .
H26A H 0.4727 0.2501 0.0135 0.068 Uiso 1 1 calc R
C27 C 0.2575(7) 0.2332(3) 0.1227(5) 0.0332(14) Uani 1 1 d .
C28 C 0.1111(7) 0.2463(3) 0.1160(5) 0.0343(14) Uani 1 1 d .
C29 C 0.0375(7) 0.2879(3) 0.0539(5) 0.0419(17) Uani 1 1 d .
H29A H 0.0794 0.3067 0.0149 0.050 Uiso 1 1 calc R
C30 C -0.0972(8) 0.3014(3) 0.0498(6) 0.0469(18) Uani 1 1 d .
H30A H -0.1457 0.3293 0.0081 0.056 Uiso 1 1 calc R
C31 C -0.1592(8) 0.2739(4) 0.1067(6) 0.056(2) Uani 1 1 d .
H31A H -0.2498 0.2832 0.1039 0.067 Uiso 1 1 calc R
C32 C -0.0888(9) 0.2324(4) 0.1684(6) 0.061(2) Uani 1 1 d .
H32A H -0.1318 0.2133 0.2066 0.073 Uiso 1 1 calc R
C33 C 0.0476(8) 0.2193(4) 0.1728(6) 0.052(2) Uani 1 1 d .
H33A H 0.0961 0.1917 0.2152 0.063 Uiso 1 1 calc R
N5 N 0.3332(6) 0.2034(2) 0.2003(4) 0.0354(13) Uani 1 1 d .
N6 N 0.3049(6) 0.2514(3) 0.0529(4) 0.0438(15) Uani 1 1 d .
O5 O 0.5052(5) 0.1543(2) 0.3627(4) 0.0505(13) Uani 1 1 d .
O6 O 0.6687(5) 0.1431(2) 0.2917(4) 0.0538(14) Uani 1 1 d .
H10C H 0.674(9) 0.902(3) 0.405(4) 0.090(10) Uiso 1 1 d D
H9D H 0.872(9) 0.8979(12) 0.610(6) 0.090(10) Uiso 1 1 d D
H7C H 0.590(8) 1.115(3) 0.459(4) 0.090(10) Uiso 1 1 d D
H7D H 0.580(7) 1.095(4) 0.553(5) 0.090(10) Uiso 1 1 d D
H11C H 0.689(8) 0.835(3) 0.641(5) 0.090(10) Uiso 1 1 d D
H11D H 0.736(9) 0.7976(16) 0.573(6) 0.090(10) Uiso 1 1 d D
H8C H 0.777(7) 1.100(3) 0.368(6) 0.090(10) Uiso 1 1 d D
H9C H 0.850(9) 0.945(3) 0.673(5) 0.090(10) Uiso 1 1 d D
H10D H 0.663(9) 0.883(2) 0.501(4) 0.090(10) Uiso 1 1 d D
H8D H 0.916(5) 1.069(3) 0.392(6) 0.090(10) Uiso 1 1 d D
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 C1 O2 125.8(5) . .
O1 C1 C2 117.6(5) . .
O2 C1 C2 116.6(5) . .
N1 C2 C3 121.4(5) . .
N1 C2 C1 117.5(5) . .
C3 C2 C1 121.0(5) . .
C4 C3 C2 116.7(6) . .
C4 C3 H3A 121.6 . .
C2 C3 H3A 121.6 . .
N2 C4 C3 123.4(6) . .
N2 C4 H4A 118.3 . .
C3 C4 H4A 118.3 . .
N2 C5 N1 125.4(6) . .
N2 C5 C6 117.3(5) . .
N1 C5 C6 117.3(5) . .
C11 C6 C7 118.7(7) . .
C11 C6 C5 121.5(6) . .
C7 C6 C5 119.8(6) . .
C6 C7 C8 119.8(8) . .
C6 C7 H7A 120.1 . .
C8 C7 H7A 120.1 . .
C9 C8 C7 120.9(8) . .
C9 C8 H8A 119.6 . .
C7 C8 H8A 119.6 . .
C10 C9 C8 119.1(7) . .
C10 C9 H9A 120.4 . .
C8 C9 H9A 120.4 . .
C9 C10 C11 120.2(7) . .
C9 C10 H10A 119.9 . .
C11 C10 H10A 119.9 . .
C6 C11 C10 121.1(7) . .
C6 C11 H11A 119.4 . .
C10 C11 H11A 119.4 . .
O4 C12 O3 125.8(5) . .
O4 C12 C13 116.7(5) . .
O3 C12 C13 117.5(5) . .
N3 C13 C14 120.9(6) . .
N3 C13 C12 117.7(5) . .
C14 C13 C12 121.3(6) . .
C15 C14 C13 117.7(6) . .
C15 C14 H14A 121.2 . .
C13 C14 H14A 121.2 . .
N4 C15 C14 122.9(6) . .
N4 C15 H15A 118.5 . .
C14 C15 H15A 118.5 . .
N4 C16 N3 125.7(6) . .
N4 C16 C17 117.0(5) . .
N3 C16 C17 117.2(5) . .
C18 C17 C22 118.7(6) . .
C18 C17 C16 119.9(6) . .
C22 C17 C16 121.4(6) . .
C19 C18 C17 120.1(6) . .
C19 C18 H18A 120.0 . .
C17 C18 H18A 120.0 . .
C20 C19 C18 121.0(7) . .
C20 C19 H19A 119.5 . .
C18 C19 H19A 119.5 . .
C19 C20 C21 120.0(7) . .
C19 C20 H20A 120.0 . .
C21 C20 H20A 120.0 . .
C22 C21 C20 119.6(7) . .
C22 C21 H21A 120.2 . .
C20 C21 H21A 120.2 . .
C21 C22 C17 120.7(6) . .
C21 C22 H22A 119.7 . .
C17 C22 H22A 119.7 . .
O1 Dy1 O3 138.83(16) . .
O1 Dy1 O8 147.20(16) . .
O3 Dy1 O8 73.76(16) . .
O1 Dy1 O4 89.95(15) . 3_776
O3 Dy1 O4 98.34(14) . 3_776
O8 Dy1 O4 79.07(15) . 3_776
O1 Dy1 O2 100.24(15) . 3_676
O3 Dy1 O2 95.25(15) . 3_676
O8 Dy1 O2 74.67(15) . 3_676
O4 Dy1 O2 145.61(14) 3_776 3_676
O1 Dy1 O7 72.00(15) . .
O3 Dy1 O7 149.16(15) . .
O8 Dy1 O7 75.49(15) . .
O4 Dy1 O7 77.97(14) 3_776 .
O2 Dy1 O7 74.28(15) 3_676 .
O1 Dy1 O10 75.75(15) . .
O3 Dy1 O10 73.47(15) . .
O8 Dy1 O10 129.69(16) . .
O4 Dy1 O10 142.77(14) 3_776 .
O2 Dy1 O10 71.51(15) 3_676 .
O7 Dy1 O10 127.04(15) . .
O1 Dy1 O9 73.15(14) . .
O3 Dy1 O9 72.28(15) . .
O8 Dy1 O9 129.06(14) . .
O4 Dy1 O9 69.68(15) 3_776 .
O2 Dy1 O9 144.70(15) 3_676 .
O7 Dy1 O9 131.75(14) . .
O10 Dy1 O9 73.28(14) . .
C2 N1 C5 116.8(5) . .
C4 N2 C5 116.1(6) . .
C13 N3 C16 116.5(5) . .
C16 N4 C15 116.1(6) . .
C1 O1 Dy1 176.2(4) . .
C1 O2 Dy1 131.4(4) . 3_676
C12 O3 Dy1 162.9(4) . .
C12 O4 Dy1 128.7(4) . 3_776
Dy1 O7 H7C 123(5) . .
Dy1 O7 H7D 120(5) . .
H7C O7 H7D 104(3) . .
Dy1 O8 H8C 126(5) . .
Dy1 O8 H8D 127(5) . .
H8C O8 H8D 106(3) . .
Dy1 O9 H9D 118(6) . .
Dy1 O9 H9C 100(5) . .
H9D O9 H9C 104(3) . .
Dy1 O10 H10C 102(5) . .
Dy1 O10 H10D 120(6) . .
H10C O10 H10D 106(3) . .
H11C O11 H11D 105(3) . .
O6 C23 O5 126.9(7) . .
O6 C23 C24 115.2(6) . .
O5 C23 C24 117.8(6) . .
N5 C24 C25 122.2(6) . .
N5 C24 C23 117.4(6) . .
C25 C24 C23 120.3(6) . .
C24 C25 C26 116.5(7) . .
C24 C25 H25A 121.7 . .
C26 C25 H25A 121.7 . .
N6 C26 C25 122.9(7) . .
N6 C26 H26A 118.5 . .
C25 C26 H26A 118.5 . .
N6 C27 N5 125.0(6) . .
N6 C27 C28 118.2(6) . .
N5 C27 C28 116.8(6) . .
C33 C28 C29 118.7(7) . .
C33 C28 C27 120.8(6) . .
C29 C28 C27 120.5(6) . .
C30 C29 C28 120.6(7) . .
C30 C29 H29A 119.7 . .
C28 C29 H29A 119.7 . .
C31 C30 C29 120.0(7) . .
C31 C30 H30A 120.0 . .
C29 C30 H30A 120.0 . .
C30 C31 C32 120.6(8) . .
C30 C31 H31A 119.7 . .
C32 C31 H31A 119.7 . .
C31 C32 C33 119.2(8) . .
C31 C32 H32A 120.4 . .
C33 C32 H32A 120.4 . .
C28 C33 C32 121.0(7) . .
C28 C33 H33A 119.5 . .
C32 C33 H33A 119.5 . .
C24 N5 C27 116.8(6) . .
C26 N6 C27 116.4(6) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 O1 1.244(7) .
C1 O2 1.248(7) .
C1 C2 1.518(8) .
C2 N1 1.341(7) .
C2 C3 1.388(8) .
C3 C4 1.379(9) .
C3 H3A 0.9300 .
C4 N2 1.325(9) .
C4 H4A 0.9300 .
C5 N2 1.340(8) .
C5 N1 1.353(7) .
C5 C6 1.476(9) .
C6 C11 1.374(9) .
C6 C7 1.377(9) .
C7 C8 1.389(11) .
C7 H7A 0.9300 .
C8 C9 1.375(12) .
C8 H8A 0.9300 .
C9 C10 1.362(11) .
C9 H9A 0.9300 .
C10 C11 1.384(10) .
C10 H10A 0.9300 .
C11 H11A 0.9300 .
C12 O4 1.236(7) .
C12 O3 1.236(7) .
C12 C13 1.533(8) .
C13 N3 1.337(7) .
C13 C14 1.381(8) .
C14 C15 1.356(9) .
C14 H14A 0.9300 .
C15 N4 1.328(9) .
C15 H15A 0.9300 .
C16 N4 1.326(8) .
C16 N3 1.347(7) .
C16 C17 1.486(8) .
C17 C18 1.394(9) .
C17 C22 1.396(9) .
C18 C19 1.375(9) .
C18 H18A 0.9300 .
C19 C20 1.368(10) .
C19 H19A 0.9300 .
C20 C21 1.386(10) .
C20 H20A 0.9300 .
C21 C22 1.382(9) .
C21 H21A 0.9300 .
C22 H22A 0.9300 .
Dy1 O1 2.291(4) .
Dy1 O3 2.292(4) .
Dy1 O8 2.364(4) .
Dy1 O4 2.383(4) 3_776
Dy1 O2 2.393(4) 3_676
Dy1 O7 2.398(4) .
Dy1 O10 2.458(4) .
Dy1 O9 2.512(4) .
O2 Dy1 2.393(4) 3_676
O4 Dy1 2.383(4) 3_776
O7 H7C 0.96(2) .
O7 H7D 0.96(2) .
O8 H8C 0.95(2) .
O8 H8D 0.95(2) .
O9 H9D 0.96(2) .
O9 H9C 0.96(2) .
O10 H10C 0.95(2) .
O10 H10D 0.95(2) .
O11 H11C 0.96(2) .
O11 H11D 0.96(2) .
C23 O6 1.245(8) .
C23 O5 1.252(8) .
C23 C24 1.525(9) .
C24 N5 1.338(8) .
C24 C25 1.374(9) .
C25 C26 1.386(10) .
C25 H25A 0.9300 .
C26 N6 1.336(9) .
C26 H26A 0.9300 .
C27 N6 1.336(8) .
C27 N5 1.357(8) .
C27 C28 1.483(9) .
C28 C33 1.367(10) .
C28 C29 1.390(9) .
C29 C30 1.381(9) .
C29 H29A 0.9300 .
C30 C31 1.362(11) .
C30 H30A 0.9300 .
C31 C32 1.377(11) .
C31 H31A 0.9300 .
C32 C33 1.393(10) .
C32 H32A 0.9300 .
C33 H33A 0.9300 .
