#------------------------------------------------------------------------------
#$Date: 2016-01-12 09:32:05 +0200 (Tue, 12 Jan 2016) $
#$Revision: 174380 $
#$URL: svn://www.crystallography.net/cod/cif/7/11/84/7118406.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7118406
loop_
_publ_author_name
'Nikoleta Stavgianoudaki'
'Milosz Siczek'
'Tadeusz Lis'
'Ross Inglis'
'Constantinos J. Milios'
_publ_section_title
;
 A triacontanuclear [Zn12Dy18] cluster: a ring of [Dy4] cubes
;
_journal_name_full               Chem.Commun.
_journal_page_first              343
_journal_volume                  52
_journal_year                    2016
_chemical_formula_moiety
'C188 H216 Dy18 N15 O109 Zn12, 3(N O3), 12(C H4 O), 5(H2 O)'
_chemical_formula_sum            'C200 H274 Dy18 N18 O135 Zn12'
_chemical_formula_weight         8799.79
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   mixed
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2015-08-24 deposited with the CCDC.
2015-10-22 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 115.52(5)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   35.409(18)
_cell_length_b                   30.501(12)
_cell_length_c                   31.789(13)
_cell_measurement_reflns_used    12730
_cell_measurement_temperature    85(2)
_cell_measurement_theta_max      28.00
_cell_measurement_theta_min      2.7
_cell_volume                     30983(3)
_computing_cell_refinement       'CrysAlis PRO (Agilent, 2010)'
_computing_data_collection       'CrysAlis CCD (Oxford Diffraction, 2010)'
_computing_data_reduction        'CrysAlis PRO (Agilent, 2010)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_structure_solution    'SHELXL-2013 (Sheldrick, 2013)'
_diffrn_ambient_temperature      85(2)
_diffrn_measured_fraction_theta_full 0.959
_diffrn_measured_fraction_theta_max 0.897
_diffrn_measurement_device_type  'Xcalibur with Ruby CCD'
_diffrn_measurement_method       /w
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0576
_diffrn_reflns_av_unetI/netI     0.1071
_diffrn_reflns_laue_measured_fraction_full 0.959
_diffrn_reflns_laue_measured_fraction_max 0.897
_diffrn_reflns_limit_h_max       35
_diffrn_reflns_limit_h_min       -45
_diffrn_reflns_limit_k_max       37
_diffrn_reflns_limit_k_min       -40
_diffrn_reflns_limit_l_max       41
_diffrn_reflns_limit_l_min       -41
_diffrn_reflns_number            69783
_diffrn_reflns_point_group_measured_fraction_full 0.959
_diffrn_reflns_point_group_measured_fraction_max 0.897
_diffrn_reflns_theta_full        25.500
_diffrn_reflns_theta_max         27.999
_diffrn_reflns_theta_min         2.689
_exptl_absorpt_coefficient_mu    5.277
_exptl_absorpt_correction_T_max  0.642
_exptl_absorpt_correction_T_min  0.398
_exptl_absorpt_correction_type   analytical
_exptl_absorpt_process_details
;
CrysAlis RED, Oxford Diffraction Ltd.,
Version 1.171.33.66
Analytical numeric absorption correction using a multifaceted crystal
            model based on expressions derived by R.C. Clark & J.S. Reid.
(Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897)
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.887
_exptl_crystal_description       needle
_exptl_crystal_F_000             16912
_exptl_crystal_size_max          0.500
_exptl_crystal_size_mid          0.120
_exptl_crystal_size_min          0.090
_refine_diff_density_max         2.575
_refine_diff_density_min         -1.478
_refine_diff_density_rms         0.245
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.218
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1692
_refine_ls_number_reflns         33552
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.218
_refine_ls_R_factor_all          0.1614
_refine_ls_R_factor_gt           0.0784
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0550P)²+700.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1614
_refine_ls_wR_factor_ref         0.2209
_reflns_Friedel_coverage         0.000
_reflns_friedel_fraction_full    .
_reflns_friedel_fraction_max     .
_reflns_number_gt                17942
_reflns_number_total             33552
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c5cc07243c2.cif
_cod_data_source_block           ns4500a
_cod_original_cell_volume        30983(26)
_cod_database_code               7118406
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.178
_shelx_estimated_absorpt_t_max   0.648
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.5000 0.64640(3) 0.7500 0.0389(3) Uani 1 2 d S T P . .
Dy2 Dy 0.5000 0.39434(4) 0.7500 0.0414(3) Uani 1 2 d S T P G .
Dy3 Dy 0.40557(2) 0.58369(2) 0.66302(2) 0.03867(19) Uani 1 1 d . . . . .
Dy4 Dy 0.40671(2) 0.45881(3) 0.66566(2) 0.0416(2) Uani 1 1 d . . . . .
Dy5 Dy 0.31497(7) 0.52707(13) 0.65501(14) 0.0385(8) Uani 0.88(3) 1 d . . P C .
Dy51 Dy 0.3115(6) 0.5358(10) 0.6448(13) 0.062(5) Uiso 0.12(3) 1 d . . P C .
Dy6 Dy 0.35265(4) 0.51558(9) 0.55723(5) 0.0368(6) Uani 0.930(13) 1 d . . P C .
Dy61 Dy 0.3567(8) 0.5295(14) 0.5502(10) 0.061(7) Uiso 0.070(13) 1 d . . P C .
Dy7 Dy 0.39643(2) 0.69046(3) 0.71297(2) 0.04060(19) Uani 1 1 d . . . . .
Dy8 Dy 0.44143(3) 0.67581(3) 0.62269(2) 0.0425(2) Uani 1 1 d . . . . .
Dy9 Dy 0.39191(3) 0.35547(3) 0.71197(2) 0.0452(2) Uani 1 1 d . . . . .
Dy10 Dy 0.45092(3) 0.35801(3) 0.63364(2) 0.0447(2) Uani 1 1 d . . . . .
Zn1 Zn 0.29506(6) 0.63374(7) 0.67333(7) 0.0503(5) Uani 1 1 d . . . . .
Zn2 Zn 0.26132(6) 0.49142(7) 0.45871(7) 0.0556(5) Uani 1 1 d . . . . .
Zn3 Zn 0.37089(15) 0.62590(12) 0.52339(8) 0.0551(15) Uani 0.835(13) 1 d . . P C
.
Zn31 Zn 0.3515(6) 0.6390(5) 0.5266(4) 0.038(4) Uiso 0.165(13) 1 d . . P C .
Zn4 Zn 0.31946(7) 0.27256(7) 0.66338(6) 0.0518(5) Uani 1 1 d . . . . .
Zn5 Zn 0.35778(6) 0.79661(6) 0.69227(6) 0.0495(5) Uani 1 1 d . . . . .
Zn6 Zn 0.45783(7) 0.29971(8) 0.82217(7) 0.0679(7) Uani 1 1 d . . . . .
O1 O 0.4329(3) 0.6214(3) 0.7332(3) 0.040(2) Uani 1 1 d . . . . .
H1 H 0.4308 0.6078 0.7558 0.048 Uiso 1 1 calc R U . . .
O2 O 0.4716(3) 0.6176(3) 0.6746(3) 0.038(2) Uani 1 1 d . . . . .
H2 H 0.4882 0.6011 0.6682 0.045 Uiso 1 1 calc R U . . .
O3 O 0.4568(3) 0.6987(3) 0.7008(3) 0.036(2) Uani 1 1 d . . . . .
H3 H 0.4672 0.7247 0.7070 0.043 Uiso 1 1 calc R U . . .
O4 O 0.4344(3) 0.4208(3) 0.7364(3) 0.044(3) Uani 1 1 d . . . . .
H4 H 0.4332 0.4345 0.7594 0.053 Uiso 1 1 calc R U . G .
O5 O 0.4676(3) 0.4253(3) 0.6723(3) 0.042(3) Uani 1 1 d . . . . .
H5 H 0.4837 0.4417 0.6652 0.050 Uiso 1 1 calc R U . G .
O6 O 0.4533(3) 0.3397(3) 0.7064(3) 0.046(3) Uani 1 1 d . . . . .
H6 H 0.4624 0.3136 0.7154 0.055 Uiso 1 1 calc R U . G .
O7 O 0.4777(3) 0.3540(4) 0.8046(3) 0.050(3) Uani 1 1 d . . . . .
H7 H 0.4650 0.3740 0.8127 0.060 Uiso 1 1 calc R U . G .
O8 O 0.3875(3) 0.5200(3) 0.6958(3) 0.037(2) Uani 1 1 d . . . . .
H8 H 0.3967 0.5203 0.7256 0.045 Uiso 1 1 d R U . . .
O9 O 0.4158(3) 0.5205(3) 0.6282(3) 0.037(2) Uani 1 1 d . . . . .
H9 H 0.4385 0.5204 0.6245 0.044 Uiso 1 1 d R U . C .
O10 O 0.3401(3) 0.5639(3) 0.6056(3) 0.045(3) Uani 1 1 d . . . . .
H10 H 0.3251 0.5860 0.5911 0.053 Uiso 1 1 d R U . C .
O11 O 0.3461(3) 0.5999(3) 0.6841(3) 0.045(3) Uani 1 1 d . . . . .
H11 H 0.3574 0.5960 0.7138 0.054 Uiso 1 1 d R U . C .
O12 O 0.3882(3) 0.6575(3) 0.6449(3) 0.042(3) Uani 1 1 d . . . . .
H12 H 0.3636 0.6610 0.6228 0.051 Uiso 1 1 calc R U . . .
O13 O 0.4049(3) 0.6077(4) 0.5882(3) 0.048(3) Uani 1 1 d . . . . .
H13 H 0.4238 0.5917 0.5854 0.058 Uiso 1 1 d R U . C .
O14 O 0.3400(3) 0.4777(3) 0.6146(3) 0.046(3) Uani 1 1 d . . . . .
H14 H 0.3239 0.4554 0.6036 0.056 Uiso 1 1 d R U . C .
O15 O 0.3923(3) 0.3863(3) 0.6443(3) 0.042(3) Uani 1 1 d . . . . .
H15 H 0.3689 0.3828 0.6201 0.051 Uiso 1 1 calc R U . . .
O2A O 0.3886(3) 0.7541(3) 0.7457(3) 0.042(3) Uani 1 1 d . . . . .
C1A C 0.4289(5) 0.7439(5) 0.8280(6) 0.046(4) Uani 1 1 d . . . . .
C2A C 0.3943(5) 0.7591(5) 0.7901(5) 0.047(4) Uani 1 1 d . . . . .
C3A C 0.3636(6) 0.7823(5) 0.7994(6) 0.053(5) Uani 1 1 d . . . . .
H3A H 0.3392 0.7928 0.7740 0.064 Uiso 1 1 calc R U . . .
C4A C 0.3686(7) 0.7898(7) 0.8441(6) 0.069(6) Uani 1 1 d . . . . .
H4A H 0.3478 0.8054 0.8494 0.083 Uiso 1 1 calc R U . . .
C5A C 0.4032(6) 0.7748(6) 0.8805(6) 0.067(5) Uani 1 1 d . . . . .
H5A H 0.4064 0.7798 0.9114 0.080 Uiso 1 1 calc R U . . .
C6A C 0.4349(6) 0.7515(6) 0.8735(5) 0.054(5) Uani 1 1 d . . . . .
H6A H 0.4595 0.7416 0.8992 0.065 Uiso 1 1 calc R U . . .
C7A C 0.4622(5) 0.7184(6) 0.8229(6) 0.048(4) Uani 1 1 d . . . . .
O1A O 0.4981(3) 0.7165(4) 0.8566(3) 0.047(3) Uani 1 1 d . . . . .
O3A O 0.4553(3) 0.6970(3) 0.7858(3) 0.040(2) Uani 1 1 d . . . . .
O2B O 0.3234(3) 0.4763(3) 0.4892(3) 0.046(3) Uani 1 1 d . . . . .
C1B C 0.3788(5) 0.4293(5) 0.4948(5) 0.049(4) Uani 1 1 d . . . . .
C2B C 0.3459(5) 0.4573(6) 0.4689(5) 0.052(4) Uani 1 1 d . . . . .
C3B C 0.3351(6) 0.4636(6) 0.4216(5) 0.058(5) Uani 1 1 d . . . . .
H3B H 0.3129 0.4829 0.4037 0.070 Uiso 1 1 calc R U . . .
C4B C 0.3567(6) 0.4416(6) 0.4008(5) 0.065(6) Uani 1 1 d . . . . .
H4B H 0.3478 0.4446 0.3681 0.078 Uiso 1 1 calc R U . . .
C5B C 0.3905(6) 0.4156(6) 0.4258(5) 0.056(5) Uani 1 1 d . . . . .
H5B H 0.4066 0.4029 0.4115 0.067 Uiso 1 1 calc R U . . .
C6B C 0.4009(5) 0.4081(6) 0.4728(5) 0.050(4) Uani 1 1 d . . . . .
H6B H 0.4230 0.3885 0.4901 0.060 Uiso 1 1 calc R U . . .
C7B C 0.3931(5) 0.4199(6) 0.5455(5) 0.042(4) Uani 1 1 d . . . . .
O1B O 0.4112(3) 0.3834(4) 0.5606(3) 0.046(3) Uani 1 1 d . . . . .
O3B O 0.3878(3) 0.4483(3) 0.5708(3) 0.041(3) Uani 1 1 d . . . . .
O2C O 0.3259(4) 0.3321(4) 0.6940(4) 0.053(3) Uani 1 1 d . . . . .
C1C C 0.2926(6) 0.3942(6) 0.7089(5) 0.056(5) Uani 1 1 d . . . . .
C2C C 0.2995(6) 0.3495(6) 0.7104(6) 0.056(5) Uani 1 1 d . . . . .
C3C C 0.2789(6) 0.3218(6) 0.7302(6) 0.059(5) Uani 1 1 d . . . . .
H3C H 0.2838 0.2911 0.7320 0.071 Uiso 1 1 calc R U . . .
C4C C 0.2519(6) 0.3394(7) 0.7467(6) 0.068(5) Uani 1 1 d . . . . .
H4C H 0.2383 0.3206 0.7597 0.082 Uiso 1 1 calc R U . . .
C5C C 0.2446(6) 0.3833(7) 0.7444(6) 0.067(5) Uani 1 1 d . . . . .
H5C H 0.2262 0.3950 0.7562 0.081 Uiso 1 1 calc R U . . .
C6C C 0.2642(6) 0.4118(6) 0.7247(6) 0.062(5) Uani 1 1 d . . . . .
H6C H 0.2583 0.4423 0.7222 0.074 Uiso 1 1 calc R U . . .
C7C C 0.3132(7) 0.4257(6) 0.6891(6) 0.053(5) Uani 1 1 d . . . . .
O1C O 0.2943(4) 0.4619(4) 0.6727(4) 0.055(3) Uani 1 1 d . . . . .
O3C O 0.3486(4) 0.4181(4) 0.6920(4) 0.047(3) Uani 1 1 d . . . . .
O2D O 0.2430(5) 0.4502(5) 0.4075(5) 0.093(5) Uani 1 1 d . . . . .
C1D C 0.1725(8) 0.4420(7) 0.3959(8) 0.087(8) Uani 1 1 d . . . . .
C2D C 0.2068(9) 0.4343(7) 0.3851(8) 0.084(7) Uani 1 1 d . . . . .
C3D C 0.2004(9) 0.4076(9) 0.3499(10) 0.120(10) Uani 1 1 d . . . . .
H3D H 0.2232 0.4033 0.3420 0.145 Uiso 1 1 calc R U . . .
C4D C 0.1633(11) 0.3852(13) 0.3231(12) 0.186(18) Uani 1 1 d . . . . .
H4D H 0.1618 0.3624 0.3021 0.224 Uiso 1 1 calc R U . . .
C5D C 0.1288(13) 0.3988(13) 0.3295(14) 0.164(14) Uiso 1 1 d . . . . .
H5D H 0.1018 0.3897 0.3077 0.196 Uiso 1 1 calc R U . . .
C6D C 0.1321(9) 0.4256(10) 0.3673(9) 0.122(10) Uani 1 1 d . . . . .
H6D H 0.1085 0.4322 0.3731 0.146 Uiso 1 1 calc R U . . .
C7D C 0.1747(7) 0.4675(8) 0.4352(8) 0.091(8) Uani 1 1 d . . . . .
H7D H 0.1498 0.4695 0.4394 0.109 Uiso 1 1 calc R U . . .
N1D N 0.2066(4) 0.4873(5) 0.4645(5) 0.065(5) Uani 1 1 d . . . . .
C8D C 0.2039(6) 0.5114(8) 0.5041(7) 0.076(6) Uani 1 1 d . . . . .
C9D C 0.1774(7) 0.4905(12) 0.5259(8) 0.154(15) Uani 1 1 d . . . . .
H9D1 H 0.1780 0.5091 0.5513 0.231 Uiso 1 1 calc R U . . .
H9D2 H 0.1485 0.4874 0.5021 0.231 Uiso 1 1 calc R U . . .
H9D3 H 0.1887 0.4615 0.5382 0.231 Uiso 1 1 calc R U . . .
C10D C 0.1912(7) 0.5591(8) 0.4908(7) 0.094(8) Uani 1 1 d . . . . .
H10A H 0.1896 0.5744 0.5171 0.140 Uiso 1 1 calc R U . . .
H10B H 0.2120 0.5735 0.4828 0.140 Uiso 1 1 calc R U . . .
H10C H 0.1638 0.5601 0.4638 0.140 Uiso 1 1 calc R U . . .
C11D C 0.2502(6) 0.5127(6) 0.5423(6) 0.053(5) Uani 1 1 d . . . . .
O1D O 0.2557(3) 0.5201(4) 0.5829(4) 0.051(3) Uani 1 1 d . . . . .
O3D O 0.2786(4) 0.5092(4) 0.5286(4) 0.055(3) Uani 1 1 d . . . . .
O2E O 0.4035(4) 0.6828(4) 0.5405(3) 0.058(3) Uani 1 1 d . . . . .
C1E C 0.3787(5) 0.7086(6) 0.4616(5) 0.053(5) Uani 1 1 d . . . . .
C2E C 0.4046(6) 0.7102(5) 0.5097(6) 0.046(4) Uani 1 1 d . . . . .
C3E C 0.4364(6) 0.7428(6) 0.5254(5) 0.058(5) Uani 1 1 d . . . . .
H3E H 0.4540 0.7446 0.5579 0.070 Uiso 1 1 calc R U . . .
C4E C 0.4430(6) 0.7721(7) 0.4958(6) 0.073(6) Uani 1 1 d . . . . .
H4E H 0.4645 0.7936 0.5074 0.088 Uiso 1 1 calc R U . . .
C5E C 0.4165(7) 0.7686(8) 0.4479(7) 0.096(8) Uani 1 1 d . . . . .
H5E H 0.4197 0.7882 0.4265 0.115 Uiso 1 1 calc R U . . .
C6E C 0.3865(6) 0.7373(8) 0.4324(7) 0.082(7) Uani 1 1 d . . . . .
H6E H 0.3698 0.7350 0.3998 0.099 Uiso 1 1 calc R U . . .
C7E C 0.3449(5) 0.6773(6) 0.4394(5) 0.053(5) Uani 1 1 d . . . . .
H7E H 0.3294 0.6801 0.4066 0.064 Uiso 1 1 calc R U . . .
N1E N 0.3336(4) 0.6465(4) 0.4586(4) 0.046(3) Uani 1 1 d . . . . .
C8E C 0.2979(6) 0.6182(6) 0.4301(5) 0.054(5) Uani 1 1 d . . . . .
C9E C 0.3030(8) 0.5977(7) 0.3880(6) 0.091(8) Uani 1 1 d . . . . .
H9E1 H 0.2787 0.5792 0.3701 0.136 Uiso 1 1 calc R U . . .
H9E2 H 0.3050 0.6211 0.3680 0.136 Uiso 1 1 calc R U . . .
H9E3 H 0.3284 0.5798 0.3994 0.136 Uiso 1 1 calc R U . . .
C10E C 0.2566(6) 0.6433(7) 0.4114(8) 0.091(8) Uani 1 1 d . . . . .
H10D H 0.2336 0.6236 0.3927 0.137 Uiso 1 1 calc R U . . .
H10E H 0.2519 0.6549 0.4375 0.137 Uiso 1 1 calc R U . . .
H10F H 0.2577 0.6677 0.3919 0.137 Uiso 1 1 calc R U . . .
C11E C 0.2958(5) 0.5794(5) 0.4587(5) 0.042(4) Uani 1 1 d . . . . .
O1E O 0.2675(3) 0.5517(4) 0.4389(4) 0.056(3) Uani 1 1 d . . . . .
O3E O 0.3242(3) 0.5755(3) 0.5013(3) 0.046(3) Uani 1 1 d . . . . .
O2F O 0.2641(4) 0.5748(4) 0.6576(4) 0.055(3) Uani 1 1 d . . . . .
C1F C 0.1949(7) 0.6057(8) 0.6284(10) 0.099(8) Uani 1 1 d . . . . .
C2F C 0.2233(7) 0.5704(7) 0.6451(8) 0.077(6) Uani 1 1 d . . . . .
C3F C 0.2084(7) 0.5289(7) 0.6491(8) 0.077(6) Uani 1 1 d . . . . .
H3F H 0.2277 0.5052 0.6599 0.093 Uiso 1 1 calc R U . . .
C4F C 0.1665(7) 0.5211(8) 0.6377(11) 0.118(11) Uani 1 1 d . . . . .
H4F H 0.1572 0.4926 0.6410 0.142 Uiso 1 1 calc R U . . .
C5F C 0.1385(8) 0.5553(9) 0.6215(15) 0.172(17) Uani 1 1 d . . . . .
H5F H 0.1098 0.5510 0.6144 0.206 Uiso 1 1 calc R U . . .
C6F C 0.1534(8) 0.5981(8) 0.6154(14) 0.164(16) Uani 1 1 d . . . . .
H6F H 0.1339 0.6212 0.6021 0.197 Uiso 1 1 calc R U . . .
C7F C 0.2059(7) 0.6513(7) 0.6260(9) 0.094(8) Uani 1 1 d . . . . .
H7F H 0.1831 0.6710 0.6115 0.112 Uiso 1 1 calc R U . . .
N1F N 0.2416(5) 0.6677(5) 0.6409(5) 0.061(4) Uani 1 1 d . . . . .
C8F C 0.2457(6) 0.7153(6) 0.6377(6) 0.060(5) Uani 1 1 d . . . . .
C9F C 0.2259(6) 0.7396(7) 0.6652(6) 0.065(5) Uani 1 1 d . . . . .
H9F1 H 0.2290 0.7713 0.6625 0.098 Uiso 1 1 calc R U . . .
H9F2 H 0.1961 0.7322 0.6526 0.098 Uiso 1 1 calc R U . . .
H9F3 H 0.2398 0.7310 0.6980 0.098 Uiso 1 1 calc R U . . .
C10F C 0.2277(6) 0.7294(6) 0.5861(6) 0.069(6) Uani 1 1 d . . . . .
H10G H 0.2305 0.7612 0.5843 0.103 Uiso 1 1 calc R U . . .
H10H H 0.2430 0.7146 0.5709 0.103 Uiso 1 1 calc R U . . .
H10I H 0.1980 0.7213 0.5704 0.103 Uiso 1 1 calc R U . . .
C11F C 0.2936(5) 0.7276(5) 0.6608(5) 0.045(4) Uani 1 1 d . . . . .
O1F O 0.3004(4) 0.7676(4) 0.6638(4) 0.053(3) Uani 1 1 d . . . . .
O3F O 0.3202(3) 0.6975(3) 0.6705(3) 0.044(3) Uani 1 1 d . . . . .
O2G O 0.3638(6) 0.8488(4) 0.7294(5) 0.095(5) Uani 1 1 d . . . . .
C1G C 0.3510(6) 0.9038(6) 0.6717(6) 0.061(5) Uani 1 1 d . . . . .
C2G C 0.3545(6) 0.8892(6) 0.7155(6) 0.063(5) Uani 1 1 d . . . . .
C3G C 0.3513(7) 0.9199(6) 0.7458(7) 0.074(6) Uani 1 1 d . . . . .
H3G H 0.3551 0.9106 0.7759 0.089 Uiso 1 1 calc R U . . .
C4G C 0.3429(8) 0.9632(7) 0.7340(8) 0.088(7) Uani 1 1 d . . . . .
H4G H 0.3418 0.9840 0.7557 0.106 Uiso 1 1 calc R U . . .
C5G C 0.3359(10) 0.9757(8) 0.6890(9) 0.116(10) Uani 1 1 d . . . . .
H5G H 0.3267 1.0046 0.6786 0.139 Uiso 1 1 calc R U . . .
C6G C 0.3422(8) 0.9463(7) 0.6594(8) 0.099(9) Uani 1 1 d . . . . .
H6G H 0.3403 0.9561 0.6302 0.118 Uiso 1 1 calc R U . . .
C7G C 0.3563(6) 0.8749(6) 0.6378(6) 0.058(5) Uani 1 1 d . . . . .
H7G H 0.3547 0.8883 0.6101 0.069 Uiso 1 1 calc R U . . .
N1G N 0.3628(4) 0.8339(5) 0.6415(5) 0.054(4) Uani 1 1 d . . . . .
C8G C 0.3714(6) 0.8097(6) 0.6059(6) 0.057(5) Uani 1 1 d . . . . .
C9G C 0.4002(8) 0.8342(8) 0.5906(10) 0.118(11) Uani 1 1 d . . . . .
H9G1 H 0.4048 0.8168 0.5673 0.177 Uiso 1 1 calc R U . . .
H9G2 H 0.3875 0.8623 0.5770 0.177 Uiso 1 1 calc R U . . .
H9G3 H 0.4270 0.8393 0.6175 0.177 Uiso 1 1 calc R U . . .
C10G C 0.3298(7) 0.7984(8) 0.5652(6) 0.094(8) Uani 1 1 d . . . . .
H10J H 0.3350 0.7824 0.5415 0.141 Uiso 1 1 calc R U . . .
H10K H 0.3133 0.7800 0.5763 0.141 Uiso 1 1 calc R U . . .
H10L H 0.3144 0.8254 0.5516 0.141 Uiso 1 1 calc R U . . .
C11G C 0.3905(6) 0.7669(6) 0.6288(6) 0.052(4) Uani 1 1 d . . . . .
O1G O 0.4097(3) 0.7455(3) 0.6102(3) 0.046(3) Uani 1 1 d . . . . .
O3G O 0.3842(3) 0.7528(3) 0.6628(3) 0.045(3) Uani 1 1 d . . . . .
O2H O 0.2587(4) 0.2674(4) 0.6372(4) 0.062(3) Uani 1 1 d . . . . .
C1H C 0.2535(6) 0.2018(6) 0.5932(6) 0.061(5) Uani 1 1 d . . . . .
C2H C 0.2370(6) 0.2336(6) 0.6131(5) 0.052(5) Uani 1 1 d . . . . .
C3H C 0.1966(6) 0.2286(7) 0.6080(7) 0.067(5) Uani 1 1 d . . . . .
H3H H 0.1852 0.2503 0.6206 0.081 Uiso 1 1 calc R U . . .
C4H C 0.1724(6) 0.1933(7) 0.5851(6) 0.066(5) Uani 1 1 d . . . . .
H4H H 0.1444 0.1914 0.5814 0.079 Uiso 1 1 calc R U . . .
C5H C 0.1886(8) 0.1603(7) 0.5671(7) 0.084(7) Uani 1 1 d . . . . .
H5H H 0.1728 0.1347 0.5532 0.101 Uiso 1 1 calc R U . . .
C6H C 0.2274(7) 0.1662(7) 0.5705(7) 0.074(6) Uani 1 1 d . . . . .
H6H H 0.2379 0.1448 0.5565 0.089 Uiso 1 1 calc R U . . .
C7H C 0.2926(8) 0.2065(7) 0.5902(7) 0.080(7) Uani 1 1 d . . . . .
H7H H 0.2992 0.1853 0.5726 0.097 Uiso 1 1 calc R U . . .
N1H N 0.3191(6) 0.2370(5) 0.6093(5) 0.067(4) Uani 1 1 d . . . . .
C8H C 0.3550(7) 0.2421(7) 0.5973(7) 0.074(6) Uani 1 1 d . . . . .
C9H C 0.3397(10) 0.2507(11) 0.5449(9) 0.170(17) Uani 1 1 d . . . . .
H9H1 H 0.3639 0.2540 0.5378 0.255 Uiso 1 1 calc R U . . .
H9H2 H 0.3226 0.2259 0.5272 0.255 Uiso 1 1 calc R U . . .
H9H3 H 0.3230 0.2776 0.5363 0.255 Uiso 1 1 calc R U . . .
C10H C 0.3872(9) 0.2039(8) 0.6174(14) 0.170(17) Uani 1 1 d . . . . .
H10M H 0.4104 0.2084 0.6088 0.255 Uiso 1 1 calc R U . . .
H10N H 0.3980 0.2034 0.6514 0.255 Uiso 1 1 calc R U . . .
H10O H 0.3734 0.1759 0.6046 0.255 Uiso 1 1 calc R U . . .
C11H C 0.3788(6) 0.2832(6) 0.6225(6) 0.056(5) Uani 1 1 d . . . . .
O1H O 0.4054(4) 0.2986(4) 0.6112(4) 0.053(3) Uani 1 1 d . . . . .
O3H O 0.3698(4) 0.2991(4) 0.6544(4) 0.054(3) Uani 1 1 d . . . . .
O2I O 0.5125(4) 0.3010(4) 0.8819(4) 0.058(3) Uani 1 1 d . . . . .
C1I C 0.5048(6) 0.2277(6) 0.9089(6) 0.057(5) Uani 1 1 d . . . . .
C2I C 0.5244(6) 0.2695(6) 0.9150(5) 0.054(5) Uani 1 1 d . . . . .
C3I C 0.5574(6) 0.2795(7) 0.9573(6) 0.069(6) Uani 1 1 d . . . . .
H3I H 0.5700 0.3077 0.9624 0.083 Uiso 1 1 calc R U . . .
C4I C 0.5721(6) 0.2480(7) 0.9924(6) 0.064(5) Uani 1 1 d . . . . .
H4I H 0.5952 0.2547 1.0212 0.077 Uiso 1 1 calc R U . . .
C5I C 0.5535(7) 0.2067(7) 0.9861(6) 0.072(6) Uani 1 1 d . . . . .
H5I H 0.5639 0.1851 1.0098 0.086 Uiso 1 1 calc R U . . .
C6I C 0.5193(6) 0.1983(7) 0.9441(6) 0.072(6) Uani 1 1 d . . . . .
H6I H 0.5056 0.1707 0.9399 0.086 Uiso 1 1 calc R U . . .
C7I C 0.4685(6) 0.2154(6) 0.8666(6) 0.064(5) Uani 1 1 d . . . . .
H7I H 0.4608 0.1854 0.8651 0.077 Uiso 1 1 calc R U . . .
N1I N 0.4451(4) 0.2380(5) 0.8309(5) 0.051(4) Uani 1 1 d . . . . .
C8I C 0.4069(6) 0.2178(6) 0.7957(6) 0.063(5) Uani 1 1 d . . . . .
C9I C 0.4151(8) 0.1764(8) 0.7773(8) 0.122(11) Uani 1 1 d . . . . .
H9I1 H 0.3887 0.1643 0.7540 0.184 Uiso 1 1 calc R U . . .
H9I2 H 0.4340 0.1819 0.7627 0.184 Uiso 1 1 calc R U . . .
H9I3 H 0.4280 0.1553 0.8028 0.184 Uiso 1 1 calc R U . . .
C10I C 0.3758(7) 0.2114(10) 0.8144(7) 0.117(11) Uani 1 1 d . . . . .
H10P H 0.3506 0.1979 0.7905 0.175 Uiso 1 1 calc R U . . .
H10Q H 0.3875 0.1921 0.8418 0.175 Uiso 1 1 calc R U . . .
H10R H 0.3686 0.2398 0.8234 0.175 Uiso 1 1 calc R U . . .
C11I C 0.3891(6) 0.2503(6) 0.7545(6) 0.054(5) Uani 1 1 d . . . . .
O1I O 0.3547(4) 0.2387(4) 0.7212(4) 0.064(3) Uani 1 1 d . . . . .
O3I O 0.4073(3) 0.2864(3) 0.7548(3) 0.044(3) Uani 1 1 d . . . . .
O1K O 0.4050(4) 0.5296(4) 0.5316(4) 0.051(3) Uani 1 1 d . . . . .
O2K O 0.4106(4) 0.5911(5) 0.4972(5) 0.075(4) Uani 1 1 d . . . . .
C1K C 0.4153(6) 0.5506(7) 0.5055(6) 0.061(5) Uani 1 1 d . . . . .
C2K C 0.4396(8) 0.5272(7) 0.4814(8) 0.096(8) Uani 1 1 d . . . . .
H2K1 H 0.4415 0.5467 0.4578 0.143 Uiso 1 1 calc R U . . .
H2K2 H 0.4249 0.5003 0.4664 0.143 Uiso 1 1 calc R U . . .
H2K3 H 0.4678 0.5199 0.5047 0.143 Uiso 1 1 calc R U . . .
O3K O 0.3723(4) 0.6598(4) 0.7646(3) 0.048(3) Uani 1 1 d . . . . .
O4K O 0.3039(4) 0.6459(4) 0.7406(4) 0.056(3) Uani 1 1 d . . . . .
C3K C 0.3408(7) 0.6552(5) 0.7714(6) 0.050(4) Uani 1 1 d . . . . .
C4K C 0.3443(6) 0.6636(7) 0.8198(6) 0.073(6) Uani 1 1 d . . . . .
H4K1 H 0.3254 0.6438 0.8259 0.110 Uiso 1 1 calc R U . . .
H4K2 H 0.3366 0.6940 0.8222 0.110 Uiso 1 1 calc R U . . .
H4K3 H 0.3731 0.6583 0.8428 0.110 Uiso 1 1 calc R U . . .
O5K O 0.3902(3) 0.3744(4) 0.7831(4) 0.051(3) Uani 1 1 d . . . . .
O6K O 0.4177(5) 0.3292(5) 0.8459(5) 0.088(5) Uani 1 1 d . . . . .
C5K C 0.3926(7) 0.3597(8) 0.8232(7) 0.081(6) Uani 1 1 d . . . . .
C6K C 0.3663(11) 0.3817(16) 0.8398(10) 0.24(3) Uani 1 1 d . . . . .
H6K1 H 0.3749 0.3743 0.8726 0.363 Uiso 1 1 calc R U . . .
H6K2 H 0.3372 0.3725 0.8215 0.363 Uiso 1 1 calc R U . . .
H6K3 H 0.3686 0.4134 0.8367 0.363 Uiso 1 1 calc R U . . .
N1N N 0.5364(6) 0.5217(6) 0.6785(6) 0.069(5) Uani 1 1 d . . . . .
O1N O 0.5056(5) 0.5398(4) 0.6461(4) 0.069(4) Uani 1 1 d . . . . .
O2N O 0.5403(4) 0.4805(5) 0.6812(4) 0.068(4) Uani 1 1 d . . . . .
O3N O 0.5664(5) 0.5456(5) 0.7055(4) 0.076(4) Uani 1 1 d . . . . .
N2N N 0.2931(6) 0.6553(5) 0.5485(5) 0.052(4) Uani 1 1 d . . . . .
O4N O 0.3270(6) 0.6619(5) 0.5544(5) 0.089(5) Uani 1 1 d . . . . .
O5N O 0.2818(5) 0.6308(6) 0.5766(6) 0.102(5) Uani 1 1 d . . . . .
O6N O 0.2612(6) 0.6662(9) 0.5130(7) 0.170(10) Uani 1 1 d . . . . .
N1 N 0.5000 0.5211(4) 0.7500 0.016(3) Uiso 1 2 d S . P G .
O1X O 0.4799(6) 0.5576(7) 0.7336(6) 0.041(5) Uiso 0.5 1 d . . P . .
O2X O 0.4664(6) 0.5217(6) 0.7171(6) 0.035(4) Uiso 0.5 1 d . . P G .
O3X O 0.4810(6) 0.4864(7) 0.7327(7) 0.047(5) Uiso 0.5 1 d . . P . .
N3N N 0.5000 0.2410(11) 0.7500 0.102(9) Uiso 1 2 d S . P . .
O7N O 0.5087(5) 0.2598(5) 0.7878(5) 0.095(5) Uani 1 1 d . . . . .
O8N O 0.5000 0.1974(15) 0.7500 0.214(17) Uiso 1 2 d S . P . .
O1M O 0.3032(4) 0.3930(4) 0.5821(4) 0.061(3) Uani 1 1 d . . . . .
H1M H 0.2850 0.3871 0.5915 0.092 Uiso 1 1 calc R U . . .
C1M C 0.2874(7) 0.3845(7) 0.5347(6) 0.081(7) Uani 1 1 d . . . . .
H1M1 H 0.2757(14) 0.353(3) 0.5281(10) 0.122 Uiso 1 1 calc R U . . .
H1M2 H 0.311(2) 0.3879(8) 0.5239(13) 0.122 Uiso 1 1 calc R U . . .
H1M3 H 0.263(3) 0.407(2) 0.517(2) 0.122 Uiso 1 1 calc R U . . .
O2M O 0.2746(6) 0.4424(6) 0.2753(6) 0.120(6) Uiso 1 1 d . . . . .
H2M H 0.2567 0.4245 0.2577 0.179 Uiso 1 1 calc R U . . .
C2M C 0.2520(12) 0.4791(13) 0.2905(14) 0.194(17) Uiso 1 1 d . . . . .
H2M1 H 0.2508 0.4704 0.3195 0.291 Uiso 1 1 calc R U . . .
H2M2 H 0.2236 0.4833 0.2661 0.291 Uiso 1 1 calc R U . . .
H2M3 H 0.2677 0.5066 0.2955 0.291 Uiso 1 1 calc R U . . .
O3M O 0.2324(5) 0.3570(6) 0.2534(6) 0.113(6) Uiso 1 1 d . . . . .
H3M H 0.2528 0.3532 0.2469 0.169 Uiso 1 1 calc R U . . .
C3M C 0.2345(7) 0.3251(8) 0.2887(7) 0.091(7) Uiso 1 1 d . . . . .
H3M1 H 0.2561 0.3340 0.3192 0.137 Uiso 1 1 calc R U . . .
H3M2 H 0.2413 0.2961 0.2806 0.137 Uiso 1 1 calc R U . . .
H3M3 H 0.2073 0.3238 0.2900 0.137 Uiso 1 1 calc R U . . .
O4M O 0.2401(5) 0.3496(5) 0.5953(5) 0.089(4) Uiso 1 1 d . . . . .
H4M H 0.2443 0.3236 0.6051 0.133 Uiso 1 1 calc R U . . .
C4M C 0.2063(8) 0.3685(9) 0.6042(9) 0.117(9) Uiso 1 1 d . . . . .
H4MA H 0.2084 0.3578 0.6342 0.175 Uiso 1 1 calc R U . . .
H4MB H 0.1793 0.3599 0.5793 0.175 Uiso 1 1 calc R U . . .
H4MC H 0.2087 0.4005 0.6051 0.175 Uiso 1 1 calc R U . . .
O5M O 0.5456(8) 0.8405(8) 0.7187(8) 0.067(7) Uiso 0.5 1 d . . P A 1
H5M H 0.5715 0.8413 0.7354 0.100 Uiso 0.5 1 calc R U P A 1
C5M C 0.5372(12) 0.8495(12) 0.6702(12) 0.065(10) Uiso 0.5 1 d . . P A 1
H5MA H 0.5113 0.8348 0.6493 0.097 Uiso 0.5 1 calc R U P A 1
H5MB H 0.5605 0.8385 0.6642 0.097 Uiso 0.5 1 calc R U P A 1
H5MC H 0.5343 0.8811 0.6645 0.097 Uiso 0.5 1 calc R U P A 1
O6M O 0.5033(10) 0.7777(6) 0.7454(12) 0.050(6) Uiso 0.5 1 d D . P B -11
H6M H 0.5023 0.7851 0.7195 0.075 Uiso 0.5 1 calc R U P B -11
C6M C 0.4810(15) 0.8078(13) 0.7588(18) 0.112(17) Uiso 0.5 1 d D . P B -11
H6M1 H 0.4972 0.8153 0.7918 0.167 Uiso 0.5 1 calc R U P B -11
H6M2 H 0.4542 0.7950 0.7544 0.167 Uiso 0.5 1 calc R U P B -11
H6M3 H 0.4759 0.8344 0.7398 0.167 Uiso 0.5 1 calc R U P B -11
O1W O 0.3269(4) 0.5319(4) 0.7372(4) 0.058(3) Uiso 0.5 1 d . . P C 1
O8M O 0.3269(4) 0.5319(4) 0.7372(4) 0.058(3) Uiso 0.5 1 d . . P C 2
H8M H 0.3029 0.5370 0.7352 0.086 Uiso 0.5 1 d R U P C 2
C8M C 0.3482(12) 0.4992(13) 0.7746(12) 0.067(10) Uiso 0.5 1 d . . P C 2
H8M1 H 0.3274 0.4789 0.7763 0.100 Uiso 0.5 1 calc R U P C 2
H8M2 H 0.3627 0.5142 0.8045 0.100 Uiso 0.5 1 calc R U P C 2
H8M3 H 0.3686 0.4827 0.7676 0.100 Uiso 0.5 1 calc R U P C 2
O2W O 0.3701(11) 0.4621(11) 0.7935(11) 0.105(10) Uiso 0.5 1 d . . P D 1
O3W O 0.4841(4) 0.6391(4) 0.5896(4) 0.069(4) Uiso 0.5 1 d . . P C 1
O9M O 0.4841(4) 0.6391(4) 0.5896(4) 0.069(4) Uiso 0.5 1 d . . P C 2
H9MA H 0.4732 0.6290 0.5623 0.083 Uiso 0.5 1 d R U P C 2
C9M C 0.5254(15) 0.6322(15) 0.6084(16) 0.092(14) Uiso 0.5 1 d . . P C 2
H9M1 H 0.5379 0.6501 0.5922 0.138 Uiso 0.5 1 calc R U P C 2
H9M2 H 0.5309 0.6011 0.6055 0.138 Uiso 0.5 1 calc R U P C 2
H9M3 H 0.5376 0.6403 0.6415 0.138 Uiso 0.5 1 calc R U P C 2
O4W O 0.5671(10) 0.6214(10) 0.6548(11) 0.097(10) Uiso 0.5 1 d . . P E 1
O8W O 0.4789(9) 0.4745(9) 0.5702(10) 0.084(8) Uiso 0.5 1 d . . P F 10
O7W O 0.4998(4) 0.3941(4) 0.6057(4) 0.059(3) Uiso 0.5 1 d . . P G 1
O7M O 0.4998(4) 0.3941(4) 0.6057(4) 0.059(3) Uiso 0.5 1 d . . P G 2
H7M H 0.5252 0.3870 0.6178 0.088 Uiso 0.5 1 d R U P G 2
C7M C 0.4947(12) 0.4335(12) 0.5819(12) 0.062(10) Uiso 0.5 1 d . . P G 2
H7M1 H 0.4814 0.4280 0.5482 0.093 Uiso 0.5 1 calc R U P G 2
H7M2 H 0.5221 0.4471 0.5906 0.093 Uiso 0.5 1 calc R U P G 2
H7M3 H 0.4770 0.4532 0.5900 0.093 Uiso 0.5 1 calc R U P G 2
O10M O 0.4563(10) 0.6403(10) 0.4398(10) 0.095(9) Uiso 0.5 1 d . . P H 3
H10S H 0.4412 0.6567 0.4177 0.143 Uiso 0.5 1 calc R U P H 3
C10M C 0.4816(13) 0.6661(14) 0.4786(14) 0.080(12) Uiso 0.5 1 d . . P H 3
H10T H 0.5100 0.6678 0.4806 0.120 Uiso 0.5 1 calc R U P H 3
H10U H 0.4826 0.6527 0.5071 0.120 Uiso 0.5 1 calc R U P H 3
H10V H 0.4698 0.6956 0.4750 0.120 Uiso 0.5 1 calc R U P H 3
O5W O 0.4754(11) 0.6350(11) 0.5068(11) 0.045(9) Uiso 0.3 1 d . . P I 4
O6W O 0.0483(16) 0.6121(16) 0.5983(16) 0.043(12) Uiso 0.2 1 d . . P J 5
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O3 Dy1 O3 91.9(5) 2_656 .
O3 Dy1 O1 76.0(3) 2_656 2_656
O3 Dy1 O1 134.3(3) . 2_656
O3 Dy1 O1 134.3(3) 2_656 .
O3 Dy1 O1 76.0(3) . .
O1 Dy1 O1 141.7(5) 2_656 .
O3 Dy1 O2 145.8(3) 2_656 .
O3 Dy1 O2 72.3(3) . .
O1 Dy1 O2 93.3(3) 2_656 .
O1 Dy1 O2 72.3(3) . .
O3 Dy1 O2 72.3(3) 2_656 2_656
O3 Dy1 O2 145.8(3) . 2_656
O1 Dy1 O2 72.3(3) 2_656 2_656
O1 Dy1 O2 93.3(3) . 2_656
O2 Dy1 O2 135.7(5) . 2_656
O3 Dy1 O3A 64.2(3) 2_656 2_656
O3 Dy1 O3A 70.4(3) . 2_656
O1 Dy1 O3A 64.6(3) 2_656 2_656
O1 Dy1 O3A 142.5(3) . 2_656
O2 Dy1 O3A 81.9(3) . 2_656
O2 Dy1 O3A 124.0(3) 2_656 2_656
O3 Dy1 O3A 70.4(3) 2_656 .
O3 Dy1 O3A 64.2(3) . .
O1 Dy1 O3A 142.5(3) 2_656 .
O1 Dy1 O3A 64.6(3) . .
O2 Dy1 O3A 124.0(3) . .
O2 Dy1 O3A 81.9(3) 2_656 .
O3A Dy1 O3A 112.6(4) 2_656 .
O3 Dy1 O1X 120.4(4) 2_656 2_656
O3 Dy1 O1X 147.4(4) . 2_656
O1 Dy1 O1X 59.1(5) 2_656 2_656
O1 Dy1 O1X 82.9(5) . 2_656
O2 Dy1 O1X 77.8(4) . 2_656
O2 Dy1 O1X 58.7(4) 2_656 2_656
O3A Dy1 O1X 118.1(5) 2_656 2_656
O3A Dy1 O1X 127.3(5) . 2_656
O3 Dy1 O1X 147.4(4) 2_656 .
O3 Dy1 O1X 120.4(4) . .
O1 Dy1 O1X 82.9(5) 2_656 .
O1 Dy1 O1X 59.1(5) . .
O2 Dy1 O1X 58.7(4) . .
O2 Dy1 O1X 77.8(4) 2_656 .
O3A Dy1 O1X 127.3(4) 2_656 .
O3A Dy1 O1X 118.1(5) . .
O1X Dy1 O1X 28.1(7) 2_656 .
O3 Dy1 Dy7 104.4(2) 2_656 .
O3 Dy1 Dy7 39.8(2) . .
O1 Dy1 Dy7 173.8(2) 2_656 .
O1 Dy1 Dy7 41.5(2) . .
O2 Dy1 Dy7 83.0(2) . .
O2 Dy1 Dy7 113.8(2) 2_656 .
O3A Dy1 Dy7 109.8(2) 2_656 .
O3A Dy1 Dy7 41.1(2) . .
O1X Dy1 Dy7 124.5(4) 2_656 .
O1X Dy1 Dy7 99.2(4) . .
O3 Dy1 Dy7 39.8(2) 2_656 2_656
O3 Dy1 Dy7 104.4(2) . 2_656
O1 Dy1 Dy7 41.5(2) 2_656 2_656
O1 Dy1 Dy7 173.8(2) . 2_656
O2 Dy1 Dy7 113.8(2) . 2_656
O2 Dy1 Dy7 83.0(2) 2_656 2_656
O3A Dy1 Dy7 41.1(2) 2_656 2_656
O3A Dy1 Dy7 109.8(2) . 2_656
O1X Dy1 Dy7 99.2(4) 2_656 2_656
O1X Dy1 Dy7 124.5(4) . 2_656
Dy7 Dy1 Dy7 136.09(5) . 2_656
O4 Dy2 O4 139.2(5) . 2_656
O4 Dy2 O6 139.1(3) . 2_656
O4 Dy2 O6 75.0(4) 2_656 2_656
O4 Dy2 O6 75.0(4) . .
O4 Dy2 O6 139.1(3) 2_656 .
O6 Dy2 O6 89.0(5) 2_656 .
O4 Dy2 O5 92.9(3) . 2_656
O4 Dy2 O5 71.2(3) 2_656 2_656
O6 Dy2 O5 76.7(3) 2_656 2_656
O6 Dy2 O5 141.9(3) . 2_656
O4 Dy2 O5 71.1(3) . .
O4 Dy2 O5 92.9(3) 2_656 .
O6 Dy2 O5 141.9(3) 2_656 .
O6 Dy2 O5 76.7(3) . .
O5 Dy2 O5 134.1(5) 2_656 .
O4 Dy2 O7 73.3(3) . .
O4 Dy2 O7 128.9(3) 2_656 .
O6 Dy2 O7 66.0(4) 2_656 .
O6 Dy2 O7 73.0(3) . .
O5 Dy2 O7 68.8(3) 2_656 .
O5 Dy2 O7 138.0(3) . .
O4 Dy2 O7 128.9(3) . 2_656
O4 Dy2 O7 73.3(3) 2_656 2_656
O6 Dy2 O7 73.0(3) 2_656 2_656
O6 Dy2 O7 66.0(4) . 2_656
O5 Dy2 O7 138.0(3) 2_656 2_656
O5 Dy2 O7 68.8(3) . 2_656
O7 Dy2 O7 121.5(5) . 2_656
O4 Dy2 O3X 80.2(5) . 2_656
O4 Dy2 O3X 59.5(5) 2_656 2_656
O6 Dy2 O3X 122.3(5) 2_656 2_656
O6 Dy2 O3X 148.8(5) . 2_656
O5 Dy2 O3X 57.1(5) 2_656 2_656
O5 Dy2 O3X 77.5(4) . 2_656
O7 Dy2 O3X 117.5(5) . 2_656
O7 Dy2 O3X 119.4(5) 2_656 2_656
O4 Dy2 O3X 59.5(5) . .
O4 Dy2 O3X 80.2(5) 2_656 .
O6 Dy2 O3X 148.7(5) 2_656 .
O6 Dy2 O3X 122.3(5) . .
O5 Dy2 O3X 77.5(4) 2_656 .
O5 Dy2 O3X 57.1(4) . .
O7 Dy2 O3X 119.4(5) . .
O7 Dy2 O3X 117.5(5) 2_656 .
O3X Dy2 O3X 26.5(8) 2_656 .
O4 Dy2 Dy10 84.9(2) . .
O4 Dy2 Dy10 107.9(2) 2_656 .
O6 Dy2 Dy10 107.6(2) 2_656 .
O6 Dy2 Dy10 41.3(2) . .
O5 Dy2 Dy10 175.4(2) 2_656 .
O5 Dy2 Dy10 41.3(2) . .
O7 Dy2 Dy10 114.3(2) . .
O7 Dy2 Dy10 44.0(2) 2_656 .
O3X Dy2 Dy10 118.4(4) 2_656 .
O3X Dy2 Dy10 97.9(4) . .
O4 Dy2 Dy10 107.9(2) . 2_656
O4 Dy2 Dy10 84.9(2) 2_656 2_656
O6 Dy2 Dy10 41.3(2) 2_656 2_656
O6 Dy2 Dy10 107.6(2) . 2_656
O5 Dy2 Dy10 41.3(2) 2_656 2_656
O5 Dy2 Dy10 175.4(2) . 2_656
O7 Dy2 Dy10 44.0(2) . 2_656
O7 Dy2 Dy10 114.3(2) 2_656 2_656
O3X Dy2 Dy10 97.9(4) 2_656 2_656
O3X Dy2 Dy10 118.4(4) . 2_656
Dy10 Dy2 Dy10 143.31(5) . 2_656
O1 Dy3 O9 141.4(3) . .
O1 Dy3 O10 138.2(4) . .
O9 Dy3 O10 73.7(3) . .
O1 Dy3 O12 73.5(3) . .
O9 Dy3 O12 139.3(3) . .
O10 Dy3 O12 89.4(4) . .
O1 Dy3 O8 93.6(3) . .
O9 Dy3 O8 70.4(3) . .
O10 Dy3 O8 76.7(3) . .
O12 Dy3 O8 142.1(3) . .
O1 Dy3 O2 70.6(3) . .
O9 Dy3 O2 95.0(3) . .
O10 Dy3 O2 142.6(3) . .
O12 Dy3 O2 76.2(3) . .
O8 Dy3 O2 133.7(3) . .
O1 Dy3 O13 127.2(4) . .
O9 Dy3 O13 74.2(3) . .
O10 Dy3 O13 74.3(4) . .
O12 Dy3 O13 65.6(3) . .
O8 Dy3 O13 139.1(3) . .
O2 Dy3 O13 68.4(3) . .
O1 Dy3 O11 72.4(3) . .
O9 Dy3 O11 127.5(3) . .
O10 Dy3 O11 66.2(3) . .
O12 Dy3 O11 73.5(3) . .
O8 Dy3 O11 68.6(3) . .
O2 Dy3 O11 137.3(3) . .
O13 Dy3 O11 122.3(3) . .
O1 Dy3 O1X 60.0(5) . .
O9 Dy3 O1X 81.8(5) . .
O10 Dy3 O1X 147.9(5) . .
O12 Dy3 O1X 122.6(5) . .
O8 Dy3 O1X 75.7(5) . .
O2 Dy3 O1X 58.6(5) . .
O13 Dy3 O1X 118.7(5) . .
O11 Dy3 O1X 117.2(5) . .
O1 Dy3 O2X 81.6(4) . .
O9 Dy3 O2X 60.0(4) . .
O10 Dy3 O2X 122.9(5) . .
O12 Dy3 O2X 147.6(5) . .
O8 Dy3 O2X 58.2(5) . .
O2 Dy3 O2X 76.2(4) . .
O13 Dy3 O2X 118.1(5) . .
O11 Dy3 O2X 118.4(4) . .
O1X Dy3 O2X 25.3(5) . .
O1 Dy3 Dy51 110.2(5) . .
O9 Dy3 Dy51 84.6(4) . .
O10 Dy3 Dy51 36.5(7) . .
O12 Dy3 Dy51 103.6(6) . .
O8 Dy3 Dy51 46.8(8) . .
O2 Dy3 Dy51 179.1(7) . .
O13 Dy3 Dy51 110.8(7) . .
O11 Dy3 Dy51 43.2(4) . .
O1X Dy3 Dy51 122.1(8) . .
O2X Dy3 Dy51 104.2(8) . .
O1 Dy3 Dy8 83.6(2) . .
O9 Dy3 Dy8 109.3(2) . .
O10 Dy3 Dy8 108.2(3) . .
O12 Dy3 Dy8 41.0(3) . .
O8 Dy3 Dy8 174.9(2) . .
O2 Dy3 Dy8 41.2(2) . .
O13 Dy3 Dy8 43.6(3) . .
O11 Dy3 Dy8 114.3(2) . .
O1X Dy3 Dy8 99.2(4) . .
O2X Dy3 Dy8 117.0(4) . .
Dy51 Dy3 Dy8 138.2(7) . .
O14 Dy4 O15 90.2(4) . .
O14 Dy4 O5 144.4(3) . .
O15 Dy4 O5 71.5(4) . .
O14 Dy4 O9 76.2(4) . .
O15 Dy4 O9 133.5(3) . .
O5 Dy4 O9 94.3(3) . .
O14 Dy4 O8 72.2(3) . .
O15 Dy4 O8 145.4(4) . .
O5 Dy4 O8 138.0(3) . .
O9 Dy4 O8 72.0(3) . .
O14 Dy4 O4 133.2(4) . .
O15 Dy4 O4 75.8(3) . .
O5 Dy4 O4 72.8(3) . .
O9 Dy4 O4 143.3(3) . .
O8 Dy4 O4 94.5(3) . .
O14 Dy4 O3X 146.6(5) . .
O15 Dy4 O3X 123.1(5) . .
O5 Dy4 O3X 60.9(5) . .
O9 Dy4 O3X 81.3(5) . .
O8 Dy4 O3X 77.6(5) . .
O4 Dy4 O3X 62.2(5) . .
O14 Dy4 O2X 122.0(5) . .
O15 Dy4 O2X 147.7(5) . .
O5 Dy4 O2X 79.0(5) . .
O9 Dy4 O2X 60.5(4) . .
O8 Dy4 O2X 59.5(5) . .
O4 Dy4 O2X 83.1(4) . .
O3X Dy4 O2X 25.2(5) . .
O14 Dy4 O3B 64.6(3) . .
O15 Dy4 O3B 69.8(3) . .
O5 Dy4 O3B 80.2(3) . .
O9 Dy4 O3B 64.2(3) . .
O8 Dy4 O3B 123.8(3) . .
O4 Dy4 O3B 141.5(3) . .
O3X Dy4 O3B 125.6(5) . .
O2X Dy4 O3B 118.4(4) . .
O14 Dy4 O3C 70.1(4) . .
O15 Dy4 O3C 64.4(3) . .
O5 Dy4 O3C 123.3(3) . .
O9 Dy4 O3C 142.1(3) . .
O8 Dy4 O3C 81.4(3) . .
O4 Dy4 O3C 63.5(3) . .
O3X Dy4 O3C 119.2(5) . .
O2X Dy4 O3C 126.2(4) . .
O3B Dy4 O3C 113.6(3) . .
O14 Dy4 Dy6 40.2(3) . .
O15 Dy4 Dy6 102.8(2) . .
O5 Dy4 Dy6 113.1(2) . .
O9 Dy4 Dy6 41.5(2) . .
O8 Dy4 Dy6 83.0(2) . .
O4 Dy4 Dy6 173.4(3) . .
O3X Dy4 Dy6 122.8(4) . .
O2X Dy4 Dy6 100.8(4) . .
O3B Dy4 Dy6 40.7(2) . .
O3C Dy4 Dy6 110.0(2) . .
O14 Dy4 Dy9 102.9(3) . .
O15 Dy4 Dy9 39.6(2) . .
O5 Dy4 Dy9 82.5(2) . .
O9 Dy4 Dy9 173.1(2) . .
O8 Dy4 Dy9 114.4(2) . .
O4 Dy4 Dy9 41.3(2) . .
O3X Dy4 Dy9 102.2(4) . .
O2X Dy4 Dy9 124.4(4) . .
O3B Dy4 Dy9 109.1(2) . .
O3C Dy4 Dy9 40.8(2) . .
Dy6 Dy4 Dy9 134.60(5) . .
O1C Dy5 O8 100.1(4) . .
O1C Dy5 O2F 101.6(4) . .
O8 Dy5 O2F 135.7(4) . .
O1C Dy5 O1D 85.1(4) . .
O8 Dy5 O1D 146.8(4) . .
O2F Dy5 O1D 73.5(4) . .
O1C Dy5 O14 79.3(4) . .
O8 Dy5 O14 70.5(3) . .
O2F Dy5 O14 151.7(4) . .
O1D Dy5 O14 78.5(4) . .
O1C Dy5 O10 145.4(4) . .
O8 Dy5 O10 77.1(3) . .
O2F Dy5 O10 104.0(4) . .
O1D Dy5 O10 80.3(4) . .
O14 Dy5 O10 67.2(4) . .
O1C Dy5 O8M 73.6(4) . .
O8 Dy5 O8M 76.8(4) . .
O2F Dy5 O8M 73.1(4) . .
O1D Dy5 O8M 135.3(4) . .
O14 Dy5 O8M 132.5(4) . .
O10 Dy5 O8M 136.5(4) . .
O1C Dy5 O1W 73.6(4) . .
O8 Dy5 O1W 76.8(4) . .
O2F Dy5 O1W 73.1(4) . .
O1D Dy5 O1W 135.3(4) . .
O14 Dy5 O1W 132.5(4) . .
O10 Dy5 O1W 136.5(4) . .
O1C Dy5 O11 146.4(4) . .
O8 Dy5 O11 70.7(3) . .
O2F Dy5 O11 69.8(4) . .
O1D Dy5 O11 120.7(4) . .
O14 Dy5 O11 123.9(4) . .
O10 Dy5 O11 65.9(3) . .
O8M Dy5 O11 72.8(4) . .
O1W Dy5 O11 72.8(4) . .
O1C Dy5 Zn1 132.6(3) . .
O8 Dy5 Zn1 104.5(2) . .
O2F Dy5 Zn1 35.7(3) . .
O1D Dy5 Zn1 95.1(3) . .
O14 Dy5 Zn1 147.3(3) . .
O10 Dy5 Zn1 80.1(3) . .
O8M Dy5 Zn1 73.6(3) . .
O1W Dy5 Zn1 73.6(3) . .
O11 Dy5 Zn1 34.6(2) . .
O1C Dy5 Dy3 141.7(3) . .
O8 Dy5 Dy3 42.5(2) . .
O2F Dy5 Dy3 112.3(3) . .
O1D Dy5 Dy3 120.7(3) . .
O14 Dy5 Dy3 79.1(3) . .
O10 Dy5 Dy3 40.5(2) . .
O8M Dy5 Dy3 99.0(3) . .
O1W Dy5 Dy3 99.0(3) . .
O11 Dy5 Dy3 45.1(2) . .
Zn1 Dy5 Dy3 76.84(8) . .
O1C Dy5 Dy4 81.4(3) . .
O8 Dy5 Dy4 36.5(2) . .
O2F Dy5 Dy4 172.1(3) . .
O1D Dy5 Dy4 114.3(3) . .
O14 Dy5 Dy4 35.8(2) . .
O10 Dy5 Dy4 76.5(3) . .
O8M Dy5 Dy4 101.0(3) . .
O1W Dy5 Dy4 101.0(3) . .
O11 Dy5 Dy4 103.6(2) . .
Zn1 Dy5 Dy4 138.13(6) . .
Dy3 Dy5 Dy4 62.82(5) . .
O10 Dy51 O1D 92.0(16) . .
O10 Dy51 O2F 118.9(18) . .
O1D Dy51 O2F 79.6(9) . .
O10 Dy51 O11 72.7(9) . .
O1D Dy51 O11 136.8(19) . .
O2F Dy51 O11 73.8(7) . .
O10 Dy51 O14 71.0(7) . .
O1D Dy51 O14 81.4(7) . .
O2F Dy51 O14 158.8(9) . .
O11 Dy51 O14 127.2(8) . .
O10 Dy51 O8 78.8(7) . .
O1D Dy51 O8 148.2(9) . .
O2F Dy51 O8 131.5(11) . .
O11 Dy51 O8 69.5(6) . .
O14 Dy51 O8 66.8(7) . .
O10 Dy51 O1C 143.5(9) . .
O1D Dy51 O1C 82.0(8) . .
O2F Dy51 O1C 95.4(11) . .
O11 Dy51 O1C 133.3(16) . .
O14 Dy51 O1C 72.6(9) . .
O8 Dy51 O1C 87.5(13) . .
O10 Dy51 O8M 136.7(8) . .
O1D Dy51 O8M 130.3(12) . .
O2F Dy51 O8M 69.3(8) . .
O11 Dy51 O8M 69.6(7) . .
O14 Dy51 O8M 117.8(16) . .
O8 Dy51 O8M 68.8(10) . .
O1C Dy51 O8M 64.2(10) . .
O10 Dy51 O1W 136.7(8) . .
O1D Dy51 O1W 130.3(12) . .
O2F Dy51 O1W 69.3(8) . .
O11 Dy51 O1W 69.6(7) . .
O14 Dy51 O1W 117.8(16) . .
O8 Dy51 O1W 68.8(10) . .
O1C Dy51 O1W 64.2(10) . .
O10 Dy51 Zn1 88.9(11) . .
O1D Dy51 Zn1 104.7(12) . .
O2F Dy51 Zn1 38.7(5) . .
O11 Dy51 Zn1 37.3(4) . .
O14 Dy51 Zn1 159.3(13) . .
O8 Dy51 Zn1 105.5(6) . .
O1C Dy51 Zn1 127.4(10) . .
O8M Dy51 Zn1 73.6(5) . .
O1W Dy51 Zn1 73.6(5) . .
O10 Dy51 Dy3 41.3(4) . .
O1D Dy51 Dy3 133.3(16) . .
O2F Dy51 Dy3 119.4(8) . .
O11 Dy51 Dy3 46.9(4) . .
O14 Dy51 Dy3 80.8(5) . .
O8 Dy51 Dy3 44.5(4) . .
O1C Dy51 Dy3 131.6(12) . .
O8M Dy51 Dy3 96.1(7) . .
O1W Dy51 Dy3 96.1(7) . .
Zn1 Dy51 Dy3 80.8(5) . .
O10 Dy51 Dy6 34.4(4) . .
O1D Dy51 Dy6 77.3(9) . .
O2F Dy51 Dy6 142.6(17) . .
O11 Dy51 Dy6 104.6(10) . .
O14 Dy51 Dy6 38.6(5) . .
O8 Dy51 Dy6 78.2(5) . .
O1C Dy51 Dy6 109.8(6) . .
O8M Dy51 Dy6 146.5(10) . .
O1W Dy51 Dy6 146.5(10) . .
Zn1 Dy51 Dy6 122.6(12) . .
Dy3 Dy51 Dy6 62.2(4) . .
O10 Dy51 H10 19.3 . .
O1D Dy51 H10 83.3 . .
O2F Dy51 H10 100.3 . .
O11 Dy51 H10 69.1 . .
O14 Dy51 H10 86.7 . .
O8 Dy51 H10 95.2 . .
O1C Dy51 H10 156.1 . .
O8M Dy51 H10 138.6 . .
O1W Dy51 H10 138.6 . .
Zn1 Dy51 H10 74.7 . .
Dy3 Dy51 H10 52.9 . .
Dy6 Dy51 H10 48.2 . .
Dy61 Dy6 O2B 97(2) . .
Dy61 Dy6 O10 86(2) . .
O2B Dy6 O10 145.5(4) . .
Dy61 Dy6 O3B 124(2) . .
O2B Dy6 O3B 72.8(3) . .
O10 Dy6 O3B 132.6(3) . .
Dy61 Dy6 O14 154(2) . .
O2B Dy6 O14 108.3(4) . .
O10 Dy6 O14 69.0(4) . .
O3B Dy6 O14 72.0(4) . .
Dy61 Dy6 O1K 46(2) . .
O2B Dy6 O1K 82.7(4) . .
O10 Dy6 O1K 121.2(4) . .
O3B Dy6 O1K 77.8(4) . .
O14 Dy6 O1K 142.5(4) . .
Dy61 Dy6 O3D 111(2) . .
O2B Dy6 O3D 67.8(4) . .
O10 Dy6 O3D 79.1(4) . .
O3B Dy6 O3D 114.1(4) . .
O14 Dy6 O3D 73.2(4) . .
O1K Dy6 O3D 141.3(4) . .
Dy61 Dy6 O9 92(2) . .
O2B Dy6 O9 141.2(3) . .
O10 Dy6 O9 72.7(3) . .
O3B Dy6 O9 71.1(3) . .
O14 Dy6 O9 73.4(3) . .
O1K Dy6 O9 76.2(3) . .
O3D Dy6 O9 142.1(4) . .
Dy61 Dy6 O3E 36(2) . .
O2B Dy6 O3E 80.0(4) . .
O10 Dy6 O3E 82.5(3) . .
O3B Dy6 O3E 144.1(3) . .
O14 Dy6 O3E 140.5(4) . .
O1K Dy6 O3E 75.7(4) . .
O3D Dy6 O3E 75.1(4) . .
O9 Dy6 O3E 124.2(4) . .
Dy61 Dy6 Zn2 96(2) . .
O2B Dy6 Zn2 34.1(3) . .
O10 Dy6 Zn2 111.4(2) . .
O3B Dy6 Zn2 101.2(2) . .
O14 Dy6 Zn2 100.4(3) . .
O1K Dy6 Zn2 106.9(3) . .
O3D Dy6 Zn2 36.5(3) . .
O9 Dy6 Zn2 171.2(3) . .
O3E Dy6 Zn2 64.6(3) . .
Dy61 Dy6 Dy4 132(2) . .
O2B Dy6 Dy4 119.5(3) . .
O10 Dy6 Dy4 81.0(2) . .
O3B Dy6 Dy4 51.6(2) . .
O14 Dy6 Dy4 38.8(2) . .
O1K Dy6 Dy4 104.2(3) . .
O3D Dy6 Dy4 111.8(3) . .
O9 Dy6 Dy4 39.8(2) . .
O3E Dy6 Dy4 160.5(2) . .
Zn2 Dy6 Dy4 131.90(11) . .
Dy61 Dy6 Dy3 79(2) . .
O2B Dy6 Dy3 175.1(3) . .
O10 Dy6 Dy3 37.2(2) . .
O3B Dy6 Dy3 107.7(2) . .
O14 Dy6 Dy3 76.3(2) . .
O1K Dy6 Dy3 92.6(3) . .
O3D Dy6 Dy3 115.8(3) . .
O9 Dy6 Dy3 37.7(2) . .
O3E Dy6 Dy3 97.5(2) . .
Zn2 Dy6 Dy3 147.97(6) . .
Dy4 Dy6 Dy3 63.01(5) . .
Dy6 Dy61 O1K 123(3) . .
Dy6 Dy61 O3E 135(3) . .
O1K Dy61 O3E 93(2) . .
Dy6 Dy61 O10 81(3) . .
O1K Dy61 O10 137.3(15) . .
O3E Dy61 O10 91.3(11) . .
Dy6 Dy61 O2B 71(2) . .
O1K Dy61 O2B 87.1(9) . .
O3E Dy61 O2B 86.0(9) . .
O10 Dy61 O2B 135.6(17) . .
Dy6 Dy61 O9 76(3) . .
O1K Dy61 O9 80.7(8) . .
O3E Dy61 O9 142.7(19) . .
O10 Dy61 O9 70.9(8) . .
O2B Dy61 O9 129.8(16) . .
Dy6 Dy61 O3D 58(2) . .
O1K Dy61 O3D 148.0(10) . .
O3E Dy61 O3D 77.1(8) . .
O10 Dy61 O3D 73.9(9) . .
O2B Dy61 O3D 62.3(8) . .
O9 Dy61 O3D 125.2(19) . .
Dy6 Dy61 O3B 46(2) . .
O1K Dy61 O3B 76.4(9) . .
O3E Dy61 O3B 149.4(10) . .
O10 Dy61 O3B 116.2(18) . .
O2B Dy61 O3B 65.2(9) . .
O9 Dy61 O3B 64.6(9) . .
O3D Dy61 O3B 96.9(16) . .
Dy6 Dy61 O14 21(2) . .
O1K Dy61 O14 132.2(15) . .
O3E Dy61 O14 134.8(13) . .
O10 Dy61 O14 60.5(10) . .
O2B Dy61 O14 91.3(15) . .
O9 Dy61 O14 64.3(10) . .
O3D Dy61 O14 62.1(11) . .
O3B Dy61 O14 60.0(11) . .
Dy6 Dy61 O13 135(3) . .
O1K Dy61 O13 72.6(13) . .
O3E Dy61 O13 77.8(15) . .
O10 Dy61 O13 66.9(8) . .
O2B Dy61 O13 153(2) . .
O9 Dy61 O13 65.1(7) . .
O3D Dy61 O13 132.4(10) . .
O3B Dy61 O13 123.9(8) . .
O14 Dy61 O13 115.3(8) . .
Dy6 Dy61 Zn3 165(3) . .
O1K Dy61 Zn3 70.7(15) . .
O3E Dy61 Zn3 42.2(10) . .
O10 Dy61 Zn3 84.6(11) . .
O2B Dy61 Zn3 119.3(15) . .
O9 Dy61 Zn3 102.1(12) . .
O3D Dy61 Zn3 114.9(11) . .
O3B Dy61 Zn3 146.3(13) . .
O14 Dy61 Zn3 144.8(8) . .
O13 Dy61 Zn3 37.6(6) . .
Dy6 Dy61 Zn31 152(3) . .
O1K Dy61 Zn31 84.7(17) . .
O3E Dy61 Zn31 36.9(9) . .
O10 Dy61 Zn31 73.7(10) . .
O2B Dy61 Zn31 121.4(14) . .
O9 Dy61 Zn31 105.7(11) . .
O3D Dy61 Zn31 102.9(9) . .
O3B Dy61 Zn31 159.8(14) . .
O14 Dy61 Zn31 133.9(8) . .
O13 Dy61 Zn31 41.2(7) . .
Zn3 Dy61 Zn31 14.0(3) . .
O2A Dy7 O12 144.8(3) . .
O2A Dy7 O3K 82.4(4) . .
O12 Dy7 O3K 123.4(4) . .
O2A Dy7 O3 106.5(3) . .
O12 Dy7 O3 69.1(3) . .
O3K Dy7 O3 142.3(4) . .
O2A Dy7 O3A 73.1(3) . .
O12 Dy7 O3A 131.5(4) . .
O3K Dy7 O3A 77.4(4) . .
O3 Dy7 O3A 70.8(3) . .
O2A Dy7 O3G 66.8(3) . .
O12 Dy7 O3G 78.8(3) . .
O3K Dy7 O3G 139.9(4) . .
O3 Dy7 O3G 73.8(3) . .
O3A Dy7 O3G 114.5(3) . .
O2A Dy7 O1 141.3(3) . .
O12 Dy7 O1 72.7(3) . .
O3K Dy7 O1 77.3(4) . .
O3 Dy7 O1 73.5(3) . .
O3A Dy7 O1 70.6(3) . .
O3G Dy7 O1 142.5(3) . .
O2A Dy7 O3F 81.6(3) . .
O12 Dy7 O3F 81.8(3) . .
O3K Dy7 O3F 76.9(4) . .
O3 Dy7 O3F 139.9(3) . .
O3A Dy7 O3F 146.0(3) . .
O3G Dy7 O3F 73.9(3) . .
O1 Dy7 O3F 124.1(3) . .
O1A Dy8 O2 96.9(4) 2_656 .
O1A Dy8 O12 143.9(3) 2_656 .
O2 Dy8 O12 77.8(3) . .
O1A Dy8 O1G 83.1(4) 2_656 .
O2 Dy8 O1G 147.3(3) . .
O12 Dy8 O1G 83.1(4) . .
O1A Dy8 O2E 106.3(4) 2_656 .
O2 Dy8 O2E 135.3(4) . .
O12 Dy8 O2E 101.9(4) . .
O1G Dy8 O2E 74.4(4) . .
O1A Dy8 O3 77.3(3) 2_656 .
O2 Dy8 O3 70.2(3) . .
O12 Dy8 O3 67.2(3) . .
O1G Dy8 O3 78.0(3) . .
O2E Dy8 O3 151.4(4) . .
O1A Dy8 O13 146.1(4) 2_656 .
O2 Dy8 O13 70.4(3) . .
O12 Dy8 O13 66.1(3) . .
O1G Dy8 O13 124.7(4) . .
O2E Dy8 O13 69.1(3) . .
O3 Dy8 O13 123.5(3) . .
O1A Dy8 O9M 72.6(4) 2_656 .
O2 Dy8 O9M 77.2(4) . .
O12 Dy8 O9M 138.0(4) . .
O1G Dy8 O9M 132.5(4) . .
O2E Dy8 O9M 74.3(4) . .
O3 Dy8 O9M 131.9(4) . .
O13 Dy8 O9M 74.0(4) . .
O1A Dy8 O3W 72.6(4) 2_656 .
O2 Dy8 O3W 77.2(4) . .
O12 Dy8 O3W 138.0(4) . .
O1G Dy8 O3W 132.5(4) . .
O2E Dy8 O3W 74.3(4) . .
O3 Dy8 O3W 131.9(4) . .
O13 Dy8 O3W 74.0(4) . .
O1A Dy8 Zn3 136.0(3) 2_656 .
O2 Dy8 Zn3 104.0(2) . .
O12 Dy8 Zn3 79.1(2) . .
O1G Dy8 Zn3 98.0(3) . .
O2E Dy8 Zn3 35.3(3) . .
O3 Dy8 Zn3 146.3(2) . .
O13 Dy8 Zn3 34.3(2) . .
O9M Dy8 Zn3 75.0(3) . .
O3W Dy8 Zn3 75.0(3) . .
O1A Dy8 Zn31 143.1(3) 2_656 .
O2 Dy8 Zn31 109.7(3) . .
O12 Dy8 Zn31 69.0(4) . .
O1G Dy8 Zn31 87.3(4) . .
O2E Dy8 Zn31 37.0(4) . .
O3 Dy8 Zn31 135.1(4) . .
O13 Dy8 Zn31 39.8(3) . .
O9M Dy8 Zn31 88.7(5) . .
O3W Dy8 Zn31 88.7(5) . .
Zn3 Dy8 Zn31 13.8(3) . .
O1A Dy8 Dy3 139.0(3) 2_656 .
O2 Dy8 Dy3 43.2(2) . .
O12 Dy8 Dy3 40.8(2) . .
O1G Dy8 Dy3 123.9(3) . .
O2E Dy8 Dy3 110.3(3) . .
O3 Dy8 Dy3 79.3(2) . .
O13 Dy8 Dy3 44.4(2) . .
O9M Dy8 Dy3 100.2(3) . .
O3W Dy8 Dy3 100.2(3) . .
Zn3 Dy8 Dy3 75.42(5) . .
Zn31 Dy8 Dy3 74.3(2) . .
O2C Dy9 O6 144.9(4) . .
O2C Dy9 O15 107.8(4) . .
O6 Dy9 O15 68.7(3) . .
O2C Dy9 O5K 82.5(4) . .
O6 Dy9 O5K 122.6(4) . .
O15 Dy9 O5K 142.3(4) . .
O2C Dy9 O3C 73.0(4) . .
O6 Dy9 O3C 132.3(4) . .
O15 Dy9 O3C 71.9(4) . .
O5K Dy9 O3C 77.1(4) . .
O2C Dy9 O3H 67.5(4) . .
O6 Dy9 O3H 78.5(4) . .
O15 Dy9 O3H 73.5(3) . .
O5K Dy9 O3H 140.9(4) . .
O3C Dy9 O3H 114.7(4) . .
O2C Dy9 O4 140.5(4) . .
O6 Dy9 O4 73.7(4) . .
O15 Dy9 O4 73.5(3) . .
O5K Dy9 O4 76.1(4) . .
O3C Dy9 O4 70.1(4) . .
O3H Dy9 O4 142.7(4) . .
O2C Dy9 O3I 80.0(4) . .
O6 Dy9 O3I 82.7(4) . .
O15 Dy9 O3I 140.2(3) . .
O5K Dy9 O3I 76.6(4) . .
O3C Dy9 O3I 144.3(4) . .
O3H Dy9 O3I 74.1(3) . .
O4 Dy9 O3I 125.1(3) . .
O1B Dy10 O1H 84.8(4) . .
O1B Dy10 O5 98.2(3) . .
O1H Dy10 O5 146.4(4) . .
O1B Dy10 O6 146.4(4) . .
O1H Dy10 O6 81.0(4) . .
O5 Dy10 O6 78.2(3) . .
O1B Dy10 O2I 101.1(4) . 2_656
O1H Dy10 O2I 74.3(4) . 2_656
O5 Dy10 O2I 136.6(4) . 2_656
O6 Dy10 O2I 104.1(4) . 2_656
O1B Dy10 O15 80.2(3) . .
O1H Dy10 O15 78.3(4) . .
O5 Dy10 O15 69.4(3) . .
O6 Dy10 O15 67.2(3) . .
O2I Dy10 O15 152.2(4) 2_656 .
O1B Dy10 O7 144.0(4) . 2_656
O1H Dy10 O7 123.2(4) . 2_656
O5 Dy10 O7 71.4(3) . 2_656
O6 Dy10 O7 67.1(4) . 2_656
O2I Dy10 O7 70.1(4) 2_656 2_656
O15 Dy10 O7 124.2(3) . 2_656
O1B Dy10 O7M 72.9(4) . .
O1H Dy10 O7M 136.4(4) . .
O5 Dy10 O7M 75.2(4) . .
O6 Dy10 O7M 135.6(4) . .
O2I Dy10 O7M 73.9(4) 2_656 .
O15 Dy10 O7M 131.4(4) . .
O7 Dy10 O7M 71.1(4) 2_656 .
O1B Dy10 O7W 72.9(4) . .
O1H Dy10 O7W 136.4(4) . .
O5 Dy10 O7W 75.2(4) . .
O6 Dy10 O7W 135.6(4) . .
O2I Dy10 O7W 73.9(4) 2_656 .
O15 Dy10 O7W 131.4(4) . .
O7 Dy10 O7W 71.1(4) 2_656 .
O11 Zn1 N1F 161.0(5) . .
O11 Zn1 O2F 86.4(5) . .
N1F Zn1 O2F 92.3(6) . .
O11 Zn1 O4K 101.3(4) . .
N1F Zn1 O4K 97.4(6) . .
O2F Zn1 O4K 103.7(5) . .
O11 Zn1 O3F 96.6(4) . .
N1F Zn1 O3F 80.1(5) . .
O2F Zn1 O3F 165.1(4) . .
O4K Zn1 O3F 90.0(4) . .
O2D Zn2 O1E 112.2(6) . .
O2D Zn2 N1D 92.8(7) . .
O1E Zn2 N1D 109.0(6) . .
O2D Zn2 O2B 99.0(5) . .
O1E Zn2 O2B 96.7(4) . .
N1D Zn2 O2B 145.1(5) . .
O2D Zn2 O3D 153.5(6) . .
O1E Zn2 O3D 94.3(5) . .
N1D Zn2 O3D 77.0(6) . .
O2B Zn2 O3D 78.0(4) . .
Zn31 Zn3 O13 99.9(9) . .
Zn31 Zn3 N1E 76.4(9) . .
O13 Zn3 N1E 176.4(6) . .
Zn31 Zn3 O2E 87.8(10) . .
O13 Zn3 O2E 86.5(4) . .
N1E Zn3 O2E 93.1(5) . .
Zn31 Zn3 O3E 79.9(9) . .
O13 Zn3 O3E 100.3(4) . .
N1E Zn3 O3E 79.4(5) . .
O2E Zn3 O3E 166.8(6) . .
Zn31 Zn3 O2K 166.1(9) . .
O13 Zn3 O2K 93.2(5) . .
N1E Zn3 O2K 90.4(5) . .
O2E Zn3 O2K 97.5(6) . .
O3E Zn3 O2K 93.4(5) . .
Zn31 Zn3 O4N 15.2(9) . .
O13 Zn3 O4N 85.0(5) . .
N1E Zn3 O4N 91.3(5) . .
O2E Zn3 O4N 83.9(6) . .
O3E Zn3 O4N 85.3(5) . .
O2K Zn3 O4N 177.7(5) . .
Zn3 Zn31 O4N 157.1(14) . .
Zn3 Zn31 N1E 79.4(11) . .
O4N Zn31 N1E 123.0(12) . .
Zn3 Zn31 O3E 77.7(10) . .
O4N Zn31 O3E 109.1(11) . .
N1E Zn31 O3E 79.5(6) . .
Zn3 Zn31 O2E 69.4(10) . .
O4N Zn31 O2E 103.2(10) . .
N1E Zn31 O2E 89.7(7) . .
O3E Zn31 O2E 146.7(12) . .
Zn3 Zn31 O13 58.7(9) . .
O4N Zn31 O13 98.8(8) . .
N1E Zn31 O13 138.1(12) . .
O3E Zn31 O13 90.9(7) . .
O2E Zn31 O13 76.3(7) . .
Zn3 Zn31 N2N 161.5(12) . .
O4N Zn31 N2N 21.7(7) . .
N1E Zn31 N2N 111.5(10) . .
O3E Zn31 N2N 89.4(7) . .
O2E Zn31 N2N 123.7(9) . .
O13 Zn31 N2N 109.0(7) . .
O2H Zn4 O1I 119.1(5) . .
O2H Zn4 O2C 98.8(5) . .
O1I Zn4 O2C 97.2(5) . .
O2H Zn4 N1H 89.5(6) . .
O1I Zn4 N1H 105.9(6) . .
O2C Zn4 N1H 147.7(6) . .
O2H Zn4 O3H 145.4(5) . .
O1I Zn4 O3H 95.4(5) . .
O2C Zn4 O3H 78.0(5) . .
N1H Zn4 O3H 77.7(6) . .
O2G Zn5 O1F 117.0(6) . .
O2G Zn5 O2A 97.8(5) . .
O1F Zn5 O2A 99.6(4) . .
O2G Zn5 N1G 90.0(6) . .
O1F Zn5 N1G 107.5(5) . .
O2A Zn5 N1G 144.5(5) . .
O2G Zn5 O3G 148.5(6) . .
O1F Zn5 O3G 94.5(4) . .
O2A Zn5 O3G 77.5(4) . .
N1G Zn5 O3G 78.0(5) . .
O7 Zn6 N1I 165.4(5) . .
O7 Zn6 O2I 86.4(4) . .
N1I Zn6 O2I 94.0(5) . .
O7 Zn6 O6K 97.1(6) . .
N1I Zn6 O6K 97.3(6) . .
O2I Zn6 O6K 100.1(6) . .
O7 Zn6 O3I 97.0(4) . .
N1I Zn6 O3I 79.6(5) . .
O2I Zn6 O3I 166.8(5) . .
O6K Zn6 O3I 92.1(5) . .
Dy3 O1 Dy1 110.2(4) . .
Dy3 O1 Dy7 102.9(3) . .
Dy1 O1 Dy7 98.7(4) . .
Dy3 O1 H1 114.5 . .
Dy1 O1 H1 114.5 . .
Dy7 O1 H1 114.5 . .
Dy1 O2 Dy8 107.5(4) . .
Dy1 O2 Dy3 106.0(4) . .
Dy8 O2 Dy3 95.6(3) . .
Dy1 O2 H2 115.2 . .
Dy8 O2 H2 115.2 . .
Dy3 O2 H2 115.2 . .
Dy1 O3 Dy7 101.5(3) . .
Dy1 O3 Dy8 106.9(4) . .
Dy7 O3 Dy8 108.8(4) . .
Dy1 O3 H3 113.0 . .
Dy7 O3 H3 113.0 . .
Dy8 O3 H3 113.0 . .
Dy2 O4 Dy4 108.9(4) . .
Dy2 O4 Dy9 102.0(4) . .
Dy4 O4 Dy9 99.0(4) . .
Dy2 O4 H4 115.0 . .
Dy4 O4 H4 115.0 . .
Dy9 O4 H4 115.0 . .
Dy4 O5 Dy10 109.0(4) . .
Dy4 O5 Dy2 106.2(4) . .
Dy10 O5 Dy2 95.5(4) . .
Dy4 O5 H5 114.7 . .
Dy10 O5 H5 114.7 . .
Dy2 O5 H5 114.7 . .
Dy9 O6 Dy2 104.8(4) . .
Dy9 O6 Dy10 113.0(4) . .
Dy2 O6 Dy10 97.6(4) . .
Dy9 O6 H6 113.4 . .
Dy2 O6 H6 113.4 . .
Dy10 O6 H6 113.4 . .
Zn6 O7 Dy10 100.7(4) . 2_656
Zn6 O7 Dy2 149.6(5) . .
Dy10 O7 Dy2 90.4(4) 2_656 .
Zn6 O7 H7 102.5 . .
Dy10 O7 H7 102.5 2_656 .
Dy2 O7 H7 102.5 . .
Dy4 O8 Dy5 107.0(4) . .
Dy4 O8 Dy3 106.7(4) . .
Dy5 O8 Dy3 96.8(3) . .
Dy3 O8 Dy51 88.7(9) . .
Dy4 O8 H8 115.0 . .
Dy5 O8 H8 114.5 . .
Dy3 O8 H8 115.0 . .
Dy51 O8 H8 120.0 . .
Dy4 O9 Dy3 110.1(4) . .
Dy4 O9 Dy6 98.7(3) . .
Dy3 O9 Dy6 103.0(4) . .
Dy4 O9 Dy61 111.0(12) . .
Dy3 O9 Dy61 98.4(7) . .
Dy4 O9 H9 114.3 . .
Dy3 O9 H9 114.5 . .
Dy6 O9 H9 114.6 . .
Dy61 O9 H9 107.4 . .
Dy51 O10 Dy6 114.6(7) . .
Dy51 O10 Dy3 102.2(8) . .
Dy6 O10 Dy3 106.1(4) . .
Dy51 O10 Dy61 127.5(14) . .
Dy3 O10 Dy61 102.7(7) . .
Dy6 O10 Dy5 111.8(4) . .
Dy3 O10 Dy5 97.6(3) . .
Dy61 O10 Dy5 124.9(13) . .
Dy51 O10 H10 107.0 . .
Dy6 O10 H10 113.4 . .
Dy3 O10 H10 113.2 . .
Dy61 O10 H10 104.4 . .
Dy5 O10 H10 113.5 . .
Zn1 O11 Dy51 96.6(7) . .
Zn1 O11 Dy5 100.2(4) . .
Zn1 O11 Dy3 149.6(5) . .
Dy51 O11 Dy3 90.0(6) . .
Dy5 O11 Dy3 90.8(3) . .
Zn1 O11 H11 102.6 . .
Dy51 O11 H11 110.9 . .
Dy5 O11 H11 102.0 . .
Dy3 O11 H11 102.6 . .
Dy7 O12 Dy3 106.1(3) . .
Dy7 O12 Dy8 112.9(4) . .
Dy3 O12 Dy8 98.2(4) . .
Dy7 O12 H12 112.8 . .
Dy3 O12 H12 112.8 . .
Dy8 O12 H12 112.8 . .
Zn3 O13 Dy8 101.3(4) . .
Zn31 O13 Dy8 96.5(5) . .
Zn3 O13 Dy3 146.8(6) . .
Dy8 O13 Dy3 92.0(3) . .
Zn3 O13 H13 101.8 . .
Zn31 O13 H13 123.1 . .
Dy8 O13 H13 104.1 . .
Dy3 O13 H13 104.2 . .
Dy61 O13 H13 80.5 . .
Dy4 O14 Dy6 101.0(4) . .
Dy4 O14 Dy5 106.6(4) . .
Dy6 O14 Dy5 110.3(4) . .
Dy4 O14 Dy51 112.3(8) . .
Dy6 O14 Dy51 101.5(11) . .
Dy4 O14 Dy61 100.3(6) . .
Dy5 O14 Dy61 106.2(6) . .
Dy51 O14 Dy61 97.5(12) . .
Dy4 O14 H14 112.7 . .
Dy6 O14 H14 112.8 . .
Dy5 O14 H14 112.7 . .
Dy51 O14 H14 115.1 . .
Dy61 O14 H14 117.1 . .
Dy4 O15 Dy9 101.6(4) . .
Dy4 O15 Dy10 106.9(4) . .
Dy9 O15 Dy10 109.3(4) . .
Dy4 O15 H15 112.8 . .
Dy9 O15 H15 112.8 . .
Dy10 O15 H15 112.8 . .
C2A O2A Zn5 126.0(10) . .
C2A O2A Dy7 125.7(9) . .
Zn5 O2A Dy7 106.7(4) . .
C2A C1A C6A 122.3(16) . .
C2A C1A C7A 122.2(14) . .
C6A C1A C7A 115.5(15) . .
O2A C2A C1A 123.7(15) . .
O2A C2A C3A 119.1(14) . .
C1A C2A C3A 117.1(14) . .
C4A C3A C2A 121.7(16) . .
C4A C3A H3A 119.2 . .
C2A C3A H3A 119.2 . .
C5A C4A C3A 119.6(18) . .
C5A C4A H4A 120.2 . .
C3A C4A H4A 120.2 . .
C4A C5A C6A 121.3(16) . .
C4A C5A H5A 119.3 . .
C6A C5A H5A 119.3 . .
C1A C6A C5A 117.9(16) . .
C1A C6A H6A 121.0 . .
C5A C6A H6A 121.0 . .
O1A C7A O3A 118.9(16) . .
O1A C7A C1A 119.4(15) . .
O3A C7A C1A 121.7(15) . .
C7A O1A Dy8 137.5(11) . 2_656
C7A O3A Dy7 133.3(11) . .
C7A O3A Dy1 138.2(10) . .
Dy7 O3A Dy1 88.2(3) . .
C2B O2B Zn2 127.3(9) . .
C2B O2B Dy6 123.7(9) . .
Zn2 O2B Dy6 106.8(4) . .
C2B O2B Dy61 119.2(11) . .
Zn2 O2B Dy61 106.6(7) . .
C2B C1B C6B 119.5(14) . .
C2B C1B C7B 124.1(16) . .
C6B C1B C7B 116.4(15) . .
O2B C2B C1B 119.8(14) . .
O2B C2B C3B 120.7(16) . .
C1B C2B C3B 119.3(17) . .
C4B C3B C2B 119.9(17) . .
C4B C3B H3B 120.1 . .
C2B C3B H3B 120.1 . .
C5B C4B C3B 122.0(15) . .
C5B C4B H4B 119.0 . .
C3B C4B H4B 119.0 . .
C4B C5B C6B 118.6(17) . .
C4B C5B H5B 120.7 . .
C6B C5B H5B 120.7 . .
C5B C6B C1B 120.6(16) . .
C5B C6B H6B 119.7 . .
C1B C6B H6B 119.7 . .
O3B C7B O1B 123.7(13) . .
O3B C7B C1B 119.1(15) . .
O1B C7B C1B 117.2(14) . .
C7B O1B Dy10 132.5(9) . .
C7B O3B Dy6 134.7(9) . .
C7B O3B Dy61 130.1(11) . .
C7B O3B Dy4 137.5(9) . .
Dy6 O3B Dy4 87.7(3) . .
Dy61 O3B Dy4 92.3(7) . .
C2C O2C Zn4 125.6(10) . .
C2C O2C Dy9 125.7(10) . .
Zn4 O2C Dy9 107.0(5) . .
C2C C1C C6C 120.3(17) . .
C2C C1C C7C 122.3(17) . .
C6C C1C C7C 117.3(17) . .
O2C C2C C1C 120.9(16) . .
O2C C2C C3C 120.3(17) . .
C1C C2C C3C 118.8(18) . .
C4C C3C C2C 120.5(19) . .
C4C C3C H3C 119.7 . .
C2C C3C H3C 119.7 . .
C5C C4C C3C 120.4(19) . .
C5C C4C H4C 119.8 . .
C3C C4C H4C 119.8 . .
C4C C5C C6C 120.6(19) . .
C4C C5C H5C 119.7 . .
C6C C5C H5C 119.7 . .
C1C C6C C5C 119.2(18) . .
C1C C6C H6C 120.4 . .
C5C C6C H6C 120.4 . .
O3C C7C O1C 121.6(16) . .
O3C C7C C1C 120.7(16) . .
O1C C7C C1C 117.4(18) . .
C7C O1C Dy5 133.6(12) . .
C7C O1C Dy51 137.1(12) . .
C7C O3C Dy9 133.6(11) . .
C7C O3C Dy4 137.8(10) . .
Dy9 O3C Dy4 87.9(4) . .
C2D O2D Zn2 128.0(16) . .
C2D C1D C6D 121(2) . .
C2D C1D C7D 124(2) . .
C6D C1D C7D 114(3) . .
O2D C2D C3D 118(3) . .
O2D C2D C1D 124(2) . .
C3D C2D C1D 117(3) . .
C2D C3D C4D 126(3) . .
C2D C3D H3D 116.9 . .
C4D C3D H3D 116.9 . .
C3D C4D C5D 115(3) . .
C3D C4D H4D 122.6 . .
C5D C4D H4D 122.6 . .
C4D C5D C6D 123(4) . .
C4D C5D H5D 118.5 . .
C6D C5D H5D 118.5 . .
C1D C6D C5D 116(3) . .
C1D C6D H6D 122.0 . .
C5D C6D H6D 122.0 . .
N1D C7D C1D 126(2) . .
N1D C7D H7D 116.8 . .
C1D C7D H7D 116.8 . .
C7D N1D C8D 119.7(19) . .
C7D N1D Zn2 123.1(17) . .
C8D N1D Zn2 117.1(11) . .
N1D C8D C9D 117(2) . .
N1D C8D C10D 110.6(17) . .
C9D C8D C10D 111(2) . .
N1D C8D C11D 104.0(16) . .
C9D C8D C11D 107.5(17) . .
C10D C8D C11D 106.1(17) . .
C8D C9D H9D1 109.5 . .
C8D C9D H9D2 109.5 . .
H9D1 C9D H9D2 109.5 . .
C8D C9D H9D3 109.5 . .
H9D1 C9D H9D3 109.5 . .
H9D2 C9D H9D3 109.5 . .
C8D C10D H10A 109.5 . .
C8D C10D H10B 109.5 . .
H10A C10D H10B 109.5 . .
C8D C10D H10C 109.5 . .
H10A C10D H10C 109.5 . .
H10B C10D H10C 109.5 . .
O1D C11D O3D 125.6(16) . .
O1D C11D C8D 117.2(17) . .
O3D C11D C8D 117.0(16) . .
C11D O1D Dy51 131.4(13) . .
C11D O1D Dy5 134.8(11) . .
C11D O3D Zn2 118.2(11) . .
C11D O3D Dy6 140.5(11) . .
Zn2 O3D Dy6 101.2(5) . .
C11D O3D Dy61 143.1(12) . .
Zn2 O3D Dy61 97.5(7) . .
C2E O2E Zn3 123.1(10) . .
C2E O2E Zn31 122.8(11) . .
C2E O2E Dy8 134.3(10) . .
Zn3 O2E Dy8 101.9(4) . .
Zn31 O2E Dy8 101.4(5) . .
C6E C1E C2E 118.6(17) . .
C6E C1E C7E 116.8(15) . .
C2E C1E C7E 124.6(15) . .
O2E C2E C1E 125.3(15) . .
O2E C2E C3E 117.4(14) . .
C1E C2E C3E 117.2(15) . .
C4E C3E C2E 123.4(16) . .
C4E C3E H3E 118.3 . .
C2E C3E H3E 118.3 . .
C3E C4E C5E 117.1(19) . .
C3E C4E H4E 121.5 . .
C5E C4E H4E 121.5 . .
C6E C5E C4E 120.1(19) . .
C6E C5E H5E 119.9 . .
C4E C5E H5E 119.9 . .
C5E C6E C1E 123.6(19) . .
C5E C6E H6E 118.2 . .
C1E C6E H6E 118.2 . .
N1E C7E C1E 127.9(14) . .
N1E C7E H7E 116.0 . .
C1E C7E H7E 116.0 . .
C7E N1E C8E 120.1(13) . .
C7E N1E Zn31 125.9(12) . .
C8E N1E Zn31 112.7(10) . .
C7E N1E Zn3 121.2(11) . .
C8E N1E Zn3 117.1(10) . .
N1E C8E C11E 110.0(13) . .
N1E C8E C10E 111.8(15) . .
C11E C8E C10E 109.9(16) . .
N1E C8E C9E 112.1(15) . .
C11E C8E C9E 104.7(15) . .
C10E C8E C9E 108.2(16) . .
C8E C9E H9E1 109.5 . .
C8E C9E H9E2 109.5 . .
H9E1 C9E H9E2 109.5 . .
C8E C9E H9E3 109.5 . .
H9E1 C9E H9E3 109.5 . .
H9E2 C9E H9E3 109.5 . .
C8E C10E H10D 109.5 . .
C8E C10E H10E 109.5 . .
H10D C10E H10E 109.5 . .
C8E C10E H10F 109.5 . .
H10D C10E H10F 109.5 . .
H10E C10E H10F 109.5 . .
O1E C11E O3E 123.5(14) . .
O1E C11E C8E 117.6(13) . .
O3E C11E C8E 118.8(15) . .
C11E O1E Zn2 129.7(10) . .
C11E O3E Dy61 141.9(13) . .
C11E O3E Zn3 114.5(10) . .
Dy61 O3E Zn3 98.1(11) . .
C11E O3E Zn31 109.0(10) . .
Dy61 O3E Zn31 108.5(10) . .
C11E O3E Dy6 136.0(10) . .
Zn3 O3E Dy6 106.3(4) . .
Zn31 O3E Dy6 115.0(6) . .
C2F O2F Zn1 123.9(12) . .
C2F O2F Dy51 134.2(12) . .
Zn1 O2F Dy51 98.4(8) . .
C2F O2F Dy5 132.8(11) . .
Zn1 O2F Dy5 102.4(5) . .
C6F C1F C2F 119(2) . .
C6F C1F C7F 115(2) . .
C2F C1F C7F 126(2) . .
O2F C2F C3F 118(2) . .
O2F C2F C1F 122.8(19) . .
C3F C2F C1F 119(2) . .
C4F C3F C2F 122(2) . .
C4F C3F H3F 118.9 . .
C2F C3F H3F 118.9 . .
C5F C4F C3F 119(2) . .
C5F C4F H4F 120.6 . .
C3F C4F H4F 120.6 . .
C4F C5F C6F 119(2) . .
C4F C5F H5F 120.4 . .
C6F C5F H5F 120.4 . .
C1F C6F C5F 121(3) . .
C1F C6F H6F 119.4 . .
C5F C6F H6F 119.4 . .
N1F C7F C1F 128(2) . .
N1F C7F H7F 116.2 . .
C1F C7F H7F 116.2 . .
C7F N1F C8F 118.9(17) . .
C7F N1F Zn1 124.5(14) . .
C8F N1F Zn1 116.5(12) . .
N1F C8F C9F 111.0(16) . .
N1F C8F C10F 109.9(15) . .
C9F C8F C10F 113.0(15) . .
N1F C8F C11F 108.7(13) . .
C9F C8F C11F 106.7(15) . .
C10F C8F C11F 107.3(15) . .
C8F C9F H9F1 109.5 . .
C8F C9F H9F2 109.5 . .
H9F1 C9F H9F2 109.5 . .
C8F C9F H9F3 109.5 . .
H9F1 C9F H9F3 109.5 . .
H9F2 C9F H9F3 109.5 . .
C8F C10F H10G 109.5 . .
C8F C10F H10H 109.5 . .
H10G C10F H10H 109.5 . .
C8F C10F H10I 109.5 . .
H10G C10F H10I 109.5 . .
H10H C10F H10I 109.5 . .
O1F C11F O3F 127.1(16) . .
O1F C11F C8F 113.7(14) . .
O3F C11F C8F 119.0(14) . .
C11F O1F Zn5 125.7(11) . .
C11F O3F Zn1 113.0(11) . .
C11F O3F Dy7 137.0(10) . .
Zn1 O3F Dy7 105.8(4) . .
C2G O2G Zn5 128.7(12) . .
C6G C1G C2G 119.8(19) . .
C6G C1G C7G 116.8(17) . .
C2G C1G C7G 123.3(16) . .
O2G C2G C3G 119.3(17) . .
O2G C2G C1G 122.2(17) . .
C3G C2G C1G 118.3(18) . .
C4G C3G C2G 122(2) . .
C4G C3G H3G 118.8 . .
C2G C3G H3G 118.8 . .
C3G C4G C5G 118(2) . .
C3G C4G H4G 121.2 . .
C5G C4G H4G 121.2 . .
C6G C5G C4G 121(2) . .
C6G C5G H5G 119.6 . .
C4G C5G H5G 119.6 . .
C1G C6G C5G 121(2) . .
C1G C6G H6G 119.7 . .
C5G C6G H6G 119.7 . .
N1G C7G C1G 126.9(16) . .
N1G C7G H7G 116.5 . .
C1G C7G H7G 116.5 . .
C7G N1G C8G 120.4(14) . .
C7G N1G Zn5 123.3(12) . .
C8G N1G Zn5 116.1(11) . .
N1G C8G C9G 113.0(17) . .
N1G C8G C11G 105.1(13) . .
C9G C8G C11G 111.1(16) . .
N1G C8G C10G 108.5(15) . .
C9G C8G C10G 112.3(17) . .
C11G C8G C10G 106.4(16) . .
C8G C9G H9G1 109.5 . .
C8G C9G H9G2 109.5 . .
H9G1 C9G H9G2 109.5 . .
C8G C9G H9G3 109.5 . .
H9G1 C9G H9G3 109.5 . .
H9G2 C9G H9G3 109.5 . .
C8G C10G H10J 109.5 . .
C8G C10G H10K 109.5 . .
H10J C10G H10K 109.5 . .
C8G C10G H10L 109.5 . .
H10J C10G H10L 109.5 . .
H10K C10G H10L 109.5 . .
O1G C11G O3G 123.7(15) . .
O1G C11G C8G 116.4(14) . .
O3G C11G C8G 119.8(16) . .
C11G O1G Dy8 134.6(9) . .
C11G O3G Zn5 116.5(11) . .
C11G O3G Dy7 141.9(11) . .
Zn5 O3G Dy7 101.4(4) . .
C2H O2H Zn4 124.9(12) . .
C6H C1H C2H 116.9(19) . .
C6H C1H C7H 119(2) . .
C2H C1H C7H 123.8(17) . .
O2H C2H C3H 118.2(17) . .
O2H C2H C1H 123.1(17) . .
C3H C2H C1H 118.7(17) . .
C4H C3H C2H 121.9(19) . .
C4H C3H H3H 119.0 . .
C2H C3H H3H 119.0 . .
C3H C4H C5H 121(2) . .
C3H C4H H4H 119.7 . .
C5H C4H H4H 119.7 . .
C6H C5H C4H 117(2) . .
C6H C5H H5H 121.4 . .
C4H C5H H5H 121.4 . .
C5H C6H C1H 125(2) . .
C5H C6H H6H 117.7 . .
C1H C6H H6H 117.7 . .
N1H C7H C1H 125(2) . .
N1H C7H H7H 117.4 . .
C1H C7H H7H 117.4 . .
C7H N1H C8H 119.4(17) . .
C7H N1H Zn4 122.0(15) . .
C8H N1H Zn4 117.9(12) . .
N1H C8H C11H 107.0(16) . .
N1H C8H C9H 111(2) . .
C11H C8H C9H 106.6(18) . .
N1H C8H C10H 111.8(18) . .
C11H C8H C10H 104.8(19) . .
C9H C8H C10H 115(2) . .
C8H C9H H9H1 109.5 . .
C8H C9H H9H2 109.5 . .
H9H1 C9H H9H2 109.5 . .
C8H C9H H9H3 109.5 . .
H9H1 C9H H9H3 109.5 . .
H9H2 C9H H9H3 109.5 . .
C8H C10H H10M 109.5 . .
C8H C10H H10N 109.5 . .
H10M C10H H10N 109.5 . .
C8H C10H H10O 109.5 . .
H10M C10H H10O 109.5 . .
H10N C10H H10O 109.5 . .
O1H C11H O3H 124.6(16) . .
O1H C11H C8H 118.4(17) . .
O3H C11H C8H 117.0(17) . .
C11H O1H Dy10 136.1(11) . .
C11H O3H Zn4 118.7(11) . .
C11H O3H Dy9 140.1(11) . .
Zn4 O3H Dy9 101.1(5) . .
C2I O2I Zn6 124.2(11) . .
C2I O2I Dy10 132.6(11) . 2_656
Zn6 O2I Dy10 101.9(4) . 2_656
C6I C1I C2I 119.5(17) . .
C6I C1I C7I 117.7(17) . .
C2I C1I C7I 122.8(16) . .
O2I C2I C3I 116.9(16) . .
O2I C2I C1I 124.1(15) . .
C3I C2I C1I 119.1(16) . .
C2I C3I C4I 119.7(18) . .
C2I C3I H3I 120.1 . .
C4I C3I H3I 120.1 . .
C3I C4I C5I 121.1(18) . .
C3I C4I H4I 119.5 . .
C5I C4I H4I 119.5 . .
C6I C5I C4I 118.0(17) . .
C6I C5I H5I 121.0 . .
C4I C5I H5I 121.0 . .
C1I C6I C5I 122.5(19) . .
C1I C6I H6I 118.8 . .
C5I C6I H6I 118.8 . .
N1I C7I C1I 131.1(18) . .
N1I C7I H7I 114.4 . .
C1I C7I H7I 114.4 . .
C7I N1I C8I 118.7(15) . .
C7I N1I Zn6 122.4(13) . .
C8I N1I Zn6 118.8(11) . .
N1I C8I C10I 110.6(15) . .
N1I C8I C9I 112.9(18) . .
C10I C8I C9I 111(2) . .
N1I C8I C11I 106.4(15) . .
C10I C8I C11I 109.0(17) . .
C9I C8I C11I 106.9(15) . .
C8I C9I H9I1 109.5 . .
C8I C9I H9I2 109.5 . .
H9I1 C9I H9I2 109.5 . .
C8I C9I H9I3 109.5 . .
H9I1 C9I H9I3 109.5 . .
H9I2 C9I H9I3 109.5 . .
C8I C10I H10P 109.5 . .
C8I C10I H10Q 109.5 . .
H10P C10I H10Q 109.5 . .
C8I C10I H10R 109.5 . .
H10P C10I H10R 109.5 . .
H10Q C10I H10R 109.5 . .
O1I C11I O3I 123.1(16) . .
O1I C11I C8I 114.9(16) . .
O3I C11I C8I 121.9(16) . .
C11I O1I Zn4 127.9(12) . .
C11I O3I Zn6 111.8(10) . .
C11I O3I Dy9 138.8(11) . .
Zn6 O3I Dy9 106.4(4) . .
C1K O1K Dy61 136.9(17) . .
C1K O1K Dy6 146.7(12) . .
C1K O2K Zn3 116.3(13) . .
O1K C1K O2K 127.4(18) . .
O1K C1K C2K 119.0(18) . .
O2K C1K C2K 113.5(19) . .
C1K C2K H2K1 109.5 . .
C1K C2K H2K2 109.5 . .
H2K1 C2K H2K2 109.5 . .
C1K C2K H2K3 109.5 . .
H2K1 C2K H2K3 109.5 . .
H2K2 C2K H2K3 109.5 . .
C3K O3K Dy7 143.0(11) . .
C3K O4K Zn1 118.9(11) . .
O3K C3K O4K 126.3(15) . .
O3K C3K C4K 118.5(17) . .
O4K C3K C4K 115.1(17) . .
C3K C4K H4K1 109.5 . .
C3K C4K H4K2 109.5 . .
H4K1 C4K H4K2 109.5 . .
C3K C4K H4K3 109.5 . .
H4K1 C4K H4K3 109.5 . .
H4K2 C4K H4K3 109.5 . .
C5K O5K Dy9 145.6(13) . .
C5K O6K Zn6 121.9(14) . .
O6K C5K O5K 122(2) . .
O6K C5K C6K 123(2) . .
O5K C5K C6K 115(2) . .
C5K C6K H6K1 109.5 . .
C5K C6K H6K2 109.5 . .
H6K1 C6K H6K2 109.5 . .
C5K C6K H6K3 109.5 . .
H6K1 C6K H6K3 109.5 . .
H6K2 C6K H6K3 109.5 . .
O1N N1N O2N 121.5(17) . .
O1N N1N O3N 118.5(18) . .
O2N N1N O3N 119.5(17) . .
O4N N2N O6N 125.0(19) . .
O4N N2N O5N 125.0(17) . .
O6N N2N O5N 109.7(19) . .
O6N N2N Zn31 109.6(14) . .
O5N N2N Zn31 126.2(12) . .
N2N O4N Zn31 126.4(16) . .
N2N O4N Zn3 131.1(14) . .
O2X N1 O2X 178(2) 2_656 .
O2X N1 O3X 122.8(17) 2_656 .
O2X N1 O3X 59.0(12) . .
O2X N1 O3X 59.0(12) 2_656 2_656
O2X N1 O3X 122.8(17) . 2_656
O3X N1 O3X 64(2) . 2_656
O2X N1 O1X 120.0(16) 2_656 .
O2X N1 O1X 58.2(12) . .
O3X N1 O1X 116.8(12) . .
O3X N1 O1X 177.5(13) 2_656 .
O2X N1 O1X 58.2(12) 2_656 2_656
O2X N1 O1X 120.1(16) . 2_656
O3X N1 O1X 177.5(13) . 2_656
O3X N1 O1X 116.8(12) 2_656 2_656
O1X N1 O1X 62.6(18) . 2_656
O2X O1X N1 56.7(13) . .
O2X O1X O1X 114.8(13) . 2_656
N1 O1X O1X 58.7(9) . 2_656
O2X O1X Dy3 81.2(12) . .
N1 O1X Dy3 137.9(12) . .
O1X O1X Dy3 161.9(8) 2_656 .
O2X O1X Dy1 166.5(15) . .
N1 O1X Dy1 134.7(12) . .
O1X O1X Dy1 76.0(4) 2_656 .
Dy3 O1X Dy1 87.0(6) . .
N1 O2X O3X 62.5(14) . .
N1 O2X O1X 65.2(14) . .
O3X O2X O1X 127(2) . .
N1 O2X Dy4 135.6(14) . .
O3X O2X Dy4 73.2(13) . .
O1X O2X Dy4 157.5(16) . .
N1 O2X Dy3 138.7(14) . .
O3X O2X Dy3 158.2(16) . .
O1X O2X Dy3 73.5(12) . .
Dy4 O2X Dy3 85.3(5) . .
O2X O3X N1 58.5(13) . .
O2X O3X O3X 116.5(13) . 2_656
N1 O3X O3X 58.0(10) . 2_656
O2X O3X Dy4 81.6(13) . .
N1 O3X Dy4 140.0(13) . .
O3X O3X Dy4 161.9(5) 2_656 .
O2X O3X Dy2 166.3(16) . .
N1 O3X Dy2 134.8(13) . .
O3X O3X Dy2 76.8(4) 2_656 .
Dy4 O3X Dy2 85.2(6) . .
O7N N3N O7N 125(3) 2_656 .
O7N N3N O8N 117.4(16) 2_656 .
O7N N3N O8N 117.4(16) . .
C1M O1M H1M 109.5 . .
O1M C1M H1M1 109.5 . .
O1M C1M H1M2 109.5 . .
H1M1 C1M H1M2 109.5 . .
O1M C1M H1M3 109.5 . .
H1M1 C1M H1M3 109.5 . .
H1M2 C1M H1M3 109.5 . .
C2M O2M H2M 109.5 . .
O2M C2M H2M1 109.5 . .
O2M C2M H2M2 109.5 . .
H2M1 C2M H2M2 109.5 . .
O2M C2M H2M3 109.5 . .
H2M1 C2M H2M3 109.5 . .
H2M2 C2M H2M3 109.5 . .
C3M O3M H3M 109.5 . .
O3M C3M H3M1 109.5 . .
O3M C3M H3M2 109.5 . .
H3M1 C3M H3M2 109.5 . .
O3M C3M H3M3 109.5 . .
H3M1 C3M H3M3 109.5 . .
H3M2 C3M H3M3 109.5 . .
C4M O4M H4M 109.5 . .
O4M C4M H4MA 109.5 . .
O4M C4M H4MB 109.5 . .
H4MA C4M H4MB 109.5 . .
O4M C4M H4MC 109.5 . .
H4MA C4M H4MC 109.5 . .
H4MB C4M H4MC 109.5 . .
C5M O5M H5M 109.5 . .
O5M C5M H5MA 109.5 . .
O5M C5M H5MB 109.5 . .
H5MA C5M H5MB 109.5 . .
O5M C5M H5MC 109.5 . .
H5MA C5M H5MC 109.5 . .
H5MB C5M H5MC 109.5 . .
C6M O6M H6M 109.5 . .
O6M C6M H6M1 109.5 . .
O6M C6M H6M2 109.5 . .
H6M1 C6M H6M2 109.5 . .
O6M C6M H6M3 109.5 . .
H6M1 C6M H6M3 109.5 . .
H6M2 C6M H6M3 109.5 . .
C8M O8M Dy5 127.1(16) . .
C8M O8M Dy51 133.0(17) . .
C8M O8M H8M 109.5 . .
Dy5 O8M H8M 102.9 . .
Dy51 O8M H8M 100.4 . .
O8M C8M H8M1 109.5 . .
O8M C8M H8M2 109.5 . .
H8M1 C8M H8M2 109.5 . .
O8M C8M H8M3 109.5 . .
H8M1 C8M H8M3 109.5 . .
H8M2 C8M H8M3 109.5 . .
C9M O9M Dy8 130(2) . .
C9M O9M H9MA 109.5 . .
Dy8 O9M H9MA 121.0 . .
O9M C9M H9M1 109.5 . .
O9M C9M H9M2 109.5 . .
H9M1 C9M H9M2 109.5 . .
O9M C9M H9M3 109.5 . .
H9M1 C9M H9M3 109.5 . .
H9M2 C9M H9M3 109.5 . .
C7M O7M Dy10 128.6(17) . .
C7M O7M H7M 109.5 . .
Dy10 O7M H7M 119.2 . .
O7M C7M H7M1 109.5 . .
O7M C7M H7M2 109.5 . .
H7M1 C7M H7M2 109.5 . .
O7M C7M H7M3 109.5 . .
H7M1 C7M H7M3 109.5 . .
H7M2 C7M H7M3 109.5 . .
C10M O10M H10S 109.5 . .
O10M C10M H10T 109.5 . .
O10M C10M H10U 109.5 . .
H10T C10M H10U 109.5 . .
O10M C10M H10V 109.5 . .
H10T C10M H10V 109.5 . .
H10U C10M H10V 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Dy1 O3 2.296(9) 2_656
Dy1 O3 2.296(9) .
Dy1 O1 2.327(10) 2_656
Dy1 O1 2.327(10) .
Dy1 O2 2.336(9) .
Dy1 O2 2.336(9) 2_656
Dy1 O3A 2.782(10) 2_656
Dy1 O3A 2.783(10) .
Dy1 O1X 2.79(2) 2_656
Dy1 O1X 2.79(2) .
Dy1 Dy7 3.595(2) .
Dy1 Dy7 3.595(2) 2_656
Dy2 O4 2.318(11) .
Dy2 O4 2.318(11) 2_656
Dy2 O6 2.334(10) 2_656
Dy2 O6 2.334(10) .
Dy2 O5 2.421(9) 2_656
Dy2 O5 2.421(9) .
Dy2 O7 2.516(10) .
Dy2 O7 2.516(10) 2_656
Dy2 O3X 2.88(2) 2_656
Dy2 O3X 2.88(2) .
Dy2 Dy10 3.520(2) .
Dy2 Dy10 3.520(2) 2_656
Dy3 O1 2.319(9) .
Dy3 O9 2.326(9) .
Dy3 O10 2.329(10) .
Dy3 O12 2.339(10) .
Dy3 O8 2.417(9) .
Dy3 O2 2.435(10) .
Dy3 O13 2.480(9) .
Dy3 O11 2.517(10) .
Dy3 O1X 2.740(18) .
Dy3 O2X 2.825(19) .
Dy3 Dy51 3.45(2) .
Dy3 Dy8 3.5430(15) .
Dy4 O14 2.291(10) .
Dy4 O15 2.306(10) .
Dy4 O5 2.311(10) .
Dy4 O9 2.323(9) .
Dy4 O8 2.329(9) .
Dy4 O4 2.336(9) .
Dy4 O3X 2.71(2) .
Dy4 O2X 2.799(19) .
Dy4 O3B 2.811(9) .
Dy4 O3C 2.820(11) .
Dy4 Dy6 3.586(3) .
Dy4 Dy9 3.6113(16) .
Dy5 O1C 2.270(13) .
Dy5 O8 2.335(10) .
Dy5 O2F 2.344(12) .
Dy5 O1D 2.359(11) .
Dy5 O14 2.384(10) .
Dy5 O10 2.394(11) .
Dy5 O8M 2.465(12) .
Dy5 O1W 2.465(12) .
Dy5 O11 2.474(11) .
Dy5 Zn1 3.431(4) .
Dy51 O10 2.10(4) .
Dy51 O1D 2.16(3) .
Dy51 O2F 2.23(2) .
Dy51 O11 2.36(2) .
Dy51 O14 2.43(2) .
Dy51 O8 2.52(3) .
Dy51 O1C 2.59(4) .
Dy51 O8M 2.75(4) .
Dy51 O1W 2.75(4) .
Dy51 Zn1 3.25(2) .
Dy51 Dy6 3.71(3) .
Dy51 H10 2.4896 .
Dy6 Dy61 0.53(5) .
Dy6 O2B 2.291(10) .
Dy6 O10 2.305(10) .
Dy6 O3B 2.342(11) .
Dy6 O14 2.358(11) .
Dy6 O1K 2.364(12) .
Dy6 O3D 2.385(12) .
Dy6 O9 2.403(9) .
Dy6 O3E 2.443(11) .
Dy6 Zn2 3.476(3) .
Dy61 O1K 2.04(4) .
Dy61 O3E 2.04(4) .
Dy61 O10 2.33(2) .
Dy61 O2B 2.41(3) .
Dy61 O9 2.48(3) .
Dy61 O3D 2.62(3) .
Dy61 O3B 2.68(4) .
Dy61 O14 2.84(5) .
Dy61 O13 2.88(4) .
Dy61 Zn3 3.16(5) .
Dy61 Zn31 3.41(5) .
Dy7 O2A 2.276(10) .
Dy7 O12 2.288(9) .
Dy7 O3K 2.347(11) .
Dy7 O3 2.347(10) .
Dy7 O3A 2.363(10) .
Dy7 O3G 2.398(10) .
Dy7 O1 2.410(10) .
Dy7 O3F 2.454(11) .
Dy7 Zn5 3.466(2) .
Dy7 Dy8 3.8622(18) .
Dy8 O1A 2.310(11) 2_656
Dy8 O2 2.345(9) .
Dy8 O12 2.347(10) .
Dy8 O1G 2.356(11) .
Dy8 O2E 2.376(10) .
Dy8 O3 2.404(8) .
Dy8 O13 2.444(11) .
Dy8 O9M 2.454(13) .
Dy8 O3W 2.454(13) .
Dy8 Zn3 3.425(3) .
Dy8 Zn31 3.515(13) .
Dy9 O2C 2.270(12) .
Dy9 O6 2.307(11) .
Dy9 O15 2.353(10) .
Dy9 O5K 2.359(11) .
Dy9 O3C 2.360(11) .
Dy9 O3H 2.385(11) .
Dy9 O4 2.414(10) .
Dy9 O3I 2.438(10) .
Dy9 Zn4 3.457(3) .
Dy9 Dy10 3.880(2) .
Dy10 O1B 2.270(10) .
Dy10 O1H 2.324(12) .
Dy10 O5 2.335(10) .
Dy10 O6 2.346(9) .
Dy10 O2I 2.346(12) 2_656
Dy10 O15 2.403(10) .
Dy10 O7 2.445(10) 2_656
Dy10 O7M 2.513(12) .
Dy10 O7W 2.513(12) .
Dy10 Zn6 3.415(3) 2_656
Zn1 O11 1.980(10) .
Zn1 N1F 2.009(15) .
Zn1 O2F 2.052(12) .
Zn1 O4K 2.056(11) .
Zn1 O3F 2.158(11) .
Zn2 O2D 1.933(14) .
Zn2 O1E 1.986(12) .
Zn2 N1D 2.028(15) .
Zn2 O2B 2.036(10) .
Zn2 O3D 2.107(11) .
Zn3 Zn31 0.838(18) .
Zn3 O13 1.966(10) .
Zn3 N1E 2.010(12) .
Zn3 O2E 2.024(12) .
Zn3 O3E 2.144(11) .
Zn3 O2K 2.193(15) .
Zn3 O4N 2.433(18) .
Zn31 O4N 1.64(3) .
Zn31 N1E 1.988(17) .
Zn31 O3E 2.160(17) .
Zn31 O2E 2.160(18) .
Zn31 O13 2.266(19) .
Zn31 N2N 2.50(3) .
Zn4 O2H 1.949(12) .
Zn4 O1I 2.006(11) .
Zn4 O2C 2.025(11) .
Zn4 N1H 2.029(15) .
Zn4 O3H 2.084(12) .
Zn5 O2G 1.937(13) .
Zn5 O1F 2.037(12) .
Zn5 O2A 2.040(9) .
Zn5 N1G 2.043(13) .
Zn5 O3G 2.073(11) .
Zn6 O7 1.972(11) .
Zn6 N1I 1.982(14) .
Zn6 O2I 2.047(11) .
Zn6 O6K 2.078(15) .
Zn6 O3I 2.157(10) .
Zn6 Dy10 3.415(3) 2_656
O1 H1 0.8600 .
O2 H2 0.8600 .
O3 H3 0.8600 .
O4 H4 0.8600 .
O5 H5 0.8600 .
O6 H6 0.8600 .
O7 Dy10 2.445(10) 2_656
O7 H7 0.8600 .
O8 H8 0.8601 .
O9 H9 0.8600 .
O10 H10 0.8600 .
O11 H11 0.8601 .
O12 H12 0.8600 .
O13 H13 0.8601 .
O14 H14 0.8599 .
O15 H15 0.8600 .
O2A C2A 1.345(17) .
C1A C2A 1.38(2) .
C1A C6A 1.39(2) .
C1A C7A 1.48(2) .
C2A C3A 1.43(2) .
C3A C4A 1.37(2) .
C3A H3A 0.9500 .
C4A C5A 1.35(2) .
C4A H4A 0.9500 .
C5A C6A 1.43(2) .
C5A H5A 0.9500 .
C6A H6A 0.9500 .
C7A O1A 1.264(18) .
C7A O3A 1.275(18) .
O1A Dy8 2.310(11) 2_656
O2B C2B 1.353(19) .
C1B C2B 1.39(2) .
C1B C6B 1.41(2) .
C1B C7B 1.496(19) .
C2B C3B 1.40(2) .
C3B C4B 1.38(2) .
C3B H3B 0.9500 .
C4B C5B 1.37(2) .
C4B H4B 0.9500 .
C5B C6B 1.39(2) .
C5B H5B 0.9500 .
C6B H6B 0.9500 .
C7B O3B 1.250(18) .
C7B O1B 1.271(18) .
O2C C2C 1.36(2) .
C1C C2C 1.38(2) .
C1C C6C 1.41(2) .
C1C C7C 1.50(2) .
C2C C3C 1.43(2) .
C3C C4C 1.38(2) .
C3C H3C 0.9500 .
C4C C5C 1.36(3) .
C4C H4C 0.9500 .
C5C C6C 1.41(2) .
C5C H5C 0.9500 .
C6C H6C 0.9500 .
C7C O3C 1.24(2) .
C7C O1C 1.281(19) .
O2D C2D 1.27(3) .
C1D C2D 1.42(3) .
C1D C6D 1.42(3) .
C1D C7D 1.44(3) .
C2D C3D 1.32(3) .
C3D C4D 1.40(3) .
C3D H3D 0.9500 .
C4D C5D 1.39(4) .
C4D H4D 0.9500 .
C5D C6D 1.42(4) .
C5D H5D 0.9500 .
C6D H6D 0.9500 .
C7D N1D 1.27(2) .
C7D H7D 0.9500 .
N1D C8D 1.50(2) .
C8D C9D 1.53(3) .
C8D C10D 1.53(3) .
C8D C11D 1.56(3) .
C9D H9D1 0.9800 .
C9D H9D2 0.9800 .
C9D H9D3 0.9800 .
C10D H10A 0.9800 .
C10D H10B 0.9800 .
C10D H10C 0.9800 .
C11D O1D 1.238(19) .
C11D O3D 1.26(2) .
O2E C2E 1.303(17) .
C1E C6E 1.39(2) .
C1E C2E 1.41(2) .
C1E C7E 1.45(2) .
C2E C3E 1.42(2) .
C3E C4E 1.39(2) .
C3E H3E 0.9500 .
C4E C5E 1.41(2) .
C4E H4E 0.9500 .
C5E C6E 1.35(3) .
C5E H5E 0.9500 .
C6E H6E 0.9500 .
C7E N1E 1.27(2) .
C7E H7E 0.9500 .
N1E C8E 1.48(2) .
C8E C11E 1.51(2) .
C8E C10E 1.53(2) .
C8E C9E 1.56(2) .
C9E H9E1 0.9800 .
C9E H9E2 0.9800 .
C9E H9E3 0.9800 .
C10E H10D 0.9800 .
C10E H10E 0.9800 .
C10E H10F 0.9800 .
C11E O1E 1.253(19) .
C11E O3E 1.300(16) .
O2F C2F 1.33(2) .
C1F C6F 1.36(3) .
C1F C2F 1.41(3) .
C1F C7F 1.46(3) .
C2F C3F 1.40(3) .
C3F C4F 1.39(3) .
C3F H3F 0.9500 .
C4F C5F 1.38(3) .
C4F H4F 0.9500 .
C5F C6F 1.45(3) .
C5F H5F 0.9500 .
C6F H6F 0.9500 .
C7F N1F 1.25(2) .
C7F H7F 0.9500 .
N1F C8F 1.47(2) .
C8F C9F 1.53(2) .
C8F C10F 1.54(2) .
C8F C11F 1.58(2) .
C9F H9F1 0.9800 .
C9F H9F2 0.9800 .
C9F H9F3 0.9800 .
C10F H10G 0.9800 .
C10F H10H 0.9800 .
C10F H10I 0.9800 .
C11F O1F 1.241(18) .
C11F O3F 1.252(18) .
O2G C2G 1.30(2) .
C1G C6G 1.35(3) .
C1G C2G 1.42(2) .
C1G C7G 1.47(2) .
C2G C3G 1.38(2) .
C3G C4G 1.37(3) .
C3G H3G 0.9500 .
C4G C5G 1.40(3) .
C4G H4G 0.9500 .
C5G C6G 1.39(3) .
C5G H5G 0.9500 .
C6G H6G 0.9500 .
C7G N1G 1.27(2) .
C7G H7G 0.9500 .
N1G C8G 1.49(2) .
C8G C9G 1.50(3) .
C8G C11G 1.51(2) .
C8G C10G 1.52(3) .
C9G H9G1 0.9800 .
C9G H9G2 0.9800 .
C9G H9G3 0.9800 .
C10G H10J 0.9800 .
C10G H10K 0.9800 .
C10G H10L 0.9800 .
C11G O1G 1.258(19) .
C11G O3G 1.270(18) .
O2H C2H 1.32(2) .
C1H C6H 1.41(3) .
C1H C2H 1.42(3) .
C1H C7H 1.44(3) .
C2H C3H 1.38(2) .
C3H C4H 1.37(2) .
C3H H3H 0.9500 .
C4H C5H 1.40(3) .
C4H H4H 0.9500 .
C5H C6H 1.34(3) .
C5H H5H 0.9500 .
C6H H6H 0.9500 .
C7H N1H 1.27(2) .
C7H H7H 0.9500 .
N1H C8H 1.49(2) .
C8H C11H 1.53(2) .
C8H C9H 1.53(3) .
C8H C10H 1.56(3) .
C9H H9H1 0.9800 .
C9H H9H2 0.9800 .
C9H H9H3 0.9800 .
C10H H10M 0.9800 .
C10H H10N 0.9800 .
C10H H10O 0.9800 .
C11H O1H 1.24(2) .
C11H O3H 1.28(2) .
O2I C2I 1.348(19) .
O2I Dy10 2.345(12) 2_656
C1I C6I 1.35(2) .
C1I C2I 1.43(2) .
C1I C7I 1.45(2) .
C2I C3I 1.38(2) .
C3I C4I 1.39(2) .
C3I H3I 0.9500 .
C4I C5I 1.39(3) .
C4I H4I 0.9500 .
C5I C6I 1.38(2) .
C5I H5I 0.9500 .
C6I H6I 0.9500 .
C7I N1I 1.28(2) .
C7I H7I 0.9500 .
N1I C8I 1.47(2) .
C8I C10I 1.47(3) .
C8I C9I 1.47(3) .
C8I C11I 1.55(2) .
C9I H9I1 0.9800 .
C9I H9I2 0.9800 .
C9I H9I3 0.9800 .
C10I H10P 0.9800 .
C10I H10Q 0.9800 .
C10I H10R 0.9800 .
C11I O1I 1.273(19) .
C11I O3I 1.273(19) .
O1K C1K 1.22(2) .
O2K C1K 1.26(2) .
C1K C2K 1.55(3) .
C2K H2K1 0.9800 .
C2K H2K2 0.9800 .
C2K H2K3 0.9800 .
O3K C3K 1.23(2) .
O4K C3K 1.28(2) .
C3K C4K 1.51(2) .
C4K H4K1 0.9800 .
C4K H4K2 0.9800 .
C4K H4K3 0.9800 .
O5K C5K 1.32(2) .
O6K C5K 1.27(3) .
C5K C6K 1.42(3) .
C6K H6K1 0.9800 .
C6K H6K2 0.9800 .
C6K H6K3 0.9800 .
N1N O1N 1.261(19) .
N1N O2N 1.264(19) .
N1N O3N 1.268(19) .
N2N O4N 1.151(19) .
N2N O6N 1.25(2) .
N2N O5N 1.35(2) .
N1 O2X 1.200(18) 2_656
N1 O2X 1.200(18) .
N1 O3X 1.25(2) .
N1 O3X 1.25(2) 2_656
N1 O1X 1.30(2) .
N1 O1X 1.30(2) 2_656
O1X O2X 1.22(2) .
O1X O1X 1.35(4) 2_656
O2X O3X 1.21(2) .
O3X O3X 1.32(4) 2_656
N3N O7N 1.245(18) 2_656
N3N O7N 1.245(18) .
N3N O8N 1.33(5) .
O1M C1M 1.39(2) .
O1M H1M 0.8400 .
C1M H1M1 1.04(11) .
C1M H1M2 1.04(11) .
C1M H1M3 1.04(11) .
O2M C2M 1.57(4) .
O2M H2M 0.8400 .
C2M H2M1 0.9800 .
C2M H2M2 0.9800 .
C2M H2M3 0.9800 .
O3M C3M 1.46(2) .
O3M H3M 0.8400 .
C3M H3M1 0.9800 .
C3M H3M2 0.9800 .
C3M H3M3 0.9800 .
O4M C4M 1.46(3) .
O4M H4M 0.8400 .
C4M H4MA 0.9800 .
C4M H4MB 0.9800 .
C4M H4MC 0.9800 .
O5M C5M 1.46(4) .
O5M H5M 0.8400 .
C5M H5MA 0.9800 .
C5M H5MB 0.9800 .
C5M H5MC 0.9800 .
O6M C6M 1.392(19) .
O6M H6M 0.8400 .
C6M H6M1 0.9800 .
C6M H6M2 0.9800 .
C6M H6M3 0.9800 .
O8M C8M 1.49(4) .
O8M H8M 0.8400 .
C8M H8M1 0.9800 .
C8M H8M2 0.9800 .
C8M H8M3 0.9800 .
O9M C9M 1.33(5) .
O9M H9MA 0.8400 .
C9M H9M1 0.9800 .
C9M H9M2 0.9800 .
C9M H9M3 0.9800 .
O7M C7M 1.39(4) .
O7M H7M 0.8400 .
C7M H7M1 0.9800 .
C7M H7M2 0.9800 .
C7M H7M3 0.9800 .
O10M C10M 1.41(4) .
O10M H10S 0.8400 .
C10M H10T 0.9800 .
C10M H10U 0.9800 .
C10M H10V 0.9800 .
