#------------------------------------------------------------------------------
#$Date: 2021-09-06 12:07:55 +0300 (Mon, 06 Sep 2021) $
#$Revision: 268523 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/12/86/7128602.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7128602
loop_
_publ_author_name
'Wang, Yang'
'Del Rosal, Iker'
'Qin, Guorui'
'Zhao, Lanxiao'
'Maron, Laurent'
'Shi, Xianghui'
'Cheng, Jianhua'
_publ_section_title
;
 Scandium and lanthanum hydride complexes stabilized by super-bulky
 penta-arylcyclopentadienyl ligands.
;
_journal_issue                   63
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              7766
_journal_page_last               7769
_journal_paper_doi               10.1039/d1cc01841h
_journal_volume                  57
_journal_year                    2021
_chemical_formula_moiety         'C120  H100  O1  Sc1'
_chemical_formula_sum            'C69 H95 O Sc'
_chemical_formula_weight         985.40
_chemical_name_common            '[(CpAr)Sc(H)(OBu)]2'
_chemical_properties_physical    Air-sensitive,Moisture-sensitive
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     iterative
_atom_sites_solution_secondary   iterative
_audit_creation_method           SHELXL-2018/3
_audit_update_record
;
2020-12-09 deposited with the CCDC.	2021-07-05 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 114.8710(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   16.5086(13)
_cell_length_b                   26.3426(19)
_cell_length_c                   15.7814(12)
_cell_measurement_reflns_used    35980
_cell_measurement_temperature    193(2)
_cell_measurement_theta_max      26.409
_cell_measurement_theta_min      1.422
_cell_volume                     6226.5(8)
_computing_molecular_graphics    'ORTEP-3 for Windows (Farrugia, 2014)'
_computing_publication_material  'WinGX publication routines (Farrugia, 2018)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_structure_solution    'SUPERFLIP (Palatinus & Chapuis,2007)'
_diffrn_ambient_temperature      193(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0645
_diffrn_reflns_av_unetI/netI     0.0789
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -31
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            31757
_diffrn_reflns_point_group_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_theta_full        24.999
_diffrn_reflns_theta_max         24.999
_diffrn_reflns_theta_min         1.546
_exptl_absorpt_coefficient_mu    0.157
_exptl_absorpt_correction_T_max  0.980
_exptl_absorpt_correction_T_min  0.967
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            Colorless
_exptl_crystal_density_diffrn    1.051
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Fragment
_exptl_crystal_F_000             2152
_exptl_crystal_recrystallization_method
'Re-crystallisation from solvent: Hexane'
_exptl_crystal_size_max          0.220
_exptl_crystal_size_mid          0.180
_exptl_crystal_size_min          0.130
_refine_diff_density_max         0.679
_refine_diff_density_min         -0.389
_refine_diff_density_rms         0.065
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.023
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     626
_refine_ls_number_reflns         10920
_refine_ls_number_restraints     16
_refine_ls_restrained_S_all      1.028
_refine_ls_R_factor_all          0.1375
_refine_ls_R_factor_gt           0.0827
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.1177P)²+3.7635P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2029
_refine_ls_wR_factor_ref         0.2406
_reflns_Friedel_coverage         0.000
_reflns_number_gt                6544
_reflns_number_total             10920
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d1cc01841h2.cif
_cod_data_source_block           D160
_cod_depositor_comments
'Adding full bibliography for 7128601--7128603.cif.'
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7128602
_shelx_shelxl_version_number     2018/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.966
_shelx_estimated_absorpt_t_max   0.980
_shelx_res_file
;
TITL 001 in P2(1)/c
    shelx.res
    created by SHELXL-2018/3 at 16:21:59 on 11-Mar-2019
CELL  0.71073  16.5086  26.3426  15.7814   90.000  114.871   90.000
ZERR     4.00   0.0013   0.0019   0.0012    0.000    0.001    0.000
LATT   1
SYMM  - X, 1/2 + Y, 1/2 - Z
SFAC  C    H    O    SC
UNIT  276 380 4 4
MERG   2
OMIT    -2.00  50.00
OMIT    -4   2   4
OMIT     1   9   2
OMIT    -1   0   4
OMIT     4   4   2
OMIT    -1   1   6
OMIT    -3   5   6
OMIT    -3   9   6
OMIT     2   6   3
OMIT    -4   5   2
OMIT    -7   1   5
OMIT     6   7   1
OMIT     2   2   3
OMIT    -6   4   7
OMIT     4   5   0
OMIT    -3   3   3
OMIT     3   2   3
OMIT     0   1   4
OMIT     1   2   1
OMIT    -3   1   1
OMIT    -1   1   5
OMIT    -7   2   6
OMIT     2   3   6
OMIT    -1   7   5
OMIT    -2   7   3
OMIT     3   1   4
OMIT    -2   1   3
OMIT     1   2   0
OMIT     3   3   1
OMIT    -1   1   2
OMIT    -4   5   1
OMIT    -3   2   2
OMIT    -3   4   4
OMIT     0   3   1
OMIT     1   1   1
OMIT    -1   1   4
OMIT     4  10   0
OMIT     0   9   3
OMIT    -4   1   7
OMIT     3   7   0
OMIT    -3  11   5
OMIT    -3   2   4
OMIT     0   2   1
OMIT     2   2   2
OMIT    -5   2   7
SADI C41 C42 C41 C42'
DFIX 1.50 0.01 C42 C43 C42 C44 C42' C43' C42' C44'
EADP C42 C43 C44 C42' C43' C44'
SADI C58 C59 C58 C59'
DFIX 1.50 0.01 C59 C60 C59 C61 C59' C60' C59' C61'
EADP C59 C60 C61 C59' C60' C61'
SADI C65 C66 C65 C66'
DFIX 1.50 0.01 C66 C67 C66 C68 C66' C67' C66' C68'
EADP C71 C72 C73
EADP C66 C67 C68 C66' C67' C68'
EQIV $1 -1-x, 2-y, -1-z
DFIX 2.1 0.01 H68E H55A_$1
FMAP   2
PLAN    5
SIZE     0.130   0.180   0.220
ACTA
BOND   $H
L.S.  20
TEMP   -80.00
WGHT    0.117700    3.763500
FVAR       0.26073   0.63775   0.65664   0.39883
C2    1    0.020347    0.907901    0.086013    11.00000    0.04397    0.04273 =
         0.04727    0.01121    0.01182   -0.00173
AFIX  23
H2A   2   -0.003198    0.912684    0.133726    11.00000   -1.20000
H2B   2    0.085419    0.901899    0.119222    11.00000   -1.20000
AFIX   0
C3    1   -0.022545    0.861836    0.029018    11.00000    0.03888    0.04149 =
         0.05530    0.00626    0.02164   -0.00063
AFIX  23
H3A   2   -0.006586    0.859568   -0.024719    11.00000   -1.20000
H3B   2   -0.088279    0.864851    0.004337    11.00000   -1.20000
AFIX   0
C4    1    0.008060    0.813955    0.087973    11.00000    0.07337    0.04485 =
         0.08692    0.01542    0.03090    0.00247
AFIX  23
H4A   2    0.073316    0.810292    0.108791    11.00000   -1.20000
H4B   2   -0.003168    0.818124    0.144461    11.00000   -1.20000
AFIX   0
C5    1   -0.036856    0.765701    0.038766    11.00000    0.08738    0.05026 =
         0.13375    0.00931    0.06206    0.00263
AFIX  33
H5A   2   -0.013482    0.736846    0.081364    11.00000   -1.50000
H5B   2   -0.101418    0.768408    0.019382    11.00000   -1.50000
H5C   2   -0.024792    0.760561   -0.016354    11.00000   -1.50000
AFIX   0
C10   1   -0.232309    0.964041   -0.015908    11.00000    0.02378    0.03155 =
         0.03311   -0.00306    0.00914   -0.00156
C11   1   -0.235103    1.008756    0.034031    11.00000    0.02372    0.03688 =
         0.02885   -0.00110    0.00987   -0.00110
C12   1   -0.237599    1.051527   -0.021964    11.00000    0.02482    0.03391 =
         0.03303   -0.00065    0.01115   -0.00030
C13   1   -0.238505    1.033998   -0.107229    11.00000    0.02623    0.03611 =
         0.03289    0.00289    0.01205    0.00060
C14   1   -0.233812    0.980034   -0.103598    11.00000    0.02501    0.04178 =
         0.02648   -0.00126    0.01083   -0.00374
C15   1   -0.232219    0.911435    0.017855    11.00000    0.02878    0.03269 =
         0.03948    0.00439    0.01733    0.00287
C16   1   -0.276221    0.872175   -0.043201    11.00000    0.03702    0.03691 =
         0.04579   -0.00380    0.01936   -0.00331
AFIX  43
H16   2   -0.305475    0.879077   -0.108227    11.00000   -1.20000
AFIX   0
C17   1   -0.278587    0.822936   -0.011593    11.00000    0.05218    0.03326 =
         0.07343    0.00095    0.03458   -0.00242
C18   1   -0.326944    0.781490   -0.081897    11.00000    0.07757    0.04102 =
         0.08688   -0.00916    0.03083   -0.01263
AFIX  13
H18   2   -0.391970    0.790002   -0.108327    11.00000   -1.20000
AFIX   0
C19   1   -0.302102    0.780048   -0.161193    11.00000    0.26101    0.09895 =
         0.12271   -0.05405    0.08289   -0.07900
AFIX  33
H19A  2   -0.308523    0.814035   -0.188525    11.00000   -1.50000
H19B  2   -0.239976    0.768847   -0.139356    11.00000   -1.50000
H19C  2   -0.341268    0.756303   -0.208483    11.00000   -1.50000
AFIX   0
C20   1   -0.317219    0.729436   -0.039673    11.00000    0.14150    0.05853 =
         0.15324    0.00057   -0.00004   -0.02053
AFIX  33
H20A  2   -0.333809    0.730546    0.013069    11.00000   -1.50000
H20B  2   -0.356401    0.705642   -0.086845    11.00000   -1.50000
H20C  2   -0.255109    0.718186   -0.017718    11.00000   -1.50000
AFIX   0
C21   1   -0.238926    0.814682    0.083000    11.00000    0.07104    0.03675 =
         0.07854    0.01388    0.03467    0.00176
AFIX  43
H21   2   -0.241372    0.781588    0.105729    11.00000   -1.20000
AFIX   0
C22   1   -0.195426    0.852670    0.146765    11.00000    0.07662    0.04743 =
         0.05618    0.01953    0.02244    0.01448
C23   1   -0.160232    0.842205    0.251286    11.00000    0.16150    0.06899 =
         0.05238    0.02072    0.02794    0.00569
AFIX  13
H23   2   -0.154170    0.804631    0.260914    11.00000   -1.20000
AFIX   0
C24   1   -0.075986    0.864929    0.307434    11.00000    0.14375    0.21175 =
         0.06598    0.01325    0.00832    0.02664
AFIX  33
H24A  2   -0.058672    0.856258    0.373162    11.00000   -1.50000
H24B  2   -0.030749    0.852228    0.287795    11.00000   -1.50000
H24C  2   -0.080751    0.901887    0.299862    11.00000   -1.50000
AFIX   0
C25   1   -0.227776    0.861302    0.286950    11.00000    0.21394    0.21466 =
         0.08173    0.03929    0.09101    0.00292
AFIX  33
H25A  2   -0.286370    0.846273    0.249575    11.00000   -1.50000
H25B  2   -0.208152    0.851498    0.352519    11.00000   -1.50000
H25C  2   -0.232067    0.898366    0.281601    11.00000   -1.50000
AFIX   0
C26   1   -0.190767    0.900664    0.113120    11.00000    0.05041    0.04252 =
         0.04438    0.00419    0.01559    0.00206
AFIX  43
H26   2   -0.158757    0.926687    0.155731    11.00000   -1.20000
AFIX   0
C27   1   -0.251864    1.012205    0.119232    11.00000    0.03966    0.03423 =
         0.03197    0.00182    0.01866    0.00020
C28   1   -0.325772    0.987636    0.121289    11.00000    0.03920    0.04789 =
         0.03583   -0.00218    0.01785   -0.01029
AFIX  43
H28   2   -0.360738    0.966093    0.070842    11.00000   -1.20000
AFIX   0
C29   1   -0.349677    0.993857    0.195404    11.00000    0.05052    0.05445 =
         0.04665   -0.00155    0.02901   -0.00931
C30   1   -0.433401    0.968444    0.192605    11.00000    0.06664    0.08288 =
         0.06297   -0.01728    0.04136   -0.02610
AFIX  13
H30   2   -0.441682    0.936296    0.156192    11.00000   -1.20000
AFIX   0
C31   1   -0.514163    1.000738    0.140980    11.00000    0.05331    0.12925 =
         0.10766   -0.00086    0.04321   -0.01480
AFIX  33
H31A  2   -0.516758    1.009745    0.079638    11.00000   -1.50000
H31B  2   -0.568063    0.981818    0.132824    11.00000   -1.50000
H31C  2   -0.510416    1.031744    0.176761    11.00000   -1.50000
AFIX   0
C32   1   -0.427698    0.954049    0.286975    11.00000    0.11234    0.16833 =
         0.10228    0.02244    0.07118   -0.05074
AFIX  33
H32A  2   -0.374635    0.933004    0.319596    11.00000   -1.50000
H32B  2   -0.423544    0.984835    0.323443    11.00000   -1.50000
H32C  2   -0.481191    0.934910    0.279506    11.00000   -1.50000
AFIX   0
C33   1   -0.297837    1.026398    0.267331    11.00000    0.06289    0.06817 =
         0.03808   -0.00428    0.03465   -0.00518
AFIX  43
H33   2   -0.314063    1.032108    0.317601    11.00000   -1.20000
AFIX   0
C34   1   -0.223756    1.050528    0.267676    11.00000    0.04919    0.06174 =
         0.03836   -0.00934    0.02502   -0.01149
C35   1   -0.166462    1.084498    0.348783    11.00000    0.07661    0.10037 =
         0.04937   -0.02975    0.04030   -0.03508
AFIX  13
H35   2   -0.197985    1.088500    0.390372    11.00000   -1.20000
AFIX   0
C36   1   -0.077251    1.060278    0.405519    11.00000    0.07458    0.15809 =
         0.05082   -0.01981    0.00812   -0.04130
AFIX  33
H36A  2   -0.041595    1.082796    0.457238    11.00000   -1.50000
H36B  2   -0.086268    1.027772    0.430517    11.00000   -1.50000
H36C  2   -0.045844    1.054506    0.365719    11.00000   -1.50000
AFIX   0
C37   1   -0.155667    1.137737    0.314555    11.00000    0.14209    0.08599 =
         0.09536   -0.04966    0.05675   -0.03949
AFIX  33
H37A  2   -0.214725    1.152439    0.277970    11.00000   -1.50000
H37B  2   -0.122568    1.159520    0.368454    11.00000   -1.50000
H37C  2   -0.122837    1.135133    0.275459    11.00000   -1.50000
AFIX   0
C38   1   -0.200586    1.043146    0.194185    11.00000    0.03718    0.05008 =
         0.03995   -0.00516    0.02093   -0.01112
AFIX  43
H38   2   -0.148985    1.059379    0.194726    11.00000   -1.20000
AFIX   0
C39   1   -0.252999    1.104165    0.003144    11.00000    0.03924    0.02959 =
         0.03850   -0.00102    0.01885   -0.00210
C40   1   -0.334525    1.115022    0.004682    11.00000    0.03898    0.03927 =
         0.06689   -0.00337    0.02825   -0.00347
AFIX  43
H40   2   -0.377993    1.088894   -0.009993    11.00000   -1.20000
AFIX   0
C41   1   -0.354551    1.163166    0.027139    11.00000    0.05270    0.04357 =
         0.08403   -0.00448    0.04055    0.00616
PART    2
C42   1   -0.442854    1.174701    0.029198    21.00000    0.05393    0.07335 =
         0.15946   -0.02595    0.05090   -0.00159
AFIX  13
H42   2   -0.439646    1.206361    0.065442    21.00000   -1.20000
AFIX   0
C43   1   -0.515203    1.178375   -0.069070    21.00000    0.05393    0.07335 =
         0.15946   -0.02595    0.05090   -0.00159
AFIX  33
H43A  2   -0.500490    1.205534   -0.102673    21.00000   -1.50000
H43B  2   -0.519657    1.146048   -0.101470    21.00000   -1.50000
H43C  2   -0.572387    1.185925   -0.066805    21.00000   -1.50000
AFIX   0
C44   1   -0.482795    1.132124    0.060600    21.00000    0.05393    0.07335 =
         0.15946   -0.02595    0.05090   -0.00159
AFIX  33
H44A  2   -0.539897    1.143011    0.059747    21.00000   -1.50000
H44B  2   -0.492710    1.103113    0.018521    21.00000   -1.50000
H44C  2   -0.442087    1.122201    0.124218    21.00000   -1.50000
AFIX   0
PART    1
C42'  1   -0.445596    1.173250    0.028321   -21.00000    0.05393    0.07335 =
         0.15946   -0.02595    0.05090   -0.00159
AFIX  13
H42'  2   -0.422967    1.203928    0.068799   -21.00000   -1.20000
AFIX   0
C43'  1   -0.501810    1.205118   -0.056738   -21.00000    0.05393    0.07335 =
         0.15946   -0.02595    0.05090   -0.00159
AFIX  33
H43D  2   -0.464047    1.217890   -0.086137   -21.00000   -1.50000
H43E  2   -0.549757    1.184165   -0.101546   -21.00000   -1.50000
H43F  2   -0.527795    1.233802   -0.037258   -21.00000   -1.50000
AFIX   0
C44'  1   -0.445839    1.141607    0.108418   -21.00000    0.05393    0.07335 =
         0.15946   -0.02595    0.05090   -0.00159
AFIX  33
H44D  2   -0.385519    1.128720    0.145740   -21.00000   -1.50000
H44E  2   -0.465096    1.162638    0.147798   -21.00000   -1.50000
H44F  2   -0.487058    1.113001    0.083510   -21.00000   -1.50000
AFIX   0
PART    0
C45   1   -0.290152    1.200545    0.048309    11.00000    0.06430    0.03702 =
         0.08966   -0.00814    0.04590   -0.00019
AFIX  43
H45   2   -0.303565    1.233713    0.062320    11.00000   -1.20000
AFIX   0
C46   1   -0.206400    1.191479    0.049896    11.00000    0.05803    0.03483 =
         0.06443   -0.00729    0.03282   -0.00505
C47   1   -0.135425    1.232559    0.079038    11.00000    0.06977    0.04294 =
         0.08613   -0.01507    0.04221   -0.01591
AFIX  13
H47   2   -0.079168    1.217117    0.081424    11.00000   -1.20000
AFIX   0
C48   1   -0.115732    1.253965    0.175069    11.00000    0.09737    0.07306 =
         0.09152   -0.02709    0.04055   -0.02484
AFIX  33
H48A  2   -0.069686    1.280258    0.190827    11.00000   -1.50000
H48B  2   -0.170288    1.268765    0.174837    11.00000   -1.50000
H48C  2   -0.094513    1.226687    0.221517    11.00000   -1.50000
AFIX   0
C49   1   -0.162864    1.275224    0.007025    11.00000    0.11801    0.06388 =
         0.09990    0.00127    0.04730   -0.03750
AFIX  33
H49A  2   -0.116385    1.301406    0.026855    11.00000   -1.50000
H49B  2   -0.170603    1.261559   -0.053669    11.00000   -1.50000
H49C  2   -0.219233    1.290116    0.001623    11.00000   -1.50000
AFIX   0
C50   1   -0.189282    1.142502    0.026862    11.00000    0.04081    0.04031 =
         0.04982   -0.00190    0.02685   -0.00191
AFIX  43
H50   2   -0.132664    1.135282    0.027457    11.00000   -1.20000
AFIX   0
C51   1   -0.252007    1.064849   -0.191594    11.00000    0.03183    0.04682 =
         0.02785    0.00389    0.01006   -0.00829
C52   1   -0.302801    1.108965   -0.210814    11.00000    0.04214    0.04547 =
         0.03940    0.00988    0.01144   -0.00066
AFIX  43
H52   2   -0.328542    1.119305   -0.169899    11.00000   -1.20000
AFIX   0
C53   1   -0.316570    1.138355   -0.289499    11.00000    0.05665    0.05696 =
         0.04927    0.01688    0.00074   -0.01034
C54   1   -0.368611    1.188132   -0.305917    11.00000    0.09385    0.06837 =
         0.06650    0.03470    0.01453    0.00717
AFIX  13
H54   2   -0.377323    1.201363   -0.368565    11.00000   -1.20000
AFIX   0
C55   1   -0.458240    1.181702   -0.306679    11.00000    0.08335    0.10252 =
         0.23585    0.06675    0.03956    0.04330
AFIX  33
H55A  2   -0.491887    1.156091   -0.353245    11.00000   -1.50000
H55B  2   -0.451657    1.170669   -0.244808    11.00000   -1.50000
H55C  2   -0.490351    1.214100   -0.322487    11.00000   -1.50000
AFIX   0
C56   1   -0.316856    1.227757   -0.233831    11.00000    0.12048    0.06653 =
         0.10175    0.00803    0.03258    0.01093
AFIX  33
H56A  2   -0.257630    1.232091   -0.233159    11.00000   -1.50000
H56B  2   -0.349080    1.260119   -0.249696    11.00000   -1.50000
H56C  2   -0.310387    1.216688   -0.172018    11.00000   -1.50000
AFIX   0
C57   1   -0.280351    1.121825   -0.349210    11.00000    0.07904    0.07357 =
         0.03114    0.01603    0.01233   -0.02120
AFIX  43
H57   2   -0.289676    1.141480   -0.403001    11.00000   -1.20000
AFIX   0
C58   1   -0.231227    1.077833   -0.333306    11.00000    0.05984    0.06813 =
         0.03341    0.00171    0.01556   -0.02294
PART    2
C59   1   -0.191405    1.058363   -0.399931    31.00000    0.09593    0.10843 =
         0.05062   -0.00118    0.03889   -0.01534
AFIX  13
H59   2   -0.189267    1.086038   -0.442315    31.00000   -1.20000
AFIX   0
C60   1   -0.102514    1.031175   -0.354956    31.00000    0.09593    0.10843 =
         0.05062   -0.00118    0.03889   -0.01534
AFIX  33
H60A  2   -0.056732    1.054891   -0.314783    31.00000   -1.50000
H60B  2   -0.107499    1.002765   -0.317338    31.00000   -1.50000
H60C  2   -0.085797    1.018279   -0.403646    31.00000   -1.50000
AFIX   0
C61   1   -0.246365    1.013958   -0.455343    31.00000    0.09593    0.10843 =
         0.05062   -0.00118    0.03889   -0.01534
AFIX  33
H61A  2   -0.308451    1.024730   -0.490461    31.00000   -1.50000
H61B  2   -0.222272    1.001947   -0.498885    31.00000   -1.50000
H61C  2   -0.243973    0.986433   -0.412577    31.00000   -1.50000
AFIX   0
PART    1
C59'  1   -0.200377    1.060657   -0.406250   -31.00000    0.09593    0.10843 =
         0.05062   -0.00118    0.03889   -0.01534
AFIX  13
H59'  2   -0.215932    1.092931   -0.443009   -31.00000   -1.20000
AFIX   0
C60'  1   -0.101664    1.068295   -0.365902   -31.00000    0.09593    0.10843 =
         0.05062   -0.00118    0.03889   -0.01534
AFIX  33
H60D  2   -0.084388    1.094144   -0.316760   -31.00000   -1.50000
H60E  2   -0.071510    1.036256   -0.339326   -31.00000   -1.50000
H60F  2   -0.084293    1.079499   -0.415134   -31.00000   -1.50000
AFIX   0
C61'  1   -0.269443    1.028586   -0.480364   -31.00000    0.09593    0.10843 =
         0.05062   -0.00118    0.03889   -0.01534
AFIX  33
H61D  2   -0.328601    1.036394   -0.483280   -31.00000   -1.50000
H61E  2   -0.268767    1.035850   -0.540966   -31.00000   -1.50000
H61F  2   -0.255984    0.992606   -0.465158   -31.00000   -1.50000
AFIX   0
PART    0
C62   1   -0.216567    1.050457   -0.253036    11.00000    0.04243    0.05450 =
         0.03648    0.00224    0.01251   -0.01087
AFIX  43
H62   2   -0.180813    1.020710   -0.239906    11.00000   -1.20000
AFIX   0
C63   1   -0.247734    0.946303   -0.185093    11.00000    0.03626    0.04038 =
         0.02838   -0.00448    0.01462   -0.00609
C64   1   -0.334225    0.941599   -0.253878    11.00000    0.03626    0.06763 =
         0.03898   -0.00801    0.01388   -0.00372
AFIX  43
H64   2   -0.381014    0.959845   -0.247549    11.00000   -1.20000
AFIX   0
C65   1   -0.354032    0.911070   -0.331309    11.00000    0.05135    0.09055 =
         0.03985   -0.01767    0.01564   -0.01702
PART    2
C66   1   -0.446664    0.903508   -0.402490    41.00000    0.07302    0.17939 =
         0.07012   -0.03486    0.00916   -0.04049
AFIX  13
H66   2   -0.471035    0.913789   -0.356770    41.00000   -1.20000
AFIX   0
C67   1   -0.483933    0.852530   -0.409247    41.00000    0.07302    0.17939 =
         0.07012   -0.03486    0.00916   -0.04049
AFIX  33
H67A  2   -0.440930    0.830884   -0.360580    41.00000   -1.50000
H67B  2   -0.539423    0.854366   -0.400898    41.00000   -1.50000
H67C  2   -0.496424    0.838176   -0.470792    41.00000   -1.50000
AFIX   0
C68   1   -0.483025    0.949225   -0.457564    41.00000    0.07302    0.17939 =
         0.07012   -0.03486    0.00916   -0.04049
AFIX  33
H68A  2   -0.439606    0.976903   -0.433585    41.00000   -1.50000
H68B  2   -0.495450    0.942651   -0.523004    41.00000   -1.50000
H68C  2   -0.538449    0.958840   -0.453110    41.00000   -1.50000
AFIX   0
PART    1
C66'  1   -0.450146    0.904931   -0.405798   -41.00000    0.07302    0.17939 =
         0.07012   -0.03486    0.00916   -0.04049
AFIX  13
H66'  2   -0.468848    0.938114   -0.388880   -41.00000   -1.20000
AFIX   0
C67'  1   -0.502322    0.875686   -0.365470   -41.00000    0.07302    0.17939 =
         0.07012   -0.03486    0.00916   -0.04049
AFIX  33
H67D  2   -0.466888    0.871553   -0.298134   -41.00000   -1.50000
H67E  2   -0.557549    0.893978   -0.376474   -41.00000   -1.50000
H67F  2   -0.516990    0.842211   -0.395166   -41.00000   -1.50000
AFIX   0
C68'  1   -0.462674    0.924000   -0.499116   -41.00000    0.07302    0.17939 =
         0.07012   -0.03486    0.00916   -0.04049
AFIX  33
H68D  2   -0.408891    0.942205   -0.493545   -41.00000   -1.50000
H68E  2   -0.473418    0.895303   -0.542022   -41.00000   -1.50000
H68F  2   -0.513977    0.947069   -0.523330   -41.00000   -1.50000
AFIX   0
PART    0
C69   1   -0.282918    0.885699   -0.339121    11.00000    0.07969    0.07878 =
         0.04894   -0.03355    0.02985   -0.02218
AFIX  43
H69   2   -0.294959    0.864528   -0.391793    11.00000   -1.20000
AFIX   0
C70   1   -0.196530    0.890345   -0.273412    11.00000    0.05427    0.06178 =
         0.05889   -0.02478    0.02650   -0.00543
C71   1   -0.118855    0.862775   -0.283699    11.00000    0.11245    0.10680 =
         0.12875   -0.04167    0.07671   -0.00344
AFIX  13
H71   2   -0.062285    0.877652   -0.236091    11.00000   -1.20000
AFIX   0
C72   1   -0.118325    0.807730   -0.261171    11.00000    0.11245    0.10680 =
         0.12875   -0.04167    0.07671   -0.00344
AFIX  33
H72A  2   -0.118155    0.803950   -0.199319    11.00000   -1.50000
H72B  2   -0.171660    0.791393   -0.308096    11.00000   -1.50000
H72C  2   -0.064813    0.791694   -0.261301    11.00000   -1.50000
AFIX   0
C73   1   -0.119152    0.872370   -0.380065    11.00000    0.11245    0.10680 =
         0.12875   -0.04167    0.07671   -0.00344
AFIX  33
H73A  2   -0.119495    0.909004   -0.391022    11.00000   -1.50000
H73B  2   -0.065651    0.857258   -0.381859    11.00000   -1.50000
H73C  2   -0.172498    0.856956   -0.428654    11.00000   -1.50000
AFIX   0
C74   1   -0.179421    0.920570   -0.195427    11.00000    0.03916    0.04752 =
         0.03628   -0.01032    0.01391   -0.00579
AFIX  43
H74   2   -0.120064    0.923569   -0.148691    11.00000   -1.20000
AFIX   0
O1    3    0.005643    0.954039    0.031685    11.00000    0.03647    0.03630 =
         0.03743    0.00490    0.01533   -0.00177
SC1   4   -0.087488    1.009190    0.017353    11.00000    0.02743    0.03634 =
         0.03090   -0.00223    0.01243   -0.00126
H1    2   -0.027238    1.024755    0.173682    11.00000    0.05519
HKLF    4




REM  001 in P2(1)/c
REM wR2 = 0.2406, GooF = S = 1.023, Restrained GooF = 1.028 for all data
REM R1 = 0.0827 for 6544 Fo > 4sig(Fo) and 0.1375 for all 10920 data
REM 626 parameters refined using 16 restraints

END

WGHT      0.1174      3.8288

REM Highest difference peak  0.679,  deepest hole -0.389,  1-sigma level  0.065
Q1    1  -0.2893  1.1472 -0.4549  11.00000  0.05    0.68
Q2    1  -0.3910  0.7989 -0.1808  11.00000  0.05    0.57
Q3    1  -0.0809  0.9737  0.0375  11.00000  0.05    0.54
Q4    1  -0.0704  0.8418 -0.2258  11.00000  0.05    0.45
Q5    1   0.0000  1.0000  0.0000  10.50000  0.05    0.41
;
_shelx_res_checksum              67601
_shelx_hkl_file
;
   0   0   1   -0.32    0.23
   0   0   2  619.26   13.84
   0   0   3    0.55    1.35
   0   0   4 2543.87   52.23
   0   0   5   -0.86    0.34
   0   0  -5    0.01    1.19
   0   0   5   -0.88    1.37
   0   0  -6  754.90   17.04
   0   0   6  734.02   19.73
   0   0   7    0.33    1.75
   0   0   7   -0.26    0.63
   0   0  -7    0.59    1.42
   0   0   8  135.18    7.72
   0   0  -8  140.12    5.56
   0   0  -9   -0.04    1.83
   0   0   9   -1.42    2.04
   0   0  10  183.37    9.98
   0   0  11    0.49    2.21
   0   0  12    2.65    3.08
   0   0  13    1.04    2.66
   0   0  14   63.49    8.06
   0   0  15    0.87    2.59
   0   0  16    7.73    4.70
   0   0  17    7.63    3.90
   0  -1   1 5692.87  116.00
   0  -1   2   20.98    1.58
   0   1   2   30.26    1.85
   0  -1   2   25.14    1.70
   0  -1   3 3494.60   84.63
   0   1   3 4325.39   79.98
   0  -1   3 4368.69   80.13
   0   1  -4    9.74    1.25
   0   1   4   10.39    2.08
   0  -1   4    6.65    1.54
   0  -1   4    9.77    2.18
   0   1  -5  527.10   11.77
   0  -1   5  529.42   14.59
   0   1   5  492.17   14.20
   0  -1  -6  609.05   14.65
   0   1  -6  594.62   13.62
   0  -1   6  584.57   16.86
   0   1   6  600.26   16.78
   0  -1   7  412.14   13.66
   0   1   7  386.57   13.33
   0  -1  -7  396.17   11.04
   0   1  -7  395.54    9.99
   0   1  -8  115.00    4.68
   0   1   8  124.40    7.39
   0  -1   8  134.90    7.72
   0  -1  -8  120.57    5.37
   0  -1  -9  111.80    5.50
   0  -1   9  104.90    7.08
   0   1   9  114.90    7.53
   0   1  -9  103.84    4.71
   0  -1  10    5.08    2.69
   0  -1  10   -0.22    0.81
   0   1  10    2.04    2.60
   0  -1  11   80.61    7.04
   0   1  11   80.19    6.90
   0   1  12    8.45    3.69
   0  -1  12    6.49    3.29
   0   1  13  161.72   10.76
   0  -1  13  161.58   10.65
   0  -1  14   12.65    4.28
   0   1  14    7.08    3.23
   0   1  15    9.00    3.81
   0  -1  15   19.39    5.15
   0  -1  16    1.66    2.89
   0   1  16    3.58    3.37
   0  -1  17   -0.02    2.40
   0   1  17   -3.80    2.25
   0  -2   0 4118.52   86.84
   0   2   1    7.76    0.69
   0  -2   1   11.35    1.22
   0  -2  -1   12.45    0.93
   0  -2   1    9.53    0.80
   0  -2   2   65.05    2.84
   0  -2   2   66.80    3.13
   0  -2   3  149.53    5.44
   0   2   3  140.62    5.27
   0  -2   3  143.97    5.46
   0   2   4    6.93    1.89
   0  -2   4    4.79    1.77
   0  -2   4    4.99    1.82
   0   2  -5   68.96    2.48
   0  -2   5   64.71    4.52
   0   2   5   67.04    4.38
   0  -2   5   68.02    4.46
   0  -2   6  470.38   14.37
   0   2   6  486.70   14.29
   0  -2   6  472.45   14.44
   0   2  -6  475.27   10.77
   0   2  -7   19.23    1.76
   0  -2  -7   20.30    2.70
   0   2   7   20.83    3.52
   0  -2   7   21.83    3.62
   0  -2   7   20.27    3.19
   0   2   8  345.17   13.05
   0   2  -8  357.94    8.89
   0  -2   8  334.84   12.87
   0  -2  -8  337.35   10.64
   0  -2   8  354.47   12.91
   0  -2  -9   16.55    2.99
   0  -2   9   15.65    3.35
   0   2   9   14.95    3.66
   0  -2   9    8.96    3.14
   0   2  10  109.06    7.73
   0  -2 -10  126.45    6.39
   0  -2  10  127.28    8.21
   0  -2  11   11.32    3.71
   0  -2  11    0.47    0.74
   0   2  11    3.87    2.57
   0  -2  12    0.44    2.49
   0   2  12    1.57    3.07
   0  -2  13    6.09    3.21
   0   2  13    4.17    2.88
   0  -2  14   28.71    5.86
   0   2  14   39.55    6.54
   0   2  15    0.43    2.58
   0  -2  15    6.90    3.41
   0   2  16    2.27    3.60
   0  -2  16    5.87    3.46
   0   2  17    0.08    2.59
   0  -2  17    6.26    3.62
   0  -3   0   -1.02    0.58
   0  -3   1    2.26    0.58
   0   3   1    1.05    0.52
   0  -3  -1    1.43    0.76
   0  -3   1    0.64    0.91
   0  -3   2 2092.94   45.36
   0  -3   2 2099.91   41.92
   0  -3   3 3250.37   69.43
   0  -3   3 3258.47   64.80
   0  -3   4   60.93    4.03
   0   3   4   55.30    3.56
   0  -3   4   52.09    3.81
   0  -3   5  777.23   20.73
   0  -3   5  793.13   20.00
   0   3   5  796.82   19.63
   0  -3   6    3.36    1.97
   0  -3   6    5.11    2.14
   0   3   6    2.85    1.86
   0  -3  -7   78.13    4.86
   0  -3   7   92.06    5.98
   0   3   7   78.75    5.43
   0  -3   7   89.02    5.77
   0  -3  -8    5.41    2.35
   0   3  -8    2.96    0.99
   0  -3   8    3.31    2.27
   0   3   8    1.19    2.12
   0  -3   8    4.50    2.18
   0   3   9  131.36    7.97
   0  -3   9  137.99    8.11
   0  -3  -9  126.29    6.54
   0  -3   9  126.65    7.72
   0  -3 -10    1.37    2.48
   0  -3  10    0.27    1.80
   0  -3  10   -0.72    2.42
   0   3  10   -0.83    2.53
   0  -3  11   43.81    6.34
   0  -3  11   50.04    5.74
   0   3  11   53.66    6.20
   0   3  12    5.06    3.22
   0  -3  12    2.13    1.52
   0  -3  12    0.84    3.37
   0  -3  13   57.34    7.64
   0   3  13   55.70    7.29
   0  -3  14   12.83    5.22
   0   3  14   16.10    4.57
   0   3  15    6.86    3.76
   0  -3  15    1.64    3.69
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   0   4   2  989.61   20.75
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   0  -4   3  406.85   11.91
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   0  -6   4  268.93    8.92
   0   6   4  272.31    8.57
   0  -6   4  282.05    6.52
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   0 -11  16   16.39    4.58
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   0  12  -2  209.19    6.35
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   0 -20  -5   33.77    8.34
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  -1   0   7    1.59    1.60
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  -1   0   6   30.17    2.98
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  -1   0   4  189.41    6.86
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   1   0  -2  470.01   10.46
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   1   0   2 4072.30   79.58
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   1   0   3    0.78    1.19
   1   0   4 1108.74   26.46
   1   0   4 1110.01   25.44
   1   0   5   -1.65    1.29
   1   0   5    2.27    1.80
   1   0   6   16.98    3.12
   1   0   7    2.77    2.04
   1   0   8  632.72   19.62
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   1   0  13    4.18    2.99
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   1   0  16    4.48    3.00
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  -1  -1  17   36.61    6.88
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  -1   1  16   -1.25    2.21
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  -1   1  11   10.72    3.56
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  -1   1  10    6.18    3.12
  -1  -1  10    6.29    2.83
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   1   1  -9   13.23    2.20
  -1   1   9   13.84    3.61
   1  -1  -9   15.10    2.70
  -1  -1   9   16.23    3.56
  -1  -1   9   11.62    2.80
   1   1  -8   24.51    2.43
  -1  -1   8   25.24    3.99
   1  -1  -8   26.68    2.88
  -1   1   8   24.64    3.88
  -1  -1   8   23.68    3.42
   1  -1  -7   17.39    2.39
  -1  -1   7   20.41    3.52
  -1   1   7   20.75    3.53
  -1  -1   7   20.07    2.93
  -1   1   7   20.80    2.77
   1   1  -7   22.59    2.13
  -1  -1   6   15.47    2.50
   1  -1  -6   14.66    2.08
  -1  -1   6   11.99    2.66
   1   1  -6   20.63    1.85
  -1   1   6   15.63    2.25
  -1   1   6   11.75    2.70
   1  -1  -5   92.80    4.02
  -1   1   5   98.22    4.30
  -1   1   5   91.64    5.11
  -1  -1   5   86.67    4.57
  -1  -1   5   85.89    5.02
   1   1  -5   94.20    3.46
  -1   1   4    3.58    1.33
  -1   1   4    2.19    1.82
  -1  -1   4    6.43    2.01
   1   1  -4    5.14    1.12
   1  -1  -4    6.25    1.56
  -1  -1   4    3.98    1.48
   1  -1  -3 1229.50   25.63
  -1   1   3 1228.92   26.56
  -1  -1   3 1211.66   26.02
  -1   1   3 1219.17   26.08
   1   1  -3 1231.90   25.24
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   1   1  -2   16.31    0.93
  -1  -1   2   18.42    1.50
   1  -1  -2   16.30    1.20
  -1   1   1 1712.87   35.05
  -1  -1   1 1804.33   35.19
   1  -1  -1 1734.23   35.58
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   1  -1   0   22.33    1.12
   1  -1   1   23.19    1.50
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  -1   1  -1   25.36    1.52
   1   1   2  835.87   18.29
   1  -1   2  836.75   18.41
   1  -1   2  846.56   19.62
   1  -1   3 1484.72   31.99
   1  -1   3 1496.22   33.95
   1   1   3 1542.45   32.06
   1   1   4  469.36   12.82
   1  -1   4  460.34   13.32
   1  -1   4  459.49   12.89
   1  -1   5  440.78   13.35
   1   1   5  436.36   12.94
   1  -1   5  435.34   13.42
   1  -1   6  164.91    7.59
   1   1   6  158.20    7.41
   1  -1   6  166.27    7.76
   1  -1   7   99.52    6.13
   1   1   7   91.60    6.15
   1  -1   7  100.12    6.44
   1   1   8    1.05    2.03
   1  -1   8   -1.85    1.74
  -1   1  -8    3.39    1.63
   1  -1   8    4.05    2.21
  -1  -1  -9  123.84    5.98
   1   1   9  124.13    7.92
   1  -1   9  122.72    7.86
   1   1  10   16.38    4.04
   1  -1  10   14.77    3.73
   1   1  11   80.68    7.20
   1  -1  11   75.24    7.64
   1  -1  12    1.04    2.57
   1   1  12   -3.92    2.13
   1   1  13    1.43    2.73
   1  -1  13    0.99    2.80
   1  -1  14    1.72    3.10
   1   1  14    8.02    4.03
   1  -1  15    7.83    3.64
   1   1  15    5.34    3.46
   1   1  16   -1.09    2.15
   1  -1  16    0.58    2.08
   1   1  17   -3.06    2.09
   1  -1  17   -1.12    2.63
  -1   2  18    4.94    2.91
  -1  -2  18    9.33    3.25
  -1   2  17    5.77    3.18
  -1  -2  17   -0.19    2.23
  -1   2  16   14.05    4.47
  -1  -2  16   19.79    4.71
  -1  -2  15    3.92    3.71
  -1   2  15    8.15    3.59
  -1   2  14    6.50    2.94
  -1  -2  14    3.06    2.60
  -1   2  13   24.22    5.33
  -1  -2  13   25.62    5.30
  -1  -2  12    1.36    1.70
  -1   2  12    2.54    2.93
  -1  -2  12    5.13    3.68
  -1   2  11    3.91    2.80
  -1  -2  11    2.55    2.90
  -1  -2  11    1.91    2.06
   1  -2 -10    6.88    2.67
  -1  -2  10    5.81    3.18
  -1   2  10    4.06    2.68
  -1  -2  10    5.68    2.50
   1   2  -9   -1.32    1.19
   1  -2  -9    2.58    2.11
  -1  -2   9    2.22    2.39
  -1   2   9    0.94    2.30
  -1  -2   9    2.11    1.55
   1  -2  -8   23.96    3.06
  -1  -2   8   19.29    3.77
   1   2  -8   26.60    2.18
  -1   2   8   26.12    4.03
  -1  -2   7   26.19    3.78
  -1   2   7   22.66    3.65
   1   2  -7   26.58    2.07
   1  -2  -7   24.80    2.82
   1   2  -6  160.90    4.62
   1  -2  -6  156.80    5.98
  -1   2   6  147.18    6.99
  -1  -2   6  155.12    7.09
  -1  -2   5  109.30    5.65
   1   2  -5  120.89    3.57
  -1   2   5  109.62    5.84
   1  -2  -5  116.69    4.96
  -1   2   4   52.19    3.83
   1   2  -4   48.45    1.93
  -1  -2   4   50.86    3.82
   1  -2  -4   49.27    3.05
   1  -2  -3  203.14    6.10
  -1   2   3  209.39    6.64
  -1  -2   3  217.63    6.63
  -1  -2   2  819.55   17.52
   1  -2  -2  823.35   17.80
   1  -2  -1   -1.40    0.51
  -1  -2   1   -0.14    0.52
  -1  -2   1   -2.53    0.60
  -1  -2   0   85.17    3.07
   1  -2   0   80.88    2.75
   1  -2   1   24.28    1.19
   1  -2   1   23.02    1.69
  -1   2  -1   25.97    1.56
  -1   2  -1   24.38    1.56
   1  -2   2 1181.89   25.15
   1  -2   2 1189.80   26.98
   1   2   3 2904.98   57.98
   1  -2   3 2896.38   62.15
   1  -2   3 2860.53   58.21
   1  -2   4   53.53    3.73
   1  -2   4   47.94    3.53
   1   2   4   48.96    3.68
   1   2   5  299.44   10.19
   1  -2   5  327.18   11.04
   1  -2   5  328.27   10.84
   1  -2   6   23.11    3.36
   1  -2   6   20.29    3.36
   1   2   6   22.20    3.31
   1   2   7   44.02    4.64
   1  -2   7   42.61    4.64
   1  -2   7   45.52    4.41
  -1   2  -8  201.83    6.14
   1  -2   8  192.23    9.33
   1   2   8  191.42    9.36
   1  -2   8  198.50    9.73
   1  -2   9   78.65    6.30
  -1  -2  -9   68.26    5.02
   1   2   9   75.41    6.29
   1  -2   9   77.09    6.13
   1  -2  10   50.91    6.11
   1  -2  10   44.42    5.35
   1   2  10   52.88    6.05
   1  -2  11    5.64    3.09
   1   2  11    4.01    2.76
   1   2  12    9.19    3.62
   1  -2  12    7.79    3.56
   1   2  13   17.43    4.75
   1  -2  13   11.82    3.95
   1  -2  14   -2.35    2.36
   1   2  14    2.19    3.08
   1   2  15    1.12    2.92
   1  -2  15    5.30    2.82
   1  -2  16    6.34    4.25
   1   2  16    1.14    2.56
   1   2  17   -1.11    2.08
   1  -2  17    0.42    2.27
  -1   3  18    8.13    3.13
  -1  -3  18   -0.12    2.41
  -1   3  17    8.57    3.52
  -1  -3  17   -4.14    2.71
  -1   3  16    1.99    2.94
  -1  -3  16   -3.97    2.67
  -1   3  15   13.84    4.64
  -1  -3  15   12.37    5.10
  -1   3  14   -0.98    2.15
  -1  -3  14   -3.04    2.75
  -1  -3  13   14.48    4.97
  -1  -3  13    5.96    2.37
  -1   3  13   13.84    4.39
  -1  -3  12   11.91    4.28
  -1   3  12   13.12    4.06
  -1  -3  12   10.55    3.10
  -1   3  11   23.09    4.59
  -1  -3  11   23.34    5.06
  -1  -3  10    0.93    0.90
  -1   3  10    0.92    2.21
   1  -3 -10    3.87    2.71
  -1  -3  10    1.68    2.71
  -1  -3   9   57.61    5.82
  -1   3   9   50.28    5.46
   1  -3  -9   47.65    4.35
   1  -3  -8   33.98    3.59
   1   3  -8   29.77    1.81
  -1   3   8   32.82    4.21
  -1  -3   8   22.35    3.89
   1  -3  -7    0.61    1.92
  -1  -3   7    1.03    0.62
  -1   3   7   -0.27    1.77
  -1  -3   7   -0.17    1.94
   1   3  -7    0.31    0.60
   1   3  -6   11.07    1.01
  -1  -3   6    9.39    2.07
  -1  -3   6   11.21    2.64
  -1   3   6    8.76    2.54
   1  -3  -6    9.05    2.21
   1  -3  -5 1392.45   29.62
  -1   3   5 1379.47   30.19
  -1  -3   5 1395.12   30.26
  -1  -3   5 1205.82   31.33
  -1  -3   4  142.54    6.07
   1  -3  -4  150.64    5.62
  -1   3   4  158.77    6.20
  -1  -3   4  145.75    5.93
  -1  -3   3 4149.62   87.08
  -1  -3   3 4160.50   81.10
   1  -3  -3 4087.53   82.47
   1  -3  -2  130.84    3.86
   1  -3  -2  132.98    4.52
  -1  -3   2  133.30    4.20
  -1  -3   2  133.90    5.34
   1  -3  -1    9.87    1.18
   1  -3  -1   10.13    1.15
  -1  -3   1   10.48    1.59
  -1  -3   1    9.07    0.81
  -1   3   1    6.83    0.87
  -1  -3   0  103.54    3.98
   1  -3   0  110.59    3.73
   1   3   1 1121.31   23.10
   1  -3   1 1146.60   25.62
   1  -3   1 1147.14   23.58
   1  -3   2  127.51    3.41
   1  -3   2  121.59    5.02
   1  -3   2  125.03    4.59
   1  -3   3  194.02    6.84
   1  -3   3  200.39    7.40
   1  -3   4   64.47    4.23
   1  -3   4   59.46    4.19
   1   3   4   65.97    4.09
   1  -3   5  192.16    7.96
   1   3   5  176.90    7.40
   1  -3   5  184.19    7.67
   1  -3   6    2.95    1.99
   1   3   6    5.05    2.04
   1  -3   6    3.69    2.14
   1  -3   7   70.34    5.49
   1  -3   7   68.76    5.37
  -1   3  -7   64.50    2.68
   1   3   7   66.97    5.18
   1  -3   8   13.61    3.44
   1   3   8   16.04    3.50
   1  -3   8   12.81    3.55
   1   3   9   24.19    4.19
   1  -3   9   29.12    4.95
   1  -3   9   24.89    4.38
   1   3  10    8.76    3.02
   1  -3  10   16.84    3.93
  -1  -3 -10   14.15    3.21
   1  -3  10   15.06    4.01
   1  -3  11   24.61    4.69
   1   3  11   23.95    4.78
   1  -3  11   28.25    5.52
   1   3  12    0.61    2.48
   1  -3  12    3.39    3.30
   1  -3  13    9.86    3.81
   1   3  13    2.46    3.12
   1   3  14    6.77    3.58
   1  -3  14   11.64    4.51
   1  -3  15    2.00    2.64
   1   3  15   10.14    4.20
   1   3  16    5.45    3.18
   1  -3  16    7.79    3.80
   1   3  17    4.47    2.66
   1  -3  17    6.48    3.02
  -1   4  18    3.19    2.60
  -1  -4  18    0.56    3.81
  -1   4  17    7.02    2.90
  -1  -4  17    5.02    4.82
  -1   4  16   22.04    5.51
  -1  -4  16   27.03    6.53
  -1  -4  15   20.29    5.74
  -1   4  15   30.19    6.21
  -1  -4  14   38.22    6.94
  -1   4  14   47.49    6.87
  -1  -4  13   -3.84    2.55
  -1   4  13   -4.09    2.10
  -1  -4  13   -0.34    0.98
  -1  -4  12   -1.69    2.79
  -1   4  12    4.21    3.07
  -1  -4  12    1.78    1.38
  -1   4  11   83.72    6.96
  -1  -4  11   83.48    7.44
   1  -4 -11   85.23    6.13
  -1   4  10   -0.39    2.16
   1  -4 -10    3.08    2.94
  -1  -4  10    1.04    2.48
  -1  -4  10    6.81    2.41
  -1  -4   9   -0.78    1.59
  -1   4   9   -1.26    1.77
  -1  -4   9    1.96    2.31
   1  -4  -9    1.03    2.42
  -1  -4   8    5.73    2.26
  -1   4   8   -0.38    2.00
  -1  -4   8    3.15    2.60
   1  -4  -8    3.17    2.39
  -1  -4   7   63.89    4.99
  -1   4   7   53.23    4.87
  -1  -4   7   67.21    4.96
   1  -4  -7   59.15    4.40
   1  -4  -6    8.60    2.36
  -1   4   6   11.86    2.72
  -1  -4   6    9.13    2.41
  -1  -4   6    6.73    2.26
   1  -4  -5   22.84    2.94
  -1  -4   5   27.50    3.25
  -1   4   5   28.33    3.25
  -1  -4   5   23.93    3.14
  -1  -4   4  187.70    6.76
  -1  -4   4  178.23    7.33
   1  -4  -4  200.23    7.00
  -1  -4   3   -0.79    2.00
  -1  -4   3    0.99    1.27
   1  -4  -3    4.20    1.82
  -1   4   3    0.61    0.56
   1  -4  -2 3064.94   62.31
   1  -4  -2 3098.72   64.89
  -1  -4   2 3053.85   66.04
  -1   4   2 3101.41   60.76
  -1  -4   2 3090.26   60.47
   1  -4  -1  216.16    6.50
  -1  -4   1  215.36    7.46
  -1   4   1  216.08    5.65
   1  -4  -1  224.26    6.39
  -1  -4   1  210.49    5.11
  -1  -4   0   87.43    4.10
   1  -4   0   88.73    3.73
  -1   4   0   86.11    2.84
   1  -4   1    3.84    1.02
   1   4   1    5.52    0.81
   1  -4   1    5.18    1.51
  -1  -4  -1    3.96    1.41
   1  -4   2 1356.75   28.69
   1   4   2 1368.58   28.03
   1  -4   2 1382.60   27.95
   1  -4   2 1328.93   31.12
   1  -4   3   10.73    2.01
   1  -4   3   11.60    2.37
   1   4   3    8.64    1.61
   1  -4   4  224.23    8.80
   1  -4   4  239.74    8.42
   1  -4   5  111.63    6.15
   1  -4   5  102.74    5.67
   1   4   5  107.77    5.61
   1  -4   6  519.58   15.73
   1   4   6  502.46   15.06
   1  -4   6  516.61   16.24
   1  -4   7    0.54    1.99
   1   4   7   -0.27    1.55
   1  -4   7    1.91    1.85
   1  -4   8   69.46    5.84
   1   4   8   66.47    5.57
   1  -4   8   72.84    5.97
   1  -4   9   16.44    4.18
   1   4   9   16.36    3.66
   1  -4   9   13.18    3.64
   1  -4  10    9.53    3.27
   1   4  10    9.11    3.23
   1  -4  10   15.23    4.23
  -1  -4 -10   14.70    3.59
   1  -4  11   -3.09    3.08
   1  -4  11    3.65    2.29
   1   4  11    3.14    2.33
   1  -4  12   58.37    7.05
   1  -4  12   78.36    8.62
   1   4  12   78.60    8.04
   1  -4  13    4.65    3.55
   1   4  13    0.57    2.14
   1  -4  14   25.82    6.51
   1   4  14   26.72    6.00
   1  -4  15   -0.58    3.30
   1   4  15    4.24    3.36
   1   4  16    3.63    2.91
   1  -4  16    6.97    4.90
   1  -4  17   14.37    4.50
   1   4  17   18.14    5.02
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  -1  -5  17   -5.72    3.09
  -1   5  17    4.49    3.17
  -1   5  16    2.02    2.55
  -1  -5  16    1.67    3.79
  -1  -5  15    1.27    1.43
  -1   5  15    4.34    2.99
  -1  -5  15   -2.09    3.03
  -1  -5  14   -0.63    1.21
  -1  -5  14    4.16    3.90
  -1   5  14    2.45    2.51
  -1  -5  13    5.83    2.36
  -1  -5  13   -1.65    3.00
  -1   5  13    6.23    3.48
  -1  -5  12   13.91    4.70
  -1   5  12    8.84    3.64
  -1  -5  12    9.66    3.07
  -1   5  11   -1.62    1.78
  -1  -5  11    0.98    2.80
  -1  -5  11    2.08    2.18
   1  -5 -11    0.73    2.77
   1  -5 -10    8.01    3.27
  -1  -5  10    8.75    3.09
  -1   5  10    9.73    3.26
  -1  -5  10   10.83    3.70
  -1  -5   9    7.78    3.31
  -1   5   9   15.67    3.76
  -1  -5   9   10.26    3.07
   1  -5  -9   12.18    3.20
   1  -5  -8   80.52    5.46
  -1   5   8   96.61    6.17
  -1  -5   8   82.88    6.18
  -1  -5   8   93.79    6.22
  -1   5   7   84.38    5.54
  -1  -5   7   77.47    5.52
  -1  -5   7   83.09    5.68
   1  -5  -7   77.90    5.20
  -1   5   6  101.56    5.81
   1  -5  -6  102.69    5.61
  -1  -5   6   99.59    6.09
  -1  -5   6  104.92    5.81
  -1   5   5    6.93    1.94
  -1  -5   5    9.83    2.76
   1  -5  -5   14.81    2.82
  -1  -5   5   11.43    2.39
  -1  -5   4  119.60    6.22
   1  -5  -4  129.11    5.84
  -1  -5   4  124.15    5.42
  -1  -5   3   64.06    5.17
   1  -5  -3   66.23    3.34
  -1   5   3   62.45    3.69
   1  -5  -3   69.52    4.08
  -1  -5   3   64.20    3.45
   1  -5  -2    0.62    1.70
   1  -5  -2    1.12    1.65
  -1   5   2   -0.23    1.56
  -1  -5   2   -0.65    2.39
  -1  -5   2    0.95    0.99
  -1  -5   1  720.08   14.76
   1  -5  -1  707.25   17.23
   1  -5  -1  714.66   16.50
  -1   5   1  712.19   15.21
  -1  -5   1  676.91   18.25
  -1   5   0 1542.71   30.59
  -1  -5   0 1527.69   34.47
   1  -5   0 1494.79   33.88
  -1  -5  -1  630.43   16.14
   1  -5   1  625.74   16.13
  -1   5  -1  610.88   13.85
  -1   5  -1  625.53   14.03
   1  -5   1  651.94   14.28
   1   5   1  620.58   13.20
   1  -5   2 1234.37   25.14
   1   5   2 1213.06   24.97
   1  -5   2 1172.78   28.31
  -1  -5  -2 1197.05   28.01
   1   5   3  450.75   11.50
   1  -5   3  444.10   13.44
   1  -5   3  455.01   10.03
   1  -5   3  443.08   12.01
   1  -5   4  226.17    8.12
   1  -5   4  213.88    8.64
   1  -5   5  502.34   14.75
   1  -5   5  498.68   15.60
   1  -5   6  163.21    7.83
   1  -5   6  166.17    8.25
   1   5   6  169.03    7.56
   1  -5   7  133.21    7.53
   1   5   7  134.72    7.05
   1  -5   7  146.09    7.98
   1  -5   8   43.81    5.11
   1   5   8   47.19    5.04
   1  -5   8   48.41    5.45
   1  -5   9   29.72    4.64
   1   5   9   33.19    4.74
   1  -5   9   20.97    4.54
  -1  -5 -10    6.56    3.37
   1   5  10    2.27    2.52
   1  -5  10    2.55    3.35
   1  -5  10    6.69    2.83
   1   5  11    2.76    2.80
   1  -5  11    6.39    2.59
   1  -5  11    4.83    3.64
   1  -5  12    2.79    2.55
   1   5  12    0.46    2.48
   1  -5  12   -2.46    2.66
   1  -5  13    2.66    2.80
   1  -5  13   -1.44    3.00
   1   5  13    4.00    2.97
   1  -5  14    7.90    4.45
   1   5  14    8.27    3.71
   1   5  15   -5.89    2.03
   1  -5  15   -3.24    2.95
   1  -5  16    3.29    4.41
   1   5  16    4.20    2.77
   1   5  17    2.34    3.03
   1  -5  17    4.33    3.79
  -1   6  17    1.31    2.39
  -1  -6  17    7.57    4.59
  -1  -6  16   34.04    7.46
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  -1  -6   9  224.42   10.67
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   1  -6  -6  194.70    8.33
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  -1  -6   5  140.82    6.44
   1  -6  -5  147.95    6.80
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   1  -6  -4  368.31   11.38
   1  -6  -4  374.01   10.52
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   1   6   4  760.18   18.01
   1  -6   4  732.58   15.55
   1  -6   4  729.39   18.55
   1  -6   4  718.63   20.33
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   1  -7  -5   86.42    5.41
   1  -7  -5   88.47    4.65
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   1  -7  -4   50.40    3.64
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   1  -7  -3 1516.22   33.78
  -1   7   3 1505.84   31.52
   1  -7  -3 1493.04   33.95
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   1  -7   1 1186.16   25.41
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   1  -7   4   33.26    1.90
   1   7   4   32.33    2.94
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   1   7   5    0.31    1.61
   1  -7   5    1.71    1.60
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   1  -7   6    0.55    1.98
   1   7   6    3.30    1.65
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   1  -7   7  301.63   12.67
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   1   7   8    6.63    2.66
   1  -7   8    7.51    2.80
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   1   7  13   94.97    8.23
   1  -7  13   98.65   10.04
   1  -7  14   26.78    5.24
   1   7  14   20.39    5.16
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   1  -8  -7  133.74    7.51
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   1  -8  -4 1172.29   27.67
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   1  -8  -3   59.38    4.72
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   1   8   2  608.94   13.24
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   1  -8   2  588.19   17.40
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   1   8   4  242.21    7.87
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   1   8   5    0.07    1.40
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   1   8   6  199.44    8.17
   1  -8   6  190.77    9.53
   1  -8   6  191.77    8.76
   1   8   7   39.06    4.16
   1  -8   7   39.92    5.14
   1  -8   7   46.98    4.98
   1  -8   8   70.66    6.12
   1  -8   8   73.54    6.39
   1  -8   9   11.16    3.90
   1   8   9   15.17    3.46
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   1  -8  13   32.57    6.61
   1   8  13   36.06    5.79
   1  -8  13   38.35    6.43
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   1  -9  -4   35.00    4.03
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   1  -9  -3   54.78    5.08
   1  -9  -3   48.87    4.39
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   1  -9  -2   37.21    3.82
   1  -9  -2   45.88    4.99
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   1   9  -1  223.60    5.23
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   1   9  -1  223.32    5.25
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   1  -9  -1  215.83    8.24
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   1   9   2  131.28    3.98
   1  -9   2  129.94    5.35
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   1  -9   2  116.24    7.24
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  -1   9  -3  844.00   19.96
  -1   9  -3  853.90   20.18
   1   9   3  856.66   18.79
   1  -9   3  789.33   22.99
   1  -9   3  871.28   19.31
   1  -9   4  185.93    5.86
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   1  -9   4  187.66    8.99
   1   9   4  178.78    6.58
   1  -9   5    3.63    2.47
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   1  -9   5    2.95    0.91
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   1  -9   6    2.26    2.46
   1  -9   6    3.48    2.16
   1   9   6    0.57    1.63
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   1  -9   7   86.29    6.22
   1  -9   7   87.50    6.88
   1  -9   8   38.39    5.13
   1   9   8   40.70    4.66
   1  -9   8   36.11    5.31
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   1  -9  10    8.93    3.96
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   1  -9  10    4.01    2.87
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   1  -9  11  105.15    8.91
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   1  -9  12    4.47    3.67
   1  -9  13   65.70    8.64
   1  -9  13   57.24    7.69
   1   9  13   45.27    6.58
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   1  -9  14    9.85    4.65
   1  -9  14    4.18    2.64
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   1  -9  15    6.82    4.32
   1  -9  15   11.87    4.55
   1   9  16    6.41    4.01
   1  -9  16   14.89    5.79
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   1 -10 -11   48.57    6.33
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   1 -10  -6  235.20    9.42
  -1 -10   6  246.17    6.74
  -1 -10   6  208.04   10.84
  -1  10   6  243.40    9.08
   1 -10  -5   65.45    5.71
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   1 -10  -3    3.05    2.90
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   1 -10  -2   87.79    6.74
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   1  10  -1  138.04    3.51
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   1 -10   2  428.47   11.84
  -1 -10  -2  402.16   14.09
   1 -10   2  402.68   14.31
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   1 -10   3    7.83    1.95
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  -1  10  -3    9.72    1.99
  -1 -10  -4  206.15    9.46
  -1  10  -4  209.52    8.10
   1 -10   4  201.78    9.84
   1  10   4  221.58    7.29
   1 -10   4  215.25    6.75
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   1  10   7    5.77    2.25
   1 -10   7    7.12    2.88
   1  10   8   73.38    5.65
   1 -10   8   80.40    7.00
   1 -10   8   73.48    6.11
   1 -10   9   23.75    4.90
   1 -10   9   22.01    4.68
   1  10   9   21.66    3.90
   1 -10  10   82.56    8.08
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  -1  11  16   17.03    4.14
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   1 -11  -2  119.84    6.58
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   1 -13  -3   26.49    5.21
   1  13  -3   22.32    2.18
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   1 -13  -2   69.63    7.25
  -1  13   2   67.15    3.80
  -1 -13   2   71.32    7.86
   1 -13  -2   59.83    5.31
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  -2   0  12    0.34    2.55
  -2   0  11   -0.03    1.72
  -2   0  11    1.71    2.91
   2   0 -10  188.87    7.24
  -2   0  10  186.67    8.69
  -2   0  10  185.62    9.86
   2   0  -9    1.45    1.76
  -2   0   9    0.95    1.38
  -2   0   9   -3.39    2.01
  -2   0   8  256.37   10.71
   2   0  -8  248.82    8.09
  -2   0   8  253.42    9.34
   2   0  -7    1.31    1.59
  -2   0   7   -1.06    1.86
  -2   0   7    0.75    1.38
  -2   0   6  325.93    9.76
  -2   0   6  311.34   10.81
   2   0  -6  319.06    8.89
  -2   0   5   -0.06    1.04
  -2   0   5    1.79    2.07
   2   0  -5   -0.10    1.33
  -2   0   4 2606.55   54.41
  -2   0   4 2497.18   52.37
   2   0  -4 2595.50   52.02
  -2   0   3   -1.04    1.45
  -2   0   3   -0.48    0.96
   2   0  -3    0.86    0.87
  -2   0   2  757.66   16.78
  -2   0   2  770.15   17.06
   2   0  -2  747.24   16.48
  -2   0   1   -3.78    0.87
  -2   0   0 9992.89  195.84
  -2   0  -1   -0.44    0.63
  -2   0  -1    0.96    0.73
  -2   0  -2  771.80   17.67
  -2   0  -2  769.07   17.85
   2   0   3   -1.74    1.05
   2   0   4    9.59    2.26
   2   0   5    0.57    1.56
   2   0   6    1.72    1.85
   2   0   7   -0.58    1.78
   2   0   8   -0.21    1.81
   2   0   9    1.38    2.38
   2   0  10   85.00    7.17
   2   0  11   -2.36    2.33
   2   0  12    6.23    3.47
   2   0  13   -0.31    2.30
   2   0  14   94.80   10.03
   2   0  15    6.26    3.39
   2   0  16   -2.23    2.29
   2   0  17    3.77    3.08
  -2  -1  18    6.74    2.99
  -2   1  18    3.13    2.72
  -2  -1  17   21.14    5.50
  -2   1  17   24.06    5.58
  -2  -1  16   -0.82    2.47
  -2   1  16    2.86    3.09
  -2   1  15  100.19    9.89
  -2  -1  15   90.28    9.48
  -2  -1  14    1.29    2.52
  -2   1  14    4.40    2.94
  -2  -1  13   13.73    4.41
  -2   1  13   10.89    4.02
  -2   1  12    4.95    3.33
  -2  -1  12   10.67    4.07
  -2  -1  12    9.29    2.77
  -2   1  11  133.21    8.70
  -2  -1  11  120.45    7.45
  -2  -1  11  122.12    8.32
   2  -1 -10   -2.52    2.00
  -2   1  10    2.27    2.34
  -2  -1  10    2.09    1.71
  -2  -1  10   -0.19    2.13
  -2   1   9  403.15   14.76
   2   1  -9  407.31   11.20
  -2  -1   9  415.03   14.81
  -2   1   9  412.93   13.31
  -2  -1   9  427.20   13.87
   2  -1  -9  415.25   12.05
  -2  -1   8  190.39    9.10
  -2   1   8  195.39    7.76
  -2   1   8  193.96    9.21
   2   1  -8  193.62    6.55
  -2  -1   8  201.86    8.19
   2  -1  -8  204.32    7.22
  -2  -1   7  256.03   10.02
  -2  -1   7  244.52    9.15
   2  -1  -7  275.83    8.37
  -2   1   7  243.60    8.53
  -2   1   7  268.37   10.28
   2   1  -7  256.24    7.52
   2   1  -6   50.89    3.01
  -2  -1   6   51.36    4.37
  -2  -1   6   54.84    3.63
  -2   1   6   53.60    3.25
  -2   1   6   50.65    4.35
   2  -1  -6   64.49    3.66
   2  -1  -5   13.29    2.11
   2   1  -5   15.20    1.76
  -2   1   5   12.84    2.70
  -2  -1   5    9.93    1.97
  -2  -1   5   11.18    2.60
  -2   1   5   16.45    1.75
   2  -1  -4 3698.49   72.71
  -2  -1   4 3685.18   76.20
   2   1  -4 3608.08   72.12
  -2   1   4 3741.48   75.75
  -2   1   4 3500.08   72.26
  -2  -1   4 3505.83   72.25
  -2  -1   3  108.93    4.78
  -2  -1   3  108.10    4.39
   2  -1  -3  122.38    4.29
  -2   1   3  115.70    4.88
   2   1  -3  110.70    3.68
  -2   1   2   29.52    2.31
  -2  -1   2   27.01    2.03
  -2  -1   2   27.16    2.03
   2  -1  -2   23.87    1.75
  -2  -1   1  840.53   18.00
   2  -1  -1  851.02   18.36
  -2   1   1  870.13   18.27
  -2   1   0   34.74    1.89
  -2  -1   0   25.18    1.60
  -2  -1  -1  322.48    8.14
  -2   1  -1  315.56    8.24
  -2  -1  -1  316.35    8.00
   2  -1   1  300.36    8.60
   2  -1   2 2667.39   58.15
  -2  -1  -2 2656.11   53.95
  -2  -1  -2 2756.66   54.59
  -2   1  -2 2710.72   54.25
  -2   1  -2 2745.34   54.69
   2  -1   3   18.08    2.44
   2   1   3   17.71    2.29
   2  -1   3   20.71    2.53
   2  -1   4  116.47    5.92
   2   1   4  118.22    5.79
   2  -1   4  122.75    5.89
   2  -1   5   31.21    3.66
   2  -1   5   31.33    3.57
   2   1   5   27.02    3.39
   2   1   6  139.37    7.17
   2  -1   6  113.07    6.65
   2   1   7   72.98    5.75
   2  -1   7   92.65    6.45
   2   1   8    0.15    2.19
   2  -1   8    1.89    2.38
   2  -1   9   -1.30    1.89
   2   1   9   -2.49    1.82
   2   1  10   -3.22    1.35
   2  -1  10    1.29    2.18
   2  -1  11   16.44    4.25
   2   1  11   29.08    5.43
   2   1  12   35.58    6.17
   2  -1  12   48.13    6.92
   2  -1  13  215.35   13.15
   2   1  13  221.10   13.04
   2   1  14   -1.92    2.06
   2  -1  14    3.48    2.93
   2  -1  15    4.76    3.18
   2   1  15   -2.24    2.54
   2  -1  16    1.77    2.63
   2   1  16   -1.49    2.24
   2  -1  17   -1.27    2.56
   2   1  17    6.51    3.57
  -2   2  18    8.38    3.65
  -2  -2  18    8.33    3.45
  -2   2  17    3.38    2.87
  -2  -2  17    1.93    2.91
  -2  -2  16   24.79    5.65
  -2   2  16   30.24    6.32
  -2   2  15   13.59    4.89
  -2  -2  15   13.67    4.58
  -2   2  14    8.32    3.81
  -2  -2  14    6.17    3.82
  -2  -2  13   12.79    3.47
  -2  -2  13   12.18    5.02
  -2   2  13   12.10    4.08
  -2   2  12   15.93    4.28
  -2  -2  12    3.20    3.33
  -2  -2  12    5.64    2.54
  -2  -2  11    7.94    3.88
  -2  -2  11   10.54    3.04
  -2   2  11    6.00    3.49
   2  -2 -10  200.84    8.18
  -2  -2  10  206.79   10.36
  -2   2  10  208.85   10.16
  -2  -2  10  195.11    9.32
   2  -2  -9    0.76    2.13
  -2   2   9    2.38    2.58
   2   2  -9    1.00    1.26
  -2  -2   9    0.32    1.75
  -2  -2   9    1.78    2.51
   2  -2  -8  158.58    6.61
  -2  -2   8  164.16    8.36
  -2   2   8  150.12    7.94
  -2  -2   8  161.08    7.61
   2   2  -8  159.18    5.37
  -2   2   7 1018.45   25.99
   2  -2  -7 1033.59   24.23
  -2  -2   7 1093.31   26.53
  -2  -2   7 1049.16   26.28
   2   2  -7 1074.07   22.75
  -2  -2   6    4.29    1.82
   2   2  -6    1.71    1.01
  -2  -2   6   -0.42    2.10
  -2   2   6    1.97    2.11
   2  -2  -6    5.17    1.85
   2  -2  -5  110.38    4.82
  -2  -2   5  108.96    5.79
  -2  -2   5  107.21    5.12
   2   2  -5  107.06    3.74
  -2   2   5  113.31    5.79
  -2   2   5  106.19    3.94
  -2  -2   4    3.71    1.97
  -2  -2   4    2.35    1.90
  -2   2   4    3.93    2.26
   2  -2  -4    4.27    1.70
   2  -2  -3    6.20    1.59
  -2  -2   3    1.50    1.41
  -2   2   3    1.67    1.81
  -2  -2   3    3.10    1.60
   2  -2  -2 1468.03   30.57
  -2   2   2 1465.58   30.28
  -2  -2   2 1435.36   29.95
   2  -2  -1  312.35    7.63
   2  -2  -1  321.05    8.14
  -2  -2   1  324.77    7.70
  -2   2   1  316.68    7.98
  -2  -2   1  317.88    8.62
  -2  -2   0  925.59   19.06
  -2   2   0  923.25   19.50
   2  -2   0  907.81   20.58
   2  -2   1  362.71    9.98
  -2  -2  -1  377.90    9.14
  -2  -2  -1  367.36    8.98
  -2   2  -1  363.32    9.40
  -2   2  -2    4.80    1.49
  -2   2  -2    3.90    1.49
   2  -2   2    4.06    1.52
   2   2   3   32.73    2.88
   2  -2   3   26.13    2.78
   2  -2   3   30.71    3.08
   2   2   4   12.35    2.30
   2  -2   4   13.35    2.48
   2  -2   4   11.50    2.44
   2  -2   5  136.87    6.99
   2  -2   5  150.01    7.02
   2   2   5  128.54    6.61
   2  -2   6   98.37    6.10
   2  -2   6   91.65    5.98
   2   2   6   98.68    6.01
   2  -2   7    4.27    2.26
   2   2   7    0.08    1.90
   2  -2   7    3.76    2.25
   2   2   8   18.64    3.83
   2  -2   8   17.27    3.63
   2  -2   8   21.37    4.03
   2  -2   9    6.87    3.12
   2   2   9   11.26    3.67
   2  -2  10   23.70    4.69
   2   2  10   26.77    5.01
   2  -2  11    3.80    3.02
   2   2  11    2.74    2.54
   2   2  12   26.86    5.51
   2  -2  12   28.63    5.68
   2   2  13    2.81    2.68
   2  -2  13    0.77    2.70
   2   2  14   69.95    8.90
   2  -2  14   77.51    9.31
   2   2  15    2.78    2.92
   2  -2  15    1.59    3.09
   2   2  16   10.31    3.82
   2  -2  16    9.51    4.15
  -2  -3  18    3.80    4.18
  -2   3  18   -2.13    1.99
  -2   3  17    3.40    3.37
  -2  -3  17    0.61    4.40
  -2   3  16   -1.22    2.73
  -2  -3  16   -0.77    3.63
  -2   3  15   25.28    6.07
  -2  -3  15   15.72    5.61
  -2   3  14    4.60    3.28
  -2  -3  14    5.98    4.10
  -2  -3  14    7.42    2.63
  -2  -3  13    2.58    2.07
  -2  -3  13    4.11    3.74
  -2   3  13    1.81    2.90
  -2  -3  12    2.73    1.79
  -2   3  12    1.29    2.78
  -2  -3  12    2.52    3.69
   2  -3 -11   54.59    4.93
  -2  -3  11   51.24    5.47
  -2   3  11   52.58    6.09
  -2  -3  11   53.33    6.50
  -2  -3  10    3.29    2.34
  -2   3  10    1.25    2.22
   2  -3 -10    3.67    2.59
  -2  -3  10    3.21    2.62
   2   3  -9  253.26    6.98
  -2  -3   9  252.90   10.51
  -2   3   9  276.20   11.59
  -2  -3   9  245.07   11.15
   2  -3  -9  251.83    9.32
  -2  -3   8   12.09    3.23
  -2  -3   8   12.29    2.71
   2  -3  -8   17.96    3.05
  -2   3   8   14.50    3.53
   2   3  -8   16.87    1.59
   2  -3  -7   25.04    3.06
  -2  -3   7   16.69    2.94
  -2   3   7   23.81    3.71
  -2  -3   7   19.86    3.56
  -2   3   6    7.25    2.50
  -2  -3   6    6.88    2.62
  -2  -3   6    4.47    1.88
   2  -3  -6   10.10    2.35
   2  -3  -5   28.77    3.00
  -2   3   5   29.35    3.60
  -2  -3   5   32.06    3.49
  -2   3   4   15.59    2.90
  -2  -3   4   19.63    2.58
   2  -3  -4   21.47    2.56
  -2  -3   3    8.29    1.92
  -2   3   3   11.30    2.39
  -2  -3   3    4.81    1.62
   2  -3  -3   11.59    2.01
  -2  -3   2  401.64    9.73
   2  -3  -2  385.91   10.10
  -2  -3   2  399.04   11.25
  -2  -3   1 1872.87   37.06
   2  -3  -1 1848.68   39.41
   2  -3  -1 1853.48   38.21
  -2  -3   1 1842.04   40.50
  -2  -3   0   30.61    2.41
   2  -3   0   33.19    2.13
  -2   3   0   25.82    1.84
  -2  -3   0   33.25    1.63
  -2  -3  -1 1474.90   29.81
  -2   3  -1 1439.18   30.52
   2  -3   1 1456.30   32.80
   2  -3   1 1473.06   30.38
  -2  -3  -1 1506.39   30.10
  -2   3  -2   80.11    3.98
  -2   3  -2   84.18    4.10
   2  -3   2   72.14    4.11
   2   3   3  387.11   10.81
   2  -3   4    5.54    2.06
   2  -3   4    5.76    1.93
   2   3   4    7.11    1.93
   2  -3   5  623.14   17.64
   2  -3   5  623.31   18.42
   2   3   5  643.65   17.39
   2  -3   6   23.42    3.71
   2   3   6   24.34    3.53
   2  -3   6   20.11    3.72
   2  -3   7   57.97    5.12
   2   3   7   61.77    5.13
   2  -3   7   62.29    5.39
   2  -3   8    5.88    2.76
   2  -3   8    9.97    3.19
   2   3   8    5.85    2.70
   2   3   9   58.99    6.24
   2  -3   9   58.55    5.54
   2  -3   9   53.59    6.35
   2   3  10   45.34    5.99
   2  -3  10   59.74    6.84
   2   3  11    2.60    2.88
   2  -3  11    3.71    2.97
   2  -3  12   41.72    6.89
   2   3  12   50.49    7.04
   2   3  13   60.79    7.76
   2  -3  13   79.39    9.07
   2  -3  14   13.41    4.41
   2   3  14    5.75    3.73
   2   3  15   16.30    4.95
   2  -3  15   14.22    4.58
   2   3  16    6.82    2.92
   2  -3  16    2.48    2.71
  -2  -4  18    8.16    4.64
  -2   4  18    6.74    2.80
  -2   4  17    0.40    2.64
  -2  -4  17    0.17    3.49
  -2   4  16   26.45    6.09
  -2  -4  16   26.00    6.70
  -2   4  15    4.82    3.63
  -2  -4  15   -4.77    3.13
  -2  -4  15    1.35    2.29
  -2   4  14    1.90    3.07
  -2  -4  14    3.59    2.36
  -2  -4  14    5.12    3.99
  -2  -4  13    0.54    1.72
  -2   4  13    1.91    2.72
  -2  -4  13   -0.88    3.51
  -2  -4  12    9.61    4.04
  -2  -4  12    6.61    2.64
  -2   4  12    3.35    2.91
  -2  -4  11   -2.05    2.74
   2  -4 -11    2.60    2.78
  -2   4  11    0.09    2.38
  -2  -4  11    0.14    1.96
  -2  -4  10    1.07    1.84
  -2  -4  10   -0.96    2.20
  -2   4  10   -0.31    2.16
   2  -4 -10    3.13    2.73
  -2  -4   9    0.84    1.07
  -2   4   9    1.15    2.56
   2  -4  -9    2.69    2.60
  -2  -4   9    4.67    2.97
  -2   4   8  177.16    8.76
   2  -4  -8  179.69    7.63
  -2  -4   8  168.90    8.52
  -2   4   7   80.59    5.45
   2  -4  -7   72.05    4.76
  -2  -4   7   72.14    5.34
  -2   4   6  186.32    7.89
  -2  -4   6  180.64    7.89
   2  -4  -6  180.29    7.21
  -2   4   5   49.25    4.20
  -2  -4   5   51.56    4.14
  -2  -4   5   31.84    3.29
   2  -4  -5   50.77    3.67
  -2  -4   4  329.77    9.57
  -2  -4   4  310.42   10.61
   2  -4  -4  316.35    9.51
  -2   4   4  318.99    9.84
  -2  -4   3 4319.61   85.36
   2  -4  -3 4401.00   87.59
  -2  -4   3 4362.21   92.61
   2  -4  -2 1574.74   33.67
   2  -4  -2 1568.73   34.20
  -2  -4   2 1571.45   36.17
  -2  -4   2 1643.37   32.51
   2  -4  -1  464.31   11.84
  -2  -4   1  497.53   10.85
  -2  -4   1  483.89   13.19
   2  -4  -1  489.76   11.74
  -2  -4   0    1.27    1.47
   2  -4   0   -0.27    1.09
  -2   4   0   -0.57    0.22
   2  -4   0   -0.03    0.31
  -2  -4   0   -0.31    0.62
   2  -4   1   65.34    3.70
   2  -4   1   68.93    3.09
  -2  -4  -1   67.90    2.85
  -2   4  -1   72.67    3.45
  -2  -4  -1   68.89    2.82
  -2   4  -2   95.41    4.42
  -2   4  -2   99.26    4.50
   2  -4   2   94.40    3.38
   2  -4   2   84.20    4.77
   2   4   2   94.48    3.96
   2   4   3    0.65    0.70
  -2   4  -3    0.89    1.44
   2  -4   3    0.83    1.59
  -2   4  -3   -1.54    0.99
   2  -4   4   87.03    5.34
   2  -4   4   92.65    5.30
   2  -4   5    5.52    2.22
   2   4   5    3.99    2.06
   2  -4   5    1.72    2.01
   2  -4   6 1086.89   29.48
   2  -4   6 1143.84   28.44
   2   4   6 1113.24   27.55
   2   4   7    5.47    2.27
   2  -4   7    5.28    2.57
   2  -4   7    6.61    2.57
   2  -4   8   66.86    6.33
   2   4   8   66.61    5.75
   2  -4   8   59.19    5.65
   2   4   9    2.76    2.42
   2  -4   9    0.37    2.03
   2  -4   9    2.75    3.02
   2  -4  10    4.33    2.46
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   2   4  10    7.15    2.67
   2  -4  11    3.79    3.79
   2   4  11    3.72    3.09
   2  -4  11    6.47    2.99
   2  -4  12   21.56    5.73
   2   4  12   24.67    5.06
   2   4  13   18.63    4.63
   2  -4  13   14.09    4.86
   2  -4  14  115.21   11.28
   2   4  14  121.95   10.24
   2  -4  15   -1.05    3.74
   2   4  15    5.40    2.99
   2   4  16   11.07    4.25
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  -2   5  13   22.47    5.07
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  -2   5  12    6.11    3.15
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  -2  -5   3  902.45   20.05
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   2  -5  -2  933.23   21.27
   2  -5  -2  953.38   21.64
  -2  -5   2  932.74   19.95
  -2  -5   1  381.57    8.82
  -2  -5   1  397.92   11.83
   2  -5  -1  386.73   10.15
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   2  -5  -1  362.91   10.10
   2  -5   0 7746.76  160.45
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   2   5   2    0.18    0.97
   2   5   3  785.68   18.23
  -2   5  -3  761.82   18.93
  -2   5  -3  766.14   19.18
   2  -5   3  789.61   20.79
   2  -5   4   23.67    3.37
   2   5   4   14.15    2.20
   2  -5   4   26.87    3.28
   2  -5   5  730.61   21.43
   2  -5   5  780.64   20.41
   2  -5   6   -1.53    1.43
   2  -5   6    0.50    2.02
   2   5   6    2.29    1.89
   2   5   7   51.89    5.00
   2  -5   7   55.87    5.37
   2  -5   7   58.17    5.62
   2  -5   8   24.14    4.44
   2  -5   8   26.77    4.68
   2   5   8   19.63    3.79
   2  -5   9   84.73    7.77
   2  -5   9   76.05    6.76
   2   5   9   84.58    6.55
   2  -5  10   32.40    5.14
   2  -5  10   25.35    5.32
   2   5  10   34.44    5.25
   2   5  11   50.93    6.64
   2  -5  11   49.97    6.62
   2  -5  11   50.25    7.15
   2  -5  12   31.18    6.27
   2  -5  12   32.82    5.88
   2   5  12   32.30    5.74
   2   5  13    8.20    3.29
   2  -5  13   13.57    5.33
   2  -5  14    2.43    3.68
   2   5  14    4.98    3.14
   2  -5  15   42.23    8.31
   2   5  15   56.04    8.28
   2  -5  16    3.44    4.06
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  -2   6  13   12.48    4.38
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  -2   6  11   33.47    5.19
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   2  -6  -9    1.04    2.59
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   2  -6  -8  180.74    8.30
  -2   6   8  186.47    9.06
  -2  -6   8  189.45    9.19
  -2  -6   8  177.07    8.86
   2  -6  -7    0.17    2.14
  -2   6   7   -1.41    2.12
  -2  -6   7   -0.51    2.03
  -2  -6   7   -0.22    1.92
  -2   6   6  483.27   14.88
  -2  -6   6  535.42   15.17
   2  -6  -6  530.76   15.22
  -2  -6   6  560.14   16.73
   2  -6  -5   40.07    2.80
   2  -6  -5   40.03    3.75
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   2  -6   2  651.63   17.15
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   2   6   3   24.49    2.42
   2  -6   3   23.98    1.87
   2  -6   4  163.31    7.80
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   2   6   4  161.92    6.65
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   2  -6   5   12.23    2.82
   2   6   5   10.04    2.27
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   2  -6   6  200.86    9.11
   2  -6   6  193.94    9.46
   2  -6   7   18.98    3.93
   2   6   7   22.98    3.71
   2  -6   7   23.84    4.22
   2   6   8   85.71    6.51
   2  -6   8  120.22    7.73
   2  -6   8   93.96    6.95
   2   6   9    5.51    2.68
   2  -6   9    5.60    2.96
   2  -6   9    6.30    3.38
   2  -6  10   34.55    5.85
   2  -6  10   36.50    5.53
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   2   6  11   22.57    4.85
   2  -6  11   20.49    5.40
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   2   6  12   48.68    6.81
   2  -6  12   35.24    6.12
   2  -6  13   20.89    6.21
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   2   6  14   57.79    8.06
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   2  -7   4   47.16    4.73
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   2  -7   5  662.72   20.25
   2   7   5  677.23   17.82
   2   7   6   25.01    3.33
   2  -7   6   40.70    5.00
   2  -7   6   38.64    4.53
   2  -7   7   93.29    6.74
   2  -7   7   78.54    6.33
   2  -7   8   58.27    6.14
   2   7   8   66.35    5.69
   2  -7   8   67.92    6.55
   2  -7   9   66.36    6.23
   2   7   9   68.70    6.01
   2  -7   9   62.93    6.74
   2  -7  10   32.93    5.82
   2   7  10   22.42    4.52
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   2   7  11   85.22    8.16
   2  -7  11   82.84    8.53
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   2   7  13   14.23    4.17
   2  -7  14    1.15    3.85
   2   7  14    1.88    2.85
   2   7  15   41.22    6.95
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   2  -8  -6   44.50    4.54
   2  -8  -6   38.54    3.45
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   2  -8  -5  294.96    9.32
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   2  -8  -5  286.35   10.73
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   2  -8  -4    6.15    2.56
  -2   8   3   83.78    4.94
   2  -8  -3   78.94    5.29
  -2  -8   3   81.33    3.88
   2  -8  -3   83.35    5.49
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   2  -8  -2  134.56    6.30
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   2  -8  -2  140.35    6.95
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   2  -8  -1  227.03    8.17
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   2  -8  -1  231.97    8.74
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   2  -8   0    2.82    1.18
   2  -8   0    5.18    2.58
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  -2  -8  -1  511.98   16.01
   2  -8   1  536.17   13.69
   2  -8   1  533.91   15.57
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   2  -8   2   76.30    3.99
   2  -8   2   76.00    5.49
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   2   8   3   34.15    2.67
   2  -8   3   32.67    2.51
   2  -8   3   37.34    4.16
  -2   8  -4  356.95   11.57
   2   8   4  354.24   10.62
   2  -8   4  352.10   13.02
   2  -8   4  363.61    9.08
  -2   8  -4  356.29   11.68
   2  -8   5  387.54   14.31
   2   8   5  397.44   12.06
  -2   8  -5  366.81   12.64
  -2   8  -5  391.25   13.22
   2   8   6  199.15    8.41
   2  -8   6  174.51    8.77
   2  -8   6  202.92   10.06
   2  -8   7   81.56    6.26
   2  -8   7   87.29    6.85
   2   8   7   87.44    5.86
   2  -8   8   22.77    4.43
   2  -8   8   34.56    5.31
   2  -8   9   16.01    3.91
   2  -8   9   23.91    4.83
   2   8   9   18.47    3.73
   2   8  10   80.58    6.68
   2  -8  10   81.02    8.18
   2  -8  10   72.10    6.95
   2  -8  11   46.24    7.00
   2   8  11   39.69    6.00
   2  -8  11   47.44    6.92
   2   8  12   60.36    7.18
   2  -8  12   84.41    9.26
   2  -8  12   62.30    7.71
   2  -8  13    6.40    4.40
   2   8  13    2.34    2.74
   2  -8  13   -0.26    2.36
   2  -8  14    9.13    3.71
   2   8  14   13.54    4.87
   2  -8  14   16.29    5.44
   2   8  15    1.21    2.69
  -2   8 -16   75.11   14.36
  -2   8 -16   56.66   12.03
   2   8  16   36.36    6.74
  -2  -9  17    6.03    4.52
  -2   9  17    7.31    3.65
  -2   9  16    2.15    2.78
  -2  -9  16   -3.03    1.79
  -2  -9  16   -2.81    3.58
  -2   9  15    8.35    3.85
  -2  -9  15    5.64    4.29
  -2  -9  15    8.75    3.13
  -2   9  14    3.63    2.76
  -2  -9  14    3.50    2.30
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  -2  -9  13    8.63    3.67
  -2  -9  13   10.07    4.44
   2  -9 -13    6.46    4.20
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   2  -9 -12   40.21    5.74
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  -2   9  12   30.80    5.49
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   2  -9 -11    1.40    3.10
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   2  -9 -10    3.81    3.55
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   2  -9  -9  102.95    7.44
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   2  -9  -8  118.35    6.24
   2  -9  -8  118.32    7.40
  -2  -9   8  114.81    7.29
  -2  -9   8  126.73    8.22
   2  -9  -7   29.87    4.55
   2  -9  -7   36.48    3.55
  -2  -9   7   23.64    4.37
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  -2  -9   7   30.25    3.93
  -2  -9   6    0.54    2.52
  -2   9   6    4.12    2.68
   2  -9  -6    2.90    2.10
   2  -9  -6    3.58    2.62
  -2  -9   6    1.93    1.88
   2  -9  -5   91.43    5.39
   2  -9  -5   97.42    6.17
  -2  -9   5   86.49    7.03
  -2   9   5   95.37    5.46
  -2  -9   5   99.31    5.13
   2  -9  -4   43.80    4.34
   2  -9  -4   41.11    4.00
  -2  -9   4   39.93    5.52
  -2  -9   4   40.30    3.14
  -2   9   4   34.49    3.67
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  -2  -9   3  241.40    7.03
   2  -9  -3  247.47    9.41
  -2   9   3  236.22    8.05
   2  -9  -3  229.82    9.13
   2  -9  -2    9.82    3.46
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   2  -9  -2   12.31    2.72
  -2  -9   2   13.15    1.39
  -2  -9   2   11.48    4.92
   2  -9  -1   29.64    3.34
   2  -9  -1   28.93    4.15
  -2   9   1   28.50    2.61
  -2  -9   1   29.35    5.18
  -2   9   0   90.88    3.98
   2  -9   0   95.02    5.94
  -2  -9   0   89.63    6.56
  -2   9  -1   73.20    3.68
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  -2  -9  -1   71.85    2.39
   2  -9   1   73.89    4.31
   2  -9   1   77.41    5.54
  -2   9  -2    2.86    1.39
   2  -9   2    2.82    2.35
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   2  -9   2    2.16    1.62
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  -2  -9  -2    2.88    0.98
  -2   9  -3  102.01    5.28
  -2   9  -3   96.24    5.15
  -2  -9  -3  121.39    7.03
   2   9   3  128.06    4.84
   2  -9   3  130.66    4.98
   2  -9   3  112.19    6.89
  -2  -9  -4  133.97    7.54
   2   9   4  145.24    5.92
   2  -9   4  144.41    5.07
   2  -9   4  137.00    7.76
   2  -9   5  244.51   11.16
  -2   9  -5  270.60   10.34
   2   9   5  271.68    9.46
  -2   9  -5  281.88   10.64
   2  -9   5  271.83    7.08
   2   9   6  169.96    7.65
  -2   9  -6  161.65    8.13
   2  -9   6  162.27    9.18
  -2   9  -6  164.33    8.46
   2  -9   7  135.21    8.24
   2  -9   7  137.94    8.66
   2   9   7  156.91    7.83
   2  -9   8   21.76    4.57
   2   9   8   16.82    3.60
   2  -9   8   17.41    4.21
   2  -9   9   -2.57    1.68
   2   9   9    0.41    0.70
   2  -9   9   -0.53    2.10
   2  -9  10   95.11    8.31
   2  -9  10   97.25    8.12
   2   9  10   95.62    7.11
   2  -9  11   63.53    7.99
   2  -9  11   66.32    7.95
   2   9  11   71.99    7.34
   2  -9  12    0.84    3.65
   2  -9  12   -3.00    1.68
   2   9  12    2.73    2.30
   2  -9  13   29.45    7.21
   2   9  13   36.34    6.07
   2  -9  13   26.93    5.74
   2   9  14   -1.64    2.75
   2  -9  14   10.64    3.78
   2  -9  15   47.54    7.84
   2   9  15   43.53    7.20
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   2 -10  -6  163.98    7.31
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   2 -12   0  255.51   10.94
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  -2 -29  -4   -4.93    3.59
  -2 -29  -5   -7.23    2.72
   2 -29   5    6.52    4.73
  -2 -29  -6   -3.21    3.36
   2 -29   6    6.34    5.63
  -2 -29  -7   -2.58    4.15
   2 -29   7   19.96    6.65
  -2 -30   7    1.97    5.39
   2 -30  -7    6.49    4.46
   2 -30  -6    5.85    4.73
  -2 -30   6    6.92    6.76
   2 -30  -5   20.84    6.28
  -2 -30   5    7.00    7.26
   2 -30  -4   -1.01    4.16
  -2 -30   4   11.71    7.96
  -2 -30   3   13.97    8.89
   2 -30  -3   25.49    7.08
  -2 -30   2    5.74    8.60
   2 -30  -2    6.80    4.52
  -2 -30   2   -2.88    3.35
   2 -30  -1   33.77    8.61
  -2 -30   1   15.94    5.84
  -2 -30   1   24.94    9.48
   2 -30  -1   16.26    6.06
   2 -30   0    4.60    4.58
   2 -30   0   12.78    7.45
  -2 -30   0    4.35    4.19
  -2 -30   0    3.45    8.56
   2 -30   1   15.32    7.57
  -2 -30  -1    7.65    4.73
  -2 -30  -1   17.71   10.56
  -2 -30  -2    3.41    4.47
  -2 -30  -2    9.02    9.90
   2 -30   2   12.15    5.46
   2 -30   3   11.09    6.84
  -2 -30  -3   12.67   11.16
  -2 -30  -3   10.17    4.85
  -2 -30  -4   -1.17    3.37
   2 -30   4    7.27    5.36
  -2 -30  -5   13.15    4.78
   2 -30   5   19.31    7.36
  -2 -30  -6   -2.39    3.74
   2 -30   6   14.48    5.91
  -2 -31   6    9.85    5.75
   2 -31  -6   -6.87    3.25
   2 -31  -5   -0.40    3.47
  -2 -31   5   -2.36    5.23
   2 -31  -4    3.69    4.42
  -2 -31   4    0.55    6.50
  -2 -31   3    4.51    7.20
   2 -31  -3    0.06    3.83
   2 -31  -2    6.72    5.04
  -2 -31   2   21.43    9.80
   2 -31  -1    0.36    3.81
  -2 -31   1    4.22    4.41
  -2 -31   1    1.94    8.34
   2 -31   0   10.07    6.51
  -2 -31   0   22.08   10.28
  -2 -31   0    6.62    4.52
   2 -31   0    3.27    4.19
  -2 -31  -1   -0.67    3.25
   2 -31   1   11.36    6.25
  -2 -31  -1   15.74    9.49
  -2 -31  -2    7.48    4.56
  -2 -31  -2    7.16    9.70
   2 -31   2    5.31    6.20
  -2 -31  -3    3.18    4.20
   2 -31   3    3.05    5.19
   2 -31   4    9.62    6.15
  -2 -31  -4    9.70    4.03
   2 -32  -4    3.67    4.29
  -2 -32   4   18.05    7.75
   2 -32  -3    5.29    4.76
  -2 -32   3    9.13    7.74
   2 -32  -2    9.27    5.16
  -2 -32   2    1.93    7.87
  -2 -32   1   17.11    5.22
  -2 -32   1   36.89   10.83
   2 -32  -1   16.99    6.10
  -2 -32   0   -0.63    3.54
  -2 -32   0    2.80    8.05
   2 -32   0    1.22    5.82
   2 -32   1    4.43    5.91
  -2 -32  -1   11.70    4.80
  -2 -32  -1    2.02    8.22
  -2 -32  -2   20.94   10.82
   2 -32   2    4.11    5.44
  -2 -32  -2    0.70    3.77
  -2 -32  -3    4.07    3.59
  -3   0  18   27.91    6.03
  -3   0  17   -1.99    2.24
  -3   0  16   32.71    6.20
  -3   0  15   -0.27    2.72
  -3   0  14   32.54    6.03
  -3   0  13   -0.77    2.68
  -3   0  12  191.68    9.39
  -3   0  12  208.63   11.42
  -3   0  11   -0.54    1.68
  -3   0  11    2.37    2.89
  -3   0  10  200.56    8.67
   3   0 -10  205.54    7.88
  -3   0  10  215.47   10.73
  -3   0   9   -0.36    2.44
  -3   0   9    0.05    1.33
   3   0  -9   -1.22    1.63
  -3   0   8   50.58    5.02
   3   0  -8   44.92    3.62
  -3   0   7    1.44    1.41
  -3   0   7   -2.67    1.98
   3   0  -7    0.23    1.54
  -3   0   6  642.74   16.03
  -3   0   6  648.74   17.62
   3   0  -6  636.61   15.72
   3   0  -5   -1.53    1.20
  -3   0   5    3.92    2.52
  -3   0   5   -1.26    1.18
  -3   0   4  823.27   19.96
  -3   0   4  820.71   18.90
   3   0  -4  820.41   18.71
  -3   0   3   -1.39    1.47
   3   0  -3   -0.32    1.22
  -3   0   3   -0.23    1.83
  -3   0   2   18.15    1.59
  -3   0   2   20.47    2.27
  -3   0   1   -0.04    0.82
  -3   0   0  761.41   17.04
  -3   0  -1   -0.93    0.98
  -3   0  -2  543.27   13.99
  -3   0  -2  535.46   14.02
  -3   0  -3    1.95    1.44
  -3   0  -3    1.32    1.33
  -3   0  -4   57.89    4.49
  -3   0  -4   57.31    4.31
   3   0   5    1.79    1.66
   3   0   6  383.06   13.49
   3   0   7    1.29    2.01
   3   0   8    2.72    2.24
   3   0   9    0.27    2.07
   3   0  10   49.17    6.49
   3   0  11    0.66    2.49
   3   0  12   70.72    8.29
   3   0  13    2.27    3.15
   3   0  14    9.38    4.17
   3   0  15    5.91    3.53
  -3   1  18    4.99    3.28
  -3  -1  18    3.47    3.53
  -3   1  17   41.58    7.45
  -3  -1  17   27.00    5.87
  -3   1  16    3.64    3.50
  -3  -1  16    3.47    3.32
  -3  -1  15   17.11    4.93
  -3   1  15   25.17    5.62
  -3  -1  14    4.86    3.31
  -3   1  14   -2.08    2.81
  -3  -1  13  127.93    7.89
  -3  -1  13  129.66    9.49
  -3   1  13  126.49    9.30
  -3  -1  12    2.46    2.15
  -3   1  12   -3.28    2.14
  -3  -1  12    0.88    2.73
  -3   1  11  151.15    9.54
  -3  -1  11  137.73    7.56
  -3  -1  11  152.00    9.36
   3  -1 -11  140.83    7.02
  -3  -1  10   16.64    3.15
   3   1 -10   18.71    2.58
  -3   1  10   17.23    2.87
   3  -1 -10   23.69    3.35
  -3   1  10   12.19    3.59
  -3  -1  10   22.29    4.53
  -3   1   9   40.23    4.93
  -3   1   9   39.35    3.43
   3  -1  -9   44.92    3.84
  -3  -1   9   35.95    4.79
   3   1  -9   38.16    3.20
  -3  -1   9   39.50    3.74
  -3   1   8   10.57    3.19
  -3  -1   8    7.94    2.95
   3  -1  -8   12.76    2.55
  -3  -1   8   13.96    2.43
   3   1  -8    7.93    1.93
  -3   1   8   11.56    2.13
  -3  -1   7  815.57   21.27
   3  -1  -7  783.73   19.26
   3   1  -7  825.88   18.67
  -3  -1   7  805.97   20.18
  -3   1   7  760.29   19.14
  -3   1   7  771.27   21.10
  -3  -1   6    8.74    1.98
   3   1  -6    6.82    1.66
   3  -1  -6    6.21    2.03
  -3   1   6    8.85    1.56
  -3  -1   6    9.35    2.85
  -3   1   6    8.88    3.07
  -3   1   5  160.67    5.04
  -3   1   5  149.37    7.21
  -3  -1   5  172.35    6.14
   3  -1  -5  155.89    5.95
   3   1  -5  158.57    5.51
  -3  -1   5  157.81    7.17
   3   1  -4  344.81    9.22
  -3   1   4  350.69   10.73
  -3  -1   4  352.14    9.97
   3  -1  -4  352.65    9.77
  -3  -1   4  359.20   10.90
  -3   1   4  352.32    8.67
  -3  -1   3    5.43    1.99
  -3   1   3    4.22    1.29
  -3   1   3    4.00    2.02
  -3  -1   3    8.75    2.01
   3  -1  -3    6.47    1.56
  -3  -1   2  535.81   13.23
  -3   1   2  550.27   13.20
  -3  -1   2  533.96   13.02
   3  -1  -2  529.86   12.97
  -3   1   1   -1.52    0.92
  -3  -1   1   -1.12    0.87
  -3   1   0   11.70    1.71
  -3  -1   0   12.07    1.59
  -3  -1  -1 1445.38   30.24
  -3   1  -1 1418.75   30.39
  -3   1  -2    9.30    1.95
  -3  -1  -2    7.44    1.75
  -3  -1  -2    7.26    1.80
  -3   1  -2    5.77    1.69
  -3  -1  -3  179.48    7.10
  -3  -1  -3  181.74    7.06
  -3   1  -3  171.40    7.15
  -3   1  -3  176.36    7.11
  -3   1  -4   57.59    4.29
  -3   1  -4   65.51    4.61
   3   1   5   23.42    3.38
   3  -1   5   26.69    3.68
   3  -1   6   48.50    4.88
   3   1   6   44.69    4.74
   3  -1   7  195.82    9.69
   3   1   7  198.98    9.82
   3   1   8    1.27    1.74
   3  -1   8    1.09    1.94
   3   1   9   21.88    4.34
   3  -1   9   26.74    4.68
   3  -1  10    0.21    2.25
   3   1  10    5.73    2.87
   3   1  11   79.48    8.35
   3  -1  11   60.40    7.54
   3  -1  12   10.20    3.81
   3   1  12    5.04    3.39
   3   1  13   83.51    9.36
   3  -1  13   83.34    9.58
   3   1  14   -1.01    2.14
   3  -1  14    4.89    3.60
   3  -1  15   13.54    4.40
   3   1  15    7.45    3.85
  -3   2  18   21.04    5.70
  -3  -2  18   16.42    4.98
  -3  -2  17   -0.13    2.77
  -3   2  17    5.79    3.42
  -3   2  16   10.75    4.32
  -3  -2  16   13.99    5.51
  -3  -2  15   32.03    6.86
  -3   2  15   41.37    6.89
  -3  -2  14   40.78    7.08
  -3   2  14   38.35    6.45
  -3   2  13   38.00    6.47
  -3  -2  13   45.56    5.21
  -3  -2  13   37.59    6.67
  -3  -2  12   72.01    5.80
  -3   2  12   79.00    7.49
  -3  -2  12   81.84    8.06
   3  -2 -11   46.72    4.61
  -3  -2  11   36.23    5.61
  -3   2  11   46.45    6.08
  -3  -2  11   52.03    5.12
   3  -2 -10   83.41    5.40
   3   2 -10   84.48    4.29
  -3  -2  10   78.56    5.67
  -3  -2  10   79.13    7.12
  -3   2  10   70.48    6.29
  -3  -2   9  115.49    7.68
  -3  -2   9  114.21    6.34
   3   2  -9  114.81    4.87
  -3   2   9  102.94    6.97
   3  -2  -9  114.83    5.97
   3   2  -8    2.36    1.32
   3  -2  -8    0.65    1.79
  -3   2   8   -0.87    0.93
  -3  -2   8   -1.70    1.49
  -3  -2   8    0.42    2.26
  -3   2   8   -1.87    1.89
  -3  -2   7   34.50    3.41
  -3   2   7   31.95    2.46
  -3   2   7   26.84    3.88
   3   2  -7   28.23    2.42
  -3  -2   7   29.14    3.90
   3  -2  -7   35.22    3.33
  -3  -2   6   53.49    4.72
  -3  -2   6   48.78    3.93
  -3   2   6   52.37    2.69
   3  -2  -6   48.99    3.61
   3   2  -6   53.93    2.93
  -3   2   6   56.91    4.94
  -3   2   5  152.20    4.44
  -3  -2   5  141.66    6.65
  -3  -2   5  142.64    6.26
  -3   2   5  152.69    7.30
   3  -2  -5  156.20    6.13
  -3   2   4   58.04    4.90
  -3  -2   4   57.43    4.68
  -3  -2   4   61.85    4.76
   3  -2  -4   58.38    3.76
   3  -2  -3   33.41    2.75
  -3   2   3   30.41    3.11
  -3  -2   3   34.46    3.36
  -3  -2   3   32.70    3.04
   3  -2  -2    6.18    1.58
  -3  -2   2    8.01    1.72
  -3   2   2    5.52    1.68
  -3  -2   1    7.09    1.56
  -3   2   1    7.86    1.51
  -3  -2   1    7.12    1.37
   3  -2  -1    6.07    1.41
  -3  -2   0  271.16    7.24
  -3   2   0  252.29    7.48
  -3  -2  -1 1792.64   36.92
  -3   2  -1 1796.00   37.37
   3  -2   1 1792.29   39.87
  -3  -2  -2   26.11    2.58
  -3   2  -2   19.20    2.39
   3  -2   2   13.87    2.27
  -3  -2  -2   19.92    2.33
  -3   2  -2   17.07    2.30
  -3   2  -3   16.56    2.68
  -3  -2  -3   16.99    2.52
  -3  -2  -3   16.93    2.47
   3  -2   3   13.52    2.55
  -3   2  -3   17.79    2.77
  -3   2  -4   18.43    2.98
  -3   2  -4   17.80    2.94
   3  -2   4   14.29    2.80
   3  -2   5    2.56    2.03
   3   2   5    4.22    2.12
   3  -2   6   33.44    4.39
   3   2   6   24.21    3.82
   3  -2   7   65.98    5.62
   3   2   7   66.00    5.63
   3   2   8   11.74    3.00
   3  -2   8   12.53    3.67
   3   2   9   30.15    5.06
   3  -2   9   18.09    3.98
   3  -2  10    6.74    3.59
   3   2  10    3.66    2.79
   3  -2  11   39.82    6.57
   3   2  11   51.83    7.10
   3  -2  12   54.71    7.71
   3   2  12   58.91    7.67
   3   2  13    6.16    3.80
   3  -2  13    6.31    3.65
   3   2  14   16.01    5.14
   3  -2  14   20.98    5.45
   3   2  15    1.82    3.01
  -3   2 -16   39.96   12.14
  -3   2 -16   49.86   13.74
  -3  -3  18    5.32    4.04
  -3   3  18    4.33    2.58
  -3   3  17   32.05    6.80
  -3  -3  17   33.54    7.12
  -3  -3  16   -1.68    3.83
  -3   3  16    4.96    3.53
  -3   3  15   13.91    4.35
  -3  -3  15   10.62    5.08
  -3   3  14    2.12    2.85
  -3  -3  14   -0.01    3.54
  -3  -3  14    4.91    2.29
  -3  -3  13  137.68   10.03
  -3  -3  13  150.76    8.73
  -3   3  13  154.08   10.37
  -3   3  12   40.27    6.04
  -3  -3  12   47.29    6.53
  -3  -3  12   39.68    5.09
  -3  -3  11  192.85    9.40
  -3  -3  11  176.46   10.24
  -3   3  11  185.38   10.49
   3  -3 -11  178.86    8.40
  -3  -3  10    1.98    2.63
  -3  -3  10    1.96    1.83
   3  -3 -10   -0.59    2.15
  -3   3  10    1.41    2.59
   3  -3  -9   14.21    3.08
  -3  -3   9   20.98    3.38
  -3  -3   9   15.21    3.79
  -3   3   9   15.01    3.74
  -3  -3   8    1.12    1.63
  -3  -3   8    1.78    2.52
   3  -3  -8   -0.35    1.76
  -3   3   8   -1.25    2.14
  -3   3   7   22.78    3.81
  -3  -3   7   19.71    3.46
   3  -3  -7   27.75    3.24
  -3  -3   7   23.69    3.14
  -3  -3   6  253.41    9.58
   3  -3  -6  247.86    8.63
  -3  -3   6  247.13    9.04
  -3   3   6  248.96    9.52
  -3  -3   5  829.83   21.27
   3  -3  -5  834.73   20.13
  -3  -3   5  817.07   20.47
  -3   3   5  846.27   21.07
  -3  -3   4   20.90    3.08
  -3  -3   4   21.76    3.40
  -3   3   4   21.82    3.25
   3  -3  -4   22.78    2.70
  -3   3   3   15.04    2.57
  -3  -3   3    8.12    2.34
   3  -3  -3   11.27    2.26
  -3  -3   2  269.22    7.82
   3  -3  -2  264.96    8.05
   3  -3  -2  266.37    6.66
  -3  -3   2  271.24    8.73
  -3   3   2  262.74    8.11
  -3  -3   1 1182.17   27.69
  -3   3   1 1201.40   25.66
   3  -3  -1 1185.22   26.35
   3  -3  -1 1209.27   26.12
  -3  -3   1 1205.18   25.04
  -3  -3   0 1044.04   21.74
  -3   3   0 1004.42   22.30
   3  -3   0 1019.43   23.59
   3  -3   1   56.16    3.58
  -3  -3  -1   62.40    3.17
  -3   3  -1   66.56    3.55
  -3  -3  -2  547.20   13.97
  -3  -3  -2  554.18   13.88
  -3   3  -2  549.63   14.29
  -3   3  -2  557.02   14.49
   3  -3   2  555.31   15.46
  -3  -3  -3   35.51    3.28
  -3   3  -3   42.70    3.49
  -3  -3  -3   43.22    3.31
  -3   3  -3   40.18    3.42
   3  -3   3   47.09    4.04
   3  -3   4    1.18    1.55
   3   3   4    1.78    1.70
  -3   3  -4    2.89    1.53
  -3   3  -4    4.10    1.66
   3  -3   5   -0.65    1.40
  -3   3  -5    0.65    1.49
  -3   3  -5    2.19    1.76
   3   3   5   -0.78    1.48
   3  -3   6   43.69    4.99
   3   3   6   40.05    4.54
   3  -3   6   41.03    4.78
   3  -3   7   15.05    3.52
   3  -3   7   20.84    4.02
   3   3   7   14.46    3.34
   3  -3   8    3.03    2.71
   3   3   8    4.31    2.27
   3   3   9   18.32    4.01
   3  -3   9   13.25    3.61
   3   3  10   16.28    4.02
   3  -3  10   24.90    5.09
   3   3  11   32.01    5.86
   3  -3  11   30.72    5.82
   3  -3  12    0.78    2.63
   3   3  12    3.63    2.66
   3  -3  13   35.03    6.77
   3   3  13   32.66    6.46
   3  -3  14    5.98    3.04
   3   3  14    2.02    2.71
   3   3  15   22.57    5.61
  -3   3 -16    1.99    6.40
  -3   3 -16    4.83    7.68
  -3   4  18   27.57    5.93
  -3  -4  18   24.59    6.74
  -3  -4  17   -0.51    3.98
  -3   4  17   -0.35    2.49
  -3  -4  16   15.91    5.62
  -3   4  16    7.58    4.30
  -3   4  15   24.14    5.57
  -3  -4  15   26.11    6.70
  -3  -4  14  169.62   11.61
  -3  -4  14  169.82    9.80
  -3   4  14  171.35   11.32
  -3  -4  13    6.46    4.57
  -3   4  13   17.77    4.63
  -3  -4  13   18.41    3.82
  -3  -4  12  117.47    8.85
   3  -4 -12  109.37    7.17
  -3   4  12  112.62    8.34
  -3  -4  12  122.62    7.81
  -3  -4  11   22.64    4.07
  -3   4  11   24.21    4.71
  -3  -4  11   23.40    5.07
   3  -4 -11   29.06    4.28
  -3  -4  10   34.76    4.43
  -3   4  10   28.95    4.89
   3  -4 -10   31.46    4.12
  -3  -4  10   25.97    4.62
  -3  -4   9   -1.65    2.43
  -3  -4   9   -0.52    1.66
   3  -4  -9   -4.11    1.95
  -3   4   9    0.33    2.26
  -3   4   8   52.67    5.12
  -3  -4   8   45.99    4.54
  -3  -4   8   54.77    5.21
   3  -4  -8   47.28    4.39
  -3   4   7  182.54    8.45
  -3  -4   7  155.19    7.59
  -3  -4   7  161.30    7.74
   3  -4  -7  161.55    7.14
  -3  -4   6  309.85   10.66
   3  -4  -6  313.96   10.25
  -3   4   6  343.56   11.33
  -3  -4   5  236.80    8.86
  -3   4   5  258.84    9.45
   3  -4  -5  249.03    8.64
   3  -4  -4   10.65    2.44
  -3   4   4    5.03    2.81
  -3  -4   4    6.81    2.24
  -3  -4   3   24.97    2.87
  -3  -4   3   22.88    3.77
   3  -4  -3   20.50    2.63
  -3   4   3   24.55    3.25
  -3  -4   2  988.63   21.60
   3  -4  -2  992.37   22.78
   3  -4  -2 1009.08   21.94
  -3  -4   2 1010.84   24.40
  -3   4   2  987.06   22.25
  -3  -4   1   16.33    2.59
  -3  -4   1   15.34    1.79
   3  -4  -1   16.43    1.77
   3  -4  -1   16.30    2.24
  -3   4   1   16.73    1.95
  -3   4   0  429.77   10.97
   3  -4   0  428.74   11.51
  -3  -4   0  412.03   12.36
  -3  -4   0  421.97   10.15
  -3   4  -1    0.32    1.01
  -3  -4  -1    1.21    0.98
   3  -4   1   -0.15    1.38
   3  -4   1   -0.80    1.04
   3  -4   2   18.75    2.80
  -3  -4  -2   18.62    2.20
  -3   4  -2   16.97    2.42
  -3  -4  -2   21.68    2.33
  -3  -4  -3  126.36    5.67
   3  -4   3  123.89    6.35
  -3   4  -3  133.12    6.15
  -3   4  -3  119.84    5.92
  -3  -4  -3  123.92    5.56
  -3   4  -4  123.40    6.30
   3   4   4  130.01    6.19
   3  -4   4  127.22    6.79
  -3   4  -4  130.52    6.52
   3   4   5   58.37    4.57
  -3   4  -5   57.83    4.88
   3  -4   5   58.67    4.92
  -3   4  -5   60.30    4.80
   3   4   6   14.45    3.12
   3  -4   6   12.08    3.20
   3  -4   7   44.83    5.41
   3  -4   7   44.35    5.34
   3   4   7   38.72    4.81
   3  -4   8   93.30    7.32
   3  -4   8   87.61    6.86
   3   4   8   87.48    6.68
   3  -4   9    7.45    3.38
   3   4   9    0.01    2.23
   3  -4   9    5.11    2.84
   3   4  10    7.50    3.22
   3  -4  10    8.23    4.18
   3   4  11    7.68    3.67
   3  -4  11   11.85    4.48
   3   4  12   23.66    5.15
   3  -4  12   13.59    4.92
   3  -4  13   -2.08    2.88
   3   4  13   -0.04    2.51
   3   4  14   26.92    6.36
   3   4  15    2.97    3.02
  -3   4 -15   -3.27    5.73
  -3   4 -15    2.36    6.60
  -3   4 -16   59.26   14.20
  -3   4 -16   60.58   13.73
  -3   5  18    2.29    2.85
  -3  -5  18    5.57    4.46
  -3   5  17   12.49    4.58
  -3  -5  17    9.39    5.04
  -3   5  16   -1.08    2.07
  -3  -5  16   -2.81    3.42
  -3  -5  15   25.79    4.85
  -3  -5  15   29.78    6.59
  -3   5  15   20.17    5.15
  -3  -5  14    6.49    4.45
  -3  -5  14    4.52    2.34
  -3   5  14   13.85    4.34
  -3   5  13  134.92    9.89
  -3  -5  13  154.90    9.08
  -3  -5  13  149.90   10.72
  -3   5  12   -1.92    2.39
  -3  -5  12    2.77    3.59
   3  -5 -12   -1.78    2.92
  -3  -5  12   -1.12    1.55
  -3  -5  11   97.42    7.68
  -3  -5  11   83.70    6.48
  -3   5  11   87.93    7.28
   3  -5 -11   83.85    6.43
  -3  -5  10    2.79    2.51
   3  -5 -10    2.96    2.69
  -3  -5  10    0.69    2.02
  -3   5  10    0.83    2.65
  -3   5   9  114.23    7.46
  -3  -5   9  105.70    7.21
  -3  -5   9   88.29    6.14
   3  -5  -9   98.68    6.11
   3  -5  -8   22.58    3.45
  -3  -5   8   21.68    3.83
  -3   5   8   25.90    4.09
  -3   5   7    9.02    3.13
   3  -5  -7   11.95    2.91
  -3  -5   7    9.48    3.05
   3  -5  -6   17.83    3.00
  -3   5   6   19.98    3.53
  -3  -5   6   13.33    2.84
  -3  -5   5   46.00    3.90
   3  -5  -5   47.31    2.26
  -3  -5   5   39.27    4.45
   3  -5  -5   51.78    3.95
  -3   5   5   43.97    4.57
  -3  -5   4   -0.06    1.95
   3  -5  -4   -3.13    1.76
  -3   5   4    1.53    2.60
  -3  -5   4   -2.47    3.24
  -3  -5   3  491.56   15.20
   3  -5  -3  499.38   11.43
   3  -5  -3  476.76   13.21
  -3  -5   3  494.98   12.67
  -3  -5   2  215.51    8.73
   3  -5  -2  207.84    7.40
  -3  -5   2  212.36    6.66
   3  -5  -2  204.20    6.08
  -3  -5   1  127.92    4.48
   3  -5  -1  129.98    4.91
  -3  -5   1  133.86    6.33
   3  -5  -1  127.07    5.38
  -3  -5   0  243.71    6.46
  -3   5   0  242.45    7.41
   3  -5   0  244.22    7.94
  -3  -5   0  230.93    8.70
  -3  -5  -1  558.19   15.96
  -3  -5  -1  553.00   12.93
   3  -5   1  539.08   13.40
   3  -5   1  567.63   15.28
  -3   5  -1  539.04   13.88
  -3  -5  -2 1186.67   26.01
  -3  -5  -2 1181.03   25.80
   3  -5   2 1192.09   25.66
   3  -5   2 1174.53   28.96
  -3   5  -2 1207.67   27.09
  -3   5  -3   12.33    2.41
   3  -5   3   12.30    2.72
  -3   5  -3   10.44    2.29
  -3  -5  -3   12.23    2.10
  -3  -5  -3    9.39    2.02
  -3   5  -4  365.44   12.05
  -3   5  -4  367.74   12.23
   3  -5   4  354.89   12.67
  -3   5  -5   98.84    6.08
   3  -5   5   88.24    6.16
   3   5   5   68.34    4.71
  -3   5  -5   99.89    5.98
  -3   5  -6  135.79    7.73
  -3   5  -6  131.87    7.49
   3  -5   6  119.91    7.64
   3   5   6  117.62    6.88
   3   5   7   19.59    3.73
   3  -5   7   30.97    4.79
   3  -5   8    1.70    2.00
   3  -5   8    4.54    2.76
   3   5   8    2.51    1.98
   3  -5   9   16.99    3.87
   3   5   9    7.54    3.13
   3  -5   9    8.33    3.35
   3  -5  10   23.00    5.44
   3  -5  10   24.74    5.15
   3   5  10   13.94    4.03
   3   5  11   78.37    8.16
   3  -5  11   85.61    9.00
   3   5  12   10.88    3.89
   3  -5  12    9.41    4.25
   3   5  13   25.27    5.70
   3   5  14    9.19    4.17
  -3   5 -15   37.77    9.95
  -3   5 -15   30.02    9.56
   3   5  15   27.10    6.18
  -3   5 -16   -2.68    4.45
  -3   5 -16    5.13    6.36
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  -3   6  18    6.58    3.61
  -3   6  17    2.85    2.89
  -3  -6  17    4.98    4.93
  -3   6  16   13.57    4.71
  -3  -6  16    7.89    4.48
  -3  -6  15    3.01    3.84
  -3  -6  15    0.93    2.10
  -3   6  15    1.81    2.85
  -3   6  14   96.58    8.48
  -3  -6  14  102.40    7.77
  -3  -6  14   85.39    9.25
  -3  -6  13   97.63    9.19
  -3  -6  13   72.78    6.42
  -3   6  13   89.26    8.60
   3  -6 -12   84.60    6.79
  -3  -6  12   78.42    6.54
  -3   6  12   84.93    7.64
  -3  -6  12  102.69    8.28
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   3  -6 -11   -1.36    2.87
  -3  -6  11   -1.47    3.09
  -3   6  11    1.31    2.74
  -3  -6  10    2.80    0.90
  -3   6  10   -1.09    2.27
   3  -6 -10    2.05    2.88
  -3  -6  10   -2.52    1.98
   3  -6  -9   47.24    4.87
  -3  -6   9   39.69    5.10
  -3   6   9   47.83    5.40
   3  -6  -8   56.22    5.08
  -3   6   8   61.60    5.43
  -3  -6   8   61.52    5.52
   3  -6  -7   44.67    4.30
  -3  -6   7   42.30    4.55
  -3   6   7   41.64    4.75
  -3  -6   7   41.23    4.31
   3  -6  -6    0.31    0.93
  -3  -6   6   -0.83    1.92
   3  -6  -6   -1.37    1.99
  -3   6   6   -0.54    2.43
  -3  -6   6    1.35    2.53
  -3  -6   5  271.42   10.93
  -3  -6   5  271.21    8.99
  -3   6   5  225.50    9.27
   3  -6  -5  260.44    7.13
   3  -6  -5  261.14    9.44
  -3  -6   4  112.29    5.51
   3  -6  -4  112.60    5.88
   3  -6  -4  115.21    4.56
  -3  -6   4  108.88    7.91
  -3  -6   3  138.20    7.85
  -3  -6   3  145.77    5.66
   3  -6  -3  134.18    4.73
   3  -6  -3  135.88    6.13
   3  -6  -2   11.93    1.89
   3  -6  -2   14.21    2.44
  -3  -6   2   15.17    3.32
  -3  -6   2   15.71    2.30
  -3  -6   1  150.59    7.15
   3  -6  -1  140.70    5.92
  -3  -6   1  156.44    4.87
   3  -6  -1  148.01    5.62
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   3  -6   0   13.56    2.21
  -3  -6   0   16.08    1.47
   3  -6   1  500.06   12.86
  -3  -6  -1  499.57   15.04
  -3   6  -1  507.59   13.15
  -3  -6  -1  509.33   11.90
   3  -6   1  504.16   14.45
  -3  -6  -2    0.70    1.13
   3  -6   2   -0.63    1.09
  -3   6  -2    0.39    1.26
  -3  -6  -2    1.52    1.09
   3  -6   2    1.50    1.81
  -3   6  -3  349.15   11.36
  -3   6  -3  358.54   11.40
  -3  -6  -3  353.03   10.31
  -3  -6  -3  346.09   10.35
   3  -6   3  339.48   12.16
  -3   6  -4    0.66    1.41
   3   6   4    2.80    1.66
  -3   6  -4    2.17    1.66
   3  -6   4    4.08    2.32
  -3   6  -5   79.92    5.54
  -3   6  -5   78.88    5.46
   3  -6   5   74.05    5.78
   3  -6   6   56.67    5.42
  -3   6  -6   59.25    5.53
  -3   6  -6   49.91    5.22
   3   6   7   69.11    5.69
  -3   6  -7   61.95    5.39
   3  -6   7   54.08    5.93
  -3   6  -7   57.69    5.91
   3   6   8   18.98    3.88
   3  -6   8   18.58    4.24
   3   6   9   50.52    6.01
   3  -6   9   38.01    5.66
   3  -6   9   55.06    6.72
   3  -6  10  165.35   10.82
   3   6  10  179.81   10.43
   3  -6  10  171.98   11.42
   3  -6  11    8.33    3.63
   3   6  11    6.17    3.19
   3  -6  11   13.29    4.61
   3   6  12   16.85    4.44
   3   6  13   17.03    4.55
  -3   6 -14   71.80   11.51
   3   6  14   63.13    8.55
  -3   6 -14   57.71   11.22
  -3   6 -15   11.66    5.79
   3   6  15   11.22    4.37
  -3   6 -15   12.93    5.87
  -3   6 -16   45.47   11.86
  -3   6 -16   41.46   11.21
  -3  -7  18   -1.41    3.22
  -3   7  18    0.44    3.04
  -3   7  17   -2.71    2.82
  -3  -7  17    3.64    4.02
  -3  -7  16   -1.13    3.12
  -3   7  16    0.59    2.60
  -3  -7  15    1.46    2.06
  -3  -7  15    4.10    3.92
  -3   7  15    4.42    2.90
  -3   7  14   14.14    4.36
  -3  -7  14    5.53    2.65
  -3  -7  14   13.41    5.39
  -3   7  13  106.07    8.57
  -3  -7  13  107.45    9.08
  -3  -7  12   -0.48    0.87
  -3   7  12   13.79    4.25
  -3  -7  12   16.35    4.95
   3  -7 -12    3.54    3.55
  -3  -7  11   10.41    3.90
  -3   7  11    8.85    3.82
   3  -7 -11   13.91    4.00
  -3  -7  10   -2.70    1.55
   3  -7 -10    0.06    2.93
  -3  -7  10   -1.53    2.42
  -3   7  10   -0.51    2.33
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   3  -7  -9   48.17    5.28
  -3   7   9   56.18    5.86
  -3  -7   9   57.62    5.87
   3  -7  -8   19.20    3.89
  -3   7   8   30.99    4.52
  -3  -7   8   30.67    4.36
  -3  -7   8   36.20    4.73
  -3  -7   7  226.64    9.49
   3  -7  -7  223.19    7.30
  -3  -7   7  234.56   10.47
   3  -7  -7  230.93    9.57
  -3   7   7  235.57    9.84
   3  -7  -6  403.63   13.12
  -3  -7   6  394.49   14.37
  -3  -7   6  393.78   12.58
   3  -7  -6  417.67   10.79
  -3  -7   5   65.51    6.18
   3  -7  -5   58.27    4.86
  -3  -7   5   61.53    4.28
   3  -7  -5   64.89    3.64
   3  -7  -4   28.10    3.11
  -3   7   4   24.93    3.25
  -3  -7   4   28.59    4.78
   3  -7  -4   28.55    3.52
  -3  -7   4   29.77    2.98
   3  -7  -3  356.46   11.30
   3  -7  -3  364.48   10.01
  -3   7   3  367.12   11.08
  -3  -7   3  367.09    9.82
  -3  -7   3  376.84   13.58
   3  -7  -2  162.54    6.78
  -3  -7   2  171.19    8.49
   3  -7  -2  169.54    6.14
  -3  -7   2  174.36    5.76
  -3   7   2  175.52    6.53
  -3   7   1   21.42    2.35
   3  -7  -1   24.96    2.67
  -3  -7   1   19.85    1.97
   3  -7  -1   20.59    2.83
  -3  -7   1   20.02    3.59
  -3  -7   0    7.34    1.14
   3  -7   0    6.23    2.10
  -3  -7   0    8.47    2.92
   3  -7   1  291.84   10.12
  -3  -7  -1  293.72   10.81
  -3  -7  -1  293.69    7.64
   3  -7   1  290.01    8.94
   3  -7   2  731.61   17.19
  -3  -7  -2  732.20   16.80
  -3   7  -2  730.34   18.28
   3  -7   2  721.88   20.04
  -3  -7  -2  711.16   20.39
  -3  -7  -2  711.28   16.83
   3  -7   3   29.18    3.75
  -3  -7  -3   33.22    2.96
  -3  -7  -3   34.01    2.91
  -3   7  -3   29.86    3.36
   3  -7   3   23.96    2.21
  -3   7  -3   30.02    3.35
  -3   7  -4   12.43    2.68
   3   7   4   13.00    2.39
   3  -7   4    8.53    3.00
  -3   7  -4   10.17    2.69
   3   7   5  280.67   10.03
   3  -7   5  279.09   11.78
  -3   7  -5  271.40   10.86
  -3   7  -5  263.69   10.58
   3  -7   6   73.81    6.00
  -3   7  -6   76.72    5.82
  -3   7  -6   69.96    5.59
  -3   7  -7   22.38    4.10
  -3   7  -7   21.78    4.07
   3  -7   7   21.69    4.15
   3   7   8   10.80    3.00
  -3   7  -8    9.63    3.00
  -3   7  -8    8.60    3.21
   3  -7   8    7.53    2.97
   3  -7   9   23.80    4.86
   3   7   9   34.77    5.18
   3  -7  10  113.76    8.93
   3   7  10  103.94    7.94
   3  -7  11   40.28    6.56
   3   7  11   30.90    5.65
  -3   7 -12   20.84    5.64
   3  -7  12   17.46    4.94
   3   7  12   18.60    4.69
  -3   7 -13    7.79    4.56
  -3   7 -13    0.26    3.28
   3   7  13   -4.62    1.88
   3   7  14   18.56    4.89
  -3   7 -14    8.99    5.43
  -3   7 -14    4.07    5.68
   3   7  15   34.81    6.78
  -3   7 -15   36.68    9.24
  -3   7 -15   38.21   10.28
  -3   7 -16   15.70    7.33
  -3   7 -16    6.82    7.75
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  -3  -8  17    4.22    4.19
  -3   8  17    1.65    2.72
  -3   8  16   10.62    4.23
  -3  -8  16    1.02    4.01
  -3  -8  16    4.05    2.42
  -3  -8  15    0.02    3.28
  -3  -8  15   -1.47    0.99
  -3   8  15    2.05    2.98
  -3  -8  14   10.69    4.48
  -3   8  14   12.54    3.97
  -3   8  13    1.49    2.85
  -3  -8  13   -0.32    3.37
   3  -8 -13   -1.41    3.15
  -3  -8  13    0.02    1.11
   3  -8 -12   44.08    5.56
  -3  -8  12   41.28    5.62
  -3   8  12   35.71    6.04
  -3  -8  12   48.69    7.02
  -3  -8  11   93.05    7.53
   3  -8 -11  107.09    7.77
  -3  -8  11   96.37    7.44
  -3   8  11  110.77    8.21
  -3  -8  10    0.25    2.59
  -3   8  10    1.58    2.86
   3  -8 -10    2.20    3.44
  -3  -8  10   -0.45    2.16
  -3  -8   9   18.05    4.03
  -3  -8   9   27.38    4.72
   3  -8  -9   29.17    4.75
  -3   8   9   28.26    4.51
  -3  -8   8    2.39    2.78
   3  -8  -8    1.14    1.55
  -3  -8   8   -1.20    2.13
   3  -8  -8   -1.71    2.38
  -3   8   8   -0.46    2.55
  -3  -8   7  120.85    7.89
   3  -8  -7  116.31    5.15
   3  -8  -7  112.37    6.70
  -3  -8   7  114.12    6.49
  -3  -8   6    0.91    2.03
  -3   8   6    2.02    1.17
   3  -8  -6    2.52    2.41
  -3  -8   6    2.83    3.58
   3  -8  -6    4.71    1.89
  -3  -8   5  544.01   17.76
   3  -8  -5  518.59   15.66
  -3  -8   5  551.73   14.55
  -3   8   5  525.71   15.30
   3  -8  -5  529.86   13.81
   3  -8  -4  129.97    5.88
   3  -8  -4  117.14    6.34
  -3   8   4  123.92    6.31
  -3  -8   4  128.47    8.37
  -3  -8   4  121.34    5.34
  -3   8   3    2.48    2.44
   3  -8  -3    3.64    2.21
  -3  -8   3    0.19    1.48
  -3  -8   3   -1.54    3.60
   3  -8  -3    2.51    2.32
   3  -8  -2  121.56    6.10
  -3  -8   2  132.79    8.30
   3  -8  -2  115.37    5.51
  -3   8   2  122.80    5.48
  -3  -8   2  115.49    4.48
  -3   8   1  199.40    6.75
   3  -8  -1  189.55    7.45
  -3  -8   1  187.27    9.05
   3  -8  -1  194.76    7.43
  -3  -8   1  183.44    5.47
  -3  -8   0  102.06    6.80
   3  -8   0   99.95    5.46
  -3  -8   0   98.77    3.37
  -3   8   0  104.92    4.61
  -3  -8  -1    1.46    2.23
  -3  -8  -1    0.33    0.61
   3  -8   1    0.01    1.62
  -3   8  -1    0.23    0.57
   3  -8   1   -0.78    1.60
   3  -8   2    4.96    1.71
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   3  -8   2    3.71    2.05
  -3   8  -2    1.31    0.97
  -3  -8  -2    4.52    1.32
  -3  -8  -2    6.41    1.38
   3  -8   3  686.43   20.53
  -3  -8  -3  695.49   17.10
  -3   8  -3  730.70   18.59
  -3  -8  -3  700.83   17.27
  -3   8  -3  762.75   19.04
  -3  -8  -3  689.83   20.61
   3  -8   3  707.82   16.79
  -3   8  -4  430.07   13.74
  -3   8  -4  434.95   13.65
   3  -8   4  394.22   14.61
   3  -8   5  117.63    7.49
  -3   8  -5  107.39    6.61
  -3   8  -5  101.47    6.39
   3   8   5  114.73    6.02
  -3   8  -6   20.97    3.80
  -3   8  -6   23.85    3.89
   3  -8   6   18.37    3.84
   3   8   6   24.25    3.58
   3  -8   7  120.27    7.99
   3   8   7   88.34    6.18
  -3   8  -7   93.66    6.61
  -3   8  -7  106.04    7.12
   3   8   8    1.39    0.82
  -3   8  -8   10.13    3.12
  -3   8  -8    4.83    2.64
   3  -8   8    4.25    2.61
   3   8   9   11.82    3.61
  -3   8  -9   17.37    4.17
  -3   8  -9   20.40    4.60
   3  -8   9   15.20    4.33
   3  -8  10   10.24    4.06
  -3   8 -10   17.17    5.11
  -3   8 -10   14.39    4.58
   3   8  10   13.78    3.80
   3   8  11    5.19    3.13
  -3   8 -11    3.70    3.42
  -3   8 -11    1.60    2.76
   3  -8  11    2.78    2.73
   3  -8  12    3.73    2.58
  -3   8 -12   -1.56    2.37
  -3   8 -12    4.16    3.75
   3   8  12    1.52    2.48
   3  -8  13   17.39    4.93
   3   8  13   12.49    4.05
  -3   8 -13   11.82    5.14
  -3   8 -13   23.03    6.41
  -3   8 -14   36.34    8.54
   3   8  14   33.73    6.53
  -3   8 -14   37.70    8.57
   3   8  15   -2.04    2.67
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  -3   8 -15    0.57    4.64
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  -3   9  18    0.49    2.50
  -3   9  17    4.70    3.46
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  -3  -9  16    0.66    3.15
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  -3  -9  15    6.31    4.31
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  -3  -9  14   -0.06    3.27
  -3   9  14    3.60    2.66
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  -3   9  13    0.68    2.64
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  -3   9  12    7.12    3.75
   3  -9 -12   11.48    4.33
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  -3  -9  12   11.42    4.66
  -3   9  11   20.87    4.93
   3  -9 -11   22.35    4.76
  -3  -9  11   19.82    4.36
  -3  -9  11   24.79    4.99
  -3   9  10   75.39    7.00
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  -3  -9  10   83.44    6.98
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   3  -9  -9    4.62    2.16
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   3  -9  -9    3.10    3.32
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   3  -9  -8   24.13    3.00
   3  -9  -8   19.92    4.16
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   3  -9  -7   89.36    6.62
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   3  -9  -7   91.88    4.92
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   3  -9  -6   21.74    4.00
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   3  -9  -5   42.82    4.75
   3  -9  -5   49.71    4.25
  -3   9   5   49.18    4.70
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  -3 -28  -7    8.08    5.09
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   3 -29  -9   -6.71    3.94
  -3 -29   8    8.92    6.17
   3 -29  -8   -4.08    3.77
  -3 -29   7    9.03    6.64
   3 -29  -7   -6.72    3.67
  -3 -29   6    7.98    6.83
   3 -29  -6    4.46    4.65
  -3 -29   5    7.37    7.78
   3 -29  -5   -1.70    3.59
  -3 -29   4   31.54   10.59
   3 -29  -4   17.84    5.43
   3 -29  -3    1.27    3.83
  -3 -29   3    1.05    7.85
   3 -29  -2   -2.59    3.97
  -3 -29   2    0.65    3.68
  -3 -29   2    9.17    8.69
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   3 -29  -1    2.66    4.55
  -3 -29   1   -2.74    3.72
   3 -29  -1   11.68    6.39
  -3 -29   0    8.80    5.47
   3 -29   0   12.54    5.96
   3 -29   0    4.26    4.55
  -3 -29   0    1.02    9.40
   3 -29   1    2.51    6.09
  -3 -29  -1    5.96   10.21
  -3 -29  -1   -1.94    3.03
  -3 -29  -2    6.62   10.80
   3 -29   2   19.71    7.46
  -3 -29  -2   15.93    6.06
   3 -29   3    8.13    5.00
  -3 -29  -3   -5.03   10.38
  -3 -29  -3   -3.99    3.47
  -3 -29  -4    2.42   11.29
   3 -29   4   10.46    5.97
  -3 -29  -4   -0.29    4.43
   3 -29   5   13.03    5.56
  -3 -29  -5    7.31    4.31
  -3 -29  -6   34.70    6.94
   3 -29   6   28.87    8.40
   3 -30  -8    5.02    4.75
  -3 -30   8    6.34    6.30
   3 -30  -7    6.07    4.18
  -3 -30   7   -0.20    5.24
   3 -30  -6   12.54    4.87
  -3 -30   6   16.21    7.65
   3 -30  -5   -3.63    3.45
  -3 -30   5    2.22    7.23
   3 -30  -4    1.12    4.64
  -3 -30   4   17.43    8.92
   3 -30  -3   30.21    7.21
  -3 -30   3   23.18   10.55
  -3 -30   2   10.79    4.80
  -3 -30   2    9.44    9.34
   3 -30  -2    9.71    4.76
  -3 -30   1   -0.55    3.13
   3 -30  -1    6.23    5.09
  -3 -30   1    3.58    9.30
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   3 -30   0   -3.27    3.54
  -3 -30   0   -3.44    8.65
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   3 -30   1   17.86    7.22
  -3 -30  -1   18.26   10.54
  -3 -30  -1    0.38    4.03
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  -3 -30  -2    4.18    9.74
   3 -30   2   -0.92    4.85
  -3 -30  -3   12.53    5.11
  -3 -30  -3   10.28   10.72
   3 -30   3   14.03    6.60
   3 -30   4   17.70    7.18
  -3 -30  -4   18.58    5.34
   3 -30   5   41.57    8.54
  -3 -30  -5   34.59    7.34
  -3 -31   6    3.09    6.78
   3 -31  -6    0.65    3.56
   3 -31  -5   10.53    5.35
  -3 -31   5    8.87    6.84
   3 -31  -4    1.68    5.02
  -3 -31   4    8.33    8.17
   3 -31  -3    3.18    4.76
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   3 -31  -2    0.78    4.44
  -3 -31   2   -4.83    3.33
  -3 -31   2    7.29    8.53
  -3 -31   1    6.61    9.35
  -3 -31   1    4.47    4.23
   3 -31  -1    5.08    5.01
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  -3 -31   0   -9.40    8.76
  -3 -31   0   -4.54    3.59
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  -3 -31  -1    5.54    4.24
  -3 -31  -1    0.42    9.53
  -3 -31  -2   -1.81   10.26
   3 -31   2    6.10    5.38
  -3 -31  -2    5.00    4.10
   3 -31   3    0.91    4.85
  -3 -31  -3   -4.20   10.41
  -3 -31  -3    8.59    3.81
  -3 -31  -4    5.68    3.88
   3 -31   4   16.23    7.56
   3 -32  -4    6.33    4.61
  -3 -32   4   16.27    7.74
  -3 -32   3   15.51    8.77
   3 -32  -3    0.98    4.62
  -3 -32   2   25.04    9.36
   3 -32  -1    5.92    4.48
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  -3 -32   1   13.45    9.81
  -3 -32   0   -5.19    3.10
  -3 -32   0    6.64    9.63
  -3 -32  -1    8.86    4.59
   3 -32   1   11.02    6.44
  -3 -32  -1    1.76    9.33
   3 -32   2   17.40    5.82
  -3 -32  -2   11.16    4.27
  -3 -32  -2   -2.27    9.23
  -4   0  19    7.47    3.49
  -4   0  18    9.05    4.19
  -4   0  17    2.25    2.66
  -4   0  16   49.70    7.89
  -4   0  15    4.21    3.21
  -4   0  14   55.05    7.44
  -4   0  13   -0.86    2.97
  -4   0  12   32.06    5.65
  -4   0  12   41.94    3.99
  -4   0  11    0.44    3.02
   4   0 -11    0.86    2.06
  -4   0  11    2.98    1.55
  -4   0  10  127.35    6.29
  -4   0  10  100.44    7.39
   4   0 -10  124.32    6.07
  -4   0   9    0.94    2.46
  -4   0   9   -1.90    1.14
   4   0  -9   -1.20    1.71
  -4   0   8  234.15   10.22
   4   0  -8  217.00    8.06
  -4   0   8  226.65    7.97
   4   0  -7    0.63    1.46
  -4   0   7   -0.78    2.27
  -4   0   7    0.21    1.18
   4   0  -6    4.39    1.70
  -4   0   6    7.15    3.10
  -4   0   6    3.72    1.58
  -4   0   5    1.69    2.98
  -4   0   5    0.11    1.95
   4   0  -5   -0.63    1.31
   4   0  -4  281.30    8.61
  -4   0   4  280.00    9.63
  -4   0   4  294.54    8.53
  -4   0   3   -0.43    1.21
  -4   0   3    1.34    2.36
  -4   0   2 5323.80  104.30
  -4   0   1    0.77    1.36
  -4   0   0 4732.01   92.92
  -4   0  -1    1.21    1.14
  -4   0  -2  630.58   16.41
  -4   0  -3    0.58    1.52
  -4   0  -3   -0.75    1.36
  -4   0  -4  177.48    7.92
  -4   0  -4  179.30    8.00
  -4   0  -5    2.76    2.16
  -4   0  -5   -0.27    1.84
  -4   0  -6   15.13    3.34
  -4   0  -6   12.83    3.32
  -4   0  -7    1.44    2.04
  -4   0  -7    0.45    1.80
  -4   0 -12    2.54    3.76
  -4   0 -12   -0.12    3.77
  -4   0 -13    5.39    5.13
  -4   0 -13   -3.82    3.49
  -4   0 -14    6.42    6.78
  -4   0 -14    3.27    5.53
  -4   0 -15    1.26    5.95
  -4   0 -15    3.60    5.29
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  -4  -1  19   25.12    5.26
  -4  -1  18    2.31    2.67
  -4   1  18    0.21    2.27
  -4   1  17   12.91    4.70
  -4  -1  17   21.83    5.80
  -4  -1  16    6.33    3.60
  -4   1  16   10.88    4.31
  -4   1  15   13.88    4.61
  -4  -1  15    7.95    3.63
  -4  -1  14    2.26    3.61
  -4   1  14   -1.96    2.18
  -4  -1  13  262.65   13.54
  -4   1  13  267.35   13.69
  -4  -1  12   33.77    4.28
  -4  -1  12   37.28    6.24
  -4   1  12   27.63    5.42
  -4   1  11   25.24    5.02
  -4  -1  11   40.94    5.94
  -4   1  11   32.49    3.70
   4  -1 -11   41.08    4.27
  -4  -1  11   35.94    4.01
   4  -1 -10   50.46    4.33
  -4   1  10   42.38    5.40
  -4  -1  10   50.36    4.26
   4   1 -10   49.38    4.05
  -4  -1  10   41.03    5.48
  -4   1  10   47.82    3.85
  -4  -1   9    4.65    2.90
   4  -1  -9    5.21    2.20
  -4   1   9    4.39    1.64
  -4   1   9    4.49    2.87
  -4  -1   9    4.16    1.90
   4   1  -9    2.75    1.76
   4   1  -8   68.98    4.16
  -4   1   8   76.54    4.07
   4  -1  -8   74.01    4.70
  -4  -1   8   73.59    4.40
  -4   1   8   67.77    5.74
  -4  -1   8   71.32    6.17
   4  -1  -7  113.70    5.61
   4   1  -7  111.31    5.08
  -4   1   7  108.52    6.65
  -4  -1   7  110.86    5.19
  -4   1   7  114.06    4.58
  -4  -1   7  108.96    6.69
  -4   1   6  178.93    8.50
  -4  -1   6  180.03    6.77
  -4  -1   6  187.57    8.32
   4  -1  -6  175.00    6.91
  -4   1   6  187.03    5.77
   4   1  -6  168.35    6.34
   4  -1  -5  339.57   10.19
  -4   1   5  340.98    8.84
  -4  -1   5  343.51   10.32
  -4  -1   5  342.76   11.39
  -4   1   5  326.46   11.29
   4  -1  -4  430.74   11.81
  -4  -1   4  429.04   12.08
  -4   1   4  429.30   10.85
  -4   1   4  439.69   12.91
  -4  -1   4  425.58   12.56
  -4  -1   3  594.36   15.23
   4  -1  -3  578.59   14.86
  -4   1   3  593.98   13.97
  -4   1   3  593.05   15.44
  -4  -1   3  591.23   14.96
  -4  -1   2 1657.45   38.94
  -4   1   2 1848.86   37.63
  -4  -1   2 1833.65   37.36
  -4  -1   1 3657.35   72.20
  -4   1   1 3621.06   72.42
  -4   1   0   60.05    3.51
  -4  -1   0   74.64    3.80
  -4   1  -1  457.16   12.45
  -4  -1  -1  466.76   12.32
  -4   1  -2   11.37    2.21
  -4  -1  -2   11.36    2.17
  -4   1  -3   31.83    3.57
  -4   1  -3   38.78    3.84
  -4  -1  -3   31.96    3.53
  -4  -1  -3   35.05    3.56
  -4  -1  -4   40.09    4.18
  -4   1  -4   43.61    4.23
  -4  -1  -4   36.32    4.01
  -4   1  -4   38.48    4.19
  -4  -1  -5   19.89    3.44
  -4  -1  -5   21.69    3.59
  -4   1  -5   19.58    3.45
  -4   1  -5   17.38    3.38
  -4   1  -6    4.26    2.45
  -4  -1  -6   10.03    2.91
  -4  -1  -6    9.37    3.02
  -4   1  -6    9.32    2.86
  -4  -1  -7   13.62    3.39
  -4   1  -7    9.71    3.23
  -4  -1  -7    9.53    3.07
  -4   1  -7   12.54    3.37
  -4   1  -8   -3.17    1.73
  -4   1  -8   -0.44    1.94
  -4   1  -9   13.75    4.19
  -4   1  -9   12.04    3.80
  -4   1 -11   73.14    9.17
  -4   1 -11   64.53    8.93
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  -4   1 -12    5.45    4.81
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  -4  -1 -14   16.75    7.57
  -4   1 -14   14.88    6.74
  -4  -1 -14   16.85    7.23
  -4   1 -15    6.17    5.72
  -4  -1 -15   -0.32    6.88
  -4   1 -15    9.72    6.86
  -4  -1 -15   -7.44    4.49
  -4  -2  19    6.37    3.69
  -4   2  19   -1.11    2.19
  -4  -2  18   10.38    5.08
  -4   2  18   11.94    4.17
  -4  -2  17    3.45    3.98
  -4   2  17    8.88    3.60
  -4  -2  16   28.92    6.75
  -4   2  16   26.64    6.01
  -4  -2  15    6.34    4.20
  -4   2  15    8.60    3.66
  -4  -2  14  126.06    9.85
  -4   2  14  127.77    9.70
  -4   2  13   16.30    4.74
  -4  -2  13    8.42    4.41
  -4  -2  13   13.20    3.39
  -4  -2  12   44.65    4.86
  -4  -2  12   34.66    6.12
  -4   2  12   43.29    6.26
  -4  -2  11   13.46    4.41
  -4  -2  11   13.17    3.08
  -4   2  11    9.94    3.82
   4  -2 -11   14.36    3.31
  -4  -2  10   62.48    4.71
   4  -2 -10   66.46    5.03
  -4   2  10   64.86    4.12
  -4   2  10   68.71    6.51
  -4  -2  10   67.47    6.55
   4   2 -10   63.64    4.01
  -4   2   9   14.05    3.74
  -4  -2   9   13.27    2.77
   4  -2  -9   13.87    3.09
  -4  -2   9   16.49    3.91
  -4   2   9   15.99    2.16
   4   2  -9   15.32    2.24
  -4  -2   8   78.40    4.80
  -4  -2   8   70.19    6.13
  -4   2   8   74.57    3.71
   4   2  -8   68.27    3.85
  -4   2   8   66.10    5.74
   4  -2  -8   67.26    4.79
  -4   2   7   48.27    5.04
  -4  -2   7   43.14    4.64
  -4   2   7   46.59    2.58
  -4  -2   7   43.58    3.73
   4  -2  -7   48.57    3.89
  -4  -2   6    8.95    2.45
   4  -2  -6    6.81    2.25
  -4   2   6    7.84    3.03
  -4  -2   6    7.70    3.06
  -4   2   6    8.77    1.18
   4  -2  -5    3.08    1.92
  -4   2   5    1.07    0.87
  -4  -2   5   -0.44    2.61
  -4  -2   5   -0.76    2.78
  -4   2   5    3.48    3.14
  -4  -2   4   31.83    3.80
  -4   2   4   27.39    3.60
  -4  -2   4   29.77    3.63
   4  -2  -4   28.62    3.02
  -4   2   3 1005.69   23.67
  -4  -2   3 1050.62   24.45
   4  -2  -3  999.47   23.45
  -4  -2   3 1049.03   23.60
  -4  -2   2  620.13   15.26
  -4   2   2  641.23   15.80
   4  -2  -2  614.72   15.50
  -4  -2   1  565.76   13.84
  -4   2   1  572.88   14.33
  -4  -2   0 1777.62   36.90
  -4   2   0 1772.56   37.35
  -4  -2  -1  395.76   10.91
  -4   2  -1  403.37   11.34
  -4  -2  -2  142.12    5.95
  -4   2  -2  130.72    6.00
  -4   2  -3  141.10    6.65
  -4  -2  -3  141.41    6.60
  -4  -2  -3  133.14    6.40
  -4   2  -3  139.46    6.71
  -4  -2  -4   32.54    3.76
  -4  -2  -4   32.46    3.81
  -4   2  -4   30.06    3.78
  -4   2  -4   33.75    3.90
  -4   2  -5   21.00    3.73
  -4   2  -5   17.23    3.35
  -4  -2  -5   19.94    3.43
  -4  -2  -5   22.49    3.53
  -4  -2  -6   -1.09    1.94
  -4   2  -6    5.16    2.41
  -4   2  -6    0.29    1.85
  -4  -2  -6    2.14    2.15
  -4   2  -7   43.87    5.47
  -4   2  -7   42.90    5.46
  -4   2  -8   66.48    7.05
  -4   2  -8   93.64    7.30
  -4   2  -9   -0.58    2.55
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  -4   2 -10   70.73    8.32
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  -4   2 -11   16.80    5.47
  -4   2 -12    6.43    4.55
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  -4   2 -13    7.54    5.55
  -4  -2 -13   23.80    7.09
  -4   2 -13    1.93    4.63
  -4   2 -14   -6.17    4.73
  -4   2 -14    9.38    5.71
  -4  -2 -14    7.86    6.37
  -4  -2 -14   -1.61    4.27
  -4   2 -15   17.40    7.06
  -4   2 -15   20.84    8.36
  -4  -2 -15   12.89    6.46
  -4  -2 -15   18.64    9.17
  -4   3  19    9.85    3.41
  -4  -3  19    6.28    4.26
  -4  -3  18    0.57    4.02
  -4   3  18   -3.31    2.44
  -4   3  17   15.89    4.90
  -4  -3  17   16.29    5.82
  -4  -3  16   13.66    5.12
  -4   3  16    7.09    4.03
  -4   3  15   44.47    6.89
  -4  -3  15   39.59    7.19
  -4  -3  14   15.64    4.97
  -4   3  14   19.08    4.75
  -4  -3  13  104.38    7.00
  -4   3  13  114.76    9.26
  -4  -3  13   91.98    8.85
  -4  -3  12   23.11    5.34
  -4  -3  12   24.94    4.02
   4  -3 -12   12.48    3.51
  -4   3  12   20.31    5.07
  -4  -3  11   51.44    4.80
  -4  -3  11   57.11    6.85
   4  -3 -11   54.74    5.21
  -4   3  11   55.79    6.37
  -4   3  10   -0.46    2.68
  -4  -3  10    2.76    1.99
   4  -3 -10    5.60    2.84
  -4  -3  10    1.51    3.06
  -4  -3   9  183.66    8.24
  -4   3   9  182.46    9.44
   4  -3  -9  172.14    7.95
  -4  -3   9  178.29    9.18
  -4  -3   8    0.96    2.59
  -4   3   8    1.97    3.03
  -4  -3   8   -0.68    1.64
   4  -3  -8    4.93    2.40
  -4   3   7  154.90    8.24
   4  -3  -7  164.05    7.21
  -4  -3   7  167.44    8.07
  -4  -3   7  160.31    7.34
  -4  -3   6    5.01    2.82
  -4  -3   6    6.59    2.71
  -4   3   6    7.79    3.29
   4  -3  -6    6.00    2.25
  -4   3   5  488.03   14.44
   4  -3  -5  472.19   13.54
  -4  -3   5  494.07   14.31
  -4  -3   5  469.00   14.52
   4  -3  -4    0.39    1.65
  -4  -3   4    0.03    2.97
  -4   3   4    1.60    2.56
  -4  -3   4    3.15    2.41
   4  -3  -3 1878.81   40.59
  -4  -3   3 1895.14   39.68
  -4   3   3 1886.01   40.14
  -4  -3   2 1433.91   30.24
  -4   3   2 1422.23   30.89
  -4  -3   2 1418.44   32.72
   4  -3  -2 1374.69   30.91
  -4  -3   1 2049.12   41.79
   4  -3  -1 2028.04   43.03
  -4   3   1 2024.84   42.46
  -4  -3   1 2067.64   45.68
  -4   3   0  990.34   22.39
  -4  -3   0  968.90   21.63
   4  -3   1  295.19    9.85
  -4   3  -1  292.68    9.27
  -4  -3  -1  301.54    8.78
  -4   3  -2   16.63    2.66
   4  -3   2   16.26    2.83
  -4  -3  -2   15.61    2.30
   4  -3   3    4.03    1.99
  -4  -3  -3    6.13    1.99
  -4   3  -3    6.51    1.94
  -4  -3  -3    8.73    2.13
  -4   3  -3    3.37    1.56
  -4  -3  -4  115.72    6.26
  -4   3  -4  116.01    6.57
  -4  -3  -4  109.67    6.04
  -4   3  -4  116.77    6.47
   4  -3   4  117.69    6.72
  -4   3  -5   13.81    3.03
  -4  -3  -5   13.44    2.92
  -4   3  -5   12.97    2.98
  -4  -3  -5   15.14    3.10
  -4  -3  -6   22.62    3.96
  -4  -3  -6   17.90    3.56
  -4   3  -6   26.07    4.15
  -4   3  -6   20.45    3.87
  -4   3  -7   30.99    4.76
  -4   3  -7   37.30    5.21
  -4   3  -8    3.27    2.50
  -4   3  -8    1.08    2.25
  -4   3  -9   53.20    7.00
  -4   3  -9   59.94    7.18
   4   3   9   56.72    6.65
  -4   3 -10  196.70   12.28
  -4   3 -10  197.87   12.50
   4   3  10  206.45   11.94
  -4   3 -11   18.29    5.41
  -4   3 -11   14.33    4.73
  -4   3 -12   -4.64    2.64
  -4   3 -12   -2.57    3.31
  -4   3 -13    0.76    4.39
  -4  -3 -13   13.21    6.21
  -4  -3 -13   -0.89    3.80
  -4   3 -13   -0.80    4.86
  -4   3 -14   14.22    6.89
  -4   3 -14   13.51    6.23
  -4  -3 -14   20.10    7.51
  -4  -3 -14   17.44    6.65
  -4   3 -15    8.50    6.23
  -4  -3 -15   17.94    7.56
  -4   3 -15   -2.17    5.84
  -4  -3 -15    8.22    7.72
  -4  -4  19    0.87    3.98
  -4   4  19    8.53    3.42
  -4  -4  18    3.70    4.21
  -4   4  18   14.20    4.39
  -4   4  17    2.07    3.09
  -4  -4  17   -0.89    3.72
  -4   4  16   12.60    4.40
  -4  -4  16    5.81    4.43
  -4  -4  15    5.96    4.50
  -4   4  15   -0.84    2.05
  -4   4  14   52.16    7.17
  -4  -4  14   79.75    8.71
  -4  -4  14   67.89    5.90
  -4  -4  13   34.45    6.24
  -4  -4  13   22.92    4.09
  -4   4  13   31.45    6.08
  -4  -4  12  230.95   10.74
  -4  -4  12  211.84   11.62
  -4   4  12  204.09   11.41
   4  -4 -12  203.13    9.66
   4  -4 -11   -2.35    2.42
  -4  -4  11    0.06    2.00
  -4   4  11   -1.63    2.83
  -4  -4  11    0.40    3.13
   4  -4 -10  240.86   10.01
  -4  -4  10  250.82   10.52
  -4   4  10  254.44   11.73
  -4  -4  10  266.22   12.00
   4  -4  -9   94.92    6.18
  -4  -4   9   90.96    5.95
  -4  -4   9   98.96    6.94
  -4   4   9   95.29    6.99
  -4  -4   8   -2.65    1.84
  -4   4   8    0.22    2.74
   4  -4  -8    0.70    2.26
  -4  -4   8   -1.21    2.16
  -4  -4   7   49.49    4.95
  -4   4   7   53.81    5.17
  -4  -4   7   48.11    4.58
   4  -4  -7   51.70    4.43
  -4  -4   6   92.08    6.26
   4  -4  -6   97.54    5.51
  -4  -4   6   92.68    5.79
  -4   4   6   86.32    6.43
   4  -4  -5   10.91    2.73
  -4  -4   5   18.61    3.95
  -4  -4   5   14.51    2.99
  -4   4   5   12.04    3.26
  -4  -4   4  885.39   21.54
  -4   4   4  891.79   22.07
   4  -4  -4  928.77   22.18
   4  -4  -3   33.72    3.44
  -4  -4   3   33.20    3.46
  -4  -4   3   40.12    4.14
  -4   4   3   33.45    3.69
   4  -4  -2  585.64   15.01
  -4  -4   2  565.42   15.95
   4  -4  -2  566.26   13.63
  -4  -4   2  555.07   13.99
  -4   4   2  572.25   14.78
   4  -4  -1  148.16    6.04
  -4  -4   1  155.10    6.96
   4  -4  -1  161.61    5.67
  -4  -4   1  148.16    5.48
  -4   4   1  165.11    6.26
  -4  -4   0   72.81    3.53
  -4   4   0   61.76    3.71
   4  -4   0   60.30    3.83
  -4  -4  -1   36.55    2.74
  -4   4  -1   42.14    3.35
   4  -4   1   43.81    3.51
   4  -4   2   15.77    2.84
  -4   4  -2   17.87    2.63
  -4  -4  -2   17.31    2.33
  -4  -4  -3    0.34    1.29
  -4  -4  -3    0.05    1.25
  -4   4  -3    0.33    1.12
  -4   4  -3   -0.58    0.97
   4  -4   3   -0.56    1.32
  -4  -4  -4   44.86    4.16
  -4  -4  -4   36.89    3.91
   4  -4   4   53.29    4.70
  -4   4  -4   41.77    4.34
  -4   4  -4   42.52    4.43
  -4  -4  -5   42.76    4.42
   4  -4   5   54.67    5.52
  -4   4  -5   48.65    5.03
  -4  -4  -5   51.48    4.56
  -4   4  -5   52.51    5.15
  -4   4  -6   37.49    4.89
  -4  -4  -6   38.37    4.76
   4  -4   6   42.19    5.22
  -4   4  -6   29.39    4.50
  -4  -4  -6   33.63    4.61
  -4   4  -7   93.06    6.79
  -4   4  -7   93.81    6.93
   4  -4   7  105.26    7.40
  -4   4  -8    5.63    2.18
  -4   4  -8    7.91    2.76
  -4   4  -9   16.86    4.52
  -4   4  -9   22.42    4.74
   4   4   9   19.80    4.11
  -4   4 -10   38.79    6.71
   4   4  10   60.67    7.34
  -4   4 -10   43.69    7.00
  -4   4 -11    4.04    3.52
  -4   4 -11    9.92    4.28
  -4   4 -12    1.66    3.92
  -4   4 -12    8.01    4.91
  -4  -4 -13   15.11    6.21
  -4   4 -13   10.65    5.53
  -4  -4 -13   19.72    6.74
  -4   4 -13   17.65    7.07
  -4   4 -14    8.42    5.46
  -4  -4 -14   15.34    6.32
  -4  -4 -14    3.31    5.61
  -4   4 -14    2.86    5.62
  -4   4 -15    2.67    5.60
  -4  -4 -15    1.31    5.32
  -4   4 -15   -6.47    3.72
  -4  -4 -15   -1.14    6.48
  -4  -5  18   -0.81    3.38
  -4   5  18    4.87    3.42
  -4   5  17    3.82    3.03
  -4  -5  17    5.12    4.82
  -4   5  16    5.08    3.68
  -4  -5  16    1.99    4.33
  -4  -5  15   30.14    6.45
  -4   5  15   32.25    6.02
  -4  -5  14   -0.85    3.50
  -4  -5  14    3.83    2.13
  -4   5  14    4.63    3.41
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  -4  -5  13   12.10    4.77
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   4  -5 -12    2.77    3.32
  -4   5  12    6.18    3.36
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  -4  -5  11  117.28    7.43
  -4  -5  11  133.05    9.33
   4  -5 -11  115.14    7.52
  -4   5  11  133.07    8.99
   4  -5 -10    0.55    2.63
  -4  -5  10   -1.84    1.91
  -4  -5  10    0.19    3.02
  -4   5  10    0.09    2.80
  -4   5   9  260.28   11.50
  -4  -5   9  267.67   11.52
   4  -5  -9  254.65   10.37
  -4  -5   9  274.98   11.04
   4  -5  -8   16.40    3.36
  -4   5   8   18.80    4.19
  -4  -5   8   14.57    3.67
  -4  -5   8   10.50    3.07
  -4   5   7   18.04    3.90
   4  -5  -7   22.92    3.55
  -4  -5   7   23.42    3.73
  -4  -5   7   24.89    3.90
  -4  -5   6    1.37    2.16
  -4   5   6    2.50    2.93
   4  -5  -6    1.80    2.28
  -4  -5   6    3.89    1.91
  -4  -5   5  111.83    6.18
   4  -5  -5  110.82    5.99
  -4   5   5  107.90    6.85
  -4   5   4   20.75    3.50
  -4  -5   4   23.85    3.46
  -4  -5   4   27.63    4.50
   4  -5  -4   23.14    3.14
  -4  -5   3  589.05   14.83
   4  -5  -3  585.55   13.48
  -4  -5   3  593.98   17.15
  -4   5   3  573.88   15.59
   4  -5  -3  592.23   15.76
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   4  -5  -2   -0.16    0.89
   4  -5  -2    1.76    1.74
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   4  -5  -1   94.01    4.34
   4  -5  -1   94.46    4.83
  -4  -5   1  102.84    4.31
  -4  -5   1   94.27    5.61
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   4  -5   0   12.84    2.15
  -4  -5   0   13.16    1.73
  -4  -5   0   14.32    2.96
   4  -5   1  360.86   11.52
   4  -5   1  364.71   10.28
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  -4   5  -1  367.37   10.91
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  -4   5  -5  269.17   10.96
  -4  -5  -5  252.52   10.04
   4  -5   5  271.09   11.61
   4  -5   6  202.08   10.30
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  -4   5 -13    6.58    4.38
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  -4  -5 -14    6.07    5.14
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  -4  -6  16   17.28    5.86
  -4   6  16   19.94    5.25
  -4   6  15    4.31    3.35
  -4  -6  15   11.98    5.04
  -4   6  14   32.73    5.96
  -4  -6  14   27.34    4.61
  -4  -6  14   31.24    6.38
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   4  -6 -13   28.53    4.93
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  -4   6  12  106.79    8.32
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  -4   6   8   15.39    3.76
  -4  -6   8    8.19    2.26
  -4  -6   8   18.29    3.68
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  -4   6   7    6.84    3.27
   4  -6  -7    3.53    2.44
   4  -6  -6  126.50    6.58
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  -4   6   6  126.94    7.46
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   4  -6  -5  224.57    8.90
  -4  -6   5  215.55    8.28
  -4   6   5  230.84    9.41
  -4  -6   4 1169.44   26.05
  -4   6   4 1122.08   26.70
   4  -6  -4 1149.95   24.65
   4  -6  -4 1143.35   27.18
  -4  -6   4 1088.44   29.36
  -4  -6   3   38.15    3.43
   4  -6  -3   35.18    2.15
  -4   6   3   34.32    3.77
   4  -6  -3   32.68    3.45
  -4  -6   3   38.64    4.47
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  -4  -6   2   19.36    3.59
   4  -6  -2   22.21    2.14
   4  -6  -2   30.48    3.29
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   4  -6  -1   76.47    4.56
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   4  -6  -1   74.34    4.08
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  -4  -6 -15   11.17    7.51
  -4   6 -15    9.82    5.22
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  -4   7  15   13.99    4.26
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  -4   7  14    6.50    3.46
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   4  -7 -11   62.37    6.11
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   4  -7 -10   49.15    5.54
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   4  -7  -2   78.33    4.81
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   4  -7  -1  186.04    6.96
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   4 -14 -14    0.59    4.13
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   4 -14 -12   47.19    7.21
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   4 -14 -11   11.46    5.26
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   4 -14 -10  127.41   10.00
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   4 -14  -8    4.06    3.87
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   4 -14  -7   22.10    5.36
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  -4 -14   6   88.44    9.39
   4 -14  -6  105.74    7.94
   4 -14  -6  102.38    7.76
  -4 -14   6  100.66    5.68
  -4  14   6  114.19    7.69
   4 -14  -5   43.53    5.24
  -4  14   5   49.92    5.30
   4 -14  -5   44.50    5.64
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   4 -14  -4    6.20    3.15
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   4 -14  -2  115.86    7.37
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   4 -28  -5   12.56    5.49
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   5   0  -9    2.82    2.08
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   5   0  -8  769.33   19.95
  -5   0   8  775.85   22.18
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  -5   0   7    2.22    2.85
   5   0  -7   -0.42    1.50
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   6   0  -9    1.99    1.88
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   6   0  -8  320.18   10.99
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   6 -11  -5  213.24    7.00
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   6 -11  -4  175.27    8.92
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   6 -11  -3  401.05   12.36
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   6 -15  -4   27.98    3.93
   6 -15  -4   25.06    4.80
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   6 -15  -3    2.07    2.60
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   6 -15  -3    6.41    3.40
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   6 -15  -2   28.29    4.74
   6 -15  -2   32.00    4.38
   6 -15  -1   14.66    3.93
   6 -15  -1   19.38    4.10
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   6 -15   0   49.11    5.71
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   6 -15   2   30.47    4.32
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   6 -15   3    5.62    2.71
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   7  -1  -7  427.42   13.89
  -7   1   7  424.90   12.26
  -7  -1   7  440.47   15.57
  -7  -1   7  425.16   13.64
  -7   1   7  429.89   15.27
  -7   1   6   38.73    5.43
  -7  -1   6   40.59    4.24
  -7   1   6   36.33    3.51
  -7  -1   6   35.80    5.17
  -7   1   5   47.35    3.58
  -7  -1   5   54.98    5.68
  -7   1   5   39.77    4.80
  -7  -1   5   44.70    4.02
  -7   1   4  289.78    9.37
  -7  -1   4  286.75   10.00
  -7  -1   4  285.49   10.82
  -7   1   4  284.50   11.07
  -7   1   3  268.20   10.33
  -7  -1   3  277.49    9.99
  -7  -1   3  279.45   10.49
  -7  -1   2    1.33    2.02
  -7   1   2    1.42    1.74
  -7   1   1  603.50   16.93
  -7  -1   1  591.89   16.67
  -7  -1   0    9.02    2.45
  -7   1   0    6.84    2.16
  -7   1  -1   50.46    4.32
  -7  -1  -1   59.33    4.67
  -7  -1  -2    6.75    2.38
  -7   1  -2    6.18    2.29
  -7   1  -3   38.22    4.58
  -7  -1  -3   34.89    4.39
  -7   1  -4    2.35    1.99
  -7  -1  -4   -0.51    1.64
  -7  -1  -5  237.39   11.25
  -7   1  -5  236.32   11.36
  -7  -1  -6    8.57    3.26
  -7   1  -6    2.34    2.18
  -7  -1  -7   45.21    6.06
  -7  -1  -7   48.97    6.26
  -7   1  -7   57.82    6.91
  -7  -1  -8    6.36    3.44
  -7   1  -8    8.83    3.87
  -7  -1  -8    7.77    3.74
  -7   1  -8   10.07    4.01
  -7  -1  -9   35.29    6.43
  -7   1  -9   40.43    6.71
  -7  -1  -9   33.98    6.40
  -7   1  -9   37.20    6.47
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  -7  -1 -10    2.55    3.16
  -7   1 -10    2.18    3.35
  -7   1 -10    3.69    3.52
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  -7   1 -11   -3.60    2.93
  -7  -1 -11    7.24    4.12
  -7   1 -11    0.03    2.70
  -7   1 -12   11.30    4.43
  -7  -1 -12    5.45    4.07
  -7   1 -12    5.70    4.68
  -7  -1 -12    6.06    4.52
  -7   1 -13    1.83    3.92
  -7  -1 -13    6.69    4.37
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  -7  -1 -13    3.66    4.73
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  -7   2  18   10.62    4.34
  -7  -2  18    0.65    3.96
  -7  -2  17   -1.72    3.65
  -7   2  17    8.89    3.72
  -7  -2  16    9.97    5.68
  -7   2  16    8.90    4.87
  -7  -2  15   20.96    6.38
  -7   2  15   16.56    4.88
  -7   2  14   40.65    6.90
  -7  -2  14   41.00    7.04
   7  -2 -13    6.54    3.36
  -7  -2  13    7.53    4.90
  -7   2  13    7.12    4.55
  -7   2  12   93.15    8.70
   7  -2 -12   89.48    6.47
  -7  -2  12   73.69    8.05
   7  -2 -11   -0.87    2.32
  -7  -2  11    2.92    1.91
  -7   2  11    0.07    3.06
  -7  -2  11   -0.73    3.89
  -7  -2  10   29.87    3.66
   7  -2 -10   25.93    4.28
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  -7   2  10   17.74    4.87
   7  -2  -9   36.18    4.41
  -7  -2   9   35.95    5.84
  -7   2   9   42.00    6.21
  -7   2   9   34.64    2.30
  -7  -2   9   31.65    3.79
  -7  -2   8   86.86    5.97
  -7   2   8   86.16    7.70
   7  -2  -8   86.98    5.84
  -7   2   8   86.29    3.64
  -7  -2   8   88.88    7.76
  -7  -2   7    4.02    3.51
  -7   2   7    6.37    3.61
  -7   2   7    4.10    2.08
   7  -2  -7    8.44    2.75
  -7  -2   7    1.20    3.64
  -7  -2   6   10.06    3.14
   7  -2  -6    8.45    2.56
  -7   2   6    9.91    2.19
  -7   2   6    5.14    3.34
  -7  -2   6    7.25    3.48
  -7  -2   5  139.83    7.08
  -7   2   5  139.65    7.83
   7  -2  -5  134.62    6.97
  -7  -2   5  124.15    7.43
  -7   2   5  135.24    5.44
  -7   2   4   -0.54    2.33
  -7  -2   4   -0.08    1.74
  -7  -2   4    3.88    2.75
  -7   2   3  382.24   12.96
  -7  -2   3  378.65   12.44
  -7   2   2  339.72   11.64
  -7  -2   2  330.15   11.29
  -7   2   1   13.28    2.87
  -7  -2   1   14.95    2.80
  -7   2   0 1075.93   26.35
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  -7   2  -1   16.01    3.12
  -7  -2  -1   20.46    3.24
  -7  -2  -2   37.62    4.21
  -7   2  -2   32.60    4.27
  -7  -2  -3   27.73    4.12
  -7   2  -3   27.35    4.18
  -7  -2  -4  142.40    8.01
  -7   2  -4  132.48    7.93
  -7   2  -5   16.72    3.82
  -7  -2  -5   15.39    3.53
  -7   2  -6   62.35    6.65
  -7  -2  -6   51.02    6.06
  -7  -2  -7    1.65    2.80
  -7  -2  -7    0.30    2.34
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  -7   2  -8  200.97   11.94
  -7   2  -8  218.95   12.57
  -7  -2  -8  229.76   12.65
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  -7   2 -10   60.16    8.41
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  -7   2 -11    3.91    3.78
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  -7  -2 -11    4.32    3.51
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   7  -3 -13   44.37    5.39
   7  -3 -12   30.58    4.64
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  -7   3   9   83.17    7.50
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   7  -3  -8  208.86    9.40
  -7  -3   8  223.46   10.91
  -7   3   8  219.90   10.99
  -7   3   7   47.81    5.90
  -7   3   7   42.03    2.70
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  -7   3   6   52.75    3.45
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  -7   3   6   50.19    5.86
   7  -3  -6   52.74    5.00
  -7   3   5    8.19    3.25
   7  -3  -5    6.89    2.43
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  -7  -3   5    6.02    2.83
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   7  -4 -10   44.65    5.17
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   7  -4  -7  160.81    8.07
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   7  -4  -6   37.78    4.59
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   7  -4  -5    0.81    1.88
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   7  -4  -4  148.83    7.32
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  -7   6  14    1.00    3.35
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  -7  -6  13    3.95    1.89
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   7  -6 -12   36.54    5.06
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   7  -6 -11   92.56    6.88
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   7  -6 -10    2.99    3.05
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   7  -6  -8    1.82    2.83
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   7  -6  -7  104.96    7.10
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   7  -6  -6   34.97    4.50
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   7  -6  -4  104.20    6.33
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   7  -6  -3  102.18    6.12
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  -7   6   3   91.37    6.17
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   7  -6  -2  349.56   12.17
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   7  -6  -1   48.32    4.22
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   7  -7 -11   -0.89    2.50
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   7  -7 -10    2.89    3.03
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   7  -7  -9   17.98    4.08
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   7  -7  -8  179.40    9.50
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   7  -7  -5  181.98    9.06
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   7  -9 -10    3.40    3.60
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   7  -9  -9    2.21    3.02
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   7  -9  -5    2.65    2.59
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   7  -9  -4    5.37    2.91
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   7  -9  -3   40.82    4.72
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   7  -9  -3   43.77    3.50
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   7  -9   1  425.01   13.60
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   7  -9   5   53.30    6.92
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   7 -10 -14   57.56    7.31
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   7 -10 -13   18.03    5.22
  -7 -10  13   18.14    3.97
  -7 -10  13   23.91    5.97
  -7  10  13   16.94    5.41
  -7 -10  12  122.15    8.99
  -7 -10  12  119.18    9.31
  -7  10  12  141.56   10.27
   7 -10 -12  125.42    9.29
  -7  10  11   90.27    8.42
  -7 -10  11   80.38    7.65
   7 -10 -11   80.84    7.82
   7 -10 -10    6.44    4.01
  -7  10  10   12.59    4.94
  -7 -10  10    1.03    3.14
  -7 -10   9   89.01    9.20
  -7  10   9  101.81    8.80
   7 -10  -9   98.35    7.95
  -7 -10   9   95.01    7.51
  -7 -10   8  100.71    7.33
  -7 -10   8   76.90    9.07
   7 -10  -8   75.21    6.63
  -7  10   8   95.73    8.42
  -7 -10   7  116.85    7.78
  -7 -10   7  117.80   10.21
   7 -10  -7  111.25    7.79
  -7  10   7  145.90    9.15
   7 -10  -6    2.42    2.88
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  -7 -10   6    6.09    5.33
  -7  10   6   -0.60    3.38
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  -7 -10   5    1.48    3.25
  -7 -10   5   -1.23    4.13
   7 -10  -5   -1.26    2.33
   7 -10  -5    0.01    0.93
   7 -10  -4    1.17    1.26
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  -7  10   4    1.55    2.71
   7 -10  -4   -1.55    2.22
  -7 -10   4    4.01    3.81
  -7 -10   3   38.11    5.80
  -7  10   3   30.72    4.41
   7 -10  -3   38.89    4.80
   7 -10  -3   35.92    3.38
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   7 -10  -2    7.32    2.79
   7 -10  -2    5.22    2.08
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   7 -10  -1   93.15    6.02
   7 -10  -1  103.73    6.63
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  -7  10   1  107.97    6.61
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   7 -10   0   49.90    5.01
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   7 -10   1   73.71    5.90
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   7 -10   1   70.03    5.15
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   7 -10   2  381.69   15.02
  -7 -10  -2  376.49   12.29
  -7  10  -2  407.36   14.35
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  -7 -10  -3    4.59    2.24
   7 -10   3    2.66    2.59
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   7 -10   4   69.40    7.17
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   7 -10   5   15.10    4.45
  -7 -10  -5   15.60    3.30
  -7 -10  -6  218.24   10.63
  -7  10  -6  235.49   12.34
   7 -10   6  224.56   13.16
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   7 -10   7    2.59    3.16
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   7 -10   8   27.60    6.21
  -7 -10  -8   23.23    4.69
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  -7  11  16    0.89    2.86
  -7 -11  16   -0.77    3.83
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  -7  11  15   35.33    6.71
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   7 -11 -15   28.48    5.80
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   7 -11 -14   18.39    5.57
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   7 -11 -13   62.43    7.69
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   7 -11 -12   -3.24    3.67
  -7  11  12    1.09    3.80
  -7 -11  11  154.65    9.99
  -7  11  11  188.77   11.12
   7 -11 -11  156.86   10.11
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  -7 -11  10    9.01    3.67
  -7  11  10   21.20    5.53
   7 -11 -10   20.92    5.10
   7 -11  -9   12.30    4.33
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  -7 -11   9    7.77    3.92
  -7 -11   8   23.86    7.01
  -7  11   8   26.53    5.81
   7 -11  -8   31.33    5.59
  -7 -11   8   33.42    4.86
   7 -11  -7  114.93    8.04
  -7  11   7  117.72    8.30
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  -7 -11   7  118.05    7.39
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  -7 -11   6   39.37    4.81
   7 -11  -6   37.67    5.45
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   7 -11  -5   25.29    2.46
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   7 -11  -5   21.95    4.32
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  -7 -11   5   27.72    4.31
  -7 -11   4   10.29    3.31
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   7 -11  -4    8.43    2.01
   7 -11  -4    8.87    3.25
   7 -11  -3    0.94    1.63
   7 -11  -3    2.88    2.46
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   7 -11  -2  121.87    6.48
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  -7 -11   2  132.08    9.66
   7 -11  -2  132.45    7.83
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   7 -11  -1   20.14    3.84
   7 -11  -1   20.71    3.45
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   7 -11   0   -0.99    2.01
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   7 -11   1  159.20    7.94
   7 -11   1  154.18    8.66
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   7 -11   2   31.03    3.88
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   7 -11   3  225.65   11.53
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   7 -11   4   17.86    4.54
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   7 -11   5   24.21    5.55
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   7 -11   7   68.17    8.51
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   7 -11   8   14.54    4.64
   7 -11   9   21.98    5.55
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  -7  12  16   27.14    6.10
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   7 -12 -14   40.28    6.76
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   7 -12 -10   27.45    5.77
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   7 -12  -9   -2.78    2.81
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   7 -12  -8   84.51    7.33
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   7 -12  -7  142.02    9.32
   7 -12  -6   13.97    3.90
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   7 -12  -5    8.35    1.93
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   7 -12  -5    7.16    3.44
   7 -12  -4   10.00    2.40
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   7 -12  -3   28.74    3.47
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   7 -12   5    0.06    2.75
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   7 -12   6  187.94   12.23
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   7 -12   7    7.88    4.16
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   7 -13 -10   71.69    7.85
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   7 -13  -8    5.86    3.74
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   7 -13  -6   88.23    7.33
   7 -13  -5   40.35    5.53
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   7 -13  -5   47.97    3.79
   7 -13  -4   15.13    2.75
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   7 -13  -3   29.08    4.79
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   7 -13  -3   34.60    4.01
   7 -13  -2   25.70    4.58
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   7 -13   1   80.61    6.73
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   7 -13   4   15.63    4.63
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   7 -13   5   83.36    7.99
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   7 -14  -9    6.51    4.38
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   7 -14  -8    1.14    3.62
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  -7  14   8    4.55    4.55
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  -7  14   7   46.13    6.36
   7 -14  -7   55.09    6.79
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   7 -14  -6   31.03    5.33
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   7 -14  -5   48.48    5.91
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   7 -14  -4   -0.27    2.52
   7 -14  -4    0.25    1.94
   7 -14  -3    5.57    2.38
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   7 -14  -3    7.82    3.28
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   7 -14  -2    9.32    3.30
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  -7  14   2    9.14    3.24
   7 -14  -2    6.65    2.70
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   7 -14  -1   48.99    5.20
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   7 -14  -1   54.97    5.76
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   7 -14   0   44.03    4.85
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  -7  14  -1   35.83    4.59
   7 -14   1   49.67    5.78
   7 -14   1   57.06    5.58
   7 -14   2   43.61    5.00
   7 -14   2   37.98    5.76
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  -7  14  -2   30.09    4.29
   7 -14   3    0.68    1.86
  -7 -14  -3    1.73    3.93
   7 -14   3    0.74    2.65
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   7 -14   4   24.14    5.26
  -7  14  -4   29.62    4.76
  -7 -14  -4   29.38    7.12
  -7  14  -5    3.25    2.24
  -7 -14  -5   -1.33    4.90
   7 -14   5    3.39    3.95
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  -7  14  -6   16.68    4.17
   7 -14   6   16.15    5.13
  -7 -14  -7   -0.17    4.37
   7 -14   7    2.50    3.34
  -7  14  -7   -2.10    1.89
   7 -14   8    3.52    3.98
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   7 -14   9    3.80    3.83
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   7 -14  10   12.61    4.13
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   7 -14  11    2.17    2.74
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   7 -15 -16   -0.62    4.49
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   7 -15 -15   -3.64    4.09
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   7 -15 -14   14.95    5.40
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   7 -15 -13    0.52    4.00
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   7 -15 -12   -0.11    4.26
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   7 -15 -11    6.02    4.47
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  -7  15  11   17.33    4.40
  -7 -15  11    5.69    3.76
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   7 -15 -10   88.19    9.19
  -7  15  10   89.09    7.98
  -7 -15  10  104.44   10.64
  -7  15   9   29.38    5.97
  -7 -15   9   22.58    6.84
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   7 -15  -9   31.33    6.40
   7 -15  -8    2.74    3.91
  -7 -15   8    1.56    2.85
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  -7 -15   8    4.76    6.11
   7 -15  -7    3.90    3.78
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  -7 -15   6   47.85    8.94
   7 -15  -6   55.61    6.51
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   7 -15  -5   15.02    4.11
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   7 -15  -4    5.43    3.38
   7 -15  -4    5.28    2.53
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   7 -15  -3    7.41    3.48
  -7  15   3   12.16    3.93
   7 -15  -3   11.63    3.23
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   7 -15  -2   49.73    5.20
   7 -15  -2   49.48    5.62
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  -7  15   2   38.38    5.10
   7 -15  -1    6.14    3.14
   7 -15  -1    2.46    2.59
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  -7  15   1    1.95    2.41
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   7 -15   0   79.45    6.36
   7 -15   0  114.45    7.81
   7 -15   1    3.10    2.85
   7 -15   1   -0.69    2.43
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   7 -15   2   19.92    4.61
  -7  15  -2   11.67    2.75
   7 -15   2   17.06    3.83
  -7 -15  -3    6.67    5.11
  -7  15  -3   10.82    2.92
   7 -15   3   15.27    4.60
   7 -15   4   23.19    5.58
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  -7  15  -4   19.12    3.99
   7 -15   5   36.48    6.85
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   7 -15   6    3.95    3.88
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   7 -15   7   -0.12    3.15
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   7 -15   8   -0.01    3.19
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   7 -15   9    6.96    4.25
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   7 -15  10    1.63    4.05
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   7 -16 -14    8.91    5.50
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   7 -16 -13   25.17    6.67
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   7 -16 -11    4.16    4.40
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   7 -16 -10   10.58    4.84
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   7 -16  -9   60.96    8.22
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   7 -16  -6    0.91    2.88
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   7 -16  -5  137.09    9.20
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   7 -16  -3   18.90    3.64
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   7 -19   7   12.07    5.54
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  -8   0 -11    1.67    2.92
  -8   0 -12   11.82    4.45
  -8   0 -13   10.71    4.06
  -8   1  19    3.95    3.04
  -8  -1  19    6.15    4.59
  -8   1  18    2.68    3.65
  -8  -1  18    1.47    4.25
  -8   1  17   25.49    6.07
  -8  -1  17    9.75    5.95
  -8   1  16    5.55    4.11
  -8  -1  16    5.60    5.43
  -8  -1  15    7.87    4.32
  -8   1  15   11.78    4.40
  -8  -1  14   26.60    6.52
  -8   1  14    7.17    4.12
   8  -1 -13    0.78    2.55
  -8   1  13   -0.63    4.33
  -8  -1  13    1.27    4.42
   8  -1 -12    2.50    2.81
  -8   1  12    2.50    4.23
  -8  -1  12    2.59    4.56
  -8   1  11  289.12   14.15
   8  -1 -11  298.27   12.18
  -8  -1  11  308.76   14.29
  -8  -1  10    6.03    2.28
  -8   1  10   -0.82    4.49
  -8  -1  10   -3.29    3.70
   8  -1 -10    2.90    2.56
   8  -1  -9   67.17    5.55
  -8   1   9   58.41    7.16
  -8  -1   9   56.85    6.91
  -8  -1   9   60.16    5.01
  -8   1   8    3.09    2.46
  -8  -1   8    3.53    4.36
  -8   1   8    3.52    4.05
  -8  -1   8    1.57    3.32
  -8   1   7  205.22   10.48
  -8  -1   7  184.39   10.27
  -8   1   7  203.79    8.04
  -8  -1   7  191.59    8.87
  -8  -1   6  210.16    8.87
  -8   1   6  216.64    8.19
  -8   1   6  198.85   10.26
  -8  -1   6  212.73   10.30
  -8   1   5   95.10    5.18
  -8  -1   5   86.43    7.12
  -8  -1   5   88.27    5.71
  -8   1   5   85.86    6.75
  -8   1   4  486.15   15.90
  -8  -1   4  483.93   14.95
  -8  -1   4  483.13   15.62
  -8  -1   3  314.08   11.84
  -8   1   3  304.92   11.70
  -8  -1   2  105.50    6.52
  -8   1   2   90.77    6.10
  -8   1   1  101.19    6.20
  -8  -1   1  102.67    6.30
  -8  -1   0   12.38    2.94
  -8   1   0   12.35    2.91
  -8  -1  -1  263.36   10.61
  -8   1  -1  260.78   10.69
  -8  -1  -2    4.67    2.40
  -8   1  -2    3.04    2.06
  -8  -1  -3    8.40    2.75
  -8   1  -3   11.53    2.92
  -8   1  -4    1.17    1.82
  -8  -1  -4    2.56    1.81
  -8  -1  -5   59.20    6.42
  -8   1  -5   66.32    6.70
  -8   1  -6    1.14    2.46
  -8  -1  -6   -0.33    2.14
  -8   1  -7  100.57    8.58
  -8  -1  -7   86.75    8.47
  -8  -1  -8    3.64    3.13
  -8   1  -8    0.33    2.61
  -8  -1  -9   -2.02    2.64
  -8   1  -9    2.29    3.01
  -8  -1 -10    3.27    3.83
  -8   1 -10    4.96    3.48
  -8   1 -11   11.83    4.03
  -8  -1 -11   10.18    4.08
  -8  -1 -12    4.81    3.78
  -8   1 -12   10.40    4.26
  -8   1 -13    6.62    4.09
  -8  -1 -13    8.98    4.54
  -8   2  19    7.88    3.67
  -8  -2  19    4.72    4.76
  -8   2  18   25.79    6.04
  -8  -2  18    6.21    4.92
  -8   2  17    1.83    3.12
  -8  -2  17    5.66    5.10
  -8   2  16   13.06    4.75
  -8  -2  16   25.40    7.07
  -8  -2  15    6.09    4.52
  -8   2  15    2.07    3.11
  -8  -2  14    2.21    4.07
  -8   2  14    2.83    3.77
   8  -2 -13    6.20    2.88
  -8  -2  13    2.88    4.93
  -8   2  13   13.57    5.03
  -8   2  12   -1.56    3.29
  -8  -2  12    6.50    4.63
   8  -2 -12   -0.66    2.30
   8  -2 -11    7.02    3.24
  -8  -2  11    9.55    4.68
  -8   2  11    1.65    3.50
   8  -2 -10    0.76    2.42
  -8   2  10    3.21    4.08
  -8  -2  10   -1.43    3.81
  -8  -2  10   -0.40    2.38
   8  -2  -9    0.10    2.44
  -8  -2   9    6.02    4.66
  -8  -2   9    3.05    3.19
  -8   2   9   -0.64    3.64
  -8   2   8   93.46    4.75
   8  -2  -8   97.43    6.44
  -8  -2   8  103.69    7.36
  -8  -2   8   97.10    7.88
  -8   2   8   86.37    7.75
  -8   2   7  161.59    6.64
  -8  -2   7  154.46    8.51
   8  -2  -7  147.83    8.00
  -8   2   7  145.49    9.51
  -8  -2   7  161.77    9.28
  -8  -2   6  564.58   17.00
  -8  -2   6  531.84   17.52
  -8   2   6  561.16   18.44
  -8   2   6  553.24   14.86
  -8  -2   5  575.95   17.22
  -8   2   5  589.99   18.33
  -8   2   5  577.76   15.60
  -8  -2   5  571.66   17.93
  -8   2   4   21.05    4.18
  -8  -2   4   26.77    4.24
  -8  -2   4   23.30    3.58
  -8  -2   3  404.91   13.67
  -8   2   3  391.25   13.88
  -8   2   2  368.24   12.93
  -8  -2   2  372.40   12.62
  -8   2   1   69.10    5.25
  -8  -2   1   61.20    4.99
  -8   2   0   52.31    4.65
  -8  -2   0   49.47    4.37
  -8  -2  -1   73.84    5.53
  -8   2  -1   86.24    5.89
  -8  -2  -2   29.46    4.16
  -8   2  -2   36.35    4.60
  -8  -2  -3    0.28    1.72
  -8   2  -3   -2.06    1.20
  -8  -2  -4    5.25    2.54
  -8   2  -4   10.50    3.27
  -8   2  -5    0.30    1.85
  -8  -2  -5   -0.57    2.00
  -8   2  -6   12.03    3.88
  -8  -2  -6   17.28    4.12
  -8  -2  -7   -3.82    2.67
  -8   2  -7   -1.39    2.83
  -8   2  -8   27.27    5.63
  -8  -2  -8   40.61    6.47
  -8   2  -9    1.01    2.89
  -8  -2  -9    3.53    3.39
  -8   2 -10   37.30    7.21
  -8  -2 -10   30.75    6.59
  -8  -2 -11    0.84    3.12
  -8   2 -11    4.64    3.56
  -8   2 -12   27.58    5.93
  -8  -2 -12   20.88    5.61
  -8  -2 -13   20.87    5.37
  -8   2 -13   13.81    4.64
  -8   3  19   12.27    3.95
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  -8   3  18    5.62    3.75
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  -8   3  16   10.20    4.43
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  -8   3  15    7.08    3.93
  -8   3  14    0.90    3.18
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  -8  -3  12   57.17    7.78
  -8   3  12   57.55    7.36
   8  -3 -12   49.24    5.60
  -8   3  11   19.55    5.14
  -8  -3  11   18.10    5.70
  -8  -3  11   16.58    2.88
   8  -3 -11   15.02    3.93
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  -8   3  10   10.50    4.88
  -8  -3  10    0.06    3.92
   8  -3 -10    7.41    3.22
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  -8   3   9   33.37    5.90
   8  -3  -9   48.41    5.44
  -8  -3   9   26.96    5.94
   8  -3  -8   -1.60    2.15
  -8  -3   8   -0.64    3.61
  -8   3   8    5.08    3.91
  -8  -3   8   -2.30    3.43
   8  -3  -7  104.05    6.75
  -8  -3   7  111.39    7.66
  -8   3   7  111.82    5.10
  -8  -3   7  102.87    7.70
  -8   3   7  113.53    8.44
  -8   3   6   23.44    4.94
   8  -3  -6   25.28    3.97
  -8   3   6   22.46    2.59
  -8  -3   6   19.19    4.36
  -8  -3   6   27.87    4.32
  -8   3   5   29.49    4.66
  -8  -3   5   39.17    5.16
   8  -3  -5   29.64    4.09
  -8   3   5   35.22    3.03
  -8  -3   5   35.76    4.28
  -8  -3   4   -0.01    2.56
  -8   3   4   -0.72    2.37
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  -8  -3   3  258.61   10.33
  -8   3   3  269.80   11.10
  -8  -3   2    9.70    2.69
  -8   3   2    9.69    3.01
  -8   3   1   35.33    4.45
  -8  -3   1   29.65    3.81
  -8   3   0   -0.04    1.71
  -8  -3   0    1.01    1.73
  -8   3  -1   76.85    5.75
  -8  -3  -1   86.12    5.80
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  -8  -3  -2   12.20    3.04
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  -8   3  -3    4.08    2.03
  -8   3  -4   17.90    4.10
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  -8  -3  -5   31.14    5.08
  -8   3  -5   27.80    4.87
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  -8   3  -7   26.97    5.64
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  -8  -3 -10    4.47    3.59
  -8   3 -11   23.02    6.12
  -8  -3 -11   36.23    6.86
  -8   3 -12    5.72    3.67
  -8  -3 -12    8.37    3.90
  -8   3 -13   23.99    6.37
  -8  -3 -13   21.98    6.09
  -8   4  19   11.44    4.54
  -8  -4  19    7.46    4.59
  -8  -4  18    3.33    5.11
  -8   4  18   13.12    5.39
  -8   4  17    4.78    3.73
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  -8  -4  16    8.73    5.82
  -8  -4  15   19.02    5.72
  -8   4  15   14.62    4.97
  -8  -4  14    2.60    4.34
  -8   4  14    1.05    3.70
   8  -4 -14   -3.13    2.92
   8  -4 -13    3.40    2.80
  -8   4  13    3.03    4.27
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   8  -4 -12   -4.05    1.85
  -8   4  12    0.93    4.15
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  -8  -4  11    7.63    2.99
  -8   4  11    3.34    4.15
   8  -4 -10   35.68    5.13
  -8  -4  10   33.41    4.94
  -8   4  10   61.05    7.67
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   8  -4  -9   12.83    3.69
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  -8   4   9   15.69    5.02
  -8  -4   9   10.61    4.01
  -8  -4   8   79.05    7.63
  -8   4   8   85.50    7.66
  -8  -4   8   86.85    7.73
   8  -4  -8   72.97    6.16
  -8  -4   7    2.08    3.61
   8  -4  -7   -2.83    2.12
  -8   4   7   -0.18    1.64
  -8  -4   7    0.48    3.45
  -8   4   7   -0.04    3.25
  -8  -4   6    0.21    3.03
  -8  -4   6    0.00    2.79
  -8   4   6    2.32    3.32
   8  -4  -6    0.03    1.98
  -8   4   6    0.76    1.23
  -8   4   5   -1.37    2.77
  -8  -4   5   -2.16    3.13
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   8  -4  -5   -0.19    2.14
   8  -4  -4  264.72   10.65
  -8  -4   4  252.00   10.63
  -8   4   4  259.65   10.96
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  -8  -4   3  174.29    8.27
  -8  -4   3  186.22    9.10
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  -8   4   2   55.58    5.27
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  -8  -4   0   49.74    4.24
  -8   4   0   47.61    4.84
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  -8   4  -4    4.97    2.51
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  -8   4  -6   20.06    4.69
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  -8   4  -7    9.05    3.78
  -8  -4  -8   49.41    6.90
  -8   4  -8   49.83    7.43
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  -8  -5  17   16.99    6.30
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   8  -5 -13   11.38    4.16
   8  -5 -12    2.64    2.84
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   8  -5 -10   17.08    4.04
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  -8   5   7   96.88    8.09
  -8  -5   7   96.95    7.52
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   8  -5  -6    4.29    2.65
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  -8   5   6    3.40    3.55
  -8  -5   5   28.04    3.99
   8  -5  -5   46.31    4.98
  -8   5   5   45.42    5.54
  -8  -5   5   56.85    5.85
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   8  -5  -4   13.79    3.36
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  -8  -5   4   13.05    3.63
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  -8   5   3  123.34    7.60
  -8  -5   3  118.97    7.60
  -8  -5   3  121.94    7.04
  -8   5   2  365.44   13.17
  -8  -5   2  365.54   12.30
  -8  -5   2  363.70   13.98
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  -8   5  -2   31.01    4.38
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  -8   5  -4   36.76    5.19
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  -8  -5  -7   69.50    7.55
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  -8   6  16    7.58    4.47
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  -8  -6  15    3.06    4.43
  -8   6  14    0.06    3.63
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   8  -6 -12    4.37    3.22
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  -8  -6  11   16.53    4.04
  -8  -6  11   10.46    4.84
   8  -6 -11   15.23    4.26
  -8   6  11   16.32    5.02
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  -8   6  10  113.83    9.24
  -8  -6  10  116.71    8.69
   8  -6 -10  109.41    7.71
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   8  -6  -9    6.05    3.29
  -8   6   9   -0.97    4.08
  -8  -6   9    3.99    3.83
  -8   6   8   79.19    7.73
  -8  -6   8   74.62    7.42
  -8  -6   8   82.83    8.15
   8  -6  -8   74.11    6.24
  -8  -6   7  123.43    8.72
  -8  -6   7  145.55    9.63
  -8   6   7  142.99    9.49
   8  -6  -7  153.99    8.79
  -8  -6   6    6.39    3.40
  -8   6   6    2.33    3.29
   8  -6  -6   -0.95    2.24
  -8  -6   6    2.88    3.24
  -8   6   6    3.00    0.91
  -8  -6   5   56.54    5.77
   8  -6  -5   57.86    5.33
  -8   6   5   62.67    6.08
  -8  -6   4   -0.40    2.74
   8  -6  -4    5.88    2.51
  -8  -6   4    0.94    2.66
  -8   6   4    4.13    2.96
  -8  -6   3  153.74    8.86
  -8  -6   3  159.61    7.93
   8  -6  -3  154.31    8.00
  -8   6   3  162.27    8.55
  -8   6   2    1.04    1.90
  -8  -6   2   -1.37    1.92
  -8  -6   2   -1.49    1.92
  -8   6   1   -2.20    1.64
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  -8  -6   1    1.35    1.84
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  -8  -6   0    3.60    2.13
  -8  -6  -1  125.71    6.82
  -8   6  -1  115.54    7.05
  -8  -6  -2   25.59    3.87
  -8   6  -2   24.85    3.97
  -8   6  -3    0.09    1.52
  -8  -6  -3    0.98    2.14
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  -8   6  -4  126.41    8.16
  -8  -6  -5    4.34    2.39
  -8   6  -5    5.08    2.64
  -8   6  -6  199.19   11.47
  -8  -6  -6  182.10   10.20
  -8   6  -7    4.76    2.66
  -8  -6  -7    1.03    2.66
  -8  -6  -8   15.49    4.45
  -8   6  -8   15.32    4.42
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  -8   6 -11    1.48    2.95
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  -8   7  19    5.33    3.76
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  -8   7  18   33.46    6.72
  -8   7  17   28.32    6.18
  -8  -7  17   25.14    6.70
  -8  -7  16    4.43    5.10
  -8   7  16    2.64    3.55
  -8   7  15    9.82    4.65
  -8  -7  15   14.51    5.79
  -8  -7  14   21.58    6.10
   8  -7 -14   25.32    5.02
  -8   7  14   21.02    5.52
  -8   7  13    7.57    4.33
   8  -7 -13    7.29    3.67
  -8  -7  13   13.70    5.36
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   8  -7 -10   22.50    4.59
  -8  -7  10   20.37    5.28
  -8   7  10   23.37    5.95
   8  -7  -9   29.16    4.85
  -8  -7   9   29.08    5.60
  -8  -7   9   35.20    6.59
  -8   7   9   26.20    5.88
   8  -7  -8   -3.92    2.00
  -8   7   8   -1.95    3.56
  -8  -7   8   -3.79    4.38
  -8  -7   8    2.40    4.11
  -8  -7   7   63.78    7.49
  -8   7   7   56.51    6.57
   8  -7  -7   66.35    6.25
  -8  -7   7   55.45    6.27
  -8  -7   6  141.72    8.54
  -8   7   6  150.43    9.35
   8  -7  -6  145.80    8.34
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   8  -7  -5    6.83    2.83
  -8  -7   5   16.42    4.06
  -8   7   5   15.24    4.04
   8  -7  -4  272.74   11.51
  -8   7   4  301.67   12.28
  -8  -7   4  300.73   12.99
  -8  -7   4  299.19   11.35
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  -8   7   3    1.23    2.53
  -8  -7   3    4.31    3.21
   8  -7  -3    2.15    2.25
  -8  -7   2   25.71    4.70
  -8   7   2   37.07    4.59
  -8  -7   2   25.26    3.65
   8  -7  -2   30.11    4.23
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  -8  -7   1    4.04    2.94
  -8   7   1    5.11    2.36
  -8   7   0   95.77    6.52
  -8  -7   0   96.40    7.65
  -8  -7   0  102.55    6.00
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  -8  -7  -1  200.11    8.69
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  -8   7  -2   14.32    3.13
  -8   7  -3   85.32    6.65
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  -8   7  -4    0.78    1.51
  -8   7  -5   26.95    5.05
  -8  -7  -5   27.94    4.69
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  -8   7  -6    5.02    2.85
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  -8   7  -8   12.25    3.74
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  -8   7  -9   46.47    7.69
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  -8  -8  17    4.28    4.55
  -8   8  17    3.44    3.02
  -8   8  16    6.62    4.23
  -8  -8  16   20.89    6.51
  -8   8  15    2.55    3.77
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   8  -8 -15    4.78    4.52
   8  -8 -14    8.56    3.98
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   8  -8 -11   10.44    3.85
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   8  -8  -5  108.03    7.19
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  -8   8   3  138.13    8.29
   8  -8  -3  152.75    8.30
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   8 -11 -15   22.05    5.55
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  -8 -11  14    9.69    4.80
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   8 -11 -14   15.92    4.85
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   8 -11 -13  159.46   10.90
  -8 -11  13  162.03   11.08
  -8  11  13  122.36   10.25
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  -8  11  12    1.83    4.00
   8 -11 -12   -0.21    3.97
   8 -11 -11   81.79    8.21
  -8 -11  11  106.08    8.32
  -8  11  11   96.14    8.66
  -8 -11  10   33.06    5.49
  -8  11  10   46.66    7.04
  -8 -11  10   27.18    5.47
   8 -11 -10   46.87    6.60
  -8 -11   9   62.06    8.58
   8 -11  -9   56.27    6.79
  -8  11   9   51.68    7.09
  -8 -11   9   65.96    6.69
  -8  11   8   29.79    5.94
  -8 -11   8   35.63    7.63
   8 -11  -8   22.68    5.09
  -8 -11   8   31.54    5.22
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   8 -11  -7   26.97    4.92
  -8 -11   7   29.85    4.94
  -8  11   7   31.93    5.80
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   8 -11  -6   13.41    3.69
  -8 -11   6   14.51    4.44
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   8 -11  -5   50.70    5.66
  -8  11   5   46.19    5.97
   8 -11  -5   50.22    3.40
  -8 -11   5   44.48    6.99
  -8 -11   5   51.37    5.39
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   8 -11  -4   47.05    3.58
   8 -11  -4   37.73    5.13
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   8 -11   0    3.46    2.35
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   8 -11   1   33.25    5.00
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   8 -11   3   70.60    6.71
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   8 -11   4   -0.03    2.72
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  -8 -11  -5  173.05    9.01
  -8 -11  -5  158.76   11.94
   8 -11   5  166.74   11.38
  -8  11  -5  177.63   10.64
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   8 -11   6   42.13    7.23
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   8 -12 -16   23.71    5.91
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   8 -12 -14   66.97    8.27
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   8 -12 -13    7.19    4.57
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   8 -12 -12  109.75    9.41
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   8 -12 -11   35.91    6.42
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   8 -12  -8   28.60    5.50
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   8 -12  -7    9.50    4.04
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   8 -12  -6   32.44    5.07
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   8 -12  -5   64.00    6.58
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   8 -12   1    5.99    2.60
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   8 -14   2   98.51    7.93
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   8 -15   1   34.11    5.49
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   8 -15   2   61.27    5.37
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   8 -15   3   73.64    8.17
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   8 -15   4   56.71    7.84
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  -9   3  10   17.11    5.47
  -9   3   9  177.25   11.23
  -9  -3   9  155.74   10.22
   9  -3  -9  168.26    9.13
  -9  -3   9  156.72    9.48
  -9   3   8    9.05    4.45
  -9  -3   8   10.52    5.05
  -9  -3   8    6.42    4.10
   9  -3  -8    0.54    2.46
  -9  -3   7   39.20    5.82
  -9   3   7   40.21    3.78
  -9  -3   7   32.15    4.92
   9  -3  -7   35.51    4.81
  -9   3   7   42.00    5.91
  -9   3   6   82.52    4.69
  -9  -3   6   82.12    7.24
  -9   3   6   81.76    7.46
  -9  -3   6   82.67    6.69
  -9  -3   5  365.62   13.62
  -9   3   5  371.19   14.30
  -9  -3   5  370.62   14.10
  -9  -3   4   55.45    5.80
  -9   3   4   49.03    5.59
  -9  -3   4   46.87    5.01
  -9   3   3  105.15    7.15
  -9  -3   3  114.32    7.33
  -9  -3   3  117.39    7.47
  -9  -3   2    2.99    2.61
  -9   3   2    8.66    3.15
  -9  -3   1  244.42   10.32
  -9   3   1  228.80   10.47
  -9   3   0    2.84    1.99
  -9  -3   0    1.94    2.22
  -9   3  -1    9.60    2.82
  -9  -3  -1    8.29    2.84
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  -9  -3  -2   13.56    3.30
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  -9   4  15    5.69    4.43
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  -9  -4  13    5.39    5.35
  -9   4  13    3.34    4.73
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  -9  -4  12  101.71    9.15
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  -9  -4  11    0.49    4.50
   9  -4 -11   -0.65    2.50
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   9  -4 -10   16.47    4.18
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   9  -4  -9   28.77    4.87
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   9  -4  -8   36.96    5.00
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   9  -4  -7   98.48    6.85
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   9  -4  -6   68.19    5.76
  -9   4   6   69.09    4.06
  -9  -4   6   65.51    6.35
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  -9   4   6   64.14    6.63
  -9   4   5   55.00    5.98
  -9  -4   5   50.15    5.41
  -9  -4   5   40.32    5.60
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  -9   4  -4    8.78    3.27
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  -9   4  -6    2.32    2.87
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  -9   4  -7   -1.79    2.51
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  -9  -5  16    3.47    5.22
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   9  -5 -12   83.83    7.71
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   9  -5  -9  278.67   12.24
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  -9   5   6   42.05    3.03
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   9  -8  -4   10.08    3.09
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   9 -13  -1   29.61    4.89
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   9 -13  -1   25.77    4.35
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   9 -13   0    4.67    1.66
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   9 -13   4   43.15    7.21
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  -9  13  -7    2.50    2.42
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   9 -14  -9    1.79    3.88
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   9 -14  -8   35.15    6.18
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   9 -14  -4    0.73    2.43
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   9 -14  -3    4.85    3.21
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   9 -15  -2   11.87    3.52
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 -14   2  16   56.69    9.70
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 -14   2   9    1.26    5.34
 -14   2   8  145.46   11.67
 -14  -2   8  130.47   11.92
 -14  -2   7    4.23    5.77
 -14   2   7    6.38    5.50
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 -14  -2   6   10.11    3.41
 -14  -2   6   14.15    5.82
 -14   2   6    6.87    5.69
 -14  -2   5   35.23    6.85
 -14   2   5   27.80    6.91
 -14  -2   5   28.18    5.23
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 -14  -3  10   10.90    6.10
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 -14  -3   9   81.73   10.02
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 -20   2   4    5.96    5.99
 -20  -3  12    3.64    7.27
 -20   3  12    4.58    7.08
 -20   3  11    9.69    7.80
 -20  -3  11    9.48    7.89
 -20  -3  10   -4.03    5.74
 -20   3  10    0.67    6.39
 -20   3   9    3.98    6.42
 -20  -3   9   -3.22    6.72
 -20  -3   8   -8.77    6.02
 -20   3   8   -8.61    5.12
 -20  -3   7   13.19    7.09
 -20   3   7   21.72    8.06
 -20   3   6   -0.46    6.59
 -20  -3   6   10.58    7.31
 -20  -3   5    4.08    6.29
 -20   3   5    2.65    6.32
 -20   3   4   -1.52    5.82
 -20  -3   4   -1.35    5.49
 -20  -4  11    9.03    7.58
 -20   4  11    4.15    7.14
 -20  -4  10   -5.97    6.05
 -20   4  10    4.39    7.27
 -20   4   9    8.44    6.65
 -20  -4   9    9.48    8.05
 -20   4   8   -4.12    5.76
 -20  -4   8    1.29    6.33
 -20   4   7    5.13    6.52
 -20  -4   7    5.39    6.55
 -20   4   6   23.74    7.89
 -20  -4   6   33.01    9.12
 -20  -4   5    6.86    7.10
 -20   4   5   -5.35    5.24
 -20   5  11    3.11    7.16
 -20  -5  11    1.66    7.58
 -20   5  10    2.45    6.65
 -20  -5  10   -9.53    6.78
 -20   5   9    4.46    6.76
 -20  -5   9    0.78    7.00
 -20  -5   8    4.84    7.08
 -20   5   8    6.10    6.41
 -20   5   7    4.23    6.12
 -20  -5   7    2.06    6.94
 -20   5   6    1.14    5.36
 -20  -5   6   -6.35    6.49
 -20   5   5    3.52    6.00
 -20  -5   5   11.64    7.19
 -20   6  11   10.45    7.48
 -20  -6  11   -5.94    6.44
 -20   6  10    4.57    7.19
 -20  -6  10   -0.71    7.04
 -20  -6   9    6.82    7.55
 -20   6   9    7.36    7.06
 -20   6   8    8.04    7.47
 -20  -6   8   -1.94    6.14
 -20  -6   7   -7.41    5.76
 -20   6   7    0.96    5.18
 -20   6   6    0.63    6.14
 -20  -6   6   -2.47    6.21
 -20  -7  10    3.70    6.21
 -20   7  10   -2.61    5.42
 -20   7   9   14.88    7.59
 -20  -7   9   24.47    8.81
 -20   7   8   -8.01    5.86
 -20  -7   8    5.54    7.17
 -20   7   7    4.67    6.09
 -20  -7   7    6.41    7.17
 -20  -7   6   -2.87    6.03
 -20   7   6    0.00    5.50
 -20  -8   8   20.89    8.88
 -20   8   8   39.31    8.27
   0   0   0    0.00    0.00

_diffrn_radiation_type                  'Mo K\a'
_diffrn_radiation_probe                 x-ray
_diffrn_radiation_wavelength            0.71073
_diffrn_standards_number                0
_diffrn_standards_interval_time         .
_diffrn_standards_interval_count        .
_diffrn_standards_decay_%               ?
_diffrn_reflns_limit_h_min              -20
_diffrn_reflns_limit_h_max              17
_diffrn_reflns_limit_k_min              -32
_diffrn_reflns_limit_k_max              21
_diffrn_reflns_limit_l_min              -17
_diffrn_reflns_limit_l_max              19
_diffrn_reflns_theta_min                1.422
_diffrn_reflns_theta_max                26.409
_diffrn_reflns_av_unetI/netI            0.19295
_diffrn_reflns_number                   35980
_diffrn_reflns_number_extinctions       0
_diffrn_reflns_number_accepted          35980
_diffrn_reflns_number_rejected          0
_diffrn_ambient_temperature             273(2)
_computing_data_collection              ?
_computing_cell_refinement              ?
_computing_data_reduction               ?
_exptl_crystal_description              Fragment
_exptl_crystal_colour                   Colorless
_exptl_crystal_size_max                 0
_exptl_crystal_size_mid                 0
_exptl_crystal_size_min                 0
_exptl_crystal_density_method           'not measured'
_exptl_crystal_F000                     2547
_cell_length_a                          16.5086(13)
_cell_length_b                          26.3426(19)
_cell_length_c                          15.7814(12)
_cell_angle_alpha                       90
_cell_angle_beta                        114.8710(10)
_cell_angle_gamma                       90
_cell_volume                            6226.5(8)
_cell_measurement_temperature           273(2)
_cell_measurement_wavelength            0.71073
_cell_measurement_reflns_used           0
_cell_measurement_theta_max             0
_cell_measurement_theta_min             0
_exptl_absorpt_coefficient_mu           0.144
_exptl_absorpt_correction_type          none
loop_
    _atom_type_symbol
    _atom_type_number_in_cell
C 360
H 300
O 3
Sc 3
_cell_formula_units_Z                   3
_chemical_formula_moiety               'C120  H100  O1  Sc1'
_chemical_formula_sum                  'C120  H100  O1  Sc1'
_chemical_compound_source               ?
_space_group_crystal_system            ' '
_space_group_name_H-M_alt              ' '
_space_group_name_Hall                  ?
_space_group_IT_number                  0
_computing_structure_solution          'SUPERFLIP (Palatinus & Chapuis,2007)'
_computing_structure_refinement        'SHELXL-2018/3 (Sheldrick, 2015)'
_computing_molecular_graphics          'ORTEP-3 for Windows (Farrugia, 2012)'
_computing_publication_material        'WinGX publication routines (Farrugia, 2012)'
_atom_sites_solution_primary            iterative
_atom_sites_solution_secondary          iterative
_refine_ls_number_constraints           0
_refine_ls_number_restraints            0
;
_shelx_hkl_checksum              6028
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C2 C 0.0203(3) 0.90790(15) 0.0860(3) 0.0472(10) Uani 1 1 d . . . . .
H2A H -0.003198 0.912684 0.133726 0.057 Uiso 1 1 calc R U . . .
H2B H 0.085419 0.901899 0.119222 0.057 Uiso 1 1 calc R U . . .
C3 C -0.0225(3) 0.86184(15) 0.0290(3) 0.0446(10) Uani 1 1 d . . . . .
H3A H -0.006586 0.859568 -0.024719 0.054 Uiso 1 1 calc R U . . .
H3B H -0.088279 0.864851 0.004337 0.054 Uiso 1 1 calc R U . . .
C4 C 0.0081(4) 0.81395(17) 0.0880(4) 0.0693(14) Uani 1 1 d . . . . .
H4A H 0.073316 0.810292 0.108791 0.083 Uiso 1 1 calc R U . . .
H4B H -0.003168 0.818124 0.144461 0.083 Uiso 1 1 calc R U . . .
C5 C -0.0369(4) 0.76570(19) 0.0388(5) 0.0852(17) Uani 1 1 d . . . . .
H5A H -0.013482 0.736846 0.081364 0.128 Uiso 1 1 calc R U . . .
H5B H -0.101418 0.768408 0.019382 0.128 Uiso 1 1 calc R U . . .
H5C H -0.024792 0.760561 -0.016354 0.128 Uiso 1 1 calc R U . . .
C10 C -0.2323(2) 0.96404(13) -0.0159(2) 0.0304(8) Uani 1 1 d . . . . .
C11 C -0.2351(2) 1.00876(13) 0.0340(2) 0.0302(8) Uani 1 1 d . . . . .
C12 C -0.2376(2) 1.05153(13) -0.0220(2) 0.0309(8) Uani 1 1 d . . . . .
C13 C -0.2385(2) 1.03400(14) -0.1072(2) 0.0319(8) Uani 1 1 d . . . . .
C14 C -0.2338(2) 0.98003(14) -0.1036(2) 0.0311(8) Uani 1 1 d . . . . .
C15 C -0.2322(2) 0.91143(13) 0.0179(2) 0.0326(8) Uani 1 1 d . . . . .
C16 C -0.2762(3) 0.87218(14) -0.0432(3) 0.0392(9) Uani 1 1 d . . . . .
H16 H -0.305475 0.879077 -0.108227 0.047 Uiso 1 1 calc R U . . .
C17 C -0.2786(3) 0.82294(15) -0.0116(3) 0.0502(11) Uani 1 1 d . . . . .
C18 C -0.3269(4) 0.78149(18) -0.0819(4) 0.0698(14) Uani 1 1 d . . . . .
H18 H -0.391970 0.790002 -0.108327 0.084 Uiso 1 1 calc R U . . .
C19 C -0.3021(7) 0.7800(3) -0.1612(6) 0.160(4) Uani 1 1 d . . . . .
H19A H -0.308523 0.814035 -0.188525 0.240 Uiso 1 1 calc R U . . .
H19B H -0.239976 0.768847 -0.139356 0.240 Uiso 1 1 calc R U . . .
H19C H -0.341268 0.756303 -0.208483 0.240 Uiso 1 1 calc R U . . .
C20 C -0.3172(6) 0.7294(2) -0.0397(6) 0.139(3) Uani 1 1 d . . . . .
H20A H -0.333809 0.730546 0.013069 0.208 Uiso 1 1 calc R U . . .
H20B H -0.356401 0.705642 -0.086845 0.208 Uiso 1 1 calc R U . . .
H20C H -0.255109 0.718186 -0.017718 0.208 Uiso 1 1 calc R U . . .
C21 C -0.2389(3) 0.81468(17) 0.0830(4) 0.0610(13) Uani 1 1 d . . . . .
H21 H -0.241372 0.781588 0.105729 0.073 Uiso 1 1 calc R U . . .
C22 C -0.1954(3) 0.85267(18) 0.1468(3) 0.0619(13) Uani 1 1 d . . . . .
C23 C -0.1602(6) 0.8422(2) 0.2513(4) 0.100(2) Uani 1 1 d . . . . .
H23 H -0.154170 0.804631 0.260914 0.120 Uiso 1 1 calc R U . . .
C24 C -0.0760(6) 0.8649(4) 0.3074(5) 0.153(4) Uani 1 1 d . . . . .
H24A H -0.058672 0.856258 0.373162 0.229 Uiso 1 1 calc R U . . .
H24B H -0.030749 0.852228 0.287795 0.229 Uiso 1 1 calc R U . . .
H24C H -0.080751 0.901887 0.299862 0.229 Uiso 1 1 calc R U . . .
C25 C -0.2278(7) 0.8613(4) 0.2870(5) 0.160(4) Uani 1 1 d . . . . .
H25A H -0.286370 0.846273 0.249575 0.240 Uiso 1 1 calc R U . . .
H25B H -0.208152 0.851498 0.352519 0.240 Uiso 1 1 calc R U . . .
H25C H -0.232067 0.898366 0.281601 0.240 Uiso 1 1 calc R U . . .
C26 C -0.1908(3) 0.90066(16) 0.1131(3) 0.0473(10) Uani 1 1 d . . . . .
H26 H -0.158757 0.926687 0.155731 0.057 Uiso 1 1 calc R U . . .
C27 C -0.2519(2) 1.01221(14) 0.1192(2) 0.0341(8) Uani 1 1 d . . . . .
C28 C -0.3258(3) 0.98764(15) 0.1213(3) 0.0403(9) Uani 1 1 d . . . . .
H28 H -0.360738 0.966093 0.070842 0.048 Uiso 1 1 calc R U . . .
C29 C -0.3497(3) 0.99386(16) 0.1954(3) 0.0476(10) Uani 1 1 d . . . . .
C30 C -0.4334(3) 0.9684(2) 0.1926(3) 0.0660(14) Uani 1 1 d . . . . .
H30 H -0.441682 0.936296 0.156192 0.079 Uiso 1 1 calc R U . . .
C31 C -0.5142(4) 1.0007(3) 0.1410(5) 0.0936(19) Uani 1 1 d . . . . .
H31A H -0.516758 1.009745 0.079638 0.140 Uiso 1 1 calc R U . . .
H31B H -0.568063 0.981818 0.132824 0.140 Uiso 1 1 calc R U . . .
H31C H -0.510416 1.031744 0.176761 0.140 Uiso 1 1 calc R U . . .
C32 C -0.4277(5) 0.9540(3) 0.2870(5) 0.119(3) Uani 1 1 d . . . . .
H32A H -0.374635 0.933004 0.319596 0.178 Uiso 1 1 calc R U . . .
H32B H -0.423544 0.984835 0.323443 0.178 Uiso 1 1 calc R U . . .
H32C H -0.481191 0.934910 0.279506 0.178 Uiso 1 1 calc R U . . .
C33 C -0.2978(3) 1.02640(17) 0.2673(3) 0.0518(11) Uani 1 1 d . . . . .
H33 H -0.314063 1.032108 0.317601 0.062 Uiso 1 1 calc R U . . .
C34 C -0.2238(3) 1.05053(17) 0.2677(3) 0.0475(11) Uani 1 1 d . . . . .
C35 C -0.1665(4) 1.0845(2) 0.3488(3) 0.0707(16) Uani 1 1 d . . . . .
H35 H -0.197985 1.088500 0.390372 0.085 Uiso 1 1 calc R U . . .
C36 C -0.0773(4) 1.0603(3) 0.4055(4) 0.101(2) Uani 1 1 d . . . . .
H36A H -0.041595 1.082796 0.457238 0.151 Uiso 1 1 calc R U . . .
H36B H -0.086268 1.027772 0.430517 0.151 Uiso 1 1 calc R U . . .
H36C H -0.045844 1.054506 0.365719 0.151 Uiso 1 1 calc R U . . .
C37 C -0.1557(5) 1.1377(2) 0.3146(5) 0.105(2) Uani 1 1 d . . . . .
H37A H -0.214725 1.152439 0.277970 0.158 Uiso 1 1 calc R U . . .
H37B H -0.122568 1.159520 0.368454 0.158 Uiso 1 1 calc R U . . .
H37C H -0.122837 1.135133 0.275459 0.158 Uiso 1 1 calc R U . . .
C38 C -0.2006(3) 1.04315(15) 0.1942(3) 0.0408(9) Uani 1 1 d . . . . .
H38 H -0.148985 1.059379 0.194726 0.049 Uiso 1 1 calc R U . . .
C39 C -0.2530(2) 1.10416(14) 0.0031(2) 0.0349(9) Uani 1 1 d . . . . .
C40 C -0.3345(3) 1.11502(15) 0.0047(3) 0.0463(10) Uani 1 1 d . . . . .
H40 H -0.377993 1.088894 -0.009993 0.056 Uiso 1 1 calc R U . . .
C41 C -0.3546(3) 1.16317(17) 0.0271(3) 0.0561(12) Uani 1 1 d D . . . .
C42 C -0.4429(6) 1.1747(6) 0.0292(10) 0.0935(16) Uani 0.638(12) 1 d D . P A 2
H42 H -0.439646 1.206361 0.065442 0.112 Uiso 0.638(12) 1 calc R U P A 2
C43 C -0.5152(6) 1.1784(5) -0.0691(8) 0.0935(16) Uani 0.638(12) 1 d D . P A 2
H43A H -0.500490 1.205534 -0.102673 0.140 Uiso 0.638(12) 1 calc R U P A 2
H43B H -0.519657 1.146048 -0.101470 0.140 Uiso 0.638(12) 1 calc R U P A 2
H43C H -0.572387 1.185925 -0.066805 0.140 Uiso 0.638(12) 1 calc R U P A 2
C44 C -0.4828(7) 1.1321(4) 0.0606(10) 0.0935(16) Uani 0.638(12) 1 d D . P A 2
H44A H -0.539897 1.143011 0.059747 0.140 Uiso 0.638(12) 1 calc R U P A 2
H44B H -0.492710 1.103113 0.018521 0.140 Uiso 0.638(12) 1 calc R U P A 2
H44C H -0.442087 1.122201 0.124218 0.140 Uiso 0.638(12) 1 calc R U P A 2
C42' C -0.4456(12) 1.1732(12) 0.0283(18) 0.0935(16) Uani 0.362(12) 1 d D . P A
1
H42' H -0.422967 1.203928 0.068799 0.112 Uiso 0.362(12) 1 calc R U P A 1
C43' C -0.5018(11) 1.2051(8) -0.0567(13) 0.0935(16) Uani 0.362(12) 1 d D . P A
1
H43D H -0.464047 1.217890 -0.086137 0.140 Uiso 0.362(12) 1 calc R U P A 1
H43E H -0.549757 1.184165 -0.101546 0.140 Uiso 0.362(12) 1 calc R U P A 1
H43F H -0.527795 1.233802 -0.037258 0.140 Uiso 0.362(12) 1 calc R U P A 1
C44' C -0.4458(13) 1.1416(7) 0.1084(14) 0.0935(16) Uani 0.362(12) 1 d D . P A 1
H44D H -0.385519 1.128720 0.145740 0.140 Uiso 0.362(12) 1 calc R U P A 1
H44E H -0.465096 1.162638 0.147798 0.140 Uiso 0.362(12) 1 calc R U P A 1
H44F H -0.487058 1.113001 0.083510 0.140 Uiso 0.362(12) 1 calc R U P A 1
C45 C -0.2902(3) 1.20055(17) 0.0483(3) 0.0591(12) Uani 1 1 d . . . . .
H45 H -0.303565 1.233713 0.062320 0.071 Uiso 1 1 calc R U . . .
C46 C -0.2064(3) 1.19148(16) 0.0499(3) 0.0500(11) Uani 1 1 d . . . . .
C47 C -0.1354(3) 1.23256(17) 0.0790(3) 0.0631(13) Uani 1 1 d . . . . .
H47 H -0.079168 1.217117 0.081424 0.076 Uiso 1 1 calc R U . . .
C48 C -0.1157(4) 1.2540(2) 0.1751(4) 0.0870(18) Uani 1 1 d . . . . .
H48A H -0.069686 1.280258 0.190827 0.131 Uiso 1 1 calc R U . . .
H48B H -0.170288 1.268765 0.174837 0.131 Uiso 1 1 calc R U . . .
H48C H -0.094513 1.226687 0.221517 0.131 Uiso 1 1 calc R U . . .
C49 C -0.1629(4) 1.2752(2) 0.0070(4) 0.093(2) Uani 1 1 d . . . . .
H49A H -0.116385 1.301406 0.026855 0.140 Uiso 1 1 calc R U . . .
H49B H -0.170603 1.261559 -0.053669 0.140 Uiso 1 1 calc R U . . .
H49C H -0.219233 1.290116 0.001623 0.140 Uiso 1 1 calc R U . . .
C50 C -0.1893(3) 1.14250(15) 0.0269(3) 0.0410(9) Uani 1 1 d . . . . .
H50 H -0.132664 1.135282 0.027457 0.049 Uiso 1 1 calc R U . . .
C51 C -0.2520(2) 1.06485(15) -0.1916(2) 0.0363(9) Uani 1 1 d . . . . .
C52 C -0.3028(3) 1.10897(15) -0.2108(3) 0.0443(10) Uani 1 1 d . . . . .
H52 H -0.328542 1.119305 -0.169899 0.053 Uiso 1 1 calc R U . . .
C53 C -0.3166(3) 1.13835(18) -0.2895(3) 0.0616(14) Uani 1 1 d . . . . .
C54 C -0.3686(4) 1.1881(2) -0.3059(4) 0.0828(18) Uani 1 1 d . . . . .
H54 H -0.377323 1.201363 -0.368565 0.099 Uiso 1 1 calc R U . . .
C55 C -0.4582(5) 1.1817(3) -0.3067(6) 0.150(4) Uani 1 1 d . . . . .
H55A H -0.491887 1.156091 -0.353245 0.225 Uiso 1 1 calc R U . . .
H55B H -0.451657 1.170669 -0.244808 0.225 Uiso 1 1 calc R U . . .
H55C H -0.490351 1.214100 -0.322487 0.225 Uiso 1 1 calc R U . . .
C56 C -0.3169(5) 1.2278(2) -0.2338(4) 0.101(2) Uani 1 1 d . . . . .
H56A H -0.257630 1.232091 -0.233159 0.152 Uiso 1 1 calc R U . . .
H56B H -0.349080 1.260119 -0.249696 0.152 Uiso 1 1 calc R U . . .
H56C H -0.310387 1.216688 -0.172018 0.152 Uiso 1 1 calc R U . . .
C57 C -0.2804(4) 1.1218(2) -0.3492(3) 0.0649(15) Uani 1 1 d . . . . .
H57 H -0.289676 1.141480 -0.403001 0.078 Uiso 1 1 calc R U . . .
C58 C -0.2312(3) 1.07783(19) -0.3333(3) 0.0552(12) Uani 1 1 d D . . . .
C59 C -0.1914(7) 1.0584(6) -0.3999(9) 0.0822(15) Uani 0.657(10) 1 d D . P B 2
H59 H -0.189267 1.086038 -0.442315 0.099 Uiso 0.657(10) 1 calc R U P B 2
C60 C -0.1025(6) 1.0312(5) -0.3550(5) 0.0822(15) Uani 0.657(10) 1 d D . P B 2
H60A H -0.056732 1.054891 -0.314783 0.123 Uiso 0.657(10) 1 calc R U P B 2
H60B H -0.107499 1.002765 -0.317338 0.123 Uiso 0.657(10) 1 calc R U P B 2
H60C H -0.085797 1.018279 -0.403646 0.123 Uiso 0.657(10) 1 calc R U P B 2
C61 C -0.2464(8) 1.0140(4) -0.4553(6) 0.0822(15) Uani 0.657(10) 1 d D . P B 2
H61A H -0.308451 1.024730 -0.490461 0.123 Uiso 0.657(10) 1 calc R U P B 2
H61B H -0.222272 1.001947 -0.498885 0.123 Uiso 0.657(10) 1 calc R U P B 2
H61C H -0.243973 0.986433 -0.412577 0.123 Uiso 0.657(10) 1 calc R U P B 2
C59' C -0.2004(11) 1.0607(14) -0.4063(16) 0.0822(15) Uani 0.343(10) 1 d D . P B
1
H59' H -0.215932 1.092931 -0.443009 0.099 Uiso 0.343(10) 1 calc R U P B 1
C60' C -0.1017(10) 1.0683(9) -0.3659(10) 0.0822(15) Uani 0.343(10) 1 d D . P B
1
H60D H -0.084388 1.094144 -0.316760 0.123 Uiso 0.343(10) 1 calc R U P B 1
H60E H -0.071510 1.036256 -0.339326 0.123 Uiso 0.343(10) 1 calc R U P B 1
H60F H -0.084293 1.079499 -0.415134 0.123 Uiso 0.343(10) 1 calc R U P B 1
C61' C -0.2694(14) 1.0286(8) -0.4804(12) 0.0822(15) Uani 0.343(10) 1 d D . P B
1
H61D H -0.328601 1.036394 -0.483280 0.123 Uiso 0.343(10) 1 calc R U P B 1
H61E H -0.268767 1.035850 -0.540966 0.123 Uiso 0.343(10) 1 calc R U P B 1
H61F H -0.255984 0.992606 -0.465158 0.123 Uiso 0.343(10) 1 calc R U P B 1
C62 C -0.2166(3) 1.05046(16) -0.2530(3) 0.0459(10) Uani 1 1 d . . . . .
H62 H -0.180813 1.020710 -0.239906 0.055 Uiso 1 1 calc R U . . .
C63 C -0.2477(2) 0.94630(14) -0.1851(2) 0.0347(9) Uani 1 1 d . . . . .
C64 C -0.3342(3) 0.94160(17) -0.2539(3) 0.0483(11) Uani 1 1 d . . . . .
H64 H -0.381014 0.959845 -0.247549 0.058 Uiso 1 1 calc R U . . .
C65 C -0.3540(3) 0.9111(2) -0.3313(3) 0.0618(13) Uani 1 1 d D . . . .
C66 C -0.4467(12) 0.9035(8) -0.4025(17) 0.115(2) Uani 0.399(7) 1 d D . P C 2
H66 H -0.471035 0.913789 -0.356770 0.138 Uiso 0.399(7) 1 calc R U P C 2
C67 C -0.4839(11) 0.8525(7) -0.4092(12) 0.115(2) Uani 0.399(7) 1 d D . P C 2
H67A H -0.440930 0.830884 -0.360580 0.172 Uiso 0.399(7) 1 calc R U P C 2
H67B H -0.539423 0.854366 -0.400898 0.172 Uiso 0.399(7) 1 calc R U P C 2
H67C H -0.496424 0.838176 -0.470792 0.172 Uiso 0.399(7) 1 calc R U P C 2
C68 C -0.4830(11) 0.9492(7) -0.4576(11) 0.115(2) Uani 0.399(7) 1 d D . P C 2
H68A H -0.439606 0.976903 -0.433585 0.172 Uiso 0.399(7) 1 calc R U P C 2
H68B H -0.495450 0.942651 -0.523004 0.172 Uiso 0.399(7) 1 calc R U P C 2
H68C H -0.538449 0.958840 -0.453110 0.172 Uiso 0.399(7) 1 calc R U P C 2
C66' C -0.4501(8) 0.9049(8) -0.4058(9) 0.115(2) Uani 0.601(7) 1 d D . P C 1
H66' H -0.468848 0.938114 -0.388880 0.138 Uiso 0.601(7) 1 calc R U P C 1
C67' C -0.5023(7) 0.8757(5) -0.3655(7) 0.115(2) Uani 0.601(7) 1 d D . P C 1
H67D H -0.466888 0.871553 -0.298134 0.172 Uiso 0.601(7) 1 calc R U P C 1
H67E H -0.557549 0.893978 -0.376474 0.172 Uiso 0.601(7) 1 calc R U P C 1
H67F H -0.516990 0.842211 -0.395166 0.172 Uiso 0.601(7) 1 calc R U P C 1
C68' C -0.4627(7) 0.9240(5) -0.4991(6) 0.115(2) Uani 0.601(7) 1 d D . P C 1
H68D H -0.408891 0.942205 -0.493545 0.172 Uiso 0.601(7) 1 calc R U P C 1
H68E H -0.473418 0.895303 -0.542022 0.172 Uiso 0.601(7) 1 calc DR U P C 1
H68F H -0.513977 0.947069 -0.523330 0.172 Uiso 0.601(7) 1 calc R U P C 1
C69 C -0.2829(4) 0.8857(2) -0.3391(3) 0.0682(15) Uani 1 1 d . . . . .
H69 H -0.294959 0.864528 -0.391793 0.082 Uiso 1 1 calc R U . . .
C70 C -0.1965(3) 0.89034(18) -0.2734(3) 0.0574(12) Uani 1 1 d . . . . .
C71 C -0.1189(5) 0.8628(3) -0.2837(5) 0.1071(13) Uani 1 1 d . . . . .
H71 H -0.062285 0.877652 -0.236091 0.129 Uiso 1 1 calc R U . . .
C72 C -0.1183(5) 0.8077(3) -0.2612(5) 0.1071(13) Uani 1 1 d . . . . .
H72A H -0.118155 0.803950 -0.199319 0.161 Uiso 1 1 calc R U . . .
H72B H -0.171660 0.791393 -0.308096 0.161 Uiso 1 1 calc R U . . .
H72C H -0.064813 0.791694 -0.261301 0.161 Uiso 1 1 calc R U . . .
C73 C -0.1192(5) 0.8724(3) -0.3801(5) 0.1071(13) Uani 1 1 d . . . . .
H73A H -0.119495 0.909004 -0.391022 0.161 Uiso 1 1 calc R U . . .
H73B H -0.065651 0.857258 -0.381859 0.161 Uiso 1 1 calc R U . . .
H73C H -0.172498 0.856956 -0.428654 0.161 Uiso 1 1 calc R U . . .
C74 C -0.1794(3) 0.92057(15) -0.1954(3) 0.0417(10) Uani 1 1 d . . . . .
H74 H -0.120064 0.923569 -0.148691 0.050 Uiso 1 1 calc R U . . .
O1 O 0.00564(16) 0.95404(9) 0.03168(16) 0.0368(6) Uani 1 1 d . . . . .
Sc1 Sc -0.08749(4) 1.00919(3) 0.01735(4) 0.0315(2) Uani 1 1 d . . . . .
H1 H -0.027(3) 1.0248(15) 0.174(3) 0.055(12) Uiso 1 1 d . . . . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
C2 0.044(2) 0.043(3) 0.047(2) 0.0112(19) 0.0118(19) -0.0017(19)
C3 0.039(2) 0.041(3) 0.055(2) 0.0063(19) 0.022(2) -0.0006(18)
C4 0.073(3) 0.045(3) 0.087(4) 0.015(3) 0.031(3) 0.002(2)
C5 0.087(4) 0.050(3) 0.134(5) 0.009(3) 0.062(4) 0.003(3)
C10 0.0238(18) 0.032(2) 0.0331(18) -0.0031(15) 0.0091(15) -0.0016(15)
C11 0.0237(18) 0.037(2) 0.0289(17) -0.0011(15) 0.0099(14) -0.0011(15)
C12 0.0248(19) 0.034(2) 0.0330(18) -0.0006(15) 0.0112(15) -0.0003(15)
C13 0.0262(19) 0.036(2) 0.0329(19) 0.0029(15) 0.0121(15) 0.0006(15)
C14 0.0250(19) 0.042(3) 0.0265(17) -0.0013(15) 0.0108(15) -0.0037(15)
C15 0.029(2) 0.033(2) 0.039(2) 0.0044(16) 0.0173(16) 0.0029(15)
C16 0.037(2) 0.037(2) 0.046(2) -0.0038(18) 0.0194(18) -0.0033(17)
C17 0.052(3) 0.033(3) 0.073(3) 0.001(2) 0.035(2) -0.0024(19)
C18 0.078(4) 0.041(3) 0.087(4) -0.009(3) 0.031(3) -0.013(2)
C19 0.261(12) 0.099(6) 0.123(6) -0.054(5) 0.083(7) -0.079(7)
C20 0.142(7) 0.059(4) 0.153(7) 0.001(4) 0.000(5) -0.021(4)
C21 0.071(3) 0.037(3) 0.079(3) 0.014(2) 0.035(3) 0.002(2)
C22 0.077(3) 0.047(3) 0.056(3) 0.020(2) 0.022(3) 0.014(2)
C23 0.162(7) 0.069(4) 0.052(3) 0.021(3) 0.028(4) 0.006(4)
C24 0.144(8) 0.212(10) 0.066(4) 0.013(5) 0.008(5) 0.027(7)
C25 0.214(11) 0.215(10) 0.082(5) 0.039(5) 0.091(6) 0.003(8)
C26 0.050(3) 0.043(3) 0.044(2) 0.0042(19) 0.016(2) 0.0021(19)
C27 0.040(2) 0.034(2) 0.0320(18) 0.0018(16) 0.0187(17) 0.0002(17)
C28 0.039(2) 0.048(2) 0.036(2) -0.0022(17) 0.0179(17) -0.0103(18)
C29 0.051(3) 0.054(3) 0.047(2) -0.002(2) 0.029(2) -0.009(2)
C30 0.067(3) 0.083(4) 0.063(3) -0.017(3) 0.041(3) -0.026(3)
C31 0.053(3) 0.129(6) 0.108(5) -0.001(4) 0.043(3) -0.015(3)
C32 0.112(6) 0.168(7) 0.102(5) 0.022(5) 0.071(4) -0.051(5)
C33 0.063(3) 0.068(3) 0.038(2) -0.004(2) 0.035(2) -0.005(2)
C34 0.049(3) 0.062(3) 0.038(2) -0.0093(19) 0.025(2) -0.011(2)
C35 0.077(4) 0.100(4) 0.049(3) -0.030(3) 0.040(3) -0.035(3)
C36 0.075(4) 0.158(6) 0.051(3) -0.020(3) 0.008(3) -0.041(4)
C37 0.142(6) 0.086(5) 0.095(4) -0.050(4) 0.057(4) -0.039(4)
C38 0.037(2) 0.050(3) 0.040(2) -0.0052(18) 0.0209(18) -0.0111(18)
C39 0.039(2) 0.030(2) 0.039(2) -0.0010(16) 0.0189(17) -0.0021(16)
C40 0.039(2) 0.039(3) 0.067(3) -0.003(2) 0.028(2) -0.0035(18)
C41 0.053(3) 0.044(3) 0.084(3) -0.004(2) 0.041(3) 0.006(2)
C42 0.054(3) 0.073(3) 0.159(5) -0.026(3) 0.051(3) -0.002(2)
C43 0.054(3) 0.073(3) 0.159(5) -0.026(3) 0.051(3) -0.002(2)
C44 0.054(3) 0.073(3) 0.159(5) -0.026(3) 0.051(3) -0.002(2)
C42' 0.054(3) 0.073(3) 0.159(5) -0.026(3) 0.051(3) -0.002(2)
C43' 0.054(3) 0.073(3) 0.159(5) -0.026(3) 0.051(3) -0.002(2)
C44' 0.054(3) 0.073(3) 0.159(5) -0.026(3) 0.051(3) -0.002(2)
C45 0.064(3) 0.037(3) 0.090(3) -0.008(2) 0.046(3) 0.000(2)
C46 0.058(3) 0.035(3) 0.064(3) -0.007(2) 0.033(2) -0.005(2)
C47 0.070(3) 0.043(3) 0.086(3) -0.015(2) 0.042(3) -0.016(2)
C48 0.097(5) 0.073(4) 0.092(4) -0.027(3) 0.041(4) -0.025(3)
C49 0.118(5) 0.064(4) 0.100(4) 0.001(3) 0.047(4) -0.037(3)
C50 0.041(2) 0.040(3) 0.050(2) -0.0019(18) 0.0269(19) -0.0019(18)
C51 0.032(2) 0.047(2) 0.0278(18) 0.0039(16) 0.0101(16) -0.0083(17)
C52 0.042(2) 0.045(3) 0.039(2) 0.0099(18) 0.0114(18) -0.0007(19)
C53 0.057(3) 0.057(3) 0.049(3) 0.017(2) 0.001(2) -0.010(2)
C54 0.094(5) 0.068(4) 0.066(3) 0.035(3) 0.015(3) 0.007(3)
C55 0.083(5) 0.103(6) 0.236(10) 0.067(6) 0.040(6) 0.043(4)
C56 0.120(6) 0.067(4) 0.102(5) 0.008(4) 0.033(4) 0.011(4)
C57 0.079(4) 0.074(4) 0.031(2) 0.016(2) 0.012(2) -0.021(3)
C58 0.060(3) 0.068(3) 0.033(2) 0.002(2) 0.016(2) -0.023(2)
C59 0.096(3) 0.108(4) 0.051(2) -0.001(2) 0.039(2) -0.015(3)
C60 0.096(3) 0.108(4) 0.051(2) -0.001(2) 0.039(2) -0.015(3)
C61 0.096(3) 0.108(4) 0.051(2) -0.001(2) 0.039(2) -0.015(3)
C59' 0.096(3) 0.108(4) 0.051(2) -0.001(2) 0.039(2) -0.015(3)
C60' 0.096(3) 0.108(4) 0.051(2) -0.001(2) 0.039(2) -0.015(3)
C61' 0.096(3) 0.108(4) 0.051(2) -0.001(2) 0.039(2) -0.015(3)
C62 0.042(2) 0.055(3) 0.036(2) 0.0022(18) 0.0125(19) -0.0109(19)
C63 0.036(2) 0.040(2) 0.0284(18) -0.0045(15) 0.0146(16) -0.0061(17)
C64 0.036(2) 0.068(3) 0.039(2) -0.0080(19) 0.0139(19) -0.004(2)
C65 0.051(3) 0.091(4) 0.040(2) -0.018(2) 0.016(2) -0.017(3)
C66 0.073(3) 0.179(6) 0.070(3) -0.035(3) 0.009(2) -0.040(3)
C67 0.073(3) 0.179(6) 0.070(3) -0.035(3) 0.009(2) -0.040(3)
C68 0.073(3) 0.179(6) 0.070(3) -0.035(3) 0.009(2) -0.040(3)
C66' 0.073(3) 0.179(6) 0.070(3) -0.035(3) 0.009(2) -0.040(3)
C67' 0.073(3) 0.179(6) 0.070(3) -0.035(3) 0.009(2) -0.040(3)
C68' 0.073(3) 0.179(6) 0.070(3) -0.035(3) 0.009(2) -0.040(3)
C69 0.080(4) 0.079(4) 0.049(3) -0.034(2) 0.030(3) -0.022(3)
C70 0.054(3) 0.062(3) 0.059(3) -0.025(2) 0.027(2) -0.005(2)
C71 0.112(3) 0.107(3) 0.129(3) -0.042(3) 0.077(3) -0.003(3)
C72 0.112(3) 0.107(3) 0.129(3) -0.042(3) 0.077(3) -0.003(3)
C73 0.112(3) 0.107(3) 0.129(3) -0.042(3) 0.077(3) -0.003(3)
C74 0.039(2) 0.048(3) 0.036(2) -0.0103(18) 0.0139(18) -0.0058(18)
O1 0.0365(15) 0.0363(15) 0.0374(13) 0.0049(11) 0.0153(12) -0.0018(11)
Sc1 0.0274(4) 0.0363(4) 0.0309(4) -0.0022(3) 0.0124(3) -0.0013(3)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sc Sc 0.2519 0.3716 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 C2 C3 113.9(3) . . ?
O1 C2 H2A 108.8 . . ?
C3 C2 H2A 108.8 . . ?
O1 C2 H2B 108.8 . . ?
C3 C2 H2B 108.8 . . ?
H2A C2 H2B 107.7 . . ?
C2 C3 C4 110.6(4) . . ?
C2 C3 H3A 109.5 . . ?
C4 C3 H3A 109.5 . . ?
C2 C3 H3B 109.5 . . ?
C4 C3 H3B 109.5 . . ?
H3A C3 H3B 108.1 . . ?
C5 C4 C3 114.7(4) . . ?
C5 C4 H4A 108.6 . . ?
C3 C4 H4A 108.6 . . ?
C5 C4 H4B 108.6 . . ?
C3 C4 H4B 108.6 . . ?
H4A C4 H4B 107.6 . . ?
C4 C5 H5A 109.5 . . ?
C4 C5 H5B 109.5 . . ?
H5A C5 H5B 109.5 . . ?
C4 C5 H5C 109.5 . . ?
H5A C5 H5C 109.5 . . ?
H5B C5 H5C 109.5 . . ?
C11 C10 C14 107.3(3) . . ?
C11 C10 C15 124.5(3) . . ?
C14 C10 C15 128.1(3) . . ?
C11 C10 Sc1 75.16(19) . . ?
C14 C10 Sc1 72.11(19) . . ?
C15 C10 Sc1 120.5(2) . . ?
C12 C11 C10 108.0(3) . . ?
C12 C11 C27 123.1(3) . . ?
C10 C11 C27 127.7(3) . . ?
C12 C11 Sc1 73.3(2) . . ?
C10 C11 Sc1 72.17(19) . . ?
C27 C11 Sc1 129.9(2) . . ?
C13 C12 C11 108.5(3) . . ?
C13 C12 C39 128.3(3) . . ?
C11 C12 C39 122.3(3) . . ?
C13 C12 Sc1 73.08(19) . . ?
C11 C12 Sc1 74.4(2) . . ?
C39 C12 Sc1 126.8(2) . . ?
C12 C13 C14 108.0(3) . . ?
C12 C13 C51 127.4(3) . . ?
C14 C13 C51 124.3(3) . . ?
C12 C13 Sc1 74.48(19) . . ?
C14 C13 Sc1 72.01(19) . . ?
C51 C13 Sc1 124.2(2) . . ?
C13 C14 C10 108.1(3) . . ?
C13 C14 C63 124.8(3) . . ?
C10 C14 C63 125.9(3) . . ?
C13 C14 Sc1 75.02(19) . . ?
C10 C14 Sc1 74.55(18) . . ?
C63 C14 Sc1 126.2(2) . . ?
C16 C15 C26 118.2(3) . . ?
C16 C15 C10 121.6(3) . . ?
C26 C15 C10 120.2(3) . . ?
C15 C16 C17 121.9(4) . . ?
C15 C16 H16 119.1 . . ?
C17 C16 H16 119.1 . . ?
C21 C17 C16 117.6(4) . . ?
C21 C17 C18 122.9(4) . . ?
C16 C17 C18 119.4(4) . . ?
C19 C18 C20 109.7(6) . . ?
C19 C18 C17 113.0(5) . . ?
C20 C18 C17 113.9(5) . . ?
C19 C18 H18 106.6 . . ?
C20 C18 H18 106.6 . . ?
C17 C18 H18 106.6 . . ?
C18 C19 H19A 109.5 . . ?
C18 C19 H19B 109.5 . . ?
H19A C19 H19B 109.5 . . ?
C18 C19 H19C 109.5 . . ?
H19A C19 H19C 109.5 . . ?
H19B C19 H19C 109.5 . . ?
C18 C20 H20A 109.5 . . ?
C18 C20 H20B 109.5 . . ?
H20A C20 H20B 109.5 . . ?
C18 C20 H20C 109.5 . . ?
H20A C20 H20C 109.5 . . ?
H20B C20 H20C 109.5 . . ?
C17 C21 C22 122.7(4) . . ?
C17 C21 H21 118.7 . . ?
C22 C21 H21 118.7 . . ?
C26 C22 C21 118.4(4) . . ?
C26 C22 C23 121.4(5) . . ?
C21 C22 C23 120.0(4) . . ?
C24 C23 C22 115.1(6) . . ?
C24 C23 C25 107.7(7) . . ?
C22 C23 C25 109.5(6) . . ?
C24 C23 H23 108.1 . . ?
C22 C23 H23 108.1 . . ?
C25 C23 H23 108.1 . . ?
C23 C24 H24A 109.5 . . ?
C23 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
C23 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
C23 C25 H25A 109.5 . . ?
C23 C25 H25B 109.5 . . ?
H25A C25 H25B 109.5 . . ?
C23 C25 H25C 109.5 . . ?
H25A C25 H25C 109.5 . . ?
H25B C25 H25C 109.5 . . ?
C22 C26 C15 121.2(4) . . ?
C22 C26 H26 119.4 . . ?
C15 C26 H26 119.4 . . ?
C38 C27 C28 118.5(3) . . ?
C38 C27 C11 121.8(3) . . ?
C28 C27 C11 119.4(3) . . ?
C29 C28 C27 121.7(4) . . ?
C29 C28 H28 119.2 . . ?
C27 C28 H28 119.2 . . ?
C33 C29 C28 117.6(4) . . ?
C33 C29 C30 122.3(4) . . ?
C28 C29 C30 120.0(4) . . ?
C31 C30 C32 110.6(5) . . ?
C31 C30 C29 110.8(4) . . ?
C32 C30 C29 113.9(4) . . ?
C31 C30 H30 107.0 . . ?
C32 C30 H30 107.0 . . ?
C29 C30 H30 107.0 . . ?
C30 C31 H31A 109.5 . . ?
C30 C31 H31B 109.5 . . ?
H31A C31 H31B 109.5 . . ?
C30 C31 H31C 109.5 . . ?
H31A C31 H31C 109.5 . . ?
H31B C31 H31C 109.5 . . ?
C30 C32 H32A 109.5 . . ?
C30 C32 H32B 109.5 . . ?
H32A C32 H32B 109.5 . . ?
C30 C32 H32C 109.5 . . ?
H32A C32 H32C 109.5 . . ?
H32B C32 H32C 109.5 . . ?
C34 C33 C29 121.9(4) . . ?
C34 C33 H33 119.1 . . ?
C29 C33 H33 119.1 . . ?
C33 C34 C38 119.5(4) . . ?
C33 C34 C35 120.8(4) . . ?
C38 C34 C35 119.7(4) . . ?
C36 C35 C34 110.9(5) . . ?
C36 C35 C37 111.5(5) . . ?
C34 C35 C37 111.3(4) . . ?
C36 C35 H35 107.6 . . ?
C34 C35 H35 107.6 . . ?
C37 C35 H35 107.6 . . ?
C35 C36 H36A 109.5 . . ?
C35 C36 H36B 109.5 . . ?
H36A C36 H36B 109.5 . . ?
C35 C36 H36C 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
C35 C37 H37A 109.5 . . ?
C35 C37 H37B 109.5 . . ?
H37A C37 H37B 109.5 . . ?
C35 C37 H37C 109.5 . . ?
H37A C37 H37C 109.5 . . ?
H37B C37 H37C 109.5 . . ?
C34 C38 C27 120.8(4) . . ?
C34 C38 H38 119.6 . . ?
C27 C38 H38 119.6 . . ?
C40 C39 C50 118.4(4) . . ?
C40 C39 C12 118.1(3) . . ?
C50 C39 C12 123.5(3) . . ?
C39 C40 C41 121.9(4) . . ?
C39 C40 H40 119.1 . . ?
C41 C40 H40 119.1 . . ?
C45 C41 C40 118.0(4) . . ?
C45 C41 C42 120.3(8) . . ?
C40 C41 C42 121.7(8) . . ?
C45 C41 C42' 122.1(14) . . ?
C40 C41 C42' 119.9(14) . . ?
C44 C42 C41 115.1(10) . . ?
C44 C42 C43 96.9(12) . . ?
C41 C42 C43 110.2(9) . . ?
C44 C42 H42 111.3 . . ?
C41 C42 H42 111.3 . . ?
C43 C42 H42 111.3 . . ?
C42 C43 H43A 109.5 . . ?
C42 C43 H43B 109.5 . . ?
H43A C43 H43B 109.5 . . ?
C42 C43 H43C 109.5 . . ?
H43A C43 H43C 109.5 . . ?
H43B C43 H43C 109.5 . . ?
C42 C44 H44A 109.5 . . ?
C42 C44 H44B 109.5 . . ?
H44A C44 H44B 109.5 . . ?
C42 C44 H44C 109.5 . . ?
H44A C44 H44C 109.5 . . ?
H44B C44 H44C 109.5 . . ?
C44' C42' C43' 145.5(15) . . ?
C44' C42' C41 105.1(12) . . ?
C43' C42' C41 108.8(11) . . ?
C44' C42' H42' 92.5 . . ?
C43' C42' H42' 92.5 . . ?
C41 C42' H42' 92.5 . . ?
C42' C43' H43D 109.5 . . ?
C42' C43' H43E 109.5 . . ?
H43D C43' H43E 109.5 . . ?
C42' C43' H43F 109.5 . . ?
H43D C43' H43F 109.5 . . ?
H43E C43' H43F 109.5 . . ?
C42' C44' H44D 109.5 . . ?
C42' C44' H44E 109.5 . . ?
H44D C44' H44E 109.5 . . ?
C42' C44' H44F 109.5 . . ?
H44D C44' H44F 109.5 . . ?
H44E C44' H44F 109.5 . . ?
C41 C45 C46 122.6(4) . . ?
C41 C45 H45 118.7 . . ?
C46 C45 H45 118.7 . . ?
C45 C46 C50 117.4(4) . . ?
C45 C46 C47 121.2(4) . . ?
C50 C46 C47 121.4(4) . . ?
C46 C47 C48 112.4(4) . . ?
C46 C47 C49 110.5(4) . . ?
C48 C47 C49 110.0(4) . . ?
C46 C47 H47 107.9 . . ?
C48 C47 H47 107.9 . . ?
C49 C47 H47 107.9 . . ?
C47 C48 H48A 109.5 . . ?
C47 C48 H48B 109.5 . . ?
H48A C48 H48B 109.5 . . ?
C47 C48 H48C 109.5 . . ?
H48A C48 H48C 109.5 . . ?
H48B C48 H48C 109.5 . . ?
C47 C49 H49A 109.5 . . ?
C47 C49 H49B 109.5 . . ?
H49A C49 H49B 109.5 . . ?
C47 C49 H49C 109.5 . . ?
H49A C49 H49C 109.5 . . ?
H49B C49 H49C 109.5 . . ?
C39 C50 C46 121.7(4) . . ?
C39 C50 H50 119.1 . . ?
C46 C50 H50 119.1 . . ?
C62 C51 C52 118.1(4) . . ?
C62 C51 C13 121.9(4) . . ?
C52 C51 C13 120.0(3) . . ?
C51 C52 C53 121.0(4) . . ?
C51 C52 H52 119.5 . . ?
C53 C52 H52 119.5 . . ?
C57 C53 C52 118.4(5) . . ?
C57 C53 C54 121.9(4) . . ?
C52 C53 C54 119.7(5) . . ?
C55 C54 C56 109.3(6) . . ?
C55 C54 C53 113.0(5) . . ?
C56 C54 C53 111.4(5) . . ?
C55 C54 H54 107.7 . . ?
C56 C54 H54 107.7 . . ?
C53 C54 H54 107.7 . . ?
C54 C55 H55A 109.5 . . ?
C54 C55 H55B 109.5 . . ?
H55A C55 H55B 109.5 . . ?
C54 C55 H55C 109.5 . . ?
H55A C55 H55C 109.5 . . ?
H55B C55 H55C 109.5 . . ?
C54 C56 H56A 109.5 . . ?
C54 C56 H56B 109.5 . . ?
H56A C56 H56B 109.5 . . ?
C54 C56 H56C 109.5 . . ?
H56A C56 H56C 109.5 . . ?
H56B C56 H56C 109.5 . . ?
C58 C57 C53 122.1(4) . . ?
C58 C57 H57 118.9 . . ?
C53 C57 H57 118.9 . . ?
C57 C58 C62 117.9(4) . . ?
C57 C58 C59' 118.4(15) . . ?
C62 C58 C59' 123.7(16) . . ?
C57 C58 C59 122.9(8) . . ?
C62 C58 C59 119.2(8) . . ?
C61 C59 C60 97.6(10) . . ?
C61 C59 C58 109.1(9) . . ?
C60 C59 C58 116.4(10) . . ?
C61 C59 H59 111.0 . . ?
C60 C59 H59 111.0 . . ?
C58 C59 H59 111.0 . . ?
C59 C60 H60A 109.5 . . ?
C59 C60 H60B 109.5 . . ?
H60A C60 H60B 109.5 . . ?
C59 C60 H60C 109.5 . . ?
H60A C60 H60C 109.5 . . ?
H60B C60 H60C 109.5 . . ?
C59 C61 H61A 109.5 . . ?
C59 C61 H61B 109.5 . . ?
H61A C61 H61B 109.5 . . ?
C59 C61 H61C 109.5 . . ?
H61A C61 H61C 109.5 . . ?
H61B C61 H61C 109.5 . . ?
C60' C59' C61' 137.9(18) . . ?
C60' C59' C58 107.0(12) . . ?
C61' C59' C58 111.9(13) . . ?
C60' C59' H59' 95.8 . . ?
C61' C59' H59' 95.8 . . ?
C58 C59' H59' 95.8 . . ?
C59' C60' H60D 109.5 . . ?
C59' C60' H60E 109.5 . . ?
H60D C60' H60E 109.5 . . ?
C59' C60' H60F 109.5 . . ?
H60D C60' H60F 109.5 . . ?
H60E C60' H60F 109.5 . . ?
C59' C61' H61D 109.5 . . ?
C59' C61' H61E 109.5 . . ?
H61D C61' H61E 109.5 . . ?
C59' C61' H61F 109.5 . . ?
H61D C61' H61F 109.5 . . ?
H61E C61' H61F 109.5 . . ?
C51 C62 C58 122.4(4) . . ?
C51 C62 H62 118.8 . . ?
C58 C62 H62 118.8 . . ?
C74 C63 C64 119.0(3) . . ?
C74 C63 C14 123.6(3) . . ?
C64 C63 C14 117.4(3) . . ?
C65 C64 C63 121.7(4) . . ?
C65 C64 H64 119.1 . . ?
C63 C64 H64 119.1 . . ?
C64 C65 C69 117.4(4) . . ?
C64 C65 C66 122.2(15) . . ?
C69 C65 C66 120.3(14) . . ?
C64 C65 C66' 121.5(10) . . ?
C69 C65 C66' 121.1(10) . . ?
C68 C66 C67 131.3(14) . . ?
C68 C66 C65 112.1(11) . . ?
C67 C66 C65 116.6(12) . . ?
C68 C66 H66 91.0 . . ?
C67 C66 H66 91.0 . . ?
C65 C66 H66 91.0 . . ?
C66 C67 H67A 109.5 . . ?
C66 C67 H67B 109.5 . . ?
H67A C67 H67B 109.5 . . ?
C66 C67 H67C 109.5 . . ?
H67A C67 H67C 109.5 . . ?
H67B C67 H67C 109.5 . . ?
C66 C68 H68A 109.5 . . ?
C66 C68 H68B 109.5 . . ?
H68A C68 H68B 109.5 . . ?
C66 C68 H68C 109.5 . . ?
H68A C68 H68C 109.5 . . ?
H68B C68 H68C 109.5 . . ?
C67' C66' C68' 137.5(9) . . ?
C67' C66' C65 109.0(8) . . ?
C68' C66' C65 113.1(8) . . ?
C67' C66' H66' 92.2 . . ?
C68' C66' H66' 92.2 . . ?
C65 C66' H66' 92.2 . . ?
C66' C67' H67D 109.5 . . ?
C66' C67' H67E 109.5 . . ?
H67D C67' H67E 109.5 . . ?
C66' C67' H67F 109.5 . . ?
H67D C67' H67F 109.5 . . ?
H67E C67' H67F 109.5 . . ?
C66' C68' H68D 109.5 . . ?
C66' C68' H68E 109.5 . . ?
H68D C68' H68E 109.5 . . ?
C66' C68' H68F 109.5 . . ?
H68D C68' H68F 109.5 . . ?
H68E C68' H68F 109.5 . . ?
C70 C69 C65 122.3(4) . . ?
C70 C69 H69 118.8 . . ?
C65 C69 H69 118.8 . . ?
C69 C70 C74 118.7(4) . . ?
C69 C70 C71 121.7(4) . . ?
C74 C70 C71 119.6(5) . . ?
C72 C71 C73 113.1(5) . . ?
C72 C71 C70 110.8(5) . . ?
C73 C71 C70 111.7(6) . . ?
C72 C71 H71 107.0 . . ?
C73 C71 H71 107.0 . . ?
C70 C71 H71 107.0 . . ?
C71 C72 H72A 109.5 . . ?
C71 C72 H72B 109.5 . . ?
H72A C72 H72B 109.5 . . ?
C71 C72 H72C 109.5 . . ?
H72A C72 H72C 109.5 . . ?
H72B C72 H72C 109.5 . . ?
C71 C73 H73A 109.5 . . ?
C71 C73 H73B 109.5 . . ?
H73A C73 H73B 109.5 . . ?
C71 C73 H73C 109.5 . . ?
H73A C73 H73C 109.5 . . ?
H73B C73 H73C 109.5 . . ?
C63 C74 C70 120.8(4) . . ?
C63 C74 H74 119.6 . . ?
C70 C74 H74 119.6 . . ?
C2 O1 Sc1 126.1(2) . . ?
C2 O1 Sc1 130.1(2) . 3_575 ?
Sc1 O1 Sc1 101.81(10) . 3_575 ?
O1 Sc1 O1 78.20(10) . 3_575 ?
O1 Sc1 C14 107.81(11) . . ?
O1 Sc1 C14 115.82(11) 3_575 . ?
O1 Sc1 C10 106.81(11) . . ?
O1 Sc1 C10 149.15(11) 3_575 . ?
C14 Sc1 C10 33.34(11) . . ?
O1 Sc1 C13 135.67(11) . . ?
O1 Sc1 C13 100.05(11) 3_575 . ?
C14 Sc1 C13 32.97(11) . . ?
C10 Sc1 C13 54.61(11) . . ?
O1 Sc1 C12 160.43(11) . . ?
O1 Sc1 C12 115.32(11) 3_575 . ?
C14 Sc1 C12 54.31(11) . . ?
C10 Sc1 C12 54.18(11) . . ?
C13 Sc1 C12 32.44(11) . . ?
O1 Sc1 C11 133.28(11) . . ?
O1 Sc1 C11 147.60(11) 3_575 . ?
C14 Sc1 C11 54.42(11) . . ?
C10 Sc1 C11 32.67(11) . . ?
C13 Sc1 C11 53.88(11) . . ?
C12 Sc1 C11 32.35(11) . . ?
O1 Sc1 Sc1 39.12(7) . 3_575 ?
O1 Sc1 Sc1 39.07(7) 3_575 3_575 ?
C14 Sc1 Sc1 118.54(9) . 3_575 ?
C10 Sc1 Sc1 137.70(9) . 3_575 ?
C13 Sc1 Sc1 124.97(9) . 3_575 ?
C12 Sc1 Sc1 151.94(9) . 3_575 ?
C11 Sc1 Sc1 170.30(9) . 3_575 ?
O1 Sc1 H1 92.4(10) . . ?
O1 Sc1 H1 105.4(10) 3_575 . ?
C14 Sc1 H1 136.7(10) . . ?
C10 Sc1 H1 104.8(10) . . ?
C13 Sc1 H1 129.4(10) . . ?
C12 Sc1 H1 97.0(10) . . ?
C11 Sc1 H1 83.7(10) . . ?
Sc1 Sc1 H1 101.5(10) 3_575 . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C2 O1 1.448(4) . ?
C2 C3 1.499(6) . ?
C2 H2A 0.9900 . ?
C2 H2B 0.9900 . ?
C3 C4 1.522(6) . ?
C3 H3A 0.9900 . ?
C3 H3B 0.9900 . ?
C4 C5 1.511(7) . ?
C4 H4A 0.9900 . ?
C4 H4B 0.9900 . ?
C5 H5A 0.9800 . ?
C5 H5B 0.9800 . ?
C5 H5C 0.9800 . ?
C10 C11 1.429(5) . ?
C10 C14 1.437(5) . ?
C10 C15 1.484(5) . ?
C10 Sc1 2.520(3) . ?
C11 C12 1.422(5) . ?
C11 C27 1.485(5) . ?
C11 Sc1 2.559(3) . ?
C12 C13 1.417(5) . ?
C12 C39 1.493(5) . ?
C12 Sc1 2.545(3) . ?
C13 C14 1.424(5) . ?
C13 C51 1.494(5) . ?
C13 Sc1 2.527(3) . ?
C14 C63 1.499(5) . ?
C14 Sc1 2.488(3) . ?
C15 C16 1.392(5) . ?
C15 C26 1.394(5) . ?
C16 C17 1.396(5) . ?
C16 H16 0.9500 . ?
C17 C21 1.372(6) . ?
C17 C18 1.522(6) . ?
C18 C19 1.472(9) . ?
C18 C20 1.503(8) . ?
C18 H18 1.0000 . ?
C19 H19A 0.9800 . ?
C19 H19B 0.9800 . ?
C19 H19C 0.9800 . ?
C20 H20A 0.9800 . ?
C20 H20B 0.9800 . ?
C20 H20C 0.9800 . ?
C21 C22 1.386(7) . ?
C21 H21 0.9500 . ?
C22 C26 1.386(6) . ?
C22 C23 1.526(7) . ?
C23 C24 1.429(10) . ?
C23 C25 1.530(11) . ?
C23 H23 1.0000 . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C25 H25A 0.9800 . ?
C25 H25B 0.9800 . ?
C25 H25C 0.9800 . ?
C26 H26 0.9500 . ?
C27 C38 1.392(5) . ?
C27 C28 1.394(5) . ?
C28 C29 1.392(5) . ?
C28 H28 0.9500 . ?
C29 C33 1.392(6) . ?
C29 C30 1.520(6) . ?
C30 C31 1.500(8) . ?
C30 C32 1.501(7) . ?
C30 H30 1.0000 . ?
C31 H31A 0.9800 . ?
C31 H31B 0.9800 . ?
C31 H31C 0.9800 . ?
C32 H32A 0.9800 . ?
C32 H32B 0.9800 . ?
C32 H32C 0.9800 . ?
C33 C34 1.376(6) . ?
C33 H33 0.9500 . ?
C34 C38 1.379(5) . ?
C34 C35 1.522(6) . ?
C35 C36 1.506(8) . ?
C35 C37 1.540(8) . ?
C35 H35 1.0000 . ?
C36 H36A 0.9800 . ?
C36 H36B 0.9800 . ?
C36 H36C 0.9800 . ?
C37 H37A 0.9800 . ?
C37 H37B 0.9800 . ?
C37 H37C 0.9800 . ?
C38 H38 0.9500 . ?
C39 C40 1.386(5) . ?
C39 C50 1.391(5) . ?
C40 C41 1.394(6) . ?
C40 H40 0.9500 . ?
C41 C45 1.383(6) . ?
C41 C42 1.503(10) . ?
C41 C42' 1.534(14) . ?
C42 C44 1.488(9) . ?
C42 C43 1.511(9) . ?
C42 H42 1.0000 . ?
C43 H43A 0.9800 . ?
C43 H43B 0.9800 . ?
C43 H43C 0.9800 . ?
C44 H44A 0.9800 . ?
C44 H44B 0.9800 . ?
C44 H44C 0.9800 . ?
C42' C44' 1.516(10) . ?
C42' C43' 1.523(10) . ?
C42' H42' 1.0000 . ?
C43' H43D 0.9800 . ?
C43' H43E 0.9800 . ?
C43' H43F 0.9800 . ?
C44' H44D 0.9800 . ?
C44' H44E 0.9800 . ?
C44' H44F 0.9800 . ?
C45 C46 1.393(6) . ?
C45 H45 0.9500 . ?
C46 C50 1.401(5) . ?
C46 C47 1.517(6) . ?
C47 C48 1.519(7) . ?
C47 C49 1.525(7) . ?
C47 H47 1.0000 . ?
C48 H48A 0.9800 . ?
C48 H48B 0.9800 . ?
C48 H48C 0.9800 . ?
C49 H49A 0.9800 . ?
C49 H49B 0.9800 . ?
C49 H49C 0.9800 . ?
C50 H50 0.9500 . ?
C51 C62 1.380(5) . ?
C51 C52 1.390(6) . ?
C52 C53 1.398(6) . ?
C52 H52 0.9500 . ?
C53 C57 1.382(7) . ?
C53 C54 1.529(7) . ?
C54 C55 1.484(9) . ?
C54 C56 1.515(8) . ?
C54 H54 1.0000 . ?
C55 H55A 0.9800 . ?
C55 H55B 0.9800 . ?
C55 H55C 0.9800 . ?
C56 H56A 0.9800 . ?
C56 H56B 0.9800 . ?
C56 H56C 0.9800 . ?
C57 C58 1.376(7) . ?
C57 H57 0.9500 . ?
C58 C62 1.388(6) . ?
C58 C59' 1.511(15) . ?
C58 C59 1.543(10) . ?
C59 C61 1.513(8) . ?
C59 C60 1.515(9) . ?
C59 H59 1.0000 . ?
C60 H60A 0.9800 . ?
C60 H60B 0.9800 . ?
C60 H60C 0.9800 . ?
C61 H61A 0.9800 . ?
C61 H61B 0.9800 . ?
C61 H61C 0.9800 . ?
C59' C60' 1.493(10) . ?
C59' C61' 1.503(9) . ?
C59' H59' 1.0000 . ?
C60' H60D 0.9800 . ?
C60' H60E 0.9800 . ?
C60' H60F 0.9800 . ?
C61' H61D 0.9800 . ?
C61' H61E 0.9800 . ?
C61' H61F 0.9800 . ?
C62 H62 0.9500 . ?
C63 C74 1.383(5) . ?
C63 C64 1.389(5) . ?
C64 C65 1.382(6) . ?
C64 H64 0.9500 . ?
C65 C69 1.401(7) . ?
C65 C66 1.482(14) . ?
C65 C66' 1.535(10) . ?
C66 C68 1.459(10) . ?
C66 C67 1.462(10) . ?
C66 H66 1.0000 . ?
C67 H67A 0.9800 . ?
C67 H67B 0.9800 . ?
C67 H67C 0.9800 . ?
C68 H68A 0.9800 . ?
C68 H68B 0.9800 . ?
C68 H68C 0.9800 . ?
C66' C67' 1.484(9) . ?
C66' C68' 1.486(9) . ?
C66' H66' 1.0000 . ?
C67' H67D 0.9800 . ?
C67' H67E 0.9800 . ?
C67' H67F 0.9800 . ?
C68' H68D 0.9800 . ?
C68' H68E 0.9800 . ?
C68' H68F 0.9800 . ?
C69 C70 1.371(7) . ?
C69 H69 0.9500 . ?
C70 C74 1.391(5) . ?
C70 C71 1.541(8) . ?
C71 C72 1.492(9) . ?
C71 C73 1.540(9) . ?
C71 H71 1.0000 . ?
C72 H72A 0.9800 . ?
C72 H72B 0.9800 . ?
C72 H72C 0.9800 . ?
C73 H73A 0.9800 . ?
C73 H73B 0.9800 . ?
C73 H73C 0.9800 . ?
C74 H74 0.9500 . ?
O1 Sc1 2.057(3) . ?
O1 Sc1 2.060(2) 3_575 ?
Sc1 Sc1 3.1952(14) 3_575 ?
Sc1 H1 2.28(4) . ?
