#------------------------------------------------------------------------------
#$Date: 2021-10-06 16:51:40 +0300 (Wed, 06 Oct 2021) $
#$Revision: 269630 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/12/89/7128912.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7128912
loop_
_publ_author_name
'Wang, Qi-Li-Sha'
'Lin, Yue-Jian'
'Jin, Guo-Xin'
_publ_section_title
;
 Same knot, longer rope: altering ligand geometry provides control over
 nuclearity in self-assembled trefoil knots.
;
_journal_issue                   76
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              9772
_journal_page_last               9775
_journal_paper_doi               10.1039/d1cc03699h
_journal_volume                  57
_journal_year                    2021
_chemical_formula_sum            'C258 H300 F24 N24 O64 Rh8 S8'
_chemical_formula_weight         6296.96
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2016/6
_audit_update_record
;
2021-05-31 deposited with the CCDC.	2021-08-30 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 99.200(5)
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   71.010(4)
_cell_length_b                   16.0851(10)
_cell_length_c                   49.267(2)
_cell_measurement_reflns_used    9216
_cell_measurement_temperature    170(2)
_cell_measurement_theta_max      62.40
_cell_measurement_theta_min      2.37
_cell_volume                     55549(5)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2016/6 (Sheldrick, 2016)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_diffrn_ambient_temperature      170(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54178
_diffrn_reflns_av_R_equivalents  0.1766
_diffrn_reflns_av_unetI/netI     0.1159
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       86
_diffrn_reflns_limit_h_min       -86
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       60
_diffrn_reflns_limit_l_min       -58
_diffrn_reflns_number            414239
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        67.679
_diffrn_reflns_theta_max         70.000
_diffrn_reflns_theta_min         2.039
_exptl_absorpt_coefficient_mu    5.143
_exptl_absorpt_correction_T_max  0.753
_exptl_absorpt_correction_T_min  0.475
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    1.506
_exptl_crystal_description       block
_exptl_crystal_F_000             25856
_exptl_crystal_size_max          0.250
_exptl_crystal_size_mid          0.220
_exptl_crystal_size_min          0.180
_refine_diff_density_max         2.502
_refine_diff_density_min         -1.628
_refine_diff_density_rms         0.110
_refine_ls_extinction_coef       0.000018(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2016/6 (Sheldrick 2016)'
_refine_ls_goodness_of_fit_ref   1.067
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2724
_refine_ls_number_reflns         52659
_refine_ls_number_restraints     134
_refine_ls_restrained_S_all      1.071
_refine_ls_R_factor_all          0.1506
_refine_ls_R_factor_gt           0.1040
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.2000P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2942
_refine_ls_wR_factor_ref         0.3509
_reflns_Friedel_coverage         0.000
_reflns_number_gt                27742
_reflns_number_total             52659
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d1cc03699h2.cif
_cod_data_source_block           platon_sq
_cod_depositor_comments
'Adding full bibliography for 7128912--7128915.cif.'
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               7128912
_shelx_shelxl_version_number     2016/6
_shelx_space_group_comment
; 
The symmetry employed for this shelxl refinement is uniquely defined 
by the following loop, which should always be used as a source of 
symmetry information in preference to the above space-group names. 
They are only intended as comments. 
;
_shelx_estimated_absorpt_t_min   0.360
_shelx_estimated_absorpt_t_max   0.458
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Rh1 Rh 0.30069(2) 0.88369(6) 0.16811(2) 0.1019(2) Uani 1 1 d . . . . .
Rh2 Rh 0.27795(2) 1.16754(6) 0.21953(2) 0.1069(3) Uani 1 1 d . . . . .
Rh3 Rh 0.45528(2) 0.61216(6) 0.58923(2) 0.1027(2) Uani 1 1 d . . . . .
Rh4 Rh 0.44936(2) 0.35456(6) 0.51309(2) 0.0959(2) Uani 1 1 d . . . . .
Rh5 Rh 0.43130(2) 1.15520(6) 0.24636(2) 0.1041(2) Uani 1 1 d . . . . .
Rh6 Rh 0.45247(2) 0.90187(4) 0.18071(2) 0.08504(19) Uani 1 1 d . . . . .
Rh7 Rh 0.31389(2) 0.18594(5) 0.48268(2) 0.0942(2) Uani 1 1 d . . . . .
Rh8 Rh 0.31343(2) 0.50030(6) 0.53000(2) 0.1056(3) Uani 1 1 d . . . . .
N1 N 0.30294(13) 1.0180(6) 0.16574(18) 0.107(2) Uani 1 1 d . . . . .
N2 N 0.29276(11) 0.9203(6) 0.20800(16) 0.093(2) Uani 1 1 d . . . . .
N3 N 0.28355(11) 1.0364(5) 0.22862(17) 0.097(2) Uani 1 1 d . . . . .
N4 N 0.29300(14) 1.1326(7) 0.1865(2) 0.122(3) Uani 1 1 d . . . . .
N5 N 0.44256(12) 0.4909(5) 0.58307(16) 0.095(2) Uani 1 1 d . . . . .
N6 N 0.45684(12) 0.5926(6) 0.54530(18) 0.103(2) Uani 1 1 d . . . . .
N7 N 0.45365(12) 0.4865(6) 0.51451(17) 0.102(2) Uani 1 1 d . . . . .
N8 N 0.44059(10) 0.3854(6) 0.55213(15) 0.092(2) Uani 1 1 d . . . . .
N9 N 0.42593(11) 1.1157(5) 0.20348(18) 0.093(2) Uani 1 1 d . . . . .
N10 N 0.44217(11) 1.0305(6) 0.25048(18) 0.102(2) Uani 1 1 d . . . . .
N11 N 0.45034(10) 0.9260(5) 0.22430(15) 0.0894(19) Uani 1 1 d . . . . .
N12 N 0.43474(10) 1.0109(5) 0.17639(15) 0.0884(18) Uani 1 1 d . . . . .
N13 N 0.30610(12) 0.3125(6) 0.4705(2) 0.108(3) Uani 1 1 d . . . . .
N14 N 0.32776(12) 0.2533(6) 0.51830(16) 0.100(2) Uani 1 1 d . . . . .
N15 N 0.32627(13) 0.3792(6) 0.53860(18) 0.104(2) Uani 1 1 d . . . . .
N16 N 0.30615(11) 0.4418(6) 0.48957(19) 0.101(2) Uani 1 1 d . . . . .
N17 N 0.30461(11) 1.1924(5) 0.24499(18) 0.098(2) Uani 1 1 d . . . . .
N18 N 0.42833(11) 0.6646(5) 0.57632(17) 0.096(2) Uani 1 1 d . . . . .
N19 N 0.42064(10) 0.3744(5) 0.49495(17) 0.093(2) Uani 1 1 d . . . . .
N20 N 0.40376(11) 1.1093(5) 0.25035(17) 0.091(2) Uani 1 1 d . . . . .
N21 N 0.42729(10) 0.8310(4) 0.17930(15) 0.0819(17) Uani 1 1 d . . . . .
N22 N 0.33887(12) 0.1969(5) 0.46391(17) 0.094(2) Uani 1 1 d . . . . .
N23 N 0.33967(11) 0.5388(5) 0.51836(18) 0.0924(19) Uani 1 1 d . . . . .
N24 N 0.32943(11) 0.8799(5) 0.18824(16) 0.0921(19) Uani 1 1 d . . . . .
O1 O 0.35906(11) 1.1661(5) 0.31928(16) 0.112(2) Uani 1 1 d . . . . .
O2 O 0.37251(10) 1.2405(5) 0.28814(16) 0.1075(19) Uani 1 1 d . . . . .
O3 O 0.37377(11) 0.7934(5) 0.51830(16) 0.111(2) Uani 1 1 d . . . . .
O4 O 0.35986(13) 0.7550(6) 0.55292(19) 0.132(3) Uani 1 1 d . . . . .
O5 O 0.35992(9) 0.4604(4) 0.43803(13) 0.0946(16) Uani 1 1 d . . . . .
O6 O 0.34928(9) 0.3974(4) 0.47336(14) 0.0959(17) Uani 1 1 d . . . . .
O7 O 0.34884(9) 0.9657(4) 0.27909(13) 0.0953(16) Uani 1 1 d . . . . .
O8 O 0.33469(9) 1.0269(4) 0.23980(14) 0.0914(15) Uani 1 1 d . . . . .
O9 O 0.37819(9) 0.6559(4) 0.20939(14) 0.0945(16) Uani 1 1 d . . . . .
O10 O 0.36182(10) 0.7027(5) 0.16943(15) 0.1066(19) Uani 1 1 d . . . . .
O11 O 0.38551(11) 0.2935(5) 0.40778(14) 0.1055(19) Uani 1 1 d . . . . .
O12 O 0.40503(12) 0.2211(6) 0.44089(19) 0.126(3) Uani 1 1 d . . . . .
O13 O 0.39213(10) 0.6508(5) 0.47572(16) 0.113(2) Uani 1 1 d . . . . .
O14 O 0.40827(11) 0.5843(5) 0.51200(17) 0.115(2) Uani 1 1 d . . . . .
O15 O 0.38885(8) 0.8277(4) 0.25244(13) 0.0920(16) Uani 1 1 d . . . . .
O16 O 0.39943(9) 0.9165(4) 0.22303(13) 0.0919(15) Uani 1 1 d . . . . .
O17 O 0.40773(14) 0.5909(6) 0.6510(2) 0.141(3) Uani 1 1 d . . . . .
O18 O 0.38800(19) 0.6013(8) 0.6859(2) 0.174(4) Uani 1 1 d . . . . .
O19 O 0.3991(2) 0.4645(7) 0.6709(3) 0.188(5) Uani 1 1 d . . . . .
S1 S 0.39519(6) 0.5508(3) 0.66567(8) 0.1388(11) Uani 1 1 d . . . . .
F1 F 0.36814(16) 0.6138(8) 0.6314(3) 0.182(4) Uani 1 1 d . . . . .
F2 F 0.37863(16) 0.5048(7) 0.6161(2) 0.191(4) Uani 1 1 d . . . . .
F3 F 0.35920(16) 0.5023(8) 0.6470(3) 0.202(4) Uani 1 1 d . . . . .
C1 C 0.29519(14) 1.0500(7) 0.1865(2) 0.100(3) Uani 1 1 d . . . . .
C2 C 0.28979(13) 1.0018(8) 0.2068(2) 0.098(3) Uani 1 1 d . . . . .
C3 C 0.28803(13) 0.8927(6) 0.23234(18) 0.089(2) Uani 1 1 d . . . . .
C4 C 0.28982(13) 0.8180(7) 0.2458(2) 0.096(3) Uani 1 1 d . . . . .
H4 H 0.293835 0.769736 0.237259 0.115 Uiso 1 1 calc R U . . .
C5 C 0.28563(15) 0.8147(8) 0.2723(2) 0.106(3) Uani 1 1 d . . . . .
H5 H 0.286896 0.763389 0.281951 0.127 Uiso 1 1 calc R U . . .
C6 C 0.27952(15) 0.8857(8) 0.2851(2) 0.105(3) Uani 1 1 d . . . . .
H6 H 0.276277 0.880657 0.303039 0.126 Uiso 1 1 calc R U . . .
C7 C 0.27813(15) 0.9627(7) 0.2724(2) 0.101(3) Uani 1 1 d . . . . .
H7 H 0.274434 1.010374 0.281618 0.122 Uiso 1 1 calc R U . . .
C8 C 0.28234(13) 0.9688(7) 0.2452(2) 0.100(3) Uani 1 1 d . . . . .
C9 C 0.3004(2) 1.1561(9) 0.1637(3) 0.120(4) Uani 1 1 d . . . . .
C10 C 0.3019(3) 1.2384(12) 0.1531(4) 0.168(6) Uani 1 1 d . U . . .
H10 H 0.298135 1.286080 0.162307 0.201 Uiso 1 1 calc R U . . .
C11 C 0.3092(4) 1.2444(15) 0.1286(5) 0.209(9) Uani 1 1 d D U . . .
H11 H 0.310355 1.297040 0.120272 0.250 Uiso 1 1 calc R U . . .
C12 C 0.3147(3) 1.1739(16) 0.1167(4) 0.194(8) Uani 1 1 d D U . . .
H12 H 0.319252 1.180385 0.099718 0.233 Uiso 1 1 calc R U . . .
C13 C 0.3144(3) 1.0944(12) 0.1268(3) 0.160(6) Uani 1 1 d . . . . .
H13 H 0.319295 1.047390 0.118635 0.192 Uiso 1 1 calc R U . . .
C14 C 0.3059(2) 1.0904(11) 0.1507(3) 0.140(5) Uani 1 1 d . . . . .
C15 C 0.44632(14) 0.4607(7) 0.5593(2) 0.095(2) Uani 1 1 d . . . . .
C16 C 0.45311(13) 0.5147(7) 0.5400(2) 0.096(3) Uani 1 1 d . . . . .
C17 C 0.45937(14) 0.6246(7) 0.5204(2) 0.104(3) Uani 1 1 d . . . . .
C18 C 0.46357(16) 0.7051(9) 0.5127(3) 0.119(3) Uani 1 1 d . . . . .
H18 H 0.465946 0.747521 0.526243 0.142 Uiso 1 1 calc R U . . .
C19 C 0.4643(2) 0.7229(12) 0.4860(3) 0.144(5) Uani 1 1 d . . . . .
H19 H 0.466264 0.778348 0.480422 0.173 Uiso 1 1 calc R U . . .
C20 C 0.46191(16) 0.6549(11) 0.4659(3) 0.129(5) Uani 1 1 d . . . . .
H20 H 0.462606 0.667113 0.447204 0.155 Uiso 1 1 calc R U . . .
C21 C 0.45873(15) 0.5743(9) 0.4731(2) 0.116(4) Uani 1 1 d . . . . .
H21 H 0.457680 0.529847 0.460239 0.139 Uiso 1 1 calc R U . . .
C22 C 0.45712(14) 0.5624(9) 0.5013(2) 0.107(3) Uani 1 1 d . . . . .
C23 C 0.43161(14) 0.3574(6) 0.57374(18) 0.090(2) Uani 1 1 d . . . . .
C24 C 0.42197(14) 0.2862(7) 0.5779(2) 0.098(3) Uani 1 1 d . . . . .
H24 H 0.421388 0.241406 0.565183 0.117 Uiso 1 1 calc R U . . .
C25 C 0.41282(15) 0.2801(7) 0.6015(2) 0.101(3) Uani 1 1 d . . . . .
H25 H 0.405785 0.231775 0.604560 0.121 Uiso 1 1 calc R U . . .
C26 C 0.41436(16) 0.3464(7) 0.6200(3) 0.109(3) Uani 1 1 d . . . . .
H26 H 0.408292 0.341099 0.635754 0.131 Uiso 1 1 calc R U . . .
C27 C 0.42426(15) 0.4202(7) 0.6169(2) 0.104(3) Uani 1 1 d . . . . .
H27 H 0.425135 0.464141 0.629885 0.125 Uiso 1 1 calc R U . . .
C28 C 0.43288(14) 0.4246(7) 0.5928(2) 0.096(3) Uani 1 1 d . . . . .
C29 C 0.44326(12) 1.0013(7) 0.2253(2) 0.090(2) Uani 1 1 d . . . . .
C30 C 0.43517(11) 1.0432(6) 0.2010(2) 0.088(2) Uani 1 1 d . . . . .
C31 C 0.41821(15) 1.1324(6) 0.1765(2) 0.097(3) Uani 1 1 d . . . . .
C32 C 0.40580(18) 1.1960(7) 0.1646(3) 0.115(3) Uani 1 1 d . . . . .
H32 H 0.401442 1.237370 0.175901 0.137 Uiso 1 1 calc R U . . .
C33 C 0.4003(2) 1.1974(9) 0.1378(3) 0.128(4) Uani 1 1 d . . . . .
H33 H 0.393077 1.242913 0.129500 0.153 Uiso 1 1 calc R U . . .
C34 C 0.4052(2) 1.1330(9) 0.1217(3) 0.126(4) Uani 1 1 d . . . . .
H34 H 0.399902 1.133005 0.102747 0.151 Uiso 1 1 calc R U . . .
C35 C 0.41705(16) 1.0692(8) 0.1315(2) 0.112(3) Uani 1 1 d . . . . .
H35 H 0.420572 1.026849 0.119860 0.134 Uiso 1 1 calc R U . . .
C36 C 0.42372(14) 1.0701(6) 0.1599(2) 0.094(2) Uani 1 1 d . . . . .
C37 C 0.45480(13) 0.8978(7) 0.2507(2) 0.098(3) Uani 1 1 d . . . . .
C38 C 0.46172(14) 0.8250(9) 0.2630(3) 0.117(4) Uani 1 1 d . . . . .
H38 H 0.464910 0.779549 0.252312 0.141 Uiso 1 1 calc R U . . .
C39 C 0.46394(18) 0.8193(11) 0.2911(3) 0.139(5) Uani 1 1 d D . . . .
H39 H 0.469069 0.769725 0.299856 0.167 Uiso 1 1 calc R U . . .
C40 C 0.45892(19) 0.8834(12) 0.3070(3) 0.138(5) Uani 1 1 d D . . . .
H40 H 0.460962 0.877002 0.326411 0.165 Uiso 1 1 calc R U . . .
C41 C 0.45133(17) 0.9539(11) 0.2963(2) 0.126(4) Uani 1 1 d . . . . .
H41 H 0.447267 0.995789 0.307702 0.151 Uiso 1 1 calc R U . . .
C42 C 0.44943(13) 0.9652(9) 0.2668(2) 0.108(3) Uani 1 1 d . . . . .
C43 C 0.31052(13) 0.3604(6) 0.4925(2) 0.086(2) Uani 1 1 d . . . . .
C44 C 0.32121(14) 0.3303(6) 0.5164(2) 0.093(2) Uani 1 1 d . . . . .
C45 C 0.33927(16) 0.2506(7) 0.5445(2) 0.104(3) Uani 1 1 d . . . . .
C46 C 0.34994(18) 0.1878(8) 0.5576(2) 0.113(3) Uani 1 1 d . . . . .
H46 H 0.350234 0.134357 0.549464 0.136 Uiso 1 1 calc R U . . .
C47 C 0.3605(2) 0.2052(10) 0.5835(3) 0.131(4) Uani 1 1 d . . . . .
H47 H 0.368391 0.163462 0.592948 0.158 Uiso 1 1 calc R U . . .
C48 C 0.3594(2) 0.2823(10) 0.5954(2) 0.126(4) Uani 1 1 d . . . . .
H48 H 0.366627 0.291789 0.613100 0.151 Uiso 1 1 calc R U . . .
C49 C 0.34854(19) 0.3456(9) 0.5829(2) 0.117(4) Uani 1 1 d . . . . .
H49 H 0.348332 0.398555 0.591407 0.140 Uiso 1 1 calc R U . . .
C50 C 0.33774(15) 0.3296(7) 0.5573(2) 0.099(3) Uani 1 1 d . . . . .
C51 C 0.29823(13) 0.4486(7) 0.4619(2) 0.097(3) Uani 1 1 d . . . . .
C52 C 0.29231(15) 0.5176(9) 0.4462(3) 0.124(4) Uani 1 1 d . . . . .
H52 H 0.292399 0.571437 0.454214 0.148 Uiso 1 1 calc R U . . .
C53 C 0.28625(17) 0.5054(9) 0.4185(3) 0.128(4) Uani 1 1 d . . . . .
H53 H 0.282158 0.551780 0.407120 0.154 Uiso 1 1 calc R U . . .
C54 C 0.28602(18) 0.4280(10) 0.4070(3) 0.130(4) Uani 1 1 d . . . . .
H54 H 0.281305 0.422076 0.387985 0.156 Uiso 1 1 calc R U . . .
C55 C 0.29235(14) 0.3579(8) 0.4220(2) 0.107(3) Uani 1 1 d . . . . .
H55 H 0.292323 0.304727 0.413565 0.128 Uiso 1 1 calc R U . . .
C56 C 0.29879(13) 0.3687(7) 0.4501(2) 0.096(3) Uani 1 1 d . . . . .
C57 C 0.31952(15) 1.2273(6) 0.2350(2) 0.101(3) Uani 1 1 d . . . . .
H57 H 0.317895 1.246563 0.216528 0.122 Uiso 1 1 calc R U . . .
C58 C 0.33689(14) 1.2349(6) 0.2515(2) 0.092(2) Uani 1 1 d . . . . .
H58 H 0.347178 1.260486 0.244472 0.111 Uiso 1 1 calc R U . . .
C59 C 0.33958(14) 1.2062(6) 0.2778(2) 0.093(2) Uani 1 1 d . . . . .
C60 C 0.32389(15) 1.1706(7) 0.2874(2) 0.099(3) Uani 1 1 d . . . . .
H60 H 0.325313 1.148620 0.305478 0.118 Uiso 1 1 calc R U . . .
C61 C 0.30682(14) 1.1675(7) 0.2710(2) 0.104(3) Uani 1 1 d . . . . .
H61 H 0.296093 1.147033 0.278232 0.125 Uiso 1 1 calc R U . . .
C62 C 0.35893(15) 1.2088(6) 0.2949(2) 0.098(3) Uani 1 1 d . . . . .
C63 C 0.37694(18) 1.1609(9) 0.3377(3) 0.122(4) Uani 1 1 d . . . . .
H63A H 0.381631 1.217272 0.343300 0.146 Uiso 1 1 calc R U . . .
H63B H 0.386627 1.132803 0.328541 0.146 Uiso 1 1 calc R U . . .
C64 C 0.37346(17) 1.1123(7) 0.3622(3) 0.109(3) Uani 1 1 d . . . . .
C65 C 0.3891(2) 1.0897(9) 0.3810(3) 0.139(4) Uani 1 1 d . . . . .
H65 H 0.401367 1.108521 0.378587 0.167 Uiso 1 1 calc R U . . .
C66 C 0.3871(2) 1.0375(9) 0.4045(3) 0.132(4) Uani 1 1 d . . . . .
H66 H 0.398031 1.021586 0.417091 0.158 Uiso 1 1 calc R U . . .
C67 C 0.36909(16) 1.0110(7) 0.4083(2) 0.105(3) Uani 1 1 d . . . . .
C68 C 0.35336(18) 1.0419(8) 0.3899(2) 0.115(3) Uani 1 1 d . . . . .
H68 H 0.340782 1.030070 0.393068 0.138 Uiso 1 1 calc R U . . .
C69 C 0.35599(18) 1.0898(8) 0.3669(2) 0.114(3) Uani 1 1 d . . . . .
H69 H 0.345113 1.106731 0.354280 0.137 Uiso 1 1 calc R U . . .
C70 C 0.36660(19) 0.9620(7) 0.4318(2) 0.109(3) Uani 1 1 d . . . . .
C71 C 0.37869(19) 0.9727(7) 0.4576(3) 0.119(3) Uani 1 1 d . . . . .
H71 H 0.388973 1.011144 0.459315 0.143 Uiso 1 1 calc R U . . .
C72 C 0.3754(2) 0.9268(9) 0.4801(3) 0.130(4) Uani 1 1 d . . . . .
H72 H 0.383632 0.934207 0.497115 0.156 Uiso 1 1 calc R U . . .
C73 C 0.36029(18) 0.8697(8) 0.4788(3) 0.114(3) Uani 1 1 d . . . . .
C74 C 0.35001(19) 0.8588(9) 0.4533(3) 0.128(4) Uani 1 1 d . . . . .
H74 H 0.340720 0.815783 0.451268 0.153 Uiso 1 1 calc R U . . .
C75 C 0.3517(2) 0.9018(8) 0.4311(3) 0.125(4) Uani 1 1 d . . . . .
H75 H 0.342967 0.893027 0.414638 0.151 Uiso 1 1 calc R U . . .
C76 C 0.35704(18) 0.8273(8) 0.5036(3) 0.116(3) Uani 1 1 d . . . . .
H76A H 0.351561 0.867151 0.515528 0.140 Uiso 1 1 calc R U . . .
H76B H 0.347626 0.782264 0.498636 0.140 Uiso 1 1 calc R U . . .
C77 C 0.37387(17) 0.7619(7) 0.5434(2) 0.103(3) Uani 1 1 d . . . . .
C78 C 0.41277(14) 0.6403(6) 0.5862(2) 0.095(2) Uani 1 1 d . . . . .
H78 H 0.413991 0.600770 0.600708 0.114 Uiso 1 1 calc R U . . .
C79 C 0.39451(15) 0.6720(6) 0.5755(2) 0.094(2) Uani 1 1 d . . . . .
H79 H 0.383531 0.653568 0.582574 0.113 Uiso 1 1 calc R U . . .
C80 C 0.39295(14) 0.7297(6) 0.5548(2) 0.096(2) Uani 1 1 d . . . . .
C81 C 0.40902(17) 0.7578(7) 0.5456(2) 0.107(3) Uani 1 1 d . . . . .
H81 H 0.408013 0.799711 0.531887 0.128 Uiso 1 1 calc R U . . .
C82 C 0.42703(17) 0.7248(7) 0.5564(3) 0.113(3) Uani 1 1 d . . . . .
H82 H 0.438174 0.744035 0.550018 0.136 Uiso 1 1 calc R U . . .
C83 C 0.40623(13) 0.3450(6) 0.50724(19) 0.090(2) Uani 1 1 d . . . . .
H83 H 0.409245 0.314396 0.523852 0.108 Uiso 1 1 calc R U . . .
C84 C 0.38732(13) 0.3581(6) 0.49645(19) 0.089(2) Uani 1 1 d . . . . .
H84 H 0.377642 0.334116 0.505214 0.107 Uiso 1 1 calc R U . . .
C85 C 0.38218(13) 0.4063(6) 0.47270(18) 0.086(2) Uani 1 1 d . . . . .
C86 C 0.39711(14) 0.4380(6) 0.4601(2) 0.093(2) Uani 1 1 d . . . . .
H86 H 0.394312 0.469970 0.443750 0.111 Uiso 1 1 calc R U . . .
C87 C 0.41609(15) 0.4225(7) 0.4717(2) 0.099(3) Uani 1 1 d . . . . .
H87 H 0.426062 0.445720 0.463394 0.119 Uiso 1 1 calc R U . . .
C88 C 0.36225(14) 0.4198(5) 0.46154(19) 0.086(2) Uani 1 1 d . . . . .
C89 C 0.34048(14) 0.4777(7) 0.4254(2) 0.103(3) Uani 1 1 d . . . . .
H89A H 0.332995 0.498149 0.439330 0.124 Uiso 1 1 calc R U . . .
H89B H 0.334351 0.426514 0.416984 0.124 Uiso 1 1 calc R U . . .
C90 C 0.34128(13) 0.5430(7) 0.4036(2) 0.094(2) Uani 1 1 d . . . . .
C91 C 0.3296(2) 0.5360(8) 0.3801(3) 0.127(4) Uani 1 1 d . . . . .
H91 H 0.322012 0.487348 0.376967 0.152 Uiso 1 1 calc R U . . .
C92 C 0.32792(19) 0.5975(9) 0.3590(3) 0.129(4) Uani 1 1 d . . . . .
H92 H 0.319321 0.591378 0.342270 0.154 Uiso 1 1 calc R U . . .
C93 C 0.33987(15) 0.6691(7) 0.3645(2) 0.099(3) Uani 1 1 d . . . . .
C94 C 0.3524(2) 0.6720(10) 0.3883(3) 0.136(4) Uani 1 1 d . . . . .
H94 H 0.360918 0.717736 0.391544 0.164 Uiso 1 1 calc R U . . .
C95 C 0.3531(2) 0.6115(10) 0.4077(3) 0.141(5) Uani 1 1 d . . . . .
H95 H 0.361941 0.616423 0.424260 0.169 Uiso 1 1 calc R U . . .
C96 C 0.33858(13) 0.7366(6) 0.3431(2) 0.093(2) Uani 1 1 d . . . . .
C97 C 0.33885(17) 0.8168(7) 0.3510(2) 0.109(3) Uani 1 1 d . . . . .
H97 H 0.340480 0.829509 0.370030 0.130 Uiso 1 1 calc R U . . .
C98 C 0.33675(19) 0.8824(8) 0.3317(3) 0.117(3) Uani 1 1 d . . . . .
H98 H 0.337224 0.938607 0.337620 0.141 Uiso 1 1 calc R U . . .
C99 C 0.33392(13) 0.8625(6) 0.3031(2) 0.092(2) Uani 1 1 d . . . . .
C100 C 0.33358(16) 0.7813(7) 0.2958(2) 0.104(3) Uani 1 1 d . . . . .
H100 H 0.332001 0.767017 0.276908 0.125 Uiso 1 1 calc R U . . .
C101 C 0.33554(15) 0.7167(7) 0.3159(2) 0.104(3) Uani 1 1 d . . . . .
H101 H 0.334728 0.660117 0.310289 0.125 Uiso 1 1 calc R U . . .
C102 C 0.33014(14) 0.9296(7) 0.2829(2) 0.105(3) Uani 1 1 d . . . . .
H10A H 0.322035 0.972739 0.289499 0.126 Uiso 1 1 calc R U . . .
H10B H 0.323410 0.907576 0.265176 0.126 Uiso 1 1 calc R U . . .
C103 C 0.34888(12) 1.0133(5) 0.25658(19) 0.083(2) Uani 1 1 d . . . . .
C104 C 0.38829(12) 1.1249(6) 0.2311(2) 0.088(2) Uani 1 1 d . . . . .
H104 H 0.389812 1.157230 0.215435 0.105 Uiso 1 1 calc R U . . .
C105 C 0.37057(13) 1.0957(6) 0.23352(19) 0.087(2) Uani 1 1 d . . . . .
H105 H 0.359971 1.109160 0.219907 0.104 Uiso 1 1 calc R U . . .
C106 C 0.36797(12) 1.0469(5) 0.25549(17) 0.081(2) Uani 1 1 d . . . . .
C107 C 0.38394(13) 1.0326(6) 0.2754(2) 0.088(2) Uani 1 1 d . . . . .
H107 H 0.382653 1.000551 0.291179 0.106 Uiso 1 1 calc R U . . .
C108 C 0.40115(14) 1.0633(6) 0.27253(19) 0.092(2) Uani 1 1 d . . . . .
H108 H 0.411753 1.052568 0.286450 0.111 Uiso 1 1 calc R U . . .
C109 C 0.41084(11) 0.8491(6) 0.16272(18) 0.083(2) Uani 1 1 d . . . . .
H109 H 0.410604 0.893053 0.149807 0.099 Uiso 1 1 calc R U . . .
C110 C 0.39435(12) 0.8053(6) 0.16401(18) 0.083(2) Uani 1 1 d . . . . .
H110 H 0.382920 0.819490 0.152118 0.100 Uiso 1 1 calc R U . . .
C111 C 0.39437(11) 0.7406(6) 0.18262(17) 0.081(2) Uani 1 1 d . . . . .
C112 C 0.41151(13) 0.7215(6) 0.1991(2) 0.094(2) Uani 1 1 d . . . . .
H112 H 0.412213 0.677132 0.211921 0.113 Uiso 1 1 calc R U . . .
C113 C 0.42728(12) 0.7666(6) 0.1966(2) 0.096(3) Uani 1 1 d . . . . .
H113 H 0.438977 0.751725 0.207774 0.115 Uiso 1 1 calc R U . . .
C114 C 0.37635(13) 0.6985(6) 0.1859(2) 0.094(2) Uani 1 1 d . . . . .
C115 C 0.36191(15) 0.6090(7) 0.2148(3) 0.108(3) Uani 1 1 d . . . . .
H11A H 0.358507 0.565662 0.200592 0.129 Uiso 1 1 calc R U . . .
H11B H 0.350778 0.645943 0.214879 0.129 Uiso 1 1 calc R U . . .
C116 C 0.36774(15) 0.5694(7) 0.2429(2) 0.102(3) Uani 1 1 d . . . . .
C117 C 0.3681(2) 0.4863(8) 0.2466(3) 0.135(5) Uani 1 1 d . . . . .
H117 H 0.364922 0.450540 0.231150 0.163 Uiso 1 1 calc R U . . .
C118 C 0.3730(3) 0.4526(8) 0.2727(3) 0.141(5) Uani 1 1 d . . . . .
H118 H 0.372678 0.393812 0.274576 0.169 Uiso 1 1 calc R U . . .
C119 C 0.37823(16) 0.4985(6) 0.2958(2) 0.101(3) Uani 1 1 d . . . . .
C120 C 0.37724(19) 0.5850(8) 0.2925(3) 0.122(4) Uani 1 1 d . . . . .
H120 H 0.380248 0.620417 0.307999 0.146 Uiso 1 1 calc R U . . .
C121 C 0.37189(19) 0.6184(7) 0.2667(3) 0.123(4) Uani 1 1 d . . . . .
H121 H 0.370958 0.677115 0.264964 0.147 Uiso 1 1 calc R U . . .
C122 C 0.3848(2) 0.4612(7) 0.3233(2) 0.114(3) Uani 1 1 d . . . . .
C123 C 0.4005(3) 0.4066(13) 0.3285(4) 0.168(6) Uani 1 1 d . U . . .
H123 H 0.407703 0.396698 0.314058 0.202 Uiso 1 1 calc R U . . .
C124 C 0.4059(2) 0.3684(13) 0.3525(3) 0.159(5) Uani 1 1 d . U . . .
H124 H 0.417246 0.335878 0.354680 0.190 Uiso 1 1 calc R U . . .
C125 C 0.39630(18) 0.3732(7) 0.3737(3) 0.112(3) Uani 1 1 d . . . . .
C126 C 0.3847(3) 0.4414(14) 0.3734(4) 0.178(7) Uani 1 1 d . U . . .
H126 H 0.381175 0.461430 0.389965 0.214 Uiso 1 1 calc R U . . .
C127 C 0.3781(3) 0.4823(13) 0.3480(4) 0.177(7) Uani 1 1 d . . . . .
H127 H 0.368810 0.525130 0.347572 0.212 Uiso 1 1 calc R U . . .
C128 C 0.40293(18) 0.3239(8) 0.3977(3) 0.118(3) Uani 1 1 d . . . . .
H12A H 0.410804 0.357903 0.411959 0.142 Uiso 1 1 calc R U . . .
H12B H 0.410687 0.276508 0.392951 0.142 Uiso 1 1 calc R U . . .
C129 C 0.38929(18) 0.2432(6) 0.4309(2) 0.100(3) Uani 1 1 d . . . . .
C130 C 0.33717(15) 0.2261(7) 0.4381(2) 0.099(3) Uani 1 1 d . . . . .
H130 H 0.324955 0.238454 0.427946 0.119 Uiso 1 1 calc R U . . .
C131 C 0.35359(15) 0.2379(6) 0.4263(2) 0.098(3) Uani 1 1 d . . . . .
H131 H 0.352459 0.258008 0.407989 0.117 Uiso 1 1 calc R U . . .
C132 C 0.37096(13) 0.2215(6) 0.44044(19) 0.091(2) Uani 1 1 d . . . . .
C133 C 0.37217(16) 0.1877(6) 0.4665(2) 0.096(2) Uani 1 1 d . . . . .
H133 H 0.384192 0.171978 0.476550 0.115 Uiso 1 1 calc R U . . .
C134 C 0.35597(15) 0.1773(6) 0.4776(2) 0.098(3) Uani 1 1 d . . . . .
H134 H 0.356902 0.155286 0.495661 0.117 Uiso 1 1 calc R U . . .
C135 C 0.34040(14) 0.5842(6) 0.4971(2) 0.093(2) Uani 1 1 d . . . . .
H135 H 0.328699 0.600396 0.486213 0.112 Uiso 1 1 calc R U . . .
C136 C 0.35728(15) 0.6110(6) 0.4889(2) 0.101(3) Uani 1 1 d . . . . .
H136 H 0.357180 0.645910 0.473356 0.121 Uiso 1 1 calc R U . . .
C137 C 0.37446(13) 0.5843(6) 0.50469(19) 0.087(2) Uani 1 1 d . . . . .
C138 C 0.37382(12) 0.5360(6) 0.52770(19) 0.090(2) Uani 1 1 d . . . . .
H138 H 0.385203 0.518725 0.539133 0.107 Uiso 1 1 calc R U . . .
C139 C 0.35617(16) 0.5135(6) 0.5336(2) 0.100(3) Uani 1 1 d . . . . .
H139 H 0.355612 0.478821 0.549055 0.120 Uiso 1 1 calc R U . . .
C140 C 0.39362(15) 0.6089(7) 0.4980(2) 0.098(3) Uani 1 1 d . . . . .
C141 C 0.4113(2) 0.6816(12) 0.4685(3) 0.147(5) Uani 1 1 d . . . . .
H14A H 0.415686 0.731966 0.479194 0.177 Uiso 1 1 calc R U . . .
H14B H 0.421228 0.638024 0.472510 0.177 Uiso 1 1 calc R U . . .
C142 C 0.4077(2) 0.7007(10) 0.4385(3) 0.127(4) Uani 1 1 d . . . . .
C143 C 0.4128(2) 0.6380(9) 0.4201(3) 0.129(4) Uani 1 1 d . . . . .
H143 H 0.417137 0.585094 0.427053 0.155 Uiso 1 1 calc R U . . .
C144 C 0.41142(19) 0.6545(9) 0.3929(3) 0.124(4) Uani 1 1 d . . . . .
H144 H 0.415442 0.613579 0.381123 0.149 Uiso 1 1 calc R U . . .
C145 C 0.40427(16) 0.7297(8) 0.3816(2) 0.107(3) Uani 1 1 d . . . . .
C146 C 0.39792(19) 0.7880(10) 0.3989(3) 0.130(4) Uani 1 1 d . . . . .
H146 H 0.391957 0.837767 0.391528 0.156 Uiso 1 1 calc R U . . .
C147 C 0.4004(2) 0.7728(11) 0.4278(3) 0.139(4) Uani 1 1 d . . . . .
H147 H 0.396770 0.814307 0.439649 0.167 Uiso 1 1 calc R U . . .
C148 C 0.40377(14) 0.7479(7) 0.3518(2) 0.100(3) Uani 1 1 d . . . . .
C149 C 0.41876(16) 0.7232(8) 0.3379(3) 0.113(3) Uani 1 1 d . . . . .
H149 H 0.428630 0.689782 0.347670 0.136 Uiso 1 1 calc R U . . .
C150 C 0.42000(15) 0.7437(7) 0.3119(2) 0.103(3) Uani 1 1 d . . . . .
H150 H 0.430600 0.726333 0.303731 0.124 Uiso 1 1 calc R U . . .
C151 C 0.40541(13) 0.7913(6) 0.2969(2) 0.092(2) Uani 1 1 d . . . . .
C152 C 0.39037(16) 0.8135(7) 0.3094(2) 0.104(3) Uani 1 1 d . . . . .
H152 H 0.380116 0.843889 0.299195 0.125 Uiso 1 1 calc R U . . .
C153 C 0.38965(16) 0.7928(7) 0.3367(2) 0.106(3) Uani 1 1 d . . . . .
H153 H 0.379078 0.810357 0.344827 0.127 Uiso 1 1 calc R U . . .
C154 C 0.40766(13) 0.8224(7) 0.26903(19) 0.093(2) Uani 1 1 d . . . . .
H15A H 0.413778 0.877850 0.270537 0.111 Uiso 1 1 calc R U . . .
H15B H 0.415816 0.783895 0.260376 0.111 Uiso 1 1 calc R U . . .
C155 C 0.38707(12) 0.8765(5) 0.23007(18) 0.080(2) Uani 1 1 d . . . . .
C156 C 0.34301(14) 0.9243(6) 0.17912(18) 0.092(2) Uani 1 1 d . . . . .
H156 H 0.339610 0.956702 0.162960 0.110 Uiso 1 1 calc R U . . .
C157 C 0.36184(14) 0.9254(6) 0.19209(19) 0.090(2) Uani 1 1 d . . . . .
H157 H 0.371147 0.958218 0.185175 0.108 Uiso 1 1 calc R U . . .
C158 C 0.36669(12) 0.8765(5) 0.21577(17) 0.0804(19) Uani 1 1 d . . . . .
C159 C 0.35273(12) 0.8304(6) 0.22474(19) 0.087(2) Uani 1 1 d . . . . .
H159 H 0.355601 0.796508 0.240665 0.105 Uiso 1 1 calc R U . . .
C160 C 0.33445(14) 0.8337(6) 0.21034(19) 0.093(2) Uani 1 1 d . . . . .
H160 H 0.324914 0.800853 0.216680 0.111 Uiso 1 1 calc R U . . .
C161 C 0.3016(2) 0.8186(9) 0.1302(2) 0.120(4) Uani 1 1 d . . . . .
C162 C 0.29932(15) 0.7611(9) 0.1504(2) 0.115(3) Uani 1 1 d . . . . .
C163 C 0.28263(17) 0.7761(10) 0.1614(3) 0.122(4) Uani 1 1 d . . . . .
C164 C 0.27365(18) 0.8436(12) 0.1470(3) 0.143(5) Uani 1 1 d . . . . .
C165 C 0.2859(3) 0.8728(10) 0.1270(3) 0.148(6) Uani 1 1 d . . . . .
C166 C 0.3176(3) 0.8268(13) 0.1133(3) 0.175(7) Uani 1 1 d . . . . .
H16A H 0.328540 0.793729 0.121793 0.263 Uiso 1 1 calc R U . . .
H16B H 0.321323 0.885314 0.112672 0.263 Uiso 1 1 calc R U . . .
H16C H 0.313175 0.806710 0.094604 0.263 Uiso 1 1 calc R U . . .
C167 C 0.3126(2) 0.6907(9) 0.1598(3) 0.140(4) Uani 1 1 d . . . . .
H16D H 0.307939 0.639833 0.150053 0.210 Uiso 1 1 calc R U . . .
H16E H 0.313125 0.682465 0.179655 0.210 Uiso 1 1 calc R U . . .
H16F H 0.325366 0.703840 0.155960 0.210 Uiso 1 1 calc R U . . .
C168 C 0.2742(2) 0.7259(12) 0.1810(4) 0.162(6) Uani 1 1 d . . . . .
H16G H 0.265630 0.760495 0.189991 0.244 Uiso 1 1 calc R U . . .
H16H H 0.284301 0.703268 0.194906 0.244 Uiso 1 1 calc R U . . .
H16I H 0.266910 0.680032 0.171268 0.244 Uiso 1 1 calc R U . . .
C169 C 0.2546(3) 0.8824(14) 0.1516(5) 0.216(11) Uani 1 1 d . . . . .
H16J H 0.244346 0.862508 0.137418 0.325 Uiso 1 1 calc R U . . .
H16K H 0.255460 0.943073 0.150620 0.325 Uiso 1 1 calc R U . . .
H16L H 0.251883 0.866234 0.169793 0.325 Uiso 1 1 calc R U . . .
C170 C 0.2805(4) 0.9362(14) 0.1075(4) 0.214(10) Uani 1 1 d . . . . .
H17A H 0.291943 0.960550 0.101966 0.322 Uiso 1 1 calc R U . . .
H17B H 0.273422 0.979305 0.115677 0.322 Uiso 1 1 calc R U . . .
H17C H 0.272398 0.912631 0.091375 0.322 Uiso 1 1 calc R U . . .
C171 C 0.2535(2) 1.2214(13) 0.1935(4) 0.146(5) Uani 1 1 d . . . . .
C172 C 0.24715(15) 1.1584(8) 0.2084(3) 0.119(4) Uani 1 1 d . . . . .
C173 C 0.25216(16) 1.1823(8) 0.2373(3) 0.117(4) Uani 1 1 d . . . . .
C174 C 0.26174(16) 1.2610(8) 0.2388(3) 0.116(3) Uani 1 1 d . . . . .
C175 C 0.26354(18) 1.2837(9) 0.2120(4) 0.135(5) Uani 1 1 d . . . . .
C176 C 0.2525(3) 1.2294(16) 0.1616(5) 0.208(10) Uani 1 1 d . . . . .
H17D H 0.245918 1.281082 0.155213 0.312 Uiso 1 1 calc R U . . .
H17E H 0.245510 1.181939 0.152464 0.312 Uiso 1 1 calc R U . . .
H17F H 0.265463 1.230292 0.157093 0.312 Uiso 1 1 calc R U . . .
C177 C 0.23756(19) 1.0814(12) 0.1978(5) 0.180(8) Uani 1 1 d . . . . .
H17G H 0.223743 1.090500 0.194117 0.271 Uiso 1 1 calc R U . . .
H17H H 0.240535 1.037034 0.211389 0.271 Uiso 1 1 calc R U . . .
H17I H 0.242017 1.065387 0.180667 0.271 Uiso 1 1 calc R U . . .
C178 C 0.24676(19) 1.1357(9) 0.2608(4) 0.149(5) Uani 1 1 d . . . . .
H17J H 0.255646 1.149226 0.277513 0.224 Uiso 1 1 calc R U . . .
H17K H 0.247285 1.075897 0.257135 0.224 Uiso 1 1 calc R U . . .
H17L H 0.233778 1.151060 0.263164 0.224 Uiso 1 1 calc R U . . .
C179 C 0.2680(2) 1.3094(10) 0.2644(4) 0.163(6) Uani 1 1 d . . . . .
H17M H 0.279195 1.342939 0.262287 0.244 Uiso 1 1 calc R U . . .
H17N H 0.271323 1.270994 0.279914 0.244 Uiso 1 1 calc R U . . .
H17O H 0.257638 1.345945 0.267973 0.244 Uiso 1 1 calc R U . . .
C180 C 0.2713(3) 1.3653(11) 0.2048(5) 0.182(8) Uani 1 1 d . . . . .
H18A H 0.262089 1.409314 0.206926 0.273 Uiso 1 1 calc R U . . .
H18B H 0.273616 1.364025 0.185759 0.273 Uiso 1 1 calc R U . . .
H18C H 0.283310 1.376417 0.217122 0.273 Uiso 1 1 calc R U . . .
C181 C 0.46574(18) 0.6067(9) 0.6323(2) 0.115(3) Uani 1 1 d . . . . .
C182 C 0.48001(17) 0.5769(9) 0.6175(3) 0.124(4) Uani 1 1 d D . . . .
C183 C 0.48479(17) 0.6452(11) 0.6003(3) 0.141(5) Uani 1 1 d D U . . .
C184 C 0.47213(19) 0.7144(9) 0.6057(3) 0.126(4) Uani 1 1 d . . . . .
C185 C 0.46207(19) 0.6885(9) 0.6261(3) 0.121(4) Uani 1 1 d . . . . .
C186 C 0.4587(3) 0.5586(13) 0.6531(4) 0.176(7) Uani 1 1 d . . . . .
H18D H 0.468150 0.559147 0.669984 0.264 Uiso 1 1 calc R U . . .
H18E H 0.456517 0.501203 0.646729 0.264 Uiso 1 1 calc R U . . .
H18F H 0.446724 0.582663 0.656869 0.264 Uiso 1 1 calc R U . . .
C187 C 0.4881(3) 0.4956(14) 0.6179(4) 0.197(9) Uani 1 1 d . . . . .
H18G H 0.502043 0.500053 0.619599 0.295 Uiso 1 1 calc R U . . .
H18H H 0.483082 0.466547 0.600818 0.295 Uiso 1 1 calc R U . . .
H18I H 0.484873 0.464375 0.633606 0.295 Uiso 1 1 calc R U . . .
C188 C 0.4995(3) 0.6435(13) 0.5822(4) 0.177(6) Uani 1 1 d . U . . .
H18J H 0.496753 0.686852 0.568152 0.266 Uiso 1 1 calc R U . . .
H18K H 0.499419 0.589014 0.573283 0.266 Uiso 1 1 calc R U . . .
H18L H 0.512051 0.653499 0.593190 0.266 Uiso 1 1 calc R U . . .
C189 C 0.4715(3) 0.8019(11) 0.5932(3) 0.167(6) Uani 1 1 d . . . . .
H18M H 0.467264 0.798334 0.573271 0.251 Uiso 1 1 calc R U . . .
H18N H 0.484227 0.826802 0.596834 0.251 Uiso 1 1 calc R U . . .
H18O H 0.462525 0.836442 0.601417 0.251 Uiso 1 1 calc R U . . .
C190 C 0.4474(2) 0.7435(11) 0.6368(3) 0.155(5) Uani 1 1 d . . . . .
H19A H 0.437159 0.708934 0.641764 0.232 Uiso 1 1 calc R U . . .
H19B H 0.442131 0.783063 0.622432 0.232 Uiso 1 1 calc R U . . .
H19C H 0.453596 0.774095 0.653011 0.232 Uiso 1 1 calc R U . . .
C191 C 0.45265(15) 0.2423(11) 0.5033(2) 0.136(5) Uani 1 1 d D U . . .
C192 C 0.46021(16) 0.2848(8) 0.4821(2) 0.108(3) Uani 1 1 d D . . . .
C193 C 0.47540(16) 0.3311(9) 0.4965(2) 0.115(4) Uani 1 1 d . . . . .
C194 C 0.47784(16) 0.3099(10) 0.5259(3) 0.125(4) Uani 1 1 d . . . . .
C195 C 0.46430(17) 0.2402(8) 0.5270(3) 0.117(4) Uani 1 1 d . . . . .
C196 C 0.4394(2) 0.1705(10) 0.4953(3) 0.174(8) Uani 1 1 d D U . . .
H19D H 0.443801 0.138798 0.480533 0.261 Uiso 1 1 calc R U . . .
H19E H 0.426486 0.191496 0.488878 0.261 Uiso 1 1 calc R U . . .
H19F H 0.439204 0.134235 0.511256 0.261 Uiso 1 1 calc R U . . .
C197 C 0.4530(2) 0.2880(10) 0.4508(2) 0.136(4) Uani 1 1 d . . . . .
H19G H 0.449629 0.345358 0.445310 0.203 Uiso 1 1 calc R U . . .
H19H H 0.441746 0.252383 0.446299 0.203 Uiso 1 1 calc R U . . .
H19I H 0.463087 0.268335 0.440918 0.203 Uiso 1 1 calc R U . . .
C198 C 0.4868(2) 0.3968(11) 0.4849(4) 0.160(6) Uani 1 1 d . . . . .
H19J H 0.500330 0.381053 0.487954 0.241 Uiso 1 1 calc R U . . .
H19K H 0.485278 0.450010 0.493953 0.241 Uiso 1 1 calc R U . . .
H19L H 0.482326 0.402318 0.465076 0.241 Uiso 1 1 calc R U . . .
C199 C 0.49161(17) 0.3391(12) 0.5485(3) 0.150(5) Uani 1 1 d . . . . .
H19M H 0.485753 0.341094 0.565193 0.225 Uiso 1 1 calc R U . . .
H19N H 0.495905 0.394926 0.544347 0.225 Uiso 1 1 calc R U . . .
H19O H 0.502562 0.301244 0.551351 0.225 Uiso 1 1 calc R U . . .
C200 C 0.4626(2) 0.1948(10) 0.5534(3) 0.140(5) Uani 1 1 d . . . . .
H20A H 0.451425 0.158093 0.550272 0.209 Uiso 1 1 calc R U . . .
H20B H 0.461065 0.235265 0.567732 0.209 Uiso 1 1 calc R U . . .
H20C H 0.474097 0.161719 0.559127 0.209 Uiso 1 1 calc R U . . .
C201 C 0.42760(18) 1.2831(7) 0.2560(3) 0.112(3) Uani 1 1 d . . . . .
C202 C 0.4346(2) 1.2408(9) 0.2806(3) 0.128(4) Uani 1 1 d . . . . .
C203 C 0.4535(3) 1.2047(12) 0.2794(4) 0.166(7) Uani 1 1 d D . . . .
C204 C 0.4565(2) 1.2286(11) 0.2540(5) 0.156(6) Uani 1 1 d D . . . .
C205 C 0.4417(2) 1.2753(8) 0.2383(3) 0.136(5) Uani 1 1 d . . . . .
C206 C 0.4092(2) 1.3305(8) 0.2509(3) 0.135(5) Uani 1 1 d . . . . .
H20D H 0.398822 1.295099 0.255227 0.203 Uiso 1 1 calc R U . . .
H20E H 0.406459 1.347415 0.231583 0.203 Uiso 1 1 calc R U . . .
H20F H 0.410227 1.380019 0.262669 0.203 Uiso 1 1 calc R U . . .
C207 C 0.4245(3) 1.2335(10) 0.3047(3) 0.154(6) Uani 1 1 d . . . . .
H20G H 0.411584 1.256575 0.300021 0.231 Uiso 1 1 calc R U . . .
H20H H 0.431512 1.264354 0.320257 0.231 Uiso 1 1 calc R U . . .
H20I H 0.423653 1.174836 0.309734 0.231 Uiso 1 1 calc R U . . .
C208 C 0.4656(3) 1.1520(15) 0.3007(5) 0.248(13) Uani 1 1 d D U . . .
H20J H 0.473772 1.115542 0.291642 0.372 Uiso 1 1 calc R U . . .
H20K H 0.457371 1.118148 0.310442 0.372 Uiso 1 1 calc R U . . .
H20L H 0.473623 1.188018 0.313860 0.372 Uiso 1 1 calc R U . . .
C209 C 0.4737(3) 1.2044(19) 0.2403(7) 0.284(14) Uani 1 1 d D U . . .
H20M H 0.474993 1.243896 0.225605 0.426 Uiso 1 1 calc R U . . .
H20N H 0.471809 1.148276 0.232617 0.426 Uiso 1 1 calc R U . . .
H20O H 0.485354 1.205400 0.254066 0.426 Uiso 1 1 calc R U . . .
C210 C 0.4394(3) 1.3185(11) 0.2113(4) 0.188(8) Uani 1 1 d . U . . .
H21A H 0.438600 1.378587 0.214069 0.281 Uiso 1 1 calc R U . . .
H21B H 0.427792 1.298965 0.199623 0.281 Uiso 1 1 calc R U . . .
H21C H 0.450490 1.306239 0.202283 0.281 Uiso 1 1 calc R U . . .
C211 C 0.48278(12) 0.9182(7) 0.1859(2) 0.098(3) Uani 1 1 d . . . . .
C212 C 0.47838(13) 0.8328(6) 0.1839(2) 0.099(3) Uani 1 1 d . . . . .
C213 C 0.46750(14) 0.8149(7) 0.1590(3) 0.109(3) Uani 1 1 d . . . . .
C214 C 0.46443(16) 0.8927(9) 0.1436(3) 0.119(4) Uani 1 1 d . . . . .
C215 C 0.47466(15) 0.9560(7) 0.1609(3) 0.111(3) Uani 1 1 d . . . . .
C216 C 0.49458(16) 0.9622(9) 0.2094(3) 0.130(4) Uani 1 1 d . . . . .
H21D H 0.507590 0.969351 0.205479 0.195 Uiso 1 1 calc R U . . .
H21E H 0.494890 0.929380 0.226182 0.195 Uiso 1 1 calc R U . . .
H21F H 0.488983 1.016878 0.211844 0.195 Uiso 1 1 calc R U . . .
C217 C 0.48629(19) 0.7713(9) 0.2059(3) 0.141(5) Uani 1 1 d . . . . .
H21G H 0.476975 0.726726 0.206714 0.212 Uiso 1 1 calc R U . . .
H21H H 0.488878 0.799519 0.223722 0.212 Uiso 1 1 calc R U . . .
H21I H 0.498150 0.747481 0.201519 0.212 Uiso 1 1 calc R U . . .
C218 C 0.46082(19) 0.7336(10) 0.1486(4) 0.156(6) Uani 1 1 d . . . . .
H21J H 0.470731 0.706704 0.139971 0.234 Uiso 1 1 calc R U . . .
H21K H 0.449239 0.740257 0.135033 0.234 Uiso 1 1 calc R U . . .
H21L H 0.457992 0.699120 0.163876 0.234 Uiso 1 1 calc R U . . .
C219 C 0.4543(2) 0.9063(15) 0.1146(3) 0.180(7) Uani 1 1 d . U . . .
H21M H 0.447629 0.959880 0.113528 0.271 Uiso 1 1 calc R U . . .
H21N H 0.445034 0.861569 0.109577 0.271 Uiso 1 1 calc R U . . .
H21O H 0.463628 0.906391 0.101984 0.271 Uiso 1 1 calc R U . . .
C220 C 0.4749(2) 1.0455(9) 0.1533(4) 0.163(6) Uani 1 1 d . U . . .
H22A H 0.462172 1.069224 0.152901 0.244 Uiso 1 1 calc R U . . .
H22B H 0.478733 1.051017 0.135162 0.244 Uiso 1 1 calc R U . . .
H22C H 0.484060 1.075191 0.166974 0.244 Uiso 1 1 calc R U . . .
C221 C 0.28576(15) 0.1482(7) 0.4887(2) 0.101(3) Uani 1 1 d . . . . .
C222 C 0.28870(17) 0.1239(7) 0.4609(2) 0.107(3) Uani 1 1 d . . . . .
C223 C 0.30407(18) 0.0696(7) 0.4627(3) 0.117(3) Uani 1 1 d . . . . .
C224 C 0.31171(17) 0.0566(7) 0.4921(2) 0.108(3) Uani 1 1 d . . . . .
C225 C 0.29957(16) 0.1032(7) 0.5075(2) 0.106(3) Uani 1 1 d . . . . .
C226 C 0.27071(15) 0.2039(8) 0.4960(3) 0.116(3) Uani 1 1 d . . . . .
H22D H 0.262919 0.173656 0.507416 0.174 Uiso 1 1 calc R U . . .
H22E H 0.262605 0.222913 0.479125 0.174 Uiso 1 1 calc R U . . .
H22F H 0.276639 0.252013 0.506153 0.174 Uiso 1 1 calc R U . . .
C227 C 0.27697(18) 0.1527(9) 0.4350(3) 0.129(4) Uani 1 1 d . . . . .
H22G H 0.283928 0.143248 0.419667 0.193 Uiso 1 1 calc R U . . .
H22H H 0.274279 0.212167 0.436426 0.193 Uiso 1 1 calc R U . . .
H22I H 0.264935 0.121684 0.431883 0.193 Uiso 1 1 calc R U . . .
C228 C 0.3121(2) 0.0344(9) 0.4396(3) 0.138(5) Uani 1 1 d . . . . .
H22J H 0.307834 -0.023301 0.436587 0.208 Uiso 1 1 calc R U . . .
H22K H 0.326057 0.035940 0.443759 0.208 Uiso 1 1 calc R U . . .
H22L H 0.307769 0.067031 0.422959 0.208 Uiso 1 1 calc R U . . .
C229 C 0.3270(2) -0.0009(8) 0.5032(4) 0.141(5) Uani 1 1 d . . . . .
H22M H 0.333679 0.020514 0.520731 0.212 Uiso 1 1 calc R U . . .
H22N H 0.336003 -0.006181 0.490150 0.212 Uiso 1 1 calc R U . . .
H22O H 0.321520 -0.055478 0.506086 0.212 Uiso 1 1 calc R U . . .
C230 C 0.30162(19) 0.1071(8) 0.5381(2) 0.116(3) Uani 1 1 d . . . . .
H23A H 0.296891 0.160836 0.543603 0.175 Uiso 1 1 calc R U . . .
H23B H 0.315093 0.100998 0.546120 0.175 Uiso 1 1 calc R U . . .
H23C H 0.294210 0.062176 0.544724 0.175 Uiso 1 1 calc R U . . .
C231 C 0.30125(17) 0.5039(7) 0.5674(2) 0.179(7) Uani 1 1 d G U . . .
C232 C 0.31297(12) 0.5750(8) 0.5664(2) 0.144(5) Uani 1 1 d G . . . .
C233 C 0.30523(13) 0.6225(5) 0.5430(3) 0.129(4) Uani 1 1 d G . . . .
C234 C 0.28872(11) 0.5808(6) 0.5295(2) 0.127(4) Uani 1 1 d G U . . .
C235 C 0.28625(13) 0.5075(5) 0.5446(2) 0.137(4) Uani 1 1 d DG U . . .
C236 C 0.3010(3) 0.4274(14) 0.5861(4) 0.177(7) Uani 1 1 d . . . . .
H23D H 0.307073 0.441253 0.604771 0.265 Uiso 1 1 calc R U . . .
H23E H 0.307892 0.381602 0.578989 0.265 Uiso 1 1 calc R U . . .
H23F H 0.287725 0.410479 0.586299 0.265 Uiso 1 1 calc R U . . .
C237 C 0.3293(3) 0.5912(14) 0.5881(5) 0.205(10) Uani 1 1 d . . . . .
H23G H 0.336759 0.637641 0.582665 0.307 Uiso 1 1 calc R U . . .
H23H H 0.337313 0.541416 0.591010 0.307 Uiso 1 1 calc R U . . .
H23I H 0.324615 0.605216 0.605254 0.307 Uiso 1 1 calc R U . . .
C238 C 0.3127(2) 0.7048(9) 0.5346(4) 0.165(7) Uani 1 1 d . . . . .
H23J H 0.317994 0.697798 0.517579 0.248 Uiso 1 1 calc R U . . .
H23K H 0.322612 0.725034 0.549186 0.248 Uiso 1 1 calc R U . . .
H23L H 0.302184 0.745146 0.531546 0.248 Uiso 1 1 calc R U . . .
C239 C 0.2756(2) 0.6146(12) 0.5045(4) 0.172(7) Uani 1 1 d . . . . .
H23M H 0.264417 0.640579 0.510427 0.258 Uiso 1 1 calc R U . . .
H23N H 0.271399 0.568910 0.491814 0.258 Uiso 1 1 calc R U . . .
H23O H 0.282428 0.655977 0.495261 0.258 Uiso 1 1 calc R U . . .
C240 C 0.26994(19) 0.4446(11) 0.5347(4) 0.175(7) Uani 1 1 d D U . . .
H24A H 0.257685 0.468661 0.537288 0.263 Uiso 1 1 calc R U . . .
H24B H 0.272158 0.393072 0.545320 0.263 Uiso 1 1 calc R U . . .
H24C H 0.269719 0.432404 0.515124 0.263 Uiso 1 1 calc R U . . .
C241 C 0.3743(2) 0.5471(10) 0.6394(3) 0.125(4) Uani 1 1 d . . . . .
O41 O 0.27201(18) 0.7559(9) 0.0714(3) 0.179(4) Uani 1 1 d . . . . .
O42 O 0.24953(15) 0.8913(9) 0.0471(3) 0.184(5) Uani 1 1 d . U . . .
O43 O 0.2595(2) 0.6606(12) 0.1138(3) 0.218(7) Uani 1 1 d . U . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rh Rh 0.0927 3.6045 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N24 Rh1 C164 160.6(6) . . ?
N24 Rh1 C165 137.1(6) . . ?
C164 Rh1 C165 40.9(7) . . ?
N24 Rh1 C163 123.7(4) . . ?
C164 Rh1 C163 38.0(6) . . ?
C165 Rh1 C163 66.2(6) . . ?
N24 Rh1 C162 98.1(4) . . ?
C164 Rh1 C162 63.0(5) . . ?
C165 Rh1 C162 63.7(5) . . ?
C163 Rh1 C162 38.0(5) . . ?
N24 Rh1 C161 103.4(4) . . ?
C164 Rh1 C161 65.1(5) . . ?
C165 Rh1 C161 38.3(6) . . ?
C163 Rh1 C161 64.9(5) . . ?
C162 Rh1 C161 37.7(5) . . ?
N24 Rh1 N1 88.8(3) . . ?
C164 Rh1 N1 110.1(6) . . ?
C165 Rh1 N1 93.5(5) . . ?
C163 Rh1 N1 147.2(4) . . ?
C162 Rh1 N1 152.8(4) . . ?
C161 Rh1 N1 115.1(4) . . ?
N24 Rh1 N2 87.4(3) . . ?
C164 Rh1 N2 100.1(4) . . ?
C165 Rh1 N2 135.1(6) . . ?
C163 Rh1 N2 96.9(4) . . ?
C162 Rh1 N2 127.1(4) . . ?
C161 Rh1 N2 161.7(4) . . ?
N1 Rh1 N2 79.3(3) . . ?
N17 Rh2 C175 107.1(5) . . ?
N17 Rh2 N4 89.5(4) . . ?
C175 Rh2 N4 112.2(6) . . ?
N17 Rh2 C173 118.0(4) . . ?
C175 Rh2 C173 64.0(5) . . ?
N4 Rh2 C173 152.4(5) . . ?
N17 Rh2 C171 145.5(6) . . ?
C175 Rh2 C171 39.7(6) . . ?
N4 Rh2 C171 96.0(5) . . ?
C173 Rh2 C171 63.1(6) . . ?
N17 Rh2 C172 157.4(5) . . ?
C175 Rh2 C172 65.2(5) . . ?
N4 Rh2 C172 113.0(5) . . ?
C173 Rh2 C172 39.4(5) . . ?
C171 Rh2 C172 36.8(6) . . ?
N17 Rh2 N3 86.8(3) . . ?
C175 Rh2 N3 161.7(4) . . ?
N4 Rh2 N3 78.9(3) . . ?
C173 Rh2 N3 99.3(4) . . ?
C171 Rh2 N3 127.6(6) . . ?
C172 Rh2 N3 97.4(4) . . ?
N17 Rh2 C174 95.5(4) . . ?
C175 Rh2 C174 37.5(5) . . ?
N4 Rh2 C174 149.2(5) . . ?
C173 Rh2 C174 38.3(5) . . ?
C171 Rh2 C174 63.7(6) . . ?
C172 Rh2 C174 65.1(5) . . ?
N3 Rh2 C174 131.6(4) . . ?
N18 Rh3 C184 103.7(5) . . ?
N18 Rh3 C181 118.3(4) . . ?
C184 Rh3 C181 64.3(5) . . ?
N18 Rh3 C182 157.0(4) . . ?
C184 Rh3 C182 66.5(6) . . ?
C181 Rh3 C182 38.9(5) . . ?
N18 Rh3 C183 141.7(5) . . ?
C184 Rh3 C183 40.7(6) . . ?
C181 Rh3 C183 65.7(5) . . ?
C182 Rh3 C183 39.9(4) . . ?
N18 Rh3 N5 88.8(3) . . ?
C184 Rh3 N5 163.2(5) . . ?
C181 Rh3 N5 100.0(4) . . ?
C182 Rh3 N5 97.7(5) . . ?
C183 Rh3 N5 129.2(5) . . ?
N18 Rh3 C185 95.5(5) . . ?
C184 Rh3 C185 37.6(5) . . ?
C181 Rh3 C185 36.9(5) . . ?
C182 Rh3 C185 63.7(5) . . ?
C183 Rh3 C185 64.7(5) . . ?
N5 Rh3 C185 131.3(4) . . ?
N18 Rh3 N6 86.9(3) . . ?
C184 Rh3 N6 111.9(4) . . ?
C181 Rh3 N6 154.8(4) . . ?
C182 Rh3 N6 115.9(4) . . ?
C183 Rh3 N6 94.8(4) . . ?
N5 Rh3 N6 79.5(3) . . ?
C185 Rh3 N6 149.1(4) . . ?
C191 Rh4 N19 100.7(4) . . ?
C191 Rh4 C192 40.9(4) . . ?
N19 Rh4 C192 102.2(4) . . ?
C191 Rh4 N7 158.5(4) . . ?
N19 Rh4 N7 89.2(3) . . ?
C192 Rh4 N7 118.6(4) . . ?
C191 Rh4 C194 66.8(5) . . ?
N19 Rh4 C194 167.2(5) . . ?
C192 Rh4 C194 66.6(5) . . ?
N7 Rh4 C194 101.5(5) . . ?
C191 Rh4 C193 65.9(5) . . ?
N19 Rh4 C193 133.5(4) . . ?
C192 Rh4 C193 38.1(5) . . ?
N7 Rh4 C193 93.4(4) . . ?
C194 Rh4 C193 39.8(4) . . ?
C191 Rh4 N8 120.5(4) . . ?
N19 Rh4 N8 86.9(3) . . ?
C192 Rh4 N8 160.2(4) . . ?
N7 Rh4 N8 78.7(3) . . ?
C194 Rh4 N8 101.9(4) . . ?
C193 Rh4 N8 139.0(4) . . ?
C191 Rh4 C195 37.0(5) . . ?
N19 Rh4 C195 130.4(4) . . ?
C192 Rh4 C195 64.4(4) . . ?
N7 Rh4 C195 140.0(5) . . ?
C194 Rh4 C195 40.1(5) . . ?
C193 Rh4 C195 64.6(4) . . ?
N8 Rh4 C195 96.2(4) . . ?
C205 Rh5 N20 133.1(5) . . ?
C205 Rh5 C204 39.0(6) . . ?
N20 Rh5 C204 159.4(6) . . ?
C205 Rh5 C201 39.2(5) . . ?
N20 Rh5 C201 99.6(4) . . ?
C204 Rh5 C201 63.7(6) . . ?
C205 Rh5 N10 137.4(5) . . ?
N20 Rh5 N10 89.3(3) . . ?
C204 Rh5 N10 102.8(5) . . ?
C201 Rh5 N10 159.0(4) . . ?
C205 Rh5 C202 64.4(5) . . ?
N20 Rh5 C202 97.8(5) . . ?
C204 Rh5 C202 61.6(7) . . ?
C201 Rh5 C202 38.3(5) . . ?
N10 Rh5 C202 122.0(5) . . ?
C205 Rh5 N9 95.6(4) . . ?
N20 Rh5 N9 88.1(3) . . ?
C204 Rh5 N9 110.2(6) . . ?
C201 Rh5 N9 119.1(4) . . ?
N10 Rh5 N9 79.9(3) . . ?
C202 Rh5 N9 157.2(5) . . ?
C205 Rh5 C203 65.5(7) . . ?
N20 Rh5 C203 127.6(7) . . ?
C204 Rh5 C203 36.3(7) . . ?
C201 Rh5 C203 65.9(6) . . ?
N10 Rh5 C203 93.6(6) . . ?
C202 Rh5 C203 39.2(7) . . ?
N9 Rh5 C203 143.8(7) . . ?
N21 Rh6 C212 115.9(3) . . ?
N21 Rh6 C214 112.6(4) . . ?
C212 Rh6 C214 64.7(5) . . ?
N21 Rh6 C211 154.0(3) . . ?
C212 Rh6 C211 38.5(4) . . ?
C214 Rh6 C211 65.2(4) . . ?
N21 Rh6 C213 96.8(3) . . ?
C212 Rh6 C213 37.4(4) . . ?
C214 Rh6 C213 39.9(5) . . ?
C211 Rh6 C213 64.4(4) . . ?
N21 Rh6 N12 87.6(3) . . ?
C212 Rh6 N12 156.5(3) . . ?
C214 Rh6 N12 106.1(4) . . ?
C211 Rh6 N12 118.2(4) . . ?
C213 Rh6 N12 144.4(4) . . ?
N21 Rh6 C215 151.1(4) . . ?
C212 Rh6 C215 64.0(4) . . ?
C214 Rh6 C215 39.3(5) . . ?
C211 Rh6 C215 38.2(4) . . ?
C213 Rh6 C215 65.3(4) . . ?
N12 Rh6 C215 94.8(3) . . ?
N21 Rh6 N11 86.4(3) . . ?
C212 Rh6 N11 102.2(4) . . ?
C214 Rh6 N11 160.0(4) . . ?
C211 Rh6 N11 95.0(4) . . ?
C213 Rh6 N11 135.6(4) . . ?
N12 Rh6 N11 79.8(3) . . ?
C215 Rh6 N11 122.3(4) . . ?
N22 Rh7 C224 105.5(4) . . ?
N22 Rh7 C221 159.5(4) . . ?
C224 Rh7 C221 66.1(4) . . ?
N22 Rh7 N14 90.4(3) . . ?
C224 Rh7 N14 110.5(4) . . ?
C221 Rh7 N14 110.0(4) . . ?
N22 Rh7 C225 142.4(4) . . ?
C224 Rh7 C225 39.2(4) . . ?
C221 Rh7 C225 38.7(4) . . ?
N14 Rh7 C225 92.5(4) . . ?
N22 Rh7 N13 89.7(3) . . ?
C224 Rh7 N13 161.3(4) . . ?
C221 Rh7 N13 95.9(4) . . ?
N14 Rh7 N13 79.5(4) . . ?
C225 Rh7 N13 127.6(4) . . ?
N22 Rh7 C222 120.0(4) . . ?
C224 Rh7 C222 65.1(5) . . ?
C221 Rh7 C222 39.7(4) . . ?
N14 Rh7 C222 149.5(4) . . ?
C225 Rh7 C222 64.8(4) . . ?
N13 Rh7 C222 98.1(4) . . ?
N22 Rh7 C223 95.9(4) . . ?
C224 Rh7 C223 40.0(5) . . ?
C221 Rh7 C223 65.4(4) . . ?
N14 Rh7 C223 150.4(5) . . ?
C225 Rh7 C223 65.4(5) . . ?
N13 Rh7 C223 129.2(5) . . ?
C222 Rh7 C223 37.3(5) . . ?
N23 Rh8 C231 135.3(4) . . ?
N23 Rh8 C232 101.1(4) . . ?
C231 Rh8 C232 38.37(14) . . ?
N23 Rh8 N15 87.4(3) . . ?
C231 Rh8 N15 94.1(3) . . ?
C232 Rh8 N15 113.5(4) . . ?
N23 Rh8 C235 159.8(3) . . ?
C231 Rh8 C235 38.32(14) . . ?
C232 Rh8 C235 64.09(16) . . ?
N15 Rh8 C235 110.7(4) . . ?
N23 Rh8 C233 95.9(3) . . ?
C231 Rh8 C233 64.04(16) . . ?
C232 Rh8 C233 38.22(13) . . ?
N15 Rh8 C233 151.7(4) . . ?
C235 Rh8 C233 63.89(15) . . ?
N23 Rh8 C234 124.2(3) . . ?
C231 Rh8 C234 63.99(16) . . ?
C232 Rh8 C234 63.92(15) . . ?
N15 Rh8 C234 148.3(3) . . ?
C235 Rh8 C234 38.14(13) . . ?
C233 Rh8 C234 38.08(13) . . ?
N23 Rh8 N16 88.2(3) . . ?
C231 Rh8 N16 136.1(4) . . ?
C232 Rh8 N16 163.9(3) . . ?
N15 Rh8 N16 79.7(3) . . ?
C235 Rh8 N16 103.4(3) . . ?
C233 Rh8 N16 128.4(4) . . ?
C234 Rh8 N16 100.0(3) . . ?
C1 N1 C14 101.4(10) . . ?
C1 N1 Rh1 107.3(7) . . ?
C14 N1 Rh1 150.1(9) . . ?
C2 N2 C3 107.5(8) . . ?
C2 N2 Rh1 106.5(6) . . ?
C3 N2 Rh1 145.6(7) . . ?
C2 N3 C8 102.0(9) . . ?
C2 N3 Rh2 108.0(7) . . ?
C8 N3 Rh2 149.7(7) . . ?
C1 N4 C9 102.4(11) . . ?
C1 N4 Rh2 109.3(7) . . ?
C9 N4 Rh2 148.1(10) . . ?
C15 N5 C28 101.7(8) . . ?
C15 N5 Rh3 108.4(6) . . ?
C28 N5 Rh3 149.7(7) . . ?
C16 N6 C17 103.6(9) . . ?
C16 N6 Rh3 107.1(7) . . ?
C17 N6 Rh3 149.3(9) . . ?
C16 N7 C22 99.9(9) . . ?
C16 N7 Rh4 109.9(7) . . ?
C22 N7 Rh4 150.2(7) . . ?
C15 N8 C23 104.6(8) . . ?
C15 N8 Rh4 109.3(6) . . ?
C23 N8 Rh4 146.0(7) . . ?
C30 N9 C31 101.7(8) . . ?
C30 N9 Rh5 109.1(6) . . ?
C31 N9 Rh5 149.0(7) . . ?
C29 N10 C42 101.8(9) . . ?
C29 N10 Rh5 108.2(7) . . ?
C42 N10 Rh5 149.9(8) . . ?
C29 N11 C37 107.7(8) . . ?
C29 N11 Rh6 106.4(6) . . ?
C37 N11 Rh6 145.6(7) . . ?
C30 N12 C36 101.2(8) . . ?
C30 N12 Rh6 107.7(6) . . ?
C36 N12 Rh6 150.8(7) . . ?
C43 N13 C56 103.1(9) . . ?
C43 N13 Rh7 107.5(8) . . ?
C56 N13 Rh7 149.4(8) . . ?
C44 N14 C45 103.9(9) . . ?
C44 N14 Rh7 107.6(6) . . ?
C45 N14 Rh7 148.0(8) . . ?
C44 N15 C50 104.9(9) . . ?
C44 N15 Rh8 108.5(7) . . ?
C50 N15 Rh8 146.6(7) . . ?
C43 N16 C51 103.5(9) . . ?
C43 N16 Rh8 107.6(7) . . ?
C51 N16 Rh8 148.9(7) . . ?
C61 N17 C57 119.7(9) . . ?
C61 N17 Rh2 117.9(7) . . ?
C57 N17 Rh2 122.3(7) . . ?
C78 N18 C82 120.2(9) . . ?
C78 N18 Rh3 122.7(7) . . ?
C82 N18 Rh3 117.1(7) . . ?
C83 N19 C87 118.3(8) . . ?
C83 N19 Rh4 120.3(6) . . ?
C87 N19 Rh4 121.2(6) . . ?
C104 N20 C108 117.7(8) . . ?
C104 N20 Rh5 121.6(7) . . ?
C108 N20 Rh5 120.6(6) . . ?
C113 N21 C109 117.6(7) . . ?
C113 N21 Rh6 118.8(6) . . ?
C109 N21 Rh6 123.5(6) . . ?
C134 N22 C130 120.0(9) . . ?
C134 N22 Rh7 121.0(7) . . ?
C130 N22 Rh7 119.0(7) . . ?
C135 N23 C139 118.7(8) . . ?
C135 N23 Rh8 122.5(7) . . ?
C139 N23 Rh8 118.9(7) . . ?
C160 N24 C156 117.7(8) . . ?
C160 N24 Rh1 120.9(7) . . ?
C156 N24 Rh1 121.4(6) . . ?
C62 O1 C63 117.3(9) . . ?
C77 O3 C76 120.4(10) . . ?
C88 O5 C89 116.8(7) . . ?
C103 O7 C102 116.3(7) . . ?
C114 O9 C115 117.4(8) . . ?
C129 O11 C128 113.8(9) . . ?
C140 O13 C141 114.4(9) . . ?
C155 O15 C154 117.0(7) . . ?
O17 S1 O19 114.8(7) . . ?
O17 S1 O18 115.2(7) . . ?
O19 S1 O18 120.2(8) . . ?
O17 S1 C241 99.4(6) . . ?
O19 S1 C241 102.3(9) . . ?
O18 S1 C241 99.9(8) . . ?
N4 C1 N1 116.3(10) . . ?
N4 C1 C2 121.1(11) . . ?
N1 C1 C2 122.5(11) . . ?
N2 C2 N3 116.2(9) . . ?
N2 C2 C1 122.2(10) . . ?
N3 C2 C1 121.0(11) . . ?
C4 C3 N2 133.9(10) . . ?
C4 C3 C8 122.2(9) . . ?
N2 C3 C8 103.4(8) . . ?
C3 C4 C5 118.3(11) . . ?
C4 C5 C6 121.4(11) . . ?
C7 C6 C5 121.7(10) . . ?
C6 C7 C8 118.6(10) . . ?
N3 C8 C7 131.2(10) . . ?
N3 C8 C3 110.9(9) . . ?
C7 C8 C3 117.7(10) . . ?
C14 C9 N4 110.9(11) . . ?
C14 C9 C10 121.1(14) . . ?
N4 C9 C10 128.0(16) . . ?
C11 C10 C9 116.1(19) . . ?
C12 C11 C10 119.2(18) . . ?
C11 C12 C13 126.6(17) . . ?
C12 C13 C14 112.4(18) . . ?
C9 C14 C13 124.5(15) . . ?
C9 C14 N1 109.0(10) . . ?
C13 C14 N1 126.4(16) . . ?
N8 C15 N5 118.6(8) . . ?
N8 C15 C16 120.4(10) . . ?
N5 C15 C16 119.9(10) . . ?
N6 C16 N7 118.6(9) . . ?
N6 C16 C15 122.2(10) . . ?
N7 C16 C15 118.8(10) . . ?
C22 C17 N6 108.9(10) . . ?
C22 C17 C18 120.1(11) . . ?
N6 C17 C18 131.0(12) . . ?
C19 C18 C17 120.1(15) . . ?
C18 C19 C20 118.7(15) . . ?
C21 C20 C19 122.4(13) . . ?
C20 C21 C22 114.9(14) . . ?
C17 C22 N7 108.9(9) . . ?
C17 C22 C21 123.6(12) . . ?
N7 C22 C21 127.5(13) . . ?
C24 C23 N8 133.1(9) . . ?
C24 C23 C28 121.2(9) . . ?
N8 C23 C28 105.5(8) . . ?
C23 C24 C25 118.9(10) . . ?
C26 C25 C24 118.9(11) . . ?
C25 C26 C27 124.3(10) . . ?
C26 C27 C28 115.2(11) . . ?
N5 C28 C27 128.8(10) . . ?
N5 C28 C23 109.6(8) . . ?
C27 C28 C23 121.5(10) . . ?
N11 C29 N10 115.8(9) . . ?
N11 C29 C30 121.0(9) . . ?
N10 C29 C30 122.8(10) . . ?
N12 C30 N9 119.0(9) . . ?
N12 C30 C29 122.6(9) . . ?
N9 C30 C29 118.1(9) . . ?
N9 C31 C36 108.7(8) . . ?
N9 C31 C32 131.6(10) . . ?
C36 C31 C32 119.6(10) . . ?
C33 C32 C31 119.5(12) . . ?
C32 C33 C34 120.2(12) . . ?
C35 C34 C33 123.8(13) . . ?
C34 C35 C36 115.8(12) . . ?
C31 C36 C35 120.8(10) . . ?
C31 C36 N12 109.3(9) . . ?
C35 C36 N12 129.6(10) . . ?
N11 C37 C38 135.8(12) . . ?
N11 C37 C42 103.6(9) . . ?
C38 C37 C42 120.5(11) . . ?
C39 C38 C37 118.6(14) . . ?
C38 C39 C40 121.7(14) . . ?
C41 C40 C39 122.8(14) . . ?
C40 C41 C42 118.1(14) . . ?
N10 C42 C37 111.1(9) . . ?
N10 C42 C41 130.6(13) . . ?
C37 C42 C41 118.1(12) . . ?
N13 C43 N16 117.0(10) . . ?
N13 C43 C44 121.2(9) . . ?
N16 C43 C44 121.3(9) . . ?
N14 C44 N15 116.3(10) . . ?
N14 C44 C43 122.0(9) . . ?
N15 C44 C43 121.7(10) . . ?
C46 C45 N14 130.6(11) . . ?
C46 C45 C50 121.7(10) . . ?
N14 C45 C50 107.6(9) . . ?
C45 C46 C47 117.2(13) . . ?
C48 C47 C46 120.7(13) . . ?
C49 C48 C47 123.0(13) . . ?
C48 C49 C50 117.5(12) . . ?
N15 C50 C49 132.8(11) . . ?
N15 C50 C45 107.2(9) . . ?
C49 C50 C45 119.6(11) . . ?
C52 C51 N16 130.5(11) . . ?
C52 C51 C56 121.9(12) . . ?
N16 C51 C56 107.3(9) . . ?
C51 C52 C53 117.3(14) . . ?
C54 C53 C52 121.3(13) . . ?
C53 C54 C55 122.9(14) . . ?
C54 C55 C56 116.9(13) . . ?
N13 C56 C55 131.3(11) . . ?
N13 C56 C51 109.1(9) . . ?
C55 C56 C51 119.7(10) . . ?
N17 C57 C58 120.1(10) . . ?
C59 C58 C57 120.7(9) . . ?
C58 C59 C60 117.6(10) . . ?
C58 C59 C62 120.4(9) . . ?
C60 C59 C62 121.9(9) . . ?
C61 C60 C59 120.1(10) . . ?
N17 C61 C60 121.6(9) . . ?
O2 C62 O1 124.5(10) . . ?
O2 C62 C59 124.6(10) . . ?
O1 C62 C59 110.8(9) . . ?
O1 C63 C64 107.2(10) . . ?
C69 C64 C65 118.5(13) . . ?
C69 C64 C63 123.9(11) . . ?
C65 C64 C63 117.7(12) . . ?
C64 C65 C66 121.3(14) . . ?
C67 C66 C65 119.6(12) . . ?
C66 C67 C68 117.1(12) . . ?
C66 C67 C70 120.9(12) . . ?
C68 C67 C70 121.7(11) . . ?
C69 C68 C67 121.1(12) . . ?
C64 C69 C68 122.1(12) . . ?
C71 C70 C75 116.2(11) . . ?
C71 C70 C67 121.2(12) . . ?
C75 C70 C67 122.5(11) . . ?
C72 C71 C70 119.6(12) . . ?
C71 C72 C73 122.5(12) . . ?
C74 C73 C72 114.9(13) . . ?
C74 C73 C76 125.8(13) . . ?
C72 C73 C76 119.3(12) . . ?
C75 C74 C73 126.4(14) . . ?
C74 C75 C70 120.1(13) . . ?
O3 C76 C73 112.5(11) . . ?
O4 C77 O3 121.9(11) . . ?
O4 C77 C80 126.9(11) . . ?
O3 C77 C80 110.9(10) . . ?
N18 C78 C79 121.5(9) . . ?
C80 C79 C78 118.8(10) . . ?
C79 C80 C81 119.8(10) . . ?
C79 C80 C77 118.8(10) . . ?
C81 C80 C77 121.3(10) . . ?
C80 C81 C82 120.3(10) . . ?
N18 C82 C81 119.4(11) . . ?
N19 C83 C84 122.2(9) . . ?
C83 C84 C85 120.9(9) . . ?
C84 C85 C86 117.0(9) . . ?
C84 C85 C88 120.5(9) . . ?
C86 C85 C88 122.5(9) . . ?
C87 C86 C85 120.0(9) . . ?
N19 C87 C86 121.5(9) . . ?
O6 C88 O5 124.6(8) . . ?
O6 C88 C85 122.7(9) . . ?
O5 C88 C85 112.7(8) . . ?
O5 C89 C90 107.3(8) . . ?
C91 C90 C95 118.5(11) . . ?
C91 C90 C89 118.4(10) . . ?
C95 C90 C89 123.0(10) . . ?
C90 C91 C92 123.4(12) . . ?
C91 C92 C93 116.2(12) . . ?
C94 C93 C92 118.7(11) . . ?
C94 C93 C96 122.6(11) . . ?
C92 C93 C96 118.6(9) . . ?
C93 C94 C95 122.0(14) . . ?
C94 C95 C90 121.1(14) . . ?
C97 C96 C101 120.2(10) . . ?
C97 C96 C93 119.3(9) . . ?
C101 C96 C93 120.2(10) . . ?
C96 C97 C98 121.7(11) . . ?
C97 C98 C99 118.7(11) . . ?
C100 C99 C98 118.0(10) . . ?
C100 C99 C102 122.6(10) . . ?
C98 C99 C102 119.2(10) . . ?
C99 C100 C101 121.8(10) . . ?
C96 C101 C100 119.5(11) . . ?
C99 C102 O7 107.6(8) . . ?
O8 C103 O7 123.4(8) . . ?
O8 C103 C106 125.4(8) . . ?
O7 C103 C106 111.2(7) . . ?
N20 C104 C105 121.9(9) . . ?
C104 C105 C106 120.5(9) . . ?
C105 C106 C107 116.8(8) . . ?
C105 C106 C103 118.7(8) . . ?
C107 C106 C103 124.4(8) . . ?
C108 C107 C106 121.1(9) . . ?
C107 C108 N20 121.8(9) . . ?
N21 C109 C110 121.6(8) . . ?
C109 C110 C111 120.2(8) . . ?
C112 C111 C110 117.5(8) . . ?
C112 C111 C114 121.9(9) . . ?
C110 C111 C114 120.4(8) . . ?
C113 C112 C111 119.4(9) . . ?
N21 C113 C112 123.6(9) . . ?
O10 C114 O9 124.5(9) . . ?
O10 C114 C111 124.1(10) . . ?
O9 C114 C111 111.3(8) . . ?
O9 C115 C116 106.2(8) . . ?
C117 C116 C121 116.6(11) . . ?
C117 C116 C115 122.2(12) . . ?
C121 C116 C115 121.1(10) . . ?
C116 C117 C118 120.5(13) . . ?
C119 C118 C117 124.0(11) . . ?
C118 C119 C120 116.2(11) . . ?
C118 C119 C122 123.2(10) . . ?
C120 C119 C122 120.6(10) . . ?
C121 C120 C119 119.8(12) . . ?
C120 C121 C116 122.8(11) . . ?
C123 C122 C127 111.1(13) . . ?
C123 C122 C119 122.5(11) . . ?
C127 C122 C119 125.9(12) . . ?
C124 C123 C122 123.5(15) . . ?
C123 C124 C125 123.8(16) . . ?
C124 C125 C126 114.6(14) . . ?
C124 C125 C128 117.9(12) . . ?
C126 C125 C128 124.7(12) . . ?
C125 C126 C127 119.7(15) . . ?
C122 C127 C126 122.2(15) . . ?
C125 C128 O11 106.0(10) . . ?
O12 C129 O11 123.6(10) . . ?
O12 C129 C132 127.1(10) . . ?
O11 C129 C132 109.3(10) . . ?
N22 C130 C131 119.1(10) . . ?
C132 C131 C130 121.2(10) . . ?
C131 C132 C133 118.3(9) . . ?
C131 C132 C129 124.4(9) . . ?
C133 C132 C129 117.1(9) . . ?
C134 C133 C132 119.3(10) . . ?
N22 C134 C133 122.0(10) . . ?
N23 C135 C136 124.1(10) . . ?
C135 C136 C137 117.2(10) . . ?
C138 C137 C136 119.1(9) . . ?
C138 C137 C140 118.6(9) . . ?
C136 C137 C140 122.3(9) . . ?
C139 C138 C137 118.1(9) . . ?
N23 C139 C138 122.8(10) . . ?
O14 C140 O13 127.2(10) . . ?
O14 C140 C137 120.7(10) . . ?
O13 C140 C137 112.0(9) . . ?
C142 C141 O13 106.1(11) . . ?
C147 C142 C143 118.6(13) . . ?
C147 C142 C141 124.1(15) . . ?
C143 C142 C141 117.2(15) . . ?
C144 C143 C142 119.9(13) . . ?
C143 C144 C145 122.0(13) . . ?
C146 C145 C144 118.3(11) . . ?
C146 C145 C148 120.9(11) . . ?
C144 C145 C148 120.8(11) . . ?
C145 C146 C147 119.7(14) . . ?
C142 C147 C146 121.1(15) . . ?
C153 C148 C149 115.6(10) . . ?
C153 C148 C145 123.0(10) . . ?
C149 C148 C145 121.4(9) . . ?
C150 C149 C148 124.3(10) . . ?
C149 C150 C151 118.8(10) . . ?
C152 C151 C150 118.4(10) . . ?
C152 C151 C154 122.1(9) . . ?
C150 C151 C154 119.2(9) . . ?
C151 C152 C153 121.5(10) . . ?
C148 C153 C152 121.3(10) . . ?
O15 C154 C151 108.3(7) . . ?
O16 C155 O15 125.6(8) . . ?
O16 C155 C158 124.4(8) . . ?
O15 C155 C158 109.9(7) . . ?
N24 C156 C157 123.2(8) . . ?
C156 C157 C158 117.7(9) . . ?
C159 C158 C157 118.6(8) . . ?
C159 C158 C155 122.8(8) . . ?
C157 C158 C155 118.6(8) . . ?
C158 C159 C160 119.0(9) . . ?
N24 C160 C159 123.7(9) . . ?
C162 C161 C165 108.1(13) . . ?
C162 C161 C166 129.5(15) . . ?
C165 C161 C166 122.5(15) . . ?
C162 C161 Rh1 71.1(7) . . ?
C165 C161 Rh1 70.1(7) . . ?
C166 C161 Rh1 124.2(10) . . ?
C161 C162 C163 111.5(13) . . ?
C161 C162 C167 125.9(12) . . ?
C163 C162 C167 122.7(14) . . ?
C161 C162 Rh1 71.2(8) . . ?
C163 C162 Rh1 70.8(8) . . ?
C167 C162 Rh1 125.6(8) . . ?
C164 C163 C162 106.5(13) . . ?
C164 C163 C168 124.4(13) . . ?
C162 C163 C168 128.6(15) . . ?
C164 C163 Rh1 70.3(9) . . ?
C162 C163 Rh1 71.2(8) . . ?
C168 C163 Rh1 130.1(10) . . ?
C163 C164 C165 108.3(12) . . ?
C163 C164 C169 125.6(18) . . ?
C165 C164 C169 126.1(19) . . ?
C163 C164 Rh1 71.6(8) . . ?
C165 C164 Rh1 69.7(7) . . ?
C169 C164 Rh1 123.4(11) . . ?
C161 C165 C170 130(2) . . ?
C161 C165 C164 105.6(13) . . ?
C170 C165 C164 124(2) . . ?
C161 C165 Rh1 71.6(7) . . ?
C170 C165 Rh1 128.7(13) . . ?
C164 C165 Rh1 69.4(7) . . ?
C172 C171 C175 110.1(15) . . ?
C172 C171 C176 129.2(19) . . ?
C175 C171 C176 120.5(19) . . ?
C172 C171 Rh2 71.8(8) . . ?
C175 C171 Rh2 68.9(7) . . ?
C176 C171 Rh2 122.0(10) . . ?
C171 C172 C173 106.2(13) . . ?
C171 C172 C177 127.3(18) . . ?
C173 C172 C177 126.5(16) . . ?
C171 C172 Rh2 71.4(7) . . ?
C173 C172 Rh2 70.0(6) . . ?
C177 C172 Rh2 122.5(9) . . ?
C174 C173 C172 108.6(13) . . ?
C174 C173 C178 126.1(13) . . ?
C172 C173 C178 125.1(13) . . ?
C174 C173 Rh2 72.0(7) . . ?
C172 C173 Rh2 70.5(7) . . ?
C178 C173 Rh2 127.0(9) . . ?
C175 C174 C173 107.5(13) . . ?
C175 C174 C179 127.2(15) . . ?
C173 C174 C179 125.3(14) . . ?
C175 C174 Rh2 68.8(7) . . ?
C173 C174 Rh2 69.7(7) . . ?
C179 C174 Rh2 128.1(9) . . ?
C174 C175 C171 107.5(14) . . ?
C174 C175 C180 123.3(18) . . ?
C171 C175 C180 128.3(18) . . ?
C174 C175 Rh2 73.7(7) . . ?
C171 C175 Rh2 71.3(8) . . ?
C180 C175 Rh2 128.9(11) . . ?
C185 C181 C182 109.7(12) . . ?
C185 C181 C186 127.0(15) . . ?
C182 C181 C186 122.7(15) . . ?
C185 C181 Rh3 73.5(7) . . ?
C182 C181 Rh3 70.7(7) . . ?
C186 C181 Rh3 128.9(10) . . ?
C181 C182 C187 128.4(16) . . ?
C181 C182 C183 107.2(12) . . ?
C187 C182 C183 124.4(15) . . ?
C181 C182 Rh3 70.4(7) . . ?
C187 C182 Rh3 122.6(11) . . ?
C183 C182 Rh3 70.3(7) . . ?
C182 C183 C188 126.1(16) . . ?
C182 C183 C184 104.8(10) . . ?
C188 C183 C184 129.1(16) . . ?
C182 C183 Rh3 69.7(6) . . ?
C188 C183 Rh3 126.8(12) . . ?
C184 C183 Rh3 68.7(6) . . ?
C185 C184 C183 107.6(13) . . ?
C185 C184 C189 125.5(15) . . ?
C183 C184 C189 126.7(13) . . ?
C185 C184 Rh3 73.7(8) . . ?
C183 C184 Rh3 70.6(7) . . ?
C189 C184 Rh3 125.4(10) . . ?
C181 C185 C184 110.4(13) . . ?
C181 C185 C190 126.9(13) . . ?
C184 C185 C190 122.4(15) . . ?
C181 C185 Rh3 69.6(7) . . ?
C184 C185 Rh3 68.7(7) . . ?
C190 C185 Rh3 122.9(10) . . ?
C195 C191 C192 113.9(12) . . ?
C195 C191 C196 119.5(13) . . ?
C192 C191 C196 118.0(13) . . ?
C195 C191 Rh4 83.4(11) . . ?
C192 C191 Rh4 78.7(9) . . ?
C196 C191 Rh4 134.7(9) . . ?
C193 C192 C191 103.5(10) . . ?
C193 C192 C197 126.1(11) . . ?
C191 C192 C197 130.1(12) . . ?
C193 C192 Rh4 72.4(6) . . ?
C191 C192 Rh4 60.4(8) . . ?
C197 C192 Rh4 126.6(8) . . ?
C192 C193 C194 109.5(11) . . ?
C192 C193 C198 126.8(12) . . ?
C194 C193 C198 123.6(14) . . ?
C192 C193 Rh4 69.5(6) . . ?
C194 C193 Rh4 69.1(6) . . ?
C198 C193 Rh4 124.5(10) . . ?
C199 C194 C193 130.2(14) . . ?
C199 C194 C195 125.6(13) . . ?
C193 C194 C195 103.8(11) . . ?
C199 C194 Rh4 127.6(10) . . ?
C193 C194 Rh4 71.1(6) . . ?
C195 C194 Rh4 71.2(6) . . ?
C191 C195 C194 105.4(12) . . ?
C191 C195 C200 130.3(13) . . ?
C194 C195 C200 122.7(13) . . ?
C191 C195 Rh4 59.6(9) . . ?
C194 C195 Rh4 68.7(7) . . ?
C200 C195 Rh4 125.2(8) . . ?
C202 C201 C205 107.2(14) . . ?
C202 C201 C206 124.5(12) . . ?
C205 C201 C206 128.3(15) . . ?
C202 C201 Rh5 71.7(7) . . ?
C205 C201 Rh5 70.0(7) . . ?
C206 C201 Rh5 126.0(8) . . ?
C201 C202 C203 110.9(13) . . ?
C201 C202 C207 125.2(15) . . ?
C203 C202 C207 124.0(16) . . ?
C201 C202 Rh5 70.0(6) . . ?
C203 C202 Rh5 72.8(9) . . ?
C207 C202 Rh5 124.5(10) . . ?
C204 C203 C202 101.7(14) . . ?
C204 C203 C208 130(2) . . ?
C202 C203 C208 128(2) . . ?
C204 C203 Rh5 68.0(9) . . ?
C202 C203 Rh5 68.0(7) . . ?
C208 C203 Rh5 124.5(13) . . ?
C203 C204 C205 115.9(16) . . ?
C203 C204 C209 126(2) . . ?
C205 C204 C209 118(2) . . ?
C203 C204 Rh5 75.7(9) . . ?
C205 C204 Rh5 70.4(7) . . ?
C209 C204 Rh5 119.1(13) . . ?
C204 C205 C201 104.3(14) . . ?
C204 C205 C210 134.1(16) . . ?
C201 C205 C210 121.3(17) . . ?
C204 C205 Rh5 70.6(8) . . ?
C201 C205 Rh5 70.8(6) . . ?
C210 C205 Rh5 126.8(10) . . ?
C212 C211 C215 107.9(10) . . ?
C212 C211 C216 127.3(11) . . ?
C215 C211 C216 124.8(11) . . ?
C212 C211 Rh6 70.4(5) . . ?
C215 C211 Rh6 71.7(5) . . ?
C216 C211 Rh6 125.3(7) . . ?
C213 C212 C211 110.7(10) . . ?
C213 C212 C217 126.5(11) . . ?
C211 C212 C217 122.6(11) . . ?
C213 C212 Rh6 71.8(6) . . ?
C211 C212 Rh6 71.1(5) . . ?
C217 C212 Rh6 127.8(8) . . ?
C212 C213 C218 127.5(14) . . ?
C212 C213 C214 107.4(10) . . ?
C218 C213 C214 125.0(13) . . ?
C212 C213 Rh6 70.8(6) . . ?
C218 C213 Rh6 126.9(8) . . ?
C214 C213 Rh6 69.8(6) . . ?
C215 C214 C213 106.2(11) . . ?
C215 C214 C219 125.0(15) . . ?
C213 C214 C219 128.6(14) . . ?
C215 C214 Rh6 71.3(7) . . ?
C213 C214 Rh6 70.3(7) . . ?
C219 C214 Rh6 127.1(9) . . ?
C211 C215 C214 107.8(10) . . ?
C211 C215 C220 128.1(13) . . ?
C214 C215 C220 124.0(14) . . ?
C211 C215 Rh6 70.1(6) . . ?
C214 C215 Rh6 69.4(6) . . ?
C220 C215 Rh6 122.8(8) . . ?
C225 C221 C222 106.5(10) . . ?
C225 C221 C226 126.5(10) . . ?
C222 C221 C226 126.9(11) . . ?
C225 C221 Rh7 71.2(6) . . ?
C222 C221 Rh7 70.9(6) . . ?
C226 C221 Rh7 125.7(8) . . ?
C223 C222 C221 109.7(11) . . ?
C223 C222 C227 125.2(12) . . ?
C221 C222 C227 125.1(12) . . ?
C223 C222 Rh7 71.5(7) . . ?
C221 C222 Rh7 69.4(6) . . ?
C227 C222 Rh7 125.9(8) . . ?
C222 C223 C228 126.4(13) . . ?
C222 C223 C224 108.1(10) . . ?
C228 C223 C224 125.4(12) . . ?
C222 C223 Rh7 71.2(6) . . ?
C228 C223 Rh7 123.2(9) . . ?
C224 C223 Rh7 68.7(6) . . ?
C225 C224 C229 126.8(12) . . ?
C225 C224 C223 106.6(10) . . ?
C229 C224 C223 126.1(12) . . ?
C225 C224 Rh7 71.4(7) . . ?
C229 C224 Rh7 128.3(9) . . ?
C223 C224 Rh7 71.3(7) . . ?
C221 C225 C224 108.9(10) . . ?
C221 C225 C230 125.3(11) . . ?
C224 C225 C230 125.7(11) . . ?
C221 C225 Rh7 70.1(6) . . ?
C224 C225 Rh7 69.4(6) . . ?
C230 C225 Rh7 124.5(8) . . ?
C235 C231 C232 108.0 . . ?
C235 C231 C236 115.2(12) . . ?
C232 C231 C236 136.8(12) . . ?
C235 C231 Rh8 71.2(3) . . ?
C232 C231 Rh8 71.0(3) . . ?
C236 C231 Rh8 122.3(8) . . ?
C233 C232 C231 108.0 . . ?
C233 C232 C237 130.9(14) . . ?
C231 C232 C237 121.0(14) . . ?
C233 C232 Rh8 71.4(3) . . ?
C231 C232 Rh8 70.6(3) . . ?
C237 C232 Rh8 126.1(8) . . ?
C232 C233 C234 108.0 . . ?
C232 C233 C238 126.1(11) . . ?
C234 C233 C238 125.9(11) . . ?
C232 C233 Rh8 70.4(3) . . ?
C234 C233 Rh8 71.1(3) . . ?
C238 C233 Rh8 126.3(8) . . ?
C235 C234 C233 108.0 . . ?
C235 C234 C239 127.5(10) . . ?
C233 C234 C239 124.3(10) . . ?
C235 C234 Rh8 70.5(3) . . ?
C233 C234 Rh8 70.8(3) . . ?
C239 C234 Rh8 127.6(8) . . ?
C234 C235 C231 108.0 . . ?
C234 C235 C240 121.5(11) . . ?
C231 C235 C240 130.4(11) . . ?
C234 C235 Rh8 71.3(3) . . ?
C231 C235 Rh8 70.5(3) . . ?
C240 C235 Rh8 121.2(8) . . ?
F1 C241 F3 107.2(16) . . ?
F1 C241 F2 106.1(13) . . ?
F3 C241 F2 104.4(12) . . ?
F1 C241 S1 114.9(11) . . ?
F3 C241 S1 113.8(11) . . ?
F2 C241 S1 109.8(12) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Rh1 N24 2.122(7) . ?
Rh1 C164 2.131(12) . ?
Rh1 C165 2.134(11) . ?
Rh1 C163 2.148(15) . ?
Rh1 C162 2.152(13) . ?
Rh1 C161 2.153(12) . ?
Rh1 N1 2.171(10) . ?
Rh1 N2 2.209(8) . ?
Rh2 N17 2.135(9) . ?
Rh2 C175 2.135(12) . ?
Rh2 N4 2.158(11) . ?
Rh2 C173 2.166(12) . ?
Rh2 C171 2.168(13) . ?
Rh2 C172 2.173(11) . ?
Rh2 N3 2.179(9) . ?
Rh2 C174 2.197(12) . ?
Rh3 N18 2.095(8) . ?
Rh3 C184 2.118(12) . ?
Rh3 C181 2.134(11) . ?
Rh3 C182 2.137(11) . ?
Rh3 C183 2.145(12) . ?
Rh3 N5 2.151(8) . ?
Rh3 C185 2.183(13) . ?
Rh3 N6 2.207(9) . ?
Rh4 C191 1.893(19) . ?
Rh4 N19 2.116(7) . ?
Rh4 C192 2.134(10) . ?
Rh4 N7 2.143(10) . ?
Rh4 C194 2.144(11) . ?
Rh4 C193 2.171(10) . ?
Rh4 N8 2.172(7) . ?
Rh4 C195 2.179(12) . ?
Rh5 C205 2.127(12) . ?
Rh5 N20 2.129(8) . ?
Rh5 C204 2.130(13) . ?
Rh5 C201 2.137(11) . ?
Rh5 N10 2.148(10) . ?
Rh5 C202 2.160(12) . ?
Rh5 N9 2.180(9) . ?
Rh5 C203 2.226(15) . ?
Rh6 N21 2.112(7) . ?
Rh6 C212 2.133(9) . ?
Rh6 C214 2.139(12) . ?
Rh6 C211 2.143(9) . ?
Rh6 C213 2.146(10) . ?
Rh6 N12 2.149(8) . ?
Rh6 C215 2.165(10) . ?
Rh6 N11 2.211(8) . ?
Rh7 N22 2.135(8) . ?
Rh7 C224 2.142(12) . ?
Rh7 C221 2.153(10) . ?
Rh7 N14 2.162(8) . ?
Rh7 C225 2.169(11) . ?
Rh7 N13 2.170(10) . ?
Rh7 C222 2.174(10) . ?
Rh7 C223 2.177(11) . ?
Rh8 N23 2.127(7) . ?
Rh8 C231 2.158(9) . ?
Rh8 C232 2.163(8) . ?
Rh8 N15 2.163(10) . ?
Rh8 C235 2.168(8) . ?
Rh8 C233 2.175(8) . ?
Rh8 C234 2.178(8) . ?
Rh8 N16 2.189(9) . ?
N1 C1 1.340(14) . ?
N1 C14 1.413(17) . ?
N2 C2 1.327(14) . ?
N2 C3 1.370(12) . ?
N3 C2 1.349(13) . ?
N3 C8 1.373(13) . ?
N4 C1 1.339(15) . ?
N4 C9 1.368(15) . ?
N5 C15 1.333(13) . ?
N5 C28 1.395(13) . ?
N6 C16 1.298(14) . ?
N6 C17 1.370(14) . ?
N7 C16 1.342(13) . ?
N7 C22 1.424(15) . ?
N8 C15 1.307(13) . ?
N8 C23 1.401(11) . ?
N9 C30 1.354(12) . ?
N9 C31 1.380(13) . ?
N10 C29 1.341(12) . ?
N10 C42 1.372(15) . ?
N11 C29 1.315(13) . ?
N11 C37 1.365(13) . ?
N12 C30 1.314(12) . ?
N12 C36 1.406(12) . ?
N13 C43 1.329(13) . ?
N13 C56 1.389(14) . ?
N14 C44 1.321(13) . ?
N14 C45 1.415(13) . ?
N15 C44 1.350(13) . ?
N15 C50 1.383(14) . ?
N16 C43 1.348(13) . ?
N16 C51 1.394(14) . ?
N17 C61 1.328(13) . ?
N17 C57 1.359(13) . ?
N18 C78 1.335(12) . ?
N18 C82 1.370(14) . ?
N19 C83 1.355(12) . ?
N19 C87 1.376(13) . ?
N20 C104 1.356(12) . ?
N20 C108 1.356(13) . ?
N21 C113 1.343(12) . ?
N21 C109 1.345(11) . ?
N22 C134 1.329(13) . ?
N22 C130 1.344(13) . ?
N23 C135 1.286(13) . ?
N23 C139 1.350(14) . ?
N24 C160 1.320(12) . ?
N24 C156 1.334(13) . ?
O1 C62 1.381(13) . ?
O1 C63 1.440(14) . ?
O2 C62 1.185(12) . ?
O3 C77 1.335(13) . ?
O3 C76 1.399(14) . ?
O4 C77 1.171(13) . ?
O5 C88 1.317(11) . ?
O5 C89 1.447(11) . ?
O6 C88 1.220(11) . ?
O7 C103 1.348(11) . ?
O7 C102 1.488(12) . ?
O8 C103 1.217(10) . ?
O9 C114 1.333(12) . ?
O9 C115 1.441(12) . ?
O10 C114 1.209(12) . ?
O11 C129 1.389(12) . ?
O11 C128 1.487(13) . ?
O12 C129 1.201(13) . ?
O13 C140 1.277(13) . ?
O13 C141 1.545(15) . ?
O14 C140 1.219(13) . ?
O15 C155 1.343(11) . ?
O15 C154 1.452(11) . ?
O16 C155 1.184(10) . ?
O17 S1 1.392(9) . ?
O18 S1 1.440(11) . ?
O19 S1 1.432(11) . ?
S1 C241 1.807(16) . ?
F1 C241 1.203(17) . ?
F2 C241 1.410(16) . ?
F3 C241 1.393(15) . ?
C1 C2 1.366(14) . ?
C3 C4 1.369(14) . ?
C3 C8 1.464(15) . ?
C4 C5 1.382(14) . ?
C5 C6 1.408(17) . ?
C6 C7 1.385(16) . ?
C7 C8 1.421(14) . ?
C9 C14 1.33(2) . ?
C9 C10 1.43(2) . ?
C10 C11 1.39(3) . ?
C11 C12 1.361(17) . ?
C12 C13 1.38(3) . ?
C13 C14 1.407(19) . ?
C15 C16 1.428(14) . ?
C17 C22 1.365(17) . ?
C17 C18 1.394(17) . ?
C18 C19 1.356(18) . ?
C19 C20 1.47(2) . ?
C20 C21 1.372(19) . ?
C21 C22 1.425(14) . ?
C23 C24 1.366(14) . ?
C23 C28 1.426(15) . ?
C24 C25 1.423(14) . ?
C25 C26 1.397(16) . ?
C26 C27 1.400(16) . ?
C27 C28 1.419(13) . ?
C29 C30 1.414(14) . ?
C31 C36 1.389(15) . ?
C31 C32 1.414(15) . ?
C32 C33 1.316(17) . ?
C33 C34 1.380(19) . ?
C34 C35 1.368(17) . ?
C35 C36 1.402(15) . ?
C37 C38 1.374(16) . ?
C37 C42 1.433(17) . ?
C38 C39 1.371(18) . ?
C39 C40 1.376(15) . ?
C40 C41 1.33(2) . ?
C41 C42 1.449(16) . ?
C43 C44 1.380(14) . ?
C45 C46 1.361(16) . ?
C45 C50 1.431(16) . ?
C46 C47 1.399(17) . ?
C47 C48 1.38(2) . ?
C48 C49 1.363(19) . ?
C49 C50 1.391(15) . ?
C51 C52 1.379(16) . ?
C51 C56 1.413(15) . ?
C52 C53 1.380(19) . ?
C53 C54 1.37(2) . ?
C54 C55 1.382(18) . ?
C55 C56 1.398(15) . ?
C57 C58 1.370(14) . ?
C58 C59 1.359(14) . ?
C59 C60 1.400(14) . ?
C59 C62 1.495(15) . ?
C60 C61 1.345(15) . ?
C63 C64 1.490(18) . ?
C64 C69 1.348(17) . ?
C64 C65 1.375(19) . ?
C65 C66 1.46(2) . ?
C66 C67 1.388(18) . ?
C67 C68 1.412(16) . ?
C67 C70 1.436(16) . ?
C68 C69 1.408(17) . ?
C70 C71 1.425(16) . ?
C70 C75 1.431(19) . ?
C71 C72 1.382(19) . ?
C72 C73 1.406(19) . ?
C73 C74 1.359(18) . ?
C73 C76 1.451(18) . ?
C74 C75 1.313(19) . ?
C77 C80 1.475(15) . ?
C78 C79 1.414(14) . ?
C79 C80 1.370(14) . ?
C80 C81 1.371(15) . ?
C81 C82 1.409(16) . ?
C83 C84 1.379(13) . ?
C84 C85 1.403(13) . ?
C85 C86 1.406(13) . ?
C85 C88 1.450(13) . ?
C86 C87 1.400(14) . ?
C89 C90 1.509(15) . ?
C90 C91 1.318(16) . ?
C90 C95 1.381(18) . ?
C91 C92 1.425(18) . ?
C92 C93 1.430(17) . ?
C93 C94 1.354(17) . ?
C93 C96 1.509(14) . ?
C94 C95 1.357(19) . ?
C96 C97 1.346(15) . ?
C96 C101 1.360(14) . ?
C97 C98 1.412(17) . ?
C98 C99 1.428(16) . ?
C99 C100 1.353(15) . ?
C99 C102 1.463(14) . ?
C100 C101 1.425(15) . ?
C103 C106 1.468(12) . ?
C104 C105 1.367(13) . ?
C105 C106 1.373(12) . ?
C106 C107 1.394(13) . ?
C107 C108 1.346(13) . ?
C109 C110 1.376(12) . ?
C110 C111 1.387(13) . ?
C111 C112 1.384(12) . ?
C111 C114 1.479(13) . ?
C112 C113 1.356(13) . ?
C115 C116 1.519(16) . ?
C116 C117 1.348(16) . ?
C116 C121 1.406(17) . ?
C117 C118 1.392(19) . ?
C118 C119 1.356(18) . ?
C119 C120 1.402(16) . ?
C119 C122 1.486(16) . ?
C120 C121 1.374(18) . ?
C122 C123 1.41(2) . ?
C122 C127 1.415(19) . ?
C123 C124 1.34(2) . ?
C124 C125 1.339(18) . ?
C125 C126 1.37(2) . ?
C125 C128 1.439(17) . ?
C126 C127 1.43(2) . ?
C129 C132 1.494(15) . ?
C130 C131 1.396(14) . ?
C131 C132 1.342(14) . ?
C132 C133 1.384(13) . ?
C133 C134 1.361(14) . ?
C135 C136 1.391(15) . ?
C136 C137 1.405(14) . ?
C137 C138 1.381(14) . ?
C137 C140 1.504(14) . ?
C138 C139 1.379(14) . ?
C141 C142 1.491(18) . ?
C142 C147 1.34(2) . ?
C142 C143 1.44(2) . ?
C143 C144 1.356(18) . ?
C144 C145 1.393(17) . ?
C145 C146 1.390(17) . ?
C145 C148 1.491(15) . ?
C146 C147 1.427(19) . ?
C148 C153 1.357(15) . ?
C148 C149 1.411(16) . ?
C149 C150 1.341(15) . ?
C150 C151 1.398(13) . ?
C151 C152 1.361(15) . ?
C151 C154 1.496(13) . ?
C152 C153 1.395(15) . ?
C155 C158 1.505(12) . ?
C156 C157 1.387(14) . ?
C157 C158 1.404(13) . ?
C158 C159 1.366(13) . ?
C159 C160 1.377(13) . ?
C161 C162 1.390(18) . ?
C161 C165 1.41(2) . ?
C161 C166 1.51(2) . ?
C162 C163 1.401(17) . ?
C162 C167 1.497(19) . ?
C163 C164 1.39(2) . ?
C163 C168 1.46(2) . ?
C164 C165 1.49(2) . ?
C164 C169 1.54(2) . ?
C165 C170 1.41(2) . ?
C171 C172 1.37(2) . ?
C171 C175 1.46(2) . ?
C171 C176 1.57(3) . ?
C172 C173 1.465(19) . ?
C172 C177 1.47(2) . ?
C173 C174 1.434(18) . ?
C173 C178 1.48(2) . ?
C174 C175 1.39(2) . ?
C174 C179 1.49(2) . ?
C175 C180 1.49(2) . ?
C181 C185 1.367(19) . ?
C181 C182 1.421(18) . ?
C181 C186 1.44(2) . ?
C182 C187 1.43(2) . ?
C182 C183 1.462(15) . ?
C183 C188 1.48(2) . ?
C183 C184 1.48(2) . ?
C184 C185 1.388(17) . ?
C184 C189 1.53(2) . ?
C185 C190 1.52(2) . ?
C191 C195 1.319(17) . ?
C191 C192 1.424(13) . ?
C191 C196 1.503(16) . ?
C192 C193 1.405(18) . ?
C192 C197 1.548(16) . ?
C193 C194 1.470(17) . ?
C193 C198 1.50(2) . ?
C194 C199 1.439(19) . ?
C194 C195 1.48(2) . ?
C195 C200 1.510(16) . ?
C201 C202 1.409(19) . ?
C201 C205 1.430(17) . ?
C201 C206 1.50(2) . ?
C202 C203 1.47(2) . ?
C202 C207 1.49(2) . ?
C203 C204 1.36(2) . ?
C203 C208 1.507(17) . ?
C204 C205 1.42(2) . ?
C204 C209 1.536(17) . ?
C205 C210 1.49(2) . ?
C211 C212 1.408(15) . ?
C211 C215 1.410(16) . ?
C211 C216 1.495(16) . ?
C212 C213 1.372(16) . ?
C212 C217 1.507(16) . ?
C213 C218 1.456(17) . ?
C213 C214 1.462(18) . ?
C214 C215 1.446(17) . ?
C214 C219 1.51(2) . ?
C215 C220 1.487(17) . ?
C221 C225 1.433(16) . ?
C221 C222 1.470(15) . ?
C221 C226 1.482(16) . ?
C222 C223 1.390(17) . ?
C222 C227 1.483(17) . ?
C223 C228 1.465(17) . ?
C223 C224 1.479(18) . ?
C224 C225 1.448(16) . ?
C224 C229 1.463(18) . ?
C225 C230 1.491(15) . ?
C231 C235 1.4200 . ?
C231 C232 1.4200 . ?
C231 C236 1.54(2) . ?
C232 C233 1.4200 . ?
C232 C237 1.47(2) . ?
C233 C234 1.4200 . ?
C233 C238 1.507(19) . ?
C234 C235 1.4200 . ?
C234 C239 1.52(2) . ?
C235 C240 1.557(13) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C9 N4 C1 N1 -1.2(14) . . . . ?
Rh2 N4 C1 N1 174.7(7) . . . . ?
C9 N4 C1 C2 178.7(11) . . . . ?
Rh2 N4 C1 C2 -5.4(13) . . . . ?
C14 N1 C1 N4 -0.3(13) . . . . ?
Rh1 N1 C1 N4 -171.7(8) . . . . ?
C14 N1 C1 C2 179.8(11) . . . . ?
Rh1 N1 C1 C2 8.4(12) . . . . ?
C3 N2 C2 N3 1.1(12) . . . . ?
Rh1 N2 C2 N3 175.9(7) . . . . ?
C3 N2 C2 C1 172.3(9) . . . . ?
Rh1 N2 C2 C1 -13.0(12) . . . . ?
C8 N3 C2 N2 -0.6(11) . . . . ?
Rh2 N3 C2 N2 -175.8(7) . . . . ?
C8 N3 C2 C1 -171.8(9) . . . . ?
Rh2 N3 C2 C1 12.9(11) . . . . ?
N4 C1 C2 N2 -176.3(10) . . . . ?
N1 C1 C2 N2 3.6(16) . . . . ?
N4 C1 C2 N3 -5.6(16) . . . . ?
N1 C1 C2 N3 174.3(9) . . . . ?
C2 N2 C3 C4 -172.6(11) . . . . ?
Rh1 N2 C3 C4 16.3(19) . . . . ?
C2 N2 C3 C8 -1.1(10) . . . . ?
Rh1 N2 C3 C8 -172.2(8) . . . . ?
N2 C3 C4 C5 171.8(10) . . . . ?
C8 C3 C4 C5 1.6(14) . . . . ?
C3 C4 C5 C6 0.5(15) . . . . ?
C4 C5 C6 C7 -2.5(16) . . . . ?
C5 C6 C7 C8 2.3(16) . . . . ?
C2 N3 C8 C7 174.3(11) . . . . ?
Rh2 N3 C8 C7 -15(2) . . . . ?
C2 N3 C8 C3 -0.2(10) . . . . ?
Rh2 N3 C8 C3 170.8(10) . . . . ?
C6 C7 C8 N3 -174.5(10) . . . . ?
C6 C7 C8 C3 -0.3(14) . . . . ?
C4 C3 C8 N3 173.6(9) . . . . ?
N2 C3 C8 N3 0.8(10) . . . . ?
C4 C3 C8 C7 -1.7(14) . . . . ?
N2 C3 C8 C7 -174.5(8) . . . . ?
C1 N4 C9 C14 2.4(16) . . . . ?
Rh2 N4 C9 C14 -170.4(14) . . . . ?
C1 N4 C9 C10 179.9(16) . . . . ?
Rh2 N4 C9 C10 7(3) . . . . ?
C14 C9 C10 C11 0(3) . . . . ?
N4 C9 C10 C11 -176.7(17) . . . . ?
C9 C10 C11 C12 -1(3) . . . . ?
C10 C11 C12 C13 -2(4) . . . . ?
C11 C12 C13 C14 5(4) . . . . ?
N4 C9 C14 C13 -178.9(15) . . . . ?
C10 C9 C14 C13 4(3) . . . . ?
N4 C9 C14 N1 -2.7(18) . . . . ?
C10 C9 C14 N1 179.7(13) . . . . ?
C12 C13 C14 C9 -6(3) . . . . ?
C12 C13 C14 N1 178.4(17) . . . . ?
C1 N1 C14 C9 1.8(15) . . . . ?
Rh1 N1 C14 C9 165.2(12) . . . . ?
C1 N1 C14 C13 177.9(16) . . . . ?
Rh1 N1 C14 C13 -19(3) . . . . ?
C23 N8 C15 N5 -0.5(12) . . . . ?
Rh4 N8 C15 N5 -179.0(7) . . . . ?
C23 N8 C15 C16 -168.7(9) . . . . ?
Rh4 N8 C15 C16 12.8(11) . . . . ?
C28 N5 C15 N8 0.1(12) . . . . ?
Rh3 N5 C15 N8 176.9(7) . . . . ?
C28 N5 C15 C16 168.4(9) . . . . ?
Rh3 N5 C15 C16 -14.8(11) . . . . ?
C17 N6 C16 N7 3.4(12) . . . . ?
Rh3 N6 C16 N7 -178.3(7) . . . . ?
C17 N6 C16 C15 -169.1(9) . . . . ?
Rh3 N6 C16 C15 9.2(12) . . . . ?
C22 N7 C16 N6 -4.5(12) . . . . ?
Rh4 N7 C16 N6 175.0(7) . . . . ?
C22 N7 C16 C15 168.3(9) . . . . ?
Rh4 N7 C16 C15 -12.3(11) . . . . ?
N8 C15 C16 N6 171.9(9) . . . . ?
N5 C15 C16 N6 3.9(15) . . . . ?
N8 C15 C16 N7 -0.6(14) . . . . ?
N5 C15 C16 N7 -168.6(9) . . . . ?
C16 N6 C17 C22 -0.5(11) . . . . ?
Rh3 N6 C17 C22 -177.4(10) . . . . ?
C16 N6 C17 C18 179.5(11) . . . . ?
Rh3 N6 C17 C18 3(2) . . . . ?
C22 C17 C18 C19 4.1(18) . . . . ?
N6 C17 C18 C19 -176.0(12) . . . . ?
C17 C18 C19 C20 -4.3(19) . . . . ?
C18 C19 C20 C21 1(2) . . . . ?
C19 C20 C21 C22 2.5(17) . . . . ?
N6 C17 C22 N7 -2.1(12) . . . . ?
C18 C17 C22 N7 177.9(9) . . . . ?
N6 C17 C22 C21 179.7(10) . . . . ?
C18 C17 C22 C21 -0.3(17) . . . . ?
C16 N7 C22 C17 3.6(11) . . . . ?
Rh4 N7 C22 C17 -175.4(10) . . . . ?
C16 N7 C22 C21 -178.2(10) . . . . ?
Rh4 N7 C22 C21 3(2) . . . . ?
C20 C21 C22 C17 -2.9(16) . . . . ?
C20 C21 C22 N7 179.3(10) . . . . ?
C15 N8 C23 C24 176.2(11) . . . . ?
Rh4 N8 C23 C24 -6(2) . . . . ?
C15 N8 C23 C28 0.7(10) . . . . ?
Rh4 N8 C23 C28 178.1(9) . . . . ?
N8 C23 C24 C25 -174.0(10) . . . . ?
C28 C23 C24 C25 1.0(15) . . . . ?
C23 C24 C25 C26 -1.5(15) . . . . ?
C24 C25 C26 C27 0.7(17) . . . . ?
C25 C26 C27 C28 0.4(16) . . . . ?
C15 N5 C28 C27 -176.4(10) . . . . ?
Rh3 N5 C28 C27 10(2) . . . . ?
C15 N5 C28 C23 0.4(11) . . . . ?
Rh3 N5 C28 C23 -173.6(10) . . . . ?
C26 C27 C28 N5 175.5(10) . . . . ?
C26 C27 C28 C23 -0.9(15) . . . . ?
C24 C23 C28 N5 -176.9(9) . . . . ?
N8 C23 C28 N5 -0.7(11) . . . . ?
C24 C23 C28 C27 0.2(15) . . . . ?
N8 C23 C28 C27 176.4(9) . . . . ?
C37 N11 C29 N10 -0.1(11) . . . . ?
Rh6 N11 C29 N10 -175.2(6) . . . . ?
C37 N11 C29 C30 -172.3(8) . . . . ?
Rh6 N11 C29 C30 12.6(9) . . . . ?
C42 N10 C29 N11 0.0(10) . . . . ?
Rh5 N10 C29 N11 177.7(6) . . . . ?
C42 N10 C29 C30 172.0(8) . . . . ?
Rh5 N10 C29 C30 -10.2(10) . . . . ?
C36 N12 C30 N9 0.3(10) . . . . ?
Rh6 N12 C30 N9 176.1(6) . . . . ?
C36 N12 C30 C29 173.8(8) . . . . ?
Rh6 N12 C30 C29 -10.4(10) . . . . ?
C31 N9 C30 N12 0.7(11) . . . . ?
Rh5 N9 C30 N12 -176.0(6) . . . . ?
C31 N9 C30 C29 -173.1(8) . . . . ?
Rh5 N9 C30 C29 10.2(9) . . . . ?
N11 C29 C30 N12 -1.9(13) . . . . ?
N10 C29 C30 N12 -173.6(9) . . . . ?
N11 C29 C30 N9 171.6(8) . . . . ?
N10 C29 C30 N9 -0.1(13) . . . . ?
C30 N9 C31 C36 -1.4(10) . . . . ?
Rh5 N9 C31 C36 172.6(9) . . . . ?
C30 N9 C31 C32 175.2(12) . . . . ?
Rh5 N9 C31 C32 -11(2) . . . . ?
N9 C31 C32 C33 -179.4(12) . . . . ?
C36 C31 C32 C33 -3.1(18) . . . . ?
C31 C32 C33 C34 6(2) . . . . ?
C32 C33 C34 C35 -6(2) . . . . ?
C33 C34 C35 C36 3(2) . . . . ?
N9 C31 C36 C35 176.7(9) . . . . ?
C32 C31 C36 C35 -0.4(16) . . . . ?
N9 C31 C36 N12 1.7(11) . . . . ?
C32 C31 C36 N12 -175.4(9) . . . . ?
C34 C35 C36 C31 0.5(16) . . . . ?
C34 C35 C36 N12 174.4(11) . . . . ?
C30 N12 C36 C31 -1.2(10) . . . . ?
Rh6 N12 C36 C31 -173.0(10) . . . . ?
C30 N12 C36 C35 -175.6(11) . . . . ?
Rh6 N12 C36 C35 13(2) . . . . ?
C29 N11 C37 C38 176.8(11) . . . . ?
Rh6 N11 C37 C38 -12(2) . . . . ?
C29 N11 C37 C42 0.2(10) . . . . ?
Rh6 N11 C37 C42 171.8(8) . . . . ?
N11 C37 C38 C39 -178.2(11) . . . . ?
C42 C37 C38 C39 -2.0(15) . . . . ?
C37 C38 C39 C40 1.8(18) . . . . ?
C38 C39 C40 C41 1(2) . . . . ?
C39 C40 C41 C42 -4(2) . . . . ?
C29 N10 C42 C37 0.2(10) . . . . ?
Rh5 N10 C42 C37 -175.6(10) . . . . ?
C29 N10 C42 C41 -176.2(10) . . . . ?
Rh5 N10 C42 C41 8(2) . . . . ?
N11 C37 C42 N10 -0.2(10) . . . . ?
C38 C37 C42 N10 -177.5(9) . . . . ?
N11 C37 C42 C41 176.7(8) . . . . ?
C38 C37 C42 C41 -0.6(14) . . . . ?
C40 C41 C42 N10 179.8(12) . . . . ?
C40 C41 C42 C37 3.6(16) . . . . ?
C56 N13 C43 N16 3.1(11) . . . . ?
Rh7 N13 C43 N16 -177.7(6) . . . . ?
C56 N13 C43 C44 -169.0(9) . . . . ?
Rh7 N13 C43 C44 10.2(10) . . . . ?
C51 N16 C43 N13 -1.4(10) . . . . ?
Rh8 N16 C43 N13 176.1(6) . . . . ?
C51 N16 C43 C44 170.7(9) . . . . ?
Rh8 N16 C43 C44 -11.7(10) . . . . ?
C45 N14 C44 N15 -2.6(11) . . . . ?
Rh7 N14 C44 N15 171.4(7) . . . . ?
C45 N14 C44 C43 174.5(9) . . . . ?
Rh7 N14 C44 C43 -11.6(11) . . . . ?
C50 N15 C44 N14 1.0(12) . . . . ?
Rh8 N15 C44 N14 -179.4(7) . . . . ?
C50 N15 C44 C43 -176.1(9) . . . . ?
Rh8 N15 C44 C43 3.5(11) . . . . ?
N13 C43 C44 N14 1.0(14) . . . . ?
N16 C43 C44 N14 -170.8(9) . . . . ?
N13 C43 C44 N15 177.9(9) . . . . ?
N16 C43 C44 N15 6.1(14) . . . . ?
C44 N14 C45 C46 -178.8(12) . . . . ?
Rh7 N14 C45 C46 12(2) . . . . ?
C44 N14 C45 C50 3.1(11) . . . . ?
Rh7 N14 C45 C50 -166.0(10) . . . . ?
N14 C45 C46 C47 177.9(12) . . . . ?
C50 C45 C46 C47 -4.2(18) . . . . ?
C45 C46 C47 C48 2(2) . . . . ?
C46 C47 C48 C49 -1(2) . . . . ?
C47 C48 C49 C50 2(2) . . . . ?
C44 N15 C50 C49 173.8(12) . . . . ?
Rh8 N15 C50 C49 -6(2) . . . . ?
C44 N15 C50 C45 1.1(11) . . . . ?
Rh8 N15 C50 C45 -178.2(10) . . . . ?
C48 C49 C50 N15 -175.6(11) . . . . ?
C48 C49 C50 C45 -3.6(17) . . . . ?
C46 C45 C50 N15 179.0(10) . . . . ?
N14 C45 C50 N15 -2.6(12) . . . . ?
C46 C45 C50 C49 5.1(17) . . . . ?
N14 C45 C50 C49 -176.5(10) . . . . ?
C43 N16 C51 C52 -174.8(10) . . . . ?
Rh8 N16 C51 C52 10(2) . . . . ?
C43 N16 C51 C56 -1.0(10) . . . . ?
Rh8 N16 C51 C56 -176.4(9) . . . . ?
N16 C51 C52 C53 175.3(10) . . . . ?
C56 C51 C52 C53 2.3(16) . . . . ?
C51 C52 C53 C54 0.4(18) . . . . ?
C52 C53 C54 C55 -2(2) . . . . ?
C53 C54 C55 C56 1.4(18) . . . . ?
C43 N13 C56 C55 177.0(10) . . . . ?
Rh7 N13 C56 C55 -1(2) . . . . ?
C43 N13 C56 C51 -3.5(10) . . . . ?
Rh7 N13 C56 C51 178.0(9) . . . . ?
C54 C55 C56 N13 -179.3(11) . . . . ?
C54 C55 C56 C51 1.3(15) . . . . ?
C52 C51 C56 N13 177.3(9) . . . . ?
N16 C51 C56 N13 2.9(11) . . . . ?
C52 C51 C56 C55 -3.1(15) . . . . ?
N16 C51 C56 C55 -177.6(9) . . . . ?
C61 N17 C57 C58 1.7(15) . . . . ?
Rh2 N17 C57 C58 -173.8(7) . . . . ?
N17 C57 C58 C59 1.3(15) . . . . ?
C57 C58 C59 C60 -1.3(15) . . . . ?
C57 C58 C59 C62 175.3(9) . . . . ?
C58 C59 C60 C61 -1.6(15) . . . . ?
C62 C59 C60 C61 -178.2(10) . . . . ?
C57 N17 C61 C60 -4.7(16) . . . . ?
Rh2 N17 C61 C60 171.0(9) . . . . ?
C59 C60 C61 N17 4.7(17) . . . . ?
C63 O1 C62 O2 0.8(15) . . . . ?
C63 O1 C62 C59 178.2(9) . . . . ?
C58 C59 C62 O2 6.1(15) . . . . ?
C60 C59 C62 O2 -177.5(10) . . . . ?
C58 C59 C62 O1 -171.3(9) . . . . ?
C60 C59 C62 O1 5.1(13) . . . . ?
C62 O1 C63 C64 -179.9(9) . . . . ?
O1 C63 C64 C69 -8.7(17) . . . . ?
O1 C63 C64 C65 171.5(11) . . . . ?
C69 C64 C65 C66 4(2) . . . . ?
C63 C64 C65 C66 -175.8(13) . . . . ?
C64 C65 C66 C67 -1(2) . . . . ?
C65 C66 C67 C68 -4.4(19) . . . . ?
C65 C66 C67 C70 -177.7(12) . . . . ?
C66 C67 C68 C69 6.9(17) . . . . ?
C70 C67 C68 C69 -179.9(11) . . . . ?
C65 C64 C69 C68 -2.0(19) . . . . ?
C63 C64 C69 C68 178.2(12) . . . . ?
C67 C68 C69 C64 -3.8(19) . . . . ?
C66 C67 C70 C71 32.6(17) . . . . ?
C68 C67 C70 C71 -140.4(12) . . . . ?
C66 C67 C70 C75 -149.2(13) . . . . ?
C68 C67 C70 C75 37.8(17) . . . . ?
C75 C70 C71 C72 -0.9(18) . . . . ?
C67 C70 C71 C72 177.3(12) . . . . ?
C70 C71 C72 C73 -1(2) . . . . ?
C71 C72 C73 C74 4(2) . . . . ?
C71 C72 C73 C76 -176.5(12) . . . . ?
C72 C73 C74 C75 -7(2) . . . . ?
C76 C73 C74 C75 173.5(14) . . . . ?
C73 C74 C75 C70 6(2) . . . . ?
C71 C70 C75 C74 -1.6(19) . . . . ?
C67 C70 C75 C74 -179.8(12) . . . . ?
C77 O3 C76 C73 171.2(10) . . . . ?
C74 C73 C76 O3 130.8(14) . . . . ?
C72 C73 C76 O3 -48.3(16) . . . . ?
C76 O3 C77 O4 6.7(17) . . . . ?
C76 O3 C77 C80 179.9(9) . . . . ?
C82 N18 C78 C79 3.6(15) . . . . ?
Rh3 N18 C78 C79 -174.8(7) . . . . ?
N18 C78 C79 C80 -0.9(15) . . . . ?
C78 C79 C80 C81 -2.4(15) . . . . ?
C78 C79 C80 C77 179.1(9) . . . . ?
O4 C77 C80 C79 14.2(18) . . . . ?
O3 C77 C80 C79 -158.6(9) . . . . ?
O4 C77 C80 C81 -164.3(12) . . . . ?
O3 C77 C80 C81 22.9(14) . . . . ?
C79 C80 C81 C82 2.9(17) . . . . ?
C77 C80 C81 C82 -178.6(11) . . . . ?
C78 N18 C82 C81 -3.0(16) . . . . ?
Rh3 N18 C82 C81 175.5(8) . . . . ?
C80 C81 C82 N18 -0.2(17) . . . . ?
C87 N19 C83 C84 3.5(14) . . . . ?
Rh4 N19 C83 C84 178.6(7) . . . . ?
N19 C83 C84 C85 -3.1(15) . . . . ?
C83 C84 C85 C86 2.0(13) . . . . ?
C83 C84 C85 C88 -179.9(9) . . . . ?
C84 C85 C86 C87 -1.4(14) . . . . ?
C88 C85 C86 C87 -179.6(9) . . . . ?
C83 N19 C87 C86 -3.0(15) . . . . ?
Rh4 N19 C87 C86 -178.0(8) . . . . ?
C85 C86 C87 N19 2.0(15) . . . . ?
C89 O5 C88 O6 -1.3(13) . . . . ?
C89 O5 C88 C85 -179.4(8) . . . . ?
C84 C85 C88 O6 7.2(14) . . . . ?
C86 C85 C88 O6 -174.8(9) . . . . ?
C84 C85 C88 O5 -174.7(8) . . . . ?
C86 C85 C88 O5 3.4(12) . . . . ?
C88 O5 C89 C90 164.8(8) . . . . ?
O5 C89 C90 C91 139.8(11) . . . . ?
O5 C89 C90 C95 -42.7(15) . . . . ?
C95 C90 C91 C92 -3(2) . . . . ?
C89 C90 C91 C92 174.2(12) . . . . ?
C90 C91 C92 C93 1(2) . . . . ?
C91 C92 C93 C94 2.9(19) . . . . ?
C91 C92 C93 C96 -179.6(11) . . . . ?
C92 C93 C94 C95 -4(2) . . . . ?
C96 C93 C94 C95 178.7(14) . . . . ?
C93 C94 C95 C90 1(3) . . . . ?
C91 C90 C95 C94 2(2) . . . . ?
C89 C90 C95 C94 -175.1(14) . . . . ?
C94 C93 C96 C97 -44.3(17) . . . . ?
C92 C93 C96 C97 138.3(12) . . . . ?
C94 C93 C96 C101 141.3(13) . . . . ?
C92 C93 C96 C101 -36.1(15) . . . . ?
C101 C96 C97 C98 -2.5(18) . . . . ?
C93 C96 C97 C98 -176.9(11) . . . . ?
C96 C97 C98 C99 1.3(18) . . . . ?
C97 C98 C99 C100 -0.7(17) . . . . ?
C97 C98 C99 C102 174.9(10) . . . . ?
C98 C99 C100 C101 1.4(16) . . . . ?
C102 C99 C100 C101 -174.1(10) . . . . ?
C97 C96 C101 C100 3.1(16) . . . . ?
C93 C96 C101 C100 177.4(10) . . . . ?
C99 C100 C101 C96 -2.6(16) . . . . ?
C100 C99 C102 O7 -101.5(11) . . . . ?
C98 C99 C102 O7 83.1(12) . . . . ?
C103 O7 C102 C99 163.7(8) . . . . ?
C102 O7 C103 O8 -0.4(13) . . . . ?
C102 O7 C103 C106 178.6(8) . . . . ?
C108 N20 C104 C105 -0.3(13) . . . . ?
Rh5 N20 C104 C105 -180.0(7) . . . . ?
N20 C104 C105 C106 -1.8(14) . . . . ?
C104 C105 C106 C107 2.9(13) . . . . ?
C104 C105 C106 C103 -177.0(8) . . . . ?
O8 C103 C106 C105 -2.2(13) . . . . ?
O7 C103 C106 C105 178.9(7) . . . . ?
O8 C103 C106 C107 178.0(9) . . . . ?
O7 C103 C106 C107 -1.0(12) . . . . ?
C105 C106 C107 C108 -1.9(13) . . . . ?
C103 C106 C107 C108 177.9(8) . . . . ?
C106 C107 C108 N20 -0.1(14) . . . . ?
C104 N20 C108 C107 1.2(14) . . . . ?
Rh5 N20 C108 C107 -179.0(7) . . . . ?
C113 N21 C109 C110 2.4(13) . . . . ?
Rh6 N21 C109 C110 -174.7(6) . . . . ?
N21 C109 C110 C111 -0.3(13) . . . . ?
C109 C110 C111 C112 -1.3(13) . . . . ?
C109 C110 C111 C114 174.3(8) . . . . ?
C110 C111 C112 C113 0.8(14) . . . . ?
C114 C111 C112 C113 -174.8(9) . . . . ?
C109 N21 C113 C112 -3.0(15) . . . . ?
Rh6 N21 C113 C112 174.2(8) . . . . ?
C111 C112 C113 N21 1.4(16) . . . . ?
C115 O9 C114 O10 2.8(15) . . . . ?
C115 O9 C114 C111 -177.6(8) . . . . ?
C112 C111 C114 O10 -167.2(10) . . . . ?
C110 C111 C114 O10 17.4(14) . . . . ?
C112 C111 C114 O9 13.2(13) . . . . ?
C110 C111 C114 O9 -162.2(8) . . . . ?
C114 O9 C115 C116 -178.4(8) . . . . ?
O9 C115 C116 C117 -119.4(12) . . . . ?
O9 C115 C116 C121 64.8(13) . . . . ?
C121 C116 C117 C118 -2(2) . . . . ?
C115 C116 C117 C118 -178.3(13) . . . . ?
C116 C117 C118 C119 -2(2) . . . . ?
C117 C118 C119 C120 4(2) . . . . ?
C117 C118 C119 C122 -175.6(14) . . . . ?
C118 C119 C120 C121 -2(2) . . . . ?
C122 C119 C120 C121 177.5(12) . . . . ?
C119 C120 C121 C116 -2(2) . . . . ?
C117 C116 C121 C120 4(2) . . . . ?
C115 C116 C121 C120 -179.9(12) . . . . ?
C118 C119 C122 C123 58(2) . . . . ?
C120 C119 C122 C123 -122.2(16) . . . . ?
C118 C119 C122 C127 -131.0(18) . . . . ?
C120 C119 C122 C127 49(2) . . . . ?
C127 C122 C123 C124 12(3) . . . . ?
C119 C122 C123 C124 -175.7(17) . . . . ?
C122 C123 C124 C125 4(3) . . . . ?
C123 C124 C125 C126 -22(3) . . . . ?
C123 C124 C125 C128 175.4(19) . . . . ?
C124 C125 C126 C127 23(3) . . . . ?
C128 C125 C126 C127 -175.9(17) . . . . ?
C123 C122 C127 C126 -10(3) . . . . ?
C119 C122 C127 C126 178.1(18) . . . . ?
C125 C126 C127 C122 -8(3) . . . . ?
C124 C125 C128 O11 -141.9(14) . . . . ?
C126 C125 C128 O11 58(2) . . . . ?
C129 O11 C128 C125 179.1(9) . . . . ?
C128 O11 C129 O12 -4.9(15) . . . . ?
C128 O11 C129 C132 175.9(9) . . . . ?
C134 N22 C130 C131 -2.2(15) . . . . ?
Rh7 N22 C130 C131 176.3(7) . . . . ?
N22 C130 C131 C132 -0.6(15) . . . . ?
C130 C131 C132 C133 3.7(15) . . . . ?
C130 C131 C132 C129 -171.3(10) . . . . ?
O12 C129 C132 C131 -170.0(11) . . . . ?
O11 C129 C132 C131 9.2(14) . . . . ?
O12 C129 C132 C133 15.0(16) . . . . ?
O11 C129 C132 C133 -165.8(8) . . . . ?
C131 C132 C133 C134 -4.1(15) . . . . ?
C129 C132 C133 C134 171.2(9) . . . . ?
C130 N22 C134 C133 1.7(15) . . . . ?
Rh7 N22 C134 C133 -176.7(8) . . . . ?
C132 C133 C134 N22 1.5(16) . . . . ?
C139 N23 C135 C136 -1.6(14) . . . . ?
Rh8 N23 C135 C136 179.5(7) . . . . ?
N23 C135 C136 C137 2.0(15) . . . . ?
C135 C136 C137 C138 -2.3(13) . . . . ?
C135 C136 C137 C140 180.0(8) . . . . ?
C136 C137 C138 C139 2.3(13) . . . . ?
C140 C137 C138 C139 -179.8(8) . . . . ?
C135 N23 C139 C138 1.6(14) . . . . ?
Rh8 N23 C139 C138 -179.5(7) . . . . ?
C137 C138 C139 N23 -2.0(14) . . . . ?
C141 O13 C140 O14 -8.2(17) . . . . ?
C141 O13 C140 C137 177.2(10) . . . . ?
C138 C137 C140 O14 2.7(14) . . . . ?
C136 C137 C140 O14 -179.6(10) . . . . ?
C138 C137 C140 O13 177.6(9) . . . . ?
C136 C137 C140 O13 -4.6(13) . . . . ?
C140 O13 C141 C142 160.2(12) . . . . ?
O13 C141 C142 C147 83.5(18) . . . . ?
O13 C141 C142 C143 -97.6(15) . . . . ?
C147 C142 C143 C144 5(2) . . . . ?
C141 C142 C143 C144 -174.3(13) . . . . ?
C142 C143 C144 C145 -3(2) . . . . ?
C143 C144 C145 C146 -2(2) . . . . ?
C143 C144 C145 C148 177.1(12) . . . . ?
C144 C145 C146 C147 5(2) . . . . ?
C148 C145 C146 C147 -173.5(12) . . . . ?
C143 C142 C147 C146 -1(2) . . . . ?
C141 C142 C147 C146 177.8(13) . . . . ?
C145 C146 C147 C142 -4(2) . . . . ?
C146 C145 C148 C153 -35.8(18) . . . . ?
C144 C145 C148 C153 145.3(13) . . . . ?
C146 C145 C148 C149 140.3(13) . . . . ?
C144 C145 C148 C149 -38.6(18) . . . . ?
C153 C148 C149 C150 2.5(19) . . . . ?
C145 C148 C149 C150 -173.9(12) . . . . ?
C148 C149 C150 C151 -1.4(19) . . . . ?
C149 C150 C151 C152 -1.1(17) . . . . ?
C149 C150 C151 C154 173.4(11) . . . . ?
C150 C151 C152 C153 2.5(17) . . . . ?
C154 C151 C152 C153 -171.8(10) . . . . ?
C149 C148 C153 C152 -1.0(17) . . . . ?
C145 C148 C153 C152 175.3(11) . . . . ?
C151 C152 C153 C148 -1.4(19) . . . . ?
C155 O15 C154 C151 160.6(8) . . . . ?
C152 C151 C154 O15 -36.5(14) . . . . ?
C150 C151 C154 O15 149.2(9) . . . . ?
C154 O15 C155 O16 -1.3(13) . . . . ?
C154 O15 C155 C158 -178.6(7) . . . . ?
C160 N24 C156 C157 -1.6(14) . . . . ?
Rh1 N24 C156 C157 178.2(7) . . . . ?
N24 C156 C157 C158 0.7(14) . . . . ?
C156 C157 C158 C159 0.2(13) . . . . ?
C156 C157 C158 C155 179.7(8) . . . . ?
O16 C155 C158 C159 -179.0(9) . . . . ?
O15 C155 C158 C159 -1.7(12) . . . . ?
O16 C155 C158 C157 1.5(13) . . . . ?
O15 C155 C158 C157 178.8(8) . . . . ?
C157 C158 C159 C160 -0.2(13) . . . . ?
C155 C158 C159 C160 -179.7(8) . . . . ?
C156 N24 C160 C159 1.6(14) . . . . ?
Rh1 N24 C160 C159 -178.2(7) . . . . ?
C158 C159 C160 N24 -0.7(15) . . . . ?
C165 C161 C162 C163 -1.2(15) . . . . ?
C166 C161 C162 C163 178.8(13) . . . . ?
Rh1 C161 C162 C163 59.5(9) . . . . ?
C165 C161 C162 C167 178.5(12) . . . . ?
C166 C161 C162 C167 -2(2) . . . . ?
Rh1 C161 C162 C167 -120.8(12) . . . . ?
C165 C161 C162 Rh1 -60.7(9) . . . . ?
C166 C161 C162 Rh1 119.3(15) . . . . ?
C161 C162 C163 C164 2.1(15) . . . . ?
C167 C162 C163 C164 -177.6(12) . . . . ?
Rh1 C162 C163 C164 61.9(10) . . . . ?
C161 C162 C163 C168 173.5(13) . . . . ?
C167 C162 C163 C168 -6(2) . . . . ?
Rh1 C162 C163 C168 -126.8(14) . . . . ?
C161 C162 C163 Rh1 -59.7(9) . . . . ?
C167 C162 C163 Rh1 120.6(11) . . . . ?
C162 C163 C164 C165 -2.1(15) . . . . ?
C168 C163 C164 C165 -173.9(13) . . . . ?
Rh1 C163 C164 C165 60.3(9) . . . . ?
C162 C163 C164 C169 179.2(14) . . . . ?
C168 C163 C164 C169 7(2) . . . . ?
Rh1 C163 C164 C169 -118.4(15) . . . . ?
C162 C163 C164 Rh1 -62.4(9) . . . . ?
C168 C163 C164 Rh1 125.8(14) . . . . ?
C162 C161 C165 C170 -173.1(17) . . . . ?
C166 C161 C165 C170 7(3) . . . . ?
Rh1 C161 C165 C170 126(2) . . . . ?
C162 C161 C165 C164 -0.1(14) . . . . ?
C166 C161 C165 C164 179.9(12) . . . . ?
Rh1 C161 C165 C164 -61.5(8) . . . . ?
C162 C161 C165 Rh1 61.4(9) . . . . ?
C166 C161 C165 Rh1 -118.6(13) . . . . ?
C163 C164 C165 C161 1.4(15) . . . . ?
C169 C164 C165 C161 -179.9(14) . . . . ?
Rh1 C164 C165 C161 62.9(9) . . . . ?
C163 C164 C165 C170 175.0(15) . . . . ?
C169 C164 C165 C170 -6(2) . . . . ?
Rh1 C164 C165 C170 -123.5(16) . . . . ?
C163 C164 C165 Rh1 -61.5(9) . . . . ?
C169 C164 C165 Rh1 117.1(15) . . . . ?
C175 C171 C172 C173 3.3(14) . . . . ?
C176 C171 C172 C173 178.7(13) . . . . ?
Rh2 C171 C172 C173 61.8(8) . . . . ?
C175 C171 C172 C177 -175.7(12) . . . . ?
C176 C171 C172 C177 0(2) . . . . ?
Rh2 C171 C172 C177 -117.2(13) . . . . ?
C175 C171 C172 Rh2 -58.5(9) . . . . ?
C176 C171 C172 Rh2 116.9(15) . . . . ?
C171 C172 C173 C174 -0.4(13) . . . . ?
C177 C172 C173 C174 178.6(12) . . . . ?
Rh2 C172 C173 C174 62.3(8) . . . . ?
C171 C172 C173 C178 175.1(11) . . . . ?
C177 C172 C173 C178 -5.9(19) . . . . ?
Rh2 C172 C173 C178 -122.2(12) . . . . ?
C171 C172 C173 Rh2 -62.7(8) . . . . ?
C177 C172 C173 Rh2 116.3(13) . . . . ?
C172 C173 C174 C175 -2.8(13) . . . . ?
C178 C173 C174 C175 -178.2(11) . . . . ?
Rh2 C173 C174 C175 58.6(8) . . . . ?
C172 C173 C174 C179 175.7(12) . . . . ?
C178 C173 C174 C179 0.3(19) . . . . ?
Rh2 C173 C174 C179 -122.9(13) . . . . ?
C172 C173 C174 Rh2 -61.4(8) . . . . ?
C178 C173 C174 Rh2 123.2(12) . . . . ?
C173 C174 C175 C171 4.7(13) . . . . ?
C179 C174 C175 C171 -173.8(12) . . . . ?
Rh2 C174 C175 C171 63.8(9) . . . . ?
C173 C174 C175 C180 174.6(12) . . . . ?
C179 C174 C175 C180 -4(2) . . . . ?
Rh2 C174 C175 C180 -126.2(14) . . . . ?
C173 C174 C175 Rh2 -59.1(8) . . . . ?
C179 C174 C175 Rh2 122.4(13) . . . . ?
C172 C171 C175 C174 -5.1(14) . . . . ?
C176 C171 C175 C174 179.0(12) . . . . ?
Rh2 C171 C175 C174 -65.3(8) . . . . ?
C172 C171 C175 C180 -174.4(14) . . . . ?
C176 C171 C175 C180 10(2) . . . . ?
Rh2 C171 C175 C180 125.3(15) . . . . ?
C172 C171 C175 Rh2 60.2(9) . . . . ?
C176 C171 C175 Rh2 -115.6(12) . . . . ?
C185 C181 C182 C187 179.8(15) . . . . ?
C186 C181 C182 C187 8(2) . . . . ?
Rh3 C181 C182 C187 -116.7(16) . . . . ?
C185 C181 C182 C183 -2.5(15) . . . . ?
C186 C181 C182 C183 -174.5(13) . . . . ?
Rh3 C181 C182 C183 61.1(9) . . . . ?
C185 C181 C182 Rh3 -63.5(9) . . . . ?
C186 C181 C182 Rh3 124.4(13) . . . . ?
C181 C182 C183 C188 177.4(15) . . . . ?
C187 C182 C183 C188 -5(2) . . . . ?
Rh3 C182 C183 C188 -121.4(16) . . . . ?
C181 C182 C183 C184 -1.1(14) . . . . ?
C187 C182 C183 C184 176.8(14) . . . . ?
Rh3 C182 C183 C184 60.1(8) . . . . ?
C181 C182 C183 Rh3 -61.2(8) . . . . ?
C187 C182 C183 Rh3 116.7(15) . . . . ?
C182 C183 C184 C185 4.2(14) . . . . ?
C188 C183 C184 C185 -174.3(15) . . . . ?
Rh3 C183 C184 C185 65.0(9) . . . . ?
C182 C183 C184 C189 178.9(13) . . . . ?
C188 C183 C184 C189 0(2) . . . . ?
Rh3 C183 C184 C189 -120.3(14) . . . . ?
C182 C183 C184 Rh3 -60.8(9) . . . . ?
C188 C183 C184 Rh3 120.7(17) . . . . ?
C182 C181 C185 C184 5.3(15) . . . . ?
C186 C181 C185 C184 176.9(14) . . . . ?
Rh3 C181 C185 C184 -56.5(10) . . . . ?
C182 C181 C185 C190 178.3(13) . . . . ?
C186 C181 C185 C190 -10(2) . . . . ?
Rh3 C181 C185 C190 116.5(14) . . . . ?
C182 C181 C185 Rh3 61.8(9) . . . . ?
C186 C181 C185 Rh3 -126.6(15) . . . . ?
C183 C184 C185 C181 -5.9(15) . . . . ?
C189 C184 C185 C181 179.3(13) . . . . ?
Rh3 C184 C185 C181 57.0(10) . . . . ?
C183 C184 C185 C190 -179.2(12) . . . . ?
C189 C184 C185 C190 6(2) . . . . ?
Rh3 C184 C185 C190 -116.3(13) . . . . ?
C183 C184 C185 Rh3 -62.9(9) . . . . ?
C189 C184 C185 Rh3 122.2(15) . . . . ?
N19 Rh4 C191 C195 -147.7(7) . . . . ?
C192 Rh4 C191 C195 116.0(10) . . . . ?
N7 Rh4 C191 C195 95.9(12) . . . . ?
C194 Rh4 C191 C195 35.5(7) . . . . ?
C193 Rh4 C191 C195 79.2(8) . . . . ?
N8 Rh4 C191 C195 -55.0(8) . . . . ?
N19 Rh4 C191 C192 96.3(7) . . . . ?
N7 Rh4 C191 C192 -20.1(15) . . . . ?
C194 Rh4 C191 C192 -80.5(7) . . . . ?
C193 Rh4 C191 C192 -36.8(6) . . . . ?
N8 Rh4 C191 C192 -171.0(6) . . . . ?
C195 Rh4 C191 C192 -116.0(10) . . . . ?
N19 Rh4 C191 C196 -22.1(13) . . . . ?
C192 Rh4 C191 C196 -118.4(15) . . . . ?
N7 Rh4 C191 C196 -138.5(12) . . . . ?
C194 Rh4 C191 C196 161.1(14) . . . . ?
C193 Rh4 C191 C196 -155.2(14) . . . . ?
N8 Rh4 C191 C196 70.6(14) . . . . ?
C195 Rh4 C191 C196 125.6(16) . . . . ?
C195 C191 C192 C193 -17.1(17) . . . . ?
C196 C191 C192 C193 -164.8(11) . . . . ?
Rh4 C191 C192 C193 60.4(8) . . . . ?
C195 C191 C192 C197 167.8(13) . . . . ?
C196 C191 C192 C197 20(2) . . . . ?
Rh4 C191 C192 C197 -114.7(13) . . . . ?
C195 C191 C192 Rh4 -77.5(14) . . . . ?
C196 C191 C192 Rh4 134.9(12) . . . . ?
C191 C192 C193 C194 5.1(13) . . . . ?
C197 C192 C193 C194 -179.6(11) . . . . ?
Rh4 C192 C193 C194 57.6(8) . . . . ?
C191 C192 C193 C198 -170.9(13) . . . . ?
C197 C192 C193 C198 4(2) . . . . ?
Rh4 C192 C193 C198 -118.4(13) . . . . ?
C191 C192 C193 Rh4 -52.5(8) . . . . ?
C197 C192 C193 Rh4 122.9(12) . . . . ?
C192 C193 C194 C199 178.4(13) . . . . ?
C198 C193 C194 C199 -5(2) . . . . ?
Rh4 C193 C194 C199 -123.7(15) . . . . ?
C192 C193 C194 C195 6.4(12) . . . . ?
C198 C193 C194 C195 -177.5(11) . . . . ?
Rh4 C193 C194 C195 64.2(7) . . . . ?
C192 C193 C194 Rh4 -57.8(8) . . . . ?
C198 C193 C194 Rh4 118.3(12) . . . . ?
C192 C191 C195 C194 21.3(16) . . . . ?
C196 C191 C195 C194 168.4(11) . . . . ?
Rh4 C191 C195 C194 -53.2(8) . . . . ?
C192 C191 C195 C200 -173.2(13) . . . . ?
C196 C191 C195 C200 -26(2) . . . . ?
Rh4 C191 C195 C200 112.3(14) . . . . ?
C192 C191 C195 Rh4 74.5(12) . . . . ?
C196 C191 C195 Rh4 -138.3(13) . . . . ?
C199 C194 C195 C191 171.2(13) . . . . ?
C193 C194 C195 C191 -16.2(13) . . . . ?
Rh4 C194 C195 C191 47.9(9) . . . . ?
C199 C194 C195 C200 4.3(19) . . . . ?
C193 C194 C195 C200 176.9(10) . . . . ?
Rh4 C194 C195 C200 -119.0(11) . . . . ?
C199 C194 C195 Rh4 123.3(13) . . . . ?
C193 C194 C195 Rh4 -64.1(7) . . . . ?
C205 C201 C202 C203 0.2(14) . . . . ?
C206 C201 C202 C203 -176.8(12) . . . . ?
Rh5 C201 C202 C203 61.6(10) . . . . ?
C205 C201 C202 C207 179.8(12) . . . . ?
C206 C201 C202 C207 2.8(19) . . . . ?
Rh5 C201 C202 C207 -118.8(13) . . . . ?
C205 C201 C202 Rh5 -61.4(7) . . . . ?
C206 C201 C202 Rh5 121.6(11) . . . . ?
C201 C202 C203 C204 0.3(17) . . . . ?
C207 C202 C203 C204 -179.3(13) . . . . ?
Rh5 C202 C203 C204 60.2(11) . . . . ?
C201 C202 C203 C208 -177.3(16) . . . . ?
C207 C202 C203 C208 3(3) . . . . ?
Rh5 C202 C203 C208 -117.4(19) . . . . ?
C201 C202 C203 Rh5 -59.9(9) . . . . ?
C207 C202 C203 Rh5 120.5(13) . . . . ?
C202 C203 C204 C205 -0.7(19) . . . . ?
C208 C203 C204 C205 176.8(17) . . . . ?
Rh5 C203 C204 C205 59.5(12) . . . . ?
C202 C203 C204 C209 -176.0(17) . . . . ?
C208 C203 C204 C209 1(3) . . . . ?
Rh5 C203 C204 C209 -115.8(19) . . . . ?
C202 C203 C204 Rh5 -60.2(10) . . . . ?
C208 C203 C204 Rh5 117(2) . . . . ?
C203 C204 C205 C201 0.9(18) . . . . ?
C209 C204 C205 C201 176.6(15) . . . . ?
Rh5 C204 C205 C201 63.3(8) . . . . ?
C203 C204 C205 C210 174.7(16) . . . . ?
C209 C204 C205 C210 -10(3) . . . . ?
Rh5 C204 C205 C210 -122.9(16) . . . . ?
C203 C204 C205 Rh5 -62.4(13) . . . . ?
C209 C204 C205 Rh5 113.3(16) . . . . ?
C202 C201 C205 C204 -0.6(13) . . . . ?
C206 C201 C205 C204 176.2(12) . . . . ?
Rh5 C201 C205 C204 -63.1(9) . . . . ?
C202 C201 C205 C210 -175.4(12) . . . . ?
C206 C201 C205 C210 1.4(18) . . . . ?
Rh5 C201 C205 C210 122.1(12) . . . . ?
C202 C201 C205 Rh5 62.5(8) . . . . ?
C206 C201 C205 Rh5 -120.6(11) . . . . ?
C215 C211 C212 C213 -1.1(11) . . . . ?
C216 C211 C212 C213 -178.8(10) . . . . ?
Rh6 C211 C212 C213 61.2(7) . . . . ?
C215 C211 C212 C217 174.2(10) . . . . ?
C216 C211 C212 C217 -3.4(16) . . . . ?
Rh6 C211 C212 C217 -123.4(11) . . . . ?
C215 C211 C212 Rh6 -62.3(6) . . . . ?
C216 C211 C212 Rh6 120.0(10) . . . . ?
C211 C212 C213 C218 176.9(11) . . . . ?
C217 C212 C213 C218 1.7(19) . . . . ?
Rh6 C212 C213 C218 -122.3(13) . . . . ?
C211 C212 C213 C214 -0.3(12) . . . . ?
C217 C212 C213 C214 -175.4(11) . . . . ?
Rh6 C212 C213 C214 60.5(7) . . . . ?
C211 C212 C213 Rh6 -60.8(7) . . . . ?
C217 C212 C213 Rh6 124.1(11) . . . . ?
C212 C213 C214 C215 1.6(12) . . . . ?
C218 C213 C214 C215 -175.7(11) . . . . ?
Rh6 C213 C214 C215 62.7(7) . . . . ?
C212 C213 C214 C219 176.6(12) . . . . ?
C218 C213 C214 C219 -1(2) . . . . ?
Rh6 C213 C214 C219 -122.3(13) . . . . ?
C212 C213 C214 Rh6 -61.2(8) . . . . ?
C218 C213 C214 Rh6 121.6(11) . . . . ?
C212 C211 C215 C214 2.1(11) . . . . ?
C216 C211 C215 C214 179.8(9) . . . . ?
Rh6 C211 C215 C214 -59.4(7) . . . . ?
C212 C211 C215 C220 178.1(11) . . . . ?
C216 C211 C215 C220 -4.2(17) . . . . ?
Rh6 C211 C215 C220 116.6(11) . . . . ?
C212 C211 C215 Rh6 61.5(6) . . . . ?
C216 C211 C215 Rh6 -120.8(10) . . . . ?
C213 C214 C215 C211 -2.3(12) . . . . ?
C219 C214 C215 C211 -177.5(11) . . . . ?
Rh6 C214 C215 C211 59.8(7) . . . . ?
C213 C214 C215 C220 -178.5(11) . . . . ?
C219 C214 C215 C220 6.3(18) . . . . ?
Rh6 C214 C215 C220 -116.4(11) . . . . ?
C213 C214 C215 Rh6 -62.0(7) . . . . ?
C219 C214 C215 Rh6 122.8(12) . . . . ?
C225 C221 C222 C223 -2.4(12) . . . . ?
C226 C221 C222 C223 -178.8(11) . . . . ?
Rh7 C221 C222 C223 60.4(8) . . . . ?
C225 C221 C222 C227 177.2(11) . . . . ?
C226 C221 C222 C227 0.8(18) . . . . ?
Rh7 C221 C222 C227 -120.0(11) . . . . ?
C225 C221 C222 Rh7 -62.7(7) . . . . ?
C226 C221 C222 Rh7 120.8(11) . . . . ?
C221 C222 C223 C228 -176.9(12) . . . . ?
C227 C222 C223 C228 3(2) . . . . ?
Rh7 C222 C223 C228 -117.9(13) . . . . ?
C221 C222 C223 C224 0.0(13) . . . . ?
C227 C222 C223 C224 -179.6(11) . . . . ?
Rh7 C222 C223 C224 59.0(8) . . . . ?
C221 C222 C223 Rh7 -59.1(8) . . . . ?
C227 C222 C223 Rh7 121.3(11) . . . . ?
C222 C223 C224 C225 2.4(13) . . . . ?
C228 C223 C224 C225 179.3(12) . . . . ?
Rh7 C223 C224 C225 63.0(8) . . . . ?
C222 C223 C224 C229 175.1(12) . . . . ?
C228 C223 C224 C229 -8(2) . . . . ?
Rh7 C223 C224 C229 -124.2(13) . . . . ?
C222 C223 C224 Rh7 -60.6(8) . . . . ?
C228 C223 C224 Rh7 116.3(13) . . . . ?
C222 C221 C225 C224 3.9(12) . . . . ?
C226 C221 C225 C224 -179.6(10) . . . . ?
Rh7 C221 C225 C224 -58.7(8) . . . . ?
C222 C221 C225 C230 -178.7(11) . . . . ?
C226 C221 C225 C230 -2.3(18) . . . . ?
Rh7 C221 C225 C230 118.7(12) . . . . ?
C222 C221 C225 Rh7 62.5(7) . . . . ?
C226 C221 C225 Rh7 -121.0(11) . . . . ?
C229 C224 C225 C221 -176.6(12) . . . . ?
C223 C224 C225 C221 -3.9(13) . . . . ?
Rh7 C224 C225 C221 59.1(8) . . . . ?
C229 C224 C225 C230 6(2) . . . . ?
C223 C224 C225 C230 178.7(11) . . . . ?
Rh7 C224 C225 C230 -118.3(12) . . . . ?
C229 C224 C225 Rh7 124.4(13) . . . . ?
C223 C224 C225 Rh7 -63.0(8) . . . . ?
C235 C231 C232 C233 0.0 . . . . ?
C236 C231 C232 C233 179.2(13) . . . . ?
Rh8 C231 C232 C233 61.9(3) . . . . ?
C235 C231 C232 C237 177.0(11) . . . . ?
C236 C231 C232 C237 -3.8(16) . . . . ?
Rh8 C231 C232 C237 -121.1(10) . . . . ?
C235 C231 C232 Rh8 -61.9(3) . . . . ?
C236 C231 C232 Rh8 117.3(13) . . . . ?
C231 C232 C233 C234 0.0 . . . . ?
C237 C232 C233 C234 -176.6(12) . . . . ?
Rh8 C232 C233 C234 61.5(3) . . . . ?
C231 C232 C233 C238 177.3(11) . . . . ?
C237 C232 C233 C238 0.8(15) . . . . ?
Rh8 C232 C233 C238 -121.2(10) . . . . ?
C231 C232 C233 Rh8 -61.5(3) . . . . ?
C237 C232 C233 Rh8 122.0(11) . . . . ?
C232 C233 C234 C235 0.0 . . . . ?
C238 C233 C234 C235 -177.3(11) . . . . ?
Rh8 C233 C234 C235 61.1(3) . . . . ?
C232 C233 C234 C239 175.9(11) . . . . ?
C238 C233 C234 C239 -1.5(14) . . . . ?
Rh8 C233 C234 C239 -123.1(10) . . . . ?
C232 C233 C234 Rh8 -61.1(3) . . . . ?
C238 C233 C234 Rh8 121.6(11) . . . . ?
C233 C234 C235 C231 0.0 . . . . ?
C239 C234 C235 C231 -175.7(11) . . . . ?
Rh8 C234 C235 C231 61.3(3) . . . . ?
C233 C234 C235 C240 -177.0(11) . . . . ?
C239 C234 C235 C240 7.3(15) . . . . ?
Rh8 C234 C235 C240 -115.7(10) . . . . ?
C233 C234 C235 Rh8 -61.3(3) . . . . ?
C239 C234 C235 Rh8 123.0(11) . . . . ?
C232 C231 C235 C234 0.0 . . . . ?
C236 C231 C235 C234 -179.4(10) . . . . ?
Rh8 C231 C235 C234 -61.8(3) . . . . ?
C232 C231 C235 C240 176.6(12) . . . . ?
C236 C231 C235 C240 -2.8(14) . . . . ?
Rh8 C231 C235 C240 114.8(11) . . . . ?
C232 C231 C235 Rh8 61.8(3) . . . . ?
C236 C231 C235 Rh8 -117.6(9) . . . . ?
O17 S1 C241 F1 -61.7(13) . . . . ?
O19 S1 C241 F1 -179.9(12) . . . . ?
O18 S1 C241 F1 56.1(13) . . . . ?
O17 S1 C241 F3 174.2(12) . . . . ?
O19 S1 C241 F3 56.1(14) . . . . ?
O18 S1 C241 F3 -68.0(14) . . . . ?
O17 S1 C241 F2 57.7(12) . . . . ?
O19 S1 C241 F2 -60.4(12) . . . . ?
O18 S1 C241 F2 175.5(11) . . . . ?
