#------------------------------------------------------------------------------
#$Date: 2017-07-06 04:14:48 +0300 (Thu, 06 Jul 2017) $
#$Revision: 198494 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/12/03/7120385.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7120385
loop_
_publ_author_name
'Cronin, Lee'
'Zang, Hong-Ying'
'Purcell, Jamie'
'Long, Deliang'
'Miras, Haralampos N.'
_publ_section_title
;
 Exploring Structural Complexity in the Discovery and Self-Assembly of a
 Family of Nanoscale Chalcoxides from {Se8Mo36} to {Se26Mo68}
;
_journal_name_full               'Chem. Commun.'
_journal_paper_doi               10.1039/C7CC04398H
_journal_year                    2017
_chemical_formula_sum            'C48 H276 K30 Mo68 N4 Na2 O310 S68 Se26'
_chemical_formula_weight         17846.65
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2017-03-28 deposited with the CCDC.
2017-07-05 downloaded from the CCDC.
;
_cell_angle_alpha                102.220(2)
_cell_angle_beta                 100.029(2)
_cell_angle_gamma                95.818(2)
_cell_formula_units_Z            1
_cell_length_a                   20.3775(7)
_cell_length_b                   21.0899(7)
_cell_length_c                   30.3195(12)
_cell_measurement_reflns_used    9929
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      21.1
_cell_measurement_theta_min      2.22
_cell_volume                     12410.2(8)
_computing_cell_refinement       Apex2
_computing_data_collection       Apex2
_computing_data_reduction        Apex2
_computing_molecular_graphics    Diamond3
_computing_publication_material  WinGX
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_structure_solution    'SHELXL-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker Apex II Quasar'
_diffrn_measurement_method       'ω & φ scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1076
_diffrn_reflns_av_unetI/netI     0.1103
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       32
_diffrn_reflns_limit_l_min       -32
_diffrn_reflns_number            129811
_diffrn_reflns_point_group_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_theta_full        22.710
_diffrn_reflns_theta_max         22.710
_diffrn_reflns_theta_min         1.077
_diffrn_source                   '1uS Microfocus x-ray'
_exptl_absorpt_coefficient_mu    4.187
_exptl_absorpt_correction_T_max  0.745
_exptl_absorpt_correction_T_min  0.644
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    2.388
_exptl_crystal_density_method    none
_exptl_crystal_description       block
_exptl_crystal_F_000             8492
_exptl_crystal_size_max          0.100
_exptl_crystal_size_mid          0.080
_exptl_crystal_size_min          0.040
_refine_diff_density_max         1.66
_refine_diff_density_min         -0.96
_refine_diff_density_rms         0.24
_refine_ls_extinction_coef       0.000116(14)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2014/7 (Sheldrick 2014'
_refine_ls_goodness_of_fit_ref   1.029
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2536
_refine_ls_number_reflns         33181
_refine_ls_number_restraints     12
_refine_ls_restrained_S_all      1.029
_refine_ls_R_factor_all          0.1331
_refine_ls_R_factor_gt           0.0660
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0841P)²+318.5470P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1640
_refine_ls_wR_factor_ref         0.2122
_reflns_Friedel_coverage         0.000
_reflns_number_gt                19372
_reflns_number_total             33181
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c7cc04398h2.cif
_cod_data_source_block           hz4311
_cod_depositor_comments
;
The following automatic conversions were performed:

'_atom_sites_solution_primary' value 'direct methods' was changed to
'direct'.

Automatic conversion script
Id: cif_fix_values 4973 2017-02-22 13:04:09Z antanas 
;
_cod_database_code               7120385
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.680
_shelx_estimated_absorpt_t_max   0.850
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Mo1 Mo 0.88665(8) 0.86839(8) 0.18238(6) 0.0253(4) Uani 1 1 d . . . .
Mo2 Mo 0.70410(8) 0.99904(8) 0.31954(6) 0.0285(4) Uani 1 1 d . . . .
Mo3 Mo 0.99397(9) 0.70721(9) 0.30936(6) 0.0323(4) Uani 1 1 d . . . .
Mo4 Mo 0.49960(9) 1.12150(9) 0.22790(7) 0.0380(5) Uani 1 1 d . . . .
Mo5 Mo 0.60244(9) 0.64180(9) 0.19468(6) 0.0353(5) Uani 1 1 d . . . .
Mo6 Mo 0.99978(9) 1.09525(9) 0.09012(6) 0.0323(4) Uani 1 1 d . . . .
Mo7 Mo 0.62146(9) 1.09657(9) 0.30507(6) 0.0325(4) Uani 1 1 d . . . .
Mo8 Mo 1.17256(9) 0.91885(9) 0.14647(6) 0.0295(4) Uani 1 1 d . . . .
Mo9 Mo 0.67379(9) 0.70779(9) 0.28413(6) 0.0322(4) Uani 1 1 d . . . .
Mo10 Mo 1.18154(9) 1.05488(9) 0.43762(6) 0.0344(5) Uani 1 1 d . . . .
Mo11 Mo 0.42165(9) 0.90729(10) 0.07016(7) 0.0405(5) Uani 1 1 d . . . .
Mo12 Mo 1.06580(9) 0.59825(9) 0.30239(7) 0.0409(5) Uani 1 1 d . . . .
Mo13 Mo 0.80970(8) 0.79462(8) 0.09674(6) 0.0270(4) Uani 1 1 d . . . .
Mo14 Mo 1.09889(9) 1.00905(9) 0.08310(6) 0.0321(4) Uani 1 1 d . . . .
Mo15 Mo 1.16519(8) 0.88832(8) 0.23300(6) 0.0276(4) Uani 1 1 d . . . .
Mo16 Mo 1.34738(9) 1.23044(10) 0.34274(6) 0.0387(5) Uani 1 1 d . . . .
Mo17 Mo 1.36594(9) 1.11123(10) 0.36971(6) 0.0373(5) Uani 1 1 d . . . .
Mo18 Mo 0.98669(10) 0.38725(9) 0.14510(8) 0.0465(5) Uani 1 1 d . . . .
Mo19 Mo 1.06603(10) 0.45831(10) 0.23215(8) 0.0465(5) Uani 1 1 d . . . .
Mo20 Mo 0.82366(9) 0.59496(9) 0.40388(6) 0.0366(5) Uani 1 1 d . . . .
Mo21 Mo 0.71535(11) 0.49078(10) 0.38410(7) 0.0483(6) Uani 1 1 d . . . .
Mo22 Mo 0.55180(12) 0.47175(11) 0.37247(8) 0.0632(7) Uani 1 1 d . . . .
Mo23 Mo 0.45127(11) 0.55708(12) 0.37654(8) 0.0628(7) Uani 1 1 d . . . .
Mo24 Mo 0.44993(10) 0.71575(12) 0.39555(7) 0.0542(6) Uani 1 1 d . . . .
Mo25 Mo 0.54497(9) 0.83263(11) 0.41793(7) 0.0426(5) Uani 1 1 d . . . .
Mo26 Mo 0.42464(9) 1.04920(10) 0.13999(7) 0.0417(5) Uani 1 1 d . . . .
Mo27 Mo 0.48839(9) 0.79544(9) 0.06337(7) 0.0391(5) Uani 1 1 d . . . .
Mo28 Mo 0.77642(10) 0.50291(10) 0.05476(8) 0.0467(5) Uani 1 1 d . . . .
Mo29 Mo 0.86045(11) 0.40712(10) 0.06947(7) 0.0464(5) Uani 1 1 d . . . .
Mo30 Mo 0.89030(8) 1.12853(8) 0.25207(6) 0.0283(4) Uani 1 1 d . . . .
Mo31 Mo 0.90866(9) 1.14818(8) 0.16500(6) 0.0306(4) Uani 1 1 d . . . .
Mo32 Mo 1.08752(9) 1.13813(9) 0.44314(6) 0.0334(5) Uani 1 1 d . . . .
Mo33 Mo 1.11536(9) 1.33002(9) 0.38467(6) 0.0355(5) Uani 1 1 d . . . .
Mo34 Mo 1.23555(9) 1.32749(9) 0.34960(6) 0.0377(5) Uani 1 1 d . . . .
Se1 Se 0.83263(10) 0.67553(9) 0.31877(7) 0.0300(5) Uani 1 1 d . . . .
Se2 Se 0.67120(14) 0.53106(12) 0.12787(9) 0.0559(7) Uani 1 1 d . . . .
Se3 Se 0.63051(10) 0.85434(10) 0.33423(7) 0.0298(5) Uani 1 1 d . . . .
Se4 Se 0.46773(11) 0.70200(12) 0.13958(8) 0.0474(6) Uani 1 1 d . . . .
Se5 Se 1.01657(9) 0.80445(9) 0.23614(7) 0.0281(5) Uani 1 1 d . . . .
Se6 Se 0.81183(9) 0.97804(9) 0.24862(7) 0.0261(5) Uani 1 1 d . . . .
Se7 Se 0.85251(11) 0.64737(11) 0.04210(8) 0.0396(6) Uani 1 1 d . . . .
Se8 Se 0.65297(10) 0.82406(10) 0.05905(8) 0.0364(5) Uani 1 1 d . . . .
Se9' Se 1.1946(2) 1.1703(2) 0.37126(16) 0.0427(11) Uani 0.5 1 d . P A 2
Se9 Se 1.23284(18) 1.20590(19) 0.41714(13) 0.0256(9) Uani 0.5 1 d . P B 1
Se10 Se 1.22424(10) 1.00325(10) 0.33619(7) 0.0323(5) Uani 1 1 d . . . .
Se11 Se 1.34359(10) 1.11765(12) 0.47772(7) 0.0399(6) Uani 1 1 d . . . .
Se12 Se 1.13449(10) 1.29867(10) 0.49030(7) 0.0351(5) Uani 1 1 d . . . .
Se13 Se 1.01585(10) 1.18339(10) 0.34848(7) 0.0327(5) Uani 1 1 d . . . .
S1 S 0.7482(3) 0.5519(3) 0.3344(2) 0.0440(15) Uani 1 1 d . . . .
S2 S 0.5313(3) 1.1089(3) 0.15736(19) 0.0435(14) Uani 1 1 d . . . .
S3 S 0.5166(3) 0.5265(3) 0.4369(2) 0.0629(19) Uani 1 1 d . . . .
S4 S 0.5020(3) 0.5202(3) 0.3157(2) 0.065(2) Uani 1 1 d . . . .
S5 S 0.5078(3) 0.7740(4) 0.4680(2) 0.0574(18) Uani 1 1 d . . . .
S6 S 1.1882(3) 1.1488(3) 0.4929(2) 0.0530(16) Uani 1 1 d . . . .
S7 S 0.7163(3) 0.6445(3) 0.22562(19) 0.0371(13) Uani 1 1 d . . . .
S8 S 0.7712(2) 0.8624(2) 0.15504(17) 0.0291(12) Uani 1 1 d . . . .
S9 S 0.9725(2) 1.2016(2) 0.23740(18) 0.0318(12) Uani 1 1 d . . . .
S10 S 0.9607(3) 0.6039(3) 0.3213(2) 0.0380(14) Uani 1 1 d . . . .
S11 S 0.5745(3) 0.7317(3) 0.24328(19) 0.0373(13) Uani 1 1 d . . . .
S12 S 0.7102(2) 1.0706(3) 0.27110(18) 0.0325(12) Uani 1 1 d . . . .
S13 S 1.1146(3) 1.1194(2) 0.11942(18) 0.0331(12) Uani 1 1 d . . . .
S14 S 0.4008(3) 0.8185(3) 0.1022(2) 0.0459(15) Uani 1 1 d . . . .
S15 S 0.5256(3) 0.8969(3) 0.0517(2) 0.0430(14) Uani 1 1 d . . . .
S16 S 1.3017(3) 1.1245(3) 0.30278(18) 0.0415(14) Uani 1 1 d . . . .
S17 S 0.5969(3) 1.0065(3) 0.33586(18) 0.0353(13) Uani 1 1 d . . . .
S18 S 1.2300(2) 0.9769(3) 0.21931(18) 0.0341(13) Uani 1 1 d . . . .
S19 S 0.8461(3) 1.0601(2) 0.18018(18) 0.0329(12) Uani 1 1 d . . . .
S20 S 0.7644(3) 0.4265(3) 0.0987(2) 0.0509(16) Uani 1 1 d . . . .
S21 S 0.4038(3) 1.0435(3) 0.2122(2) 0.0449(15) Uani 1 1 d . . . .
S22 S 1.0910(2) 0.8480(2) 0.16290(17) 0.0294(12) Uani 1 1 d . . . .
S23 S 1.1285(3) 1.2748(3) 0.31311(19) 0.0397(14) Uani 1 1 d . . . .
S24 S 0.9831(3) 0.9825(2) 0.06794(17) 0.0332(13) Uani 1 1 d . . . .
S25 S 0.9124(2) 0.7746(2) 0.13499(17) 0.0303(12) Uani 1 1 d . . . .
S26 S 1.0822(3) 0.6880(3) 0.2708(2) 0.0433(15) Uani 1 1 d . . . .
S27 S 0.8867(3) 0.5010(3) 0.0448(2) 0.0515(16) Uani 1 1 d . . . .
S28 S 1.3962(3) 1.2168(3) 0.41447(19) 0.0456(15) Uani 1 1 d . . . .
S29 S 0.7718(3) 0.5523(3) 0.4560(2) 0.0465(15) Uani 1 1 d . . . .
S30 S 0.9632(3) 0.3922(3) 0.2179(2) 0.0515(16) Uani 1 1 d . . . .
S31 S 1.0936(3) 1.0577(3) 0.3808(2) 0.0541(17) Uani 1 1 d . . . .
S32 S 1.2249(3) 1.3656(3) 0.4252(2) 0.0484(15) Uani 1 1 d . . . .
S33 S 1.0759(3) 0.4714(3) 0.1588(2) 0.0539(17) Uani 1 1 d . . . .
S34 S 0.5096(3) 0.7582(3) 0.34714(19) 0.0467(15) Uani 1 1 d . . . .
K1 K 0.8871(3) 0.8563(2) -0.00998(17) 0.0476(13) Uani 1 1 d . . . .
K2 K 0.9818(3) 0.9448(3) 0.3173(2) 0.0704(18) Uani 1 1 d . . . .
K3 K 0.3752(3) 0.3822(3) 0.2978(3) 0.085(2) Uani 1 1 d . . . .
K4 K 0.8494(5) 1.1176(4) 0.0064(3) 0.052(3) Uani 0.55 1 d . P C 1
K4' K 0.9310(17) 1.2445(15) 0.0607(11) 0.067(8) Uiso 0.2 1 d . P C 2
K5 K 0.7906(3) 0.8311(4) 0.3993(2) 0.089(2) Uani 1 1 d . . . .
K6 K 0.8925(12) 0.4393(11) 0.4419(8) 0.087(7) Uani 0.3 1 d . P . .
K7 K 0.8479(5) 1.2999(5) 0.2491(4) 0.047(3) Uani 0.5 1 d . P G .
K8 K 0.2947(5) 0.7515(6) -0.0110(4) 0.059(3) Uani 0.5 1 d . P D .
K9' K 0.5642(10) 0.6243(9) 0.0543(6) 0.044(5) Uiso 0.3 1 d . P D 2
K9 K 0.6602(5) 0.6401(5) 0.0286(5) 0.091(4) Uani 0.6 1 d . P D 1
K9" K 0.536(2) 0.6019(19) 0.0506(12) 0.008(8) Uiso 0.1 1 d . P D 3
K10 K 1.5498(5) 1.2522(5) 0.3424(4) 0.084(4) Uani 0.6 1 d . P E 1
K11 K 0.9787(7) 1.3379(7) 0.5617(4) 0.079(4) Uani 0.5 1 d . P G .
K12' K 1.265(2) 0.9152(19) 0.4645(14) 0.067(11) Uiso 0.15 1 d . P F 2
K12 K 1.3456(6) 0.9413(6) 0.4229(4) 0.062(4) Uani 0.45 1 d . P F 1
K13 K 1.0331(9) 0.9899(9) 0.4991(6) 0.071(5) Uiso 0.35 1 d . P F .
K14 K 0.4613(10) 0.6335(10) 0.5132(6) 0.081(6) Uani 0.35 1 d . P . .
K15 K 0.5710(12) 1.1789(12) 0.0655(8) 0.067(7) Uiso 0.25 1 d . P . .
K16 K 1.1847(8) 1.1744(8) 0.2347(6) 0.061(4) Uani 0.35 1 d . P E .
K17 K 0.356(2) 0.529(2) 0.1168(16) 0.079(13) Uiso 0.15 1 d . P . .
K18 K 1.1829(10) 1.2873(10) 0.1360(7) 0.070(6) Uani 0.3 1 d . P E .
K19' K 0.832(2) 1.174(2) 0.3761(15) 0.044(13) Uiso 0.15 1 d . P G 2
K19 K 0.8109(8) 1.1892(8) 0.3627(6) 0.056(4) Uani 0.4 1 d . P G 1
K20 K 0.9576(10) 0.4534(8) 0.3401(7) 0.060(5) Uani 0.3 1 d . P . .
K21 K 1.0410(10) 0.4488(9) 0.0349(7) 0.065(6) Uani 0.3 1 d . P D .
K22 K 0.6405(9) 0.4832(10) 0.5070(6) 0.079(6) Uani 0.35 1 d . P . .
K23 K 0.8067(9) 0.9816(7) 0.0719(6) 0.072(5) Uani 0.35 1 d . P C 1
K24 K 0.6172(12) 0.4761(10) 0.2499(7) 0.075(6) Uani 0.3 1 d . P D 1
K24' K 0.697(3) 0.424(3) 0.206(2) 0.068(16) Uiso 0.1 1 d . P D 2
K25 K 1.218(3) 0.616(2) 0.2147(17) 0.078(14) Uiso 0.15 1 d . P H 1
K25' K 1.253(3) 0.630(3) 0.2245(19) 0.044(14) Uiso 0.1 1 d . P H 2
K26 K 0.8306(17) 0.4207(16) -0.0642(12) 0.079(9) Uiso 0.2 1 d . P D .
K27 K 0.4413(8) 0.6320(10) 0.2584(6) 0.059(5) Uani 0.3 1 d . P D .
Na1 Na 1.1936(6) 1.5088(5) 0.3524(4) 0.060(4) Uani 0.8 1 d . P I 1
Na1' Na 1.230(2) 1.524(2) 0.3245(16) 0.047(11) Uiso 0.2 1 d . P I 2
O1 O 1.0350(7) 0.7463(7) 0.3622(5) 0.044(4) Uani 1 1 d . . . .
O2 O 0.9189(6) 0.6686(6) 0.2326(5) 0.033(3) Uani 1 1 d . . . .
O3 O 1.0040(7) 0.5468(6) 0.2317(5) 0.042(4) Uani 1 1 d . . . .
O4 O 1.1291(7) 0.5502(6) 0.2624(5) 0.047(4) Uani 1 1 d . . . .
O5 O 1.1190(7) 0.6215(8) 0.3542(6) 0.059(5) Uani 1 1 d . . . .
O6 O 1.0515(7) 0.4972(7) 0.2994(5) 0.050(4) Uani 1 1 d . . . .
O7 O 1.1215(8) 0.4080(7) 0.2417(6) 0.063(5) Uani 1 1 d . . . .
O8 O 1.0241(8) 0.3203(7) 0.1355(6) 0.061(5) Uani 1 1 d . . . .
O9 O 0.9621(8) 0.3944(7) 0.0754(5) 0.054(4) Uani 1 1 d . . . .
O10 O 0.8839(8) 0.3460(6) 0.1165(5) 0.048(4) Uani 1 1 d . . . .
O11 O 0.9182(7) 0.4683(6) 0.1394(5) 0.045(4) Uani 1 1 d . . . .
O12 O 0.8294(8) 0.3502(7) 0.0217(6) 0.061(5) Uani 1 1 d . . . .
O13 O 0.7342(8) 0.4616(8) 0.0017(5) 0.061(5) Uani 1 1 d . . . .
O14 O 0.8274(7) 0.5843(7) 0.1306(5) 0.044(4) Uani 1 1 d . . . .
O15 O 0.7836(7) 0.5949(7) 0.0419(5) 0.049(4) Uani 1 1 d . . . .
O16 O 0.6967(7) 0.5424(7) 0.0793(5) 0.048(4) Uani 1 1 d . . . .
O17 O 0.6226(7) 0.5929(7) 0.1328(5) 0.047(4) Uani 1 1 d . . . .
O18 O 0.8601(8) 0.6283(7) -0.0126(5) 0.050(4) Uani 1 1 d . . . .
O19 O 0.8121(6) 0.7145(7) 0.0434(4) 0.038(4) Uani 1 1 d . . . .
O20 O 0.7100(6) 0.7696(6) 0.0636(5) 0.036(3) Uani 1 1 d . . . .
O21 O 0.7670(7) 0.7051(7) 0.1299(5) 0.042(4) Uani 1 1 d . . . .
O22 O 0.8459(6) 0.7838(6) 0.2232(5) 0.034(3) Uani 1 1 d . . . .
O23 O 0.8730(6) 0.9280(6) 0.2440(4) 0.029(3) Uani 1 1 d . . . .
O24 O 0.9730(6) 0.8666(6) 0.2302(4) 0.026(3) Uani 1 1 d . . . .
O25 O 0.9851(6) 0.7889(6) 0.2810(4) 0.031(3) Uani 1 1 d . . . .
O26 O 0.8974(6) 0.7310(6) 0.3166(4) 0.031(3) Uani 1 1 d . . . .
O27 O 0.7735(6) 0.7276(6) 0.3239(5) 0.036(3) Uani 1 1 d . . . .
O28 O 0.8574(6) 0.6716(6) 0.3753(4) 0.031(3) Uani 1 1 d . . . .
O29 O 0.7597(7) 0.6841(6) 0.4220(5) 0.037(3) Uani 1 1 d . . . .
O30 O 0.8838(7) 0.5474(6) 0.3982(5) 0.046(4) Uani 1 1 d . . . .
O31 O 0.7573(9) 0.4255(7) 0.3744(6) 0.064(5) Uani 1 1 d . . . .
O32 O 0.6385(8) 0.4521(7) 0.4156(6) 0.057(4) Uani 1 1 d . . . .
O33 O 0.6267(8) 0.4516(7) 0.3338(5) 0.056(4) Uani 1 1 d . . . .
O34 O 0.6394(7) 0.5600(8) 0.3908(5) 0.049(4) Uani 1 1 d . . . .
O35 O 0.5052(8) 0.3975(8) 0.3588(6) 0.071(5) Uani 1 1 d . . . .
O36 O 0.3798(8) 0.5031(9) 0.3649(7) 0.083(6) Uani 1 1 d . . . .
O37 O 0.4181(7) 0.6294(8) 0.3426(6) 0.062(5) Uani 1 1 d . . . .
O38 O 0.4223(8) 0.6354(8) 0.4240(6) 0.066(5) Uiso 1 1 d . . . .
O39 O 0.5306(7) 0.6516(8) 0.3975(5) 0.053(4) Uani 1 1 d . . . .
O40 O 0.3785(7) 0.7483(9) 0.3891(6) 0.068(5) Uani 1 1 d . . . .
O41 O 0.6449(7) 0.7806(8) 0.4315(5) 0.044(4) Uani 1 1 d . . . .
O42 O 0.4885(7) 0.8843(8) 0.4136(5) 0.059(5) Uani 1 1 d . . . .
O43 O 0.6189(6) 0.8778(6) 0.3892(4) 0.033(3) Uani 1 1 d . . . .
O44 O 0.6725(6) 0.7900(6) 0.3368(4) 0.030(3) Uani 1 1 d . . . .
O45 O 0.6994(6) 0.9097(6) 0.3376(4) 0.031(3) Uani 1 1 d . . . .
O46 O 0.6435(6) 0.6511(6) 0.3091(5) 0.036(3) Uani 1 1 d . . . .
O47 O 0.5679(7) 0.5789(7) 0.2119(5) 0.046(4) Uani 1 1 d . . . .
O48 O 0.5161(7) 0.6432(7) 0.1464(5) 0.048(4) Uani 1 1 d . . . .
O49 O 0.3920(7) 0.6601(9) 0.1179(7) 0.075(6) Uani 1 1 d . . . .
O50 O 0.4957(7) 0.7165(7) 0.0923(5) 0.047(4) Uani 1 1 d . . . .
O51 O 0.4457(7) 0.7580(7) 0.0108(5) 0.049(4) Uani 1 1 d . . . .
O52 O 0.5664(7) 0.8365(7) 0.1427(5) 0.041(4) Uani 1 1 d . . . .
O53 O 0.5824(7) 0.7698(7) 0.0552(5) 0.047(4) Uani 1 1 d . . . .
O54 O 0.6506(8) 0.8309(9) 0.0054(5) 0.066(5) Uani 1 1 d . . . .
O55 O 0.3688(7) 0.8865(8) 0.0189(5) 0.054(4) Uani 1 1 d . . . .
O56 O 0.4448(7) 1.0082(7) 0.0750(5) 0.047(4) Uani 1 1 d . . . .
O57 O 0.3581(7) 0.9603(7) 0.1087(5) 0.047(4) Uani 1 1 d . . . .
O58 O 0.3756(7) 1.1024(8) 0.1245(5) 0.056(4) Uani 1 1 d . . . .
O59 O 0.4794(7) 0.9565(7) 0.1414(5) 0.043(4) Uani 1 1 d . . . .
O60 O 0.4674(8) 1.1915(7) 0.2329(6) 0.059(5) Uani 1 1 d . . . .
O61 O 0.5580(6) 1.0331(6) 0.2384(5) 0.033(3) Uani 1 1 d . . . .
O62 O 0.5212(6) 1.1178(7) 0.2985(5) 0.040(4) Uani 1 1 d . . . .
O63 O 0.6019(7) 1.1556(6) 0.2580(5) 0.041(4) Uani 1 1 d . . . .
O64 O 0.6582(7) 1.1559(7) 0.3524(5) 0.048(4) Uani 1 1 d . . . .
O65 O 0.7539(6) 1.0448(6) 0.3683(4) 0.037(3) Uani 1 1 d . . . .
O66 O 0.6484(6) 0.9166(6) 0.2481(5) 0.030(3) Uani 1 1 d . . . .
O67 O 0.7799(6) 0.9530(6) 0.2916(4) 0.031(3) Uani 1 1 d . . . .
O68 O 0.8587(6) 1.0500(6) 0.2801(4) 0.028(3) Uani 1 1 d . . . .
O69 O 0.8286(6) 1.1750(6) 0.2583(5) 0.039(4) Uani 1 1 d . . . .
O70 O 0.9331(6) 1.1663(6) 0.3238(5) 0.036(3) Uani 1 1 d . . . .
O71 O 1.0235(6) 1.2668(6) 0.3692(5) 0.039(4) Uani 1 1 d . . . .
O72 O 1.0060(6) 1.1611(7) 0.3981(5) 0.041(4) Uani 1 1 d . . . .
O73 O 1.0933(6) 1.3333(6) 0.4502(5) 0.038(3) Uani 1 1 d . . . .
O74 O 1.1127(6) 1.3389(6) 0.5381(5) 0.036(3) Uani 1 1 d . . . .
O75 O 1.0785(7) 1.2296(6) 0.4820(5) 0.046(4) Uani 1 1 d . . . .
O76 O 1.0890(7) 1.3982(7) 0.3745(5) 0.051(4) Uani 1 1 d . . . .
O77 O 1.2412(7) 1.3968(7) 0.3300(5) 0.050(4) Uani 1 1 d . . . .
O78 O 1.3387(6) 1.3294(7) 0.3729(5) 0.043(4) Uani 1 1 d . . . .
O79 O 1.2738(7) 1.2659(7) 0.2988(5) 0.045(4) Uani 1 1 d . . . .
O80 O 1.2492(7) 1.2305(6) 0.3717(5) 0.042(4) Uani 1 1 d . . B 1
O81 O 1.4137(7) 1.2470(8) 0.3191(5) 0.053(4) Uani 1 1 d . . . .
O82 O 1.4377(7) 1.0913(7) 0.3542(5) 0.052(4) Uani 1 1 d . . . .
O83 O 1.3798(7) 1.0830(7) 0.4332(5) 0.043(4) Uani 1 1 d . . . .
O84 O 1.3941(6) 1.1016(7) 0.5232(4) 0.038(4) Uani 1 1 d . . . .
O85 O 1.2812(7) 1.0536(7) 0.4702(5) 0.045(4) Uani 1 1 d . . . .
O86 O 1.3102(6) 1.0179(7) 0.3517(5) 0.040(4) Uani 1 1 d . . . .
O87 O 1.0346(7) 1.0992(6) 0.4687(4) 0.038(3) Uani 1 1 d . . . .
O88 O 1.1493(7) 0.9973(7) 0.4621(4) 0.041(4) Uani 1 1 d . . . .
O89 O 1.2083(7) 0.9848(7) 0.3854(4) 0.038(4) Uani 1 1 d . . . .
O90 O 1.2102(6) 0.9256(7) 0.3043(4) 0.038(4) Uani 1 1 d . . . .
O91 O 1.0939(6) 0.8456(5) 0.2647(4) 0.024(3) Uani 1 1 d . . . .
O92 O 1.2161(6) 0.8306(6) 0.2312(5) 0.036(3) Uani 1 1 d . . . .
O93 O 1.2290(7) 0.8718(7) 0.1284(5) 0.047(4) Uani 1 1 d . . . .
O94 O 1.1074(6) 0.9098(6) 0.0818(4) 0.032(3) Uani 1 1 d . . . .
O95 O 1.1972(6) 1.0001(6) 0.1180(4) 0.026(3) Uani 1 1 d . . . .
O96 O 1.1166(6) 1.0109(7) 0.0310(4) 0.037(4) Uani 1 1 d . . . .
O97 O 0.9917(7) 1.1194(6) 0.0406(4) 0.037(3) Uani 1 1 d . . . .
O98 O 0.8984(6) 1.0917(6) 0.0972(4) 0.034(3) Uani 1 1 d . . . .
O99 O 0.9841(6) 1.1837(6) 0.1335(4) 0.032(3) Uani 1 1 d . . . .
O100 O 1.0988(6) 0.9694(6) 0.2591(4) 0.024(3) Uani 1 1 d . . . .
O101 O 1.0978(7) 0.9898(6) 0.1558(4) 0.033(3) Uani 1 1 d . . . .
O102 O 0.9882(6) 1.0809(6) 0.1625(4) 0.032(3) Uani 1 1 d . . . .
O103 O 0.8524(7) 1.1979(7) 0.1554(5) 0.044(4) Uani 1 1 d . . . .
O104 O 0.9821(6) 1.0665(6) 0.2667(4) 0.029(3) Uani 1 1 d . . . .
O105 O 0.9180(6) 0.9276(6) 0.1606(4) 0.031(3) Uani 1 1 d . . . .
O106 O 0.8339(6) 0.8488(6) 0.0676(4) 0.032(3) Uani 1 1 d . . . .
O107 O 0.6440(7) 0.7301(7) 0.1595(5) 0.046(4) Uani 1 1 d . . . .
O108 O 0.7242(7) 0.8003(6) 0.2538(5) 0.039(4) Uani 1 1 d . . . .
O109 O 1.2426(6) 1.1240(6) 0.4018(5) 0.035(3) Uani 1 1 d . . B 1
O110 O 1.1472(6) 1.2065(6) 0.4080(4) 0.036(3) Uani 1 1 d . . B 1
O111 O 0.6096(11) 0.4656(10) 0.1069(8) 0.103(7) Uiso 1 1 d . . . .
O112 O 0.7936(11) 1.3273(11) 0.1696(8) 0.107(7) Uiso 1 1 d . . . .
O113 O 1.1023(7) 1.2530(7) 0.1946(5) 0.048(4) Uani 1 1 d . . . .
O114 O 0.9920(7) 0.8229(6) 0.0559(5) 0.041(4) Uani 1 1 d . . . .
O115 O 1.2648(7) 1.1131(7) 0.1795(5) 0.045(4) Uani 1 1 d . . . .
O116 O 0.7476(6) 1.0175(6) -0.0298(6) 0.047(4) Uani 1 1 d . . . .
O117 O 0.9156(8) 1.0401(7) 0.3692(6) 0.058(4) Uani 1 1 d . . . .
O118 O 0.9209(9) 0.7956(8) 0.4277(5) 0.066(5) Uani 1 1 d . . . .
O119 O 0.9169(11) 0.3228(9) 0.3302(12) 0.187(17) Uani 1 1 d . . . .
O120 O 0.8699(9) 0.8696(8) 0.3368(6) 0.067(5) Uani 1 1 d . . . .
O121 O 1.0938(9) 0.8883(9) 0.3613(6) 0.076(6) Uani 1 1 d . . . .
O122 O 0.7620(9) 0.8985(11) -0.0229(9) 0.110(8) Uani 1 1 d . . . .
O123 O 0.8919(11) 1.2227(10) 0.0656(7) 0.091(6) Uiso 1 1 d . . C 1
O124 O 0.8981(11) 0.7297(8) -0.0531(7) 0.089(6) Uani 1 1 d . . . .
O125 O 1.2793(10) 1.2015(10) 0.1245(8) 0.099(8) Uani 1 1 d . . . .
O126 O 0.6868(11) 1.1091(11) 0.4424(8) 0.073(6) Uiso 0.8 1 d . P . .
O127 O 0.7728(12) 0.3235(12) 0.4753(9) 0.073(7) Uiso 0.8 1 d . P J 1
O128 O 0.9427(10) 1.2593(10) 0.4490(7) 0.064(6) Uiso 0.8 1 d . P . .
O129 O 0.3650(10) 1.0334(10) -0.0012(7) 0.062(6) Uani 0.8 1 d . P . .
O130 O 0.3404(12) 0.6572(10) 0.0240(9) 0.096(9) Uani 0.8 1 d . P . .
O131 O 0.6954(9) 1.1763(12) 0.2046(8) 0.117(9) Uani 1 1 d . . . .
O132 O 1.4025(10) 1.3869(11) 0.4547(9) 0.123(9) Uani 1 1 d . . . .
O133 O 0.5618(12) 1.0526(11) 0.0552(8) 0.082(8) Uani 0.8 1 d . P S .
O134 O 0.429(3) 0.600(3) -0.009(2) 0.050(16) Uiso 0.25 1 d . P D 2
O135 O 0.5453(14) 0.6726(13) -0.0388(10) 0.062(8) Uiso 0.6 1 d . P . .
O136 O 0.7352(15) 0.7389(14) -0.0378(11) 0.075(9) Uiso 0.6 1 d . P . .
O137 O 1.012(2) 0.891(2) 0.4215(16) 0.057(12) Uiso 0.35 1 d . P F 1
O138 O 0.4870(16) 0.4908(15) 0.1136(11) 0.059(9) Uiso 0.5 1 d . P D .
O139 O 0.3118(17) 0.4549(16) 0.2431(12) 0.066(10) Uiso 0.5 1 d . P . .
O140 O 1.4141(18) 1.2439(17) 0.1495(12) 0.072(10) Uiso 0.5 1 d . P . .
O141 O 0.8294(14) 1.4281(13) 0.2919(10) 0.044(7) Uiso 0.5 1 d . P . .
O142 O 0.4138(14) 0.5049(13) 0.1976(10) 0.043(7) Uiso 0.5 1 d . P D .
O143 O 1.6086(16) 1.3163(15) 0.2913(11) 0.060(9) Uiso 0.5 1 d . P . .
O144 O 0.2119(18) 0.7810(17) 0.0447(12) 0.072(10) Uiso 0.5 1 d . P . .
O145 O 0.748(2) 1.2785(19) 0.3168(14) 0.090(12) Uiso 0.5 1 d . P . .
O146 O 1.223(2) 1.4131(19) 0.1643(14) 0.087(12) Uiso 0.5 1 d . P . .
O147 O 0.739(2) 0.3047(19) -0.1097(14) 0.074(12) Uiso 0.45 1 d . P . .
O148 O 0.771(2) 0.5399(19) -0.0803(14) 0.077(12) Uiso 0.45 1 d . P . .
O149 O 1.0552(17) 0.8617(16) 0.4333(12) 0.066(10) Uiso 0.5 1 d . P F 2
O150 O 1.1724(18) 0.7670(17) 0.3948(13) 0.074(10) Uiso 0.5 1 d . P K 1
O151 O 1.2423(19) 0.7115(18) 0.3359(14) 0.071(11) Uiso 0.45 1 d . P L 1
O152 O 1.2528(17) 1.0470(16) 0.5595(11) 0.060(9) Uiso 0.5 1 d . P M 2
O153 O 0.7618(18) 1.1578(17) 0.0621(13) 0.074(10) Uiso 0.5 1 d . P . .
O154 O 0.9704(17) 1.4677(16) 0.5779(12) 0.068(10) Uiso 0.5 1 d . P . .
O155 O 0.492(3) 0.421(3) 0.1970(19) 0.079(16) Uiso 0.35 1 d . P . .
O156 O 1.0647(18) 0.7293(17) 0.0209(13) 0.062(10) Uiso 0.45 1 d . P N 2
O157 O 0.655(2) 0.644(2) -0.1068(17) 0.087(15) Uiso 0.4 1 d . P . .
O158 O 1.170(2) 0.704(2) 0.1689(15) 0.072(13) Uiso 0.4 1 d . P . .
O159 O 1.677(3) 1.314(3) 0.4023(19) 0.063(16) Uiso 0.3 1 d . P E 1
O160 O 1.571(3) 1.257(3) 0.431(2) 0.086(17) Uiso 0.35 1 d . P . .
O161 O 1.2603(14) 0.8435(14) 0.3596(10) 0.048(8) Uiso 0.5 1 d . P . .
O162 O 0.7674(17) 0.2974(17) 0.4900(12) 0.060(10) Uiso 0.5 1 d . P O 2
O163 O 1.1412(13) 1.1225(13) 0.2969(9) 0.049(7) Uiso 0.55 1 d . P E 1
O164 O 1.3108(16) 1.2904(15) 0.4834(11) 0.048(9) Uiso 0.45 1 d . P . .
O165 O 0.946(2) 0.4013(19) -0.0485(14) 0.046(11) Uiso 0.35 1 d . P . .
O166 O 0.759(2) 1.467(2) 0.2200(15) 0.038(11) Uiso 0.3 1 d . P P 1
O167 O 0.388(2) 0.4272(19) 0.0592(14) 0.062(11) Uiso 0.4 1 d . P D .
O168 O 1.287(2) 1.016(2) 0.5530(14) 0.043(11) Uiso 0.35 1 d . P Q 1
O169 O 1.518(3) 1.076(2) 0.4763(18) 0.053(14) Uiso 0.3 1 d . P . .
O170 O 1.046(3) 0.635(2) 0.1315(18) 0.056(14) Uiso 0.3 1 d . P . .
O171 O 1.026(2) 0.728(2) -0.0156(16) 0.054(12) Uiso 0.35 1 d . P R 1
O172 O 1.361(2) 0.839(2) 0.4697(16) 0.046(13) Uiso 0.3 1 d . P . .
O173 O 1.440(3) 1.201(3) 0.072(2) 0.076(18) Uiso 0.3 1 d . P . .
O174 O 0.345(3) 0.678(2) 0.2094(18) 0.056(14) Uiso 0.3 1 d . P D 1
O175 O 0.282(3) 0.630(3) 0.408(2) 0.066(16) Uiso 0.3 1 d . P . .
O176 O 1.217(4) 1.533(3) 0.447(2) 0.07(2) Uiso 0.25 1 d . P . .
O177 O 1.279(3) 1.559(3) 0.3074(18) 0.058(15) Uiso 0.3 1 d . P I 1
O178 O 0.957(2) 0.550(2) 0.5133(17) 0.085(15) Uiso 0.4 1 d . P . .
O179 O 0.393(3) 0.300(3) 0.2244(19) 0.083(16) Uiso 0.35 1 d . P . .
O180 O 0.676(3) 1.267(3) 0.098(2) 0.069(16) Uiso 0.3 1 d . P S 1
O181 O 0.678(3) 1.136(3) 0.1191(19) 0.064(16) Uiso 0.3 1 d . P S .
O182 O 0.810(3) 1.310(3) 0.385(2) 0.076(18) Uiso 0.3 1 d . P . .
O183 O 1.620(3) 1.328(3) 0.4209(19) 0.060(15) Uiso 0.3 1 d . P T 2
O184 O 1.1449(16) 0.9611(16) 0.5522(11) 0.058(9) Uiso 0.5 1 d . P F 1
O185 O 1.148(3) 1.018(3) 0.568(2) 0.044(15) Uiso 0.25 1 d . P F 2
O186 O 0.676(3) 1.252(3) 0.152(2) 0.057(17) Uiso 0.25 1 d . P S 2
O187 O 1.629(3) 1.301(3) 0.212(2) 0.045(15) Uiso 0.25 1 d . P . .
O188 O 1.564(3) 1.141(3) 0.437(2) 0.049(16) Uiso 0.25 1 d . P . .
O189 O 0.418(3) 0.503(3) 0.010(2) 0.07(2) Uiso 0.25 1 d . P . .
O190 O 0.724(3) 1.059(3) 0.069(2) 0.067(19) Uiso 0.25 1 d . P U 2
O201 O 1.226(3) 0.727(3) 0.375(2) 0.042(15) Uiso 0.25 1 d . P V 2
O202 O 0.813(3) 1.144(3) -0.016(2) 0.043(15) Uiso 0.25 1 d . P C 2
N1 N 1.3969(9) 0.8667(10) 0.2651(8) 0.035(6) Uani 0.8 1 d . P . .
C1 C 0.9155(9) 0.5256(8) 0.1629(6) 0.039(5) Uiso 1 1 d D . . .
C2 C 0.9536(8) 0.5608(8) 0.2055(6) 0.032(5) Uani 1 1 d D . . .
C3 C 0.9164(8) 0.6132(8) 0.2040(6) 0.034(5) Uani 1 1 d D . . .
C4 C 0.8777(9) 0.5778(8) 0.1609(6) 0.033(5) Uani 1 1 d D . . .
C5 C 0.6448(9) 0.6221(9) 0.4033(7) 0.045(6) Uani 1 1 d D . . .
C6 C 0.5955(9) 0.6637(9) 0.4060(7) 0.045(6) Uani 1 1 d D . . .
C7 C 0.6449(8) 0.7191(8) 0.4212(6) 0.031(5) Uani 1 1 d D . . .
C8 C 0.6950(8) 0.6777(8) 0.4172(7) 0.039(6) Uani 1 1 d D . . .
C9 C 0.5632(8) 0.9772(8) 0.2133(5) 0.025(4) Uiso 1 1 d D . . .
C10 C 0.5277(8) 0.9434(7) 0.1693(5) 0.023(4) Uiso 1 1 d D . . .
C11 C 0.5670(9) 0.8922(9) 0.1713(6) 0.037(5) Uani 1 1 d D . . .
C12 C 0.6021(9) 0.9262(8) 0.2159(6) 0.038(5) Uani 1 1 d D . . .
C13 C 1.0689(10) 1.0018(9) 0.2343(7) 0.031(5) Uiso 1 1 d . . . .
C14 C 1.0158(9) 1.0460(9) 0.2376(6) 0.025(5) Uani 1 1 d . . . .
C15 C 1.0183(9) 1.0532(9) 0.1917(6) 0.026(5) Uiso 1 1 d . . . .
C16 C 1.0679(10) 1.0113(9) 0.1884(7) 0.032(5) Uiso 1 1 d . . . .
C17 C 1.385(2) 0.929(2) 0.2954(16) 0.112(15) Uiso 0.8 1 d . P . .
C18 C 1.3646(15) 0.8622(14) 0.2154(10) 0.051(8) Uiso 0.8 1 d . P . .
C19 C 1.468(2) 0.8640(18) 0.2702(14) 0.088(12) Uiso 0.8 1 d . P . .
C20 C 1.365(2) 0.818(2) 0.2877(16) 0.114(15) Uiso 0.8 1 d . P . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O105 Mo1 O24 97.4(5) . .
O105 Mo1 O23 97.4(5) . .
O24 Mo1 O23 75.8(4) . .
O105 Mo1 S8 101.7(4) . .
O24 Mo1 S8 155.9(4) . .
O23 Mo1 S8 87.2(3) . .
O105 Mo1 S25 101.8(4) . .
O24 Mo1 S25 88.0(3) . .
O23 Mo1 S25 156.3(4) . .
S8 Mo1 S25 102.15(18) . .
O105 Mo1 Mo13 94.3(4) . .
O24 Mo1 Mo13 140.4(3) . .
O23 Mo1 Mo13 139.7(3) . .
S8 Mo1 Mo13 52.57(13) . .
S25 Mo1 Mo13 52.56(13) . .
O105 Mo1 K2 97.5(5) . .
O24 Mo1 K2 37.6(3) . .
O23 Mo1 K2 38.3(3) . .
S8 Mo1 K2 124.23(15) . .
S25 Mo1 K2 124.22(15) . .
Mo13 Mo1 K2 168.19(12) . .
O65 Mo2 O45 98.2(6) . .
O65 Mo2 O67 97.2(6) . .
O45 Mo2 O67 75.1(5) . .
O65 Mo2 S12 100.3(5) . .
O45 Mo2 S12 156.6(4) . .
O67 Mo2 S12 88.5(3) . .
O65 Mo2 S17 101.9(5) . .
O45 Mo2 S17 88.1(4) . .
O67 Mo2 S17 156.2(4) . .
S12 Mo2 S17 101.78(18) . .
O65 Mo2 O66 168.4(5) . .
O45 Mo2 O66 74.4(5) . .
O67 Mo2 O66 72.4(4) . .
S12 Mo2 O66 84.8(3) . .
S17 Mo2 O66 87.1(3) . .
O65 Mo2 Mo7 95.6(4) . .
O45 Mo2 Mo7 140.2(3) . .
O67 Mo2 Mo7 139.5(3) . .
S12 Mo2 Mo7 51.40(13) . .
S17 Mo2 Mo7 52.49(14) . .
O66 Mo2 Mo7 95.8(3) . .
O1 Mo3 O25 98.2(6) . .
O1 Mo3 O26 97.3(6) . .
O25 Mo3 O26 75.5(5) . .
O1 Mo3 S26 102.0(5) . .
O25 Mo3 S26 87.1(4) . .
O26 Mo3 S26 155.6(4) . .
O1 Mo3 S10 100.8(5) . .
O25 Mo3 S10 156.5(4) . .
O26 Mo3 S10 88.5(3) . .
S26 Mo3 S10 102.14(19) . .
O1 Mo3 O2 167.9(6) . .
O25 Mo3 O2 72.9(5) . .
O26 Mo3 O2 72.7(5) . .
S26 Mo3 O2 86.0(3) . .
S10 Mo3 O2 86.1(3) . .
O1 Mo3 Mo12 96.1(5) . .
O25 Mo3 Mo12 138.8(3) . .
O26 Mo3 Mo12 140.2(3) . .
S26 Mo3 Mo12 52.08(14) . .
S10 Mo3 Mo12 52.18(14) . .
O2 Mo3 Mo12 96.1(3) . .
O60 Mo4 O63 101.3(7) . .
O60 Mo4 O62 99.5(7) . .
O63 Mo4 O62 68.6(5) . .
O60 Mo4 S2 102.6(6) . .
O63 Mo4 S2 86.9(4) . .
O62 Mo4 S2 149.8(4) . .
O60 Mo4 S21 102.5(6) . .
O63 Mo4 S21 151.5(4) . .
O62 Mo4 S21 92.1(4) . .
S2 Mo4 S21 102.9(2) . .
O60 Mo4 O61 166.9(7) . .
O63 Mo4 O61 69.5(5) . .
O62 Mo4 O61 68.7(5) . .
S2 Mo4 O61 86.6(3) . .
S21 Mo4 O61 84.2(3) . .
O60 Mo4 Mo26 101.0(6) . .
O63 Mo4 Mo26 136.5(4) . .
O62 Mo4 Mo26 141.9(4) . .
S2 Mo4 Mo26 51.92(16) . .
S21 Mo4 Mo26 52.15(15) . .
O61 Mo4 Mo26 92.0(3) . .
O60 Mo4 K10 60.6(6) . 1_455
O63 Mo4 K10 59.4(4) . 1_455
O62 Mo4 K10 45.9(4) . 1_455
S2 Mo4 K10 134.3(3) . 1_455
S21 Mo4 K10 121.6(2) . 1_455
O61 Mo4 K10 106.3(4) . 1_455
Mo26 Mo4 K10 160.39(15) . 1_455
O47 Mo5 O17 100.1(7) . .
O47 Mo5 O48 93.9(6) . .
O17 Mo5 O48 76.2(6) . .
O47 Mo5 S11 102.7(5) . .
O17 Mo5 S11 153.4(4) . .
O48 Mo5 S11 88.5(4) . .
O47 Mo5 S7 101.0(5) . .
O17 Mo5 S7 86.6(4) . .
O48 Mo5 S7 158.9(4) . .
S11 Mo5 S7 102.4(2) . .
O47 Mo5 O107 172.8(6) . .
O17 Mo5 O107 75.4(5) . .
O48 Mo5 O107 79.7(5) . .
S11 Mo5 O107 80.6(4) . .
S7 Mo5 O107 84.4(3) . .
O47 Mo5 Mo9 94.3(5) . .
O17 Mo5 Mo9 138.7(4) . .
O48 Mo5 Mo9 141.4(4) . .
S11 Mo5 Mo9 52.88(14) . .
S7 Mo5 Mo9 52.62(14) . .
O107 Mo5 Mo9 92.8(4) . .
O47 Mo5 K27 51.5(6) . .
O17 Mo5 K27 134.6(5) . .
O48 Mo5 K27 72.4(5) . .
S11 Mo5 K27 56.5(3) . .
S7 Mo5 K27 128.6(3) . .
O107 Mo5 K27 128.2(4) . .
Mo9 Mo5 K27 83.7(3) . .
O47 Mo5 K9' 115.3(6) . .
O17 Mo5 K9' 35.4(4) . .
O48 Mo5 K9' 46.4(5) . .
S11 Mo5 K9' 120.0(3) . .
S7 Mo5 K9' 113.0(3) . .
O107 Mo5 K9' 57.8(5) . .
Mo9 Mo5 K9' 150.0(3) . .
K27 Mo5 K9' 118.0(4) . .
O97 Mo6 O98 98.1(6) . .
O97 Mo6 O99 98.4(5) . .
O98 Mo6 O99 69.0(5) . .
O97 Mo6 S24 104.4(5) . .
O98 Mo6 S24 88.8(4) . .
O99 Mo6 S24 150.2(4) . .
O97 Mo6 S13 103.0(5) . .
O98 Mo6 S13 152.5(4) . .
O99 Mo6 S13 90.4(4) . .
S24 Mo6 S13 102.70(19) . .
O97 Mo6 O102 163.9(5) . .
O98 Mo6 O102 68.9(5) . .
O99 Mo6 O102 68.4(4) . .
S24 Mo6 O102 85.5(3) . .
S13 Mo6 O102 86.9(3) . .
O97 Mo6 Mo14 103.4(4) . .
O98 Mo6 Mo14 138.6(3) . .
O99 Mo6 Mo14 139.7(3) . .
S24 Mo6 Mo14 51.84(14) . .
S13 Mo6 Mo14 51.95(13) . .
O102 Mo6 Mo14 92.8(3) . .
O97 Mo6 K4 47.3(5) . .
O98 Mo6 K4 51.3(4) . .
O99 Mo6 K4 86.1(4) . .
S24 Mo6 K4 95.40(19) . .
S13 Mo6 K4 148.7(2) . .
O102 Mo6 K4 120.1(3) . .
Mo14 Mo6 K4 133.12(15) . .
O97 Mo6 K4' 50.8(7) . .
O98 Mo6 K4' 70.3(6) . .
O99 Mo6 K4' 49.3(6) . .
S24 Mo6 K4' 141.9(5) . .
S13 Mo6 K4' 110.4(5) . .
O102 Mo6 K4' 113.9(6) . .
Mo14 Mo6 K4' 148.4(5) . .
O97 Mo6 K1 41.6(5) . 2_775
O98 Mo6 K1 139.6(4) . 2_775
O99 Mo6 K1 107.2(3) . 2_775
S24 Mo6 K1 102.65(16) . 2_775
S13 Mo6 K1 62.63(15) . 2_775
O102 Mo6 K1 149.4(3) . 2_775
Mo14 Mo6 K1 70.98(9) . 2_775
K4 Mo6 K1 88.79(18) . 2_775
K4' Mo6 K1 77.5(5) . 2_775
O64 Mo7 O63 98.9(6) . .
O64 Mo7 O62 99.2(6) . .
O63 Mo7 O62 69.0(5) . .
O64 Mo7 O61 167.8(6) . .
O63 Mo7 O61 71.5(5) . .
O62 Mo7 O61 70.6(5) . .
O64 Mo7 S12 103.1(5) . .
O63 Mo7 S12 86.4(4) . .
O62 Mo7 S12 149.0(4) . .
O61 Mo7 S12 84.1(3) . .
O64 Mo7 S17 102.7(5) . .
O63 Mo7 S17 153.7(4) . .
O62 Mo7 S17 92.7(4) . .
O61 Mo7 S17 84.9(3) . .
S12 Mo7 S17 102.90(18) . .
O64 Mo7 Mo2 98.5(5) . .
O63 Mo7 Mo2 138.1(4) . .
O62 Mo7 Mo2 143.8(4) . .
O61 Mo7 Mo2 93.7(3) . .
S12 Mo7 Mo2 52.57(13) . .
S17 Mo7 Mo2 52.48(13) . .
O64 Mo7 K10 56.7(5) . 1_455
O63 Mo7 K10 61.4(4) . 1_455
O62 Mo7 K10 47.8(4) . 1_455
O61 Mo7 K10 111.3(3) . 1_455
S12 Mo7 K10 134.7(2) . 1_455
S17 Mo7 K10 120.2(3) . 1_455
Mo2 Mo7 K10 153.91(19) . 1_455
O64 Mo7 K19 43.8(5) . .
O63 Mo7 K19 95.4(5) . .
O62 Mo7 K19 138.7(4) . .
O61 Mo7 K19 142.3(4) . .
S12 Mo7 K19 59.3(3) . .
S17 Mo7 K19 110.6(3) . .
Mo2 Mo7 K19 72.4(3) . .
K10 Mo7 K19 90.9(3) 1_455 .
O93 Mo8 O94 98.7(6) . .
O93 Mo8 O95 98.9(6) . .
O94 Mo8 O95 69.5(5) . .
O93 Mo8 O101 166.8(6) . .
O94 Mo8 O101 71.3(5) . .
O95 Mo8 O101 69.7(4) . .
O93 Mo8 S22 105.2(5) . .
O94 Mo8 S22 87.3(4) . .
O95 Mo8 S22 148.7(3) . .
O101 Mo8 S22 83.4(3) . .
O93 Mo8 S18 102.3(5) . .
O94 Mo8 S18 153.3(4) . .
O95 Mo8 S18 90.9(4) . .
O101 Mo8 S18 85.2(4) . .
S22 Mo8 S18 102.73(18) . .
O93 Mo8 Mo15 101.8(5) . .
O94 Mo8 Mo15 138.0(3) . .
O95 Mo8 Mo15 140.7(3) . .
O101 Mo8 Mo15 91.4(3) . .
S22 Mo8 Mo15 52.06(13) . .
S18 Mo8 Mo15 52.23(13) . .
O46 Mo9 O44 97.3(6) . .
O46 Mo9 O27 97.6(6) . .
O44 Mo9 O27 75.8(5) . .
O46 Mo9 S7 101.9(5) . .
O44 Mo9 S7 155.9(4) . .
O27 Mo9 S7 87.2(4) . .
O46 Mo9 S11 101.3(4) . .
O44 Mo9 S11 88.2(4) . .
O27 Mo9 S11 156.6(4) . .
S7 Mo9 S11 102.1(2) . .
O46 Mo9 Mo5 93.8(5) . .
O44 Mo9 Mo5 140.6(3) . .
O27 Mo9 Mo5 139.8(4) . .
S7 Mo9 Mo5 52.72(14) . .
S11 Mo9 Mo5 52.45(14) . .
O46 Mo9 K5 98.1(5) . .
O44 Mo9 K5 37.4(3) . .
O27 Mo9 K5 38.4(4) . .
S7 Mo9 K5 124.11(17) . .
S11 Mo9 K5 124.20(17) . .
Mo5 Mo9 K5 168.08(14) . .
O88 Mo10 O85 93.4(6) . .
O88 Mo10 O89 93.1(6) . .
O85 Mo10 O89 81.5(6) . .
O88 Mo10 S31 102.1(5) . .
O85 Mo10 S31 159.0(4) . .
O89 Mo10 S31 83.6(4) . .
O88 Mo10 S6 102.1(5) . .
O85 Mo10 S6 84.6(4) . .
O89 Mo10 S6 160.0(4) . .
S31 Mo10 S6 105.5(2) . .
O88 Mo10 O109 169.7(6) . .
O85 Mo10 O109 78.7(5) . .
O89 Mo10 O109 79.2(5) . .
S31 Mo10 O109 84.0(3) . .
S6 Mo10 O109 84.0(4) . .
O88 Mo10 Mo32 100.4(5) . .
O85 Mo10 Mo32 137.5(4) . .
O89 Mo10 Mo32 136.7(4) . .
S31 Mo10 Mo32 53.45(17) . .
S6 Mo10 Mo32 53.34(17) . .
O109 Mo10 Mo32 89.9(3) . .
O88 Mo10 K12' 54.7(8) . .
O85 Mo10 K12' 50.3(7) . .
O89 Mo10 K12' 58.7(7) . .
S31 Mo10 K12' 130.6(7) . .
S6 Mo10 K12' 120.9(7) . .
Mo32 Mo10 K12' 154.5(6) . .
O88 Mo10 K13 31.7(5) . .
O85 Mo10 K13 116.5(4) . .
O89 Mo10 K13 116.4(4) . .
S31 Mo10 K13 83.5(3) . .
S6 Mo10 K13 82.8(3) . .
O109 Mo10 K13 158.7(4) . .
Mo32 Mo10 K13 68.8(2) . .
K12' Mo10 K13 86.1(7) . .
O55 Mo11 O56 99.0(7) . .
O55 Mo11 O57 98.1(6) . .
O56 Mo11 O57 69.9(6) . .
O55 Mo11 O59 166.1(6) . .
O56 Mo11 O59 70.7(5) . .
O57 Mo11 O59 70.0(5) . .
O55 Mo11 S15 103.5(5) . .
O56 Mo11 S15 87.0(4) . .
O57 Mo11 S15 150.5(4) . .
O59 Mo11 S15 85.6(4) . .
O55 Mo11 S14 103.6(6) . .
O56 Mo11 S14 152.2(4) . .
O57 Mo11 S14 90.8(4) . .
O59 Mo11 S14 84.2(4) . .
S15 Mo11 S14 103.2(2) . .
O55 Mo11 Mo27 99.4(5) . .
O56 Mo11 Mo27 138.4(4) . .
O57 Mo11 Mo27 142.5(4) . .
O59 Mo11 Mo27 94.5(3) . .
S15 Mo11 Mo27 52.45(15) . .
S14 Mo11 Mo27 52.96(14) . .
O55 Mo11 K8 40.6(6) . .
O56 Mo11 K8 139.0(4) . .
O57 Mo11 K8 103.3(4) . .
O59 Mo11 K8 147.1(4) . .
S15 Mo11 K8 106.2(2) . .
S14 Mo11 K8 63.4(2) . .
Mo27 Mo11 K8 71.07(16) . .
O5 Mo12 O6 97.1(7) . .
O5 Mo12 O4 100.0(7) . .
O6 Mo12 O4 69.7(5) . .
O5 Mo12 O3 167.8(6) . .
O6 Mo12 O3 72.3(5) . .
O4 Mo12 O3 70.9(5) . .
O5 Mo12 S26 102.9(6) . .
O6 Mo12 S26 153.5(5) . .
O4 Mo12 S26 89.7(4) . .
O3 Mo12 S26 85.5(3) . .
O5 Mo12 S10 103.2(6) . .
O6 Mo12 S10 88.7(4) . .
O4 Mo12 S10 150.1(4) . .
O3 Mo12 S10 83.1(4) . .
S26 Mo12 S10 103.18(19) . .
O5 Mo12 Mo3 98.8(5) . .
O6 Mo12 Mo3 140.7(4) . .
O4 Mo12 Mo3 140.9(4) . .
O3 Mo12 Mo3 93.4(3) . .
S26 Mo12 Mo3 52.66(14) . .
S10 Mo12 Mo3 52.68(13) . .
O5 Mo12 Na1 51.9(6) . 1_545
O6 Mo12 Na1 55.2(4) . 1_545
O4 Mo12 Na1 58.9(5) . 1_545
O3 Mo12 Na1 115.9(4) . 1_545
S26 Mo12 Na1 128.0(3) . 1_545
S10 Mo12 Na1 125.0(3) . 1_545
Mo3 Mo12 Na1 150.62(19) . 1_545
O5 Mo12 K20 93.1(6) . .
O6 Mo12 K20 35.3(5) . .
O4 Mo12 K20 105.0(5) . .
O3 Mo12 K20 81.8(4) . .
S26 Mo12 K20 156.1(3) . .
S10 Mo12 K20 55.3(3) . .
Mo3 Mo12 K20 107.9(3) . .
Na1 Mo12 K20 75.9(3) 1_545 .
O106 Mo13 O20 99.0(6) . .
O106 Mo13 O19 93.0(6) . .
O20 Mo13 O19 77.0(5) . .
O106 Mo13 S8 100.8(5) . .
O20 Mo13 S8 86.4(4) . .
O19 Mo13 S8 159.9(4) . .
O106 Mo13 S25 102.3(4) . .
O20 Mo13 S25 154.6(4) . .
O19 Mo13 S25 88.2(4) . .
S8 Mo13 S25 102.86(18) . .
O106 Mo13 O21 172.5(6) . .
O20 Mo13 O21 76.0(5) . .
O19 Mo13 O21 80.6(5) . .
S8 Mo13 O21 84.5(3) . .
S25 Mo13 O21 81.3(3) . .
O106 Mo13 Mo1 93.9(5) . .
O20 Mo13 Mo1 138.8(4) . .
O19 Mo13 Mo1 141.3(3) . .
S8 Mo13 Mo1 52.77(13) . .
S25 Mo13 Mo1 53.11(13) . .
O21 Mo13 Mo1 93.5(3) . .
O96 Mo14 O94 98.6(6) . .
O96 Mo14 O95 98.7(5) . .
O94 Mo14 O95 69.5(5) . .
O96 Mo14 S24 103.6(5) . .
O94 Mo14 S24 89.1(4) . .
O95 Mo14 S24 151.1(3) . .
O96 Mo14 S13 102.3(5) . .
O94 Mo14 S13 152.9(4) . .
O95 Mo14 S13 90.2(3) . .
S24 Mo14 S13 102.47(19) . .
O96 Mo14 O101 164.7(5) . .
O94 Mo14 O101 70.1(4) . .
O95 Mo14 O101 68.1(5) . .
S24 Mo14 O101 86.9(4) . .
S13 Mo14 O101 85.9(3) . .
O96 Mo14 Mo6 102.2(4) . .
O94 Mo14 Mo6 138.8(4) . .
O95 Mo14 Mo6 139.8(3) . .
S24 Mo14 Mo6 51.62(13) . .
S13 Mo14 Mo6 51.95(14) . .
O101 Mo14 Mo6 93.1(3) . .
O96 Mo14 K4 47.9(5) . 2_775
O94 Mo14 K4 50.8(3) . 2_775
O95 Mo14 K4 78.9(4) . 2_775
S24 Mo14 K4 102.9(2) . 2_775
S13 Mo14 K4 144.9(2) . 2_775
O101 Mo14 K4 119.4(3) . 2_775
Mo6 Mo14 K4 139.29(15) . 2_775
O96 Mo14 K1 44.3(5) . 2_775
O94 Mo14 K1 142.9(3) . 2_775
O95 Mo14 K1 109.8(3) . 2_775
S24 Mo14 K1 98.91(15) . 2_775
S13 Mo14 K1 60.04(15) . 2_775
O101 Mo14 K1 145.9(3) . 2_775
Mo6 Mo14 K1 66.20(8) . 2_775
K4 Mo14 K1 92.21(17) 2_775 2_775
O92 Mo15 O91 98.1(5) . .
O92 Mo15 O90 88.5(6) . .
O91 Mo15 O90 78.7(5) . .
O92 Mo15 S22 100.4(5) . .
O91 Mo15 S22 88.4(3) . .
O90 Mo15 S22 165.3(4) . .
O92 Mo15 S18 103.5(5) . .
O91 Mo15 S18 153.5(4) . .
O90 Mo15 S18 86.7(4) . .
S22 Mo15 S18 102.38(19) . .
O92 Mo15 O100 162.9(5) . .
O91 Mo15 O100 72.0(4) . .
O90 Mo15 O100 76.0(4) . .
S22 Mo15 O100 93.4(3) . .
S18 Mo15 O100 83.1(3) . .
O92 Mo15 Mo8 98.8(4) . .
O91 Mo15 Mo8 138.9(3) . .
O90 Mo15 Mo8 138.8(4) . .
S22 Mo15 Mo8 51.81(13) . .
S18 Mo15 Mo8 52.12(14) . .
O100 Mo15 Mo8 97.8(3) . .
O81 Mo16 O79 98.4(6) . .
O81 Mo16 O78 96.9(7) . .
O79 Mo16 O78 69.6(5) . .
O81 Mo16 S16 103.6(6) . .
O79 Mo16 S16 88.9(4) . .
O78 Mo16 S16 152.3(4) . .
O81 Mo16 S28 103.4(5) . .
O79 Mo16 S28 151.8(4) . .
O78 Mo16 S28 90.0(4) . .
S16 Mo16 S28 102.9(2) . .
O81 Mo16 O80 166.5(6) . .
O79 Mo16 O80 71.0(5) . .
O78 Mo16 O80 71.9(5) . .
S16 Mo16 O80 84.9(4) . .
S28 Mo16 O80 84.5(4) . .
O81 Mo16 Mo17 104.7(5) . .
O79 Mo16 Mo17 137.8(4) . .
O78 Mo16 Mo17 139.4(4) . .
S16 Mo16 Mo17 51.75(14) . .
S28 Mo16 Mo17 51.90(16) . .
O80 Mo16 Mo17 88.8(3) . .
O81 Mo16 Mo34 120.7(5) . .
O79 Mo16 Mo34 40.3(4) . .
O78 Mo16 Mo34 39.9(4) . .
S16 Mo16 Mo34 112.51(16) . .
S28 Mo16 Mo34 111.90(17) . .
O80 Mo16 Mo34 45.9(3) . .
Mo17 Mo16 Mo34 134.63(8) . .
O81 Mo16 K3 57.6(5) . 1_665
O79 Mo16 K3 54.1(4) . 1_665
O78 Mo16 K3 50.3(4) . 1_665
S16 Mo16 K3 129.32(18) . 1_665
S28 Mo16 K3 126.28(19) . 1_665
O80 Mo16 K3 108.9(4) . 1_665
Mo17 Mo16 K3 162.26(13) . 1_665
Mo34 Mo16 K3 63.06(12) . 1_665
O81 Mo16 K10 27.2(5) . .
O79 Mo16 K10 124.7(4) . .
O78 Mo16 K10 99.1(4) . .
S16 Mo16 K10 107.7(2) . .
S28 Mo16 K10 76.3(2) . .
O80 Mo16 K10 158.8(4) . .
Mo17 Mo16 K10 86.28(17) . .
Mo34 Mo16 K10 135.22(16) . .
K3 Mo16 K10 76.6(2) 1_665 .
O81 Mo16 K16 105.6(6) . .
O79 Mo16 K16 36.0(5) . .
O78 Mo16 K16 103.8(4) . .
S16 Mo16 K16 52.9(3) . .
S28 Mo16 K16 145.9(3) . .
O80 Mo16 K16 71.0(4) . .
Mo17 Mo16 K16 102.9(2) . .
Mo34 Mo16 K16 67.0(2) . .
K3 Mo16 K16 85.0(3) 1_665 .
K10 Mo16 K16 130.1(3) . .
O82 Mo17 O86 98.7(6) . .
O82 Mo17 O83 98.1(6) . .
O86 Mo17 O83 77.9(5) . .
O82 Mo17 S16 103.7(5) . .
O86 Mo17 S16 84.3(4) . .
O83 Mo17 S16 153.6(4) . .
O82 Mo17 S28 103.9(5) . .
O86 Mo17 S28 153.3(4) . .
O83 Mo17 S28 85.0(4) . .
S16 Mo17 S28 103.7(2) . .
O82 Mo17 Mo16 105.3(5) . .
O86 Mo17 Mo16 133.9(4) . .
O83 Mo17 Mo16 134.7(4) . .
S16 Mo17 Mo16 52.24(16) . .
S28 Mo17 Mo16 52.23(15) . .
O8 Mo18 O9 97.0(7) . .
O8 Mo18 O10 100.6(7) . .
O9 Mo18 O10 70.4(6) . .
O8 Mo18 S30 103.2(6) . .
O9 Mo18 S30 153.1(4) . .
O10 Mo18 S30 88.4(4) . .
O8 Mo18 S33 102.6(6) . .
O9 Mo18 S33 89.7(5) . .
O10 Mo18 S33 151.0(4) . .
S30 Mo18 S33 102.9(2) . .
O8 Mo18 O11 165.1(7) . .
O9 Mo18 O11 70.3(5) . .
O10 Mo18 O11 68.4(5) . .
S30 Mo18 O11 86.9(4) . .
S33 Mo18 O11 85.4(4) . .
O8 Mo18 Mo19 101.2(6) . .
O9 Mo18 Mo19 140.6(4) . .
O10 Mo18 Mo19 138.0(4) . .
S30 Mo18 Mo19 51.84(17) . .
S33 Mo18 Mo19 52.40(18) . .
O11 Mo18 Mo19 93.7(4) . .
O8 Mo18 K4' 52.2(8) . 1_545
O9 Mo18 K4' 61.7(7) . 1_545
O10 Mo18 K4' 54.0(7) . 1_545
S30 Mo18 K4' 118.8(6) . 1_545
S33 Mo18 K4' 134.1(6) . 1_545
O11 Mo18 K4' 113.4(6) . 1_545
Mo19 Mo18 K4' 151.7(5) . 1_545
O8 Mo18 K21 93.2(6) . .
O9 Mo18 K21 30.2(5) . .
O10 Mo18 K21 100.6(5) . .
S30 Mo18 K21 159.7(3) . .
S33 Mo18 K21 61.2(4) . .
O11 Mo18 K21 79.7(4) . .
Mo19 Mo18 K21 113.6(3) . .
K4' Mo18 K21 80.7(6) 1_545 .
O7 Mo19 O6 101.8(7) . .
O7 Mo19 O4 99.4(7) . .
O6 Mo19 O4 69.0(6) . .
O7 Mo19 S30 103.6(6) . .
O6 Mo19 S30 88.5(5) . .
O4 Mo19 S30 150.7(4) . .
O7 Mo19 S33 102.0(6) . .
O6 Mo19 S33 150.3(4) . .
O4 Mo19 S33 89.9(5) . .
S30 Mo19 S33 102.7(2) . .
O7 Mo19 O3 167.3(7) . .
O6 Mo19 O3 70.3(5) . .
O4 Mo19 O3 68.7(5) . .
S30 Mo19 O3 86.5(4) . .
S33 Mo19 O3 82.9(4) . .
O7 Mo19 Mo18 101.0(6) . .
O6 Mo19 Mo18 138.1(4) . .
O4 Mo19 Mo18 139.7(4) . .
S30 Mo19 Mo18 52.03(17) . .
S33 Mo19 Mo18 51.96(17) . .
O3 Mo19 Mo18 91.2(4) . .
O30 Mo20 O28 101.2(6) . .
O30 Mo20 O74 91.1(6) . 2_776
O28 Mo20 O74 77.7(5) . 2_776
O30 Mo20 S1 100.9(5) . .
O28 Mo20 S1 87.8(4) . .
O74 Mo20 S1 162.8(4) 2_776 .
O30 Mo20 S29 100.8(5) . .
O28 Mo20 S29 153.3(4) . .
O74 Mo20 S29 87.0(4) 2_776 .
S1 Mo20 S29 102.7(2) . .
O30 Mo20 O29 165.9(6) . .
O28 Mo20 O29 71.1(4) . .
O74 Mo20 O29 75.9(5) 2_776 .
S1 Mo20 O29 90.7(4) . .
S29 Mo20 O29 84.2(3) . .
O30 Mo20 Mo21 96.0(5) . .
O28 Mo20 Mo21 138.9(3) . .
O74 Mo20 Mo21 139.3(4) 2_776 .
S1 Mo20 Mo21 52.22(15) . .
S29 Mo20 Mo21 52.26(16) . .
O29 Mo20 Mo21 97.4(3) . .
O30 Mo20 K6 37.8(6) . .
O28 Mo20 K6 138.2(5) . .
O74 Mo20 K6 92.1(5) 2_776 .
S1 Mo20 K6 105.0(4) . .
S29 Mo20 K6 63.1(4) . .
O29 Mo20 K6 145.9(5) . .
Mo21 Mo20 K6 70.9(4) . .
O30 Mo20 K11 56.0(5) . 2_776
O28 Mo20 K11 63.3(4) . 2_776
O74 Mo20 K11 45.5(4) 2_776 2_776
S1 Mo20 K11 134.2(2) . 2_776
S29 Mo20 K11 119.2(2) . 2_776
O29 Mo20 K11 110.0(4) . 2_776
Mo21 Mo20 K11 150.7(2) . 2_776
K6 Mo20 K11 80.5(4) . 2_776
O31 Mo21 O33 98.1(7) . .
O31 Mo21 O32 100.1(7) . .
O33 Mo21 O32 70.0(6) . .
O31 Mo21 O34 167.1(7) . .
O33 Mo21 O34 70.5(6) . .
O32 Mo21 O34 70.8(5) . .
O31 Mo21 S1 102.9(6) . .
O33 Mo21 S1 88.0(4) . .
O32 Mo21 S1 150.1(4) . .
O34 Mo21 S1 83.1(4) . .
O31 Mo21 S29 103.9(6) . .
O33 Mo21 S29 152.3(5) . .
O32 Mo21 S29 89.6(5) . .
O34 Mo21 S29 85.5(4) . .
S1 Mo21 S29 103.0(2) . .
O31 Mo21 Mo20 100.3(6) . .
O33 Mo21 Mo20 139.1(4) . .
O32 Mo21 Mo20 140.2(4) . .
O34 Mo21 Mo20 92.4(4) . .
S1 Mo21 Mo20 52.39(15) . .
S29 Mo21 Mo20 52.43(15) . .
O31 Mo21 K6 43.3(7) . .
O33 Mo21 K6 141.2(6) . .
O32 Mo21 K6 107.0(5) . .
O34 Mo21 K6 147.1(5) . .
S1 Mo21 K6 102.8(4) . .
S29 Mo21 K6 61.5(4) . .
Mo20 Mo21 K6 68.0(3) . .
O35 Mo22 O33 99.9(8) . .
O35 Mo22 O32 99.4(7) . .
O33 Mo22 O32 70.4(6) . .
O35 Mo22 S3 103.7(7) . .
O33 Mo22 S3 151.6(4) . .
O32 Mo22 S3 90.2(5) . .
O35 Mo22 S4 102.2(6) . .
O33 Mo22 S4 87.8(5) . .
O32 Mo22 S4 151.6(4) . .
S3 Mo22 S4 102.2(3) . .
O35 Mo22 O34 165.5(7) . .
O33 Mo22 O34 68.6(5) . .
O32 Mo22 O34 68.9(5) . .
S3 Mo22 O34 85.4(4) . .
S4 Mo22 O34 86.5(4) . .
O35 Mo22 Mo23 102.1(6) . .
O33 Mo22 Mo23 136.9(4) . .
O32 Mo22 Mo23 139.7(5) . .
S3 Mo22 Mo23 51.81(18) . .
S4 Mo22 Mo23 51.5(2) . .
O34 Mo22 Mo23 92.4(4) . .
O35 Mo22 K3 40.9(6) . .
O33 Mo22 K3 109.0(4) . .
O32 Mo22 K3 140.3(4) . .
S3 Mo22 K3 99.2(2) . .
S4 Mo22 K3 63.29(19) . .
O34 Mo22 K3 149.8(4) . .
Mo23 Mo22 K3 68.51(13) . .
O35 Mo22 K22 100.8(7) . .
O33 Mo22 K22 105.9(5) . .
O32 Mo22 K22 36.3(5) . .
S3 Mo22 K22 54.3(3) . .
S4 Mo22 K22 150.6(4) . .
O34 Mo22 K22 75.1(4) . .
Mo23 Mo22 K22 105.7(3) . .
K3 Mo22 K22 131.4(3) . .
O36 Mo23 O37 100.9(7) . .
O36 Mo23 O38 98.8(8) . .
O37 Mo23 O38 69.4(7) . .
O36 Mo23 S4 102.9(7) . .
O37 Mo23 S4 87.7(5) . .
O38 Mo23 S4 151.1(5) . .
O36 Mo23 S3 102.6(6) . .
O37 Mo23 S3 151.2(5) . .
O38 Mo23 S3 90.8(5) . .
S4 Mo23 S3 102.8(3) . .
O36 Mo23 O39 164.8(8) . .
O37 Mo23 O39 68.9(5) . .
O38 Mo23 O39 67.4(6) . .
S4 Mo23 O39 88.3(4) . .
S3 Mo23 O39 84.5(4) . .
O36 Mo23 Mo22 101.8(7) . .
O37 Mo23 Mo22 137.2(5) . .
O38 Mo23 Mo22 140.3(5) . .
S4 Mo23 Mo22 52.04(18) . .
S3 Mo23 Mo22 51.8(2) . .
O39 Mo23 Mo22 93.2(4) . .
O36 Mo23 K3 41.0(7) . .
O37 Mo23 K3 109.1(4) . .
O38 Mo23 K3 139.7(5) . .
S4 Mo23 K3 63.6(2) . .
S3 Mo23 K3 99.5(2) . .
O39 Mo23 K3 151.9(4) . .
Mo22 Mo23 K3 68.96(12) . .
O36 Mo23 K14 99.6(7) . .
O37 Mo23 K14 105.6(6) . .
O38 Mo23 K14 37.1(5) . .
S4 Mo23 K14 151.0(3) . .
S3 Mo23 K14 54.2(4) . .
O39 Mo23 K14 73.4(4) . .
Mo22 Mo23 K14 105.6(3) . .
K3 Mo23 K14 131.1(3) . .
O40 Mo24 O37 97.9(7) . .
O40 Mo24 O38 101.7(7) . .
O37 Mo24 O38 69.9(6) . .
O40 Mo24 O39 167.5(7) . .
O37 Mo24 O39 70.9(6) . .
O38 Mo24 O39 69.7(6) . .
O40 Mo24 S5 103.1(6) . .
O37 Mo24 S5 153.3(5) . .
O38 Mo24 S5 89.7(5) . .
O39 Mo24 S5 86.3(4) . .
O40 Mo24 S34 103.4(6) . .
O37 Mo24 S34 88.5(5) . .
O38 Mo24 S34 148.8(5) . .
O39 Mo24 S34 82.3(4) . .
S5 Mo24 S34 102.3(2) . .
O40 Mo24 Mo25 99.5(6) . .
O37 Mo24 Mo25 139.6(4) . .
O38 Mo24 Mo25 139.8(5) . .
O39 Mo24 Mo25 92.8(4) . .
S5 Mo24 Mo25 52.17(16) . .
S34 Mo24 Mo25 52.07(16) . .
O40 Mo24 K27 97.7(6) . .
O37 Mo24 K27 35.2(5) . .
O38 Mo24 K27 104.4(5) . .
O39 Mo24 K27 76.5(5) . .
S5 Mo24 K27 152.0(3) . .
S34 Mo24 K27 54.1(3) . .
Mo25 Mo24 K27 106.2(2) . .
O42 Mo25 O43 98.9(6) . .
O42 Mo25 O84 91.9(7) . 2_776
O43 Mo25 O84 78.1(5) . 2_776
O42 Mo25 S34 100.3(6) . .
O43 Mo25 S34 87.7(4) . .
O84 Mo25 S34 162.6(4) 2_776 .
O42 Mo25 S5 102.4(6) . .
O43 Mo25 S5 154.3(4) . .
O84 Mo25 S5 87.2(4) 2_776 .
S34 Mo25 S5 102.1(2) . .
O42 Mo25 O41 166.8(7) . .
O43 Mo25 O41 72.3(4) . .
O84 Mo25 O41 76.9(5) 2_776 .
S34 Mo25 O41 89.4(4) . .
S5 Mo25 O41 84.0(3) . .
O42 Mo25 Mo24 96.5(6) . .
O43 Mo25 Mo24 138.9(4) . .
O84 Mo25 Mo24 139.2(4) 2_776 .
S34 Mo25 Mo24 52.06(15) . .
S5 Mo25 Mo24 51.99(17) . .
O41 Mo25 Mo24 96.5(4) . .
O58 Mo26 O56 98.5(6) . .
O58 Mo26 O57 99.4(7) . .
O56 Mo26 O57 69.9(6) . .
O58 Mo26 S2 102.9(6) . .
O56 Mo26 S2 87.3(4) . .
O57 Mo26 S2 150.2(4) . .
O58 Mo26 S21 103.2(6) . .
O56 Mo26 S21 153.1(4) . .
O57 Mo26 S21 90.9(4) . .
S2 Mo26 S21 102.9(2) . .
O58 Mo26 O59 164.1(7) . .
O56 Mo26 O59 68.5(5) . .
O57 Mo26 O59 68.0(5) . .
S2 Mo26 O59 86.2(4) . .
S21 Mo26 O59 87.2(4) . .
O58 Mo26 Mo4 101.9(6) . .
O56 Mo26 Mo4 137.3(4) . .
O57 Mo26 Mo4 140.8(4) . .
S2 Mo26 Mo4 51.82(15) . .
S21 Mo26 Mo4 52.29(16) . .
O59 Mo26 Mo4 94.0(3) . .
O51 Mo27 O50 99.9(6) . .
O51 Mo27 O53 97.8(6) . .
O50 Mo27 O53 76.1(5) . .
O51 Mo27 S15 100.7(5) . .
O50 Mo27 S15 155.0(4) . .
O53 Mo27 S15 87.3(4) . .
O51 Mo27 S14 101.3(5) . .
O50 Mo27 S14 87.4(4) . .
O53 Mo27 S14 156.6(5) . .
S15 Mo27 S14 102.2(2) . .
O51 Mo27 Mo11 95.2(5) . .
O50 Mo27 Mo11 139.1(4) . .
O53 Mo27 Mo11 139.0(4) . .
S15 Mo27 Mo11 52.04(14) . .
S14 Mo27 Mo11 52.35(15) . .
O51 Mo27 K9' 82.5(5) . .
O50 Mo27 K9' 36.4(5) . .
O53 Mo27 K9' 47.4(5) . .
S15 Mo27 K9' 134.2(3) . .
S14 Mo27 K9' 122.2(3) . .
Mo11 Mo27 K9' 173.6(3) . .
O51 Mo27 K15 36.7(6) . 2_675
O50 Mo27 K15 135.5(5) . 2_675
O53 Mo27 K15 96.7(5) . 2_675
S15 Mo27 K15 64.1(4) . 2_675
S14 Mo27 K15 106.7(4) . 2_675
Mo11 Mo27 K15 72.1(3) . 2_675
K9' Mo27 K15 108.7(4) . 2_675
O51 Mo27 K8 39.8(5) . .
O50 Mo27 K8 101.2(4) . .
O53 Mo27 K8 137.2(5) . .
S15 Mo27 K8 103.7(2) . .
S14 Mo27 K8 61.8(2) . .
Mo11 Mo27 K8 68.19(17) . .
K9' Mo27 K8 106.8(3) . .
K15 Mo27 K8 55.0(4) 2_675 .
O13 Mo28 O15 97.3(7) . .
O13 Mo28 O16 98.5(7) . .
O15 Mo28 O16 76.1(5) . .
O13 Mo28 S20 102.7(6) . .
O15 Mo28 S20 155.7(5) . .
O16 Mo28 S20 87.3(4) . .
O13 Mo28 S27 100.3(6) . .
O15 Mo28 S27 87.5(4) . .
O16 Mo28 S27 156.4(5) . .
S20 Mo28 S27 102.3(2) . .
O13 Mo28 Mo29 96.2(5) . .
O15 Mo28 Mo29 139.0(4) . .
O16 Mo28 Mo29 139.3(4) . .
S20 Mo28 Mo29 52.45(15) . .
S27 Mo28 Mo29 52.02(15) . .
O13 Mo28 K9 82.5(5) . .
O15 Mo28 K9 39.3(4) . .
O16 Mo28 K9 43.3(4) . .
S20 Mo28 K9 130.1(2) . .
S27 Mo28 K9 125.9(2) . .
Mo29 Mo28 K9 177.3(2) . .
O13 Mo28 K26 45.2(7) . .
O15 Mo28 K26 93.4(6) . .
O16 Mo28 K26 141.3(6) . .
S20 Mo28 K26 110.6(5) . .
S27 Mo28 K26 55.1(5) . .
Mo29 Mo28 K26 70.0(5) . .
K9 Mo28 K26 107.6(5) . .
O12 Mo29 O9 98.4(7) . .
O12 Mo29 O10 99.7(7) . .
O9 Mo29 O10 70.8(6) . .
O12 Mo29 O11 166.9(6) . .
O9 Mo29 O11 71.7(5) . .
O10 Mo29 O11 69.2(5) . .
O12 Mo29 S27 104.8(6) . .
O9 Mo29 S27 87.9(5) . .
O10 Mo29 S27 149.6(4) . .
O11 Mo29 S27 83.9(4) . .
O12 Mo29 S20 102.0(6) . .
O9 Mo29 S20 153.7(5) . .
O10 Mo29 S20 89.3(4) . .
O11 Mo29 S20 85.4(4) . .
S27 Mo29 S20 102.7(2) . .
O12 Mo29 Mo28 99.3(5) . .
O9 Mo29 Mo28 139.6(4) . .
O10 Mo29 Mo28 139.9(4) . .
O11 Mo29 Mo28 93.9(3) . .
S27 Mo29 Mo28 52.50(15) . .
S20 Mo29 Mo28 52.34(15) . .
O12 Mo29 K4' 64.1(7) . 1_545
O9 Mo29 K4' 53.5(7) . 1_545
O10 Mo29 K4' 45.9(6) . 1_545
O11 Mo29 K4' 102.8(6) . 1_545
S27 Mo29 K4' 134.1(5) . 1_545
S20 Mo29 K4' 122.9(5) . 1_545
Mo28 Mo29 K4' 162.5(5) . 1_545
O12 Mo29 K21 94.7(7) . .
O9 Mo29 K21 31.2(5) . .
O10 Mo29 K21 102.1(5) . .
O11 Mo29 K21 81.3(5) . .
S27 Mo29 K21 58.7(3) . .
S20 Mo29 K21 158.1(3) . .
Mo28 Mo29 K21 111.1(3) . .
K4' Mo29 K21 77.3(6) 1_545 .
O12 Mo29 K26 50.1(7) . .
O9 Mo29 K26 96.1(6) . .
O10 Mo29 K26 146.2(6) . .
O11 Mo29 K26 137.7(6) . .
S27 Mo29 K26 54.7(5) . .
S20 Mo29 K26 109.8(5) . .
Mo28 Mo29 K26 69.1(5) . .
K4' Mo29 K26 101.0(7) 1_545 .
K21 Mo29 K26 70.5(6) . .
O69 Mo30 O68 101.4(6) . .
O69 Mo30 O70 88.8(6) . .
O68 Mo30 O70 78.5(5) . .
O69 Mo30 S19 100.7(5) . .
O68 Mo30 S19 87.0(4) . .
O70 Mo30 S19 164.1(4) . .
O69 Mo30 S9 101.3(5) . .
O68 Mo30 S9 152.7(3) . .
O70 Mo30 S9 87.1(4) . .
S19 Mo30 S9 103.27(19) . .
O69 Mo30 O104 163.6(6) . .
O68 Mo30 O104 70.2(4) . .
O70 Mo30 O104 75.8(4) . .
S19 Mo30 O104 93.1(3) . .
S9 Mo30 O104 83.9(3) . .
O69 Mo30 Mo31 97.3(5) . .
O68 Mo30 Mo31 137.8(3) . .
O70 Mo30 Mo31 139.7(4) . .
S19 Mo30 Mo31 52.25(14) . .
S9 Mo30 Mo31 52.58(14) . .
O104 Mo30 Mo31 98.2(3) . .
O69 Mo30 K7 38.3(5) . .
O68 Mo30 K7 137.9(4) . .
O70 Mo30 K7 87.4(4) . .
S19 Mo30 K7 108.0(2) . .
S9 Mo30 K7 63.09(19) . .
O104 Mo30 K7 143.8(3) . .
Mo31 Mo30 K7 74.20(16) . .
O69 Mo30 K19 50.5(6) . .
O68 Mo30 K19 68.1(4) . .
O70 Mo30 K19 46.8(4) . .
S19 Mo30 K19 132.8(3) . .
S9 Mo30 K19 117.3(3) . .
O104 Mo30 K19 113.3(4) . .
Mo31 Mo30 K19 146.4(3) . .
K7 Mo30 K19 73.4(3) . .
O69 Mo30 K19' 60.1(7) . .
O68 Mo30 K19' 62.5(7) . .
O70 Mo30 K19' 39.9(7) . .
S19 Mo30 K19' 136.5(7) . .
S9 Mo30 K19' 118.1(6) . .
O104 Mo30 K19' 103.6(6) . .
Mo31 Mo30 K19' 155.3(6) . .
K7 Mo30 K19' 81.3(6) . .
O103 Mo31 O99 100.4(6) . .
O103 Mo31 O98 99.3(6) . .
O99 Mo31 O98 69.5(5) . .
O103 Mo31 O102 167.6(6) . .
O99 Mo31 O102 70.1(4) . .
O98 Mo31 O102 70.2(5) . .
O103 Mo31 S19 103.4(5) . .
O99 Mo31 S19 149.3(4) . .
O98 Mo31 S19 87.5(4) . .
O102 Mo31 S19 83.2(3) . .
O103 Mo31 S9 103.0(5) . .
O99 Mo31 S9 90.2(4) . .
O98 Mo31 S9 152.3(4) . .
O102 Mo31 S9 85.5(4) . .
S19 Mo31 S9 102.97(19) . .
O103 Mo31 Mo30 100.9(5) . .
O99 Mo31 Mo30 140.2(4) . .
O98 Mo31 Mo30 138.1(4) . .
O102 Mo31 Mo30 91.5(3) . .
S19 Mo31 Mo30 52.20(14) . .
S9 Mo31 Mo30 52.32(13) . .
O103 Mo31 K7 47.2(5) . .
O99 Mo31 K7 110.4(4) . .
O98 Mo31 K7 146.5(4) . .
O102 Mo31 K7 142.8(4) . .
S19 Mo31 K7 100.04(19) . .
S9 Mo31 K7 57.58(19) . .
Mo30 Mo31 K7 63.88(14) . .
O103 Mo31 K23 97.8(5) . .
O99 Mo31 K23 105.3(5) . .
O98 Mo31 K23 36.1(5) . .
O102 Mo31 K23 77.7(4) . .
S19 Mo31 K23 52.5(3) . .
S9 Mo31 K23 151.3(3) . .
Mo30 Mo31 K23 104.7(3) . .
K7 Mo31 K23 133.2(3) . .
O87 Mo32 O75 92.3(6) . .
O87 Mo32 O72 91.6(6) . .
O75 Mo32 O72 80.9(6) . .
O87 Mo32 S6 102.0(5) . .
O75 Mo32 S6 85.3(5) . .
O72 Mo32 S6 161.0(4) . .
O87 Mo32 S31 102.1(5) . .
O75 Mo32 S31 159.9(4) . .
O72 Mo32 S31 84.7(4) . .
S6 Mo32 S31 105.0(2) . .
O87 Mo32 O110 169.3(6) . .
O75 Mo32 O110 79.5(5) . .
O72 Mo32 O110 80.4(5) . .
S6 Mo32 O110 84.2(4) . .
S31 Mo32 O110 84.4(4) . .
O87 Mo32 Mo10 100.3(5) . .
O75 Mo32 Mo10 138.2(4) . .
O72 Mo32 Mo10 137.6(4) . .
S6 Mo32 Mo10 53.25(17) . .
S31 Mo32 Mo10 53.04(16) . .
O110 Mo32 Mo10 90.4(3) . .
O87 Mo32 K13 28.4(5) . .
O75 Mo32 K13 113.3(5) . .
O72 Mo32 K13 112.9(4) . .
S6 Mo32 K13 84.6(3) . .
S31 Mo32 K13 85.2(3) . .
O110 Mo32 K13 162.2(4) . .
Mo10 Mo32 K13 71.8(2) . .
O76 Mo33 O73 100.6(6) . .
O76 Mo33 O71 100.8(6) . .
O73 Mo33 O71 77.6(5) . .
O76 Mo33 S23 102.9(6) . .
O73 Mo33 S23 152.7(4) . .
O71 Mo33 S23 84.4(4) . .
O76 Mo33 S32 103.2(5) . .
O73 Mo33 S32 84.2(4) . .
O71 Mo33 S32 152.1(4) . .
S23 Mo33 S32 103.7(2) . .
O76 Mo33 Mo34 103.2(5) . .
O73 Mo33 Mo34 133.9(4) . .
O71 Mo33 Mo34 134.0(4) . .
S23 Mo33 Mo34 52.31(14) . .
S32 Mo33 Mo34 52.30(16) . .
O77 Mo34 O78 97.2(6) . .
O77 Mo34 O79 99.2(7) . .
O78 Mo34 O79 70.8(5) . .
O77 Mo34 O80 168.0(6) . .
O78 Mo34 O80 72.8(5) . .
O79 Mo34 O80 71.6(5) . .
O77 Mo34 S23 103.0(5) . .
O78 Mo34 S23 153.0(4) . .
O79 Mo34 S23 88.3(4) . .
O80 Mo34 S23 84.8(4) . .
O77 Mo34 S32 102.7(6) . .
O78 Mo34 S32 89.2(4) . .
O79 Mo34 S32 152.0(4) . .
O80 Mo34 S32 84.0(4) . .
S23 Mo34 S32 103.4(2) . .
O77 Mo34 Mo33 102.9(5) . .
O78 Mo34 Mo33 139.4(4) . .
O79 Mo34 Mo33 137.9(4) . .
O80 Mo34 Mo33 89.1(3) . .
S23 Mo34 Mo33 52.05(15) . .
S32 Mo34 Mo33 52.25(15) . .
O77 Mo34 Mo16 121.9(5) . .
O78 Mo34 Mo16 40.8(4) . .
O79 Mo34 Mo16 40.9(4) . .
O80 Mo34 Mo16 46.1(3) . .
S23 Mo34 Mo16 112.35(16) . .
S32 Mo34 Mo16 111.55(17) . .
Mo33 Mo34 Mo16 135.24(8) . .
O77 Mo34 K3 56.1(5) . 1_665
O78 Mo34 K3 52.1(4) . 1_665
O79 Mo34 K3 56.0(4) . 1_665
O80 Mo34 K3 111.8(3) . 1_665
S23 Mo34 K3 128.65(18) . 1_665
S32 Mo34 K3 125.72(19) . 1_665
Mo33 Mo34 K3 158.97(13) . 1_665
Mo16 Mo34 K3 65.74(12) . 1_665
O77 Mo34 K16 106.2(6) . .
O78 Mo34 K16 104.5(5) . .
O79 Mo34 K16 35.6(4) . .
O80 Mo34 K16 71.0(4) . .
S23 Mo34 K16 52.7(3) . .
S32 Mo34 K16 145.9(3) . .
Mo33 Mo34 K16 103.2(2) . .
Mo16 Mo34 K16 66.9(2) . .
K3 Mo34 K16 86.0(3) 1_665 .
O26 Se1 O27 97.8(6) . .
O26 Se1 O28 98.1(6) . .
O27 Se1 O28 100.7(6) . .
O26 Se1 K5 80.6(4) . .
O27 Se1 K5 37.0(5) . .
O28 Se1 K5 71.0(4) . .
O111 Se2 O16 102.1(9) . .
O111 Se2 O17 99.6(9) . .
O16 Se2 O17 96.6(7) . .
O111 Se2 K24' 73.7(12) . .
O16 Se2 K24' 137.8(10) . .
O17 Se2 K24' 125.5(11) . .
O111 Se2 K9' 87.6(8) . .
O16 Se2 K9' 63.1(5) . .
O17 Se2 K9' 38.9(6) . .
K24' Se2 K9' 153.9(10) . .
O111 Se2 K9" 78.0(10) . .
O16 Se2 K9" 68.3(7) . .
O17 Se2 K9" 40.5(7) . .
O44 Se3 O43 102.0(6) . .
O44 Se3 O45 96.2(6) . .
O43 Se3 O45 99.0(6) . .
O44 Se3 K5 45.0(4) . .
O43 Se3 K5 78.8(4) . .
O45 Se3 K5 62.5(4) . .
O49 Se4 O48 103.2(8) . .
O49 Se4 O50 103.5(8) . .
O48 Se4 O50 94.7(7) . .
O49 Se4 K9" 90.9(9) . .
O48 Se4 K9" 53.6(7) . .
O50 Se4 K9" 46.7(7) . .
O49 Se4 K9' 100.8(7) . .
O48 Se4 K9' 54.8(6) . .
O50 Se4 K9' 41.2(5) . .
O25 Se5 O24 95.1(6) . .
O25 Se5 O91 99.5(6) . .
O24 Se5 O91 101.5(6) . .
O25 Se5 K2 63.2(4) . .
O24 Se5 K2 46.5(4) . .
O91 Se5 K2 75.0(4) . .
O68 Se6 O67 98.8(6) . .
O68 Se6 O23 101.0(6) . .
O67 Se6 O23 99.0(6) . .
O68 Se6 K2 69.7(4) . .
O67 Se6 K2 82.7(4) . .
O23 Se6 K2 38.2(4) . .
O18 Se7 O15 102.3(8) . .
O18 Se7 O19 101.4(6) . .
O15 Se7 O19 95.6(6) . .
O18 Se7 K9 101.1(6) . .
O15 Se7 K9 39.9(5) . .
O19 Se7 K9 56.4(5) . .
O18 Se7 K21 39.9(6) . 2_765
O15 Se7 K21 107.3(6) . 2_765
O19 Se7 K21 137.7(5) . 2_765
K9 Se7 K21 130.7(4) . 2_765
O54 Se8 O53 104.1(8) . .
O54 Se8 O20 100.9(7) . .
O53 Se8 O20 96.6(6) . .
O54 Se8 K9 93.3(7) . .
O53 Se8 K9 60.4(5) . .
O20 Se8 K9 39.9(5) . .
O80 Se9 O110 99.6(7) . .
O80 Se9 O109 100.5(7) . .
O110 Se9 O109 105.1(6) . .
O90 Se10 O89 96.5(6) . .
O90 Se10 O86 102.3(6) . .
O89 Se10 O86 97.9(6) . .
O90 Se10 K12 85.9(5) . .
O89 Se10 K12 53.9(5) . .
O86 Se10 K12 49.2(5) . .
O84 Se11 O85 96.9(6) . .
O84 Se11 O83 101.4(6) . .
O85 Se11 O83 96.5(7) . .
O84 Se11 K12 84.1(5) . .
O85 Se11 K12 53.0(5) . .
O83 Se11 K12 49.5(5) . .
O74 Se12 O73 101.2(6) . .
O74 Se12 O75 96.1(7) . .
O73 Se12 O75 99.1(7) . .
O70 Se13 O72 95.0(6) . .
O70 Se13 O71 100.5(6) . .
O72 Se13 O71 97.6(7) . .
Mo21 S1 Mo20 75.39(19) . .
Mo21 S1 K24 91.9(4) . .
Mo20 S1 K24 166.5(4) . .
Mo4 S2 Mo26 76.27(19) . .
Mo4 S2 K15 149.5(4) . .
Mo26 S2 K15 113.3(4) . .
Mo23 S3 Mo22 76.4(2) . .
Mo23 S3 K14 91.2(4) . .
Mo22 S3 K14 165.3(4) . .
Mo23 S3 K22 165.2(4) . .
Mo22 S3 K22 91.4(4) . .
K14 S3 K22 99.6(5) . .
Mo23 S4 Mo22 76.5(2) . .
Mo23 S4 K24 163.6(4) . .
Mo22 S4 K24 91.5(4) . .
Mo23 S4 K27 92.2(4) . .
Mo22 S4 K27 162.9(4) . .
K24 S4 K27 96.8(4) . .
Mo23 S4 K3 81.1(2) . .
Mo22 S4 K3 81.2(2) . .
K24 S4 K3 108.4(4) . .
K27 S4 K3 110.0(3) . .
Mo24 S5 Mo25 75.84(19) . .
Mo24 S5 K14 88.8(4) . .
Mo25 S5 K14 158.6(4) . .
Mo10 S6 Mo32 73.4(2) . .
Mo10 S6 K5 129.4(3) . 2_776
Mo32 S6 K5 126.1(3) . 2_776
Mo9 S7 Mo5 74.67(16) . .
Mo13 S8 Mo1 74.66(15) . .
Mo30 S9 Mo31 75.11(16) . .
Mo30 S9 K7 80.0(2) . .
Mo31 S9 K7 87.7(2) . .
Mo12 S10 Mo3 75.14(17) . .
Mo12 S10 K20 89.9(4) . .
Mo3 S10 K20 164.4(4) . .
Mo12 S10 K11 95.3(3) . 2_776
Mo3 S10 K11 90.1(3) . 2_776
K20 S10 K11 86.9(4) . 2_776
Mo5 S11 Mo9 74.67(16) . .
Mo5 S11 K27 88.9(4) . .
Mo9 S11 K27 108.6(4) . .
Mo7 S12 Mo2 76.03(16) . .
Mo7 S12 K19 86.4(3) . .
Mo2 S12 K19 89.7(3) . .
Mo7 S12 K19' 90.3(7) . .
Mo2 S12 K19' 81.8(7) . .
Mo14 S13 Mo6 76.11(17) . .
Mo14 S13 K16 121.6(3) . .
Mo6 S13 K16 123.9(3) . .
Mo14 S13 K1 84.47(17) . 2_775
Mo6 S13 K1 80.86(17) . 2_775
K16 S13 K1 145.9(3) . 2_775
Mo14 S13 K18 153.9(4) . .
Mo6 S13 K18 114.7(4) . .
K16 S13 K18 73.6(5) . .
K1 S13 K18 74.6(4) 2_775 .
Mo11 S14 Mo27 74.70(18) . .
Mo11 S14 K8 81.8(2) . .
Mo27 S14 K8 83.7(3) . .
Mo11 S15 Mo27 75.51(18) . .
Mo11 S15 K15 84.8(4) . 2_675
Mo27 S15 K15 81.5(4) . 2_675
Mo17 S16 Mo16 76.02(18) . .
Mo17 S16 K16 159.4(4) . .
Mo16 S16 K16 92.9(4) . .
Mo2 S17 Mo7 75.03(16) . .
Mo8 S18 Mo15 75.65(17) . .
Mo30 S19 Mo31 75.54(17) . .
Mo30 S19 K23 168.4(4) . .
Mo31 S19 K23 93.3(3) . .
Mo28 S20 Mo29 75.2(2) . .
Mo28 S20 K24' 134.7(9) . .
Mo29 S20 K24' 139.8(9) . .
Mo26 S21 Mo4 75.55(18) . .
Mo8 S22 Mo15 76.13(16) . .
Mo33 S23 Mo34 75.64(18) . .
Mo33 S23 K16 159.8(4) . .
Mo34 S23 K16 93.1(3) . .
Mo6 S24 Mo14 76.54(17) . .
Mo6 S24 K1 142.2(2) . .
Mo14 S24 K1 128.2(2) . .
Mo6 S24 K23 89.7(3) . .
Mo14 S24 K23 163.3(3) . .
K1 S24 K23 68.4(3) . .
Mo13 S25 Mo1 74.33(15) . .
Mo12 S26 Mo3 75.27(18) . .
Mo12 S26 K25 90.9(7) . .
Mo3 S26 K25 166.0(8) . .
Mo29 S27 Mo28 75.5(2) . .
Mo29 S27 K26 90.8(6) . .
Mo28 S27 K26 89.8(6) . .
Mo29 S27 K21 140.5(4) . 2_765
Mo28 S27 K21 128.6(4) . 2_765
K26 S27 K21 62.5(7) . 2_765
Mo29 S27 K21 86.7(3) . .
Mo28 S27 K21 161.9(4) . .
K26 S27 K21 87.3(7) . .
K21 S27 K21 64.9(5) 2_765 .
Mo17 S28 Mo16 75.86(19) . .
Mo21 S29 Mo20 75.32(19) . .
Mo21 S29 K6 84.1(4) . .
Mo20 S29 K6 81.8(4) . .
Mo21 S29 K22 89.1(3) . .
Mo20 S29 K22 160.3(4) . .
K6 S29 K22 108.9(5) . .
Mo19 S30 Mo18 76.1(2) . .
Mo19 S30 K7 152.4(3) . 1_545
Mo18 S30 K7 129.0(3) . 1_545
Mo19 S30 K20 87.6(3) . .
Mo18 S30 K20 161.3(3) . .
K7 S30 K20 69.0(4) 1_545 .
Mo10 S31 Mo32 73.5(2) . .
Mo10 S31 K2 130.9(3) . .
Mo32 S31 K2 130.4(3) . .
Mo33 S32 Mo34 75.45(18) . .
Mo18 S33 Mo19 75.6(2) . .
Mo18 S33 K21 84.6(4) . .
Mo19 S33 K21 160.2(4) . .
Mo24 S34 Mo25 75.87(19) . .
Mo24 S34 K27 91.7(3) . .
Mo25 S34 K27 167.4(4) . .
O124 K1 O122 118.7(7) . .
O124 K1 O106 107.0(5) . .
O122 K1 O106 72.9(5) . .
O124 K1 O97 80.7(5) . 2_775
O122 K1 O97 135.5(5) . 2_775
O106 K1 O97 143.6(4) . 2_775
O124 K1 O114 77.9(5) . .
O122 K1 O114 145.2(6) . .
O106 K1 O114 73.0(4) . .
O97 K1 O114 74.0(4) 2_775 .
O124 K1 O96 139.6(5) . 2_775
O122 K1 O96 63.4(5) . 2_775
O106 K1 O96 111.4(4) . 2_775
O97 K1 O96 76.2(4) 2_775 2_775
O114 K1 O96 125.1(4) . 2_775
O124 K1 S24 138.0(5) . .
O122 K1 S24 102.9(6) . .
O106 K1 S24 79.2(3) . .
O97 K1 S24 72.7(3) 2_775 .
O114 K1 S24 64.0(3) . .
O96 K1 S24 63.5(3) 2_775 .
O124 K1 S13 82.0(4) . 2_775
O122 K1 S13 82.9(5) . 2_775
O106 K1 S13 155.7(3) . 2_775
O97 K1 S13 59.1(3) 2_775 2_775
O114 K1 S13 131.3(3) . 2_775
O96 K1 S13 57.7(3) 2_775 2_775
S24 K1 S13 109.58(18) . 2_775
O124 K1 Mo6 84.1(4) . 2_775
O122 K1 Mo6 113.9(4) . 2_775
O106 K1 Mo6 162.7(3) . 2_775
O97 K1 Mo6 23.2(3) 2_775 2_775
O114 K1 Mo6 97.2(3) . 2_775
O96 K1 Mo6 62.2(2) 2_775 2_775
S24 K1 Mo6 83.73(14) . 2_775
S13 K1 Mo6 36.51(10) 2_775 2_775
O124 K1 K23 151.4(5) . .
O122 K1 K23 49.0(6) . .
O106 K1 K23 47.4(4) . .
O97 K1 K23 127.0(4) 2_775 .
O114 K1 K23 101.1(4) . .
O96 K1 K23 64.0(4) 2_775 .
S24 K1 K23 59.1(3) . .
S13 K1 K23 116.6(3) 2_775 .
Mo6 K1 K23 124.0(3) 2_775 .
O124 K1 Mo14 116.7(4) . 2_775
O122 K1 Mo14 73.8(4) . 2_775
O106 K1 Mo14 134.0(3) . 2_775
O97 K1 Mo14 61.8(3) 2_775 2_775
O114 K1 Mo14 128.6(3) . 2_775
O96 K1 Mo14 23.1(2) 2_775 2_775
S24 K1 Mo14 78.22(13) . 2_775
S13 K1 Mo14 35.49(10) 2_775 2_775
Mo6 K1 Mo14 42.82(6) 2_775 2_775
K23 K1 Mo14 86.6(3) . 2_775
O124 K1 K18 38.0(5) . 2_775
O122 K1 K18 87.8(6) . 2_775
O106 K1 K18 120.9(4) . 2_775
O97 K1 K18 87.5(4) 2_775 2_775
O114 K1 K18 115.7(4) . 2_775
O96 K1 K18 107.8(4) 2_775 2_775
S24 K1 K18 159.6(3) . 2_775
S13 K1 K18 53.9(3) 2_775 2_775
Mo6 K1 K18 76.0(3) 2_775 2_775
K23 K1 K18 136.1(4) . 2_775
Mo14 K1 K18 88.4(3) 2_775 2_775
O24 K2 O23 55.2(4) . .
O24 K2 O120 94.8(5) . .
O23 K2 O120 71.7(4) . .
O24 K2 O117 142.5(4) . .
O23 K2 O117 87.6(4) . .
O120 K2 O117 75.2(5) . .
O24 K2 O121 95.1(4) . .
O23 K2 O121 147.1(5) . .
O120 K2 O121 100.6(5) . .
O117 K2 O121 122.1(5) . .
O24 K2 S31 132.3(3) . .
O23 K2 S31 139.2(4) . .
O120 K2 S31 131.8(4) . .
O117 K2 S31 71.9(4) . .
O121 K2 S31 69.9(4) . .
O24 K2 O25 47.8(3) . .
O23 K2 O25 85.6(4) . .
O120 K2 O25 69.5(4) . .
O117 K2 O25 144.4(4) . .
O121 K2 O25 62.2(4) . .
S31 K2 O25 131.0(3) . .
O24 K2 O104 85.5(4) . .
O23 K2 O104 66.9(4) . .
O120 K2 O104 128.8(4) . .
O117 K2 O104 74.4(4) . .
O121 K2 O104 130.5(4) . .
S31 K2 O104 73.6(3) . .
O25 K2 O104 133.0(4) . .
O24 K2 O100 60.1(3) . .
O23 K2 O100 96.3(4) . .
O120 K2 O100 154.0(4) . .
O117 K2 O100 128.6(4) . .
O121 K2 O100 76.7(4) . .
S31 K2 O100 72.3(3) . .
O25 K2 O100 87.0(3) . .
O104 K2 O100 60.8(3) . .
O24 K2 Se5 26.1(2) . .
O23 K2 Se5 78.4(3) . .
O120 K2 Se5 92.5(4) . .
O117 K2 Se5 163.7(4) . .
O121 K2 Se5 69.9(3) . .
S31 K2 Se5 124.2(2) . .
O25 K2 Se5 27.4(2) . .
O104 K2 Se5 106.9(3) . .
O100 K2 Se5 62.0(2) . .
O24 K2 Se6 77.2(3) . .
O23 K2 Se6 22.4(2) . .
O120 K2 Se6 69.7(3) . .
O117 K2 Se6 65.3(3) . .
O121 K2 Se6 166.7(4) . .
S31 K2 Se6 123.2(2) . .
O25 K2 Se6 105.1(3) . .
O104 K2 Se6 60.5(2) . .
O100 K2 Se6 107.8(3) . .
Se5 K2 Se6 100.74(14) . .
O24 K2 Mo1 27.4(2) . .
O23 K2 Mo1 27.9(2) . .
O120 K2 Mo1 83.8(4) . .
O117 K2 Mo1 115.2(4) . .
O121 K2 Mo1 121.7(4) . .
S31 K2 Mo1 142.4(2) . .
O25 K2 Mo1 65.7(2) . .
O104 K2 Mo1 73.5(2) . .
O100 K2 Mo1 76.2(2) . .
Se5 K2 Mo1 51.78(9) . .
Se6 K2 Mo1 49.90(8) . .
O179 K3 O139 90.0(14) . .
O179 K3 O36 160.5(13) . .
O139 K3 O36 79.4(8) . .
O179 K3 O35 101.4(13) . .
O139 K3 O35 135.6(8) . .
O36 K3 O35 75.9(5) . .
O179 K3 O78 118.3(12) . 1_445
O139 K3 O78 132.6(8) . 1_445
O36 K3 O78 80.4(5) . 1_445
O35 K3 O78 78.5(4) . 1_445
O179 K3 O79 81.3(12) . 1_445
O139 K3 O79 108.1(8) . 1_445
O36 K3 O79 117.4(5) . 1_445
O35 K3 O79 116.0(4) . 1_445
O78 K3 O79 48.1(4) 1_445 1_445
O179 K3 O77 126.7(12) . 1_445
O139 K3 O77 75.8(8) . 1_445
O36 K3 O77 66.7(4) . 1_445
O35 K3 O77 124.7(5) . 1_445
O78 K3 O77 56.8(4) 1_445 1_445
O79 K3 O77 56.6(4) 1_445 1_445
O179 K3 O81 67.6(12) . 1_445
O139 K3 O81 152.8(8) . 1_445
O36 K3 O81 126.3(5) . 1_445
O35 K3 O81 67.0(4) . 1_445
O78 K3 O81 55.7(4) 1_445 1_445
O79 K3 O81 55.2(4) 1_445 1_445
O77 K3 O81 104.6(4) 1_445 1_445
O179 K3 S4 104.9(12) . .
O139 K3 S4 78.7(7) . .
O36 K3 S4 57.1(3) . .
O35 K3 S4 56.9(3) . .
O78 K3 S4 122.9(4) 1_445 .
O79 K3 S4 171.0(4) 1_445 .
O77 K3 S4 121.4(4) 1_445 .
O81 K3 S4 120.7(3) 1_445 .
O179 K3 Mo34 115.6(12) . 1_445
O139 K3 Mo34 100.3(7) . 1_445
O36 K3 Mo34 82.7(4) . 1_445
O35 K3 Mo34 112.4(4) . 1_445
O78 K3 Mo34 34.6(3) 1_445 1_445
O79 K3 Mo34 34.9(3) 1_445 1_445
O77 K3 Mo34 27.2(3) 1_445 1_445
O81 K3 Mo34 77.5(3) 1_445 1_445
S4 K3 Mo34 139.5(3) . 1_445
O179 K3 Mo16 84.1(12) . 1_445
O139 K3 Mo16 142.6(7) . 1_445
O36 K3 Mo16 114.2(4) . 1_445
O35 K3 Mo16 81.7(3) . 1_445
O78 K3 Mo16 34.3(3) 1_445 1_445
O79 K3 Mo16 34.5(3) 1_445 1_445
O77 K3 Mo16 78.4(3) 1_445 1_445
O81 K3 Mo16 26.3(2) 1_445 1_445
S4 K3 Mo16 138.5(2) . 1_445
Mo34 K3 Mo16 51.20(9) 1_445 1_445
O179 K3 Mo23 140.2(12) . .
O139 K3 Mo23 82.4(7) . .
O36 K3 Mo23 22.6(3) . .
O35 K3 Mo23 61.4(4) . .
O78 K3 Mo23 94.5(3) 1_445 .
O79 K3 Mo23 138.1(4) 1_445 .
O77 K3 Mo23 89.3(3) 1_445 .
O81 K3 Mo23 124.7(3) 1_445 .
S4 K3 Mo23 35.26(14) . .
Mo34 K3 Mo23 104.22(19) 1_445 .
Mo16 K3 Mo23 124.01(19) 1_445 .
O123 K4 O116 146.9(7) . .
O123 K4 O153 65.2(9) . .
O116 K4 O153 81.7(9) . .
O123 K4 O97 72.0(6) . .
O116 K4 O97 131.6(5) . .
O153 K4 O97 123.4(9) . .
O123 K4 O96 143.3(7) . 2_775
O116 K4 O96 62.0(4) . 2_775
O153 K4 O96 132.5(9) . 2_775
O97 K4 O96 72.2(4) . 2_775
O123 K4 O94 121.9(7) . 2_775
O116 K4 O94 88.0(5) . 2_775
O153 K4 O94 153.5(9) . 2_775
O97 K4 O94 81.4(4) . 2_775
O96 K4 O94 59.5(4) 2_775 2_775
O123 K4 O98 69.3(6) . .
O116 K4 O98 101.3(5) . .
O153 K4 O98 72.1(8) . .
O97 K4 O98 58.9(4) . .
O96 K4 O98 85.5(4) 2_775 .
O94 K4 O98 134.2(5) 2_775 .
O123 K4 O144 78.9(8) . 2_675
O116 K4 O144 97.1(8) . 2_675
O153 K4 O144 81.2(10) . 2_675
O97 K4 O144 125.1(8) . 2_675
O96 K4 O144 129.8(7) 2_775 2_675
O94 K4 O144 75.9(7) 2_775 2_675
O98 K4 O144 144.7(7) . 2_675
O123 K4 Mo14 143.0(6) . 2_775
O116 K4 Mo14 69.9(3) . 2_775
O153 K4 Mo14 151.2(8) . 2_775
O97 K4 Mo14 75.5(3) . 2_775
O96 K4 Mo14 25.5(2) 2_775 2_775
O94 K4 Mo14 34.0(3) 2_775 2_775
O98 K4 Mo14 108.0(3) . 2_775
O144 K4 Mo14 106.5(7) 2_675 2_775
O123 K4 Mo6 70.3(5) . .
O116 K4 Mo6 119.9(4) . .
O153 K4 Mo6 103.1(8) . .
O97 K4 Mo6 25.1(3) . .
O96 K4 Mo6 73.9(3) 2_775 .
O94 K4 Mo6 103.2(4) 2_775 .
O98 K4 Mo6 34.0(3) . .
O144 K4 Mo6 143.1(7) 2_675 .
Mo14 K4 Mo6 87.44(19) 2_775 .
O123 K4 K23 107.6(6) . .
O116 K4 K23 57.8(5) . .
O153 K4 K23 70.7(8) . .
O97 K4 K23 89.8(4) . .
O96 K4 K23 64.5(4) 2_775 .
O94 K4 K23 123.3(4) 2_775 .
O98 K4 K23 43.6(4) . .
O144 K4 K23 144.0(8) 2_675 .
Mo14 K4 K23 89.5(3) 2_775 .
Mo6 K4 K23 67.6(3) . .
O123 K4 K8 67.7(5) . 2_675
O116 K4 K8 88.8(4) . 2_675
O153 K4 K8 43.1(8) . 2_675
O97 K4 K8 138.7(4) . 2_675
O96 K4 K8 148.9(4) 2_775 2_675
O94 K4 K8 112.8(4) 2_775 2_675
O98 K4 K8 112.2(4) . 2_675
O144 K4 K8 38.1(7) 2_675 2_675
Mo14 K4 K8 137.4(3) 2_775 2_675
Mo6 K4 K8 134.7(3) . 2_675
K23 K4 K8 110.2(4) . 2_675
O156 K4' O8 116.9(15) 2_775 1_565
O156 K4' O10 110.2(13) 2_775 1_565
O8 K4' O10 63.9(8) 1_565 1_565
O156 K4' O99 149.6(15) 2_775 .
O8 K4' O99 61.7(8) 1_565 .
O10 K4' O99 96.4(10) 1_565 .
O156 K4' O97 94.7(12) 2_775 .
O8 K4' O97 102.2(10) 1_565 .
O10 K4' O97 154.8(13) 1_565 .
O99 K4' O97 58.6(7) . .
O156 K4' O9 72.2(11) 2_775 1_565
O8 K4' O9 58.2(8) 1_565 1_565
O10 K4' O9 49.2(6) 1_565 1_565
O99 K4' O9 119.2(11) . 1_565
O97 K4' O9 143.1(13) . 1_565
O156 K4' O202 71.9(15) 2_775 .
O8 K4' O202 171.2(17) 1_565 .
O10 K4' O202 114.1(15) 1_565 .
O99 K4' O202 111.1(15) . .
O97 K4' O202 76.3(12) . .
O9 K4' O202 127.8(14) 1_565 .
O156 K4' Mo18 108.6(13) 2_775 1_565
O8 K4' Mo18 28.4(4) 1_565 1_565
O10 K4' Mo18 38.2(5) 1_565 1_565
O99 K4' Mo18 83.1(8) . 1_565
O97 K4' Mo18 130.6(11) . 1_565
O9 K4' Mo18 37.4(5) 1_565 1_565
O202 K4' Mo18 151.8(14) . 1_565
O156 K4' Mo6 120.0(12) 2_775 .
O8 K4' Mo6 87.9(8) 1_565 .
O10 K4' Mo6 129.4(11) 1_565 .
O99 K4' Mo6 34.0(4) . .
O97 K4' Mo6 25.4(4) . .
O9 K4' Mo6 143.9(11) 1_565 .
O202 K4' Mo6 87.5(12) . .
Mo18 K4' Mo6 114.1(8) 1_565 .
O156 K4' Mo29 76.9(10) 2_775 1_565
O8 K4' Mo29 80.9(8) 1_565 1_565
O10 K4' Mo29 33.4(5) 1_565 1_565
O99 K4' Mo29 129.0(10) . 1_565
O97 K4' Mo29 171.5(11) . 1_565
O9 K4' Mo29 33.2(4) 1_565 1_565
O202 K4' Mo29 101.8(13) . 1_565
Mo18 K4' Mo29 52.9(4) 1_565 1_565
Mo6 K4' Mo29 162.8(10) . 1_565
O156 K4' K8 81.1(11) 2_775 2_675
O8 K4' K8 131.9(10) 1_565 2_675
O10 K4' K8 68.0(7) 1_565 2_675
O99 K4' K8 123.9(10) . 2_675
O97 K4' K8 121.4(10) . 2_675
O9 K4' K8 91.3(8) 1_565 2_675
O202 K4' K8 46.6(11) . 2_675
Mo18 K4' K8 105.2(7) 1_565 2_675
Mo6 K4' K8 123.0(8) . 2_675
Mo29 K4' K8 59.1(5) 1_565 2_675
O156 K4' K1 74.2(10) 2_775 2_775
O8 K4' K1 87.7(8) 1_565 2_775
O10 K4' K1 150.4(11) 1_565 2_775
O99 K4' K1 75.3(7) . 2_775
O97 K4' K1 33.8(4) . 2_775
O9 K4' K1 109.9(9) 1_565 2_775
O202 K4' K1 95.3(12) . 2_775
Mo18 K4' K1 112.2(8) 1_565 2_775
Mo6 K4' K1 51.8(4) . 2_775
Mo29 K4' K1 139.7(9) 1_565 2_775
K8 K4' K1 140.1(7) 2_675 2_775
O44 K5 O27 56.5(4) . .
O44 K5 O118 142.8(5) . .
O27 K5 O118 86.8(4) . .
O44 K5 O120 96.8(5) . .
O27 K5 O120 72.2(4) . .
O118 K5 O120 75.0(5) . .
O44 K5 O152 93.0(7) . 2_776
O27 K5 O152 147.1(8) . 2_776
O118 K5 O152 124.2(8) . 2_776
O120 K5 O152 103.0(8) . 2_776
O44 K5 S6 127.1(4) . 2_776
O27 K5 S6 137.2(4) . 2_776
O118 K5 S6 74.5(4) . 2_776
O120 K5 S6 135.0(4) . 2_776
O152 K5 S6 69.3(7) 2_776 2_776
O44 K5 O185 121.1(11) . 2_776
O27 K5 O185 139.9(11) . 2_776
O118 K5 O185 90.1(11) . 2_776
O120 K5 O185 68.5(11) . 2_776
O152 K5 O185 43.0(12) 2_776 2_776
S6 K5 O185 79.4(10) 2_776 2_776
O44 K5 O45 49.2(4) . .
O27 K5 O45 89.7(4) . .
O118 K5 O45 147.6(5) . .
O120 K5 O45 73.3(4) . .
O152 K5 O45 58.5(7) 2_776 .
S6 K5 O45 126.0(3) 2_776 .
O185 K5 O45 72.3(10) 2_776 .
O44 K5 O29 83.4(4) . .
O27 K5 O29 65.7(4) . .
O118 K5 O29 75.0(4) . .
O120 K5 O29 128.9(4) . .
O152 K5 O29 128.1(7) 2_776 .
S6 K5 O29 72.3(3) 2_776 .
O185 K5 O29 150.6(11) 2_776 .
O45 K5 O29 131.8(4) . .
O44 K5 O41 58.5(4) . .
O27 K5 O41 94.6(4) . .
O118 K5 O41 126.6(5) . .
O120 K5 O41 155.0(5) . .
O152 K5 O41 76.4(7) 2_776 .
S6 K5 O41 68.8(3) 2_776 .
O185 K5 O41 118.6(11) 2_776 .
O45 K5 O41 85.8(3) . .
O29 K5 O41 57.7(4) . .
O44 K5 Se3 25.9(3) . .
O27 K5 Se3 79.7(3) . .
O118 K5 Se3 165.2(4) . .
O120 K5 Se3 95.0(4) . .
O152 K5 Se3 68.2(7) 2_776 .
S6 K5 Se3 119.7(2) 2_776 .
O185 K5 Se3 96.4(10) 2_776 .
O45 K5 Se3 27.9(2) . .
O29 K5 Se3 104.3(3) . .
O41 K5 Se3 61.1(2) . .
O44 K5 Se1 78.2(3) . .
O27 K5 Se1 22.1(3) . .
O118 K5 Se1 64.8(3) . .
O120 K5 Se1 69.9(3) . .
O152 K5 Se1 167.6(7) 2_776 .
S6 K5 Se1 122.9(2) 2_776 .
O185 K5 Se1 135.6(10) 2_776 .
O45 K5 Se1 109.2(3) . .
O29 K5 Se1 60.1(2) . .
O41 K5 Se1 105.6(3) . .
Se3 K5 Se1 101.79(15) . .
O178 K6 O30 76.4(12) . .
O178 K6 O182 165.8(18) . 1_545
O30 K6 O182 114.5(14) . 1_545
O178 K6 O31 127.9(12) . .
O30 K6 O31 67.6(6) . .
O182 K6 O31 54.6(12) 1_545 .
O178 K6 O178 59.3(16) . 2_766
O30 K6 O178 105.4(12) . 2_766
O182 K6 O178 122.4(16) 1_545 2_766
O31 K6 O178 165.1(13) . 2_766
O178 K6 S29 72.8(11) . .
O30 K6 S29 55.9(5) . .
O182 K6 S29 105.1(13) 1_545 .
O31 K6 S29 56.2(5) . .
O178 K6 S29 131.8(12) 2_766 .
O178 K6 K20 107.1(12) . .
O30 K6 K20 54.7(5) . .
O182 K6 K20 87.1(13) 1_545 .
O31 K6 K20 81.6(7) . .
O178 K6 K20 83.7(11) 2_766 .
S29 K6 K20 107.9(6) . .
O178 K6 Mo20 74.4(11) . .
O30 K6 Mo20 20.9(3) . .
O182 K6 Mo20 112.3(13) 1_545 .
O31 K6 Mo20 58.5(4) . .
O178 K6 Mo20 119.1(11) 2_766 .
S29 K6 Mo20 35.1(2) . .
K20 K6 Mo20 74.0(4) . .
O178 K6 Mo21 105.8(11) . .
O30 K6 Mo21 56.1(5) . .
O182 K6 Mo21 75.5(12) 1_545 .
O31 K6 Mo21 22.2(3) . .
O178 K6 Mo21 160.2(11) 2_766 .
S29 K6 Mo21 34.4(2) . .
K20 K6 Mo21 89.3(5) . .
Mo20 K6 Mo21 41.1(2) . .
O178 K6 K11 78.3(11) . 1_545
O30 K6 K11 153.8(9) . 1_545
O182 K6 K11 91.6(12) 1_545 1_545
O31 K6 K11 135.9(8) . 1_545
O178 K6 K11 54.7(10) 2_766 1_545
S29 K6 K11 121.7(6) . 1_545
K20 K6 K11 128.8(7) . 1_545
Mo20 K6 K11 149.1(7) . 1_545
Mo21 K6 K11 139.6(6) . 1_545
O119 K7 O112 156.7(8) 1_565 .
O119 K7 O69 84.2(6) 1_565 .
O112 K7 O69 119.1(7) . .
O119 K7 O141 74.6(8) 1_565 .
O112 K7 O141 86.3(8) . .
O69 K7 O141 140.8(7) . .
O119 K7 O145 71.8(11) 1_565 .
O112 K7 O145 116.6(9) . .
O69 K7 O145 66.8(8) . .
O141 K7 O145 75.3(9) . .
O119 K7 O103 133.0(7) 1_565 .
O112 K7 O103 62.2(6) . .
O69 K7 O103 68.9(4) . .
O141 K7 O103 147.3(7) . .
O145 K7 O103 125.0(8) . .
O119 K7 S30 91.1(8) 1_565 1_565
O112 K7 S30 71.5(5) . 1_565
O69 K7 S30 136.3(4) . 1_565
O141 K7 S30 77.7(6) . 1_565
O145 K7 S30 151.0(8) . 1_565
O103 K7 S30 83.8(4) . 1_565
O119 K7 S9 76.9(7) 1_565 .
O112 K7 S9 112.6(6) . .
O69 K7 S9 59.5(3) . .
O141 K7 S9 141.1(7) . .
O145 K7 S9 119.5(8) . .
O103 K7 S9 56.4(3) . .
S30 K7 S9 77.0(2) 1_565 .
O119 K7 Mo30 80.2(5) 1_565 .
O112 K7 Mo30 120.6(6) . .
O69 K7 Mo30 22.7(3) . .
O141 K7 Mo30 152.7(7) . .
O145 K7 Mo30 86.9(7) . .
O103 K7 Mo30 60.0(3) . .
S30 K7 Mo30 113.7(3) 1_565 .
S9 K7 Mo30 36.87(12) . .
O119 K7 K20 43.1(5) 1_565 1_565
O112 K7 K20 113.6(6) . 1_565
O69 K7 K20 127.2(5) . 1_565
O141 K7 K20 43.0(6) . 1_565
O145 K7 K20 92.4(8) . 1_565
O103 K7 K20 141.1(5) . 1_565
S30 K7 K20 60.2(3) 1_565 1_565
S9 K7 K20 98.4(4) . 1_565
Mo30 K7 K20 119.2(4) . 1_565
O119 K7 Mo31 110.7(6) 1_565 .
O112 K7 Mo31 83.7(5) . .
O69 K7 Mo31 57.3(3) . .
O141 K7 Mo31 161.7(6) . .
O145 K7 Mo31 123.0(7) . .
O103 K7 Mo31 22.4(2) . .
S30 K7 Mo31 84.6(2) 1_565 .
S9 K7 Mo31 34.75(13) . .
Mo30 K7 Mo31 41.91(11) . .
K20 K7 Mo31 129.4(4) 1_565 .
O119 K7 K24' 122.9(10) 1_565 1_565
O112 K7 K24' 44.2(9) . 1_565
O69 K7 K24' 129.1(9) . 1_565
O141 K7 K24' 49.9(10) . 1_565
O145 K7 K24' 81.2(11) . 1_565
O103 K7 K24' 103.8(9) . 1_565
S30 K7 K24' 89.3(8) 1_565 1_565
S9 K7 K24' 156.6(8) . 1_565
Mo30 K7 K24' 148.1(9) . 1_565
K20 K7 K24' 90.9(9) 1_565 1_565
Mo31 K7 K24' 126.1(8) . 1_565
O144 K8 O130 96.7(11) . .
O144 K8 O180 150.3(15) . 2_675
O130 K8 O180 106.2(14) . 2_675
O144 K8 O153 87.6(11) . 2_675
O130 K8 O153 171.9(10) . 2_675
O180 K8 O153 67.6(14) 2_675 2_675
O144 K8 O55 91.2(9) . .
O130 K8 O55 120.5(6) . .
O180 K8 O55 93.0(13) 2_675 .
O153 K8 O55 66.0(8) 2_675 .
O144 K8 O51 129.4(9) . .
O130 K8 O51 63.9(6) . .
O180 K8 O51 78.6(13) 2_675 .
O153 K8 O51 118.2(8) 2_675 .
O55 K8 O51 65.9(4) . .
O144 K8 O12 63.1(9) . 2_665
O130 K8 O12 74.7(6) . 2_665
O180 K8 O12 104.8(13) 2_675 2_665
O153 K8 O12 101.4(8) 2_675 2_665
O55 K8 O12 152.6(6) . 2_665
O51 K8 O12 137.4(5) . 2_665
O144 K8 O202 37.2(12) . 2_675
O130 K8 O202 133.9(13) . 2_675
O153 K8 O202 51.1(12) 2_675 2_675
O55 K8 O202 71.1(10) . 2_675
O51 K8 O202 134.6(11) . 2_675
O12 K8 O202 82.1(10) 2_665 2_675
O144 K8 S14 74.4(8) . .
O130 K8 S14 69.6(5) . .
O180 K8 S14 131.0(13) 2_675 .
O153 K8 S14 118.3(8) 2_675 .
O55 K8 S14 56.2(3) . .
O51 K8 S14 55.1(3) . .
O12 K8 S14 119.5(5) 2_665 .
O202 K8 S14 89.2(10) 2_675 .
O144 K8 K15 144.5(9) . 2_675
O130 K8 K15 107.5(8) . 2_675
O180 K8 K15 43.2(13) 2_675 2_675
O153 K8 K15 71.8(8) 2_675 2_675
O55 K8 K15 54.2(5) . 2_675
O51 K8 K15 49.0(5) . 2_675
O12 K8 K15 147.9(6) 2_665 2_675
O202 K8 K15 113.0(11) 2_675 2_675
S14 K8 K15 89.9(4) . 2_675
O144 K8 Mo11 86.2(8) . .
O130 K8 Mo11 100.3(5) . .
O180 K8 Mo11 107.4(12) 2_675 .
O153 K8 Mo11 86.8(8) 2_675 .
O55 K8 Mo11 21.6(3) . .
O51 K8 Mo11 55.7(3) . .
O12 K8 Mo11 147.5(5) 2_665 .
O202 K8 Mo11 78.9(10) 2_675 .
S14 K8 Mo11 34.83(14) . .
K15 K8 Mo11 64.6(4) 2_675 .
O144 K8 Mo27 109.0(8) . .
O130 K8 Mo27 64.8(5) . .
O180 K8 Mo27 97.9(12) 2_675 .
O153 K8 Mo27 120.3(8) 2_675 .
O55 K8 Mo27 57.0(3) . .
O51 K8 Mo27 20.7(3) . .
O12 K8 Mo27 137.7(4) 2_665 .
O202 K8 Mo27 117.7(10) 2_675 .
S14 K8 Mo27 34.57(12) . .
K15 K8 Mo27 61.8(4) 2_675 .
Mo11 K8 Mo27 40.74(11) . .
O50 K9' O17 98.0(7) . .
O50 K9' O134 74.9(12) . .
O17 K9' O134 138.6(14) . .
O50 K9' O53 52.2(5) . .
O17 K9' O53 115.6(8) . .
O134 K9' O53 92.5(12) . .
O50 K9' O189 156.0(16) . 2_665
O17 K9' O189 95.0(14) . 2_665
O134 K9' O189 82.0(18) . 2_665
O53 K9' O189 136.7(15) . 2_665
O50 K9' O48 50.7(5) . .
O17 K9' O48 52.2(5) . .
O134 K9' O48 98.3(13) . .
O53 K9' O48 94.7(6) . .
O189 K9' O48 128.6(15) 2_665 .
O50 K9' O135 91.4(7) . .
O17 K9' O135 161.5(10) . .
O134 K9' O135 59.4(13) . .
O53 K9' O135 58.9(6) . .
O189 K9' O135 82.2(14) 2_665 .
O48 K9' O135 141.5(8) . .
O50 K9' O16 142.6(8) . .
O17 K9' O16 47.5(5) . .
O134 K9' O16 138.7(13) . .
O53 K9' O16 122.6(7) . .
O189 K9' O16 57.9(14) 2_665 .
O48 K9' O16 99.5(6) . .
O135 K9' O16 118.1(7) . .
O50 K9' Se4 24.7(4) . .
O17 K9' Se4 77.3(5) . .
O134 K9' Se4 82.4(12) . .
O53 K9' Se4 74.3(4) . .
O189 K9' Se4 145.7(15) 2_665 .
O48 K9' Se4 26.6(3) . .
O135 K9' Se4 114.9(7) . .
O16 K9' Se4 124.8(6) . .
O50 K9' Se2 121.3(6) . .
O17 K9' Se2 23.4(3) . .
O134 K9' Se2 137.5(13) . .
O53 K9' Se2 129.2(7) . .
O189 K9' Se2 72.7(13) 2_665 .
O48 K9' Se2 73.7(4) . .
O135 K9' Se2 144.4(7) . .
O16 K9' Se2 26.4(3) . .
Se4 K9' Se2 99.8(4) . .
O50 K9' Mo27 26.9(4) . .
O17 K9' Mo27 119.0(6) . .
O134 K9' Mo27 71.3(11) . .
O53 K9' Mo27 30.2(3) . .
O189 K9' Mo27 146.0(14) 2_665 .
O48 K9' Mo27 77.1(4) . .
O135 K9' Mo27 66.3(6) . .
O16 K9' Mo27 149.3(7) . .
Se4 K9' Mo27 51.6(2) . .
Se2 K9' Mo27 141.2(5) . .
O50 K9' Mo5 71.8(5) . .
O17 K9' Mo5 26.2(3) . .
O134 K9' Mo5 127.1(13) . .
O53 K9' Mo5 98.1(5) . .
O189 K9' Mo5 119.4(14) 2_665 .
O48 K9' Mo5 29.5(3) . .
O135 K9' Mo5 157.0(8) . .
O16 K9' Mo5 72.9(4) . .
Se4 K9' Mo5 52.0(2) . .
Se2 K9' Mo5 49.6(2) . .
Mo27 K9' Mo5 93.8(4) . .
O167 K9 O20 130.5(10) 2_665 .
O167 K9 O15 98.6(10) 2_665 .
O20 K9 O15 95.8(5) . .
O167 K9 O16 105.5(9) 2_665 .
O20 K9 O16 120.9(6) . .
O15 K9 O16 53.3(4) . .
O167 K9 O135 54.1(10) 2_665 .
O20 K9 O135 91.9(6) . .
O15 K9 O135 147.7(8) . .
O16 K9 O135 142.6(7) . .
O167 K9 O189 50.2(15) 2_665 2_665
O20 K9 O189 171.6(13) . 2_665
O15 K9 O189 92.2(13) . 2_665
O16 K9 O189 62.6(13) . 2_665
O135 K9 O189 82.6(14) . 2_665
O167 K9 O19 112.5(10) 2_665 .
O20 K9 O19 50.5(4) . .
O15 K9 O19 48.8(4) . .
O16 K9 O19 95.6(5) . .
O135 K9 O19 120.5(7) . .
O189 K9 O19 137.9(13) 2_665 .
O167 K9 O53 111.2(9) 2_665 .
O20 K9 O53 49.0(4) . .
O15 K9 O53 143.7(6) . .
O16 K9 O53 131.0(6) . .
O135 K9 O53 57.1(6) . .
O189 K9 O53 122.6(13) 2_665 .
O19 K9 O53 99.1(4) . .
O167 K9 O21 161.0(10) 2_665 .
O20 K9 O21 53.7(4) . .
O15 K9 O21 62.7(5) . .
O16 K9 O21 67.2(5) . .
O135 K9 O21 141.7(6) . .
O189 K9 O21 129.1(13) 2_665 .
O19 K9 O21 53.3(4) . .
O53 K9 O21 85.2(4) . .
O167 K9 Se8 118.5(9) 2_665 .
O20 K9 Se8 23.9(3) . .
O15 K9 Se8 119.6(4) . .
O16 K9 Se8 135.8(5) . .
O135 K9 Se8 70.4(5) . .
O189 K9 Se8 148.2(13) 2_665 .
O19 K9 Se8 72.6(3) . .
O53 K9 Se8 26.7(2) . .
O21 K9 Se8 72.2(3) . .
O167 K9 Se7 103.9(9) 2_665 .
O20 K9 Se7 75.3(3) . .
O15 K9 Se7 23.1(3) . .
O16 K9 Se7 74.1(4) . .
O135 K9 Se7 136.6(7) . .
O189 K9 Se7 113.0(13) 2_665 .
O19 K9 Se7 26.0(2) . .
O53 K9 Se7 124.4(4) . .
O21 K9 Se7 57.6(3) . .
Se8 K9 Se7 98.3(2) . .
O167 K9 Mo28 92.3(9) 2_665 .
O20 K9 Mo28 119.3(4) . .
O15 K9 Mo28 28.0(3) . .
O16 K9 Mo28 29.4(3) . .
O135 K9 Mo28 145.6(6) . .
O189 K9 Mo28 67.8(12) 2_665 .
O19 K9 Mo28 76.4(3) . .
O53 K9 Mo28 155.7(5) . .
O21 K9 Mo28 72.8(3) . .
Se8 K9 Mo28 142.7(3) . .
Se7 K9 Mo28 51.01(13) . .
O50 K9" O17 93.4(11) . .
O50 K9" O189 167(2) . 2_665
O17 K9" O189 95.8(17) . 2_665
O50 K9" O189 109.1(18) . .
O17 K9" O189 119.9(19) . .
O189 K9" O189 74(2) 2_665 .
O50 K9" O48 51.5(7) . .
O17 K9" O48 52.5(7) . .
O189 K9" O48 141.2(19) 2_665 .
O189 K9" O48 101.0(18) . .
O50 K9" O135 85.9(11) . .
O17 K9" O135 137.8(15) . .
O189 K9" O135 81.1(17) 2_665 .
O189 K9" O135 99.7(18) . .
O48 K9" O135 136.8(13) . .
O50 K9" Se4 26.8(5) . .
O17 K9" Se4 77.5(8) . .
O189 K9" Se4 166.1(19) 2_665 .
O189 K9" Se4 98.5(17) . .
O48 K9" Se4 27.3(4) . .
O135 K9" Se4 112.2(10) . .
O50 K9" Se2 116.4(11) . .
O17 K9" Se2 23.1(4) . .
O189 K9" Se2 72.8(15) 2_665 .
O189 K9" Se2 110.5(17) . .
O48 K9" Se2 73.4(7) . .
O135 K9" Se2 131.9(12) . .
Se4 K9" Se2 99.7(8) . .
O50 K9" K9" 144.5(17) . 2_665
O17 K9" K9" 112.1(13) . 2_665
O189 K9" K9" 37.1(15) 2_665 2_665
O189 K9" K9" 36.9(14) . 2_665
O48 K9" K9" 127.4(16) . 2_665
O135 K9" K9" 90.5(11) . 2_665
Se4 K9" K9" 134.3(15) . 2_665
Se2 K9" K9" 92.0(10) . 2_665
O50 K9" K17 76.2(10) . .
O17 K9" K17 86.2(10) . .
O189 K9" K17 113.6(18) 2_665 .
O189 K9" K17 50.0(16) . .
O48 K9" K17 51.1(9) . .
O135 K9" K17 133.8(12) . .
Se4 K9" K17 54.3(7) . .
Se2 K9" K17 94.0(9) . .
K9" K9" K17 81.1(12) 2_665 .
O143 K10 O160 133.9(15) . .
O143 K10 O81 109.8(9) . .
O160 K10 O81 103.3(13) . .
O143 K10 O62 109.6(8) . 1_655
O160 K10 O62 105.3(13) . 1_655
O81 K10 O62 83.3(5) . 1_655
O143 K10 O159 76.4(13) . .
O160 K10 O159 59.1(17) . .
O81 K10 O159 149.2(12) . .
O62 K10 O159 124.1(11) 1_655 .
O143 K10 O64 95.8(8) . 1_655
O160 K10 O64 77.9(12) . 1_655
O81 K10 O64 139.3(6) . 1_655
O62 K10 O64 58.0(4) 1_655 1_655
O159 K10 O64 66.2(11) . 1_655
O143 K10 O35 72.6(8) . 1_665
O160 K10 O35 91.7(12) . 1_665
O81 K10 O35 68.2(5) . 1_665
O62 K10 O35 149.7(5) 1_655 1_665
O159 K10 O35 86.2(11) . 1_665
O64 K10 O35 152.0(5) 1_655 1_665
O143 K10 O63 66.5(8) . 1_655
O160 K10 O63 130.2(12) . 1_655
O81 K10 O63 109.0(5) . 1_655
O62 K10 O63 44.9(4) 1_655 1_655
O159 K10 O63 101.2(11) . 1_655
O64 K10 O63 52.9(4) 1_655 1_655
O35 K10 O63 135.1(6) 1_665 1_655
O143 K10 O60 73.1(8) . 1_655
O160 K10 O60 153.0(13) . 1_655
O81 K10 O60 59.3(5) . 1_655
O62 K10 O60 55.4(4) 1_655 1_655
O159 K10 O60 145.8(12) . 1_655
O64 K10 O60 101.7(4) 1_655 1_655
O35 K10 O60 99.2(5) 1_665 1_655
O63 K10 O60 52.1(4) 1_655 1_655
O143 K10 Mo7 95.0(7) . 1_655
O160 K10 Mo7 97.6(12) . 1_655
O81 K10 Mo7 117.1(5) . 1_655
O62 K10 Mo7 33.9(3) 1_655 1_655
O159 K10 Mo7 91.5(11) . 1_655
O64 K10 Mo7 26.5(3) 1_655 1_655
O35 K10 Mo7 167.6(5) 1_665 1_655
O63 K10 Mo7 33.7(2) 1_655 1_655
O60 K10 Mo7 76.1(3) 1_655 1_655
O143 K10 Mo4 81.8(8) . 1_655
O160 K10 Mo4 138.0(13) . 1_655
O81 K10 Mo4 76.2(4) . 1_655
O62 K10 Mo4 32.8(3) 1_655 1_655
O159 K10 Mo4 134.3(11) . 1_655
O64 K10 Mo4 76.9(3) 1_655 1_655
O35 K10 Mo4 124.6(5) 1_665 1_655
O63 K10 Mo4 33.2(3) 1_655 1_655
O60 K10 Mo4 25.5(2) 1_655 1_655
Mo7 K10 Mo4 50.80(13) 1_655 1_655
O143 K10 Mo16 125.4(8) . .
O160 K10 Mo16 87.6(13) . .
O81 K10 Mo16 16.3(3) . .
O62 K10 Mo16 83.0(4) 1_655 .
O159 K10 Mo16 140.1(11) . .
O64 K10 Mo16 131.8(4) 1_655 .
O35 K10 Mo16 72.6(3) 1_665 .
O63 K10 Mo16 117.8(4) 1_655 .
O60 K10 Mo16 72.4(3) 1_655 .
Mo7 K10 Mo16 115.9(3) 1_655 .
Mo4 K10 Mo16 84.82(19) 1_655 .
O154 K11 O74 99.8(9) . .
O154 K11 O1 122.6(9) . 2_776
O74 K11 O1 110.8(5) . 2_776
O154 K11 O30 57.9(8) . 2_776
O74 K11 O30 50.7(4) . 2_776
O1 K11 O30 108.7(5) 2_776 2_776
O154 K11 O128 114.6(9) . .
O74 K11 O128 77.4(5) . .
O1 K11 O128 118.8(6) 2_776 .
O30 K11 O128 119.2(6) 2_776 .
O154 K11 S10 75.2(8) . 2_776
O74 K11 S10 94.8(5) . 2_776
O1 K11 S10 55.4(3) 2_776 2_776
O30 K11 S10 59.2(3) 2_776 2_776
O128 K11 S10 168.2(6) . 2_776
O154 K11 Mo20 81.8(8) . 2_776
O74 K11 Mo20 31.1(3) . 2_776
O1 K11 Mo20 100.4(4) 2_776 2_776
O30 K11 Mo20 24.2(3) 2_776 2_776
O128 K11 Mo20 107.9(5) . 2_776
S10 K11 Mo20 65.8(3) 2_776 2_776
O154 K11 K20 31.4(8) . 2_776
O74 K11 K20 91.3(5) . 2_776
O1 K11 K20 99.0(4) 2_776 2_776
O30 K11 K20 40.7(4) 2_776 2_776
O128 K11 K20 142.2(5) . 2_776
S10 K11 K20 45.5(3) 2_776 2_776
Mo20 K11 K20 63.4(3) 2_776 2_776
O154 K11 K6 58.0(8) . 1_565
O74 K11 K6 93.7(5) . 1_565
O1 K11 K6 154.1(6) 2_776 1_565
O30 K11 K6 93.2(5) 2_776 1_565
O128 K11 K6 57.0(5) . 1_565
S10 K11 K6 133.3(5) 2_776 1_565
Mo20 K11 K6 105.1(4) 2_776 1_565
K20 K11 K6 88.5(4) 2_776 1_565
O172 K12' O85 127.5(18) . .
O172 K12' O126 64.4(14) . 2_776
O85 K12' O126 109.6(14) . 2_776
O172 K12' O88 176.1(19) . .
O85 K12' O88 55.7(8) . .
O126 K12' O88 113.0(13) 2_776 .
O172 K12' O89 130.5(18) . .
O85 K12' O89 53.9(8) . .
O126 K12' O89 161.6(15) 2_776 .
O88 K12' O89 52.8(7) . .
O172 K12' O161 75.8(15) . .
O85 K12' O161 107.2(14) . .
O126 K12' O161 137.0(15) 2_776 .
O88 K12' O161 105.9(13) . .
O89 K12' O161 61.3(9) . .
O172 K12' Mo10 157.1(18) . .
O85 K12' Mo10 34.3(5) . .
O126 K12' Mo10 127.4(13) 2_776 .
O88 K12' Mo10 26.7(4) . .
O89 K12' Mo10 34.6(5) . .
O161 K12' Mo10 95.7(11) . .
O161 K12 O172 81.5(12) . .
O161 K12 O83 134.8(8) . .
O172 K12 O83 143.2(11) . .
O161 K12 O86 82.8(7) . .
O172 K12 O86 163.9(11) . .
O83 K12 O86 52.8(4) . .
O161 K12 O85 116.0(8) . .
O172 K12 O85 115.1(11) . .
O83 K12 O85 50.5(4) . .
O86 K12 O85 75.1(4) . .
O161 K12 O89 67.0(7) . .
O172 K12 O89 125.4(11) . .
O83 K12 O89 76.3(4) . .
O86 K12 O89 49.5(4) . .
O85 K12 O89 52.9(4) . .
O161 K12 O42 98.8(8) . 1_655
O172 K12 O42 69.3(10) . 1_655
O83 K12 O42 103.9(5) . 1_655
O86 K12 O42 110.1(5) . 1_655
O85 K12 O42 145.2(6) . 1_655
O89 K12 O42 154.7(6) . 1_655
O161 K12 Se11 136.7(7) . .
O172 K12 Se11 125.9(10) . .
O83 K12 Se11 26.3(3) . .
O86 K12 Se11 68.8(4) . .
O85 K12 Se11 26.6(3) . .
O89 K12 Se11 69.7(4) . .
O42 K12 Se11 121.0(5) 1_655 .
O161 K12 Se10 66.6(6) . .
O172 K12 Se10 143.9(11) . .
O83 K12 Se10 68.8(3) . .
O86 K12 Se10 25.6(3) . .
O85 K12 Se10 68.4(3) . .
O89 K12 Se10 25.9(2) . .
O42 K12 Se10 130.0(5) 1_655 .
Se11 K12 Se10 74.4(2) . .
K13 K13 O87 74.5(14) 2_776 .
K13 K13 O87 73.7(14) 2_776 2_776
O87 K13 O87 148.1(7) . 2_776
K13 K13 O137 104.7(19) 2_776 .
O87 K13 O137 105.1(12) . .
O87 K13 O137 83.1(11) 2_776 .
K13 K13 O184 142.9(19) 2_776 .
O87 K13 O184 122.2(10) . .
O87 K13 O184 84.6(9) 2_776 .
O137 K13 O184 102.1(13) . .
K13 K13 O185 129(2) 2_776 .
O87 K13 O185 102.3(14) . .
O87 K13 O185 97.5(13) 2_776 .
K13 K13 O88 147.8(18) 2_776 .
O87 K13 O88 75.4(6) . .
O87 K13 O88 135.6(8) 2_776 .
O137 K13 O88 72.8(11) . .
O184 K13 O88 65.5(8) . .
O185 K13 O88 69.1(13) . .
K13 K13 O149 123.4(18) 2_776 .
O87 K13 O149 118.4(9) . .
O87 K13 O149 80.1(8) 2_776 .
O185 K13 O149 103.6(14) . .
O88 K13 O149 63.8(8) . .
K13 K13 O137 50.8(15) 2_776 2_776
O87 K13 O137 71.1(9) . 2_776
O87 K13 O137 88.6(9) 2_776 2_776
O137 K13 O137 155.5(8) . 2_776
O184 K13 O137 100.0(12) . 2_776
O88 K13 O137 126.8(10) . 2_776
K13 K13 Mo32 91.7(14) 2_776 .
O87 K13 Mo32 17.5(3) . .
O87 K13 Mo32 165.1(7) 2_776 .
O137 K13 Mo32 98.1(11) . .
O184 K13 Mo32 109.5(8) . .
O185 K13 Mo32 94.0(13) . .
O88 K13 Mo32 57.9(4) . .
O149 K13 Mo32 106.4(8) . .
O137 K13 Mo32 84.3(8) 2_776 .
K13 K13 Mo10 130.3(16) 2_776 .
O87 K13 Mo10 56.9(4) . .
O87 K13 Mo10 153.9(6) 2_776 .
O137 K13 Mo10 80.4(10) . .
O184 K13 Mo10 79.2(8) . .
O185 K13 Mo10 75.9(12) . .
O88 K13 Mo10 18.5(3) . .
O149 K13 Mo10 77.1(7) . .
O137 K13 Mo10 114.2(9) 2_776 .
Mo32 K13 Mo10 39.39(18) . .
K13 K13 K5 108.7(15) 2_776 2_776
O87 K13 K5 68.3(5) . 2_776
O87 K13 K5 122.9(6) 2_776 2_776
O137 K13 K5 142.2(11) . 2_776
O184 K13 K5 59.1(8) . 2_776
O185 K13 K5 35.1(12) . 2_776
O88 K13 K5 69.5(5) . 2_776
O149 K13 K5 127.6(8) . 2_776
O137 K13 K5 60.2(8) 2_776 2_776
Mo32 K13 K5 64.1(3) . 2_776
Mo10 K13 K5 64.6(3) . 2_776
O38 K14 O160 109.9(14) . 2_776
O38 K14 O183 121.9(14) . 2_776
O160 K14 O183 38.1(16) 2_776 2_776
O38 K14 O132 118.6(9) . 2_776
O160 K14 O132 111.1(14) 2_776 2_776
O183 K14 O132 118.7(14) 2_776 2_776
O38 K14 K22 86.0(7) . 2_666
O160 K14 K22 114.1(14) 2_776 2_666
O183 K14 K22 78.4(12) 2_776 2_666
O132 K14 K22 115.1(9) 2_776 2_666
O38 K14 S3 63.1(5) . .
O160 K14 S3 167.5(13) 2_776 .
O183 K14 S3 154.2(12) 2_776 .
O132 K14 S3 67.1(7) 2_776 .
K22 K14 S3 76.7(6) 2_666 .
O38 K14 S5 57.3(5) . .
O160 K14 S5 72.3(12) 2_776 .
O183 K14 S5 108.4(12) 2_776 .
O132 K14 S5 95.5(7) 2_776 .
K22 K14 S5 141.1(7) 2_666 .
S3 K14 S5 95.3(5) . .
O38 K14 Mo23 28.8(4) . .
O160 K14 Mo23 138.6(13) 2_776 .
O183 K14 Mo23 142.6(13) 2_776 .
O132 K14 Mo23 97.2(7) 2_776 .
K22 K14 Mo23 77.2(5) 2_666 .
S3 K14 Mo23 34.6(2) . .
S5 K14 Mo23 75.5(3) . .
O38 K14 K10 140.5(8) . 2_776
O160 K14 K10 30.9(12) 2_776 2_776
O132 K14 K10 91.1(7) 2_776 2_776
K22 K14 K10 105.2(6) 2_666 2_776
S3 K14 K10 155.9(6) . 2_776
S5 K14 K10 97.1(5) . 2_776
Mo23 K14 K10 169.4(6) . 2_776
O180 K15 O133 128.9(16) . .
O180 K15 O173 124.3(19) . 1_455
O133 K15 O173 101.8(15) . 1_455
O180 K15 O181 66.4(17) . .
O133 K15 O181 65.0(14) . .
O173 K15 O181 136.4(19) 1_455 .
O180 K15 O51 83.9(15) . 2_675
O133 K15 O51 123.4(11) . 2_675
O173 K15 O51 86.1(14) 1_455 2_675
O181 K15 O51 136.8(14) . 2_675
O133 K15 O186 111.5(15) . .
O173 K15 O186 113.0(19) 1_455 .
O181 K15 O186 48.8(16) . .
O51 K15 O186 116.4(14) 2_675 .
O180 K15 O55 92.4(15) . 2_675
O133 K15 O55 68.5(7) . 2_675
O173 K15 O55 131.0(16) 1_455 2_675
O181 K15 O55 84.8(13) . 2_675
O51 K15 O55 65.0(6) 2_675 2_675
O186 K15 O55 115.1(14) . 2_675
O180 K15 S2 108.6(15) . .
O133 K15 S2 61.3(7) . .
O173 K15 S2 73.9(14) 1_455 .
O181 K15 S2 63.3(12) . .
O51 K15 S2 159.9(9) 2_675 .
O186 K15 S2 74.3(13) . .
O55 K15 S2 128.1(8) 2_675 .
O180 K15 S15 133.6(15) . 2_675
O133 K15 S15 72.7(8) . 2_675
O173 K15 S15 76.9(14) 1_455 2_675
O181 K15 S15 129.6(13) . 2_675
O51 K15 S15 54.5(5) 2_675 2_675
O186 K15 S15 167.2(14) . 2_675
O55 K15 S15 54.2(5) 2_675 2_675
S2 K15 S15 117.4(7) . 2_675
O180 K15 K8 47.1(13) . 2_675
O133 K15 K8 113.4(9) . 2_675
O173 K15 K8 135.2(15) 1_455 2_675
O181 K15 K8 85.1(13) . 2_675
O51 K15 K8 51.9(5) 2_675 2_675
O186 K15 K8 79.5(13) . 2_675
O55 K15 K8 49.8(5) 2_675 2_675
S2 K15 K8 147.6(7) . 2_675
S15 K15 K8 87.8(6) 2_675 2_675
O180 K15 Mo27 102.3(15) . 2_675
O133 K15 Mo27 104.7(9) . 2_675
O173 K15 Mo27 82.3(14) 1_455 2_675
O181 K15 Mo27 140.3(13) . 2_675
O51 K15 Mo27 20.1(4) 2_675 2_675
O186 K15 Mo27 135.9(14) . 2_675
O55 K15 Mo27 56.8(5) 2_675 2_675
S2 K15 Mo27 148.1(7) . 2_675
S15 K15 Mo27 34.4(2) 2_675 2_675
K8 K15 Mo27 63.2(4) 2_675 2_675
O163 K16 O79 92.5(8) . .
O163 K16 O115 121.8(9) . .
O79 K16 O115 103.0(7) . .
O163 K16 O113 116.5(9) . .
O79 K16 O113 100.9(7) . .
O115 K16 O113 114.9(7) . .
O163 K16 S23 64.5(7) . .
O79 K16 S23 61.2(5) . .
O115 K16 S23 164.1(7) . .
O113 K16 S23 69.1(5) . .
O163 K16 S16 65.6(7) . .
O79 K16 S16 61.9(4) . .
O115 K16 S16 73.4(5) . .
O113 K16 S16 162.7(7) . .
S23 K16 S16 98.9(4) . .
O163 K16 S13 121.9(8) . .
O79 K16 S13 145.5(7) . .
O115 K16 S13 63.4(4) . .
O113 K16 S13 62.8(4) . .
S23 K16 S13 127.9(5) . .
S16 K16 S13 132.2(5) . .
O163 K16 Mo16 78.6(7) . .
O79 K16 Mo16 27.7(3) . .
O115 K16 Mo16 90.0(5) . .
O113 K16 Mo16 128.5(6) . .
S23 K16 Mo16 76.6(3) . .
S16 K16 Mo16 34.25(19) . .
S13 K16 Mo16 152.0(5) . .
O163 K16 Mo34 78.0(7) . .
O79 K16 Mo34 27.1(3) . .
O115 K16 Mo34 130.0(6) . .
O113 K16 Mo34 87.0(5) . .
S23 K16 Mo34 34.20(19) . .
S16 K16 Mo34 76.6(3) . .
S13 K16 Mo34 148.6(5) . .
Mo16 K16 Mo34 46.06(18) . .
O163 K16 K18 157.4(8) . .
O79 K16 K18 92.6(6) . .
O115 K16 K18 78.3(5) . .
O113 K16 K18 40.9(4) . .
S23 K16 K18 99.1(5) . .
S16 K16 K18 135.3(6) . .
S13 K16 K18 54.6(4) . .
Mo16 K16 K18 114.1(5) . .
Mo34 K16 K18 97.2(5) . .
O167 K17 O142 98.7(17) . .
O167 K17 O148 80.6(17) . 2_665
O142 K17 O148 113.7(19) . 2_665
O167 K17 O49 125.2(19) . .
O142 K17 O49 109.6(17) . .
O148 K17 O49 124.4(18) 2_665 .
O167 K17 O138 51.8(13) . .
O142 K17 O138 68.5(13) . .
O148 K17 O138 130.7(19) 2_665 .
O49 K17 O138 96.6(15) . .
O167 K17 K26 111.8(17) . 2_665
O142 K17 K26 135.2(16) . 2_665
O148 K17 K26 45.6(11) 2_665 2_665
O49 K17 K26 79.1(11) . 2_665
O138 K17 K26 156.1(17) . 2_665
O167 K17 K27 133.3(17) . .
O142 K17 K27 39.9(9) . .
O148 K17 K27 128.6(16) 2_665 .
O49 K17 K27 72.3(11) . .
O138 K17 K27 86.2(13) . .
K26 K17 K27 114.1(11) 2_665 .
O167 K17 K25' 156.3(19) . 1_455
O142 K17 K25' 72.9(13) . 1_455
O148 K17 K25' 82.7(15) 2_665 1_455
O49 K17 K25' 78.3(12) . 1_455
O138 K17 K25' 136.7(17) . 1_455
K26 K17 K25' 65.9(11) 2_665 1_455
K27 K17 K25' 51.0(9) . 1_455
O167 K17 K25 150.3(18) . 1_455
O142 K17 K25 78.0(13) . 1_455
O148 K17 K25 74.1(14) 2_665 1_455
O49 K17 K25 82.7(12) . 1_455
O138 K17 K25 144.2(17) . 1_455
K26 K17 K25 59.1(10) 2_665 1_455
K27 K17 K25 59.4(9) . 1_455
O167 K17 K9" 70.2(13) . .
O142 K17 K9" 106.0(14) . .
O148 K17 K9" 133.6(17) 2_665 .
O49 K17 K9" 57.4(10) . .
O138 K17 K9" 47.0(10) . .
K26 K17 K9" 114.7(12) 2_665 .
K27 K17 K9" 97.3(10) . .
O167 K17 K9 22.0(10) . 2_665
O142 K17 K9 118.9(14) . 2_665
O148 K17 K9 65.4(12) 2_665 2_665
O49 K17 K9 119.1(13) . 2_665
O138 K17 K9 71.3(11) . 2_665
K26 K17 K9 90.1(9) 2_665 2_665
K27 K17 K9 155.4(11) . 2_665
K25 K17 K9 139.5(12) 1_455 2_665
O146 K18 O124 105.8(12) . 2_775
O146 K18 O113 107.1(12) . .
O124 K18 O113 106.6(9) 2_775 .
O146 K18 O125 119.1(12) . .
O124 K18 O125 106.7(10) 2_775 .
O113 K18 O125 110.8(8) . .
O146 K18 O8 87.8(10) . 1_565
O124 K18 O8 63.3(7) 2_775 1_565
O113 K18 O8 54.8(5) . 1_565
O125 K18 O8 153.1(9) . 1_565
O146 K18 S13 167.9(12) . .
O124 K18 S13 80.9(6) 2_775 .
O113 K18 S13 61.0(5) . .
O125 K18 S13 67.0(6) . .
O8 K18 S13 86.4(5) 1_565 .
O146 K18 K16 118.5(11) . .
O124 K18 K16 130.2(8) 2_775 .
O113 K18 K16 41.0(4) . .
O125 K18 K16 71.4(6) . .
O8 K18 K16 95.5(6) 1_565 .
S13 K18 K16 51.7(4) . .
O146 K18 K1 139.1(11) . 2_775
O124 K18 K1 39.2(5) 2_775 2_775
O113 K18 K1 104.5(7) . 2_775
O125 K18 K1 71.1(7) . 2_775
O8 K18 K1 89.7(6) 1_565 2_775
S13 K18 K1 51.5(3) . 2_775
K16 K18 K1 102.4(5) . 2_775
O70 K19' O182 101.7(18) . .
O70 K19' O65 112.6(15) . .
O182 K19' O65 139(2) . .
O70 K19' O128 83.1(13) . .
O182 K19' O128 71.5(16) . .
O65 K19' O128 132.9(15) . .
O70 K19' S12 88.2(11) . .
O182 K19' S12 108.2(17) . .
O65 K19' S12 53.2(8) . .
O128 K19' S12 171.0(16) . .
O70 K19' Mo30 29.3(5) . .
O182 K19' Mo30 102.9(16) . .
O65 K19' Mo30 96.8(12) . .
O128 K19' Mo30 111.3(13) . .
S12 K19' Mo30 59.7(7) . .
O182 K19 O145 46.8(17) . .
O182 K19 O70 108.0(15) . .
O145 K19 O70 106.0(10) . .
O182 K19 O64 93.8(15) . .
O145 K19 O64 72.0(9) . .
O70 K19 O64 147.9(7) . .
O182 K19 O65 149.2(15) . .
O145 K19 O65 130.1(10) . .
O70 K19 O65 102.0(6) . .
O64 K19 O65 62.6(4) . .
O182 K19 O69 99.2(15) . .
O145 K19 O69 65.2(9) . .
O70 K19 O69 51.6(4) . .
O64 K19 O69 102.8(6) . .
O65 K19 O69 105.0(6) . .
O182 K19 O128 70.2(15) . .
O145 K19 O128 114.6(10) . .
O70 K19 O128 74.4(5) . .
O64 K19 O128 136.5(7) . .
O65 K19 O128 112.3(7) . .
O69 K19 O128 119.2(6) . .
O182 K19 S12 129.8(16) . .
O145 K19 S12 83.6(9) . .
O70 K19 S12 91.2(5) . .
O64 K19 S12 56.7(4) . .
O65 K19 S12 55.1(4) . .
O69 K19 S12 57.5(4) . .
O128 K19 S12 159.1(7) . .
O182 K19 Mo30 114.6(15) . .
O145 K19 Mo30 88.5(9) . .
O70 K19 Mo30 31.6(3) . .
O64 K19 Mo30 117.7(5) . .
O65 K19 Mo30 94.7(5) . .
O69 K19 Mo30 23.9(3) . .
O128 K19 Mo30 105.7(5) . .
S12 K19 Mo30 62.8(3) . .
O182 K19 Mo7 109.7(15) . .
O145 K19 Mo7 75.0(9) . .
O70 K19 Mo7 125.5(5) . .
O64 K19 Mo7 22.4(3) . .
O65 K19 Mo7 55.1(3) . .
O69 K19 Mo7 84.5(4) . .
O128 K19 Mo7 156.2(6) . .
S12 K19 Mo7 34.30(16) . .
Mo30 K19 Mo7 96.0(4) . .
O182 K19 K7 65.3(15) . .
O145 K19 K7 42.2(8) . .
O70 K19 K7 63.8(4) . .
O64 K19 K7 107.5(6) . .
O65 K19 K7 137.9(5) . .
O69 K19 K7 34.1(3) . .
O128 K19 K7 101.9(5) . .
S12 K19 K7 84.6(4) . .
Mo30 K19 K7 51.5(2) . .
Mo7 K19 K7 99.2(4) . .
O6 K20 O141 117.2(10) . 1_545
O6 K20 O119 122.6(11) . .
O141 K20 O119 73.8(8) 1_545 .
O6 K20 O154 88.0(10) . 2_776
O141 K20 O154 138.0(12) 1_545 2_776
O119 K20 O154 122.2(12) . 2_776
O6 K20 O30 121.3(7) . .
O141 K20 O30 76.2(8) 1_545 .
O119 K20 O30 116.1(10) . .
O154 K20 O30 61.9(8) 2_776 .
O6 K20 O76 72.7(6) . 1_545
O141 K20 O76 147.8(9) 1_545 1_545
O119 K20 O76 75.5(6) . 1_545
O154 K20 O76 68.7(9) 2_776 1_545
O30 K20 O76 127.1(8) . 1_545
O6 K20 S10 61.0(4) . .
O141 K20 S10 86.8(7) 1_545 .
O119 K20 S10 159.6(9) . .
O154 K20 S10 76.7(8) 2_776 .
O30 K20 S10 63.5(4) . .
O76 K20 S10 122.2(6) 1_545 .
O6 K20 K6 151.8(9) . .
O141 K20 K6 88.3(8) 1_545 .
O119 K20 K6 73.8(10) . .
O154 K20 K6 64.1(9) 2_776 .
O30 K20 K6 50.1(5) . .
O76 K20 K6 92.2(6) 1_545 .
S10 K20 K6 112.5(6) . .
O6 K20 S30 55.7(5) . .
O141 K20 S30 72.5(8) 1_545 .
O119 K20 S30 80.2(9) . .
O154 K20 S30 143.4(9) 2_776 .
O30 K20 S30 138.6(7) . .
O76 K20 S30 93.1(6) 1_545 .
S10 K20 S30 88.2(4) . .
K6 K20 S30 151.2(7) . .
O6 K20 K7 106.0(7) . 1_545
O141 K20 K7 45.7(7) 1_545 1_545
O119 K20 K7 39.3(7) . 1_545
O154 K20 K7 161.1(9) 2_776 1_545
O30 K20 K7 117.7(6) . 1_545
O76 K20 K7 102.9(5) 1_545 1_545
S10 K20 K7 121.1(6) . 1_545
K6 K20 K7 100.4(6) . 1_545
S30 K20 K7 50.8(3) . 1_545
O6 K20 Mo12 27.4(3) . .
O141 K20 Mo12 111.0(8) 1_545 .
O119 K20 Mo12 149.4(10) . .
O154 K20 Mo12 75.6(8) 2_776 .
O30 K20 Mo12 94.0(5) . .
O76 K20 Mo12 91.1(5) 1_545 .
S10 K20 Mo12 34.82(18) . .
K6 K20 Mo12 135.0(7) . .
S30 K20 Mo12 73.2(3) . .
K7 K20 Mo12 122.5(5) 1_545 .
O6 K20 K11 81.8(5) . 2_776
O141 K20 K11 115.6(8) 1_545 2_776
O119 K20 K11 148.1(10) . 2_776
O154 K20 K11 30.7(7) 2_776 2_776
O30 K20 K11 46.0(4) . 2_776
O76 K20 K11 95.7(6) 1_545 2_776
S10 K20 K11 47.6(3) . 2_776
K6 K20 K11 76.0(5) . 2_776
S30 K20 K11 131.5(4) . 2_776
K7 K20 K11 161.3(5) 1_545 2_776
Mo12 K20 K11 59.0(3) . 2_776
O9 K21 O18 111.6(7) . 2_765
O9 K21 O165 88.9(11) . .
O18 K21 O165 97.6(10) 2_765 .
O9 K21 O165 118.4(10) . 2_765
O18 K21 O165 125.4(11) 2_765 2_765
O165 K21 O165 103.7(11) . 2_765
O9 K21 S27 163.9(10) . 2_765
O18 K21 S27 69.7(5) 2_765 2_765
O165 K21 S27 75.1(9) . 2_765
O165 K21 S27 68.4(8) 2_765 2_765
O9 K21 K26 136.9(10) . 2_765
O18 K21 K26 85.5(8) 2_765 2_765
O165 K21 K26 129.2(12) . 2_765
O165 K21 K26 42.7(10) 2_765 2_765
S27 K21 K26 58.5(7) 2_765 2_765
O9 K21 S27 58.9(5) . .
O18 K21 S27 162.7(8) 2_765 .
O165 K21 S27 69.0(9) . .
O165 K21 S27 70.1(8) 2_765 .
S27 K21 S27 115.1(5) 2_765 .
K26 K21 S27 111.4(7) 2_765 .
O9 K21 S33 58.4(5) . .
O18 K21 S33 99.8(6) 2_765 .
O165 K21 S33 146.7(10) . .
O165 K21 S33 88.8(9) 2_765 .
S27 K21 S33 137.7(7) 2_765 .
K26 K21 S33 80.4(7) 2_765 .
S27 K21 S33 87.3(4) . .
O9 K21 K21 112.7(9) . 2_765
O18 K21 K21 126.2(9) 2_765 2_765
O165 K21 K21 54.9(10) . 2_765
O165 K21 K21 48.8(9) 2_765 2_765
S27 K21 K21 59.4(5) 2_765 2_765
K26 K21 K21 82.6(8) 2_765 2_765
S27 K21 K21 55.7(5) . 2_765
S33 K21 K21 129.0(8) . 2_765
O9 K21 Se7 122.8(7) . 2_765
O18 K21 Se7 22.4(3) 2_765 2_765
O165 K21 Se7 78.8(9) . 2_765
O165 K21 Se7 118.8(9) 2_765 2_765
S27 K21 Se7 53.0(3) 2_765 2_765
K26 K21 Se7 88.2(7) 2_765 2_765
S27 K21 Se7 147.8(7) . 2_765
S33 K21 Se7 122.1(5) . 2_765
K21 K21 Se7 104.8(7) 2_765 2_765
O9 K21 Mo29 25.6(4) . .
O18 K21 Mo29 132.5(6) 2_765 .
O165 K21 Mo29 73.2(9) . .
O165 K21 Mo29 101.8(9) 2_765 .
S27 K21 Mo29 143.3(6) 2_765 .
K26 K21 Mo29 136.8(8) 2_765 .
S27 K21 Mo29 34.6(2) . .
S33 K21 Mo29 74.1(3) . .
K21 K21 Mo29 87.1(7) 2_765 .
Se7 K21 Mo29 135.0(5) 2_765 .
O9 K21 Mo18 25.2(4) . .
O18 K21 Mo18 103.2(6) 2_765 .
O165 K21 Mo18 113.9(10) . .
O165 K21 Mo18 112.5(9) 2_765 .
S27 K21 Mo18 169.7(7) 2_765 .
K26 K21 Mo18 114.6(8) 2_765 .
S27 K21 Mo18 73.9(3) . .
S33 K21 Mo18 34.2(2) . .
K21 K21 Mo18 129.4(7) 2_765 .
Se7 K21 Mo18 122.0(4) 2_765 .
Mo29 K21 Mo18 47.0(2) . .
O32 K22 K14 84.8(7) . 2_666
O32 K22 O132 116.8(9) . 2_776
K14 K22 O132 116.8(8) 2_666 2_776
O32 K22 O176 105.3(15) . 2_776
K14 K22 O176 115.3(15) 2_666 2_776
O132 K22 O176 114.1(15) 2_776 2_776
O32 K22 S3 62.0(5) . .
K14 K22 S3 79.3(6) 2_666 .
O132 K22 S3 65.3(6) 2_776 .
O176 K22 S3 160.8(15) 2_776 .
O32 K22 S29 57.3(4) . .
K14 K22 S29 139.3(8) 2_666 .
O132 K22 S29 95.2(7) 2_776 .
O176 K22 S29 67.3(14) 2_776 .
S3 K22 S29 93.5(4) . .
O32 K22 Mo22 28.0(4) . .
K14 K22 Mo22 78.0(5) 2_666 .
O132 K22 Mo22 95.4(7) 2_776 .
O176 K22 Mo22 132.8(14) 2_776 .
S3 K22 Mo22 34.3(2) . .
S29 K22 Mo22 74.3(3) . .
O98 K23 O106 126.7(8) . .
O98 K23 O122 125.6(8) . .
O106 K23 O122 68.7(6) . .
O98 K23 S19 60.9(4) . .
O106 K23 S19 107.2(6) . .
O122 K23 S19 173.5(7) . .
O98 K23 O116 91.0(6) . .
O106 K23 O116 116.2(6) . .
O122 K23 O116 47.9(5) . .
S19 K23 O116 136.6(6) . .
O98 K23 S24 56.3(4) . .
O106 K23 S24 73.3(5) . .
O122 K23 S24 93.1(6) . .
S19 K23 S24 90.5(4) . .
O116 K23 S24 100.8(5) . .
O98 K23 K1 104.4(6) . .
O106 K23 K1 45.2(4) . .
O122 K23 K1 45.0(4) . .
S19 K23 K1 135.7(6) . .
O116 K23 K1 80.2(4) . .
S24 K23 K1 52.5(3) . .
O98 K23 K4 48.5(4) . .
O106 K23 K4 135.5(7) . .
O122 K23 K4 82.9(6) . .
S19 K23 K4 103.4(4) . .
O116 K23 K4 42.6(3) . .
S24 K23 K4 74.9(4) . .
K1 K23 K4 90.5(4) . .
O98 K23 Mo31 27.3(3) . .
O106 K23 Mo31 126.8(6) . .
O122 K23 Mo31 152.3(7) . .
S19 K23 Mo31 34.24(18) . .
O116 K23 Mo31 109.9(5) . .
S24 K23 Mo31 73.3(3) . .
K1 K23 Mo31 125.7(5) . .
K4 K23 Mo31 70.4(3) . .
O33 K24 O155 109.3(14) . .
O33 K24 O47 132.3(9) . .
O155 K24 O47 75.3(12) . .
O33 K24 O166 108.7(11) . 1_545
O155 K24 O166 126.9(15) . 1_545
O47 K24 O166 103.7(10) . 1_545
O33 K24 S1 60.2(5) . .
O155 K24 S1 166.2(14) . .
O47 K24 S1 104.5(7) . .
O166 K24 S1 66.9(9) 1_545 .
O33 K24 S4 59.1(6) . .
O155 K24 S4 73.3(12) . .
O47 K24 S4 78.9(6) . .
O166 K24 S4 159.8(11) 1_545 .
S1 K24 S4 93.0(5) . .
O187 K24' O112 78.9(18) 1_445 1_545
O187 K24' O141 95(2) 1_445 1_545
O112 K24' O141 70.3(14) 1_545 1_545
O187 K24' Se2 135(2) 1_445 .
O112 K24' Se2 107.3(17) 1_545 .
O141 K24' Se2 129.7(19) 1_545 .
O187 K24' S20 117(2) 1_445 .
O112 K24' S20 56.9(11) 1_545 .
O141 K24' S20 107.5(16) 1_545 .
Se2 K24' S20 50.5(8) . .
O187 K24' K7 70.5(16) 1_445 1_545
O112 K24' K7 36.5(8) 1_545 1_545
O141 K24' K7 39.7(8) 1_545 1_545
Se2 K24' K7 138.5(16) . 1_545
S20 K24' K7 90.7(12) . 1_545
O158 K25 O174 84(2) . 1_655
O158 K25 O4 118(2) . .
O174 K25 O4 152(2) 1_655 .
O158 K25 O177 156(2) . 1_545
O174 K25 O177 94(2) 1_655 1_545
O4 K25 O177 58.1(13) . 1_545
O158 K25 S26 71.5(14) . .
O174 K25 S26 129.3(19) 1_655 .
O4 K25 S26 53.7(8) . .
O177 K25 S26 92.0(14) 1_545 .
O158 K25 K26 56.5(14) . 2_765
O174 K25 K26 86.6(16) 1_655 2_765
O4 K25 K26 119.4(16) . 2_765
O177 K25 K26 147.0(17) 1_545 2_765
S26 K25 K26 112.8(13) . 2_765
O158 K25 K27 117.7(18) . 1_655
O174 K25 K27 33.8(12) 1_655 1_655
O4 K25 K27 120.1(15) . 1_655
O177 K25 K27 62.1(13) 1_545 1_655
S26 K25 K27 133.9(13) . 1_655
K26 K25 K27 108.1(11) 2_765 1_655
O158 K25 K17 98.8(17) . 1_655
O174 K25 K17 54.5(14) 1_655 1_655
O4 K25 K17 129.9(15) . 1_655
O177 K25 K17 99.3(15) 1_545 1_655
S26 K25 K17 167.9(15) . 1_655
K26 K25 K17 55.1(9) 2_765 1_655
K27 K25 K17 56.8(9) 1_655 1_655
O158 K25' O4 99.1(18) . .
O158 K25' K27 133(2) . 1_655
O4 K25' K27 127.8(16) . 1_655
O158 K25' Na1' 138(2) . 1_545
O4 K25' Na1' 40.4(9) . 1_545
K27 K25' Na1' 87.8(13) 1_655 1_545
O158 K25' K17 98.9(17) . 1_655
O4 K25' K17 122.8(16) . 1_655
K27 K25' K17 62.7(10) 1_655 1_655
Na1' K25' K17 113.0(14) 1_545 1_655
O158 K25' K26 51.0(13) . 2_765
O4 K25' K26 102.1(15) . 2_765
K27 K25' K26 114.1(13) 1_655 2_765
Na1' K25' K26 131.6(15) 1_545 2_765
K17 K25' K26 54.2(9) 1_655 2_765
O165 K26 O147 113.0(17) . .
O165 K26 O148 131.4(18) . .
O147 K26 O148 110.5(15) . .
O165 K26 O13 130.9(17) . .
O147 K26 O13 90.4(12) . .
O148 K26 O13 68.0(11) . .
O165 K26 O12 79.3(14) . .
O147 K26 O12 80.4(12) . .
O148 K26 O12 129.0(14) . .
O13 K26 O12 62.1(7) . .
O165 K26 S27 76.5(13) . .
O147 K26 S27 134.9(14) . .
O148 K26 S27 87.8(11) . .
O13 K26 S27 57.9(7) . .
O12 K26 S27 57.4(6) . .
O165 K26 K21 60.3(12) . 2_765
O147 K26 K21 164.8(15) . 2_765
O148 K26 K21 72.0(11) . 2_765
O13 K26 K21 104.1(10) . 2_765
O12 K26 K21 110.1(11) . 2_765
S27 K26 K21 59.0(7) . 2_765
O165 K26 Mo28 109.8(15) . .
O147 K26 Mo28 109.4(12) . .
O148 K26 Mo28 73.9(10) . .
O13 K26 Mo28 22.8(4) . .
O12 K26 Mo28 56.0(6) . .
S27 K26 Mo28 35.0(3) . .
K21 K26 Mo28 85.8(8) 2_765 .
O165 K26 Mo29 76.8(13) . .
O147 K26 Mo29 102.2(12) . .
O148 K26 Mo29 113.8(12) . .
O13 K26 Mo29 55.7(6) . .
O12 K26 Mo29 22.9(4) . .
S27 K26 Mo29 34.6(4) . .
K21 K26 Mo29 89.8(8) 2_765 .
Mo28 K26 Mo29 40.9(3) . .
O165 K26 K17 166.6(17) . 2_665
O147 K26 K17 70.2(12) . 2_665
O148 K26 K17 41.1(11) . 2_665
O13 K26 K17 60.6(9) . 2_665
O12 K26 K17 114.0(11) . 2_665
S27 K26 K17 110.9(10) . 2_665
K21 K26 K17 113.0(11) 2_765 2_665
Mo28 K26 K17 80.1(9) . 2_665
Mo29 K26 K17 115.8(10) . 2_665
O165 K26 K25 103.3(15) . 2_765
O147 K26 K25 64.6(12) . 2_765
O148 K26 K25 77.0(12) . 2_765
O13 K26 K25 125.9(12) . 2_765
O12 K26 K25 143.1(12) . 2_765
S27 K26 K25 159.4(12) . 2_765
K21 K26 K25 102.5(11) 2_765 2_765
Mo28 K26 K25 145.5(11) . 2_765
Mo29 K26 K25 166.0(11) . 2_765
K17 K26 K25 65.8(10) 2_665 2_765
O165 K26 K21 28.7(11) . .
O147 K26 K21 130.6(12) . .
O148 K26 K21 118.7(12) . .
O13 K26 K21 103.7(9) . .
O12 K26 K21 66.2(7) . .
S27 K26 K21 47.8(5) . .
K21 K26 K21 50.6(6) 2_765 .
Mo28 K26 K21 81.6(6) . .
Mo29 K26 K21 54.7(5) . .
K17 K26 K21 156.4(11) 2_665 .
K25 K26 K21 129.4(10) 2_765 .
O174 K27 O37 112.1(13) . .
O174 K27 O142 93.6(14) . .
O37 K27 O142 112.2(9) . .
O174 K27 O47 120.1(13) . .
O37 K27 O47 127.7(8) . .
O142 K27 O47 63.4(7) . .
O174 K27 S34 104.4(13) . .
O37 K27 S34 60.7(5) . .
O142 K27 S34 162.0(9) . .
O47 K27 S34 106.5(5) . .
O174 K27 S4 153.3(13) . .
O37 K27 S4 58.8(5) . .
O142 K27 S4 70.5(7) . .
O47 K27 S4 72.7(5) . .
S34 K27 S4 92.6(5) . .
O174 K27 S11 97.3(13) . .
O37 K27 S11 121.8(7) . .
O142 K27 S11 114.7(8) . .
O47 K27 S11 55.5(4) . .
S34 K27 S11 64.0(3) . .
S4 K27 S11 108.7(5) . .
O37 K27 K25' 85.4(9) . 1_455
O142 K27 K25' 83.7(10) . 1_455
O47 K27 K25' 139.4(10) . 1_455
S34 K27 K25' 110.9(10) . 1_455
S4 K27 K25' 119.8(9) . 1_455
S11 K27 K25' 131.5(10) . 1_455
O174 K27 Mo5 106.1(12) . .
O37 K27 Mo5 138.3(6) . .
O142 K27 Mo5 80.5(7) . .
O47 K27 Mo5 23.0(3) . .
S34 K27 Mo5 94.6(4) . .
S4 K27 Mo5 92.6(4) . .
S11 K27 Mo5 34.62(18) . .
K25' K27 Mo5 136.2(9) 1_455 .
O174 K27 Mo24 107.7(12) . .
O37 K27 Mo24 26.9(4) . .
O142 K27 Mo24 138.7(8) . .
O47 K27 Mo24 126.3(5) . .
S34 K27 Mo24 34.2(2) . .
S4 K27 Mo24 75.3(4) . .
S11 K27 Mo24 97.6(4) . .
K25' K27 Mo24 94.0(9) 1_455 .
Mo5 K27 Mo24 124.0(4) . .
O174 K27 K17 60.1(13) . .
O37 K27 K17 137.5(9) . .
O142 K27 K17 37.4(8) . .
O47 K27 K17 73.1(7) . .
S34 K27 K17 158.0(8) . .
S4 K27 K17 107.8(8) . .
S11 K27 K17 100.7(7) . .
K25' K27 K17 66.3(10) 1_455 .
Mo5 K27 K17 76.8(7) . .
Mo24 K27 K17 159.2(7) . .
O174 K27 K25 36.5(13) . 1_455
O37 K27 K25 86.1(8) . 1_455
O142 K27 K25 80.2(9) . 1_455
O47 K27 K25 136.9(8) . 1_455
S34 K27 K25 114.2(8) . 1_455
S4 K27 K25 117.5(8) . 1_455
S11 K27 K25 133.7(8) . 1_455
Mo5 K27 K25 135.6(8) . 1_455
Mo24 K27 K25 96.1(7) . 1_455
K17 K27 K25 63.8(9) . 1_455
O77 Na1 O177 87.6(12) . .
O77 Na1 O176 102.4(15) . .
O177 Na1 O176 122.4(19) . .
O77 Na1 O5 165.6(6) . 1_565
O177 Na1 O5 90.9(12) . 1_565
O176 Na1 O5 90.6(15) . 1_565
O77 Na1 O175 121.7(12) . 1_665
O177 Na1 O175 66.5(16) . 1_665
O176 Na1 O175 60.2(19) . 1_665
O5 Na1 O175 70.4(11) 1_565 1_665
O77 Na1 O6 109.9(5) . 1_565
O177 Na1 O6 109.2(12) . 1_565
O176 Na1 O6 119.3(16) . 1_565
O5 Na1 O6 57.2(4) 1_565 1_565
O175 Na1 O6 127.5(11) 1_665 1_565
O77 Na1 Mo12 138.8(5) . 1_565
O177 Na1 Mo12 88.5(11) . 1_565
O176 Na1 Mo12 114.2(15) . 1_565
O5 Na1 Mo12 26.8(3) 1_565 1_565
O175 Na1 Mo12 93.8(11) 1_665 1_565
O6 Na1 Mo12 34.9(3) 1_565 1_565
O4 Na1' O77 120.7(17) 1_565 .
O4 Na1' O175 115.3(18) 1_565 1_665
O77 Na1' O175 118.4(19) . 1_665
O4 Na1' K25' 53.6(12) 1_565 1_565
O77 Na1' K25' 134.1(16) . 1_565
O175 Na1' K25' 99.1(18) 1_665 1_565
O4 Na1' K3 127.7(14) 1_565 1_665
O77 Na1' K3 42.8(7) . 1_665
O175 Na1' K3 112.9(16) 1_665 1_665
K25' Na1' K3 100.1(12) 1_565 1_665
Mo3 O1 K11 113.2(7) . 2_776
C3 O2 Mo3 126.2(10) . .
C2 O3 Mo12 133.1(11) . .
C2 O3 Mo19 137.5(12) . .
Mo12 O3 Mo19 89.3(5) . .
Mo12 O4 Mo19 99.9(6) . .
Mo12 O4 Na1' 105.0(11) . 1_545
Mo19 O4 Na1' 105.3(11) . 1_545
Mo12 O4 K25 123.9(11) . .
Mo19 O4 K25 124.2(12) . .
Mo12 O4 K25' 123.6(10) . .
Mo19 O4 K25' 130.8(11) . .
Na1' O4 K25' 86.1(14) 1_545 .
Mo12 O5 Na1 101.3(7) . 1_545
Mo12 O6 Mo19 101.0(6) . .
Mo12 O6 K20 117.3(7) . .
Mo19 O6 K20 127.3(8) . .
Mo12 O6 Na1 89.8(5) . 1_545
Mo19 O6 Na1 99.6(6) . 1_545
K20 O6 Na1 114.5(7) . 1_545
Mo18 O8 K4' 99.4(10) . 1_545
Mo18 O8 K18 136.5(9) . 1_545
K4' O8 K18 113.4(9) 1_545 1_545
Mo29 O9 Mo18 101.0(6) . .
Mo29 O9 K21 123.1(8) . .
Mo18 O9 K21 124.6(9) . .
Mo29 O9 K4' 93.4(8) . 1_545
Mo18 O9 K4' 80.9(7) . 1_545
K21 O9 K4' 123.1(9) . 1_545
Mo18 O10 Mo29 99.1(6) . .
Mo18 O10 K4' 87.8(8) . 1_545
Mo29 O10 K4' 100.7(8) . 1_545
C1 O11 Mo29 133.4(11) . .
C1 O11 Mo18 136.5(12) . .
Mo29 O11 Mo18 89.9(5) . .
Mo29 O12 K8 123.3(8) . 2_665
Mo29 O12 K26 107.0(9) . .
K8 O12 K26 115.1(8) 2_665 .
Mo28 O13 K26 112.0(10) . .
Se7 O15 Mo28 130.1(8) . .
Se7 O15 K9 117.0(6) . .
Mo28 O15 K9 112.7(6) . .
Se2 O16 Mo28 124.6(7) . .
Se2 O16 K9 126.8(7) . .
Mo28 O16 K9 107.2(6) . .
Se2 O16 K9' 90.6(6) . .
Mo28 O16 K9' 144.5(7) . .
Se2 O17 Mo5 123.8(8) . .
Se2 O17 K9' 117.8(8) . .
Mo5 O17 K9' 118.4(6) . .
Se2 O17 K9" 116.4(10) . .
Mo5 O17 K9" 117.4(9) . .
Se7 O18 K21 117.7(8) . 2_765
Se7 O19 Mo13 132.0(7) . .
Se7 O19 K9 97.6(6) . .
Mo13 O19 K9 99.7(5) . .
Se8 O20 Mo13 125.1(7) . .
Se8 O20 K9 116.2(6) . .
Mo13 O20 K9 118.7(5) . .
Mo13 O21 K9 88.8(4) . .
Se6 O23 Mo1 125.2(6) . .
Se6 O23 K2 119.4(6) . .
Mo1 O23 K2 113.8(5) . .
Se5 O24 Mo1 129.7(7) . .
Se5 O24 K2 107.5(5) . .
Mo1 O24 K2 115.1(5) . .
Se5 O25 Mo3 127.1(7) . .
Se5 O25 K2 89.4(5) . .
Mo3 O25 K2 137.6(6) . .
Se1 O26 Mo3 123.5(6) . .
Se1 O27 Mo9 124.6(7) . .
Se1 O27 K5 120.9(6) . .
Mo9 O27 K5 112.9(5) . .
Se1 O28 Mo20 125.1(7) . .
C8 O29 Mo20 124.8(11) . .
C8 O29 K5 100.7(10) . .
Mo20 O29 K5 124.9(5) . .
Mo20 O30 K6 121.3(9) . .
Mo20 O30 K20 152.1(8) . .
K6 O30 K20 75.2(7) . .
Mo20 O30 K11 99.8(6) . 2_776
K6 O30 K11 111.6(7) . 2_776
K20 O30 K11 93.2(6) . 2_776
Mo21 O31 K6 114.5(8) . .
Mo22 O32 Mo21 99.1(6) . .
Mo22 O32 K22 115.7(8) . .
Mo21 O32 K22 124.0(7) . .
Mo22 O33 Mo21 101.3(7) . .
Mo22 O33 K24 121.2(8) . .
Mo21 O33 K24 119.0(8) . .
C5 O34 Mo21 132.7(12) . .
C5 O34 Mo22 136.3(13) . .
Mo21 O34 Mo22 90.8(6) . .
Mo22 O35 K3 116.8(8) . .
Mo22 O35 K10 130.6(8) . 1_445
K3 O35 K10 105.2(5) . 1_445
Mo23 O36 K3 116.4(9) . .
Mo23 O37 Mo24 101.6(7) . .
Mo23 O37 K27 121.2(9) . .
Mo24 O37 K27 117.9(8) . .
Mo24 O38 Mo23 99.9(7) . .
Mo24 O38 K14 124.1(8) . .
Mo23 O38 K14 114.1(8) . .
C6 O39 Mo24 133.0(13) . .
C6 O39 Mo23 135.3(14) . .
Mo24 O39 Mo23 91.7(5) . .
C7 O41 Mo25 123.9(11) . .
C7 O41 K5 99.5(10) . .
Mo25 O41 K5 122.1(5) . .
Mo25 O42 K12 156.3(8) . 1_455
Se3 O43 Mo25 126.0(7) . .
Se3 O44 Mo9 128.8(7) . .
Se3 O44 K5 109.1(6) . .
Mo9 O44 K5 114.7(5) . .
Se3 O45 Mo2 129.1(6) . .
Se3 O45 K5 89.6(5) . .
Mo2 O45 K5 139.8(5) . .
Mo5 O47 K24 135.2(9) . .
Mo5 O47 K27 105.5(7) . .
K24 O47 K27 111.2(7) . .
Se4 O48 Mo5 132.2(9) . .
Se4 O48 K9" 99.1(9) . .
Mo5 O48 K9" 111.9(9) . .
Se4 O48 K9' 98.6(7) . .
Mo5 O48 K9' 104.1(6) . .
Se4 O49 K17 124.8(12) . .
Se4 O50 Mo27 129.2(8) . .
Se4 O50 K9' 114.0(8) . .
Mo27 O50 K9' 116.7(7) . .
Se4 O50 K9" 106.5(10) . .
Mo27 O50 K9" 123.7(10) . .
Mo27 O51 K15 123.3(9) . 2_675
Mo27 O51 K8 119.6(7) . .
K15 O51 K8 79.1(6) 2_675 .
Se8 O53 Mo27 125.2(7) . .
Se8 O53 K9' 131.5(7) . .
Mo27 O53 K9' 102.4(6) . .
Se8 O53 K9 93.0(5) . .
Mo27 O53 K9 141.7(6) . .
Mo11 O55 K8 117.8(7) . .
Mo11 O55 K15 116.2(8) . 2_675
K8 O55 K15 76.0(6) . 2_675
Mo11 O56 Mo26 101.9(6) . .
Mo26 O57 Mo11 100.0(6) . .
C10 O59 Mo11 134.9(11) . .
C10 O59 Mo26 134.1(11) . .
Mo11 O59 Mo26 90.6(5) . .
Mo4 O60 K10 93.9(6) . 1_455
C9 O61 Mo7 132.9(10) . .
C9 O61 Mo4 135.9(11) . .
Mo7 O61 Mo4 89.8(4) . .
Mo7 O62 Mo4 100.5(5) . .
Mo7 O62 K10 98.3(5) . 1_455
Mo4 O62 K10 101.3(6) . 1_455
Mo7 O63 Mo4 101.9(6) . .
Mo7 O63 K10 84.9(5) . 1_455
Mo4 O63 K10 87.5(5) . 1_455
Mo7 O64 K19 113.8(7) . .
Mo7 O64 K10 96.8(6) . 1_455
K19 O64 K10 126.9(6) . 1_455
Mo2 O65 K19' 124.4(10) . .
Mo2 O65 K19 114.7(7) . .
C12 O66 Mo2 125.7(10) . .
Se6 O67 Mo2 120.8(6) . .
Se6 O68 Mo30 124.4(6) . .
Mo30 O69 K7 119.1(7) . .
Mo30 O69 K19 105.7(7) . .
K7 O69 K19 104.3(6) . .
Se13 O70 Mo30 126.9(7) . .
Se13 O70 K19' 122.1(11) . .
Mo30 O70 K19' 110.8(10) . .
Se13 O70 K19 131.3(7) . .
Mo30 O70 K19 101.6(5) . .
Se13 O71 Mo33 123.8(7) . .
Se13 O72 Mo32 122.0(7) . .
Se12 O73 Mo33 125.0(7) . .
Se12 O74 Mo20 127.7(7) . 2_776
Se12 O74 K11 128.9(7) . .
Mo20 O74 K11 103.4(5) 2_776 .
Se12 O75 Mo32 124.6(8) . .
Mo33 O76 K20 141.3(8) . 1_565
Mo34 O77 Na1 132.6(9) . .
Mo34 O77 Na1' 159.6(13) . .
Mo34 O77 K3 96.7(6) . 1_665
Na1 O77 K3 125.1(6) . 1_665
Na1' O77 K3 99.9(11) . 1_665
Mo34 O78 Mo16 99.3(6) . .
Mo34 O78 K3 93.3(5) . 1_665
Mo16 O78 K3 95.4(5) . 1_665
Mo34 O79 Mo16 98.8(5) . .
Mo34 O79 K16 117.3(7) . .
Mo16 O79 K16 116.3(7) . .
Mo34 O79 K3 89.1(5) . 1_665
Mo16 O79 K3 91.4(5) . 1_665
K16 O79 K3 135.7(6) . 1_665
Se9 O80 Mo34 130.8(7) . .
Se9 O80 Mo16 128.9(8) . .
Mo34 O80 Mo16 88.0(4) . .
Mo16 O81 K10 136.5(8) . .
Mo16 O81 K3 96.1(6) . 1_665
K10 O81 K3 111.0(5) . 1_665
Se11 O83 Mo17 122.5(7) . .
Se11 O83 K12 104.2(6) . .
Mo17 O83 K12 113.3(6) . .
Se11 O84 Mo25 129.5(8) . 2_776
Se11 O85 Mo10 122.3(7) . .
Se11 O85 K12' 139.8(11) . .
Mo10 O85 K12' 95.4(10) . .
Se11 O85 K12 100.4(6) . .
Mo10 O85 K12 113.7(6) . .
Se10 O86 Mo17 123.7(7) . .
Se10 O86 K12 105.2(6) . .
Mo17 O86 K12 112.1(6) . .
Mo32 O87 K13 134.0(8) . .
Mo32 O87 K13 164.5(8) . 2_776
K13 O87 K13 31.9(7) . 2_776
Mo10 O88 K13 129.8(8) . .
Mo10 O88 K12' 98.6(9) . .
K13 O88 K12' 131.1(10) . .
Se10 O89 Mo10 121.7(7) . .
Se10 O89 K12 100.2(6) . .
Mo10 O89 K12 110.0(6) . .
Se10 O89 K12' 142.4(10) . .
Mo10 O89 K12' 86.7(8) . .
Se10 O90 Mo15 129.5(7) . .
Se5 O91 Mo15 124.2(6) . .
Mo14 O94 Mo8 101.0(5) . .
Mo14 O94 K4 95.2(4) . 2_775
Mo8 O94 K4 123.8(5) . 2_775
Mo8 O95 Mo14 99.8(5) . .
Mo14 O96 K4 106.5(6) . 2_775
Mo14 O96 K1 112.6(6) . 2_775
K4 O96 K1 140.7(5) 2_775 2_775
Mo6 O97 K1 115.3(6) . 2_775
Mo6 O97 K4 107.7(6) . .
K1 O97 K4 136.9(5) 2_775 .
Mo6 O97 K4' 103.8(8) . .
K1 O97 K4' 109.7(8) 2_775 .
Mo31 O98 Mo6 101.4(5) . .
Mo31 O98 K23 116.6(7) . .
Mo6 O98 K23 124.7(7) . .
Mo31 O98 K4 132.5(5) . .
Mo6 O98 K4 94.8(5) . .
K23 O98 K4 87.9(6) . .
Mo31 O99 Mo6 101.0(5) . .
Mo31 O99 K4' 112.4(8) . .
Mo6 O99 K4' 96.7(8) . .
C13 O100 Mo15 124.1(12) . .
C13 O100 K2 97.9(11) . .
Mo15 O100 K2 123.4(4) . .
C16 O101 Mo8 134.0(12) . .
C16 O101 Mo14 134.9(12) . .
Mo8 O101 Mo14 91.1(5) . .
C15 O102 Mo31 133.0(12) . .
C15 O102 Mo6 135.8(12) . .
Mo31 O102 Mo6 90.8(4) . .
Mo31 O103 K7 110.4(6) . .
C14 O104 Mo30 123.5(11) . .
C14 O104 K2 98.4(10) . .
Mo30 O104 K2 126.4(5) . .
Mo13 O106 K1 141.2(7) . .
Mo13 O106 K23 130.4(7) . .
K1 O106 K23 87.4(5) . .
Se9 O109 Mo10 114.3(6) . .
Se9 O110 Mo32 115.6(7) . .
K7 O112 K24' 99.2(13) . 1_565
K18 O113 K16 98.1(7) . .
K4 O116 K23 79.6(5) . .
K7 O119 K20 97.5(10) 1_545 .
K2 O120 K5 152.2(7) . .
K1 O122 K23 86.0(7) . .
K18 O124 K1 102.7(7) 2_775 .
K19' O128 K11 141.9(11) . .
K19 O128 K11 141.2(7) . .
K14 O132 K22 118.5(9) 2_776 2_776
K13 O137 K13 24.5(8) . 2_776
K20 O141 K7 91.3(9) 1_565 .
K20 O141 K24' 158.9(15) 1_565 1_565
K7 O141 K24' 90.4(13) . 1_565
K17 O142 K27 102.7(13) . .
K8 O144 K4 94.3(11) . 2_675
K19 O145 K7 101.1(12) . .
K17 O148 K26 93.3(16) 2_665 .
K4 O153 K8 96.9(11) . 2_675
K11 O154 K20 117.9(13) . 2_776
K10 O160 K14 116(2) . 2_776
K26 O165 K21 127.3(18) . .
K26 O165 K21 77.0(14) . 2_765
K21 O165 K21 76.3(11) . 2_765
K17 O167 K9 136.0(19) . 2_665
K27 O174 K25 110(2) . 1_455
Na1 O176 K22 115(2) . 2_776
Na1 O177 K25 120(2) . 1_565
K6 O178 K6 120.7(16) . 2_766
K15 O180 K8 89.6(19) . 2_675
K19 O182 K6 144(2) . 1_565
K19' O182 K6 132(2) . 1_565
K13 O185 K5 114.7(19) . 2_776
K9" O189 K9" 106(2) 2_665 .
K4' O202 K8 88.3(14) . 2_675
C19 N1 C17 110(3) . .
C19 N1 C18 111(2) . .
C17 N1 C18 110(2) . .
C19 N1 C20 110(3) . .
C17 N1 C20 99(3) . .
C18 N1 C20 116(3) . .
O11 C1 C2 130.4(15) . .
O11 C1 C4 139.6(17) . .
C2 C1 C4 90.0(13) . .
O11 C1 C3 175.1(15) . .
C2 C1 C3 44.9(7) . .
C4 C1 C3 45.1(7) . .
O3 C2 C1 130.6(15) . .
O3 C2 C3 138.6(17) . .
C1 C2 C3 90.7(13) . .
O3 C2 C4 175.4(15) . .
C1 C2 C4 45.3(7) . .
C3 C2 C4 45.4(7) . .
O2 C3 C2 132.3(16) . .
O2 C3 C4 138.1(14) . .
C2 C3 C4 89.5(13) . .
O2 C3 C1 176.5(14) . .
C2 C3 C1 44.4(7) . .
C4 C3 C1 45.1(7) . .
O14 C4 C1 131.4(16) . .
O14 C4 C3 138.8(15) . .
C1 C4 C3 89.8(13) . .
O14 C4 C2 175.8(15) . .
C1 C4 C2 44.7(7) . .
C3 C4 C2 45.1(7) . .
O34 C5 C6 130.8(17) . .
O34 C5 C8 139.9(18) . .
C6 C5 C8 89.3(14) . .
O34 C5 C7 175.1(16) . .
C6 C5 C7 44.4(8) . .
C8 C5 C7 44.9(8) . .
O39 C6 C7 137.1(18) . .
O39 C6 C5 131.6(18) . .
C7 C6 C5 91.2(14) . .
O39 C6 C8 177.1(18) . .
C7 C6 C8 45.7(8) . .
C5 C6 C8 45.6(8) . .
O41 C7 C6 135.5(16) . .
O41 C7 C8 135.1(16) . .
C6 C7 C8 89.2(14) . .
O41 C7 C5 178.8(16) . .
C6 C7 C5 44.4(8) . .
C8 C7 C5 44.9(7) . .
O29 C8 C5 132.3(16) . .
O29 C8 C7 137.4(16) . .
C5 C8 C7 90.2(14) . .
O29 C8 C6 176.3(17) . .
C5 C8 C6 45.1(8) . .
C7 C8 C6 45.1(8) . .
O61 C9 C10 130.9(14) . .
O61 C9 C12 138.3(15) . .
C10 C9 C12 90.8(13) . .
O61 C9 C11 176.2(13) . .
C10 C9 C11 45.4(7) . .
C12 C9 C11 45.5(7) . .
O59 C10 C9 132.4(14) . .
O59 C10 C11 138.0(15) . .
C9 C10 C11 89.6(13) . .
O59 C10 C12 176.8(14) . .
C9 C10 C12 44.7(7) . .
C11 C10 C12 45.0(7) . .
O52 C11 C10 132.2(15) . .
O52 C11 C12 137.5(15) . .
C10 C11 C12 90.2(13) . .
O52 C11 C9 177.1(14) . .
C10 C11 C9 45.0(7) . .
C12 C11 C9 45.2(7) . .
O66 C12 C9 132.7(16) . .
O66 C12 C11 137.9(15) . .
C9 C12 C11 89.3(13) . .
O66 C12 C10 176.4(14) . .
C9 C12 C10 44.5(7) . .
C11 C12 C10 44.8(7) . .
O100 C13 C16 136.1(18) . .
O100 C13 C14 136.5(18) . .
C16 C13 C14 87.3(15) . .
O104 C14 C15 134.9(17) . .
O104 C14 C13 136.0(17) . .
C15 C14 C13 89.1(15) . .
O104 C14 C16 178.0(16) . .
C15 C14 C16 43.9(11) . .
C13 C14 C16 45.1(11) . .
O102 C15 C16 131.0(18) . .
O102 C15 C14 138.0(17) . .
C16 C15 C14 90.9(16) . .
O101 C16 C15 131.9(18) . .
O101 C16 C13 135.4(18) . .
C15 C16 C13 92.7(16) . .
O101 C16 C14 176.7(16) . .
C15 C16 C14 45.1(11) . .
C13 C16 C14 47.6(11) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Mo1 O105 1.655(12) .
Mo1 O24 2.085(12) .
Mo1 O23 2.099(12) .
Mo1 S8 2.335(5) .
Mo1 S25 2.349(5) .
Mo1 Mo13 2.828(2) .
Mo1 K2 4.110(6) .
Mo2 O65 1.681(13) .
Mo2 O45 2.068(12) .
Mo2 O67 2.112(12) .
Mo2 S12 2.327(5) .
Mo2 S17 2.335(5) .
Mo2 O66 2.480(13) .
Mo2 Mo7 2.844(2) .
Mo3 O1 1.667(14) .
Mo3 O25 2.093(12) .
Mo3 O26 2.116(12) .
Mo3 S26 2.333(6) .
Mo3 S10 2.335(5) .
Mo3 O2 2.475(13) .
Mo3 Mo12 2.838(2) .
Mo4 O60 1.665(14) .
Mo4 O63 2.109(14) .
Mo4 O62 2.130(13) .
Mo4 S2 2.310(6) .
Mo4 S21 2.333(6) .
Mo4 O61 2.359(12) .
Mo4 Mo26 2.855(3) .
Mo4 K10 3.853(11) 1_455
Mo5 O47 1.662(14) .
Mo5 O17 2.070(14) .
Mo5 O48 2.091(14) .
Mo5 S11 2.329(6) .
Mo5 S7 2.337(6) .
Mo5 O107 2.481(14) .
Mo5 Mo9 2.833(3) .
Mo5 K27 4.098(17) .
Mo5 K9' 4.120(18) .
Mo6 O97 1.672(12) .
Mo6 O98 2.110(13) .
Mo6 O99 2.130(12) .
Mo6 S24 2.302(5) .
Mo6 S13 2.317(5) .
Mo6 O102 2.325(12) .
Mo6 Mo14 2.856(2) .
Mo6 K4 3.761(9) .
Mo6 K4' 3.78(3) .
Mo6 K1 3.845(5) 2_775
Mo7 O64 1.691(15) .
Mo7 O63 2.098(13) .
Mo7 O62 2.121(12) .
Mo7 O61 2.269(13) .
Mo7 S12 2.290(5) .
Mo7 S17 2.335(5) .
Mo7 K10 3.764(9) 1_455
Mo7 K19 4.056(15) .
Mo8 O93 1.682(13) .
Mo8 O94 2.127(13) .
Mo8 O95 2.129(12) .
Mo8 O101 2.252(13) .
Mo8 S22 2.312(5) .
Mo8 S18 2.326(6) .
Mo8 Mo15 2.855(2) .
Mo9 O46 1.668(13) .
Mo9 O44 2.099(12) .
Mo9 O27 2.125(13) .
Mo9 S7 2.334(6) .
Mo9 S11 2.342(5) .
Mo9 K5 4.079(7) .
Mo10 O88 1.688(13) .
Mo10 O85 2.103(13) .
Mo10 O89 2.112(13) .
Mo10 S31 2.275(6) .
Mo10 S6 2.282(7) .
Mo10 O109 2.373(12) .
Mo10 Mo32 2.730(3) .
Mo10 K12' 3.71(4) .
Mo10 K13 4.087(18) .
Mo11 O55 1.673(14) .
Mo11 O56 2.102(15) .
Mo11 O57 2.135(13) .
Mo11 O59 2.247(14) .
Mo11 S15 2.303(6) .
Mo11 S14 2.322(6) .
Mo11 Mo27 2.828(3) .
Mo11 K8 4.023(11) .
Mo12 O5 1.689(15) .
Mo12 O6 2.103(14) .
Mo12 O4 2.111(13) .
Mo12 O3 2.272(15) .
Mo12 S26 2.314(6) .
Mo12 S10 2.319(6) .
Mo12 Na1 3.671(9) 1_545
Mo12 K20 4.062(16) .
Mo13 O106 1.673(12) .
Mo13 O20 2.064(13) .
Mo13 O19 2.088(13) .
Mo13 S8 2.329(5) .
Mo13 S25 2.332(5) .
Mo13 O21 2.473(14) .
Mo14 O96 1.688(12) .
Mo14 O94 2.110(12) .
Mo14 O95 2.143(12) .
Mo14 S24 2.309(6) .
Mo14 S13 2.317(5) .
Mo14 O101 2.327(13) .
Mo14 K4 3.756(9) 2_775
Mo14 K1 3.973(5) 2_775
Mo15 O92 1.676(12) .
Mo15 O91 2.106(11) .
Mo15 O90 2.139(13) .
Mo15 S22 2.320(5) .
Mo15 S18 2.330(5) .
Mo15 O100 2.377(12) .
Mo16 O81 1.676(14) .
Mo16 O79 2.131(14) .
Mo16 O78 2.131(14) .
Mo16 S16 2.317(6) .
Mo16 S28 2.318(6) .
Mo16 O80 2.321(12) .
Mo16 Mo17 2.844(3) .
Mo16 Mo34 3.218(3) .
Mo16 K3 3.764(6) 1_665
Mo16 K10 4.106(10) .
Mo16 K16 4.111(16) .
Mo17 O82 1.679(14) .
Mo17 O86 2.084(14) .
Mo17 O83 2.114(13) .
Mo17 S16 2.301(6) .
Mo17 S28 2.308(6) .
Mo18 O8 1.668(14) .
Mo18 O9 2.126(15) .
Mo18 O10 2.139(15) .
Mo18 S30 2.322(7) .
Mo18 S33 2.324(7) .
Mo18 O11 2.328(13) .
Mo18 Mo19 2.859(3) .
Mo18 K4' 3.45(3) 1_545
Mo18 K21 4.113(18) .
Mo19 O7 1.658(14) .
Mo19 O6 2.114(15) .
Mo19 O4 2.140(14) .
Mo19 S30 2.316(7) .
Mo19 S33 2.338(7) .
Mo19 O3 2.358(12) .
Mo20 O30 1.670(14) .
Mo20 O28 2.098(12) .
Mo20 O74 2.127(13) 2_776
Mo20 S1 2.324(6) .
Mo20 S29 2.326(6) .
Mo20 O29 2.418(13) .
Mo20 Mo21 2.838(3) .
Mo20 K6 4.005(19) .
Mo20 K11 4.009(14) 2_776
Mo21 O31 1.694(16) .
Mo21 O33 2.116(15) .
Mo21 O32 2.150(14) .
Mo21 O34 2.238(16) .
Mo21 S1 2.318(6) .
Mo21 S29 2.320(6) .
Mo21 K6 4.08(2) .
Mo22 O35 1.677(15) .
Mo22 O33 2.103(17) .
Mo22 O32 2.139(16) .
Mo22 S3 2.316(8) .
Mo22 S4 2.321(7) .
Mo22 O34 2.345(14) .
Mo22 Mo23 2.862(4) .
Mo22 K3 3.952(7) .
Mo22 K22 4.109(18) .
Mo23 O36 1.691(15) .
Mo23 O37 2.114(16) .
Mo23 O38 2.154(16) .
Mo23 S4 2.302(8) .
Mo23 S3 2.315(7) .
Mo23 O39 2.332(15) .
Mo23 K3 3.940(7) .
Mo23 K14 4.077(19) .
Mo24 O40 1.670(16) .
Mo24 O37 2.116(17) .
Mo24 O38 2.128(17) .
Mo24 O39 2.233(16) .
Mo24 S5 2.320(7) .
Mo24 S34 2.322(6) .
Mo24 Mo25 2.855(3) .
Mo24 K27 4.126(18) .
Mo25 O42 1.671(15) .
Mo25 O43 2.111(12) .
Mo25 O84 2.117(13) 2_776
Mo25 S34 2.323(6) .
Mo25 S5 2.326(6) .
Mo25 O41 2.422(14) .
Mo26 O58 1.663(14) .
Mo26 O56 2.106(14) .
Mo26 O57 2.130(15) .
Mo26 S2 2.313(6) .
Mo26 S21 2.328(6) .
Mo26 O59 2.351(13) .
Mo27 O51 1.662(15) .
Mo27 O50 2.045(14) .
Mo27 O53 2.083(13) .
Mo27 S15 2.316(6) .
Mo27 S14 2.340(6) .
Mo27 K9' 4.043(17) .
Mo27 K15 4.05(2) 2_675
Mo27 K8 4.099(10) .
Mo28 O13 1.691(16) .
Mo28 O15 2.054(13) .
Mo28 O16 2.080(13) .
Mo28 S20 2.320(6) .
Mo28 S27 2.322(6) .
Mo28 Mo29 2.834(3) .
Mo28 K9 4.040(10) .
Mo28 K26 4.04(3) .
Mo29 O12 1.652(16) .
Mo29 O9 2.097(15) .
Mo29 O10 2.143(14) .
Mo29 O11 2.284(15) .
Mo29 S27 2.307(6) .
Mo29 S20 2.323(6) .
Mo29 K4' 3.83(3) 1_545
Mo29 K21 4.060(19) .
Mo29 K26 4.07(3) .
Mo30 O69 1.682(13) .
Mo30 O68 2.110(12) .
Mo30 O70 2.142(13) .
Mo30 S19 2.316(6) .
Mo30 S9 2.324(5) .
Mo30 O104 2.420(12) .
Mo30 Mo31 2.838(2) .
Mo30 K7 3.815(9) .
Mo30 K19 3.999(15) .
Mo30 K19' 4.09(4) .
Mo31 O103 1.661(13) .
Mo31 O99 2.102(13) .
Mo31 O98 2.109(13) .
Mo31 O102 2.261(12) .
Mo31 S19 2.318(5) .
Mo31 S9 2.332(6) .
Mo31 K7 4.089(10) .
Mo31 K23 4.112(16) .
Mo32 O87 1.679(13) .
Mo32 O75 2.081(13) .
Mo32 O72 2.123(13) .
Mo32 S6 2.285(7) .
Mo32 S31 2.287(7) .
Mo32 O110 2.332(13) .
Mo32 K13 4.009(18) .
Mo33 O76 1.656(14) .
Mo33 O73 2.101(13) .
Mo33 O71 2.103(13) .
Mo33 S23 2.308(6) .
Mo33 S32 2.316(6) .
Mo33 Mo34 2.836(3) .
Mo34 O77 1.692(13) .
Mo34 O78 2.091(13) .
Mo34 O79 2.108(14) .
Mo34 O80 2.311(13) .
Mo34 S23 2.316(6) .
Mo34 S32 2.318(6) .
Mo34 K3 3.681(7) 1_665
Mo34 K16 4.115(17) .
Se1 O26 1.693(12) .
Se1 O27 1.716(12) .
Se1 O28 1.724(12) .
Se1 K5 3.920(7) .
Se2 O111 1.70(2) .
Se2 O16 1.698(14) .
Se2 O17 1.714(13) .
Se2 K24' 3.61(6) .
Se2 K9' 3.824(17) .
Se2 K9" 3.92(3) .
Se3 O44 1.684(12) .
Se3 O43 1.699(12) .
Se3 O45 1.707(12) .
Se3 K5 3.644(6) .
Se4 O49 1.650(16) .
Se4 O48 1.684(14) .
Se4 O50 1.706(15) .
Se4 K9" 3.63(3) .
Se4 K9' 3.723(17) .
Se5 O25 1.678(12) .
Se5 O24 1.679(11) .
Se5 O91 1.707(12) .
Se5 K2 3.642(6) .
Se6 O68 1.704(13) .
Se6 O67 1.708(12) .
Se6 O23 1.718(11) .
Se6 K2 3.927(6) .
Se7 O18 1.661(14) .
Se7 O15 1.695(15) .
Se7 O19 1.705(12) .
Se7 K9 3.853(11) .
Se7 K21 3.863(18) 2_765
Se8 O54 1.655(14) .
Se8 O53 1.716(14) .
Se8 O20 1.724(12) .
Se8 K9 3.818(10) .
Se9 O80 1.644(13) .
Se9 O110 1.721(13) .
Se9 O109 1.732(13) .
Se10 O90 1.685(14) .
Se10 O89 1.696(12) .
Se10 O86 1.710(13) .
Se10 K12 3.819(10) .
Se11 O84 1.688(12) .
Se11 O85 1.707(14) .
Se11 O83 1.714(14) .
Se11 K12 3.747(13) .
Se12 O74 1.672(13) .
Se12 O73 1.692(13) .
Se12 O75 1.700(14) .
Se13 O70 1.690(12) .
Se13 O72 1.707(13) .
Se13 O71 1.719(13) .
S1 K24 3.36(2) .
S2 K15 3.59(2) .
S3 K14 3.31(2) .
S3 K22 3.34(2) .
S4 K24 3.41(2) .
S4 K27 3.42(2) .
S4 K3 3.572(9) .
S5 K14 3.627(18) .
S6 K5 3.151(10) 2_776
S9 K7 3.454(11) .
S10 K20 3.340(16) .
S10 K11 3.457(14) 2_776
S11 K27 3.418(17) .
S12 K19 3.494(17) .
S12 K19' 3.78(5) .
S13 K16 3.437(17) .
S13 K1 3.458(7) 2_775
S13 K18 3.57(2) .
S14 K8 3.634(12) .
S15 K15 3.68(3) 2_675
S16 K16 3.282(16) .
S19 K23 3.268(19) .
S20 K24' 3.75(6) .
S23 K16 3.279(18) .
S24 K1 3.342(7) .
S24 K23 3.62(2) .
S26 K25 3.78(5) .
S27 K26 3.32(3) .
S27 K21 3.335(19) 2_765
S27 K21 3.475(19) .
S29 K6 3.61(2) .
S29 K22 3.644(17) .
S30 K7 3.291(11) 1_545
S30 K20 3.68(2) .
S31 K2 3.162(9) .
S33 K21 3.62(2) .
S34 K27 3.344(19) .
K1 O124 2.762(17) .
K1 O122 2.777(18) .
K1 O106 2.782(13) .
K1 O97 2.822(14) 2_775
K1 O114 2.909(15) .
K1 O96 3.007(14) 2_775
K1 S13 3.458(7) 2_775
K1 Mo6 3.845(5) 2_775
K1 K23 3.917(19) .
K1 Mo14 3.973(5) 2_775
K1 K18 4.26(2) 2_775
K2 O24 2.767(13) .
K2 O23 2.786(13) .
K2 O120 2.863(19) .
K2 O117 2.880(16) .
K2 O121 2.93(2) .
K2 O25 3.250(14) .
K2 O104 3.256(14) .
K2 O100 3.264(13) .
K3 O179 2.62(5) .
K3 O139 2.74(3) .
K3 O36 2.89(2) .
K3 O35 2.901(18) .
K3 O78 2.909(15) 1_445
K3 O79 3.051(15) 1_445
K3 O77 3.077(17) 1_445
K3 O81 3.197(17) 1_445
K3 Mo34 3.681(7) 1_445
K3 Mo16 3.764(6) 1_445
K4 O123 2.51(2) .
K4 O116 2.702(16) .
K4 O153 2.74(4) .
K4 O97 2.899(16) .
K4 O96 2.909(16) 2_775
K4 O94 2.922(15) 2_775
K4 O98 2.944(15) .
K4 O144 3.13(4) 2_675
K4 Mo14 3.756(9) 2_775
K4 K23 3.93(2) .
K4 K8 4.229(14) 2_675
K4' O156 2.66(5) 2_775
K4' O8 2.77(4) 1_565
K4' O10 2.80(3) 1_565
K4' O99 2.89(3) .
K4' O97 3.02(3) .
K4' O9 3.08(4) 1_565
K4' O202 3.26(7) .
K4' Mo18 3.45(3) 1_565
K4' Mo29 3.83(3) 1_565
K4' K8 4.60(3) 2_675
K4' K1 4.78(3) 2_775
K5 O44 2.727(13) .
K5 O27 2.751(15) .
K5 O118 2.868(19) .
K5 O120 2.886(19) .
K5 O152 2.90(3) 2_776
K5 S6 3.151(10) 2_776
K5 O185 3.17(6) 2_776
K5 O45 3.231(14) .
K5 O29 3.336(15) .
K5 O41 3.423(15) .
K6 O178 2.84(5) .
K6 O30 2.88(2) .
K6 O182 3.06(7) 1_545
K6 O31 3.08(3) .
K6 O178 3.10(5) 2_766
K6 K20 3.62(3) .
K6 K11 4.76(2) 1_545
K7 O119 2.53(3) 1_565
K7 O112 2.68(2) .
K7 O69 2.703(16) .
K7 O141 2.83(3) .
K7 O145 3.20(4) .
K7 O103 3.201(18) .
K7 S30 3.291(11) 1_565
K7 K20 3.96(2) 1_565
K7 K24' 4.44(6) 1_565
K8 O144 2.62(4) .
K8 O130 2.62(2) .
K8 O180 2.76(6) 2_675
K8 O153 2.91(4) 2_675
K8 O55 2.96(2) .
K8 O51 3.015(18) .
K8 O12 3.07(2) 2_665
K8 O202 3.35(6) 2_675
K8 K15 3.76(3) 2_675
K9' O50 2.69(2) .
K9' O17 2.71(2) .
K9' O134 2.99(6) .
K9' O53 3.05(2) .
K9' O189 3.06(7) 2_665
K9' O48 3.08(2) .
K9' O135 3.18(3) .
K9' O16 3.41(2) .
K9 O167 2.70(4) 2_665
K9 O20 2.730(16) .
K9 O15 2.774(17) .
K9 O16 2.901(17) .
K9 O135 3.06(3) .
K9 O189 3.15(7) 2_665
K9 O19 3.237(17) .
K9 O53 3.323(16) .
K9 O21 3.368(19) .
K9" O50 2.76(4) .
K9" O17 2.84(4) .
K9" O189 2.90(7) 2_665
K9" O189 2.92(8) .
K9" O48 2.96(4) .
K9" O135 3.38(4) .
K9" K9" 4.65(8) 2_665
K9" K17 4.75(6) .
K10 O143 2.62(3) .
K10 O160 2.62(6) .
K10 O81 2.725(17) .
K10 O62 2.819(17) 1_655
K10 O159 2.90(6) .
K10 O64 3.168(17) 1_655
K10 O35 3.25(2) 1_665
K10 O63 3.318(18) 1_655
K10 O60 3.36(2) 1_655
K10 Mo7 3.764(9) 1_655
K10 Mo4 3.853(11) 1_655
K11 O154 2.70(4) .
K11 O74 2.941(18) .
K11 O1 3.227(19) 2_776
K11 O30 3.37(2) 2_776
K11 O128 3.38(2) .
K11 S10 3.457(14) 2_776
K11 Mo20 4.009(14) 2_776
K11 K20 4.68(2) 2_776
K11 K6 4.76(2) 1_565
K12' O172 2.65(6) .
K12' O85 2.87(4) .
K12' O126 2.99(5) 2_776
K12' O88 3.06(4) .
K12' O89 3.18(4) .
K12' O161 3.20(5) .
K12 O161 2.72(3) .
K12 O172 2.83(5) .
K12 O83 2.937(19) .
K12 O86 2.995(16) .
K12 O85 3.04(2) .
K12 O89 3.134(18) .
K12 O42 3.29(2) 1_655
K13 K13 1.46(3) 2_776
K13 O87 2.66(2) .
K13 O87 2.67(2) 2_776
K13 O137 2.74(5) .
K13 O184 2.75(4) .
K13 O185 2.77(6) .
K13 O88 2.79(2) .
K13 O149 3.13(4) .
K13 O137 3.41(5) 2_776
K13 K5 5.01(2) 2_776
K14 O38 2.69(2) .
K14 O160 2.77(6) 2_776
K14 O183 2.85(6) 2_776
K14 O132 2.88(3) 2_776
K14 K22 2.94(2) 2_666
K14 K10 4.58(2) 2_776
K15 O180 2.58(6) .
K15 O133 2.60(3) .
K15 O173 2.80(6) 1_455
K15 O181 2.84(6) .
K15 O51 2.89(3) 2_675
K15 O186 3.08(7) .
K15 O55 3.15(3) 2_675
K15 S15 3.68(3) 2_675
K15 K8 3.76(3) 2_675
K15 Mo27 4.05(2) 2_675
K16 O163 2.61(3) .
K16 O79 2.70(2) .
K16 O115 2.76(2) .
K16 O113 2.78(2) .
K16 K18 4.20(2) .
K17 O167 2.69(6) .
K17 O142 2.70(5) .
K17 O148 2.76(6) 2_665
K17 O49 2.77(5) .
K17 O138 2.88(5) .
K17 K26 4.19(6) 2_665
K17 K27 4.34(5) .
K17 K25' 4.47(7) 1_455
K17 K25 4.66(7) 1_455
K17 K9 4.99(5) 2_665
K18 O146 2.61(4) .
K18 O124 2.69(3) 2_775
K18 O113 2.78(2) .
K18 O125 2.82(3) .
K18 O8 3.38(2) 1_565
K18 K1 4.26(2) 2_775
K19' O70 2.81(5) .
K19' O182 2.91(7) .
K19' O65 2.96(5) .
K19' O128 2.99(5) .
K19 O182 2.49(6) .
K19 O145 2.85(4) .
K19 O70 2.974(19) .
K19 O64 3.07(2) .
K19 O65 3.20(2) .
K19 O69 3.20(2) .
K19 O128 3.37(3) .
K20 O6 2.64(2) .
K20 O141 2.70(3) 1_545
K20 O119 2.73(2) .
K20 O154 2.76(4) 2_776
K20 O30 3.06(2) .
K20 O76 3.13(2) 1_545
K20 K7 3.96(2) 1_545
K20 K11 4.68(2) 2_776
K21 O9 2.52(2) .
K21 O18 2.80(2) 2_765
K21 O165 2.83(5) .
K21 O165 3.08(4) 2_765
K21 S27 3.335(19) 2_765
K21 K26 3.45(4) 2_765
K21 K21 3.65(4) 2_765
K21 Se7 3.863(18) 2_765
K22 O32 2.70(2) .
K22 K14 2.94(2) 2_666
K22 O132 3.02(3) 2_776
K22 O176 3.08(7) 2_776
K23 O98 2.71(2) .
K23 O106 2.889(19) .
K23 O122 2.97(3) .
K23 O116 3.38(2) .
K24 O33 2.68(2) .
K24 O155 2.76(6) .
K24 O47 2.85(2) .
K24 O166 3.19(5) 1_545
K24' O187 2.87(8) 1_445
K24' O112 3.14(6) 1_545
K24' O141 3.40(7) 1_545
K24' K7 4.44(6) 1_545
K25 O158 2.70(6) .
K25 O174 2.82(7) 1_655
K25 O4 2.93(5) .
K25 O177 3.37(7) 1_545
K25 K26 4.38(6) 2_765
K25 K27 4.46(6) 1_655
K25 K17 4.66(7) 1_655
K25' O158 2.96(7) .
K25' O4 3.38(6) .
K25' K27 3.80(6) 1_655
K25' Na1' 4.19(7) 1_545
K25' K17 4.47(7) 1_655
K25' K26 4.71(7) 2_765
K26 O165 2.40(5) .
K26 O147 2.85(5) .
K26 O148 3.00(5) .
K26 O13 3.10(4) .
K26 O12 3.26(4) .
K26 K21 3.45(4) 2_765
K26 K17 4.19(6) 2_665
K26 K25 4.38(6) 2_765
K27 O174 2.64(5) .
K27 O37 2.69(2) .
K27 O142 2.85(3) .
K27 O47 3.33(2) .
K27 K25' 3.80(6) 1_455
K27 K25 4.46(6) 1_455
Na1 O77 2.644(17) .
Na1 O177 2.66(5) .
Na1 O176 2.74(7) .
Na1 O5 2.946(18) 1_565
Na1 O175 2.96(6) 1_665
Na1 O6 3.016(17) 1_565
Na1 Mo12 3.671(9) 1_565
Na1' O4 2.72(5) 1_565
Na1' O77 2.74(4) .
Na1' O175 2.96(7) 1_665
Na1' K25' 4.19(7) 1_565
Na1' K3 4.46(4) 1_665
O1 K11 3.227(19) 2_776
O2 C3 1.289(19) .
O3 C2 1.284(19) .
O4 Na1' 2.72(5) 1_545
O5 Na1 2.946(18) 1_545
O6 Na1 3.016(17) 1_545
O8 K4' 2.77(4) 1_545
O8 K18 3.38(2) 1_545
O9 K4' 3.08(4) 1_545
O10 K4' 2.80(3) 1_545
O11 C1 1.28(2) .
O12 K8 3.07(2) 2_665
O14 C4 1.29(2) .
O18 K21 2.80(2) 2_765
O29 C8 1.29(2) .
O30 K11 3.37(2) 2_776
O34 C5 1.27(2) .
O35 K10 3.25(2) 1_445
O39 C6 1.29(2) .
O41 C7 1.27(2) .
O42 K12 3.29(2) 1_455
O51 K15 2.89(3) 2_675
O52 C11 1.30(2) .
O55 K15 3.15(3) 2_675
O59 C10 1.275(18) .
O60 K10 3.36(2) 1_455
O61 C9 1.284(18) .
O62 K10 2.819(17) 1_455
O63 K10 3.318(18) 1_455
O64 K10 3.168(17) 1_455
O66 C12 1.30(2) .
O74 Mo20 2.127(13) 2_776
O76 K20 3.13(2) 1_565
O77 K3 3.077(17) 1_665
O78 K3 2.909(15) 1_665
O79 K3 3.051(15) 1_665
O81 K3 3.198(17) 1_665
O84 Mo25 2.117(13) 2_776
O87 K13 2.67(2) 2_776
O94 K4 2.922(15) 2_775
O96 K4 2.909(16) 2_775
O96 K1 3.007(14) 2_775
O97 K1 2.822(14) 2_775
O100 C13 1.24(2) .
O101 C16 1.28(2) .
O102 C15 1.27(2) .
O104 C14 1.25(2) .
O112 K24' 3.14(6) 1_565
O119 K7 2.53(3) 1_545
O124 K18 2.69(3) 2_775
O126 K12' 2.99(5) 2_776
O132 K14 2.88(3) 2_776
O132 K22 3.02(3) 2_776
O137 K13 3.41(5) 2_776
O141 K20 2.70(3) 1_565
O141 K24' 3.40(7) 1_565
O144 K4 3.13(4) 2_675
O148 K17 2.76(6) 2_665
O152 K5 2.90(3) 2_776
O153 K8 2.91(4) 2_675
O154 K20 2.75(4) 2_776
O156 K4' 2.66(5) 2_775
O160 K14 2.77(6) 2_776
O165 K21 3.08(4) 2_765
O166 K24 3.19(5) 1_565
O167 K9 2.70(4) 2_665
O173 K15 2.80(6) 1_655
O174 K25 2.82(7) 1_455
O175 Na1' 2.96(7) 1_445
O175 Na1 2.96(6) 1_445
O176 K22 3.08(7) 2_776
O177 K25 3.37(7) 1_565
O178 K6 3.10(5) 2_766
O180 K8 2.76(6) 2_675
O182 K6 3.06(7) 1_565
O183 K14 2.85(6) 2_776
O185 K5 3.17(6) 2_776
O187 K24' 2.87(8) 1_665
O189 K9" 2.90(7) 2_665
O189 K9' 3.06(7) 2_665
O189 K9 3.15(7) 2_665
O202 K8 3.35(6) 2_675
N1 C19 1.43(4) .
N1 C17 1.50(5) .
N1 C18 1.51(3) .
N1 C20 1.51(5) .
C1 C2 1.396(10) .
C1 C4 1.412(10) .
C1 C3 1.99(2) .
C2 C3 1.407(10) .
C2 C4 1.99(2) .
C3 C4 1.414(10) .
C5 C6 1.401(10) .
C5 C8 1.413(10) .
C5 C7 2.00(2) .
C6 C7 1.401(10) .
C6 C8 1.98(2) .
C7 C8 1.414(10) .
C9 C10 1.404(10) .
C9 C12 1.408(10) .
C9 C11 1.98(2) .
C10 C11 1.412(10) .
C10 C12 2.00(2) .
C11 C12 1.415(10) .
C13 C16 1.44(3) .
C13 C14 1.50(3) .
C14 C15 1.44(3) .
C14 C16 2.03(3) .
C15 C16 1.41(3) .
