#------------------------------------------------------------------------------
#$Date: 2016-03-26 14:38:36 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180271 $
#$URL: svn://www.crystallography.net/cod/cif/7/11/57/7115708.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7115708
loop_
_publ_author_name
'Kun Zhou'
'Yun Geng'
'Li-Kai Yan'
'Xin-Long Wang'
'Xian-Chun Liu'
'Guo-Gang Shan'
'Kui-Zhan Shao'
'Zhong-Min Su'
'Ying-Ning Yu'
_publ_section_title
;
 An ultrastable {Ag55Mo6} nanocluster with a Ag-centered multishell
 structure
;
_journal_name_full               Chem.Commun.
_journal_page_first              11934
_journal_paper_doi               10.1039/C4cc05893C
_journal_volume                  50
_journal_year                    2014
_chemical_formula_sum            'C180 H270 Ag55 Mo6 O60'
_chemical_formula_weight         9902.45
_chemical_name_systematic
; 
 ? 
;
_space_group_crystal_system      trigonal
_space_group_IT_number           148
_space_group_name_Hall           '-R 3'
_space_group_name_H-M_alt        'R -3 :H'
_symmetry_space_group_name_Hall  '-R 3'
_symmetry_space_group_name_H-M   'R -3 :H'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            3
_cell_length_a                   22.261
_cell_length_b                   22.261
_cell_length_c                   47.421
_cell_measurement_reflns_used    35487
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      25.00
_cell_measurement_theta_min      1.83
_cell_volume                     20351.231
_computing_cell_refinement       'SAINT (Bruker, 1999)'
_computing_data_collection       'SMART (Bruker, 1997)'
_computing_data_reduction        SAINT
_computing_molecular_graphics    'SHELXTL-PLUS (Sheldrick, 1990)'
_computing_publication_material  SHELXL-97
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker APEX CCD area-detector'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0368
_diffrn_reflns_av_sigmaI/netI    0.0324
_diffrn_reflns_limit_h_max       26
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       26
_diffrn_reflns_limit_k_min       -25
_diffrn_reflns_limit_l_max       51
_diffrn_reflns_limit_l_min       -56
_diffrn_reflns_number            35487
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.83
_exptl_absorpt_coefficient_mu    4.186
_exptl_absorpt_correction_T_max  0.4091
_exptl_absorpt_correction_T_min  0.3869
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS (Sheldrick, 1996)'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.424
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             14001
_exptl_crystal_size_max          0.28
_exptl_crystal_size_mid          0.26
_exptl_crystal_size_min          0.26
_refine_diff_density_max         1.677
_refine_diff_density_min         -1.661
_refine_diff_density_rms         0.171
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.054
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     481
_refine_ls_number_reflns         7971
_refine_ls_number_restraints     173
_refine_ls_restrained_S_all      1.055
_refine_ls_R_factor_all          0.0803
_refine_ls_R_factor_gt           0.0592
_refine_ls_shift/su_max          0.017
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0981P)²+275.0612P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1633
_refine_ls_wR_factor_ref         0.1753
_reflns_number_gt                5891
_reflns_number_total             7971
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c4cc05893c2.cif
_cod_data_source_block           ccc
_cod_original_cell_volume        20351.2
_cod_database_code               7115708
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag13 Ag 0.0000 0.0000 0.0000 0.0455(14) Uiso 0.40 6 d SP
Ag14 Ag 0.0000 0.0000 0.01177(10) 0.0316(7) Uiso 0.30 3 d SP
Ag1 Ag 0.08670(4) 0.13846(4) -0.058982(15) 0.0515(2) Uani 1 1 d .
Ag2 Ag 0.19577(7) 0.15039(7) -0.09540(3) 0.0993(4) Uani 1 1 d .
Ag3 Ag 0.22992(4) 0.25075(5) -0.03110(2) 0.0645(3) Uani 1 1 d .
Ag4 Ag 0.17791(5) 0.28377(5) -0.08248(2) 0.0659(3) Uani 1 1 d .
Ag5 Ag 0.10307(5) 0.27981(5) -0.02986(2) 0.0759(3) Uani 1 1 d .
Ag6 Ag -0.00233(6) 0.16077(8) -0.09722(3) 0.1004(4) Uani 1 1 d .
Ag7 Ag -0.20996(9) 0.14998(9) -0.04343(4) 0.0655(5) Uani 0.50 1 d P
Ag8 Ag -0.16892(13) 0.19531(13) -0.01286(5) 0.0877(7) Uani 0.50 1 d P
Ag9 Ag -0.09129(11) 0.25492(10) -0.01225(4) 0.0713(5) Uani 0.50 1 d P
Ag10 Ag -0.04032(11) 0.28090(11) -0.04217(6) 0.0851(6) Uani 0.50 1 d P
Ag11 Ag -0.08204(10) 0.22036(10) -0.07523(4) 0.0656(5) Uani 0.50 1 d P
Ag12 Ag -0.14975(16) 0.16880(15) -0.07461(5) 0.1017(8) Uani 0.50 1 d P
Mo1 Mo 0.16660(4) 0.06233(4) -0.022840(15) 0.03361(19) Uani 1 1 d .
C1 C 0.3243(7) 0.3042(7) -0.0885(3) 0.072(3) Uani 1 1 d .
C2 C 0.4023(9) 0.3485(12) -0.0889(5) 0.154(10) Uani 1 1 d .
H2A H 0.4223 0.3259 -0.0784 0.232 Uiso 1 1 calc R
H2B H 0.4158 0.3928 -0.0805 0.232 Uiso 1 1 calc R
H2C H 0.4185 0.3551 -0.1080 0.232 Uiso 1 1 calc R
C3 C 0.0826(7) 0.3423(7) -0.0914(2) 0.068(3) Uani 1 1 d .
C4 C 0.0523(11) 0.3891(10) -0.0993(5) 0.138(7) Uani 1 1 d U
H4A H 0.0091 0.3733 -0.0896 0.206 Uiso 1 1 calc R
H4B H 0.0447 0.3870 -0.1193 0.206 Uiso 1 1 calc R
H4C H 0.0844 0.4361 -0.0939 0.206 Uiso 1 1 calc R
C5 C 0.0683(8) 0.3951(7) 0.0008(3) 0.075(3) Uani 1 1 d .
C6 C 0.0354(13) 0.4363(10) -0.0090(6) 0.179(12) Uani 1 1 d .
H6A H 0.0620 0.4831 -0.0023 0.269 Uiso 1 1 calc R
H6B H -0.0110 0.4157 -0.0018 0.269 Uiso 1 1 calc R
H6C H 0.0341 0.4363 -0.0292 0.269 Uiso 1 1 calc R
C7 C 0.2140(6) 0.3353(5) -0.0345(2) 0.063(3) Uani 1 1 d D
C8 C 0.2560(8) 0.4127(5) -0.0420(3) 0.107(5) Uani 1 1 d DU
C9 C 0.2892(13) 0.4762(8) -0.0478(5) 0.150(8) Uani 1 1 d DU
C10 C 0.3070(16) 0.4852(15) -0.0792(6) 0.196(12) Uani 1 1 d U
H10A H 0.2650 0.4618 -0.0900 0.294 Uiso 1 1 calc R
H10B H 0.3359 0.4658 -0.0834 0.294 Uiso 1 1 calc R
H10C H 0.3311 0.5337 -0.0838 0.294 Uiso 1 1 calc R
C11 C 0.3423(18) 0.5155(18) -0.0296(8) 0.231(12) Uani 1 1 d U
H11A H 0.3660 0.5629 -0.0358 0.347 Uiso 1 1 calc R
H11B H 0.3741 0.4983 -0.0292 0.347 Uiso 1 1 calc R
H11C H 0.3239 0.5128 -0.0111 0.347 Uiso 1 1 calc R
C12 C 0.2505(18) 0.5096(19) -0.0385(8) 0.255(13) Uani 1 1 d DU
H12A H 0.2067 0.4892 -0.0481 0.383 Uiso 1 1 calc R
H12B H 0.2766 0.5582 -0.0427 0.383 Uiso 1 1 calc R
H12C H 0.2428 0.5032 -0.0185 0.383 Uiso 1 1 calc R
C13 C 0.1039(5) 0.1708(6) -0.10046(18) 0.055(3) Uani 1 1 d D
C14 C 0.1036(7) 0.1771(8) -0.12709(19) 0.079(4) Uani 1 1 d D
C15 C 0.1087(14) 0.1930(14) -0.1567(5) 0.151(7) Uani 1 1 d U
C16 C 0.1866(15) 0.2392(15) -0.1633(6) 0.189(11) Uani 1 1 d U
H16A H 0.2041 0.2832 -0.1541 0.284 Uiso 1 1 calc R
H16B H 0.1929 0.2463 -0.1833 0.284 Uiso 1 1 calc R
H16C H 0.2113 0.2169 -0.1567 0.284 Uiso 1 1 calc R
C17 C 0.1063(18) 0.1324(17) -0.1738(7) 0.223(11) Uani 1 1 d U
H17A H 0.1325 0.1152 -0.1641 0.335 Uiso 1 1 calc R
H17B H 0.1259 0.1488 -0.1922 0.335 Uiso 1 1 calc R
H17C H 0.0591 0.0958 -0.1757 0.335 Uiso 1 1 calc R
C18 C 0.0764(13) 0.2326(13) -0.1648(5) 0.155(8) Uani 1 1 d U
H18A H 0.0851 0.2668 -0.1507 0.232 Uiso 1 1 calc R
H18B H 0.0273 0.2022 -0.1668 0.232 Uiso 1 1 calc R
H18C H 0.0953 0.2553 -0.1825 0.232 Uiso 1 1 calc R
C19 C -0.0945(6) 0.1474(6) -0.1121(2) 0.064(3) Uani 1 1 d D
C20 C -0.1235(9) 0.1736(8) -0.1354(3) 0.115(6) Uani 1 1 d D
C21 C -0.1476(15) 0.1929(12) -0.1551(4) 0.142(8) Uani 1 1 d U
C22 C -0.1112(13) 0.2684(13) -0.1554(6) 0.170(9) Uani 1 1 d U
H22A H -0.1293 0.2841 -0.1702 0.255 Uiso 1 1 calc R
H22B H -0.0626 0.2859 -0.1584 0.255 Uiso 1 1 calc R
H22C H -0.1176 0.2850 -0.1376 0.255 Uiso 1 1 calc R
C23 C -0.1431(16) 0.1587(15) -0.1815(6) 0.187(11) Uani 1 1 d U
H23A H -0.1682 0.1093 -0.1791 0.281 Uiso 1 1 calc R
H23B H -0.0953 0.1738 -0.1855 0.281 Uiso 1 1 calc R
H23C H -0.1628 0.1711 -0.1969 0.281 Uiso 1 1 calc R
C24 C -0.226(2) 0.167(2) -0.1478(8) 0.258(18) Uani 1 1 d U
H24A H -0.2518 0.1175 -0.1473 0.387 Uiso 1 1 calc R
H24B H -0.2454 0.1836 -0.1619 0.387 Uiso 1 1 calc R
H24C H -0.2288 0.1851 -0.1297 0.387 Uiso 1 1 calc R
C25 C -0.1411(6) 0.2575(6) -0.0519(3) 0.064(3) Uani 1 1 d .
C26 C -0.1549(7) 0.3006(7) -0.0604(3) 0.078(4) Uani 1 1 d .
C27 C -0.1737(12) 0.3520(11) -0.0705(5) 0.125(6) Uani 1 1 d U
C28 C -0.1331(17) 0.3919(17) -0.0928(7) 0.214(13) Uani 1 1 d U
H28A H -0.0858 0.4194 -0.0867 0.322 Uiso 1 1 calc R
H28B H -0.1497 0.4219 -0.0992 0.322 Uiso 1 1 calc R
H28C H -0.1356 0.3621 -0.1080 0.322 Uiso 1 1 calc R
C29 C -0.2383(15) 0.3115(15) -0.0866(6) 0.193(9) Uani 1 1 d U
H29A H -0.2745 0.2804 -0.0741 0.289 Uiso 1 1 calc R
H29B H -0.2312 0.2853 -0.1010 0.289 Uiso 1 1 calc R
H29C H -0.2513 0.3424 -0.0952 0.289 Uiso 1 1 calc R
C30 C -0.1814(16) 0.3915(17) -0.0453(7) 0.214(12) Uani 1 1 d U
H30A H -0.2107 0.3589 -0.0313 0.320 Uiso 1 1 calc R
H30B H -0.2018 0.4183 -0.0517 0.320 Uiso 1 1 calc R
H30C H -0.1365 0.4219 -0.0374 0.320 Uiso 1 1 calc R
O1 O 0.1351(3) 0.0489(4) 0.01232(12) 0.0490(16) Uani 1 1 d .
O2 O 0.1025(3) 0.0392(3) -0.04909(13) 0.0450(15) Uani 1 1 d .
O3 O 0.2070(4) 0.0130(4) -0.02831(15) 0.0541(17) Uani 1 1 d .
O4 O 0.2310(3) 0.1499(3) -0.02740(14) 0.0510(16) Uani 1 1 d .
O5 O 0.3000(5) 0.2491(5) -0.0739(2) 0.082(2) Uani 1 1 d .
O6 O 0.2913(5) 0.3245(6) -0.1011(2) 0.099(3) Uani 1 1 d .
O7 O 0.1389(5) 0.3561(5) -0.10141(18) 0.081(3) Uani 1 1 d .
O8 O 0.0467(5) 0.2927(5) -0.0750(2) 0.084(3) Uani 1 1 d .
O9 O 0.0437(5) 0.3346(5) -0.0055(2) 0.090(3) Uani 1 1 d .
O10 O 0.1206(8) 0.4242(7) 0.0165(3) 0.147(5) Uani 1 1 d U
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Ag14 Ag13 Ag14 180.0 . 10
Ag13 Ag14 Ag14 0.0 . 10
Ag13 Ag14 Mo1 99.19(8) . 12
Ag14 Ag14 Mo1 99.19(8) 10 12
Ag13 Ag14 Mo1 99.19(8) . 10
Ag14 Ag14 Mo1 99.19(8) 10 10
Mo1 Ag14 Mo1 117.50(5) 12 10
Ag13 Ag14 Mo1 99.19(8) . 11
Ag14 Ag14 Mo1 99.19(8) 10 11
Mo1 Ag14 Mo1 117.50(5) 12 11
Mo1 Ag14 Mo1 117.50(5) 10 11
C13 Ag1 O1 164.1(4) . 12
C13 Ag1 O2 114.3(3) . .
O1 Ag1 O2 77.2(2) 12 .
C13 Ag1 O2 111.4(3) . 2
O1 Ag1 O2 78.7(2) 12 2
O2 Ag1 O2 88.8(3) . 2
C13 Ag1 Ag2 52.8(3) . .
O1 Ag1 Ag2 126.31(18) 12 .
O2 Ag1 Ag2 72.75(16) . .
O2 Ag1 Ag2 142.13(15) 2 .
C13 Ag1 Ag6 50.9(3) . .
O1 Ag1 Ag6 129.55(18) 12 .
O2 Ag1 Ag6 133.72(15) . .
O2 Ag1 Ag6 66.24(15) 2 .
Ag2 Ag1 Ag6 103.03(4) . .
C13 Ag1 Ag4 51.1(3) . .
O1 Ag1 Ag4 113.04(18) 12 .
O2 Ag1 Ag4 135.10(16) . .
O2 Ag1 Ag4 135.44(16) 2 .
Ag2 Ag1 Ag4 66.36(4) . .
Ag6 Ag1 Ag4 74.90(4) . .
C13 Ag1 Ag3 100.6(3) . .
O1 Ag1 Ag3 66.36(18) 12 .
O2 Ag1 Ag3 95.13(15) . .
O2 Ag1 Ag3 142.83(14) 2 .
Ag2 Ag1 Ag3 73.17(4) . .
Ag6 Ag1 Ag3 128.61(4) . .
Ag4 Ag1 Ag3 56.29(3) . .
C13 Ag1 Ag5 98.9(3) . .
O1 Ag1 Ag5 66.95(17) 12 .
O2 Ag1 Ag5 141.82(14) . .
O2 Ag1 Ag5 96.47(15) 2 .
Ag2 Ag1 Ag5 118.61(4) . .
Ag6 Ag1 Ag5 81.79(4) . .
Ag4 Ag1 Ag5 55.96(3) . .
Ag3 Ag1 Ag5 59.12(3) . .
C19 Ag2 C13 143.9(4) 3 .
C19 Ag2 O5 99.3(4) 3 .
C13 Ag2 O5 113.3(3) . .
C19 Ag2 Ag1 143.3(3) 3 .
C13 Ag2 Ag1 45.2(2) . .
O5 Ag2 Ag1 101.9(2) . .
C19 Ag2 Ag12 52.7(3) 3 3
C13 Ag2 Ag12 163.3(3) . 3
O5 Ag2 Ag12 53.2(2) . 3
Ag1 Ag2 Ag12 123.11(7) . 3
C19 Ag2 Ag6 42.9(3) 3 3
C13 Ag2 Ag6 117.3(3) . 3
O5 Ag2 Ag6 126.2(2) . 3
Ag1 Ag2 Ag6 100.71(5) . 3
Ag12 Ag2 Ag6 73.56(7) 3 3
C19 Ag2 Ag4 157.4(3) 3 .
C13 Ag2 Ag4 46.9(3) . .
O5 Ag2 Ag4 66.4(2) . .
Ag1 Ag2 Ag4 59.21(3) . .
Ag12 Ag2 Ag4 119.03(8) 3 .
Ag6 Ag2 Ag4 159.60(5) 3 .
C7 Ag3 O4 172.1(4) . .
C7 Ag3 O5 109.2(4) . .
O4 Ag3 O5 74.9(3) . .
C7 Ag3 Ag9 55.5(3) . 11
O4 Ag3 Ag9 126.73(19) . 11
O5 Ag3 Ag9 134.2(2) . 11
C7 Ag3 Ag4 56.3(3) . .
O4 Ag3 Ag4 120.81(18) . .
O5 Ag3 Ag4 70.6(2) . .
Ag9 Ag3 Ag4 111.79(6) 11 .
C7 Ag3 Ag1 96.9(3) . .
O4 Ag3 Ag1 75.95(17) . .
O5 Ag3 Ag1 92.2(2) . .
Ag9 Ag3 Ag1 129.71(5) 11 .
Ag4 Ag3 Ag1 59.29(3) . .
C7 Ag3 Ag5 41.8(3) . .
O4 Ag3 Ag5 130.35(16) . .
O5 Ag3 Ag5 128.4(2) . .
Ag9 Ag3 Ag5 72.18(5) 11 .
Ag4 Ag3 Ag5 57.82(3) . .
Ag1 Ag3 Ag5 61.89(3) . .
O7 Ag4 C13 106.9(4) . .
O7 Ag4 O6 106.3(3) . .
C13 Ag4 O6 108.2(4) . .
O7 Ag4 C7 100.2(4) . .
C13 Ag4 C7 135.2(3) . .
O6 Ag4 C7 97.3(4) . .
O7 Ag4 Ag3 144.2(2) . .
C13 Ag4 Ag3 100.6(2) . .
O6 Ag4 Ag3 85.9(2) . .
C7 Ag4 Ag3 44.2(3) . .
O7 Ag4 Ag5 87.0(2) . .
C13 Ag4 Ag5 100.9(2) . .
O6 Ag4 Ag5 142.4(3) . .
C7 Ag4 Ag5 45.2(3) . .
Ag3 Ag4 Ag5 65.36(3) . .
O7 Ag4 Ag1 126.0(2) . .
C13 Ag4 Ag1 42.6(2) . .
O6 Ag4 Ag1 123.8(3) . .
C7 Ag4 Ag1 92.6(2) . .
Ag3 Ag4 Ag1 64.42(3) . .
Ag5 Ag4 Ag1 66.14(3) . .
O7 Ag4 Ag2 144.0(2) . .
C13 Ag4 Ag2 45.5(3) . .
O6 Ag4 Ag2 71.7(3) . .
C7 Ag4 Ag2 115.7(3) . .
Ag3 Ag4 Ag2 71.61(4) . .
Ag5 Ag4 Ag2 116.99(4) . .
Ag1 Ag4 Ag2 54.43(3) . .
C7 Ag5 O3 164.1(3) . 2
C7 Ag5 O9 120.4(4) . .
O3 Ag5 O9 75.1(3) 2 .
C7 Ag5 O8 109.6(4) . .
O3 Ag5 O8 73.3(3) 2 .
O9 Ag5 O8 85.6(3) . .
C7 Ag5 Ag8 56.5(3) . 11
O3 Ag5 Ag8 131.57(19) 2 11
O9 Ag5 Ag8 74.2(3) . 11
O8 Ag5 Ag8 139.1(2) . 11
C7 Ag5 Ag4 55.4(3) . .
O3 Ag5 Ag4 115.27(18) 2 .
O9 Ag5 Ag4 143.3(2) . .
O8 Ag5 Ag4 66.2(2) . .
Ag8 Ag5 Ag4 111.79(7) 11 .
C7 Ag5 Ag3 40.3(3) . .
O3 Ag5 Ag3 124.49(17) 2 .
O9 Ag5 Ag3 148.0(3) . .
O8 Ag5 Ag3 122.5(2) . .
Ag8 Ag5 Ag3 74.11(6) 11 .
Ag4 Ag5 Ag3 56.83(3) . .
C7 Ag5 Ag10 145.7(3) . .
O3 Ag5 Ag10 47.18(17) 2 .
O9 Ag5 Ag10 46.9(3) . .
O8 Ag5 Ag10 46.7(2) . .
Ag8 Ag5 Ag10 120.81(8) 11 .
Ag4 Ag5 Ag10 112.67(6) . .
Ag3 Ag5 Ag10 165.07(7) . .
C7 Ag5 Ag1 93.0(3) . .
O3 Ag5 Ag1 71.38(17) 2 .
O9 Ag5 Ag1 146.5(2) . .
O8 Ag5 Ag1 86.0(2) . .
Ag8 Ag5 Ag1 129.33(6) 11 .
Ag4 Ag5 Ag1 57.89(3) . .
Ag3 Ag5 Ag1 58.99(3) . .
Ag10 Ag5 Ag1 106.98(6) . .
C19 Ag6 C13 155.8(4) . .
C19 Ag6 C14 127.0(4) . .
C13 Ag6 C14 29.1(2) . .
C19 Ag6 Ag11 52.4(3) . .
C13 Ag6 Ag11 146.0(3) . .
C14 Ag6 Ag11 148.2(3) . .
C19 Ag6 Ag1 155.5(3) . .
C13 Ag6 Ag1 44.9(2) . .
C14 Ag6 Ag1 73.6(2) . .
Ag11 Ag6 Ag1 118.75(6) . .
C19 Ag6 Ag2 45.0(3) . 2
C13 Ag6 Ag2 137.0(3) . 2
C14 Ag6 Ag2 131.5(3) . 2
Ag11 Ag6 Ag2 73.67(5) . 2
Ag1 Ag6 Ag2 112.75(5) . 2
Ag8 Ag7 Ag12 114.40(14) . .
Ag8 Ag7 C25 68.4(3) . .
Ag12 Ag7 C25 64.9(3) . .
Ag8 Ag7 O10 80.6(5) . 12
Ag12 Ag7 O10 163.5(5) . 12
C25 Ag7 O10 118.3(5) . 12
Ag8 Ag7 O5 151.1(2) . 2
Ag12 Ag7 O5 68.1(3) . 2
C25 Ag7 O5 130.0(4) . 2
O10 Ag7 O5 102.5(5) 12 2
Ag8 Ag7 Ag11 91.77(11) . .
Ag12 Ag7 Ag11 22.90(9) . .
C25 Ag7 Ag11 48.4(3) . .
O10 Ag7 Ag11 166.6(4) 12 .
O5 Ag7 Ag11 89.5(2) 2 .
Ag8 Ag7 Ag9 26.91(9) . .
Ag12 Ag7 Ag9 87.78(11) . .
C25 Ag7 Ag9 48.7(3) . .
O10 Ag7 Ag9 106.4(5) 12 .
O5 Ag7 Ag9 144.0(2) 2 .
Ag11 Ag7 Ag9 64.99(7) . .
Ag9 Ag8 Ag7 122.88(16) . .
Ag9 Ag8 C25 68.8(3) . .
Ag7 Ag8 C25 64.4(3) . .
Ag9 Ag8 C7 68.6(3) . 12
Ag7 Ag8 C7 157.9(3) . 12
C25 Ag8 C7 134.9(4) . 12
Ag9 Ag8 Ag5 104.08(13) . 12
Ag7 Ag8 Ag5 110.59(12) . 12
C25 Ag8 Ag5 162.3(3) . 12
C7 Ag8 Ag5 47.6(3) 12 12
Ag9 Ag8 Ag10 30.51(10) . .
Ag7 Ag8 Ag10 92.38(11) . .
C25 Ag8 Ag10 46.0(3) . .
C7 Ag8 Ag10 97.4(3) 12 .
Ag5 Ag8 Ag10 120.39(9) 12 .
Ag9 Ag8 Ag12 88.84(13) . .
Ag7 Ag8 Ag12 34.37(10) . .
C25 Ag8 Ag12 45.2(3) . .
C7 Ag8 Ag12 145.8(3) 12 .
Ag5 Ag8 Ag12 120.64(10) 12 .
Ag10 Ag8 Ag12 58.50(9) . .
Ag8 Ag9 Ag10 122.05(16) . .
Ag8 Ag9 C25 69.5(3) . .
Ag10 Ag9 C25 62.9(3) . .
Ag8 Ag9 C7 73.2(3) . 12
Ag10 Ag9 C7 155.8(3) . 12
C25 Ag9 C7 139.8(5) . 12
Ag8 Ag9 Ag3 109.56(12) . 12
Ag10 Ag9 Ag3 109.25(12) . 12
C25 Ag9 Ag3 166.3(3) . 12
C7 Ag9 Ag3 46.7(3) 12 12
Ag8 Ag9 Ag7 30.21(10) . .
Ag10 Ag9 Ag7 91.84(11) . .
C25 Ag9 Ag7 47.0(3) . .
C7 Ag9 Ag7 101.5(3) 12 .
Ag3 Ag9 Ag7 125.93(8) 12 .
Ag8 Ag9 Ag11 87.38(12) . .
Ag10 Ag9 Ag11 35.06(9) . .
C25 Ag9 Ag11 44.2(3) . .
C7 Ag9 Ag11 147.7(3) 12 .
Ag3 Ag9 Ag11 122.74(8) 12 .
Ag7 Ag9 Ag11 57.30(6) . .
Ag9 Ag10 Ag11 114.75(14) . .
Ag9 Ag10 C25 69.7(4) . .
Ag11 Ag10 C25 64.8(3) . .
Ag9 Ag10 O3 83.9(2) . 2
Ag11 Ag10 O3 83.6(2) . 2
C25 Ag10 O3 122.4(4) . 2
Ag9 Ag10 O9 77.8(3) . .
Ag11 Ag10 O9 154.7(2) . .
C25 Ag10 O9 139.5(4) . .
O3 Ag10 O9 75.7(3) 2 .
Ag9 Ag10 O8 158.6(2) . .
Ag11 Ag10 O8 68.7(3) . .
C25 Ag10 O8 126.5(4) . .
O3 Ag10 O8 75.4(3) 2 .
O9 Ag10 O8 91.7(3) . .
Ag9 Ag10 Ag8 27.44(9) . .
Ag11 Ag10 Ag8 87.64(10) . .
C25 Ag10 Ag8 49.6(3) . .
O3 Ag10 Ag8 84.43(18) 2 .
O9 Ag10 Ag8 104.5(3) . .
O8 Ag10 Ag8 150.2(3) . .
Ag9 Ag10 Ag12 91.09(12) . .
Ag11 Ag10 Ag12 23.92(8) . .
C25 Ag10 Ag12 48.2(3) . .
O3 Ag10 Ag12 83.91(18) 2 .
O9 Ag10 Ag12 157.6(2) . .
O8 Ag10 Ag12 92.0(3) . .
Ag8 Ag10 Ag12 63.81(9) . .
Ag9 Ag10 Ag5 109.43(11) . .
Ag11 Ag10 Ag5 105.42(11) . .
C25 Ag10 Ag5 166.9(3) . .
O3 Ag10 Ag5 45.43(17) 2 .
O9 Ag10 Ag5 49.4(2) . .
O8 Ag10 Ag5 51.3(2) . .
Ag8 Ag10 Ag5 124.19(8) . .
Ag12 Ag10 Ag5 119.48(9) . .
Ag12 Ag11 Ag10 120.21(17) . .
Ag12 Ag11 C25 71.7(3) . .
Ag10 Ag11 C25 60.1(3) . .
Ag12 Ag11 C19 74.4(3) . .
Ag10 Ag11 C19 159.0(3) . .
C25 Ag11 C19 140.5(4) . .
Ag12 Ag11 O8 167.2(3) . .
Ag10 Ag11 O8 63.7(3) . .
C25 Ag11 O8 118.1(4) . .
C19 Ag11 O8 98.8(4) . .
Ag12 Ag11 Ag6 107.17(15) . .
Ag10 Ag11 Ag6 114.42(11) . .
C25 Ag11 Ag6 170.2(3) . .
C19 Ag11 Ag6 44.6(3) . .
O8 Ag11 Ag6 61.7(2) . .
Ag12 Ag11 Ag7 32.76(13) . .
Ag10 Ag11 Ag7 87.45(10) . .
C25 Ag11 Ag7 47.3(3) . .
C19 Ag11 Ag7 105.9(3) . .
O8 Ag11 Ag7 148.3(2) . .
Ag6 Ag11 Ag7 127.11(8) . .
Ag12 Ag11 Ag9 90.33(14) . .
Ag10 Ag11 Ag9 30.19(8) . .
C25 Ag11 Ag9 44.8(3) . .
C19 Ag11 Ag9 154.2(3) . .
O8 Ag11 Ag9 91.9(2) . .
Ag6 Ag11 Ag9 126.21(8) . .
Ag7 Ag11 Ag9 57.71(6) . .
Ag11 Ag12 Ag7 124.34(18) . .
Ag11 Ag12 C25 71.8(4) . .
Ag7 Ag12 C25 63.0(3) . .
Ag11 Ag12 C19 71.5(3) . .
Ag7 Ag12 C19 158.7(3) . .
C25 Ag12 C19 138.2(5) . .
Ag11 Ag12 O5 158.4(3) . 2
Ag7 Ag12 O5 65.9(3) . 2
C25 Ag12 O5 126.2(4) . 2
C19 Ag12 O5 94.5(4) . 2
Ag11 Ag12 Ag10 35.87(12) . .
Ag7 Ag12 Ag10 88.47(11) . .
C25 Ag12 Ag10 45.7(3) . .
C19 Ag12 Ag10 106.0(3) . .
O5 Ag12 Ag10 146.5(2) 2 .
Ag11 Ag12 Ag2 105.59(16) . 2
Ag7 Ag12 Ag2 112.70(14) . 2
C25 Ag12 Ag2 169.1(3) . 2
C19 Ag12 Ag2 46.1(3) . 2
O5 Ag12 Ag2 54.3(2) 2 2
Ag10 Ag12 Ag2 126.57(10) . 2
Ag11 Ag12 Ag8 93.45(15) . .
Ag7 Ag12 Ag8 31.23(8) . .
C25 Ag12 Ag8 46.1(3) . .
C19 Ag12 Ag8 154.7(3) . .
O5 Ag12 Ag8 93.1(3) 2 .
Ag10 Ag12 Ag8 57.69(8) . .
Ag2 Ag12 Ag8 124.80(11) 2 .
O3 Mo1 O2 107.8(3) . .
O3 Mo1 O4 106.6(3) . .
O2 Mo1 O4 109.2(3) . .
O3 Mo1 O1 108.5(3) . .
O2 Mo1 O1 114.8(3) . .
O4 Mo1 O1 109.6(3) . .
O3 Mo1 Ag14 125.7(2) . 10
O2 Mo1 Ag14 54.0(2) . 10
O4 Mo1 Ag14 127.5(2) . 10
O1 Mo1 Ag14 60.8(2) . 10
O6 C1 O5 126.3(13) . .
O6 C1 C2 117.9(13) . .
O5 C1 C2 115.8(14) . .
C1 C2 H2A 109.5 . .
C1 C2 H2B 109.5 . .
H2A C2 H2B 109.5 . .
C1 C2 H2C 109.5 . .
H2A C2 H2C 109.5 . .
H2B C2 H2C 109.5 . .
O7 C3 O8 125.5(11) . .
O7 C3 C4 118.2(12) . .
O8 C3 C4 116.3(12) . .
C3 C4 H4A 109.5 . .
C3 C4 H4B 109.5 . .
H4A C4 H4B 109.5 . .
C3 C4 H4C 109.5 . .
H4A C4 H4C 109.5 . .
H4B C4 H4C 109.5 . .
O9 C5 O10 120.5(14) . .
O9 C5 C6 120.9(15) . .
O10 C5 C6 118.5(15) . .
C5 C6 H6A 109.5 . .
C5 C6 H6B 109.5 . .
H6A C6 H6B 109.5 . .
C5 C6 H6C 109.5 . .
H6A C6 H6C 109.5 . .
H6B C6 H6C 109.5 . .
C8 C7 Ag3 138.4(10) . .
C8 C7 Ag5 123.2(9) . .
Ag3 C7 Ag5 97.9(4) . .
C8 C7 Ag9 96.5(8) . 11
Ag3 C7 Ag9 77.9(4) . 11
Ag5 C7 Ag9 103.6(5) . 11
C8 C7 Ag8 90.2(8) . 11
Ag3 C7 Ag8 107.2(5) . 11
Ag5 C7 Ag8 75.9(4) . 11
Ag9 C7 Ag8 38.1(2) 11 11
C8 C7 Ag4 100.5(8) . .
Ag3 C7 Ag4 79.5(4) . .
Ag5 C7 Ag4 79.4(3) . .
Ag9 C7 Ag4 157.3(5) 11 .
Ag8 C7 Ag4 155.1(6) 11 .
C9 C8 C7 179(2) . .
C8 C9 C11 114(3) . .
C8 C9 C12 110(2) . .
C11 C9 C12 91(3) . .
C8 C9 C10 109(2) . .
C11 C9 C10 116(2) . .
C12 C9 C10 114(3) . .
C9 C10 H10A 109.5 . .
C9 C10 H10B 109.5 . .
H10A C10 H10B 109.5 . .
C9 C10 H10C 109.5 . .
H10A C10 H10C 109.5 . .
H10B C10 H10C 109.5 . .
C9 C11 H11A 109.5 . .
C9 C11 H11B 109.5 . .
H11A C11 H11B 109.5 . .
C9 C11 H11C 109.5 . .
H11A C11 H11C 109.5 . .
H11B C11 H11C 109.5 . .
C9 C12 H12A 109.5 . .
C9 C12 H12B 109.5 . .
H12A C12 H12B 109.5 . .
C9 C12 H12C 109.5 . .
H12A C12 H12C 109.5 . .
H12B C12 H12C 109.5 . .
C14 C13 Ag1 167.2(10) . .
C14 C13 Ag6 90.8(8) . .
Ag1 C13 Ag6 84.2(3) . .
C14 C13 Ag2 100.3(9) . .
Ag1 C13 Ag2 82.0(3) . .
Ag6 C13 Ag2 162.4(5) . .
C14 C13 Ag4 106.2(9) . .
Ag1 C13 Ag4 86.4(3) . .
Ag6 C13 Ag4 102.5(4) . .
Ag2 C13 Ag4 87.6(4) . .
C13 C14 C15 173.1(18) . .
C13 C14 Ag6 60.1(7) . .
C15 C14 Ag6 121.1(13) . .
C18 C15 C14 114(2) . .
C18 C15 C17 126(2) . .
C14 C15 C17 109(2) . .
C18 C15 C16 106(2) . .
C14 C15 C16 107(2) . .
C17 C15 C16 91(2) . .
C15 C16 H16A 109.5 . .
C15 C16 H16B 109.5 . .
H16A C16 H16B 109.5 . .
C15 C16 H16C 109.5 . .
H16A C16 H16C 109.5 . .
H16B C16 H16C 109.5 . .
C15 C17 H17A 109.5 . .
C15 C17 H17B 109.5 . .
H17A C17 H17B 109.5 . .
C15 C17 H17C 109.5 . .
H17A C17 H17C 109.5 . .
H17B C17 H17C 109.5 . .
C15 C18 H18A 109.5 . .
C15 C18 H18B 109.5 . .
H18A C18 H18B 109.5 . .
C15 C18 H18C 109.5 . .
H18A C18 H18C 109.5 . .
H18B C18 H18C 109.5 . .
C20 C19 Ag6 140.8(10) . .
C20 C19 Ag2 122.9(9) . 2
Ag6 C19 Ag2 92.1(4) . 2
C20 C19 Ag11 101.6(8) . .
Ag6 C19 Ag11 83.0(4) . .
Ag2 C19 Ag11 105.7(5) 2 .
C20 C19 Ag12 95.9(9) . .
Ag6 C19 Ag12 107.4(5) . .
Ag2 C19 Ag12 81.2(4) 2 .
Ag11 C19 Ag12 34.09(19) . .
C21 C20 C19 177.3(18) . .
C20 C21 C22 108(2) . .
C20 C21 C23 108(2) . .
C22 C21 C23 116(2) . .
C20 C21 C24 107(2) . .
C22 C21 C24 107(2) . .
C23 C21 C24 110(2) . .
C21 C22 H22A 109.5 . .
C21 C22 H22B 109.5 . .
H22A C22 H22B 109.5 . .
C21 C22 H22C 109.5 . .
H22A C22 H22C 109.5 . .
H22B C22 H22C 109.5 . .
C21 C23 H23A 109.5 . .
C21 C23 H23B 109.5 . .
H23A C23 H23B 109.5 . .
C21 C23 H23C 109.5 . .
H23A C23 H23C 109.5 . .
H23B C23 H23C 109.5 . .
C21 C24 H24A 109.5 . .
C21 C24 H24B 109.5 . .
H24A C24 H24B 109.5 . .
C21 C24 H24C 109.5 . .
H24A C24 H24C 109.5 . .
H24B C24 H24C 109.5 . .
C26 C25 Ag10 122.9(10) . .
C26 C25 Ag7 128.6(10) . .
Ag10 C25 Ag7 108.5(5) . .
C26 C25 Ag12 127.6(11) . .
Ag10 C25 Ag12 86.1(4) . .
Ag7 C25 Ag12 52.2(3) . .
C26 C25 Ag11 124.8(11) . .
Ag10 C25 Ag11 55.1(3) . .
Ag7 C25 Ag11 84.3(4) . .
Ag12 C25 Ag11 36.6(2) . .
C26 C25 Ag9 129.6(11) . .
Ag10 C25 Ag9 47.5(3) . .
Ag7 C25 Ag9 84.2(4) . .
Ag12 C25 Ag9 102.6(5) . .
Ag11 C25 Ag9 91.0(4) . .
C26 C25 Ag8 132.3(11) . .
Ag10 C25 Ag8 84.3(4) . .
Ag7 C25 Ag8 47.2(3) . .
Ag12 C25 Ag8 88.6(4) . .
Ag11 C25 Ag8 102.8(5) . .
Ag9 C25 Ag8 41.7(2) . .
C25 C26 C27 178.5(17) . .
C28 C27 C26 113(2) . .
C28 C27 C29 97(2) . .
C26 C27 C29 105.2(19) . .
C28 C27 C30 117(2) . .
C26 C27 C30 110.2(19) . .
C29 C27 C30 113(2) . .
C27 C28 H28A 109.5 . .
C27 C28 H28B 109.5 . .
H28A C28 H28B 109.5 . .
C27 C28 H28C 109.5 . .
H28A C28 H28C 109.5 . .
H28B C28 H28C 109.5 . .
C27 C29 H29A 109.5 . .
C27 C29 H29B 109.5 . .
H29A C29 H29B 109.5 . .
C27 C29 H29C 109.5 . .
H29A C29 H29C 109.5 . .
H29B C29 H29C 109.5 . .
C27 C30 H30A 109.5 . .
C27 C30 H30B 109.5 . .
H30A C30 H30B 109.5 . .
C27 C30 H30C 109.5 . .
H30A C30 H30C 109.5 . .
H30B C30 H30C 109.5 . .
Mo1 O1 Ag1 158.3(4) . 11
Mo1 O2 Ag1 109.3(3) . .
Mo1 O2 Ag1 107.9(3) . 3
Ag1 O2 Ag1 142.3(3) . 3
Mo1 O3 Ag5 138.4(4) . 3
Mo1 O3 Ag10 134.0(4) . 3
Ag5 O3 Ag10 87.4(2) 3 3
Mo1 O4 Ag3 134.4(3) . .
C1 O5 Ag7 129.1(9) . 3
C1 O5 Ag12 133.0(8) . 3
Ag7 O5 Ag12 46.02(18) 3 3
C1 O5 Ag2 112.9(9) . .
Ag7 O5 Ag2 111.6(4) 3 .
Ag12 O5 Ag2 72.5(3) 3 .
C1 O5 Ag3 112.7(8) . .
Ag7 O5 Ag3 89.0(3) 3 .
Ag12 O5 Ag3 113.7(3) 3 .
Ag2 O5 Ag3 91.8(3) . .
C1 O6 Ag4 113.8(8) . .
C3 O7 Ag4 111.1(7) . .
C3 O8 Ag10 128.5(9) . .
C3 O8 Ag11 125.9(8) . .
Ag10 O8 Ag11 47.57(17) . .
C3 O8 Ag5 118.8(8) . .
Ag10 O8 Ag5 81.9(3) . .
Ag11 O8 Ag5 113.6(3) . .
C5 O9 Ag10 122.8(9) . .
C5 O9 Ag5 127.2(9) . .
Ag10 O9 Ag5 83.8(3) . .
C5 O10 Ag7 119.9(10) . 11
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag13 Ag14 0.558(5) .
Ag13 Ag14 0.558(5) 10
Ag14 Ag14 1.117(10) 10
Ag14 Mo1 3.2878(11) 12
Ag14 Mo1 3.2878(11) 10
Ag14 Mo1 3.2878(11) 11
Ag1 C13 2.063(9) .
Ag1 O1 2.214(6) 12
Ag1 O2 2.451(6) .
Ag1 O2 2.486(6) 2
Ag1 Ag2 2.8816(12) .
Ag1 Ag6 2.9065(12) .
Ag1 Ag4 3.0431(12) .
Ag1 Ag3 3.1926(12) .
Ag1 Ag5 3.2855(14) .
Ag2 C19 2.123(12) 3
Ag2 C13 2.318(11) .
Ag2 O5 2.481(10) .
Ag2 Ag12 2.912(3) 3
Ag2 Ag6 3.0004(18) 3
Ag2 Ag4 3.2452(15) .
Ag3 C7 2.088(11) .
Ag3 O4 2.264(7) .
Ag3 O5 2.570(9) .
Ag3 Ag9 2.805(2) 11
Ag3 Ag4 2.9443(12) .
Ag3 Ag5 3.1971(13) .
Ag4 O7 2.356(8) .
Ag4 C13 2.372(11) .
Ag4 O6 2.386(10) .
Ag4 C7 2.492(11) .
Ag4 Ag5 2.9770(14) .
Ag5 C7 2.151(12) .
Ag5 O3 2.323(7) 2
Ag5 O9 2.487(9) .
Ag5 O8 2.569(9) .
Ag5 Ag8 2.827(3) 11
Ag5 Ag10 3.257(2) .
Ag6 C19 2.045(11) .
Ag6 C13 2.267(11) .
Ag6 C14 2.615(13) .
Ag6 Ag11 2.890(2) .
Ag6 Ag2 3.0004(18) 2
Ag7 Ag8 1.742(3) .
Ag7 Ag12 1.896(4) .
Ag7 C25 2.138(12) .
Ag7 O10 2.246(14) 12
Ag7 O5 2.406(9) 2
Ag7 Ag11 2.894(3) .
Ag7 Ag9 2.907(3) .
Ag8 Ag9 1.567(3) .
Ag8 C25 2.205(12) .
Ag8 C7 2.430(12) 12
Ag8 Ag5 2.827(3) 12
Ag8 Ag10 2.881(3) .
Ag8 Ag12 3.059(3) .
Ag9 Ag10 1.726(3) .
Ag9 C25 2.196(12) .
Ag9 C7 2.363(11) 12
Ag9 Ag3 2.805(2) 12
Ag9 Ag11 3.116(3) .
Ag10 Ag11 1.971(3) .
Ag10 C25 2.085(12) .
Ag10 O3 2.392(7) 2
Ag10 O9 2.391(11) .
Ag10 O8 2.395(9) .
Ag10 Ag12 2.907(4) .
Ag11 Ag12 1.364(4) .
Ag11 C25 2.174(12) .
Ag11 C19 2.308(12) .
Ag11 O8 2.488(9) .
Ag12 C25 2.173(12) .
Ag12 C19 2.344(13) .
Ag12 O5 2.445(10) 2
Ag12 Ag2 2.912(3) 2
Mo1 O3 1.752(6) .
Mo1 O2 1.765(6) .
Mo1 O4 1.763(6) .
Mo1 O1 1.775(6) .
Mo1 Ag14 3.2878(11) 10
C1 O6 1.197(16) .
C1 O5 1.270(15) .
C1 C2 1.51(2) .
C2 H2A 0.9600 .
C2 H2B 0.9600 .
C2 H2C 0.9600 .
C3 O7 1.228(14) .
C3 O8 1.257(14) .
C3 C4 1.54(2) .
C4 H4A 0.9600 .
C4 H4B 0.9600 .
C4 H4C 0.9600 .
C5 O9 1.210(14) .
C5 O10 1.255(17) .
C5 C6 1.51(2) .
C6 H6A 0.9600 .
C6 H6B 0.9600 .
C6 H6C 0.9600 .
C7 C8 1.5343(10) .
C7 Ag9 2.363(11) 11
C7 Ag8 2.430(12) 11
C8 C9 1.257(17) .
C9 C11 1.37(4) .
C9 C12 1.458(18) .
C9 C10 1.52(3) .
C10 H10A 0.9600 .
C10 H10B 0.9600 .
C10 H10C 0.9600 .
C11 H11A 0.9600 .
C11 H11B 0.9600 .
C11 H11C 0.9600 .
C12 H12A 0.9600 .
C12 H12B 0.9600 .
C12 H12C 0.9600 .
C13 C14 1.271(9) .
C14 C15 1.44(2) .
C15 C18 1.44(3) .
C15 C17 1.55(4) .
C15 C16 1.54(3) .
C16 H16A 0.9600 .
C16 H16B 0.9600 .
C16 H16C 0.9600 .
C17 H17A 0.9600 .
C17 H17B 0.9600 .
C17 H17C 0.9600 .
C18 H18A 0.9600 .
C18 H18B 0.9600 .
C18 H18C 0.9600 .
C19 C20 1.5343(10) .
C19 Ag2 2.123(12) 2
C20 C21 1.255(18) .
C21 C22 1.46(3) .
C21 C23 1.49(3) .
C21 C24 1.58(4) .
C22 H22A 0.9600 .
C22 H22B 0.9600 .
C22 H22C 0.9600 .
C23 H23A 0.9600 .
C23 H23B 0.9600 .
C23 H23C 0.9600 .
C24 H24A 0.9600 .
C24 H24B 0.9600 .
C24 H24C 0.9600 .
C25 C26 1.216(16) .
C26 C27 1.48(2) .
C27 C28 1.39(3) .
C27 C29 1.47(3) .
C27 C30 1.54(4) .
C28 H28A 0.9600 .
C28 H28B 0.9600 .
C28 H28C 0.9600 .
C29 H29A 0.9600 .
C29 H29B 0.9600 .
C29 H29C 0.9600 .
C30 H30A 0.9600 .
C30 H30B 0.9600 .
C30 H30C 0.9600 .
O1 Ag1 2.214(6) 11
O2 Ag1 2.486(6) 3
O3 Ag5 2.323(7) 3
O3 Ag10 2.392(7) 3
O5 Ag7 2.406(9) 3
O5 Ag12 2.445(10) 3
O10 Ag7 2.246(14) 11
