#------------------------------------------------------------------------------
#$Date: 2016-02-13 14:50:18 +0200 (Sat, 13 Feb 2016) $
#$Revision: 176428 $
#$URL: svn://www.crystallography.net/cod/cif/7/11/75/7117513.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7117513
loop_
_publ_author_name
'Jixi Guo'
'Danqing Liu'
'Jiahui Zhang'
'Jiji Zhang'
'Qian Miao'
'Zuowei Xie'
_publ_section_title
;
 o-Carborane functionalized pentacenes: synthesis, molecular packing and
 ambipolar organic thin-film transistors
;
_journal_name_full               Chem.Commun.
_journal_page_first              12004
_journal_paper_doi               10.1039/C5cc03608A
_journal_volume                  51
_journal_year                    2015
_chemical_formula_sum            'C32 H38 B20'
_chemical_formula_weight         638.82
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2015-04-16 deposited with the CCDC.
2015-06-19 downloaded from the CCDC.
;
_cell_angle_alpha                114.692(5)
_cell_angle_beta                 103.244(7)
_cell_angle_gamma                94.149(7)
_cell_formula_units_Z            2
_cell_length_a                   11.066(8)
_cell_length_b                   13.248(4)
_cell_length_c                   14.418(5)
_cell_measurement_reflns_used    1494
_cell_measurement_temperature    133(2)
_cell_measurement_theta_max      30.47
_cell_measurement_theta_min      2.33
_cell_volume                     1835.3(16)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      133(2)
_diffrn_measured_fraction_theta_full 0.980
_diffrn_measured_fraction_theta_max 0.980
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0775
_diffrn_reflns_av_sigmaI/netI    0.1725
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -12
_diffrn_reflns_number            17981
_diffrn_reflns_theta_full        30.58
_diffrn_reflns_theta_max         30.58
_diffrn_reflns_theta_min         1.62
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    0.057
_exptl_absorpt_correction_T_max  0.9932
_exptl_absorpt_correction_T_min  0.9859
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    1.156
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             660
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.12
_refine_diff_density_max         0.420
_refine_diff_density_min         -0.344
_refine_diff_density_rms         0.064
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.906
_refine_ls_hydrogen_treatment    riding
_refine_ls_matrix_type           full
_refine_ls_number_parameters     469
_refine_ls_number_reflns         11040
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.906
_refine_ls_R_factor_all          0.1922
_refine_ls_R_factor_gt           0.0739
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0850P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1685
_refine_ls_wR_factor_ref         0.2199
_reflns_number_gt                4319
_reflns_number_total             11040
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c5cc03608a2.cif
_cod_data_source_block           2
_cod_original_cell_volume        1835.4(15)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7117513
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
B3 B 0.1953(3) 0.4871(3) 0.5778(2) 0.0299(7) Uani 1 1 d . . .
H3 H 0.1927 0.5324 0.5272 0.036 Uiso 1 1 calc R . .
B4 B 0.0591(3) 0.4008(3) 0.5686(2) 0.0280(7) Uani 1 1 d . . .
H4 H -0.0348 0.3895 0.5120 0.034 Uiso 1 1 calc R . .
B5 B 0.1063(3) 0.2871(3) 0.5941(2) 0.0292(7) Uani 1 1 d . . .
H5 H 0.0438 0.2016 0.5551 0.035 Uiso 1 1 calc R . .
B6 B 0.2745(3) 0.3039(3) 0.6197(2) 0.0247(7) Uani 1 1 d . . .
H6 H 0.3234 0.2298 0.5964 0.030 Uiso 1 1 calc R . .
B7 B 0.2954(3) 0.5456(3) 0.7097(2) 0.0337(8) Uani 1 1 d . . .
H7 H 0.3586 0.6306 0.7473 0.040 Uiso 1 1 calc R . .
B8 B 0.1278(3) 0.5294(3) 0.6844(2) 0.0358(8) Uani 1 1 d . . .
H8 H 0.0791 0.6037 0.7057 0.043 Uiso 1 1 calc R . .
B9 B 0.0750(3) 0.4070(3) 0.6957(2) 0.0359(8) Uani 1 1 d . . .
H9 H -0.0089 0.4007 0.7255 0.043 Uiso 1 1 calc R . .
B10 B 0.2077(3) 0.3462(3) 0.7264(2) 0.0283(7) Uani 1 1 d . . .
H10 H 0.2118 0.2994 0.7759 0.034 Uiso 1 1 calc R . .
B11 B 0.3434(3) 0.4324(3) 0.7359(2) 0.0293(7) Uani 1 1 d . . .
H11 H 0.4381 0.4428 0.7912 0.035 Uiso 1 1 calc R . .
B12 B 0.2200(3) 0.4956(3) 0.7820(2) 0.0336(8) Uani 1 1 d . . .
H12 H 0.2323 0.5484 0.8689 0.040 Uiso 1 1 calc R . .
B13 B 0.3859(4) -0.1377(3) -0.2738(3) 0.0377(9) Uani 1 1 d . . .
H13 H 0.4020 -0.1746 -0.2159 0.045 Uiso 1 1 calc R . .
B14 B 0.2343(3) -0.1579(3) -0.3603(2) 0.0384(9) Uani 1 1 d . . .
H14 H 0.1494 -0.2096 -0.3606 0.046 Uiso 1 1 calc R . .
B15 B 0.2228(3) -0.0353(3) -0.3797(2) 0.0378(9) Uani 1 1 d . . .
H15 H 0.1307 -0.0060 -0.3927 0.045 Uiso 1 1 calc R . .
B16 B 0.3675(3) 0.0621(3) -0.3051(2) 0.0321(8) Uani 1 1 d . . .
H16 H 0.3716 0.1558 -0.2677 0.038 Uiso 1 1 calc R . .
B17 B 0.3565(3) -0.2198(3) -0.4118(2) 0.0349(8) Uani 1 1 d . . .
H17 H 0.3532 -0.3134 -0.4470 0.042 Uiso 1 1 calc R . .
B18 B 0.2551(3) -0.1568(3) -0.4777(2) 0.0363(8) Uani 1 1 d . . .
H18 H 0.1841 -0.2088 -0.5572 0.044 Uiso 1 1 calc R . .
B19 B 0.3377(3) -0.0202(3) -0.4429(2) 0.0367(8) Uani 1 1 d . . .
H19 H 0.3220 0.0190 -0.4990 0.044 Uiso 1 1 calc R . .
B20 B 0.4881(3) -0.0001(3) -0.3570(2) 0.0335(8) Uani 1 1 d . . .
H20 H 0.5731 0.0531 -0.3548 0.040 Uiso 1 1 calc R . .
B21 B 0.5007(3) -0.1228(3) -0.3380(2) 0.0349(8) Uani 1 1 d . . .
H21 H 0.5933 -0.1508 -0.3233 0.042 Uiso 1 1 calc R . .
B22 B 0.4190(3) -0.1355(3) -0.4646(2) 0.0290(7) Uani 1 1 d . . .
H22 H 0.4565 -0.1730 -0.5351 0.035 Uiso 1 1 calc R . .
C1 C 0.1819(2) 0.3433(2) 0.53086(17) 0.0210(5) Uani 1 1 d . . .
C2 C 0.3210(2) 0.4275(2) 0.61303(18) 0.0249(6) Uani 1 1 d . . .
C3 C 0.4280(3) 0.4300(3) 0.5657(2) 0.0375(7) Uani 1 1 d . . .
H3A H 0.4930 0.3940 0.5916 0.056 Uiso 1 1 calc R . .
H3B H 0.4645 0.5087 0.5867 0.056 Uiso 1 1 calc R . .
H3C H 0.3963 0.3890 0.4878 0.056 Uiso 1 1 calc R . .
C4 C 0.1751(2) 0.2831(2) 0.41978(18) 0.0252(6) Uani 1 1 d . . .
C5 C 0.1723(2) 0.2424(2) 0.32836(18) 0.0250(6) Uani 1 1 d . . .
C6 C 0.1787(2) 0.1967(2) 0.22071(17) 0.0232(6) Uani 1 1 d . . .
C7 C 0.2176(2) 0.2720(2) 0.18240(18) 0.0236(6) Uani 1 1 d . . .
C8 C 0.2362(2) 0.3905(2) 0.24164(18) 0.0269(6) Uani 1 1 d . . .
H8A H 0.2252 0.4210 0.3110 0.032 Uiso 1 1 calc R . .
C9 C 0.2700(2) 0.4641(2) 0.20214(18) 0.0258(6) Uani 1 1 d . . .
C10 C 0.2828(3) 0.5836(2) 0.25905(19) 0.0293(6) Uani 1 1 d . . .
H10A H 0.2714 0.6154 0.3283 0.035 Uiso 1 1 calc R . .
C11 C 0.3108(3) 0.6529(2) 0.2163(2) 0.0337(7) Uani 1 1 d . . .
H11A H 0.3180 0.7323 0.2552 0.040 Uiso 1 1 calc R . .
C12 C 0.3295(3) 0.6068(2) 0.1132(2) 0.0335(7) Uani 1 1 d . . .
H12A H 0.3480 0.6560 0.0836 0.040 Uiso 1 1 calc R . .
C13 C 0.3214(3) 0.4940(2) 0.05673(19) 0.0300(6) Uani 1 1 d . . .
H13A H 0.3361 0.4653 -0.0112 0.036 Uiso 1 1 calc R . .
C14 C 0.2910(2) 0.4179(2) 0.09809(18) 0.0256(6) Uani 1 1 d . . .
C15 C 0.2764(2) 0.3021(2) 0.04045(19) 0.0263(6) Uani 1 1 d . . .
H15A H 0.2930 0.2725 -0.0268 0.032 Uiso 1 1 calc R . .
C16 C 0.2375(2) 0.2265(2) 0.07817(18) 0.0226(6) Uani 1 1 d . . .
C17 C 0.2147(2) 0.1079(2) 0.01623(17) 0.0224(6) Uani 1 1 d . . .
C18 C 0.1678(2) 0.0323(2) 0.05197(17) 0.0216(5) Uani 1 1 d . . .
C19 C 0.1396(2) -0.0856(2) -0.01073(18) 0.0231(6) Uani 1 1 d . . .
H19A H 0.1498 -0.1157 -0.0803 0.028 Uiso 1 1 calc R . .
C20 C 0.0974(2) -0.1593(2) 0.02531(18) 0.0222(5) Uani 1 1 d . . .
C21 C 0.0690(2) -0.2787(2) -0.03781(19) 0.0258(6) Uani 1 1 d . . .
H21A H 0.0789 -0.3096 -0.1075 0.031 Uiso 1 1 calc R . .
C22 C 0.0280(3) -0.3493(2) -0.0006(2) 0.0291(6) Uani 1 1 d . . .
H22A H 0.0106 -0.4288 -0.0438 0.035 Uiso 1 1 calc R . .
C23 C 0.0109(3) -0.3045(2) 0.10361(19) 0.0297(6) Uani 1 1 d . . .
H23A H -0.0188 -0.3546 0.1287 0.036 Uiso 1 1 calc R . .
C24 C 0.0367(3) -0.1916(2) 0.16672(19) 0.0289(6) Uani 1 1 d . . .
H24A H 0.0251 -0.1634 0.2358 0.035 Uiso 1 1 calc R . .
C25 C 0.0814(2) -0.1132(2) 0.13116(18) 0.0228(6) Uani 1 1 d . . .
C26 C 0.1084(2) 0.0024(2) 0.19358(18) 0.0238(6) Uani 1 1 d . . .
H26A H 0.0979 0.0318 0.2630 0.029 Uiso 1 1 calc R . .
C27 C 0.1511(2) 0.0780(2) 0.15736(17) 0.0208(5) Uani 1 1 d . . .
C28 C 0.2422(2) 0.0618(2) -0.08405(18) 0.0255(6) Uani 1 1 d . . .
C29 C 0.2690(3) 0.0225(2) -0.16566(19) 0.0269(6) Uani 1 1 d . . .
C30 C 0.3076(2) -0.0278(2) -0.26158(18) 0.0256(6) Uani 1 1 d . . .
C31 C 0.4625(3) -0.0061(2) -0.24817(19) 0.0292(6) Uani 1 1 d . . .
C32 C 0.5498(3) 0.0665(3) -0.1370(2) 0.0459(8) Uani 1 1 d . . .
H32A H 0.5877 0.1381 -0.1326 0.069 Uiso 1 1 calc R . .
H32B H 0.6168 0.0265 -0.1214 0.069 Uiso 1 1 calc R . .
H32C H 0.5015 0.0818 -0.0851 0.069 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C1 B3 C2 58.48(16) . .
C1 B3 B8 104.9(2) . .
C2 B3 B8 105.6(2) . .
C1 B3 B7 105.3(2) . .
C2 B3 B7 58.24(16) . .
B8 B3 B7 60.79(18) . .
C1 B3 B4 58.11(17) . .
C2 B3 B4 105.5(2) . .
B8 B3 B4 60.11(18) . .
B7 B3 B4 108.5(2) . .
C1 B3 H3 124.3 . .
C2 B3 H3 123.9 . .
B8 B3 H3 122.5 . .
B7 B3 H3 121.9 . .
B4 B3 H3 122.1 . .
C1 B4 B8 105.6(2) . .
C1 B4 B3 59.42(17) . .
B8 B4 B3 59.73(18) . .
C1 B4 B9 104.8(2) . .
B8 B4 B9 60.06(18) . .
B3 B4 B9 107.5(2) . .
C1 B4 B5 58.81(16) . .
B8 B4 B5 108.8(2) . .
B3 B4 B5 108.5(2) . .
B9 B4 B5 60.09(17) . .
C1 B4 H4 124.2 . .
B8 B4 H4 121.9 . .
B3 B4 H4 121.5 . .
B9 B4 H4 122.7 . .
B5 B4 H4 121.1 . .
C1 B5 B10 104.4(2) . .
C1 B5 B9 103.8(2) . .
B10 B5 B9 60.15(17) . .
C1 B5 B4 58.03(16) . .
B10 B5 B4 107.7(2) . .
B9 B5 B4 59.62(17) . .
C1 B5 B6 59.26(15) . .
B10 B5 B6 59.06(16) . .
B9 B5 B6 107.1(2) . .
B4 B5 B6 107.6(2) . .
C1 B5 H5 125.0 . .
B10 B5 H5 122.6 . .
B9 B5 H5 122.9 . .
B4 B5 H5 121.9 . .
B6 B5 H5 121.8 . .
C2 B6 C1 58.20(15) . .
C2 B6 B10 104.7(2) . .
C1 B6 B10 104.1(2) . .
C2 B6 B11 58.34(16) . .
C1 B6 B11 104.8(2) . .
B10 B6 B11 59.93(18) . .
C2 B6 B5 105.2(2) . .
C1 B6 B5 57.93(15) . .
B10 B6 B5 60.04(17) . .
B11 B6 B5 108.0(2) . .
C2 B6 H6 124.1 . .
C1 B6 H6 124.6 . .
B10 B6 H6 123.2 . .
B11 B6 H6 122.2 . .
B5 B6 H6 122.2 . .
C2 B7 B12 104.9(2) . .
C2 B7 B3 59.72(16) . .
B12 B7 B3 107.4(2) . .
C2 B7 B11 58.57(16) . .
B12 B7 B11 59.81(18) . .
B3 B7 B11 108.1(2) . .
C2 B7 B8 105.6(2) . .
B12 B7 B8 60.07(18) . .
B3 B7 B8 59.41(17) . .
B11 B7 B8 108.1(2) . .
C2 B7 H7 124.0 . .
B12 B7 H7 122.7 . .
B3 B7 H7 121.6 . .
B11 B7 H7 121.6 . .
B8 B7 H7 122.2 . .
B3 B8 B4 60.16(17) . .
B3 B8 B9 107.8(2) . .
B4 B8 B9 60.00(18) . .
B3 B8 B12 107.2(2) . .
B4 B8 B12 107.4(2) . .
B9 B8 B12 59.46(19) . .
B3 B8 B7 59.80(18) . .
B4 B8 B7 107.8(2) . .
B9 B8 B7 107.2(2) . .
B12 B8 B7 59.42(18) . .
B3 B8 H8 121.9 . .
B4 B8 H8 121.7 . .
B9 B8 H8 122.0 . .
B12 B8 H8 122.4 . .
B7 B8 H8 122.1 . .
B12 B9 B4 108.1(2) . .
B12 B9 B8 60.50(19) . .
B4 B9 B8 59.94(17) . .
B12 B9 B5 108.5(2) . .
B4 B9 B5 60.29(17) . .
B8 B9 B5 108.8(2) . .
B12 B9 B10 60.35(18) . .
B4 B9 B10 108.0(2) . .
B8 B9 B10 108.9(2) . .
B5 B9 B10 59.92(17) . .
B12 B9 H9 121.4 . .
B4 B9 H9 121.9 . .
B8 B9 H9 121.1 . .
B5 B9 H9 121.3 . .
B10 B9 H9 121.5 . .
B6 B10 B11 60.35(17) . .
B6 B10 B5 60.90(16) . .
B11 B10 B5 109.0(2) . .
B6 B10 B12 108.1(2) . .
B11 B10 B12 59.91(19) . .
B5 B10 B12 107.6(2) . .
B6 B10 B9 108.39(19) . .
B11 B10 B9 107.6(2) . .
B5 B10 B9 59.93(17) . .
B12 B10 B9 59.22(19) . .
B6 B10 H10 121.1 . .
B11 B10 H10 121.4 . .
B5 B10 H10 121.2 . .
B12 B10 H10 122.3 . .
B9 B10 H10 122.1 . .
C2 B11 B10 105.5(2) . .
C2 B11 B12 104.6(2) . .
B10 B11 B12 60.51(19) . .
C2 B11 B6 59.61(15) . .
B10 B11 B6 59.72(17) . .
B12 B11 B6 108.0(2) . .
C2 B11 B7 58.37(16) . .
B10 B11 B7 108.3(2) . .
B12 B11 B7 59.64(18) . .
B6 B11 B7 108.2(2) . .
C2 B11 H11 124.4 . .
B10 B11 H11 122.0 . .
B12 B11 H11 122.5 . .
B6 B11 H11 121.3 . .
B7 B11 H11 121.7 . .
B9 B12 B7 108.5(2) . .
B9 B12 B11 108.4(2) . .
B7 B12 B11 60.55(18) . .
B9 B12 B8 60.04(19) . .
B7 B12 B8 60.51(18) . .
B11 B12 B8 109.0(2) . .
B9 B12 B10 60.44(19) . .
B7 B12 B10 108.2(2) . .
B11 B12 B10 59.58(18) . .
B8 B12 B10 108.6(2) . .
B9 B12 H12 121.5 . .
B7 B12 H12 121.3 . .
B11 B12 H12 121.4 . .
B8 B12 H12 121.1 . .
B10 B12 H12 121.7 . .
C30 B13 C31 58.00(17) . .
C30 B13 B17 104.9(2) . .
C31 B13 B17 104.6(2) . .
C30 B13 B14 58.14(18) . .
C31 B13 B14 104.9(2) . .
B17 B13 B14 60.52(19) . .
C30 B13 B21 104.9(2) . .
C31 B13 B21 58.20(17) . .
B17 B13 B21 59.80(18) . .
B14 B13 B21 108.0(2) . .
C30 B13 H13 124.3 . .
C31 B13 H13 124.4 . .
B17 B13 H13 122.9 . .
B14 B13 H13 122.1 . .
B21 B13 H13 122.3 . .
C30 B14 B18 105.1(2) . .
C30 B14 B15 58.90(18) . .
B18 B14 B15 60.09(19) . .
C30 B14 B13 59.24(18) . .
B18 B14 B13 107.9(2) . .
B15 B14 B13 108.5(2) . .
C30 B14 B17 104.9(2) . .
B18 B14 B17 60.29(18) . .
B15 B14 B17 108.3(2) . .
B13 B14 B17 59.38(19) . .
C30 B14 H14 124.4 . .
B18 B14 H14 122.2 . .
B15 B14 H14 121.2 . .
B13 B14 H14 121.5 . .
B17 B14 H14 122.4 . .
C30 B15 B14 58.39(17) . .
C30 B15 B19 104.7(2) . .
B14 B15 B19 108.0(2) . .
C30 B15 B18 104.5(2) . .
B14 B15 B18 59.89(19) . .
B19 B15 B18 60.22(19) . .
C30 B15 B16 59.27(16) . .
B14 B15 B16 108.1(2) . .
B19 B15 B16 59.45(19) . .
B18 B15 B16 107.8(2) . .
C30 B15 H15 124.7 . .
B14 B15 H15 121.6 . .
B19 B15 H15 122.4 . .
B18 B15 H15 122.4 . .
B16 B15 H15 121.5 . .
C30 B16 C31 58.11(16) . .
C30 B16 B19 104.7(2) . .
C31 B16 B19 104.7(2) . .
C30 B16 B20 104.5(2) . .
C31 B16 B20 57.91(17) . .
B19 B16 B20 59.89(19) . .
C30 B16 B15 58.43(17) . .
C31 B16 B15 105.4(2) . .
B19 B16 B15 60.23(19) . .
B20 B16 B15 107.9(2) . .
C30 B16 H16 124.4 . .
C31 B16 H16 124.2 . .
B19 B16 H16 123.0 . .
B20 B16 H16 122.6 . .
B15 B16 H16 121.9 . .
B13 B17 B21 60.66(19) . .
B13 B17 B22 108.6(2) . .
B21 B17 B22 60.14(18) . .
B13 B17 B14 60.10(19) . .
B21 B17 B14 108.3(2) . .
B22 B17 B14 107.6(2) . .
B13 B17 B18 107.8(2) . .
B21 B17 B18 107.8(2) . .
B22 B17 B18 59.71(19) . .
B14 B17 B18 59.48(19) . .
B13 B17 H17 121.3 . .
B21 B17 H17 121.4 . .
B22 B17 H17 121.7 . .
B14 B17 H17 121.9 . .
B18 B17 H17 122.2 . .
B14 B18 B22 108.4(2) . .
B14 B18 B15 60.02(18) . .
B22 B18 B15 108.5(2) . .
B14 B18 B19 107.8(2) . .
B22 B18 B19 60.27(19) . .
B15 B18 B19 59.88(19) . .
B14 B18 B17 60.23(19) . .
B22 B18 B17 59.92(18) . .
B15 B18 B17 108.2(2) . .
B19 B18 B17 107.8(2) . .
B14 B18 H18 121.6 . .
B22 B18 H18 121.4 . .
B15 B18 H18 121.5 . .
B19 B18 H18 121.9 . .
B17 B18 H18 121.7 . .
B16 B19 B20 60.36(18) . .
B16 B19 B15 60.32(18) . .
B20 B19 B15 108.3(2) . .
B16 B19 B18 108.2(2) . .
B20 B19 B18 107.7(2) . .
B15 B19 B18 59.89(19) . .
B16 B19 B22 108.7(2) . .
B20 B19 B22 60.15(19) . .
B15 B19 B22 108.1(2) . .
B18 B19 B22 59.68(19) . .
B16 B19 H19 121.2 . .
B20 B19 H19 121.6 . .
B15 B19 H19 121.6 . .
B18 B19 H19 122.0 . .
B22 B19 H19 121.6 . .
C31 B20 B19 105.9(2) . .
C31 B20 B16 59.70(16) . .
B19 B20 B16 59.75(18) . .
C31 B20 B21 59.17(17) . .
B19 B20 B21 108.7(2) . .
B16 B20 B21 108.9(2) . .
C31 B20 B22 105.8(2) . .
B19 B20 B22 60.53(19) . .
B16 B20 B22 108.5(2) . .
B21 B20 B22 60.08(18) . .
C31 B20 H20 123.7 . .
B19 B20 H20 122.0 . .
B16 B20 H20 121.1 . .
B21 B20 H20 121.1 . .
B22 B20 H20 122.0 . .
C31 B21 B17 105.4(2) . .
C31 B21 B20 58.12(17) . .
B17 B21 B20 107.9(2) . .
C31 B21 B22 105.0(2) . .
B17 B21 B22 60.18(18) . .
B20 B21 B22 60.11(18) . .
C31 B21 B13 59.50(17) . .
B17 B21 B13 59.54(19) . .
B20 B21 B13 107.6(2) . .
B22 B21 B13 107.8(2) . .
C31 B21 H21 124.3 . .
B17 B21 H21 122.2 . .
B20 B21 H21 121.9 . .
B22 B21 H21 122.2 . .
B13 B21 H21 121.6 . .
B18 B22 B21 108.0(2) . .
B18 B22 B17 60.36(19) . .
B21 B22 B17 59.68(18) . .
B18 B22 B20 107.3(2) . .
B21 B22 B20 59.81(18) . .
B17 B22 B20 107.3(2) . .
B18 B22 B19 60.0(2) . .
B21 B22 B19 107.5(2) . .
B17 B22 B19 108.0(2) . .
B20 B22 B19 59.32(19) . .
B18 B22 H22 121.6 . .
B21 B22 H22 121.9 . .
B17 B22 H22 121.8 . .
B20 B22 H22 122.4 . .
B19 B22 H22 121.9 . .
C4 C1 C2 116.5(2) . .
C4 C1 B4 120.8(2) . .
C2 C1 B4 111.1(2) . .
C4 C1 B5 123.1(2) . .
C2 C1 B5 111.20(18) . .
B4 C1 B5 63.15(17) . .
C4 C1 B3 114.6(2) . .
C2 C1 B3 61.11(16) . .
B4 C1 B3 62.48(18) . .
B5 C1 B3 114.6(2) . .
C4 C1 B6 118.2(2) . .
C2 C1 B6 60.81(15) . .
B4 C1 B6 114.63(18) . .
B5 C1 B6 62.81(16) . .
B3 C1 B6 113.49(19) . .
C3 C2 C1 117.7(2) . .
C3 C2 B7 122.3(2) . .
C1 C2 B7 109.8(2) . .
C3 C2 B11 122.3(2) . .
C1 C2 B11 109.91(19) . .
B7 C2 B11 63.06(17) . .
C3 C2 B3 117.2(2) . .
C1 C2 B3 60.41(16) . .
B7 C2 B3 62.03(17) . .
B11 C2 B3 113.6(2) . .
C3 C2 B6 116.6(2) . .
C1 C2 B6 60.99(15) . .
B7 C2 B6 114.0(2) . .
B11 C2 B6 62.05(16) . .
B3 C2 B6 113.0(2) . .
C2 C3 H3A 109.5 . .
C2 C3 H3B 109.5 . .
H3A C3 H3B 109.5 . .
C2 C3 H3C 109.5 . .
H3A C3 H3C 109.5 . .
H3B C3 H3C 109.5 . .
C5 C4 C1 174.3(3) . .
C4 C5 C6 175.8(3) . .
C7 C6 C27 121.9(2) . .
C7 C6 C5 118.5(2) . .
C27 C6 C5 119.6(2) . .
C8 C7 C6 122.4(2) . .
C8 C7 C16 118.5(2) . .
C6 C7 C16 119.0(2) . .
C9 C8 C7 122.2(2) . .
C9 C8 H8A 118.9 . .
C7 C8 H8A 118.9 . .
C8 C9 C10 122.7(2) . .
C8 C9 C14 118.9(2) . .
C10 C9 C14 118.4(2) . .
C11 C10 C9 121.2(2) . .
C11 C10 H10A 119.4 . .
C9 C10 H10A 119.4 . .
C10 C11 C12 120.1(3) . .
C10 C11 H11A 119.9 . .
C12 C11 H11A 119.9 . .
C13 C12 C11 121.1(2) . .
C13 C12 H12A 119.5 . .
C11 C12 H12A 119.5 . .
C12 C13 C14 120.7(2) . .
C12 C13 H13A 119.6 . .
C14 C13 H13A 119.6 . .
C15 C14 C13 122.1(2) . .
C15 C14 C9 119.4(2) . .
C13 C14 C9 118.4(2) . .
C14 C15 C16 122.1(2) . .
C14 C15 H15A 118.9 . .
C16 C15 H15A 118.9 . .
C15 C16 C17 122.0(2) . .
C15 C16 C7 118.7(2) . .
C17 C16 C7 119.2(2) . .
C16 C17 C18 121.7(2) . .
C16 C17 C28 119.7(2) . .
C18 C17 C28 118.6(2) . .
C19 C18 C17 122.3(2) . .
C19 C18 C27 118.8(2) . .
C17 C18 C27 118.8(2) . .
C20 C19 C18 122.3(2) . .
C20 C19 H19A 118.9 . .
C18 C19 H19A 118.9 . .
C19 C20 C21 122.5(2) . .
C19 C20 C25 118.7(2) . .
C21 C20 C25 118.8(2) . .
C22 C21 C20 121.4(2) . .
C22 C21 H21A 119.3 . .
C20 C21 H21A 119.3 . .
C21 C22 C23 120.2(3) . .
C21 C22 H22A 119.9 . .
C23 C22 H22A 119.9 . .
C24 C23 C22 120.6(2) . .
C24 C23 H23A 119.7 . .
C22 C23 H23A 119.7 . .
C23 C24 C25 121.2(2) . .
C23 C24 H24A 119.4 . .
C25 C24 H24A 119.4 . .
C26 C25 C24 122.6(2) . .
C26 C25 C20 119.7(2) . .
C24 C25 C20 117.7(2) . .
C25 C26 C27 121.9(2) . .
C25 C26 H26A 119.0 . .
C27 C26 H26A 119.0 . .
C26 C27 C6 122.3(2) . .
C26 C27 C18 118.6(2) . .
C6 C27 C18 119.1(2) . .
C29 C28 C17 177.5(3) . .
C28 C29 C30 176.5(3) . .
C29 C30 C31 116.9(2) . .
C29 C30 B14 121.5(2) . .
C31 C30 B14 111.2(2) . .
C29 C30 B15 122.4(2) . .
C31 C30 B15 110.79(19) . .
B14 C30 B15 62.71(19) . .
C29 C30 B13 115.7(2) . .
C31 C30 B13 61.50(18) . .
B14 C30 B13 62.6(2) . .
B15 C30 B13 114.4(2) . .
C29 C30 B16 117.3(2) . .
C31 C30 B16 60.99(17) . .
B14 C30 B16 114.1(2) . .
B15 C30 B16 62.30(19) . .
B13 C30 B16 114.0(2) . .
C32 C31 C30 117.3(2) . .
C32 C31 B20 122.3(2) . .
C30 C31 B20 110.2(2) . .
C32 C31 B21 122.5(2) . .
C30 C31 B21 110.2(2) . .
B20 C31 B21 62.71(18) . .
C32 C31 B16 116.4(2) . .
C30 C31 B16 60.90(17) . .
B20 C31 B16 62.39(18) . .
B21 C31 B16 114.0(2) . .
C32 C31 B13 117.2(2) . .
C30 C31 B13 60.50(17) . .
B20 C31 B13 113.6(2) . .
B21 C31 B13 62.29(19) . .
B16 C31 B13 113.0(2) . .
C31 C32 H32A 109.5 . .
C31 C32 H32B 109.5 . .
H32A C32 H32B 109.5 . .
C31 C32 H32C 109.5 . .
H32A C32 H32C 109.5 . .
H32B C32 H32C 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
B3 C1 1.716(4) .
B3 C2 1.728(4) .
B3 B8 1.760(4) .
B3 B7 1.767(4) .
B3 B4 1.768(5) .
B3 H3 1.1200 .
B4 C1 1.692(4) .
B4 B8 1.767(5) .
B4 B9 1.768(4) .
B4 B5 1.780(4) .
B4 H4 1.1200 .
B5 C1 1.706(4) .
B5 B10 1.776(4) .
B5 B9 1.776(5) .
B5 B6 1.791(5) .
B5 H5 1.1200 .
B6 C2 1.728(4) .
B6 C1 1.731(4) .
B6 B10 1.758(4) .
B6 B11 1.770(4) .
B6 H6 1.1200 .
B7 C2 1.701(4) .
B7 B12 1.765(5) .
B7 B11 1.781(4) .
B7 B8 1.785(5) .
B7 H7 1.1200 .
B8 B9 1.769(5) .
B8 B12 1.777(4) .
B8 H8 1.1200 .
B9 B12 1.758(5) .
B9 B10 1.780(4) .
B9 H9 1.1200 .
B10 B11 1.762(5) .
B10 B12 1.779(5) .
B10 H10 1.1200 .
B11 C2 1.705(4) .
B11 B12 1.768(5) .
B11 H11 1.1200 .
B12 H12 1.1200 .
B13 C30 1.715(4) .
B13 C31 1.731(4) .
B13 B17 1.759(4) .
B13 B14 1.772(5) .
B13 B21 1.779(5) .
B13 H13 1.1200 .
B14 C30 1.695(4) .
B14 B18 1.766(4) .
B14 B15 1.768(5) .
B14 B17 1.780(5) .
B14 H14 1.1200 .
B15 C30 1.704(4) .
B15 B19 1.769(5) .
B15 B18 1.770(5) .
B15 B16 1.771(5) .
B15 H15 1.1200 .
B16 C30 1.719(4) .
B16 C31 1.721(4) .
B16 B19 1.755(4) .
B16 B20 1.766(5) .
B16 H16 1.1200 .
B17 B21 1.764(5) .
B17 B22 1.773(4) .
B17 B18 1.781(5) .
B17 H17 1.1200 .
B18 B22 1.769(5) .
B18 B19 1.776(5) .
B18 H18 1.1200 .
B19 B20 1.758(5) .
B19 B22 1.779(5) .
B19 H19 1.1200 .
B20 C31 1.689(4) .
B20 B21 1.767(5) .
B20 B22 1.773(4) .
B20 H20 1.1200 .
B21 C31 1.708(4) .
B21 B22 1.772(4) .
B21 H21 1.1200 .
B22 H22 1.1200 .
C1 C4 1.441(3) .
C1 C2 1.682(4) .
C2 C3 1.501(4) .
C3 H3A 0.9800 .
C3 H3B 0.9800 .
C3 H3C 0.9800 .
C4 C5 1.189(3) .
C5 C6 1.432(3) .
C6 C7 1.412(3) .
C6 C27 1.415(3) .
C7 C8 1.411(3) .
C7 C16 1.444(3) .
C8 C9 1.386(3) .
C8 H8A 0.9500 .
C9 C10 1.425(4) .
C9 C14 1.447(3) .
C10 C11 1.355(4) .
C10 H10A 0.9500 .
C11 C12 1.423(4) .
C11 H11A 0.9500 .
C12 C13 1.355(4) .
C12 H12A 0.9500 .
C13 C14 1.426(3) .
C13 H13A 0.9500 .
C14 C15 1.381(3) .
C15 C16 1.409(3) .
C15 H15A 0.9500 .
C16 C17 1.413(3) .
C17 C18 1.420(3) .
C17 C28 1.430(3) .
C18 C19 1.405(3) .
C18 C27 1.444(3) .
C19 C20 1.382(3) .
C19 H19A 0.9500 .
C20 C21 1.422(3) .
C20 C25 1.447(3) .
C21 C22 1.357(3) .
C21 H21A 0.9500 .
C22 C23 1.430(3) .
C22 H22A 0.9500 .
C23 C24 1.353(4) .
C23 H23A 0.9500 .
C24 C25 1.439(3) .
C24 H24A 0.9500 .
C25 C26 1.380(3) .
C26 C27 1.408(3) .
C26 H26A 0.9500 .
C28 C29 1.189(3) .
C29 C30 1.442(3) .
C30 C31 1.671(4) .
C31 C32 1.515(4) .
C32 H32A 0.9800 .
C32 H32B 0.9800 .
C32 H32C 0.9800 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
C2 B3 B4 C1 -35.72(17) . . . .
B8 B3 B4 C1 -135.0(2) . . . .
B7 B3 B4 C1 -96.8(2) . . . .
C1 B3 B4 B8 135.0(2) . . . .
C2 B3 B4 B8 99.3(2) . . . .
B7 B3 B4 B8 38.2(2) . . . .
C1 B3 B4 B9 97.2(2) . . . .
C2 B3 B4 B9 61.5(2) . . . .
B8 B3 B4 B9 -37.8(2) . . . .
B7 B3 B4 B9 0.4(3) . . . .
C1 B3 B4 B5 33.65(18) . . . .
C2 B3 B4 B5 -2.1(3) . . . .
B8 B3 B4 B5 -101.4(2) . . . .
B7 B3 B4 B5 -63.2(3) . . . .
B8 B4 B5 C1 -97.3(2) . . . .
B3 B4 B5 C1 -33.90(18) . . . .
B9 B4 B5 C1 -133.8(2) . . . .
C1 B4 B5 B10 96.2(2) . . . .
B8 B4 B5 B10 -1.1(3) . . . .
B3 B4 B5 B10 62.3(2) . . . .
B9 B4 B5 B10 -37.6(2) . . . .
C1 B4 B5 B9 133.8(2) . . . .
B8 B4 B5 B9 36.5(2) . . . .
B3 B4 B5 B9 100.0(2) . . . .
C1 B4 B5 B6 33.94(18) . . . .
B8 B4 B5 B6 -63.4(3) . . . .
B3 B4 B5 B6 0.0(3) . . . .
B9 B4 B5 B6 -99.9(2) . . . .
C1 B5 B6 C2 35.43(17) . . . .
B10 B5 B6 C2 -98.4(2) . . . .
B9 B5 B6 C2 -60.8(2) . . . .
B4 B5 B6 C2 2.0(2) . . . .
B10 B5 B6 C1 -133.9(2) . . . .
B9 B5 B6 C1 -96.2(2) . . . .
B4 B5 B6 C1 -33.44(18) . . . .
C1 B5 B6 B10 133.9(2) . . . .
B9 B5 B6 B10 37.7(2) . . . .
B4 B5 B6 B10 100.4(2) . . . .
C1 B5 B6 B11 96.5(2) . . . .
B10 B5 B6 B11 -37.4(2) . . . .
B9 B5 B6 B11 0.3(3) . . . .
B4 B5 B6 B11 63.1(2) . . . .
C1 B3 B7 C2 36.25(19) . . . .
B8 B3 B7 C2 135.0(2) . . . .
B4 B3 B7 C2 97.2(2) . . . .
C1 B3 B7 B12 -61.2(3) . . . .
C2 B3 B7 B12 -97.4(2) . . . .
B8 B3 B7 B12 37.6(2) . . . .
B4 B3 B7 B12 -0.3(3) . . . .
C1 B3 B7 B11 1.9(3) . . . .
C2 B3 B7 B11 -34.3(2) . . . .
B8 B3 B7 B11 100.7(3) . . . .
B4 B3 B7 B11 62.8(3) . . . .
C1 B3 B7 B8 -98.8(2) . . . .
C2 B3 B7 B8 -135.0(2) . . . .
B4 B3 B7 B8 -37.9(2) . . . .
C1 B3 B8 B4 -38.39(19) . . . .
C2 B3 B8 B4 -99.2(2) . . . .
B7 B3 B8 B4 -137.8(2) . . . .
C1 B3 B8 B9 -0.5(3) . . . .
C2 B3 B8 B9 -61.3(3) . . . .
B7 B3 B8 B9 -99.9(2) . . . .
B4 B3 B8 B9 37.9(2) . . . .
C1 B3 B8 B12 62.1(3) . . . .
C2 B3 B8 B12 1.3(3) . . . .
B7 B3 B8 B12 -37.3(2) . . . .
B4 B3 B8 B12 100.5(3) . . . .
C1 B3 B8 B7 99.4(2) . . . .
C2 B3 B8 B7 38.6(2) . . . .
B4 B3 B8 B7 137.8(2) . . . .
C1 B4 B8 B3 39.19(19) . . . .
B9 B4 B8 B3 137.5(2) . . . .
B5 B4 B8 B3 101.0(2) . . . .
C1 B4 B8 B9 -98.3(2) . . . .
B3 B4 B8 B9 -137.5(2) . . . .
B5 B4 B8 B9 -36.6(2) . . . .
C1 B4 B8 B12 -61.0(3) . . . .
B3 B4 B8 B12 -100.2(3) . . . .
B9 B4 B8 B12 37.3(2) . . . .
B5 B4 B8 B12 0.8(3) . . . .
C1 B4 B8 B7 1.6(3) . . . .
B3 B4 B8 B7 -37.6(2) . . . .
B9 B4 B8 B7 100.0(2) . . . .
B5 B4 B8 B7 63.4(3) . . . .
C2 B7 B8 B3 -39.32(19) . . . .
B12 B7 B8 B3 -137.8(2) . . . .
B11 B7 B8 B3 -100.7(2) . . . .
C2 B7 B8 B4 -1.6(3) . . . .
B12 B7 B8 B4 -100.1(2) . . . .
B3 B7 B8 B4 37.7(2) . . . .
B11 B7 B8 B4 -63.0(2) . . . .
C2 B7 B8 B9 61.6(2) . . . .
B12 B7 B8 B9 -36.8(2) . . . .
B3 B7 B8 B9 100.9(2) . . . .
B11 B7 B8 B9 0.2(3) . . . .
C2 B7 B8 B12 98.5(2) . . . .
B3 B7 B8 B12 137.8(2) . . . .
B11 B7 B8 B12 37.0(2) . . . .
C1 B4 B9 B12 61.8(3) . . . .
B8 B4 B9 B12 -38.0(2) . . . .
B3 B4 B9 B12 -0.3(3) . . . .
B5 B4 B9 B12 101.4(2) . . . .
C1 B4 B9 B8 99.8(2) . . . .
B3 B4 B9 B8 37.7(2) . . . .
B5 B4 B9 B8 139.4(2) . . . .
C1 B4 B9 B5 -39.7(2) . . . .
B8 B4 B9 B5 -139.4(2) . . . .
B3 B4 B9 B5 -101.7(2) . . . .
C1 B4 B9 B10 -2.0(3) . . . .
B8 B4 B9 B10 -101.8(3) . . . .
B3 B4 B9 B10 -64.1(3) . . . .
B5 B4 B9 B10 37.6(2) . . . .
B3 B8 B9 B12 99.8(2) . . . .
B4 B8 B9 B12 137.8(2) . . . .
B7 B8 B9 B12 36.82(19) . . . .
B3 B8 B9 B4 -38.0(2) . . . .
B12 B8 B9 B4 -137.8(2) . . . .
B7 B8 B9 B4 -101.0(2) . . . .
B3 B8 B9 B5 -1.3(3) . . . .
B4 B8 B9 B5 36.7(2) . . . .
B12 B8 B9 B5 -101.1(2) . . . .
B7 B8 B9 B5 -64.3(3) . . . .
B3 B8 B9 B10 62.4(3) . . . .
B4 B8 B9 B10 100.3(2) . . . .
B12 B8 B9 B10 -37.4(2) . . . .
B7 B8 B9 B10 -0.6(3) . . . .
C1 B5 B9 B12 -61.7(2) . . . .
B10 B5 B9 B12 37.1(2) . . . .
B4 B5 B9 B12 -100.8(2) . . . .
B6 B5 B9 B12 0.0(3) . . . .
C1 B5 B9 B4 39.06(19) . . . .
B10 B5 B9 B4 137.9(2) . . . .
B6 B5 B9 B4 100.7(2) . . . .
C1 B5 B9 B8 2.6(3) . . . .
B10 B5 B9 B8 101.4(3) . . . .
B4 B5 B9 B8 -36.5(2) . . . .
B6 B5 B9 B8 64.2(3) . . . .
C1 B5 B9 B10 -98.8(2) . . . .
B4 B5 B9 B10 -137.9(2) . . . .
B6 B5 B9 B10 -37.2(2) . . . .
C2 B6 B10 B11 -38.83(19) . . . .
C1 B6 B10 B11 -99.1(2) . . . .
B5 B6 B10 B11 -138.2(2) . . . .
C2 B6 B10 B5 99.3(2) . . . .
C1 B6 B10 B5 39.0(2) . . . .
B11 B6 B10 B5 138.2(2) . . . .
C2 B6 B10 B12 -1.2(3) . . . .
C1 B6 B10 B12 -61.5(3) . . . .
B11 B6 B10 B12 37.6(2) . . . .
B5 B6 B10 B12 -100.6(2) . . . .
C2 B6 B10 B9 61.4(3) . . . .
C1 B6 B10 B9 1.2(3) . . . .
B11 B6 B10 B9 100.3(3) . . . .
B5 B6 B10 B9 -37.9(2) . . . .
C1 B5 B10 B6 -39.76(19) . . . .
B9 B5 B10 B6 -137.7(2) . . . .
B4 B5 B10 B6 -100.3(2) . . . .
C1 B5 B10 B11 -1.9(3) . . . .
B9 B5 B10 B11 -99.9(2) . . . .
B4 B5 B10 B11 -62.5(3) . . . .
B6 B5 B10 B11 37.8(2) . . . .
C1 B5 B10 B12 61.5(3) . . . .
B9 B5 B10 B12 -36.4(2) . . . .
B4 B5 B10 B12 1.0(3) . . . .
B6 B5 B10 B12 101.3(2) . . . .
C1 B5 B10 B9 97.9(2) . . . .
B4 B5 B10 B9 37.4(2) . . . .
B6 B5 B10 B9 137.7(2) . . . .
B12 B9 B10 B6 -100.5(2) . . . .
B4 B9 B10 B6 0.5(3) . . . .
B8 B9 B10 B6 -63.0(3) . . . .
B5 B9 B10 B6 38.3(2) . . . .
B12 B9 B10 B11 -36.69(19) . . . .
B4 B9 B10 B11 64.4(3) . . . .
B8 B9 B10 B11 0.8(3) . . . .
B5 B9 B10 B11 102.1(2) . . . .
B12 B9 B10 B5 -138.8(2) . . . .
B4 B9 B10 B5 -37.8(2) . . . .
B8 B9 B10 B5 -101.3(2) . . . .
B4 B9 B10 B12 101.0(3) . . . .
B8 B9 B10 B12 37.5(2) . . . .
B5 B9 B10 B12 138.8(2) . . . .
B6 B10 B11 C2 39.63(19) . . . .
B5 B10 B11 C2 1.6(3) . . . .
B12 B10 B11 C2 -98.3(2) . . . .
B9 B10 B11 C2 -61.9(2) . . . .
B6 B10 B11 B12 137.9(2) . . . .
B5 B10 B11 B12 99.9(2) . . . .
B9 B10 B11 B12 36.39(19) . . . .
B5 B10 B11 B6 -38.1(2) . . . .
B12 B10 B11 B6 -137.9(2) . . . .
B9 B10 B11 B6 -101.5(2) . . . .
B6 B10 B11 B7 100.8(2) . . . .
B5 B10 B11 B7 62.8(3) . . . .
B12 B10 B11 B7 -37.08(19) . . . .
B9 B10 B11 B7 -0.7(3) . . . .
C1 B6 B11 C2 -36.59(18) . . . .
B10 B6 B11 C2 -134.6(2) . . . .
B5 B6 B11 C2 -97.1(2) . . . .
C2 B6 B11 B10 134.6(2) . . . .
C1 B6 B11 B10 98.0(2) . . . .
B5 B6 B11 B10 37.42(19) . . . .
C2 B6 B11 B12 96.7(2) . . . .
C1 B6 B11 B12 60.1(2) . . . .
B10 B6 B11 B12 -37.84(19) . . . .
B5 B6 B11 B12 -0.4(3) . . . .
C2 B6 B11 B7 33.6(2) . . . .
C1 B6 B11 B7 -3.0(3) . . . .
B10 B6 B11 B7 -100.9(3) . . . .
B5 B6 B11 B7 -63.5(3) . . . .
B12 B7 B11 C2 134.8(2) . . . .
B3 B7 B11 C2 34.8(2) . . . .
B8 B7 B11 C2 97.6(2) . . . .
C2 B7 B11 B10 -97.3(2) . . . .
B12 B7 B11 B10 37.5(2) . . . .
B3 B7 B11 B10 -62.5(3) . . . .
B8 B7 B11 B10 0.3(3) . . . .
C2 B7 B11 B12 -134.8(2) . . . .
B3 B7 B11 B12 -100.0(3) . . . .
B8 B7 B11 B12 -37.2(2) . . . .
C2 B7 B11 B6 -34.1(2) . . . .
B12 B7 B11 B6 100.7(2) . . . .
B3 B7 B11 B6 0.7(3) . . . .
B8 B7 B11 B6 63.5(3) . . . .
B4 B9 B12 B7 0.1(3) . . . .
B8 B9 B12 B7 -37.6(2) . . . .
B5 B9 B12 B7 64.0(3) . . . .
B10 B9 B12 B7 100.9(2) . . . .
B4 B9 B12 B11 -64.1(3) . . . .
B8 B9 B12 B11 -101.8(2) . . . .
B5 B9 B12 B11 -0.2(3) . . . .
B10 B9 B12 B11 36.72(19) . . . .
B4 B9 B12 B8 37.7(2) . . . .
B5 B9 B12 B8 101.6(2) . . . .
B10 B9 B12 B8 138.5(2) . . . .
B4 B9 B12 B10 -100.8(2) . . . .
B8 B9 B12 B10 -138.5(2) . . . .
B5 B9 B12 B10 -36.94(19) . . . .
C2 B7 B12 B9 -62.3(3) . . . .
B3 B7 B12 B9 0.1(3) . . . .
B11 B7 B12 B9 -101.1(2) . . . .
B8 B7 B12 B9 37.4(2) . . . .
C2 B7 B12 B11 38.8(2) . . . .
B3 B7 B12 B11 101.2(2) . . . .
B8 B7 B12 B11 138.5(2) . . . .
C2 B7 B12 B8 -99.7(2) . . . .
B3 B7 B12 B8 -37.3(2) . . . .
B11 B7 B12 B8 -138.5(2) . . . .
C2 B7 B12 B10 1.8(3) . . . .
B3 B7 B12 B10 64.2(3) . . . .
B11 B7 B12 B10 -37.0(2) . . . .
B8 B7 B12 B10 101.5(2) . . . .
C2 B11 B12 B9 62.7(3) . . . .
B10 B11 B12 B9 -37.1(2) . . . .
B6 B11 B12 B9 0.4(3) . . . .
B7 B11 B12 B9 101.3(2) . . . .
C2 B11 B12 B7 -38.6(2) . . . .
B10 B11 B12 B7 -138.4(2) . . . .
B6 B11 B12 B7 -100.9(2) . . . .
C2 B11 B12 B8 -1.1(3) . . . .
B10 B11 B12 B8 -100.9(3) . . . .
B6 B11 B12 B8 -63.4(3) . . . .
B7 B11 B12 B8 37.6(2) . . . .
C2 B11 B12 B10 99.8(2) . . . .
B6 B11 B12 B10 37.49(18) . . . .
B7 B11 B12 B10 138.4(2) . . . .
B3 B8 B12 B9 -100.9(2) . . . .
B4 B8 B12 B9 -37.6(2) . . . .
B7 B8 B12 B9 -138.3(2) . . . .
B3 B8 B12 B7 37.4(2) . . . .
B4 B8 B12 B7 100.7(2) . . . .
B9 B8 B12 B7 138.3(2) . . . .
B3 B8 B12 B11 -0.2(3) . . . .
B4 B8 B12 B11 63.1(3) . . . .
B9 B8 B12 B11 100.7(3) . . . .
B7 B8 B12 B11 -37.6(2) . . . .
B3 B8 B12 B10 -63.5(3) . . . .
B4 B8 B12 B10 -0.2(3) . . . .
B9 B8 B12 B10 37.4(2) . . . .
B7 B8 B12 B10 -100.9(2) . . . .
B6 B10 B12 B9 101.1(2) . . . .
B11 B10 B12 B9 138.8(2) . . . .
B5 B10 B12 B9 36.7(2) . . . .
B6 B10 B12 B7 -0.3(3) . . . .
B11 B10 B12 B7 37.5(2) . . . .
B5 B10 B12 B7 -64.6(3) . . . .
B9 B10 B12 B7 -101.4(2) . . . .
B6 B10 B12 B11 -37.78(19) . . . .
B5 B10 B12 B11 -102.1(2) . . . .
B9 B10 B12 B11 -138.8(2) . . . .
B6 B10 B12 B8 63.8(3) . . . .
B11 B10 B12 B8 101.6(2) . . . .
B5 B10 B12 B8 -0.5(3) . . . .
B9 B10 B12 B8 -37.2(2) . . . .
C31 B13 B14 C30 -35.84(18) . . . .
B17 B13 B14 C30 -134.4(2) . . . .
B21 B13 B14 C30 -96.7(2) . . . .
C30 B13 B14 B18 97.2(2) . . . .
C31 B13 B14 B18 61.4(3) . . . .
B17 B13 B14 B18 -37.2(2) . . . .
B21 B13 B14 B18 0.5(3) . . . .
C30 B13 B14 B15 33.62(19) . . . .
C31 B13 B14 B15 -2.2(3) . . . .
B17 B13 B14 B15 -100.8(2) . . . .
B21 B13 B14 B15 -63.1(3) . . . .
C30 B13 B14 B17 134.4(2) . . . .
C31 B13 B14 B17 98.6(2) . . . .
B21 B13 B14 B17 37.7(2) . . . .
B18 B14 B15 C30 -134.2(2) . . . .
B13 B14 B15 C30 -33.75(19) . . . .
B17 B14 B15 C30 -96.7(2) . . . .
C30 B14 B15 B19 96.6(2) . . . .
B18 B14 B15 B19 -37.7(2) . . . .
B13 B14 B15 B19 62.8(3) . . . .
B17 B14 B15 B19 -0.1(3) . . . .
C30 B14 B15 B18 134.2(2) . . . .
B13 B14 B15 B18 100.5(2) . . . .
B17 B14 B15 B18 37.5(2) . . . .
C30 B14 B15 B16 33.72(19) . . . .
B18 B14 B15 B16 -100.5(2) . . . .
B13 B14 B15 B16 0.0(3) . . . .
B17 B14 B15 B16 -63.0(3) . . . .
B14 B15 B16 C30 -33.37(19) . . . .
B19 B15 B16 C30 -134.0(2) . . . .
B18 B15 B16 C30 -96.7(2) . . . .
C30 B15 B16 C31 35.66(18) . . . .
B14 B15 B16 C31 2.3(3) . . . .
B19 B15 B16 C31 -98.3(2) . . . .
B18 B15 B16 C31 -61.0(3) . . . .
C30 B15 B16 B19 134.0(2) . . . .
B14 B15 B16 B19 100.6(2) . . . .
B18 B15 B16 B19 37.3(2) . . . .
C30 B15 B16 B20 96.3(2) . . . .
B14 B15 B16 B20 62.9(3) . . . .
B19 B15 B16 B20 -37.7(2) . . . .
B18 B15 B16 B20 -0.3(3) . . . .
C30 B13 B17 B21 98.8(2) . . . .
C31 B13 B17 B21 38.6(2) . . . .
B14 B13 B17 B21 137.7(2) . . . .
C30 B13 B17 B22 61.2(3) . . . .
C31 B13 B17 B22 1.0(3) . . . .
B14 B13 B17 B22 100.0(3) . . . .
B21 B13 B17 B22 -37.6(2) . . . .
C30 B13 B17 B14 -38.9(2) . . . .
C31 B13 B17 B14 -99.1(2) . . . .
B21 B13 B17 B14 -137.7(2) . . . .
C30 B13 B17 B18 -2.1(3) . . . .
C31 B13 B17 B18 -62.2(3) . . . .
B14 B13 B17 B18 36.8(2) . . . .
B21 B13 B17 B18 -100.8(3) . . . .
C30 B14 B17 B13 39.4(2) . . . .
B18 B14 B17 B13 138.5(2) . . . .
B15 B14 B17 B13 101.1(2) . . . .
C30 B14 B17 B21 1.2(3) . . . .
B18 B14 B17 B21 100.3(3) . . . .
B15 B14 B17 B21 62.9(3) . . . .
B13 B14 B17 B21 -38.2(2) . . . .
C30 B14 B17 B22 -62.4(3) . . . .
B18 B14 B17 B22 36.7(2) . . . .
B15 B14 B17 B22 -0.7(3) . . . .
B13 B14 B17 B22 -101.8(2) . . . .
C30 B14 B17 B18 -99.1(2) . . . .
B15 B14 B17 B18 -37.5(2) . . . .
B13 B14 B17 B18 -138.5(2) . . . .
C30 B14 B18 B22 61.8(3) . . . .
B15 B14 B18 B22 101.2(3) . . . .
B13 B14 B18 B22 -0.2(3) . . . .
B17 B14 B18 B22 -37.0(2) . . . .
C30 B14 B18 B15 -39.5(2) . . . .
B13 B14 B18 B15 -101.4(3) . . . .
B17 B14 B18 B15 -138.2(3) . . . .
C30 B14 B18 B19 -2.0(3) . . . .
B15 B14 B18 B19 37.5(2) . . . .
B13 B14 B18 B19 -64.0(3) . . . .
B17 B14 B18 B19 -100.8(3) . . . .
C30 B14 B18 B17 98.8(3) . . . .
B15 B14 B18 B17 138.2(3) . . . .
B13 B14 B18 B17 36.8(2) . . . .
C30 B15 B18 B14 39.1(2) . . . .
B19 B15 B18 B14 138.0(3) . . . .
B16 B15 B18 B14 101.0(2) . . . .
C30 B15 B18 B22 -61.9(3) . . . .
B14 B15 B18 B22 -101.0(3) . . . .
B19 B15 B18 B22 37.0(2) . . . .
B16 B15 B18 B22 0.0(3) . . . .
C30 B15 B18 B19 -98.9(3) . . . .
B14 B15 B18 B19 -138.0(3) . . . .
B16 B15 B18 B19 -37.0(2) . . . .
C30 B15 B18 B17 1.6(3) . . . .
B14 B15 B18 B17 -37.5(2) . . . .
B19 B15 B18 B17 100.5(3) . . . .
B16 B15 B18 B17 63.5(3) . . . .
B13 B17 B18 B14 -37.1(2) . . . .
B21 B17 B18 B14 -101.2(2) . . . .
B22 B17 B18 B14 -138.7(2) . . . .
B13 B17 B18 B22 101.6(2) . . . .
B21 B17 B18 B22 37.5(2) . . . .
B14 B17 B18 B22 138.7(2) . . . .
B13 B17 B18 B15 0.3(3) . . . .
B21 B17 B18 B15 -63.8(3) . . . .
B22 B17 B18 B15 -101.3(3) . . . .
B14 B17 B18 B15 37.4(2) . . . .
B13 B17 B18 B19 63.6(3) . . . .
B21 B17 B18 B19 -0.4(3) . . . .
B22 B17 B18 B19 -37.9(2) . . . .
B14 B17 B18 B19 100.7(2) . . . .
C30 B16 B19 B20 -98.4(2) . . . .
C31 B16 B19 B20 -38.1(2) . . . .
B15 B16 B19 B20 -137.7(2) . . . .
C30 B16 B19 B15 39.3(2) . . . .
C31 B16 B19 B15 99.6(2) . . . .
B20 B16 B19 B15 137.7(2) . . . .
C30 B16 B19 B18 2.0(3) . . . .
C31 B16 B19 B18 62.3(3) . . . .
B20 B16 B19 B18 100.4(3) . . . .
B15 B16 B19 B18 -37.3(2) . . . .
C30 B16 B19 B22 -61.3(3) . . . .
C31 B16 B19 B22 -1.0(3) . . . .
B20 B16 B19 B22 37.1(2) . . . .
B15 B16 B19 B22 -100.6(3) . . . .
C30 B15 B19 B16 -39.8(2) . . . .
B14 B15 B19 B16 -100.8(2) . . . .
B18 B15 B19 B16 -138.3(2) . . . .
C30 B15 B19 B20 -1.7(3) . . . .
B14 B15 B19 B20 -62.8(3) . . . .
B18 B15 B19 B20 -100.3(3) . . . .
B16 B15 B19 B20 38.0(2) . . . .
C30 B15 B19 B18 98.5(3) . . . .
B14 B15 B19 B18 37.5(2) . . . .
B16 B15 B19 B18 138.3(2) . . . .
C30 B15 B19 B22 61.9(3) . . . .
B14 B15 B19 B22 0.9(3) . . . .
B18 B15 B19 B22 -36.6(2) . . . .
B16 B15 B19 B22 101.7(2) . . . .
B14 B18 B19 B16 0.0(3) . . . .
B22 B18 B19 B16 -101.4(2) . . . .
B15 B18 B19 B16 37.5(2) . . . .
B17 B18 B19 B16 -63.6(3) . . . .
B14 B18 B19 B20 63.8(3) . . . .
B22 B18 B19 B20 -37.64(19) . . . .
B15 B18 B19 B20 101.3(2) . . . .
B17 B18 B19 B20 0.2(3) . . . .
B14 B18 B19 B15 -37.5(2) . . . .
B22 B18 B19 B15 -138.9(2) . . . .
B17 B18 B19 B15 -101.1(2) . . . .
B14 B18 B19 B22 101.4(2) . . . .
B15 B18 B19 B22 138.9(2) . . . .
B17 B18 B19 B22 37.80(19) . . . .
B16 B19 B20 C31 39.3(2) . . . .
B15 B19 B20 C31 1.3(3) . . . .
B18 B19 B20 C31 -62.0(3) . . . .
B22 B19 B20 C31 -99.5(2) . . . .
B15 B19 B20 B16 -38.0(2) . . . .
B18 B19 B20 B16 -101.3(2) . . . .
B22 B19 B20 B16 -138.7(2) . . . .
B16 B19 B20 B21 101.5(2) . . . .
B15 B19 B20 B21 63.5(3) . . . .
B18 B19 B20 B21 0.2(3) . . . .
B22 B19 B20 B21 -37.23(19) . . . .
B16 B19 B20 B22 138.7(2) . . . .
B15 B19 B20 B22 100.8(3) . . . .
B18 B19 B20 B22 37.44(19) . . . .
C30 B16 B20 C31 -36.33(19) . . . .
B19 B16 B20 C31 -135.2(2) . . . .
B15 B16 B20 C31 -97.3(2) . . . .
C30 B16 B20 B19 98.8(2) . . . .
C31 B16 B20 B19 135.2(2) . . . .
B15 B16 B20 B19 37.8(2) . . . .
C30 B16 B20 B21 -2.3(3) . . . .
C31 B16 B20 B21 34.1(2) . . . .
B19 B16 B20 B21 -101.1(3) . . . .
B15 B16 B20 B21 -63.2(3) . . . .
C30 B16 B20 B22 61.6(3) . . . .
C31 B16 B20 B22 97.9(2) . . . .
B19 B16 B20 B22 -37.3(2) . . . .
B15 B16 B20 B22 0.6(3) . . . .
B13 B17 B21 C31 -39.4(2) . . . .
B22 B17 B21 C31 98.8(2) . . . .
B14 B17 B21 C31 -1.5(3) . . . .
B18 B17 B21 C31 61.4(3) . . . .
B13 B17 B21 B20 -100.3(2) . . . .
B22 B17 B21 B20 37.9(2) . . . .
B14 B17 B21 B20 -62.3(3) . . . .
B18 B17 B21 B20 0.6(3) . . . .
B13 B17 B21 B22 -138.2(2) . . . .
B14 B17 B21 B22 -100.2(3) . . . .
B18 B17 B21 B22 -37.3(2) . . . .
B22 B17 B21 B13 138.2(2) . . . .
B14 B17 B21 B13 38.0(2) . . . .
B18 B17 B21 B13 100.9(2) . . . .
B19 B20 B21 C31 -97.8(2) . . . .
B16 B20 B21 C31 -34.3(2) . . . .
B22 B20 B21 C31 -135.2(2) . . . .
C31 B20 B21 B17 97.3(2) . . . .
B19 B20 B21 B17 -0.5(3) . . . .
B16 B20 B21 B17 63.0(3) . . . .
B22 B20 B21 B17 -37.9(2) . . . .
C31 B20 B21 B22 135.2(2) . . . .
B19 B20 B21 B22 37.4(2) . . . .
B16 B20 B21 B22 100.9(3) . . . .
C31 B20 B21 B13 34.5(2) . . . .
B19 B20 B21 B13 -63.3(3) . . . .
B16 B20 B21 B13 0.2(3) . . . .
B22 B20 B21 B13 -100.8(3) . . . .
C30 B13 B21 C31 35.89(19) . . . .
B17 B13 B21 C31 134.7(2) . . . .
B14 B13 B21 C31 96.7(2) . . . .
C30 B13 B21 B17 -98.8(2) . . . .
C31 B13 B21 B17 -134.7(2) . . . .
B14 B13 B21 B17 -38.1(2) . . . .
C30 B13 B21 B20 2.0(3) . . . .
C31 B13 B21 B20 -33.9(2) . . . .
B17 B13 B21 B20 100.8(3) . . . .
B14 B13 B21 B20 62.8(3) . . . .
C30 B13 B21 B22 -61.4(3) . . . .
C31 B13 B21 B22 -97.3(2) . . . .
B17 B13 B21 B22 37.4(2) . . . .
B14 B13 B21 B22 -0.6(3) . . . .
B14 B18 B22 B21 -0.2(3) . . . .
B15 B18 B22 B21 63.5(3) . . . .
B19 B18 B22 B21 100.3(2) . . . .
B17 B18 B22 B21 -37.3(2) . . . .
B14 B18 B22 B17 37.2(2) . . . .
B15 B18 B22 B17 100.8(2) . . . .
B19 B18 B22 B17 137.6(2) . . . .
B14 B18 B22 B20 -63.3(3) . . . .
B15 B18 B22 B20 0.4(3) . . . .
B19 B18 B22 B20 37.2(2) . . . .
B17 B18 B22 B20 -100.4(2) . . . .
B14 B18 B22 B19 -100.5(2) . . . .
B15 B18 B22 B19 -36.8(2) . . . .
B17 B18 B22 B19 -137.6(2) . . . .
C31 B21 B22 B18 -61.7(3) . . . .
B17 B21 B22 B18 37.6(2) . . . .
B20 B21 B22 B18 -100.0(2) . . . .
B13 B21 B22 B18 0.5(3) . . . .
C31 B21 B22 B17 -99.4(2) . . . .
B20 B21 B22 B17 -137.6(2) . . . .
B13 B21 B22 B17 -37.1(2) . . . .
C31 B21 B22 B20 38.3(2) . . . .
B17 B21 B22 B20 137.6(2) . . . .
B13 B21 B22 B20 100.5(2) . . . .
C31 B21 B22 B19 1.6(3) . . . .
B17 B21 B22 B19 101.0(2) . . . .
B20 B21 B22 B19 -36.6(2) . . . .
B13 B21 B22 B19 63.9(3) . . . .
B13 B17 B22 B18 -100.2(3) . . . .
B21 B17 B22 B18 -138.1(2) . . . .
B14 B17 B22 B18 -36.6(2) . . . .
B13 B17 B22 B21 37.8(2) . . . .
B14 B17 B22 B21 101.4(2) . . . .
B18 B17 B22 B21 138.1(2) . . . .
B13 B17 B22 B20 0.2(3) . . . .
B21 B17 B22 B20 -37.6(2) . . . .
B14 B17 B22 B20 63.8(3) . . . .
B18 B17 B22 B20 100.5(2) . . . .
B13 B17 B22 B19 -62.3(3) . . . .
B21 B17 B22 B19 -100.2(2) . . . .
B14 B17 B22 B19 1.3(3) . . . .
B18 B17 B22 B19 37.9(2) . . . .
C31 B20 B22 B18 62.1(3) . . . .
B19 B20 B22 B18 -37.5(2) . . . .
B16 B20 B22 B18 -0.6(3) . . . .
B21 B20 B22 B18 101.1(2) . . . .
C31 B20 B22 B21 -38.9(2) . . . .
B19 B20 B22 B21 -138.6(2) . . . .
B16 B20 B22 B21 -101.7(2) . . . .
C31 B20 B22 B17 -1.4(3) . . . .
B19 B20 B22 B17 -101.1(2) . . . .
B16 B20 B22 B17 -64.1(3) . . . .
B21 B20 B22 B17 37.5(2) . . . .
C31 B20 B22 B19 99.7(2) . . . .
B16 B20 B22 B19 36.9(2) . . . .
B21 B20 B22 B19 138.6(2) . . . .
B16 B19 B22 B18 100.6(2) . . . .
B20 B19 B22 B18 137.9(2) . . . .
B15 B19 B22 B18 36.7(2) . . . .
B16 B19 B22 B21 -0.4(3) . . . .
B20 B19 B22 B21 36.8(2) . . . .
B15 B19 B22 B21 -64.3(3) . . . .
B18 B19 B22 B21 -101.0(2) . . . .
B16 B19 B22 B17 62.6(3) . . . .
B20 B19 B22 B17 99.8(2) . . . .
B15 B19 B22 B17 -1.3(3) . . . .
B18 B19 B22 B17 -38.0(2) . . . .
B16 B19 B22 B20 -37.2(2) . . . .
B15 B19 B22 B20 -101.2(2) . . . .
B18 B19 B22 B20 -137.9(2) . . . .
B8 B4 C1 C4 -143.0(2) . . . .
B3 B4 C1 C4 -103.6(3) . . . .
B9 B4 C1 C4 154.5(2) . . . .
B5 B4 C1 C4 114.3(3) . . . .
B8 B4 C1 C2 -1.1(2) . . . .
B3 B4 C1 C2 38.27(18) . . . .
B9 B4 C1 C2 -63.5(3) . . . .
B5 B4 C1 C2 -103.8(2) . . . .
B8 B4 C1 B5 102.8(2) . . . .
B3 B4 C1 B5 142.1(2) . . . .
B9 B4 C1 B5 40.3(2) . . . .
B8 B4 C1 B3 -39.34(18) . . . .
B9 B4 C1 B3 -101.8(2) . . . .
B5 B4 C1 B3 -142.1(2) . . . .
B8 B4 C1 B6 65.5(3) . . . .
B3 B4 C1 B6 104.8(2) . . . .
B9 B4 C1 B6 3.0(3) . . . .
B5 B4 C1 B6 -37.3(2) . . . .
B10 B5 C1 C4 147.1(2) . . . .
B9 B5 C1 C4 -150.6(2) . . . .
B4 B5 C1 C4 -110.8(3) . . . .
B6 B5 C1 C4 107.5(3) . . . .
B10 B5 C1 C2 1.6(3) . . . .
B9 B5 C1 C2 63.8(2) . . . .
B4 B5 C1 C2 103.7(2) . . . .
B6 B5 C1 C2 -38.05(19) . . . .
B10 B5 C1 B4 -102.1(2) . . . .
B9 B5 C1 B4 -39.8(2) . . . .
B6 B5 C1 B4 -141.7(2) . . . .
B10 B5 C1 B3 -65.3(3) . . . .
B9 B5 C1 B3 -3.1(3) . . . .
B4 B5 C1 B3 36.8(2) . . . .
B6 B5 C1 B3 -104.9(2) . . . .
B10 B5 C1 B6 39.66(19) . . . .
B9 B5 C1 B6 101.9(2) . . . .
B4 B5 C1 B6 141.7(2) . . . .
C2 B3 C1 C4 -107.9(2) . . . .
B8 B3 C1 C4 152.7(2) . . . .
B7 B3 C1 C4 -144.1(2) . . . .
B4 B3 C1 C4 113.4(2) . . . .
B8 B3 C1 C2 -99.3(2) . . . .
B7 B3 C1 C2 -36.14(19) . . . .
B4 B3 C1 C2 -138.71(19) . . . .
C2 B3 C1 B4 138.71(19) . . . .
B8 B3 C1 B4 39.36(19) . . . .
B7 B3 C1 B4 102.6(2) . . . .
C2 B3 C1 B5 101.7(2) . . . .
B8 B3 C1 B5 2.3(3) . . . .
B7 B3 C1 B5 65.5(3) . . . .
B4 B3 C1 B5 -37.1(2) . . . .
C2 B3 C1 B6 32.10(19) . . . .
B8 B3 C1 B6 -67.3(3) . . . .
B7 B3 C1 B6 -4.0(3) . . . .
B4 B3 C1 B6 -106.6(2) . . . .
C2 B6 C1 C4 106.3(2) . . . .
B10 B6 C1 C4 -155.0(2) . . . .
B11 B6 C1 C4 142.9(2) . . . .
B5 B6 C1 C4 -114.9(3) . . . .
B10 B6 C1 C2 98.8(2) . . . .
B11 B6 C1 C2 36.65(18) . . . .
B5 B6 C1 C2 138.8(2) . . . .
C2 B6 C1 B4 -101.4(2) . . . .
B10 B6 C1 B4 -2.7(3) . . . .
B11 B6 C1 B4 -64.8(3) . . . .
B5 B6 C1 B4 37.4(2) . . . .
C2 B6 C1 B5 -138.8(2) . . . .
B10 B6 C1 B5 -40.1(2) . . . .
B11 B6 C1 B5 -102.2(2) . . . .
C2 B6 C1 B3 -32.20(19) . . . .
B10 B6 C1 B3 66.5(3) . . . .
B11 B6 C1 B3 4.5(3) . . . .
B5 B6 C1 B3 106.6(2) . . . .
C4 C1 C2 C3 -2.4(3) . . . .
B4 C1 C2 C3 -146.1(2) . . . .
B5 C1 C2 C3 145.6(2) . . . .
B3 C1 C2 C3 -107.2(2) . . . .
B6 C1 C2 C3 106.7(3) . . . .
C4 C1 C2 B7 143.8(2) . . . .
B4 C1 C2 B7 0.1(3) . . . .
B5 C1 C2 B7 -68.2(2) . . . .
B3 C1 C2 B7 38.92(19) . . . .
B6 C1 C2 B7 -107.1(2) . . . .
C4 C1 C2 B11 -148.7(2) . . . .
B4 C1 C2 B11 67.6(2) . . . .
B5 C1 C2 B11 -0.7(3) . . . .
B3 C1 C2 B11 106.5(2) . . . .
B6 C1 C2 B11 -39.6(2) . . . .
C4 C1 C2 B3 104.8(2) . . . .
B4 C1 C2 B3 -38.85(19) . . . .
B5 C1 C2 B3 -107.2(2) . . . .
B6 C1 C2 B3 -146.07(19) . . . .
C4 C1 C2 B6 -109.1(2) . . . .
B4 C1 C2 B6 107.2(2) . . . .
B5 C1 C2 B6 38.9(2) . . . .
B3 C1 C2 B6 146.07(19) . . . .
B12 B7 C2 C3 -152.2(2) . . . .
B3 B7 C2 C3 106.1(3) . . . .
B11 B7 C2 C3 -112.8(3) . . . .
B8 B7 C2 C3 145.2(2) . . . .
B12 B7 C2 C1 63.5(2) . . . .
B3 B7 C2 C1 -38.21(19) . . . .
B11 B7 C2 C1 102.9(2) . . . .
B8 B7 C2 C1 1.0(3) . . . .
B12 B7 C2 B11 -39.4(2) . . . .
B3 B7 C2 B11 -141.1(2) . . . .
B8 B7 C2 B11 -101.9(2) . . . .
B12 B7 C2 B3 101.7(2) . . . .
B11 B7 C2 B3 141.1(2) . . . .
B8 B7 C2 B3 39.2(2) . . . .
B12 B7 C2 B6 -2.7(3) . . . .
B3 B7 C2 B6 -104.4(2) . . . .
B11 B7 C2 B6 36.7(2) . . . .
B8 B7 C2 B6 -65.2(2) . . . .
B10 B11 C2 C3 -145.0(3) . . . .
B12 B11 C2 C3 152.1(3) . . . .
B6 B11 C2 C3 -105.4(3) . . . .
B7 B11 C2 C3 112.8(3) . . . .
B10 B11 C2 C1 -0.6(3) . . . .
B12 B11 C2 C1 -63.5(3) . . . .
B6 B11 C2 C1 39.1(2) . . . .
B7 B11 C2 C1 -102.7(2) . . . .
B10 B11 C2 B7 102.2(2) . . . .
B12 B11 C2 B7 39.3(2) . . . .
B6 B11 C2 B7 141.9(2) . . . .
B10 B11 C2 B3 64.9(3) . . . .
B12 B11 C2 B3 2.0(3) . . . .
B6 B11 C2 B3 104.6(2) . . . .
B7 B11 C2 B3 -37.3(2) . . . .
B10 B11 C2 B6 -39.7(2) . . . .
B12 B11 C2 B6 -102.6(2) . . . .
B7 B11 C2 B6 -141.9(2) . . . .
C1 B3 C2 C3 108.0(2) . . . .
B8 B3 C2 C3 -153.8(2) . . . .
B7 B3 C2 C3 -114.0(3) . . . .
B4 B3 C2 C3 143.5(2) . . . .
B8 B3 C2 C1 98.2(2) . . . .
B7 B3 C2 C1 138.0(2) . . . .
B4 B3 C2 C1 35.55(17) . . . .
C1 B3 C2 B7 -138.0(2) . . . .
B8 B3 C2 B7 -39.8(2) . . . .
B4 B3 C2 B7 -102.4(2) . . . .
C1 B3 C2 B11 -100.3(2) . . . .
B8 B3 C2 B11 -2.1(3) . . . .
B7 B3 C2 B11 37.7(2) . . . .
B4 B3 C2 B11 -64.8(3) . . . .
C1 B3 C2 B6 -32.04(17) . . . .
B8 B3 C2 B6 66.2(3) . . . .
B7 B3 C2 B6 106.0(2) . . . .
B4 B3 C2 B6 3.5(2) . . . .
C1 B6 C2 C3 -108.4(2) . . . .
B10 B6 C2 C3 153.9(2) . . . .
B11 B6 C2 C3 114.3(3) . . . .
B5 B6 C2 C3 -143.8(2) . . . .
B10 B6 C2 C1 -97.7(2) . . . .
B11 B6 C2 C1 -137.3(2) . . . .
B5 B6 C2 C1 -35.31(17) . . . .
C1 B6 C2 B7 100.2(2) . . . .
B10 B6 C2 B7 2.5(3) . . . .
B11 B6 C2 B7 -37.1(2) . . . .
B5 B6 C2 B7 64.9(2) . . . .
C1 B6 C2 B11 137.3(2) . . . .
B10 B6 C2 B11 39.6(2) . . . .
B5 B6 C2 B11 102.0(2) . . . .
C1 B6 C2 B3 31.84(18) . . . .
B10 B6 C2 B3 -65.9(2) . . . .
B11 B6 C2 B3 -105.5(2) . . . .
B5 B6 C2 B3 -3.5(2) . . . .
C2 C1 C4 C5 -58(3) . . . .
B4 C1 C4 C5 82(3) . . . .
B5 C1 C4 C5 158(3) . . . .
B3 C1 C4 C5 11(3) . . . .
B6 C1 C4 C5 -127(3) . . . .
C1 C4 C5 C6 64(5) . . . .
C4 C5 C6 C7 -61(4) . . . .
C4 C5 C6 C27 117(4) . . . .
C27 C6 C7 C8 175.1(2) . . . .
C5 C6 C7 C8 -7.5(4) . . . .
C27 C6 C7 C16 -4.0(4) . . . .
C5 C6 C7 C16 173.4(2) . . . .
C6 C7 C8 C9 -177.6(2) . . . .
C16 C7 C8 C9 1.5(4) . . . .
C7 C8 C9 C10 176.8(2) . . . .
C7 C8 C9 C14 -2.1(4) . . . .
C8 C9 C10 C11 -177.2(3) . . . .
C14 C9 C10 C11 1.6(4) . . . .
C9 C10 C11 C12 -0.7(4) . . . .
C10 C11 C12 C13 -0.9(4) . . . .
C11 C12 C13 C14 1.4(4) . . . .
C12 C13 C14 C15 177.0(3) . . . .
C12 C13 C14 C9 -0.5(4) . . . .
C8 C9 C14 C15 0.4(4) . . . .
C10 C9 C14 C15 -178.6(2) . . . .
C8 C9 C14 C13 177.9(2) . . . .
C10 C9 C14 C13 -1.0(4) . . . .
C13 C14 C15 C16 -175.4(2) . . . .
C9 C14 C15 C16 2.1(4) . . . .
C14 C15 C16 C17 175.8(2) . . . .
C14 C15 C16 C7 -2.7(4) . . . .
C8 C7 C16 C15 0.9(4) . . . .
C6 C7 C16 C15 180.0(2) . . . .
C8 C7 C16 C17 -177.7(2) . . . .
C6 C7 C16 C17 1.5(4) . . . .
C15 C16 C17 C18 -175.9(2) . . . .
C7 C16 C17 C18 2.6(4) . . . .
C15 C16 C17 C28 5.7(4) . . . .
C7 C16 C17 C28 -175.8(2) . . . .
C16 C17 C18 C19 177.2(2) . . . .
C28 C17 C18 C19 -4.4(4) . . . .
C16 C17 C18 C27 -4.1(4) . . . .
C28 C17 C18 C27 174.3(2) . . . .
C17 C18 C19 C20 178.1(2) . . . .
C27 C18 C19 C20 -0.6(4) . . . .
C18 C19 C20 C21 -179.9(2) . . . .
C18 C19 C20 C25 0.3(4) . . . .
C19 C20 C21 C22 179.9(2) . . . .
C25 C20 C21 C22 -0.3(4) . . . .
C20 C21 C22 C23 0.8(4) . . . .
C21 C22 C23 C24 -0.8(4) . . . .
C22 C23 C24 C25 0.3(4) . . . .
C23 C24 C25 C26 179.9(3) . . . .
C23 C24 C25 C20 0.2(4) . . . .
C19 C20 C25 C26 -0.1(4) . . . .
C21 C20 C25 C26 -179.9(2) . . . .
C19 C20 C25 C24 179.6(2) . . . .
C21 C20 C25 C24 -0.2(3) . . . .
C24 C25 C26 C27 -179.5(2) . . . .
C20 C25 C26 C27 0.2(4) . . . .
C25 C26 C27 C6 179.8(2) . . . .
C25 C26 C27 C18 -0.5(4) . . . .
C7 C6 C27 C26 -178.0(2) . . . .
C5 C6 C27 C26 4.7(4) . . . .
C7 C6 C27 C18 2.4(4) . . . .
C5 C6 C27 C18 -174.9(2) . . . .
C19 C18 C27 C26 0.7(3) . . . .
C17 C18 C27 C26 -178.0(2) . . . .
C19 C18 C27 C6 -179.6(2) . . . .
C17 C18 C27 C6 1.6(3) . . . .
C16 C17 C28 C29 102(7) . . . .
C18 C17 C28 C29 -76(7) . . . .
C17 C28 C29 C30 11(11) . . . .
C28 C29 C30 C31 -47(5) . . . .
C28 C29 C30 B14 94(5) . . . .
C28 C29 C30 B15 170(5) . . . .
C28 C29 C30 B13 22(5) . . . .
C28 C29 C30 B16 -117(5) . . . .
B18 B14 C30 C29 153.1(2) . . . .
B15 B14 C30 C29 113.0(3) . . . .
B13 B14 C30 C29 -104.8(3) . . . .
B17 B14 C30 C29 -144.3(2) . . . .
B18 B14 C30 C31 -63.2(3) . . . .
B15 B14 C30 C31 -103.2(2) . . . .
B13 B14 C30 C31 39.0(2) . . . .
B17 B14 C30 C31 -0.5(3) . . . .
B18 B14 C30 B15 40.0(2) . . . .
B13 B14 C30 B15 142.2(2) . . . .
B17 B14 C30 B15 102.7(2) . . . .
B18 B14 C30 B13 -102.1(2) . . . .
B15 B14 C30 B13 -142.2(2) . . . .
B17 B14 C30 B13 -39.5(2) . . . .
B18 B14 C30 B16 3.5(3) . . . .
B15 B14 C30 B16 -36.5(2) . . . .
B13 B14 C30 B16 105.6(2) . . . .
B17 B14 C30 B16 66.1(3) . . . .
B14 B15 C30 C29 -111.6(3) . . . .
B19 B15 C30 C29 146.1(3) . . . .
B18 B15 C30 C29 -151.4(2) . . . .
B16 B15 C30 C29 106.3(3) . . . .
B14 B15 C30 C31 103.9(2) . . . .
B19 B15 C30 C31 1.6(3) . . . .
B18 B15 C30 C31 64.0(3) . . . .
B16 B15 C30 C31 -38.3(2) . . . .
B19 B15 C30 B14 -102.3(2) . . . .
B18 B15 C30 B14 -39.8(2) . . . .
B16 B15 C30 B14 -142.1(2) . . . .
B14 B15 C30 B13 36.7(2) . . . .
B19 B15 C30 B13 -65.6(3) . . . .
B18 B15 C30 B13 -3.1(3) . . . .
B16 B15 C30 B13 -105.4(2) . . . .
B14 B15 C30 B16 142.1(2) . . . .
B19 B15 C30 B16 39.8(2) . . . .
B18 B15 C30 B16 102.3(2) . . . .
C31 B13 C30 C29 -108.1(2) . . . .
B17 B13 C30 C29 153.8(2) . . . .
B14 B13 C30 C29 113.8(3) . . . .
B21 B13 C30 C29 -144.0(2) . . . .
B17 B13 C30 C31 -98.1(2) . . . .
B14 B13 C30 C31 -138.1(2) . . . .
B21 B13 C30 C31 -36.0(2) . . . .
C31 B13 C30 B14 138.1(2) . . . .
B17 B13 C30 B14 40.0(2) . . . .
B21 B13 C30 B14 102.2(2) . . . .
C31 B13 C30 B15 101.4(2) . . . .
B17 B13 C30 B15 3.3(3) . . . .
B14 B13 C30 B15 -36.7(2) . . . .
B21 B13 C30 B15 65.4(3) . . . .
C31 B13 C30 B16 32.3(2) . . . .
B17 B13 C30 B16 -65.8(3) . . . .
B14 B13 C30 B16 -105.8(2) . . . .
B21 B13 C30 B16 -3.7(3) . . . .
C31 B16 C30 C29 107.2(2) . . . .
B19 B16 C30 C29 -154.4(2) . . . .
B20 B16 C30 C29 143.5(2) . . . .
B15 B16 C30 C29 -114.2(3) . . . .
B19 B16 C30 C31 98.3(2) . . . .
B20 B16 C30 C31 36.24(19) . . . .
B15 B16 C30 C31 138.6(2) . . . .
C31 B16 C30 B14 -101.9(2) . . . .
B19 B16 C30 B14 -3.5(3) . . . .
B20 B16 C30 B14 -65.6(3) . . . .
B15 B16 C30 B14 36.7(2) . . . .
C31 B16 C30 B15 -138.6(2) . . . .
B19 B16 C30 B15 -40.2(2) . . . .
B20 B16 C30 B15 -102.3(2) . . . .
C31 B16 C30 B13 -32.5(2) . . . .
B19 B16 C30 B13 65.8(3) . . . .
B20 B16 C30 B13 3.7(3) . . . .
B15 B16 C30 B13 106.1(2) . . . .
C29 C30 C31 C32 -1.2(4) . . . .
B14 C30 C31 C32 -146.8(3) . . . .
B15 C30 C31 C32 145.4(3) . . . .
B13 C30 C31 C32 -107.4(3) . . . .
B16 C30 C31 C32 106.6(3) . . . .
C29 C30 C31 B20 -147.5(2) . . . .
B14 C30 C31 B20 66.9(3) . . . .
B15 C30 C31 B20 -0.8(3) . . . .
B13 C30 C31 B20 106.4(2) . . . .
B16 C30 C31 B20 -39.6(2) . . . .
C29 C30 C31 B21 145.2(2) . . . .
B14 C30 C31 B21 -0.4(3) . . . .
B15 C30 C31 B21 -68.2(3) . . . .
B13 C30 C31 B21 39.1(2) . . . .
B16 C30 C31 B21 -107.0(2) . . . .
C29 C30 C31 B16 -107.8(3) . . . .
B14 C30 C31 B16 106.6(2) . . . .
B15 C30 C31 B16 38.8(2) . . . .
B13 C30 C31 B16 146.0(2) . . . .
C29 C30 C31 B13 106.1(2) . . . .
B14 C30 C31 B13 -39.5(2) . . . .
B15 C30 C31 B13 -107.2(2) . . . .
B16 C30 C31 B13 -146.0(2) . . . .
B19 B20 C31 C32 -144.6(3) . . . .
B16 B20 C31 C32 -105.3(3) . . . .
B21 B20 C31 C32 112.9(3) . . . .
B22 B20 C31 C32 152.2(3) . . . .
B19 B20 C31 C30 -0.3(3) . . . .
B16 B20 C31 C30 39.0(2) . . . .
B21 B20 C31 C30 -102.9(2) . . . .
B22 B20 C31 C30 -63.5(3) . . . .
B19 B20 C31 B21 102.6(3) . . . .
B16 B20 C31 B21 141.9(2) . . . .
B22 B20 C31 B21 39.4(2) . . . .
B19 B20 C31 B16 -39.3(2) . . . .
B21 B20 C31 B16 -141.9(2) . . . .
B22 B20 C31 B16 -102.5(3) . . . .
B19 B20 C31 B13 65.4(3) . . . .
B16 B20 C31 B13 104.7(3) . . . .
B21 B20 C31 B13 -37.2(2) . . . .
B22 B20 C31 B13 2.2(3) . . . .
B17 B21 C31 C32 145.5(3) . . . .
B20 B21 C31 C32 -112.6(3) . . . .
B22 B21 C31 C32 -151.9(3) . . . .
B13 B21 C31 C32 106.1(3) . . . .
B17 B21 C31 C30 1.2(3) . . . .
B20 B21 C31 C30 103.0(2) . . . .
B22 B21 C31 C30 63.8(3) . . . .
B13 B21 C31 C30 -38.3(2) . . . .
B17 B21 C31 B20 -101.8(2) . . . .
B22 B21 C31 B20 -39.2(2) . . . .
B13 B21 C31 B20 -141.3(2) . . . .
B17 B21 C31 B16 -65.0(3) . . . .
B20 B21 C31 B16 36.8(2) . . . .
B22 B21 C31 B16 -2.4(3) . . . .
B13 B21 C31 B16 -104.5(3) . . . .
B17 B21 C31 B13 39.4(2) . . . .
B20 B21 C31 B13 141.3(2) . . . .
B22 B21 C31 B13 102.0(3) . . . .
C30 B16 C31 C32 -108.0(3) . . . .
B19 B16 C31 C32 153.6(2) . . . .
B20 B16 C31 C32 114.5(3) . . . .
B15 B16 C31 C32 -143.8(2) . . . .
B19 B16 C31 C30 -98.4(2) . . . .
B20 B16 C31 C30 -137.5(2) . . . .
B15 B16 C31 C30 -35.80(18) . . . .
C30 B16 C31 B20 137.5(2) . . . .
B19 B16 C31 B20 39.1(2) . . . .
B15 B16 C31 B20 101.7(2) . . . .
C30 B16 C31 B21 100.6(2) . . . .
B19 B16 C31 B21 2.2(3) . . . .
B20 B16 C31 B21 -36.9(2) . . . .
B15 B16 C31 B21 64.8(3) . . . .
C30 B16 C31 B13 31.9(2) . . . .
B19 B16 C31 B13 -66.5(3) . . . .
B20 B16 C31 B13 -105.6(2) . . . .
B15 B16 C31 B13 -3.9(3) . . . .
C30 B13 C31 C32 107.6(3) . . . .
B17 B13 C31 C32 -153.7(3) . . . .
B14 B13 C31 C32 143.5(2) . . . .
B21 B13 C31 C32 -114.3(3) . . . .
B17 B13 C31 C30 98.7(2) . . . .
B14 B13 C31 C30 35.90(18) . . . .
B21 B13 C31 C30 138.1(2) . . . .
C30 B13 C31 B20 -100.7(2) . . . .
B17 B13 C31 B20 -2.0(3) . . . .
B14 B13 C31 B20 -64.8(3) . . . .
B21 B13 C31 B20 37.4(2) . . . .
C30 B13 C31 B21 -138.1(2) . . . .
B17 B13 C31 B21 -39.4(2) . . . .
B14 B13 C31 B21 -102.2(2) . . . .
C30 B13 C31 B16 -32.04(19) . . . .
B17 B13 C31 B16 66.7(3) . . . .
B14 B13 C31 B16 3.9(3) . . . .
B21 B13 C31 B16 106.0(2) . . . .
