#------------------------------------------------------------------------------
#$Date: 2019-01-18 01:06:46 +0200 (Fri, 18 Jan 2019) $
#$Revision: 213188 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/12/28/7122868.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7122868
loop_
_publ_author_name
'So, Cheuk-Wai'
'Ismail , Muhammad Luthfi Bin'
_publ_section_title
;
 Synthesis of a Dimeric Phosphine-Stabilized
 Phosphidogermanium(I)-Amidogermanium(II) Derivative
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/C8CC09454C
_journal_year                    2019
_chemical_formula_sum            'C43 H45 Cl Ge2 N P2'
_chemical_formula_weight         818.37
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_audit_update_record
;
2018-11-19 deposited with the CCDC.
2019-01-17 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 103.3601(8)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   11.7897(2)
_cell_length_b                   16.3455(2)
_cell_length_c                   20.0346(3)
_cell_measurement_reflns_used    8835
_cell_measurement_temperature    123.(2)
_cell_measurement_theta_max      66.33
_cell_measurement_theta_min      3.53
_cell_volume                     3756.35(10)
_computing_cell_refinement       'SAINT V8.38A (Bruker AXS Inc., 2017)'
_computing_data_collection       'APEX3 (Bruker AXS Inc., 2017)'
_computing_data_reduction        'SAINT V8.38A (Bruker AXS Inc., 2017)'
_computing_molecular_graphics    'XP (Bruker AXS Inc., 2017)'
_computing_publication_material  'APEX3 (Bruker AXS Inc., 2017)'
_computing_structure_refinement  'SHELXL-2016/6 (Sheldrick, 2016)'
_computing_structure_solution    'SHELXT (Bruker AXS Inc., 2017)'
_diffrn_ambient_temperature      123.(2)
_diffrn_detector_area_resol_mean 8.3333
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  'Multilayer Mirror'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54178
_diffrn_reflns_av_R_equivalents  0.1040
_diffrn_reflns_av_unetI/netI     0.0591
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            70144
_diffrn_reflns_theta_full        66.78
_diffrn_reflns_theta_max         66.78
_diffrn_reflns_theta_min         3.53
_diffrn_source                   'Incoatec Microfocus Source'
_diffrn_source_type              'Bruker Kappa Duo APEX2'
_exptl_absorpt_coefficient_mu    3.668
_exptl_absorpt_correction_T_max  0.96
_exptl_absorpt_correction_T_min  0.30
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction
;
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.447
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1684
_exptl_crystal_size_max          0.040
_exptl_crystal_size_mid          0.020
_exptl_crystal_size_min          0.010
_refine_diff_density_max         2.358
_refine_diff_density_min         -0.847
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.038
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     447
_refine_ls_number_reflns         6637
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.038
_refine_ls_R_factor_all          0.0655
_refine_ls_R_factor_gt           0.0527
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0822P)²+5.6051P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1389
_refine_ls_wR_factor_ref         0.1505
_reflns_number_gt                5389
_reflns_number_total             6637
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c8cc09454c2.cif
_cod_data_source_block           scw1568s
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-Scan' changed to
'multi-scan' according to
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4973 2017-02-22 13:04:09Z antanas 
;
_cod_database_code               7122868
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_posn
_atom_site_occupancy
Ge Ge1 0.66092(4) 0.52686(3) 0.05374(2) 0.03160(16) Uani d . . 1
Ge Ge2 0.96035(4) 0.57288(3) -0.01023(2) 0.03362(16) Uani d . . 1
C C1 0.7515(3) 0.6304(2) 0.1673(2) 0.0303(8) Uani d . . 1
C C2 0.6995(4) 0.7079(2) 0.1516(2) 0.0320(8) Uani d . . 1
C C3 0.6646(4) 0.7430(2) 0.0797(2) 0.0360(9) Uani d . . 1
H H3 0.696083 0.706233 0.048424 0.043 Uiso calc U R 1
C C4 0.7119(4) 0.8290(3) 0.0737(2) 0.0425(10) Uani d . . 1
H H4A 0.672279 0.867867 0.097836 0.064 Uiso calc U R 1
H H4B 0.697951 0.84435 0.025193 0.064 Uiso calc U R 1
H H4C 0.795843 0.829939 0.094191 0.064 Uiso calc U R 1
C C5 0.5314(4) 0.7425(3) 0.0565(2) 0.0460(11) Uani d . . 1
H H5A 0.502429 0.68691 0.060076 0.069 Uiso calc U R 1
H H5B 0.507952 0.76105 0.008753 0.069 Uiso calc U R 1
H H5C 0.498653 0.779356 0.085778 0.069 Uiso calc U R 1
C C6 0.6722(4) 0.7527(3) 0.2049(2) 0.0362(9) Uani d . . 1
H H6 0.637894 0.80531 0.19545 0.043 Uiso calc U R 1
C C7 0.6936(4) 0.7230(3) 0.2713(2) 0.0375(9) Uani d . . 1
H H7 0.678394 0.756036 0.307249 0.045 Uiso calc U R 1
C C8 0.7370(4) 0.6451(3) 0.2846(2) 0.0377(9) Uani d . . 1
H H8 0.74855 0.623748 0.329815 0.045 Uiso calc U R 1
C C9 0.7643(4) 0.5969(2) 0.2332(2) 0.0332(9) Uani d . . 1
C C10 0.7972(4) 0.5074(3) 0.2493(2) 0.0351(9) Uani d . . 1
H H10 0.824488 0.484113 0.209602 0.042 Uiso calc U R 1
C C11 0.6886(4) 0.4601(3) 0.2562(3) 0.0409(10) Uani d . . 1
H H11A 0.66262 0.480061 0.296357 0.061 Uiso calc U R 1
H H11B 0.707237 0.401729 0.26188 0.061 Uiso calc U R 1
H H11C 0.626436 0.468241 0.214897 0.061 Uiso calc U R 1
C C12 0.8961(4) 0.4985(3) 0.3135(2) 0.0420(10) Uani d . . 1
H H12A 0.964388 0.529056 0.307254 0.063 Uiso calc U R 1
H H12B 0.916373 0.440562 0.321026 0.063 Uiso calc U R 1
H H12C 0.870755 0.52017 0.353294 0.063 Uiso calc U R 1
C C13 0.7058(4) 0.4601(2) -0.1052(2) 0.0330(9) Uani d . . 1
C C14 0.7483(4) 0.3804(3) -0.0904(2) 0.0409(10) Uani d . . 1
H H14 0.805454 0.370369 -0.049282 0.049 Uiso calc U R 1
C C15 0.7088(4) 0.3168(3) -0.1341(3) 0.0447(11) Uani d . . 1
H H15 0.740202 0.263505 -0.123839 0.054 Uiso calc U R 1
C C16 0.6234(4) 0.3301(3) -0.1931(3) 0.0486(12) Uani d . . 1
H H16 0.594836 0.285722 -0.222876 0.058 Uiso calc U R 1
C C17 0.5797(4) 0.4072(3) -0.2088(3) 0.0482(11) Uani d . . 1
H H17 0.521214 0.416168 -0.249526 0.058 Uiso calc U R 1
C C18 0.6211(4) 0.4728(3) -0.1650(2) 0.0406(10) Uani d . . 1
H H18 0.591077 0.526273 -0.176377 0.049 Uiso calc U R 1
C C19 0.6857(4) 0.6359(3) -0.0834(2) 0.0357(9) Uani d . . 1
C C20 0.7514(4) 0.7007(3) -0.1003(3) 0.0478(11) Uani d . . 1
H H20 0.833022 0.694551 -0.095563 0.057 Uiso calc U R 1
C C21 0.6968(5) 0.7747(3) -0.1243(3) 0.0572(13) Uani d . . 1
H H21 0.741781 0.818668 -0.135484 0.069 Uiso calc U R 1
C C22 0.5787(5) 0.7841(3) -0.1318(3) 0.0537(13) Uani d . . 1
H H22 0.54255 0.834819 -0.147127 0.064 Uiso calc U R 1
C C23 0.5122(5) 0.7196(3) -0.1169(2) 0.0483(11) Uani d . . 1
H H23 0.430241 0.725365 -0.123385 0.058 Uiso calc U R 1
C C24 0.5664(4) 0.6460(3) -0.0924(2) 0.0399(10) Uani d . . 1
H H24 0.520689 0.602185 -0.081672 0.048 Uiso calc U R 1
C C25 1.0256(4) 0.5334(2) 0.1708(2) 0.0336(9) Uani d . . 1
C C26 1.0041(4) 0.4490(3) 0.1680(2) 0.0396(10) Uani d . . 1
H H26 0.941111 0.427756 0.13399 0.048 Uiso calc U R 1
C C27 1.0736(4) 0.3961(3) 0.2143(3) 0.0481(12) Uani d . . 1
H H27 1.058074 0.338974 0.212044 0.058 Uiso calc U R 1
C C28 1.1652(5) 0.4267(3) 0.2636(3) 0.0527(13) Uani d . . 1
H H28 1.211593 0.39075 0.296035 0.063 Uiso calc U R 1
C C29 1.1900(4) 0.5101(3) 0.2661(3) 0.0503(12) Uani d . . 1
H H29 1.25458 0.530578 0.299451 0.06 Uiso calc U R 1
C C30 1.1204(4) 0.5637(3) 0.2197(2) 0.0395(10) Uani d . . 1
H H30 1.137436 0.620585 0.221504 0.047 Uiso calc U R 1
C C31 0.9735(3) 0.7011(2) 0.1283(2) 0.0319(8) Uani d . . 1
C C32 0.9789(4) 0.7319(3) 0.1939(2) 0.0357(9) Uani d . . 1
H H32 0.958925 0.697945 0.227937 0.043 Uiso calc U R 1
C C33 1.0137(4) 0.8126(3) 0.2096(2) 0.0395(10) Uani d . . 1
H H33 1.01831 0.833176 0.254469 0.047 Uiso calc U R 1
C C34 1.0414(4) 0.8627(3) 0.1603(2) 0.0425(10) Uani d . . 1
H H34 1.065271 0.917511 0.171411 0.051 Uiso calc U R 1
C C35 1.0347(4) 0.8335(3) 0.0950(3) 0.0418(10) Uani d . . 1
H H35 1.053236 0.868283 0.060996 0.05 Uiso calc U R 1
C C36 1.0006(4) 0.7527(3) 0.0788(2) 0.0372(9) Uani d . . 1
H H36 0.995866 0.732697 0.033738 0.045 Uiso calc U R 1
C C37 0.7636(5) 0.0857(4) 0.0166(3) 0.0597(14) Uani d . . 1
C C38 0.7754(5) 0.1695(3) 0.0282(3) 0.0532(13) Uani d . . 1
H H38 0.710941 0.204418 0.010702 0.064 Uiso calc U R 1
C C39 0.8784(5) 0.2030(3) 0.0644(3) 0.0555(13) Uani d . . 1
H H39 0.885061 0.260463 0.071259 0.067 Uiso calc U R 1
C C40 0.9723(6) 0.1525(4) 0.0908(3) 0.0643(15) Uani d . . 1
H H40 1.043383 0.175145 0.116245 0.077 Uiso calc U R 1
C C41 0.9625(6) 0.0712(4) 0.0804(3) 0.0630(15) Uani d . . 1
H H41 1.027377 0.037096 0.098893 0.076 Uiso calc U R 1
C C42 0.8602(5) 0.0359(3) 0.0432(3) 0.0587(14) Uani d . . 1
H H42 0.855684 -0.02155 0.035846 0.07 Uiso calc U R 1
C C43 0.6540(7) 0.0491(5) -0.0243(4) 0.089(2) Uani d . . 1
H H43A 0.595586 0.047497 0.003427 0.134 Uiso calc U R 1
H H43B 0.669523 -0.006679 -0.037851 0.134 Uiso calc U R 1
H H43C 0.62469 0.082221 -0.065418 0.134 Uiso calc U R 1
Cl Cl1 0.72366(10) 0.39310(6) 0.07479(6) 0.0401(3) Uani d . . 1
N N1 0.7902(3) 0.58536(19) 0.11313(17) 0.0306(7) Uani d . . 1
P P1 0.75483(9) 0.54178(6) -0.04339(5) 0.0313(2) Uani d . . 1
P P2 0.92830(9) 0.59557(6) 0.10596(5) 0.0292(2) Uani d . . 1
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ge Ge -1.0885 0.8855 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_3
_geom_angle
N1 Ge1 Cl1 . 100.35(10)
N1 Ge1 P1 . 90.16(10)
Cl1 Ge1 P1 . 93.12(4)
P1 Ge2 P2 . 85.90(4)
P1 Ge2 Ge2 3_765 98.88(3)
P2 Ge2 Ge2 3_765 96.81(3)
C9 C1 C2 . 120.4(4)
C9 C1 N1 . 121.0(4)
C2 C1 N1 . 118.6(3)
C6 C2 C1 . 117.8(4)
C6 C2 C3 . 118.0(4)
C1 C2 C3 . 124.0(4)
C2 C3 C4 . 113.5(4)
C2 C3 C5 . 108.7(4)
C4 C3 C5 . 110.4(4)
C2 C3 H3 . 108.0
C4 C3 H3 . 108.0
C5 C3 H3 . 108.0
C3 C4 H4A . 109.5
C3 C4 H4B . 109.5
H4A C4 H4B . 109.5
C3 C4 H4C . 109.5
H4A C4 H4C . 109.5
H4B C4 H4C . 109.5
C3 C5 H5A . 109.5
C3 C5 H5B . 109.5
H5A C5 H5B . 109.5
C3 C5 H5C . 109.5
H5A C5 H5C . 109.5
H5B C5 H5C . 109.5
C7 C6 C2 . 122.0(4)
C7 C6 H6 . 119.0
C2 C6 H6 . 119.0
C8 C7 C6 . 119.3(4)
C8 C7 H7 . 120.3
C6 C7 H7 . 120.3
C7 C8 C9 . 121.3(4)
C7 C8 H8 . 119.4
C9 C8 H8 . 119.4
C8 C9 C1 . 118.8(4)
C8 C9 C10 . 118.4(4)
C1 C9 C10 . 122.6(4)
C9 C10 C11 . 109.1(3)
C9 C10 C12 . 112.1(4)
C11 C10 C12 . 111.5(4)
C9 C10 H10 . 108.0
C11 C10 H10 . 108.0
C12 C10 H10 . 108.0
C10 C11 H11A . 109.5
C10 C11 H11B . 109.5
H11A C11 H11B . 109.5
C10 C11 H11C . 109.5
H11A C11 H11C . 109.5
H11B C11 H11C . 109.5
C10 C12 H12A . 109.5
C10 C12 H12B . 109.5
H12A C12 H12B . 109.5
C10 C12 H12C . 109.5
H12A C12 H12C . 109.5
H12B C12 H12C . 109.5
C18 C13 C14 . 118.2(4)
C18 C13 P1 . 122.0(3)
C14 C13 P1 . 119.7(3)
C15 C14 C13 . 121.2(4)
C15 C14 H14 . 119.4
C13 C14 H14 . 119.4
C14 C15 C16 . 120.0(5)
C14 C15 H15 . 120.0
C16 C15 H15 . 120.0
C17 C16 C15 . 120.1(4)
C17 C16 H16 . 119.9
C15 C16 H16 . 119.9
C16 C17 C18 . 120.2(5)
C16 C17 H17 . 119.9
C18 C17 H17 . 119.9
C13 C18 C17 . 120.2(4)
C13 C18 H18 . 119.9
C17 C18 H18 . 119.9
C24 C19 C20 . 118.7(4)
C24 C19 P1 . 119.4(3)
C20 C19 P1 . 121.7(4)
C19 C20 C21 . 120.0(5)
C19 C20 H20 . 120.0
C21 C20 H20 . 120.0
C22 C21 C20 . 120.5(5)
C22 C21 H21 . 119.8
C20 C21 H21 . 119.8
C21 C22 C23 . 120.0(5)
C21 C22 H22 . 120.0
C23 C22 H22 . 120.0
C22 C23 C24 . 119.7(5)
C22 C23 H23 . 120.1
C24 C23 H23 . 120.1
C19 C24 C23 . 121.0(4)
C19 C24 H24 . 119.5
C23 C24 H24 . 119.5
C30 C25 C26 . 119.1(4)
C30 C25 P2 . 124.8(3)
C26 C25 P2 . 116.1(3)
C27 C26 C25 . 120.8(5)
C27 C26 H26 . 119.6
C25 C26 H26 . 119.6
C28 C27 C26 . 119.7(5)
C28 C27 H27 . 120.1
C26 C27 H27 . 120.1
C27 C28 C29 . 120.3(4)
C27 C28 H28 . 119.8
C29 C28 H28 . 119.8
C28 C29 C30 . 120.2(5)
C28 C29 H29 . 119.9
C30 C29 H29 . 119.9
C25 C30 C29 . 119.7(4)
C25 C30 H30 . 120.1
C29 C30 H30 . 120.1
C36 C31 C32 . 118.9(4)
C36 C31 P2 . 119.8(3)
C32 C31 P2 . 121.2(3)
C31 C32 C33 . 120.0(4)
C31 C32 H32 . 120.0
C33 C32 H32 . 120.0
C34 C33 C32 . 120.4(4)
C34 C33 H33 . 119.8
C32 C33 H33 . 119.8
C35 C34 C33 . 120.2(4)
C35 C34 H34 . 119.9
C33 C34 H34 . 119.9
C34 C35 C36 . 119.8(4)
C34 C35 H35 . 120.1
C36 C35 H35 . 120.1
C31 C36 C35 . 120.6(4)
C31 C36 H36 . 119.7
C35 C36 H36 . 119.7
C38 C37 C42 . 117.9(6)
C38 C37 C43 . 122.0(6)
C42 C37 C43 . 120.1(6)
C39 C38 C37 . 121.4(5)
C39 C38 H38 . 119.3
C37 C38 H38 . 119.3
C38 C39 C40 . 119.7(5)
C38 C39 H39 . 120.2
C40 C39 H39 . 120.2
C41 C40 C39 . 119.8(6)
C41 C40 H40 . 120.1
C39 C40 H40 . 120.1
C40 C41 C42 . 121.8(6)
C40 C41 H41 . 119.1
C42 C41 H41 . 119.1
C41 C42 C37 . 119.4(5)
C41 C42 H42 . 120.3
C37 C42 H42 . 120.3
C37 C43 H43A . 109.5
C37 C43 H43B . 109.5
H43A C43 H43B . 109.5
C37 C43 H43C . 109.5
H43A C43 H43C . 109.5
H43B C43 H43C . 109.5
C1 N1 P2 . 119.2(3)
C1 N1 Ge1 . 111.3(2)
P2 N1 Ge1 . 129.31(19)
C13 P1 C19 . 106.20(19)
C13 P1 Ge2 . 118.83(14)
C19 P1 Ge2 . 105.03(15)
C13 P1 Ge1 . 109.51(14)
C19 P1 Ge1 . 101.09(14)
Ge2 P1 Ge1 . 114.16(4)
N1 P2 C25 . 110.24(18)
N1 P2 C31 . 107.84(17)
C25 P2 C31 . 104.50(19)
N1 P2 Ge2 . 115.41(12)
C25 P2 Ge2 . 112.24(14)
C31 P2 Ge2 . 105.83(14)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
Ge1 N1 . 1.954(3)
Ge1 Cl1 . 2.3154(11)
Ge1 P1 . 2.4631(11)
Ge2 P1 . 2.4140(11)
Ge2 P2 . 2.4709(11)
Ge2 Ge2 3_765 2.5577(9)
C1 C9 . 1.405(6)
C1 C2 . 1.411(6)
C1 N1 . 1.469(5)
C2 C6 . 1.393(6)
C2 C3 . 1.517(6)
C3 C4 . 1.526(6)
C3 C5 . 1.531(6)
C3 H3 . 1.0
C4 H4A . 0.98
C4 H4B . 0.98
C4 H4C . 0.98
C5 H5A . 0.98
C5 H5B . 0.98
C5 H5C . 0.98
C6 C7 . 1.382(6)
C6 H6 . 0.95
C7 C8 . 1.376(6)
C7 H7 . 0.95
C8 C9 . 1.393(6)
C8 H8 . 0.95
C9 C10 . 1.528(6)
C10 C11 . 1.529(6)
C10 C12 . 1.530(6)
C10 H10 . 1.0
C11 H11A . 0.98
C11 H11B . 0.98
C11 H11C . 0.98
C12 H12A . 0.98
C12 H12B . 0.98
C12 H12C . 0.98
C13 C18 . 1.388(6)
C13 C14 . 1.402(6)
C13 P1 . 1.822(4)
C14 C15 . 1.370(6)
C14 H14 . 0.95
C15 C16 . 1.382(7)
C15 H15 . 0.95
C16 C17 . 1.370(7)
C16 H16 . 0.95
C17 C18 . 1.400(7)
C17 H17 . 0.95
C18 H18 . 0.95
C19 C24 . 1.387(7)
C19 C20 . 1.399(6)
C19 P1 . 1.836(4)
C20 C21 . 1.402(7)
C20 H20 . 0.95
C21 C22 . 1.375(8)
C21 H21 . 0.95
C22 C23 . 1.387(8)
C22 H22 . 0.95
C23 C24 . 1.396(7)
C23 H23 . 0.95
C24 H24 . 0.95
C25 C30 . 1.395(6)
C25 C26 . 1.401(6)
C25 P2 . 1.830(4)
C26 C27 . 1.390(7)
C26 H26 . 0.95
C27 C28 . 1.378(8)
C27 H27 . 0.95
C28 C29 . 1.393(8)
C28 H28 . 0.95
C29 C30 . 1.398(7)
C29 H29 . 0.95
C30 H30 . 0.95
C31 C36 . 1.393(6)
C31 C32 . 1.395(6)
C31 P2 . 1.831(4)
C32 C33 . 1.395(6)
C32 H32 . 0.95
C33 C34 . 1.379(7)
C33 H33 . 0.95
C34 C35 . 1.378(7)
C34 H34 . 0.95
C35 C36 . 1.397(6)
C35 H35 . 0.95
C36 H36 . 0.95
C37 C38 . 1.391(8)
C37 C42 . 1.401(8)
C37 C43 . 1.487(9)
C38 C39 . 1.376(8)
C38 H38 . 0.95
C39 C40 . 1.384(8)
C39 H39 . 0.95
C40 C41 . 1.346(9)
C40 H40 . 0.95
C41 C42 . 1.389(9)
C41 H41 . 0.95
C42 H42 . 0.95
C43 H43A . 0.98
C43 H43B . 0.98
C43 H43C . 0.98
N1 P2 . 1.675(4)
