#------------------------------------------------------------------------------
#$Date: 2016-03-26 14:23:56 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180260 $
#$URL: svn://www.crystallography.net/cod/cif/7/11/46/7114699.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7114699
loop_
_publ_author_name
'Femoni, Cristina'
'Carmela Iapalucci, M.'
'Longoni, Giuliano'
'Svensson, Per H.'
_publ_contact_author             'Prof. Giuliano Longoni'
_publ_section_title
;
 New high-nuclearity Ni--Pt carbonyl clusters: synthesis and X-ray
 structure of the ordered [Ni24Pt14(CO)44]4-- and the substitutionally
 Ni/Pt disordered [Ni10(Ni6--xPtx)Pt8(CO)30]4-- (x = 1.92) tetraanions
;
_journal_issue                   18
_journal_name_full               'Chemical Communications'
_journal_page_first              1776
_journal_paper_doi               10.1039/b103610f
_journal_year                    2001
_chemical_formula_sum            'C97 H150 N4 Ni14.08 O31 Pt9.92'
_chemical_formula_weight         4630.48
_chemical_name_systematic
; 
? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 98.4040(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   26.7155(9)
_cell_length_b                   15.2758(5)
_cell_length_c                   31.9982(11)
_cell_measurement_reflns_used    80
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      66.33
_cell_measurement_theta_min      1.25
_cell_volume                     12918.3(8)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      193(2)
_diffrn_measured_fraction_theta_full 0.986
_diffrn_measured_fraction_theta_max 0.986
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1347
_diffrn_reflns_av_sigmaI/netI    0.1195
_diffrn_reflns_limit_h_max       31
_diffrn_reflns_limit_h_min       -31
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       37
_diffrn_reflns_limit_l_min       -37
_diffrn_reflns_number            111119
_diffrn_reflns_theta_full        24.81
_diffrn_reflns_theta_max         24.81
_diffrn_reflns_theta_min         0.93
_exptl_absorpt_coefficient_mu    12.755
_exptl_absorpt_correction_T_max  0.246
_exptl_absorpt_correction_T_min  0.003
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    2.381
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       hexagonal
_exptl_crystal_F_000             8705
_exptl_crystal_size_max          0.43
_exptl_crystal_size_mid          0.21
_exptl_crystal_size_min          0.11
_refine_diff_density_max         2.158
_refine_diff_density_min         -1.788
_refine_diff_density_rms         0.264
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.888
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     751
_refine_ls_number_reflns         21957
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.888
_refine_ls_R_factor_all          0.1257
_refine_ls_R_factor_gt           0.0458
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0378P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0924
_refine_ls_wR_factor_ref         0.1162
_reflns_number_gt                10701
_reflns_number_total             21957
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b103610f.txt
_cod_data_source_block           mon
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/usr/data/users/saulius/automatic-downloads/retrospective/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 
;
_cod_original_sg_symbol_H-M      P2(1)/n
_cod_database_code               7114699
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Pt1 Pt 0.48951(2) 0.17654(3) 0.19329(2) 0.01791(15) Uani 1 1 d .
Pt2 Pt 0.50582(2) 0.11856(3) 0.27151(2) 0.01888(15) Uani 1 1 d .
Pt3 Pt 0.53975(2) 0.01557(4) 0.20912(2) 0.02804(17) Uani 1 1 d .
Pt4 Pt 0.52074(2) 0.06448(4) 0.34979(2) 0.02586(16) Uani 1 1 d .
Pt5 Pt 0.47214(2) 0.23805(4) 0.11610(2) 0.02214(16) Uani 1 1 d .
Pt6 Pt 0.45684(2) 0.27766(4) 0.25673(2) 0.02651(17) Uani 1 1 d .
Pt7 Pt 0.58902(2) 0.17358(4) 0.23426(2) 0.02198(16) Uani 1 1 d .
Pt8 Pt 0.43524(2) 0.02862(4) 0.21284(2) 0.02208(16) Uani 1 1 d .
Ni1 Ni 0.44037(6) 0.33745(11) 0.17681(6) 0.0189(5) Uani 1 1 d .
Pt9 Pt 0.52139(4) 0.08044(6) 0.13057(4) 0.0255(4) Uani 0.443(2) 1 d P
Ni2 Ni 0.52139(4) 0.08044(6) 0.13057(4) 0.0255(4) Uani 0.56 1 d P
Pt10 Pt 0.57070(4) 0.23651(7) 0.15505(4) 0.0251(4) Uani 0.349(2) 1 d P
Ni3 Ni 0.57070(4) 0.23651(7) 0.15505(4) 0.0251(4) Uani 0.65 1 d P
Pt11 Pt 0.55512(4) -0.03472(7) 0.28918(4) 0.0280(5) Uani 0.319(2) 1 d P
Ni4 Ni 0.55512(4) -0.03472(7) 0.28918(4) 0.0280(5) Uani 0.68 1 d P
Pt12 Pt 0.60438(5) 0.11751(8) 0.31492(4) 0.0294(5) Uani 0.297(2) 1 d P
Ni5 Ni 0.60438(5) 0.11751(8) 0.31492(4) 0.0294(5) Uani 0.70 1 d P
Pt13 Pt 0.45304(4) -0.02657(8) 0.29305(4) 0.0283(5) Uani 0.297(2) 1 d P
Ni6 Ni 0.45304(4) -0.02657(8) 0.29305(4) 0.0283(5) Uani 0.70 1 d P
Pt14 Pt 0.42013(5) 0.09312(8) 0.13428(5) 0.0287(6) Uani 0.216(2) 1 d P
Ni7 Ni 0.42013(5) 0.09312(8) 0.13428(5) 0.0287(6) Uani 0.78 1 d P
Ni8 Ni 0.55265(7) 0.27119(11) 0.29562(6) 0.0213(5) Uani 1 1 d .
Ni9 Ni 0.53676(7) 0.32879(11) 0.22049(6) 0.0203(5) Uani 1 1 d .
Ni10 Ni 0.47121(7) 0.21939(11) 0.33673(6) 0.0216(5) Uani 1 1 d .
Ni11 Ni 0.39000(7) 0.18966(11) 0.19966(7) 0.0217(5) Uani 1 1 d .
Ni12 Ni 0.40560(7) 0.13415(11) 0.27442(7) 0.0214(5) Uani 1 1 d .
Ni13 Ni 0.42015(7) 0.08409(12) 0.34917(7) 0.0270(5) Uani 1 1 d .
Ni14 Ni 0.51692(7) 0.38920(11) 0.14632(7) 0.0254(5) Uani 1 1 d .
Ni15 Ni 0.56295(7) 0.21990(13) 0.37105(7) 0.0293(5) Uani 1 1 d .
Ni16 Ni 0.37386(7) 0.25159(12) 0.12776(7) 0.0275(5) Uani 1 1 d .
O1 O 0.3943(4) -0.1465(7) 0.2344(4) 0.045(3) Uiso 1 1 d .
O2 O 0.3624(4) -0.0654(7) 0.1456(4) 0.038(3) Uiso 1 1 d .
O3 O 0.2955(4) 0.1342(6) 0.1506(4) 0.037(3) Uiso 1 1 d .
O4 O 0.6959(4) 0.1427(7) 0.2776(4) 0.044(3) Uiso 1 1 d .
O5 O 0.6775(4) 0.2085(7) 0.1871(4) 0.048(3) Uiso 1 1 d .
O6 O 0.5472(4) 0.5095(7) 0.0836(4) 0.055(4) Uiso 1 1 d .
O7 O 0.6447(4) 0.3289(7) 0.3484(4) 0.050(3) Uiso 1 1 d .
O8 O 0.4275(5) 0.4654(8) 0.2399(4) 0.058(4) Uiso 1 1 d .
O9 O 0.6063(4) 0.2833(7) 0.0761(4) 0.056(4) Uiso 1 1 d .
O10 O 0.3861(5) 0.0659(8) 0.0451(5) 0.063(4) Uiso 1 1 d .
O11 O 0.5579(4) 0.4604(7) 0.2870(4) 0.040(3) Uiso 1 1 d .
O12 O 0.4210(5) 0.3840(8) 0.3250(4) 0.060(4) Uiso 1 1 d .
O13 O 0.5985(5) -0.1496(8) 0.3574(4) 0.064(4) Uiso 1 1 d .
O14 O 0.5770(4) -0.0838(6) 0.1394(3) 0.033(3) Uiso 1 1 d .
O15 O 0.4453(4) -0.1586(7) 0.3565(4) 0.050(3) Uiso 1 1 d .
O16 O 0.3240(4) 0.0297(7) 0.2986(4) 0.041(3) Uiso 1 1 d .
O17 O 0.3140(4) 0.2373(7) 0.2523(4) 0.041(3) Uiso 1 1 d .
O18 O 0.5941(4) -0.1522(7) 0.2297(4) 0.039(3) Uiso 1 1 d .
O19 O 0.4981(6) 0.3349(10) 0.4095(5) 0.097(5) Uiso 1 1 d .
O20 O 0.3371(4) 0.4082(8) 0.1645(4) 0.057(4) Uiso 1 1 d .
O21 O 0.6115(4) 0.4486(7) 0.1979(4) 0.044(3) Uiso 1 1 d .
O22 O 0.6316(6) 0.2145(10) 0.4515(5) 0.095(5) Uiso 1 1 d .
O23 O 0.3863(4) 0.2418(7) 0.3843(4) 0.056(4) Uiso 1 1 d .
O24 O 0.5341(5) 0.0725(8) 0.0411(5) 0.063(4) Uiso 1 1 d .
O25 O 0.3117(5) 0.2780(8) 0.0444(5) 0.072(4) Uiso 1 1 d .
O26 O 0.4358(4) 0.5159(7) 0.1435(4) 0.051(3) Uiso 1 1 d .
O27 O 0.6758(5) 0.0537(9) 0.3861(5) 0.076(4) Uiso 1 1 d .
O28 O 0.4561(4) 0.3298(7) 0.0337(4) 0.054(4) Uiso 1 1 d .
O29 O 0.5415(6) 0.0162(10) 0.4412(6) 0.096(5) Uiso 1 1 d .
O30 O 0.3890(5) -0.0041(8) 0.4231(5) 0.070(4) Uiso 1 1 d .
C1 C 0.4158(5) -0.0778(9) 0.2434(5) 0.024(4) Uiso 1 1 d .
C2 C 0.3920(5) -0.0096(9) 0.1604(5) 0.025(4) Uiso 1 1 d .
C3 C 0.3344(5) 0.1696(9) 0.1578(5) 0.022(4) Uiso 1 1 d .
C4 C 0.6509(5) 0.1447(9) 0.2750(5) 0.023(4) Uiso 1 1 d .
C5 C 0.6319(5) 0.2078(9) 0.1913(5) 0.026(4) Uiso 1 1 d .
C6 C 0.5365(6) 0.4593(10) 0.1085(5) 0.034(4) Uiso 1 1 d .
C7 C 0.6055(6) 0.2912(10) 0.3370(5) 0.034(4) Uiso 1 1 d .
C8 C 0.4367(6) 0.3914(10) 0.2307(5) 0.032(4) Uiso 1 1 d .
C9 C 0.5910(6) 0.2669(11) 0.1083(6) 0.044(5) Uiso 1 1 d .
C10 C 0.4004(6) 0.0782(10) 0.0801(6) 0.033(4) Uiso 1 1 d .
C11 C 0.5520(6) 0.3876(10) 0.2733(6) 0.036(4) Uiso 1 1 d .
C12 C 0.4415(6) 0.3226(11) 0.3117(6) 0.041(5) Uiso 1 1 d .
C13 C 0.5812(6) -0.1062(11) 0.3294(6) 0.044(5) Uiso 1 1 d .
C14 C 0.5568(5) -0.0258(9) 0.1533(5) 0.023(4) Uiso 1 1 d .
C15 C 0.4481(6) -0.1044(10) 0.3318(6) 0.036(4) Uiso 1 1 d .
C16 C 0.3630(6) 0.0663(9) 0.3015(5) 0.029(4) Uiso 1 1 d .
C17 C 0.3524(6) 0.2027(9) 0.2454(5) 0.032(4) Uiso 1 1 d .
C18 C 0.5729(6) -0.0894(9) 0.2389(5) 0.030(4) Uiso 1 1 d .
C19 C 0.5069(7) 0.2797(13) 0.3872(7) 0.062(6) Uiso 1 1 d .
C20 C 0.3667(6) 0.3538(10) 0.1585(5) 0.035(4) Uiso 1 1 d .
C21 C 0.5741(6) 0.4029(10) 0.1946(5) 0.032(4) Uiso 1 1 d .
C22 C 0.6030(7) 0.2133(12) 0.4189(7) 0.055(6) Uiso 1 1 d .
C23 C 0.4133(6) 0.1989(10) 0.3646(6) 0.037(4) Uiso 1 1 d .
C24 C 0.5281(7) 0.0737(12) 0.0766(7) 0.054(5) Uiso 1 1 d .
C25 C 0.3367(7) 0.2677(11) 0.0765(6) 0.047(5) Uiso 1 1 d .
C26 C 0.4552(6) 0.4470(10) 0.1517(5) 0.034(4) Uiso 1 1 d .
C27 C 0.6479(7) 0.0784(11) 0.3572(6) 0.047(5) Uiso 1 1 d .
C28 C 0.4637(6) 0.2955(10) 0.0677(6) 0.041(5) Uiso 1 1 d .
C29 C 0.5319(8) 0.0346(13) 0.4047(8) 0.068(6) Uiso 1 1 d .
C30 C 0.4008(6) 0.0298(11) 0.3926(6) 0.042(5) Uiso 1 1 d .
C31 C 0.2143(5) 0.0619(9) 0.2165(5) 0.031(4) Uiso 1 1 d .
H31A H 0.2156 0.0635 0.1864 0.037 Uiso 1 1 calc R
H31B H 0.2460 0.0859 0.2306 0.037 Uiso 1 1 calc R
C32 C 0.2880(6) 0.4670(10) 0.2706(6) 0.045(5) Uiso 1 1 d .
H32A H 0.2820 0.4625 0.2401 0.053 Uiso 1 1 calc R
H32B H 0.3214 0.4438 0.2805 0.053 Uiso 1 1 calc R
C33 C 0.2503(6) -0.0852(10) 0.2114(5) 0.036(4) Uiso 1 1 d .
H33A H 0.2547 -0.1403 0.2266 0.044 Uiso 1 1 calc R
H33B H 0.2823 -0.0542 0.2166 0.044 Uiso 1 1 calc R
C34 C 0.2389(7) -0.1052(11) 0.1647(6) 0.057(6) Uiso 1 1 d .
H34A H 0.2660 -0.1392 0.1564 0.086 Uiso 1 1 calc R
H34B H 0.2357 -0.0514 0.1490 0.086 Uiso 1 1 calc R
H34C H 0.2079 -0.1376 0.1591 0.086 Uiso 1 1 calc R
C35 C 0.3146(6) -0.2823(9) 0.2856(5) 0.028(4) Uiso 1 1 d .
H35A H 0.3376 -0.2428 0.2742 0.033 Uiso 1 1 calc R
H35B H 0.2809 -0.2701 0.2709 0.033 Uiso 1 1 calc R
C36 C 0.3153(6) -0.2595(9) 0.3322(5) 0.032(4) Uiso 1 1 d .
H36A H 0.2973 -0.3044 0.3454 0.039 Uiso 1 1 calc R
H36B H 0.3500 -0.2586 0.3462 0.039 Uiso 1 1 calc R
C37 C 0.2089(6) 0.3282(10) 0.1625(6) 0.043(5) Uiso 1 1 d .
H37A H 0.2426 0.3283 0.1786 0.052 Uiso 1 1 calc R
H37B H 0.1894 0.3731 0.1743 0.052 Uiso 1 1 calc R
C38 C 0.2126(7) 0.3517(12) 0.1166(6) 0.060(6) Uiso 1 1 d .
H38A H 0.2285 0.4079 0.1156 0.091 Uiso 1 1 calc R
H38B H 0.1793 0.3536 0.1006 0.091 Uiso 1 1 calc R
H38C H 0.2325 0.3082 0.1048 0.091 Uiso 1 1 calc R
C39 C 0.3777(6) 0.5969(10) 0.3026(5) 0.038(4) Uiso 1 1 d .
H39A H 0.3838 0.5352 0.2980 0.046 Uiso 1 1 calc R
H39B H 0.3734 0.6042 0.3319 0.046 Uiso 1 1 calc R
C40 C 0.4248(5) -0.3510(10) 0.2945(5) 0.033(4) Uiso 1 1 d .
H40A H 0.4177 -0.2888 0.2946 0.040 Uiso 1 1 calc R
H40B H 0.4337 -0.3663 0.2671 0.040 Uiso 1 1 calc R
C41 C 0.4704(6) -0.3732(11) 0.3303(6) 0.054(5) Uiso 1 1 d .
H41A H 0.4623 -0.3538 0.3573 0.065 Uiso 1 1 calc R
H41B H 0.4755 -0.4360 0.3316 0.065 Uiso 1 1 calc R
C42 C 0.5187(7) -0.3292(12) 0.3219(6) 0.063(6) Uiso 1 1 d .
H42A H 0.5456 -0.3437 0.3440 0.095 Uiso 1 1 calc R
H42B H 0.5139 -0.2669 0.3210 0.095 Uiso 1 1 calc R
H42C H 0.5271 -0.3491 0.2953 0.095 Uiso 1 1 calc R
C43 C 0.3361(5) 0.6194(9) 0.2276(5) 0.029(4) Uiso 1 1 d .
H43A H 0.3611 0.6629 0.2225 0.035 Uiso 1 1 calc R
H43B H 0.3495 0.5623 0.2219 0.035 Uiso 1 1 calc R
C44 C 0.2127(6) 0.1353(11) 0.3035(6) 0.047(5) Uiso 1 1 d .
H44A H 0.2276 0.1910 0.2974 0.057 Uiso 1 1 calc R
H44B H 0.2371 0.0894 0.3006 0.057 Uiso 1 1 calc R
C45 C 0.3012(7) -0.3641(12) 0.1496(6) 0.058(6) Uiso 1 1 d .
H45A H 0.3208 -0.3122 0.1455 0.069 Uiso 1 1 calc R
H45B H 0.3216 -0.4151 0.1455 0.069 Uiso 1 1 calc R
C46 C 0.2522(7) -0.3651(12) 0.1172(6) 0.070(6) Uiso 1 1 d .
H46A H 0.2608 -0.3650 0.0891 0.105 Uiso 1 1 calc R
H46B H 0.2323 -0.3142 0.1212 0.105 Uiso 1 1 calc R
H46C H 0.2330 -0.4168 0.1213 0.105 Uiso 1 1 calc R
C47 C 0.3954(6) 0.8011(10) 0.0718(5) 0.034(4) Uiso 1 1 d .
H47A H 0.4017 0.8476 0.0925 0.041 Uiso 1 1 calc R
H47B H 0.3708 0.7617 0.0811 0.041 Uiso 1 1 calc R
C48 C 0.3722(7) 0.8418(12) 0.0287(6) 0.061(6) Uiso 1 1 d .
H48A H 0.3671 0.7968 0.0071 0.074 Uiso 1 1 calc R
H48B H 0.3948 0.8858 0.0201 0.074 Uiso 1 1 calc R
C49 C 0.3203(7) -0.1155(11) 0.0347(7) 0.060(6) Uiso 1 1 d .
H49A H 0.3244 -0.0822 0.0608 0.072 Uiso 1 1 calc R
H49B H 0.3098 -0.0754 0.0116 0.072 Uiso 1 1 calc R
C50 C 0.2800(9) -0.1835(15) 0.0360(8) 0.108(9) Uiso 1 1 d .
H50A H 0.2490 -0.1555 0.0404 0.163 Uiso 1 1 calc R
H50B H 0.2904 -0.2235 0.0588 0.163 Uiso 1 1 calc R
H50C H 0.2749 -0.2149 0.0098 0.163 Uiso 1 1 calc R
C51 C 0.4365(6) 0.6757(11) 0.0375(6) 0.048(5) Uiso 1 1 d .
H51A H 0.4337 0.7017 0.0096 0.058 Uiso 1 1 calc R
H51B H 0.4665 0.6391 0.0411 0.058 Uiso 1 1 calc R
C53 C 0.3924(8) 0.5433(13) 0.0059(7) 0.074(7) Uiso 1 1 d .
H53A H 0.3940 0.5692 -0.0215 0.088 Uiso 1 1 calc R
H53B H 0.4230 0.5092 0.0136 0.088 Uiso 1 1 calc R
C52 C 0.3915(6) 0.6174(10) 0.0384(6) 0.048(5) Uiso 1 1 d .
H52A H 0.3607 0.6512 0.0317 0.058 Uiso 1 1 calc R
H52B H 0.3923 0.5928 0.0664 0.058 Uiso 1 1 calc R
C54 C 0.3481(9) 0.4831(15) 0.0022(8) 0.113(10) Uiso 1 1 d .
H54A H 0.3514 0.4394 -0.0188 0.170 Uiso 1 1 calc R
H54B H 0.3176 0.5159 -0.0060 0.170 Uiso 1 1 calc R
H54C H 0.3468 0.4553 0.0289 0.170 Uiso 1 1 calc R
C55 C 0.4870(6) 0.8128(10) 0.0597(6) 0.042(5) Uiso 1 1 d .
H55A H 0.4773 0.8341 0.0311 0.051 Uiso 1 1 calc R
H55B H 0.4886 0.8629 0.0785 0.051 Uiso 1 1 calc R
C56 C 0.5399(6) -0.2267(11) 0.0630(6) 0.048(5) Uiso 1 1 d .
H56A H 0.5383 -0.2839 0.0496 0.057 Uiso 1 1 calc R
H56B H 0.5544 -0.2336 0.0924 0.057 Uiso 1 1 calc R
C57 C 0.4273(6) 0.1647(10) -0.0407(5) 0.038(4) Uiso 1 1 d .
H57A H 0.4415 0.1599 -0.0111 0.046 Uiso 1 1 calc R
H57B H 0.4275 0.1069 -0.0532 0.046 Uiso 1 1 calc R
C58 C 0.3724(6) 0.1977(11) -0.0443(6) 0.058(6) Uiso 1 1 d .
H58A H 0.3530 0.1580 -0.0298 0.087 Uiso 1 1 calc R
H58B H 0.3580 0.2010 -0.0735 0.087 Uiso 1 1 calc R
H58C H 0.3721 0.2548 -0.0318 0.087 Uiso 1 1 calc R
C59 C 0.4600(6) 0.7078(9) 0.1142(5) 0.034(4) Uiso 1 1 d .
H59A H 0.4894 0.6715 0.1128 0.040 Uiso 1 1 calc R
H59B H 0.4327 0.6693 0.1192 0.040 Uiso 1 1 calc R
C60 C 0.4723(6) -0.2299(10) 0.1536(5) 0.042(5) Uiso 1 1 d .
H60A H 0.5004 -0.1919 0.1498 0.050 Uiso 1 1 calc R
H60B H 0.4432 -0.1934 0.1561 0.050 Uiso 1 1 calc R
C62 C 0.5332(6) -0.3431(11) 0.1949(6) 0.059(6) Uiso 1 1 d .
H62A H 0.5388 -0.3742 0.2212 0.088 Uiso 1 1 calc R
H62B H 0.5623 -0.3079 0.1921 0.088 Uiso 1 1 calc R
H62C H 0.5277 -0.3842 0.1719 0.088 Uiso 1 1 calc R
C61 C 0.4858(6) -0.2829(10) 0.1937(6) 0.043(5) Uiso 1 1 d .
H61A H 0.4570 -0.3191 0.1976 0.052 Uiso 1 1 calc R
H61B H 0.4917 -0.2428 0.2174 0.052 Uiso 1 1 calc R
C63 C 0.7195(6) -0.0701(10) 0.2430(5) 0.037(4) Uiso 1 1 d .
H63A H 0.7139 -0.0094 0.2499 0.045 Uiso 1 1 calc R
H63B H 0.6867 -0.0988 0.2391 0.045 Uiso 1 1 calc R
C64 C 0.7488(7) 0.3887(12) 0.2194(6) 0.061(6) Uiso 1 1 d .
H64A H 0.7495 0.3255 0.2226 0.074 Uiso 1 1 calc R
H64B H 0.7139 0.4077 0.2182 0.074 Uiso 1 1 calc R
C66 C 0.7356(8) 0.3759(14) 0.1371(8) 0.102(9) Uiso 1 1 d .
H66A H 0.7506 0.3949 0.1131 0.153 Uiso 1 1 calc R
H66B H 0.7015 0.3974 0.1346 0.153 Uiso 1 1 calc R
H66C H 0.7354 0.3131 0.1381 0.153 Uiso 1 1 calc R
C65 C 0.7675(8) 0.4128(13) 0.1790(7) 0.070(6) Uiso 1 1 d .
H65A H 0.8020 0.3922 0.1804 0.084 Uiso 1 1 calc R
H65B H 0.7683 0.4762 0.1770 0.084 Uiso 1 1 calc R
C67 C 0.7022(7) -0.0228(12) 0.1669(6) 0.059(6) Uiso 1 1 d .
H67A H 0.6684 -0.0432 0.1693 0.071 Uiso 1 1 calc R
H67B H 0.7036 0.0389 0.1742 0.071 Uiso 1 1 calc R
C68 C 0.7097(7) -0.0309(12) 0.1209(6) 0.061(6) Uiso 1 1 d .
H68A H 0.7011 -0.0900 0.1113 0.073 Uiso 1 1 calc R
H68B H 0.7451 -0.0215 0.1188 0.073 Uiso 1 1 calc R
C70 C 0.7028(8) 0.1208(13) 0.0892(8) 0.093(8) Uiso 1 1 d .
H70A H 0.6821 0.1606 0.0709 0.139 Uiso 1 1 calc R
H70B H 0.7342 0.1116 0.0785 0.139 Uiso 1 1 calc R
H70C H 0.7095 0.1452 0.1171 0.139 Uiso 1 1 calc R
C69 C 0.6763(8) 0.0369(13) 0.0907(7) 0.084(7) Uiso 1 1 d .
H69A H 0.6691 0.0126 0.0624 0.100 Uiso 1 1 calc R
H69B H 0.6443 0.0464 0.1009 0.100 Uiso 1 1 calc R
C71 C 0.7539(6) 0.3339(10) 0.3141(6) 0.039(4) Uiso 1 1 d .
H71A H 0.7388 0.3357 0.3399 0.047 Uiso 1 1 calc R
H71B H 0.7299 0.3051 0.2929 0.047 Uiso 1 1 calc R
C72 C 0.6991(6) -0.2223(10) 0.1778(6) 0.048(5) Uiso 1 1 d .
H72A H 0.6709 -0.1874 0.1643 0.057 Uiso 1 1 calc R
H72B H 0.6906 -0.2436 0.2044 0.057 Uiso 1 1 calc R
C73 C 0.7921(7) 0.1992(11) 0.3509(6) 0.057(6) Uiso 1 1 d .
H73A H 0.7859 0.2211 0.3781 0.068 Uiso 1 1 calc R
H73B H 0.7622 0.1676 0.3383 0.068 Uiso 1 1 calc R
C74 C 0.8372(7) 0.1358(12) 0.3576(7) 0.075(7) Uiso 1 1 d .
H74A H 0.8299 0.0884 0.3754 0.112 Uiso 1 1 calc R
H74B H 0.8668 0.1663 0.3708 0.112 Uiso 1 1 calc R
H74C H 0.8433 0.1132 0.3308 0.112 Uiso 1 1 calc R
C75 C 0.7088(6) 0.4723(10) 0.2952(6) 0.040(5) Uiso 1 1 d .
H75A H 0.6981 0.4751 0.3228 0.048 Uiso 1 1 calc R
H75B H 0.6847 0.4357 0.2775 0.048 Uiso 1 1 calc R
C77 C 0.6559(7) 0.6085(12) 0.2802(7) 0.067(6) Uiso 1 1 d .
H77A H 0.6396 0.6261 0.2524 0.081 Uiso 1 1 calc R
H77B H 0.6340 0.5668 0.2915 0.081 Uiso 1 1 calc R
C76 C 0.7060(7) 0.5650(12) 0.2764(7) 0.069(6) Uiso 1 1 d .
H76A H 0.7333 0.6002 0.2910 0.083 Uiso 1 1 calc R
H76B H 0.7102 0.5620 0.2468 0.083 Uiso 1 1 calc R
C78 C 0.6621(11) 0.6788(18) 0.3054(10) 0.153(13) Uiso 1 1 d .
H78A H 0.6297 0.7040 0.3077 0.229 Uiso 1 1 calc R
H78B H 0.6827 0.7211 0.2938 0.229 Uiso 1 1 calc R
H78C H 0.6784 0.6616 0.3330 0.229 Uiso 1 1 calc R
N1 N 0.1715(4) 0.1238(7) 0.2254(4) 0.025(3) Uiso 1 1 d .
N4 N 0.3968(9) 0.2694(15) 0.5142(8) 0.115(8) Uiso 1 1 d .
N2 N 0.4450(5) 0.7506(8) 0.0705(4) 0.035(3) Uiso 1 1 d .
N3 N 0.7398(5) -0.0720(8) 0.2002(4) 0.038(4) Uiso 1 1 d .
C79 C 0.5490(12) -0.228(2) 0.4760(11) 0.141(13) Uiso 1 1 d .
H79A H 0.5508 -0.1881 0.4528 0.169 Uiso 1 1 calc R
H79B H 0.5272 -0.2757 0.4645 0.169 Uiso 1 1 calc R
C80 C 0.527(2) -0.193(4) 0.4974(19) 0.37(4) Uiso 1 1 d .
H80A H 0.5468 -0.1436 0.5099 0.446 Uiso 1 1 calc R
H80B H 0.5212 -0.2317 0.5202 0.446 Uiso 1 1 calc R
C81 C 0.4686(11) -0.1535(18) 0.4730(10) 0.136(12) Uiso 1 1 d .
H81A H 0.4561 -0.1107 0.4914 0.164 Uiso 1 1 calc R
H81B H 0.4733 -0.1240 0.4471 0.164 Uiso 1 1 calc R
C82 C 0.4308(10) -0.2212(16) 0.4633(9) 0.129(11) Uiso 1 1 d .
H82A H 0.3995 -0.1952 0.4508 0.194 Uiso 1 1 calc R
H82B H 0.4260 -0.2510 0.4888 0.194 Uiso 1 1 calc R
H82C H 0.4420 -0.2622 0.4439 0.194 Uiso 1 1 calc R
C83 C 0.3573(19) 0.213(3) 0.5255(16) 0.29(3) Uiso 1 1 d .
H83A H 0.3636 0.2049 0.5559 0.353 Uiso 1 1 calc R
H83B H 0.3255 0.2445 0.5192 0.353 Uiso 1 1 calc R
C84 C 0.3501(10) 0.1275(17) 0.5064(9) 0.113(10) Uiso 1 1 d .
H84A H 0.3531 0.1360 0.4768 0.135 Uiso 1 1 calc R
H84B H 0.3795 0.0935 0.5183 0.135 Uiso 1 1 calc R
C85 C 0.3093(13) 0.073(2) 0.5067(11) 0.171(14) Uiso 1 1 d .
H85A H 0.2824 0.1000 0.4874 0.205 Uiso 1 1 calc R
H85B H 0.2999 0.0803 0.5347 0.205 Uiso 1 1 calc R
C86 C 0.3027(11) -0.0201(19) 0.4984(10) 0.161(14) Uiso 1 1 d .
H86A H 0.2688 -0.0369 0.5016 0.241 Uiso 1 1 calc R
H86B H 0.3263 -0.0525 0.5181 0.241 Uiso 1 1 calc R
H86C H 0.3085 -0.0325 0.4701 0.241 Uiso 1 1 calc R
C87 C 0.3993(12) 0.335(2) 0.5550(11) 0.159(13) Uiso 1 1 d .
H87A H 0.4124 0.2973 0.5785 0.191 Uiso 1 1 calc R
H87B H 0.4271 0.3739 0.5514 0.191 Uiso 1 1 calc R
C88 C 0.3646(16) 0.392(3) 0.5730(14) 0.24(2) Uiso 1 1 d .
H88A H 0.3434 0.3532 0.5870 0.290 Uiso 1 1 calc R
H88B H 0.3427 0.4167 0.5491 0.290 Uiso 1 1 calc R
C89 C 0.3782(14) 0.466(2) 0.6029(12) 0.186(16) Uiso 1 1 d .
H89A H 0.3471 0.4963 0.6065 0.223 Uiso 1 1 calc R
H89B H 0.3917 0.4414 0.6302 0.223 Uiso 1 1 calc R
C90 C 0.4110(18) 0.526(3) 0.5931(15) 0.31(3) Uiso 1 1 d .
H90A H 0.4170 0.5683 0.6153 0.458 Uiso 1 1 calc R
H90B H 0.3973 0.5540 0.5671 0.458 Uiso 1 1 calc R
H90C H 0.4422 0.4973 0.5897 0.458 Uiso 1 1 calc R
C91 C 0.3875(14) 0.326(2) 0.4763(13) 0.194(17) Uiso 1 1 d .
H91A H 0.3942 0.2909 0.4524 0.233 Uiso 1 1 calc R
H91B H 0.3518 0.3399 0.4717 0.233 Uiso 1 1 calc R
C92 C 0.4116(15) 0.397(2) 0.4753(13) 0.211(19) Uiso 1 1 d .
H92A H 0.4469 0.3854 0.4736 0.253 Uiso 1 1 calc R
H92B H 0.4094 0.4311 0.5005 0.253 Uiso 1 1 calc R
C93 C 0.3825(14) 0.455(2) 0.4286(12) 0.196(17) Uiso 1 1 d .
H93A H 0.3853 0.4247 0.4025 0.235 Uiso 1 1 calc R
H93B H 0.3477 0.4718 0.4298 0.235 Uiso 1 1 calc R
C94 C 0.4200(15) 0.533(2) 0.4373(13) 0.25(2) Uiso 1 1 d .
H94A H 0.4120 0.5767 0.4158 0.375 Uiso 1 1 calc R
H94B H 0.4539 0.5124 0.4370 0.375 Uiso 1 1 calc R
H94C H 0.4173 0.5580 0.4644 0.375 Uiso 1 1 calc R
C96 C 0.2822(17) 0.579(3) 0.4945(17) 0.198(18) Uiso 1 1 d .
C97 C 0.2715(12) 0.639(2) 0.5241(11) 0.173(15) Uiso 1 1 d .
H97A H 0.2803 0.6154 0.5519 0.259 Uiso 1 1 calc R
H97B H 0.2360 0.6528 0.5193 0.259 Uiso 1 1 calc R
H97C H 0.2906 0.6918 0.5216 0.259 Uiso 1 1 calc R
C95 C 0.2734(14) 0.599(3) 0.4472(14) 0.25(2) Uiso 1 1 d .
H95A H 0.2832 0.5499 0.4318 0.374 Uiso 1 1 calc R
H95B H 0.2933 0.6493 0.4418 0.374 Uiso 1 1 calc R
H95C H 0.2382 0.6118 0.4384 0.374 Uiso 1 1 calc R
O31 O 0.2906(11) 0.503(2) 0.5035(10) 0.231(14) Uiso 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Pt5 Pt1 Pt2 178.46(3) . .
Pt5 Pt1 Ni11 90.22(5) . .
Pt2 Pt1 Ni11 88.92(5) . .
Pt5 Pt1 Pt9 61.95(3) . .
Pt2 Pt1 Pt9 119.59(3) . .
Ni11 Pt1 Pt9 120.85(5) . .
Pt5 Pt1 Ni9 90.29(5) . .
Pt2 Pt1 Ni9 88.79(5) . .
Ni11 Pt1 Ni9 109.09(6) . .
Pt9 Pt1 Ni9 121.01(5) . .
Pt5 Pt1 Pt14 60.75(3) . .
Pt2 Pt1 Pt14 119.82(4) . .
Ni11 Pt1 Pt14 61.03(5) . .
Pt9 Pt1 Pt14 59.82(4) . .
Ni9 Pt1 Pt14 147.79(6) . .
Pt5 Pt1 Pt7 118.34(3) . .
Pt2 Pt1 Pt7 62.16(2) . .
Ni11 Pt1 Pt7 147.84(5) . .
Pt9 Pt1 Pt7 87.61(3) . .
Ni9 Pt1 Pt7 59.91(4) . .
Pt14 Pt1 Pt7 144.50(4) . .
Pt5 Pt1 Pt6 117.14(3) . .
Pt2 Pt1 Pt6 61.32(2) . .
Ni11 Pt1 Pt6 59.23(5) . .
Pt9 Pt1 Pt6 179.01(3) . .
Ni9 Pt1 Pt6 58.35(4) . .
Pt14 Pt1 Pt6 120.23(4) . .
Pt7 Pt1 Pt6 92.58(3) . .
Pt5 Pt1 Pt10 60.78(3) . .
Pt2 Pt1 Pt10 119.70(3) . .
Ni11 Pt1 Pt10 147.47(5) . .
Pt9 Pt1 Pt10 60.51(3) . .
Ni9 Pt1 Pt10 60.51(5) . .
Pt14 Pt1 Pt10 109.80(4) . .
Pt7 Pt1 Pt10 57.56(3) . .
Pt6 Pt1 Pt10 118.83(3) . .
Pt4 Pt2 Pt1 178.51(3) . .
Pt4 Pt2 Ni12 90.45(5) . .
Pt1 Pt2 Ni12 88.62(5) . .
Pt4 Pt2 Ni8 89.98(5) . .
Pt1 Pt2 Ni8 89.23(5) . .
Ni12 Pt2 Ni8 109.48(6) . .
Pt4 Pt2 Pt11 61.60(3) . .
Pt1 Pt2 Pt11 119.88(4) . .
Ni12 Pt2 Pt11 121.56(5) . .
Ni8 Pt2 Pt11 119.72(5) . .
Pt4 Pt2 Pt6 116.33(3) . .
Pt1 Pt2 Pt6 62.19(2) . .
Ni12 Pt2 Pt6 58.84(4) . .
Ni8 Pt2 Pt6 58.62(4) . .
Pt11 Pt2 Pt6 177.67(4) . .
Pt4 Pt2 Pt13 61.30(3) . .
Pt1 Pt2 Pt13 119.14(4) . .
Ni12 Pt2 Pt13 61.23(5) . .
Ni8 Pt2 Pt13 148.28(6) . .
Pt11 Pt2 Pt13 60.32(4) . .
Pt6 Pt2 Pt13 120.02(3) . .
Pt4 Pt2 Pt12 61.34(3) . .
Pt1 Pt2 Pt12 119.23(4) . .
Ni12 Pt2 Pt12 148.25(6) . .
Ni8 Pt2 Pt12 59.98(5) . .
Pt11 Pt2 Pt12 59.74(4) . .
Pt6 Pt2 Pt12 118.56(3) . .
Pt13 Pt2 Pt12 110.44(4) . .
Pt4 Pt2 Pt3 119.14(3) . .
Pt1 Pt2 Pt3 62.34(2) . .
Ni12 Pt2 Pt3 120.03(5) . .
Ni8 Pt2 Pt3 120.29(4) . .
Pt11 Pt2 Pt3 57.55(3) . .
Pt6 Pt2 Pt3 124.53(3) . .
Pt13 Pt2 Pt3 87.55(3) . .
Pt12 Pt2 Pt3 88.36(3) . .
C18 Pt3 C14 91.6(6) . .
C18 Pt3 Pt11 46.6(5) . .
C14 Pt3 Pt11 138.2(4) . .
C18 Pt3 Pt9 138.5(5) . .
C14 Pt3 Pt9 46.9(4) . .
Pt11 Pt3 Pt9 174.80(4) . .
C18 Pt3 Pt2 106.1(5) . .
C14 Pt3 Pt2 162.1(4) . .
Pt11 Pt3 Pt2 59.53(3) . .
Pt9 Pt3 Pt2 115.33(3) . .
C18 Pt3 Pt7 113.3(4) . .
C14 Pt3 Pt7 111.6(4) . .
Pt11 Pt3 Pt7 88.41(4) . .
Pt9 Pt3 Pt7 87.98(3) . .
Pt2 Pt3 Pt7 59.95(2) . .
C18 Pt3 Pt1 162.1(5) . .
C14 Pt3 Pt1 106.2(4) . .
Pt11 Pt3 Pt1 115.49(4) . .
Pt9 Pt3 Pt1 59.37(3) . .
Pt2 Pt3 Pt1 55.96(2) . .
Pt7 Pt3 Pt1 59.45(2) . .
C18 Pt3 Pt8 114.1(4) . .
C14 Pt3 Pt8 114.5(4) . .
Pt11 Pt3 Pt8 89.66(3) . .
Pt9 Pt3 Pt8 88.10(3) . .
Pt2 Pt3 Pt8 60.23(2) . .
Pt7 Pt3 Pt8 110.64(3) . .
Pt1 Pt3 Pt8 59.74(2) . .
C29 Pt4 Pt2 176.2(6) . .
C29 Pt4 Ni15 88.5(6) . .
Pt2 Pt4 Ni15 87.87(5) . .
C29 Pt4 Ni13 93.3(6) . .
Pt2 Pt4 Ni13 86.89(5) . .
Ni15 Pt4 Ni13 106.59(6) . .
C29 Pt4 Ni10 112.3(6) . .
Pt2 Pt4 Ni10 64.78(5) . .
Ni15 Pt4 Ni10 56.14(6) . .
Ni13 Pt4 Ni10 55.94(6) . .
C29 Pt4 Pt11 122.0(6) . .
Pt2 Pt4 Pt11 60.88(3) . .
Ni15 Pt4 Pt11 120.12(5) . .
Ni13 Pt4 Pt11 119.67(6) . .
Ni10 Pt4 Pt11 125.66(6) . .
C29 Pt4 Pt13 121.1(6) . .
Pt2 Pt4 Pt13 62.15(3) . .
Ni15 Pt4 Pt13 146.16(6) . .
Ni13 Pt4 Pt13 59.53(5) . .
Ni10 Pt4 Pt13 94.62(5) . .
Pt11 Pt4 Pt13 60.38(4) . .
C29 Pt4 Pt12 116.2(6) . .
Pt2 Pt4 Pt12 62.53(3) . .
Ni15 Pt4 Pt12 60.41(5) . .
Ni13 Pt4 Pt12 145.85(6) . .
Ni10 Pt4 Pt12 95.00(5) . .
Pt11 Pt4 Pt12 59.91(4) . .
Pt13 Pt4 Pt12 112.04(4) . .
C28 Pt5 Pt1 170.9(5) . .
C28 Pt5 Ni1 109.8(5) . .
Pt1 Pt5 Ni1 63.52(4) . .
C28 Pt5 Ni14 83.2(5) . .
Pt1 Pt5 Ni14 87.77(5) . .
Ni1 Pt5 Ni14 55.47(6) . .
C28 Pt5 Ni16 94.7(5) . .
Pt1 Pt5 Ni16 86.52(5) . .
Ni1 Pt5 Ni16 56.33(6) . .
Ni14 Pt5 Ni16 105.74(6) . .
C28 Pt5 Pt14 126.1(5) . .
Pt1 Pt5 Pt14 62.11(4) . .
Ni1 Pt5 Pt14 94.57(5) . .
Ni14 Pt5 Pt14 145.94(6) . .
Ni16 Pt5 Pt14 59.87(5) . .
C28 Pt5 Pt10 113.2(5) . .
Pt1 Pt5 Pt10 62.78(3) . .
Ni1 Pt5 Pt10 93.42(5) . .
Ni14 Pt5 Pt10 60.09(5) . .
Ni16 Pt5 Pt10 145.27(6) . .
Pt14 Pt5 Pt10 112.45(4) . .
C28 Pt5 Pt9 125.4(5) . .
Pt1 Pt5 Pt9 60.84(3) . .
Ni1 Pt5 Pt9 124.36(5) . .
Ni14 Pt5 Pt9 120.65(5) . .
Ni16 Pt5 Pt9 119.49(5) . .
Pt14 Pt5 Pt9 59.90(4) . .
Pt10 Pt5 Pt9 60.81(3) . .
C8 Pt6 C12 89.5(7) . .
C8 Pt6 Ni8 114.4(5) . .
C12 Pt6 Ni8 84.7(5) . .
C8 Pt6 Ni10 133.6(5) . .
C12 Pt6 Ni10 44.7(5) . .
Ni8 Pt6 Ni10 63.32(6) . .
C8 Pt6 Ni12 133.9(4) . .
C12 Pt6 Ni12 85.3(5) . .
Ni8 Pt6 Ni12 110.70(6) . .
Ni10 Pt6 Ni12 62.29(6) . .
C8 Pt6 Ni9 75.3(4) . .
C12 Pt6 Ni9 124.1(5) . .
Ni8 Pt6 Ni9 56.38(6) . .
Ni10 Pt6 Ni9 119.70(6) . .
Ni12 Pt6 Ni9 142.01(6) . .
C8 Pt6 Ni1 45.6(5) . .
C12 Pt6 Ni1 134.3(5) . .
Ni8 Pt6 Ni1 117.79(6) . .
Ni10 Pt6 Ni1 178.71(6) . .
Ni12 Pt6 Ni1 117.35(6) . .
Ni9 Pt6 Ni1 61.41(6) . .
C8 Pt6 Ni11 92.3(5) . .
C12 Pt6 Ni11 124.5(5) . .
Ni8 Pt6 Ni11 141.58(6) . .
Ni10 Pt6 Ni11 117.74(6) . .
Ni12 Pt6 Ni11 55.46(6) . .
Ni9 Pt6 Ni11 109.82(6) . .
Ni1 Pt6 Ni11 61.89(6) . .
C8 Pt6 Pt2 160.1(5) . .
C12 Pt6 Pt2 107.8(5) . .
Ni8 Pt6 Pt2 59.51(4) . .
Ni10 Pt6 Pt2 63.11(4) . .
Ni12 Pt6 Pt2 59.38(4) . .
Ni9 Pt6 Pt2 86.75(4) . .
Ni1 Pt6 Pt2 117.90(5) . .
Ni11 Pt6 Pt2 85.89(4) . .
C8 Pt6 Pt1 106.0(5) . .
C12 Pt6 Pt1 164.3(5) . .
Ni8 Pt6 Pt1 86.46(5) . .
Ni10 Pt6 Pt1 119.59(5) . .
Ni12 Pt6 Pt1 85.69(5) . .
Ni9 Pt6 Pt1 59.65(4) . .
Ni1 Pt6 Pt1 61.41(4) . .
Ni11 Pt6 Pt1 58.78(4) . .
Pt2 Pt6 Pt1 56.49(2) . .
C5 Pt7 C4 90.2(6) . .
C5 Pt7 Pt10 45.3(4) . .
C4 Pt7 Pt10 135.4(4) . .
C5 Pt7 Pt12 136.5(4) . .
C4 Pt7 Pt12 46.4(4) . .
Pt10 Pt7 Pt12 176.96(4) . .
C5 Pt7 Ni8 130.6(4) . .
C4 Pt7 Ni8 90.0(4) . .
Pt10 Pt7 Ni8 116.37(5) . .
Pt12 Pt7 Ni8 60.60(5) . .
C5 Pt7 Ni9 89.6(4) . .
C4 Pt7 Ni9 130.2(4) . .
Pt10 Pt7 Ni9 61.51(5) . .
Pt12 Pt7 Ni9 115.46(5) . .
Ni8 Pt7 Ni9 54.85(6) . .
C5 Pt7 Pt1 106.1(4) . .
C4 Pt7 Pt1 162.1(4) . .
Pt10 Pt7 Pt1 61.38(3) . .
Pt12 Pt7 Pt1 117.21(4) . .
Ni8 Pt7 Pt1 85.12(4) . .
Ni9 Pt7 Pt1 58.97(4) . .
C5 Pt7 Pt2 161.6(4) . .
C4 Pt7 Pt2 106.8(4) . .
Pt10 Pt7 Pt2 117.53(3) . .
Pt12 Pt7 Pt2 61.05(3) . .
Ni8 Pt7 Pt2 58.28(4) . .
Ni9 Pt7 Pt2 84.90(4) . .
Pt1 Pt7 Pt2 56.17(2) . .
C5 Pt7 Pt3 108.8(4) . .
C4 Pt7 Pt3 107.8(4) . .
Pt10 Pt7 Pt3 91.38(3) . .
Pt12 Pt7 Pt3 90.03(3) . .
Ni8 Pt7 Pt3 118.03(4) . .
Ni9 Pt7 Pt3 119.23(5) . .
Pt1 Pt7 Pt3 60.30(2) . .
Pt2 Pt7 Pt3 59.76(2) . .
C2 Pt8 C1 90.8(6) . .
C2 Pt8 Pt14 47.4(4) . .
C1 Pt8 Pt14 138.0(4) . .
C2 Pt8 Pt13 136.0(4) . .
C1 Pt8 Pt13 45.5(4) . .
Pt14 Pt8 Pt13 176.48(5) . .
C2 Pt8 Ni11 86.8(4) . .
C1 Pt8 Ni11 131.4(4) . .
Pt14 Pt8 Ni11 61.52(5) . .
Pt13 Pt8 Ni11 116.22(6) . .
C2 Pt8 Ni12 125.9(4) . .
C1 Pt8 Ni12 90.2(4) . .
Pt14 Pt8 Ni12 115.95(5) . .
Pt13 Pt8 Ni12 61.78(5) . .
Ni11 Pt8 Ni12 54.46(6) . .
C2 Pt8 Pt1 107.8(4) . .
C1 Pt8 Pt1 160.3(4) . .
Pt14 Pt8 Pt1 60.36(3) . .
Pt13 Pt8 Pt1 116.26(4) . .
Ni11 Pt8 Pt1 58.28(4) . .
Ni12 Pt8 Pt1 84.26(4) . .
C2 Pt8 Pt2 163.5(4) . .
C1 Pt8 Pt2 105.5(4) . .
Pt14 Pt8 Pt2 116.17(4) . .
Pt13 Pt8 Pt2 60.45(3) . .
Ni11 Pt8 Pt2 84.38(5) . .
Ni12 Pt8 Pt2 58.09(4) . .
Pt1 Pt8 Pt2 55.81(2) . .
C2 Pt8 Pt3 113.7(4) . .
C1 Pt8 Pt3 107.0(4) . .
Pt14 Pt8 Pt3 90.04(4) . .
Pt13 Pt8 Pt3 88.86(3) . .
Ni11 Pt8 Pt3 118.24(4) . .
Ni12 Pt8 Pt3 117.54(5) . .
Pt1 Pt8 Pt3 60.00(2) . .
Pt2 Pt8 Pt3 59.46(2) . .
C26 Ni1 C8 92.4(7) . .
C26 Ni1 C20 91.3(6) . .
C8 Ni1 C20 91.9(7) . .
C26 Ni1 Ni14 48.4(5) . .
C8 Ni1 Ni14 111.3(5) . .
C20 Ni1 Ni14 132.2(5) . .
C26 Ni1 Ni16 111.0(5) . .
C8 Ni1 Ni16 130.4(5) . .
C20 Ni1 Ni16 46.6(5) . .
Ni14 Ni1 Ni16 117.03(10) . .
C26 Ni1 Pt6 132.6(5) . .
C8 Ni1 Pt6 46.9(5) . .
C20 Ni1 Pt6 109.9(5) . .
Ni14 Ni1 Pt6 116.47(9) . .
Ni16 Ni1 Pt6 114.34(8) . .
C26 Ni1 Pt5 94.8(5) . .
C8 Ni1 Pt5 161.3(5) . .
C20 Ni1 Pt5 105.1(5) . .
Ni14 Ni1 Pt5 62.55(6) . .
Ni16 Ni1 Pt5 62.13(6) . .
Pt6 Ni1 Pt5 117.93(6) . .
C26 Ni1 Ni9 91.1(5) . .
C8 Ni1 Ni9 74.4(5) . .
C20 Ni1 Ni9 166.2(5) . .
Ni14 Ni1 Ni9 57.21(7) . .
Ni16 Ni1 Ni9 143.50(9) . .
Pt6 Ni1 Ni9 59.29(6) . .
Pt5 Ni1 Ni9 88.24(6) . .
C26 Ni1 Ni11 162.5(5) . .
C8 Ni1 Ni11 91.3(5) . .
C20 Ni1 Ni11 71.5(4) . .
Ni14 Ni1 Ni11 143.94(9) . .
Ni16 Ni1 Ni11 54.88(7) . .
Pt6 Ni1 Ni11 59.51(6) . .
Pt5 Ni1 Ni11 87.00(6) . .
Ni9 Ni1 Ni11 106.31(8) . .
C26 Ni1 Pt1 136.3(5) . .
C8 Ni1 Pt1 106.9(5) . .
C20 Ni1 Pt1 125.7(4) . .
Ni14 Ni1 Pt1 87.91(7) . .
Ni16 Ni1 Pt1 85.98(7) . .
Pt6 Ni1 Pt1 61.06(4) . .
Pt5 Ni1 Pt1 56.88(4) . .
Ni9 Ni1 Pt1 58.89(5) . .
Ni11 Ni1 Pt1 57.95(5) . .
C24 Pt9 C14 101.7(7) . .
C24 Pt9 Pt3 149.9(6) . .
C14 Pt9 Pt3 48.3(4) . .
C24 Pt9 Pt1 147.2(6) . .
C14 Pt9 Pt1 111.0(4) . .
Pt3 Pt9 Pt1 62.74(3) . .
C24 Pt9 Pt14 106.8(6) . .
C14 Pt9 Pt14 117.9(4) . .
Pt3 Pt9 Pt14 91.84(5) . .
Pt1 Pt9 Pt14 60.73(4) . .
C24 Pt9 Pt5 90.0(6) . .
C14 Pt9 Pt5 168.1(5) . .
Pt3 Pt9 Pt5 119.95(4) . .
Pt1 Pt9 Pt5 57.21(3) . .
Pt14 Pt9 Pt5 59.52(3) . .
C24 Pt9 Pt10 102.3(6) . .
C14 Pt9 Pt10 115.0(4) . .
Pt3 Pt9 Pt10 92.22(4) . .
Pt1 Pt9 Pt10 61.07(3) . .
Pt14 Pt9 Pt10 111.00(5) . .
Pt5 Pt9 Pt10 59.48(3) . .
C9 Pt10 C5 103.8(7) . .
C9 Pt10 Pt7 151.1(6) . .
C5 Pt10 Pt7 47.5(4) . .
C9 Pt10 Ni14 84.8(5) . .
C5 Pt10 Ni14 130.4(4) . .
Pt7 Pt10 Ni14 114.98(6) . .
C9 Pt10 Pt5 90.4(6) . .
C5 Pt10 Pt5 162.9(4) . .
Pt7 Pt10 Pt5 117.50(4) . .
Ni14 Pt10 Pt5 59.39(5) . .
C9 Pt10 Pt9 100.5(6) . .
C5 Pt10 Pt9 107.6(4) . .
Pt7 Pt10 Pt9 88.42(4) . .
Ni14 Pt10 Pt9 118.86(6) . .
Pt5 Pt10 Pt9 59.71(3) . .
C9 Pt10 Ni9 133.9(5) . .
C5 Pt10 Ni9 90.2(5) . .
Pt7 Pt10 Ni9 60.41(5) . .
Ni14 Pt10 Ni9 54.58(6) . .
Pt5 Pt10 Ni9 86.61(5) . .
Pt9 Pt10 Ni9 116.94(6) . .
C9 Pt10 Pt1 146.0(6) . .
C5 Pt10 Pt1 107.9(4) . .
Pt7 Pt10 Pt1 61.06(3) . .
Ni14 Pt10 Pt1 83.94(5) . .
Pt5 Pt10 Pt1 56.44(3) . .
Pt9 Pt10 Pt1 58.43(3) . .
Ni9 Pt10 Pt1 58.53(4) . .
C13 Pt11 C18 102.8(7) . .
C13 Pt11 Pt3 151.6(6) . .
C18 Pt11 Pt3 48.8(5) . .
C13 Pt11 Pt2 145.3(6) . .
C18 Pt11 Pt2 111.8(5) . .
Pt3 Pt11 Pt2 62.92(3) . .
C13 Pt11 Pt4 87.9(6) . .
C18 Pt11 Pt4 169.2(5) . .
Pt3 Pt11 Pt4 120.43(5) . .
Pt2 Pt11 Pt4 57.51(3) . .
C13 Pt11 Pt12 100.7(6) . .
C18 Pt11 Pt12 116.8(4) . .
Pt3 Pt11 Pt12 92.54(5) . .
Pt2 Pt11 Pt12 61.69(4) . .
Pt4 Pt11 Pt12 60.71(4) . .
C13 Pt11 Pt13 106.6(5) . .
C18 Pt11 Pt13 115.0(4) . .
Pt3 Pt11 Pt13 90.91(5) . .
Pt2 Pt11 Pt13 60.97(4) . .
Pt4 Pt11 Pt13 60.21(4) . .
Pt12 Pt11 Pt13 112.58(5) . .
C27 Pt12 C4 99.4(7) . .
C27 Pt12 Pt7 147.0(6) . .
C4 Pt12 Pt7 47.8(4) . .
C27 Pt12 Ni15 88.5(6) . .
C4 Pt12 Ni15 131.7(4) . .
Pt7 Pt12 Ni15 115.33(6) . .
C27 Pt12 Pt11 100.3(6) . .
C4 Pt12 Pt11 107.9(4) . .
Pt7 Pt12 Pt11 89.01(5) . .
Ni15 Pt12 Pt11 117.40(6) . .
C27 Pt12 Ni8 135.9(6) . .
C4 Pt12 Ni8 91.1(4) . .
Pt7 Pt12 Ni8 60.78(5) . .
Ni15 Pt12 Ni8 54.59(7) . .
Pt11 Pt12 Ni8 117.00(7) . .
C27 Pt12 Pt4 94.1(6) . .
C4 Pt12 Pt4 163.1(4) . .
Pt7 Pt12 Pt4 117.49(5) . .
Ni15 Pt12 Pt4 58.21(5) . .
Pt11 Pt12 Pt4 59.38(4) . .
Ni8 Pt12 Pt4 86.06(5) . .
C27 Pt12 Pt2 148.9(6) . .
C4 Pt12 Pt2 108.5(4) . .
Pt7 Pt12 Pt2 61.37(3) . .
Ni15 Pt12 Pt2 83.14(6) . .
Pt11 Pt12 Pt2 58.56(4) . .
Ni8 Pt12 Pt2 58.43(5) . .
Pt4 Pt12 Pt2 56.12(3) . .
C15 Pt13 C1 103.2(7) . .
C15 Pt13 Pt8 151.5(5) . .
C1 Pt13 Pt8 48.3(4) . .
C15 Pt13 Ni13 83.5(5) . .
C1 Pt13 Ni13 128.8(4) . .
Pt8 Pt13 Ni13 114.22(6) . .
C15 Pt13 Pt4 89.2(5) . .
C1 Pt13 Pt4 165.4(4) . .
Pt8 Pt13 Pt4 118.80(5) . .
Ni13 Pt13 Pt4 59.41(5) . .
C15 Pt13 Pt11 100.4(5) . .
C1 Pt13 Pt11 110.0(4) . .
Pt8 Pt13 Pt11 90.54(5) . .
Ni13 Pt13 Pt11 118.59(7) . .
Pt4 Pt13 Pt11 59.41(4) . .
C15 Pt13 Pt2 145.1(5) . .
C1 Pt13 Pt2 110.0(4) . .
Pt8 Pt13 Pt2 62.26(3) . .
Ni13 Pt13 Pt2 83.77(5) . .
Pt4 Pt13 Pt2 56.54(3) . .
Pt11 Pt13 Pt2 58.71(3) . .
C15 Pt13 Ni12 132.5(5) . .
C1 Pt13 Ni12 91.0(4) . .
Pt8 Pt13 Ni12 60.40(5) . .
Ni13 Pt13 Ni12 53.83(7) . .
Pt4 Pt13 Ni12 86.00(5) . .
Pt11 Pt13 Ni12 116.94(6) . .
Pt2 Pt13 Ni12 58.23(4) . .
C10 Pt14 C2 103.8(7) . .
C10 Pt14 Pt8 149.8(5) . .
C2 Pt14 Pt8 47.5(5) . .
C10 Pt14 Ni16 88.4(5) . .
C2 Pt14 Ni16 123.0(4) . .
Pt8 Pt14 Ni16 113.93(7) . .
C10 Pt14 Pt5 89.0(5) . .
C2 Pt14 Pt5 166.7(5) . .
Pt8 Pt14 Pt5 119.27(6) . .
Ni16 Pt14 Pt5 59.91(5) . .
C10 Pt14 Pt9 96.0(5) . .
C2 Pt14 Pt9 113.7(4) . .
Pt8 Pt14 Pt9 90.02(5) . .
Ni16 Pt14 Pt9 120.20(6) . .
Pt5 Pt14 Pt9 60.57(3) . .
C10 Pt14 Pt1 144.4(5) . .
C2 Pt14 Pt1 109.6(5) . .
Pt8 Pt14 Pt1 62.14(4) . .
Ni16 Pt14 Pt1 83.88(6) . .
Pt5 Pt14 Pt1 57.13(3) . .
Pt9 Pt14 Pt1 59.45(4) . .
C10 Pt14 Ni11 137.5(5) . .
C2 Pt14 Ni11 86.2(4) . .
Pt8 Pt14 Ni11 60.50(5) . .
Ni16 Pt14 Ni11 53.43(7) . .
Pt5 Pt14 Ni11 86.69(5) . .
Pt9 Pt14 Ni11 117.96(7) . .
Pt1 Pt14 Ni11 58.52(5) . .
C7 Ni8 C11 94.6(7) . .
C7 Ni8 Ni15 52.2(5) . .
C11 Ni8 Ni15 129.9(5) . .
C7 Ni8 Ni9 129.6(5) . .
C11 Ni8 Ni9 48.2(5) . .
Ni15 Ni8 Ni9 175.97(10) . .
C7 Ni8 Pt6 157.1(5) . .
C11 Ni8 Pt6 80.6(5) . .
Ni15 Ni8 Pt6 114.86(8) . .
Ni9 Ni8 Pt6 62.03(6) . .
C7 Ni8 Pt2 129.2(5) . .
C11 Ni8 Pt2 135.7(5) . .
Ni15 Ni8 Pt2 89.22(8) . .
Ni9 Ni8 Pt2 91.28(8) . .
Pt6 Ni8 Pt2 61.88(4) . .
C7 Ni8 Pt12 70.6(5) . .
C11 Ni8 Pt12 148.6(5) . .
Ni15 Ni8 Pt12 62.43(7) . .
Ni9 Ni8 Pt12 121.21(9) . .
Pt6 Ni8 Pt12 123.42(7) . .
Pt2 Ni8 Pt12 61.58(5) . .
C7 Ni8 Pt7 107.1(5) . .
C11 Ni8 Pt7 102.8(5) . .
Ni15 Ni8 Pt7 121.02(8) . .
Ni9 Ni8 Pt7 62.59(6) . .
Pt6 Ni8 Pt7 95.83(7) . .
Pt2 Ni8 Pt7 61.73(4) . .
Pt12 Ni8 Pt7 58.62(5) . .
C7 Ni8 Ni10 106.1(5) . .
C11 Ni8 Ni10 118.0(5) . .
Ni15 Ni8 Ni10 56.46(7) . .
Ni9 Ni8 Ni10 120.43(9) . .
Pt6 Ni8 Ni10 58.42(6) . .
Pt2 Ni8 Ni10 62.24(5) . .
Pt12 Ni8 Ni10 93.01(7) . .
Pt7 Ni8 Ni10 123.94(8) . .
C21 Ni9 C11 92.9(7) . .
C21 Ni9 Ni14 52.4(5) . .
C11 Ni9 Ni14 130.4(5) . .
C21 Ni9 Ni8 129.1(5) . .
C11 Ni9 Ni8 48.6(5) . .
Ni14 Ni9 Ni8 177.25(10) . .
C21 Ni9 Pt6 156.1(5) . .
C11 Ni9 Pt6 80.5(5) . .
Ni14 Ni9 Pt6 116.09(8) . .
Ni8 Ni9 Pt6 61.59(6) . .
C21 Ni9 Pt1 130.9(5) . .
C11 Ni9 Pt1 135.6(5) . .
Ni14 Ni9 Pt1 89.31(8) . .
Ni8 Ni9 Pt1 90.70(7) . .
Pt6 Ni9 Pt1 62.00(4) . .
C21 Ni9 Ni1 106.2(5) . .
C11 Ni9 Ni1 119.4(5) . .
Ni14 Ni9 Ni1 56.83(7) . .
Ni8 Ni9 Ni1 120.88(9) . .
Pt6 Ni9 Ni1 59.30(6) . .
Pt1 Ni9 Ni1 61.52(5) . .
C21 Ni9 Pt7 108.3(5) . .
C11 Ni9 Pt7 103.1(5) . .
Ni14 Ni9 Pt7 119.74(8) . .
Ni8 Ni9 Pt7 62.55(6) . .
Pt6 Ni9 Pt7 95.56(6) . .
Pt1 Ni9 Pt7 61.13(4) . .
Ni1 Ni9 Pt7 122.57(8) . .
C21 Ni9 Pt10 73.0(5) . .
C11 Ni9 Pt10 148.8(5) . .
Ni14 Ni9 Pt10 61.67(7) . .
Ni8 Ni9 Pt10 120.63(8) . .
Pt6 Ni9 Pt10 122.92(7) . .
Pt1 Ni9 Pt10 60.96(5) . .
Ni1 Ni9 Pt10 91.48(8) . .
Pt7 Ni9 Pt10 58.07(4) . .
C12 Ni10 C23 90.9(7) . .
C12 Ni10 C19 94.6(8) . .
C23 Ni10 C19 91.2(8) . .
C12 Ni10 Ni15 120.1(5) . .
C23 Ni10 Ni15 126.3(5) . .
C19 Ni10 Ni15 47.6(6) . .
C12 Ni10 Ni13 122.9(5) . .
C23 Ni10 Ni13 46.2(5) . .
C19 Ni10 Ni13 117.1(6) . .
Ni15 Ni10 Ni13 116.23(10) . .
C12 Ni10 Pt6 47.7(5) . .
C23 Ni10 Pt6 118.9(5) . .
C19 Ni10 Pt6 127.5(6) . .
Ni15 Ni10 Pt6 114.00(8) . .
Ni13 Ni10 Pt6 114.46(9) . .
C12 Ni10 Pt4 163.3(5) . .
C23 Ni10 Pt4 101.2(5) . .
C19 Ni10 Pt4 96.6(6) . .
Ni15 Ni10 Pt4 61.13(6) . .
Ni13 Ni10 Pt4 61.79(6) . .
Pt6 Ni10 Pt4 115.76(7) . .
C12 Ni10 Ni12 84.5(5) . .
C23 Ni10 Ni12 77.9(5) . .
C19 Ni10 Ni12 169.0(6) . .
Ni15 Ni10 Ni12 141.34(9) . .
Ni13 Ni10 Ni12 55.54(7) . .
Pt6 Ni10 Ni12 58.92(6) . .
Pt4 Ni10 Ni12 86.80(6) . .
C12 Ni10 Ni8 82.7(5) . .
C23 Ni10 Ni8 173.0(5) . .
C19 Ni10 Ni8 86.5(6) . .
Ni15 Ni10 Ni8 55.76(7) . .
Ni13 Ni10 Ni8 140.49(9) . .
Pt6 Ni10 Ni8 58.25(6) . .
Pt4 Ni10 Ni8 85.66(6) . .
Ni12 Ni10 Ni8 104.24(9) . .
C12 Ni10 Pt2 107.6(5) . .
C23 Ni10 Pt2 128.4(5) . .
C19 Ni10 Pt2 132.8(6) . .
Ni15 Ni10 Pt2 85.55(7) . .
Ni13 Ni10 Pt2 85.09(7) . .
Pt6 Ni10 Pt2 59.88(5) . .
Pt4 Ni10 Pt2 55.89(4) . .
Ni12 Ni10 Pt2 57.34(5) . .
Ni8 Ni10 Pt2 56.98(5) . .
C3 Ni11 C17 96.6(6) . .
C3 Ni11 Ni16 52.0(4) . .
C17 Ni11 Ni16 129.6(5) . .
C3 Ni11 Ni12 128.9(4) . .
C17 Ni11 Ni12 48.4(5) . .
Ni16 Ni11 Ni12 177.06(11) . .
C3 Ni11 Pt1 128.3(4) . .
C17 Ni11 Pt1 134.6(5) . .
Ni16 Ni11 Pt1 89.88(7) . .
Ni12 Ni11 Pt1 91.07(7) . .
C3 Ni11 Pt6 159.4(4) . .
C17 Ni11 Pt6 78.5(5) . .
Ni16 Ni11 Pt6 116.45(8) . .
Ni12 Ni11 Pt6 61.71(7) . .
Pt1 Ni11 Pt6 61.98(4) . .
C3 Ni11 Pt8 104.4(4) . .
C17 Ni11 Pt8 104.2(5) . .
Ni16 Ni11 Pt8 120.00(9) . .
Ni12 Ni11 Pt8 62.86(6) . .
Pt1 Ni11 Pt8 61.94(4) . .
Pt6 Ni11 Pt8 96.25(6) . .
C3 Ni11 Pt14 70.2(4) . .
C17 Ni11 Pt14 151.6(4) . .
Ni16 Ni11 Pt14 62.02(7) . .
Ni12 Ni11 Pt14 120.81(8) . .
Pt1 Ni11 Pt14 60.44(5) . .
Pt6 Ni11 Pt14 122.39(7) . .
Pt8 Ni11 Pt14 57.98(5) . .
C3 Ni11 Ni1 108.0(4) . .
C17 Ni11 Ni1 116.6(4) . .
Ni16 Ni11 Ni1 57.90(7) . .
Ni12 Ni11 Ni1 120.31(10) . .
Pt1 Ni11 Ni1 61.40(5) . .
Pt6 Ni11 Ni1 58.60(6) . .
Pt8 Ni11 Ni1 123.28(7) . .
Pt14 Ni11 Ni1 91.63(7) . .
C16 Ni12 C17 94.0(6) . .
C16 Ni12 Ni13 52.9(5) . .
C17 Ni12 Ni13 129.9(5) . .
C16 Ni12 Ni11 127.4(5) . .
C17 Ni12 Ni11 48.7(5) . .
Ni13 Ni12 Ni11 178.09(11) . .
C16 Ni12 Pt6 157.6(5) . .
C17 Ni12 Pt6 79.3(4) . .
Ni13 Ni12 Pt6 116.13(9) . .
Ni11 Ni12 Pt6 62.83(6) . .
C16 Ni12 Pt2 130.4(5) . .
C17 Ni12 Pt2 135.0(5) . .
Ni13 Ni12 Pt2 89.41(8) . .
Ni11 Ni12 Pt2 91.39(7) . .
Pt6 Ni12 Pt2 61.78(4) . .
C16 Ni12 Pt8 105.6(5) . .
C17 Ni12 Pt8 104.3(5) . .
Ni13 Ni12 Pt8 119.21(8) . .
Ni11 Ni12 Pt8 62.69(6) . .
Pt6 Ni12 Pt8 96.80(6) . .
Pt2 Ni12 Pt8 62.18(4) . .
C16 Ni12 Ni10 107.1(5) . .
C17 Ni12 Ni10 116.2(5) . .
Ni13 Ni12 Ni10 57.35(7) . .
Ni11 Ni12 Ni10 121.60(9) . .
Pt6 Ni12 Ni10 58.78(6) . .
Pt2 Ni12 Ni10 62.74(6) . .
Pt8 Ni12 Ni10 124.84(7) . .
C16 Ni12 Pt13 72.4(4) . .
C17 Ni12 Pt13 151.2(5) . .
Ni13 Ni12 Pt13 61.39(7) . .
Ni11 Ni12 Pt13 120.50(9) . .
Pt6 Ni12 Pt13 122.26(7) . .
Pt2 Ni12 Pt13 60.53(4) . .
Pt8 Ni12 Pt13 57.82(5) . .
Ni10 Ni12 Pt13 92.29(7) . .
C30 Ni13 C23 100.7(8) . .
C30 Ni13 C16 104.9(7) . .
C23 Ni13 C16 103.8(7) . .
C30 Ni13 Ni12 151.9(6) . .
C23 Ni13 Ni12 87.6(5) . .
C16 Ni13 Ni12 47.0(4) . .
C30 Ni13 Ni10 137.2(6) . .
C23 Ni13 Ni10 48.9(5) . .
C16 Ni13 Ni10 110.9(4) . .
Ni12 Ni13 Ni10 67.11(8) . .
C30 Ni13 Pt4 110.4(6) . .
C23 Ni13 Pt4 104.0(5) . .
C16 Ni13 Pt4 129.4(4) . .
Ni12 Ni13 Pt4 93.24(8) . .
Ni10 Ni13 Pt4 62.27(6) . .
C30 Ni13 Pt13 113.0(5) . .
C23 Ni13 Pt13 146.0(5) . .
C16 Ni13 Pt13 72.3(4) . .
Ni12 Ni13 Pt13 64.78(7) . .
Ni10 Ni13 Pt13 99.82(8) . .
Pt4 Ni13 Pt13 61.06(5) . .
C6 Ni14 C26 97.5(7) . .
C6 Ni14 C21 101.3(7) . .
C26 Ni14 C21 116.8(7) . .
C6 Ni14 Ni1 143.2(5) . .
C26 Ni14 Ni1 49.2(5) . .
C21 Ni14 Ni1 107.6(5) . .
C6 Ni14 Ni9 145.9(5) . .
C26 Ni14 Ni9 98.6(5) . .
C21 Ni14 Ni9 44.6(4) . .
Ni1 Ni14 Ni9 65.96(8) . .
C6 Ni14 Pt5 115.8(5) . .
C26 Ni14 Pt5 94.9(5) . .
C21 Ni14 Pt5 127.3(4) . .
Ni1 Ni14 Pt5 61.97(6) . .
Ni9 Ni14 Pt5 92.58(7) . .
C6 Ni14 Pt10 112.7(5) . .
C26 Ni14 Pt10 146.9(5) . .
C21 Ni14 Pt10 71.5(4) . .
Ni1 Ni14 Pt10 97.88(7) . .
Ni9 Ni14 Pt10 63.75(7) . .
Pt5 Ni14 Pt10 60.52(5) . .
C22 Ni15 C19 101.4(9) . .
C22 Ni15 C7 100.7(8) . .
C19 Ni15 C7 114.9(7) . .
C22 Ni15 Ni8 146.2(6) . .
C19 Ni15 Ni8 97.6(7) . .
C7 Ni15 Ni8 45.6(5) . .
C22 Ni15 Ni10 144.4(6) . .
C19 Ni15 Ni10 50.6(7) . .
C7 Ni15 Ni10 110.8(5) . .
Ni8 Ni15 Ni10 67.78(8) . .
C22 Ni15 Pt4 110.8(6) . .
C19 Ni15 Pt4 100.2(6) . .
C7 Ni15 Pt4 126.5(5) . .
Ni8 Ni15 Pt4 92.83(8) . .
Ni10 Ni15 Pt4 62.74(6) . .
C22 Ni15 Pt12 106.8(6) . .
C19 Ni15 Pt12 150.4(7) . .
C7 Ni15 Pt12 68.8(4) . .
Ni8 Ni15 Pt12 62.98(7) . .
Ni10 Ni15 Pt12 99.91(9) . .
Pt4 Ni15 Pt12 61.38(5) . .
C25 Ni16 C20 106.2(8) . .
C25 Ni16 C3 105.5(7) . .
C20 Ni16 C3 99.8(6) . .
C25 Ni16 Ni11 153.8(6) . .
C20 Ni16 Ni11 81.2(5) . .
C3 Ni16 Ni11 48.4(4) . .
C25 Ni16 Ni1 136.8(5) . .
C20 Ni16 Ni1 50.5(5) . .
C3 Ni16 Ni1 113.5(4) . .
Ni11 Ni16 Ni1 67.22(8) . .
C25 Ni16 Pt14 112.1(6) . .
C20 Ni16 Pt14 141.7(5) . .
C3 Ni16 Pt14 70.5(4) . .
Ni11 Ni16 Pt14 64.55(7) . .
Ni1 Ni16 Pt14 98.20(8) . .
C25 Ni16 Pt5 107.5(6) . .
C20 Ni16 Pt5 108.2(5) . .
C3 Ni16 Pt5 127.9(4) . .
Ni11 Ni16 Pt5 93.34(8) . .
Ni1 Ni16 Pt5 61.54(6) . .
Pt14 Ni16 Pt5 60.21(5) . .
O1 C1 Pt13 136.2(12) . .
O1 C1 Pt8 137.3(13) . .
Pt13 C1 Pt8 86.2(6) . .
O2 C2 Pt14 131.3(12) . .
O2 C2 Pt8 143.6(12) . .
Pt14 C2 Pt8 85.1(6) . .
O3 C3 Ni11 143.9(13) . .
O3 C3 Ni16 136.3(12) . .
Ni11 C3 Ni16 79.7(5) . .
O4 C4 Pt12 132.8(12) . .
O4 C4 Pt7 141.4(13) . .
Pt12 C4 Pt7 85.9(6) . .
O5 C5 Pt10 134.1(13) . .
O5 C5 Pt7 138.6(13) . .
Pt10 C5 Pt7 87.3(6) . .
O6 C6 Ni14 175.9(15) . .
O7 C7 Ni8 148.3(14) . .
O7 C7 Ni15 129.2(13) . .
Ni8 C7 Ni15 82.1(6) . .
O8 C8 Ni1 131.3(14) . .
O8 C8 Pt6 141.2(14) . .
Ni1 C8 Pt6 87.5(6) . .
O9 C9 Pt10 176.3(15) . .
O10 C10 Pt14 177.1(16) . .
O11 C11 Ni9 139.7(14) . .
O11 C11 Ni8 137.0(14) . .
Ni9 C11 Ni8 83.2(6) . .
O12 C12 Ni10 133.7(15) . .
O12 C12 Pt6 138.6(15) . .
Ni10 C12 Pt6 87.6(7) . .
O13 C13 Pt11 176.2(17) . .
O14 C14 Pt9 135.6(13) . .
O14 C14 Pt3 139.5(13) . .
Pt9 C14 Pt3 84.8(6) . .
O15 C15 Pt13 177.2(15) . .
O16 C16 Ni12 146.2(14) . .
O16 C16 Ni13 133.7(13) . .
Ni12 C16 Ni13 80.1(6) . .
O17 C17 Ni12 138.7(14) . .
O17 C17 Ni11 138.4(13) . .
Ni12 C17 Ni11 82.9(6) . .
O18 C18 Pt11 138.3(13) . .
O18 C18 Pt3 137.1(13) . .
Pt11 C18 Pt3 84.5(6) . .
O19 C19 Ni15 140.0(19) . .
O19 C19 Ni10 136.9(18) . .
Ni15 C19 Ni10 81.8(8) . .
O20 C20 Ni16 142.6(14) . .
O20 C20 Ni1 134.3(13) . .
Ni16 C20 Ni1 82.9(6) . .
O21 C21 Ni9 146.5(14) . .
O21 C21 Ni14 130.4(13) . .
Ni9 C21 Ni14 83.0(6) . .
O22 C22 Ni15 175.6(18) . .
O23 C23 Ni13 138.0(13) . .
O23 C23 Ni10 137.0(13) . .
Ni13 C23 Ni10 84.9(7) . .
O24 C24 Pt9 176.8(18) . .
O25 C25 Ni16 177.9(17) . .
O26 C26 Ni14 138.5(13) . .
O26 C26 Ni1 139.1(13) . .
Ni14 C26 Ni1 82.4(6) . .
O27 C27 Pt12 177.9(18) . .
O28 C28 Pt5 175.6(15) . .
O29 C29 Pt4 177.0(19) . .
O30 C30 Ni13 176.9(17) . .
C32 C31 N1 118.6(12) 2_545 .
C33 C32 C31 110.7(14) 2 2
C32 C33 C34 116.3(15) 2_545 .
C36 C35 N1 117.8(12) . 2_545
C37 C36 C35 111.5(13) 2_545 .
C36 C37 C38 113.9(14) 2 .
N1 C39 C40 114.6(13) 2 1_565
C39 C40 C41 109.3(13) 1_545 .
C42 C41 C40 111.3(15) . .
C44 C43 N1 113.6(12) 2 2
C43 C44 C45 108.4(13) 2_545 2
C46 C45 C44 109.9(15) . 2_545
N2 C47 C48 114.1(13) . .
C47 C48 C49 107.5(15) . 1_565
C50 C49 C48 111.5(16) . 1_545
C52 C51 N2 117.6(14) . .
C54 C53 C52 114.7(18) . .
C51 C52 C53 109.5(15) . .
C56 C55 N2 115.9(13) 1_565 .
C55 C56 C57 108.1(13) 1_545 3_655
C56 C57 C58 111.4(13) 3_655 .
N2 C59 C60 117.9(12) . 1_565
C61 C60 C59 110.6(13) . 1_545
C60 C61 C62 115.3(15) . .
C64 C63 N3 118.1(14) 2_645 .
C65 C64 C63 111.5(16) . 2_655
C64 C65 C66 115.9(17) . .
C68 C67 N3 117.6(15) . .
C67 C68 C69 113.1(16) . .
C70 C69 C68 110.8(18) . .
C72 C71 N3 117.4(13) 2_655 2_655
C71 C72 C73 110.2(14) 2_645 2_645
C74 C73 C72 112.7(15) . 2_655
N3 C75 C76 116.2(14) 2_655 .
C78 C77 C76 112(2) . .
C77 C76 C75 111.5(16) . .
C39 N1 C35 109.4(11) 2_545 2
C39 N1 C31 108.9(11) 2_545 .
C35 N1 C31 108.7(10) 2 .
C39 N1 C43 109.3(11) 2_545 2_545
C35 N1 C43 109.4(11) 2 2_545
C31 N1 C43 111.1(11) . 2_545
C83 N4 C91 121(3) . .
C83 N4 C79 113(3) . 3_656
C91 N4 C79 116(3) . 3_656
C83 N4 C87 96(3) . .
C91 N4 C87 106(2) . .
C79 N4 C87 99(2) 3_656 .
C47 N2 C59 107.4(12) . .
C47 N2 C55 110.7(11) . .
C59 N2 C55 111.1(12) . .
C47 N2 C51 110.3(12) . .
C59 N2 C51 107.3(12) . .
C55 N2 C51 109.9(12) . .
C75 N3 C71 108.2(12) 2_645 2_645
C75 N3 C63 109.5(12) 2_645 .
C71 N3 C63 110.6(12) 2_645 .
C75 N3 C67 109.7(13) 2_645 .
C71 N3 C67 109.9(13) 2_645 .
C63 N3 C67 108.9(12) . .
C80 C79 N4 129(5) . 3_656
C79 C80 C81 114(6) . .
C82 C81 C80 114(3) . .
C84 C83 N4 119(4) . .
C85 C84 C83 127(3) . .
C84 C85 C86 132(3) . .
C88 C87 N4 137(3) . .
C87 C88 C89 127(4) . .
C90 C89 C88 118(4) . .
C92 C91 N4 120(4) . .
C91 C92 C93 107(4) . .
C94 C93 C92 92(3) . .
O31 C96 C97 122(5) . .
O31 C96 C95 115(5) . .
C97 C96 C95 122(5) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Pt1 Pt5 2.6200(9) .
Pt1 Pt2 2.6306(9) .
Pt1 Ni11 2.7032(18) .
Pt1 Pt9 2.7216(12) .
Pt1 Ni9 2.7274(19) .
Pt1 Pt14 2.7570(15) .
Pt1 Pt7 2.7874(8) .
Pt1 Pt6 2.7905(9) .
Pt1 Pt10 2.7958(12) .
Pt2 Pt4 2.6121(10) .
Pt2 Ni12 2.7032(18) .
Pt2 Ni8 2.7044(19) .
Pt2 Pt11 2.7054(12) .
Pt2 Pt6 2.7681(8) .
Pt2 Pt13 2.7683(13) .
Pt2 Pt12 2.7917(14) .
Pt2 Pt3 2.7948(9) .
Pt3 C18 2.003(15) .
Pt3 C14 2.008(15) .
Pt3 Pt11 2.6486(15) .
Pt3 Pt9 2.6793(13) .
Pt3 Pt7 2.8101(8) .
Pt3 Pt8 2.8189(8) .
Pt4 C29 1.80(2) .
Pt4 Ni15 2.673(2) .
Pt4 Ni13 2.7013(19) .
Pt4 Ni10 2.7136(19) .
Pt4 Pt11 2.7241(14) .
Pt4 Pt13 2.7463(14) .
Pt4 Pt12 2.7609(13) .
Pt5 C28 1.766(18) .
Pt5 Ni1 2.6984(19) .
Pt5 Ni14 2.7128(19) .
Pt5 Ni16 2.7133(19) .
Pt5 Pt14 2.7215(14) .
Pt5 Pt10 2.7439(12) .
Pt5 Pt9 2.7504(11) .
Pt6 C8 1.967(15) .
Pt6 C12 1.986(18) .
Pt6 Ni8 2.679(2) .
Pt6 Ni10 2.684(2) .
Pt6 Ni12 2.6882(18) .
Pt6 Ni9 2.6903(18) .
Pt6 Ni1 2.690(2) .
Pt6 Ni11 2.716(2) .
Pt7 C5 1.983(15) .
Pt7 C4 2.000(15) .
Pt7 Pt10 2.6880(14) .
Pt7 Pt12 2.6931(15) .
Pt7 Ni8 2.753(2) .
Pt7 Ni9 2.7541(18) .
Pt8 C2 1.980(15) .
Pt8 C1 2.004(14) .
Pt8 Pt14 2.6750(17) .
Pt8 Pt13 2.6774(15) .
Pt8 Ni11 2.7461(18) .
Pt8 Ni12 2.750(2) .
Ni1 C26 1.923(15) .
Ni1 C8 1.925(16) .
Ni1 C20 1.986(16) .
Ni1 Ni14 2.518(2) .
Ni1 Ni16 2.555(3) .
Ni1 Ni9 2.748(3) .
Ni1 Ni11 2.780(2) .
Pt9 C24 1.77(2) .
Pt9 C14 1.964(14) .
Pt9 Pt14 2.7320(16) .
Pt9 Pt10 2.7806(14) .
Pt10 C9 1.729(19) .
Pt10 C5 1.912(15) .
Pt10 Ni14 2.732(2) .
Pt10 Ni9 2.784(2) .
Pt11 C13 1.752(19) .
Pt11 C18 1.934(16) .
Pt11 Pt12 2.7388(17) .
Pt11 Pt13 2.7508(16) .
Pt12 C27 1.76(2) .
Pt12 C4 1.954(14) .
Pt12 Ni15 2.735(2) .
Pt12 Ni8 2.748(2) .
Pt13 C15 1.737(17) .
Pt13 C1 1.914(15) .
Pt13 Ni13 2.705(2) .
Pt13 Ni12 2.787(2) .
Pt14 C10 1.751(18) .
Pt14 C2 1.977(14) .
Pt14 Ni16 2.712(2) .
Pt14 Ni11 2.773(2) .
Ni8 C7 1.814(17) .
Ni8 C11 1.916(16) .
Ni8 Ni15 2.514(3) .
Ni8 Ni9 2.537(3) .
Ni8 Ni10 2.815(2) .
Ni9 C21 1.790(15) .
Ni9 C11 1.904(17) .
Ni9 Ni14 2.529(3) .
Ni10 C12 1.889(17) .
Ni10 C23 1.922(16) .
Ni10 C19 1.98(2) .
Ni10 Ni15 2.535(3) .
Ni10 Ni13 2.540(3) .
Ni10 Ni12 2.779(3) .
Ni11 C3 1.874(15) .
Ni11 C17 1.903(16) .
Ni11 Ni16 2.466(3) .
Ni11 Ni12 2.515(3) .
Ni12 C16 1.846(15) .
Ni12 C17 1.896(16) .
Ni12 Ni13 2.487(3) .
Ni13 C30 1.758(18) .
Ni13 C23 1.839(16) .
Ni13 C16 2.012(16) .
Ni14 C6 1.752(16) .
Ni14 C26 1.901(15) .
Ni14 C21 2.020(16) .
Ni15 C22 1.74(2) .
Ni15 C19 1.89(2) .
Ni15 C7 2.006(16) .
Ni16 C25 1.81(2) .
Ni16 C20 1.870(16) .
Ni16 C3 1.975(14) .
O1 C1 1.211(16) .
O2 C2 1.212(16) .
O3 C3 1.165(15) .
O4 C4 1.193(15) .
O5 C5 1.246(16) .
O6 C6 1.171(17) .
O7 C7 1.204(17) .
O8 C8 1.203(17) .
O9 C9 1.189(19) .
O10 C10 1.146(19) .
O11 C11 1.197(17) .
O12 C12 1.195(18) .
O13 C13 1.156(19) .
O14 C14 1.161(15) .
O15 C15 1.155(17) .
O16 C16 1.174(16) .
O17 C17 1.202(16) .
O18 C18 1.174(16) .
O19 C19 1.15(2) .
O20 C20 1.183(17) .
O21 C21 1.211(16) .
O22 C22 1.20(2) .
O23 C23 1.215(18) .
O24 C24 1.17(2) .
O25 C25 1.15(2) .
O26 C26 1.185(16) .
O27 C27 1.16(2) .
O28 C28 1.198(19) .
O29 C29 1.19(2) .
O30 C30 1.189(19) .
C31 C32 1.511(19) 2_545
C31 N1 1.540(17) .
C32 C33 1.48(2) 2
C32 C31 1.511(19) 2
C33 C32 1.48(2) 2_545
C33 C34 1.51(2) .
C35 C36 1.53(2) .
C35 N1 1.536(16) 2_545
C36 C37 1.508(19) 2_545
C37 C36 1.508(19) 2
C37 C38 1.53(2) .
C39 N1 1.535(18) 2
C39 C40 1.542(19) 1_565
C40 C39 1.542(19) 1_545
C40 C41 1.58(2) .
C41 C42 1.51(2) .
C43 C44 1.54(2) 2
C43 N1 1.550(18) 2
C44 C43 1.54(2) 2_545
C44 C45 1.60(2) 2
C45 C46 1.55(2) .
C45 C44 1.60(2) 2_545
C47 N2 1.539(17) .
C47 C48 1.56(2) .
C48 C49 1.57(2) 1_565
C49 C50 1.50(2) .
C49 C48 1.57(2) 1_545
C51 C52 1.50(2) .
C51 N2 1.551(19) .
C53 C54 1.49(3) .
C53 C52 1.54(2) .
C55 C56 1.53(2) 1_565
C55 N2 1.549(18) .
C56 C55 1.53(2) 1_545
C56 C57 1.54(2) 3_655
C57 C56 1.54(2) 3_655
C57 C58 1.54(2) .
C59 N2 1.541(19) .
C59 C60 1.58(2) 1_565
C60 C61 1.51(2) .
C60 C59 1.58(2) 1_545
C62 C61 1.56(2) .
C63 C64 1.51(2) 2_645
C63 N3 1.546(19) .
C64 C65 1.50(2) .
C64 C63 1.51(2) 2_655
C66 C65 1.58(3) .
C67 C68 1.52(2) .
C67 N3 1.55(2) .
C68 C69 1.60(2) .
C70 C69 1.47(2) .
C71 C72 1.51(2) 2_655
C71 N3 1.525(18) 2_655
C72 C71 1.51(2) 2_645
C72 C73 1.55(2) 2_645
C73 C74 1.54(2) .
C73 C72 1.55(2) 2_655
C75 N3 1.518(18) 2_655
C75 C76 1.54(2) .
C77 C78 1.34(3) .
C77 C76 1.51(2) .
N1 C39 1.535(18) 2_545
N1 C35 1.536(16) 2
N1 C43 1.550(18) 2_545
N4 C83 1.45(5) .
N4 C91 1.48(4) .
N4 C79 1.57(3) 3_656
N4 C87 1.64(3) .
N3 C75 1.518(18) 2_645
N3 C71 1.525(18) 2_645
C79 C80 1.11(6) .
C79 N4 1.57(3) 3_656
C80 C81 1.74(6) .
C81 C82 1.45(3) .
C83 C84 1.45(5) .
C84 C85 1.38(3) .
C85 C86 1.45(3) .
C87 C88 1.45(4) .
C88 C89 1.50(4) .
C89 C90 1.33(5) .
C91 C92 1.26(4) .
C92 C93 1.81(4) .
C93 C94 1.55(4) .
C96 O31 1.20(5) .
C96 C97 1.38(5) .
C96 C95 1.53(5) .
