#------------------------------------------------------------------------------
#$Date: 2023-05-05 03:37:59 +0300 (Fri, 05 May 2023) $
#$Revision: 283127 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/13/15/7131510.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7131510
loop_
_publ_author_name
'Ohms, Leon'
'Eickhoff, Liesa'
'Kramer, Pascal'
'Villinger, Alexander'
'Bresien, Jonas'
'Schulz, Axel'
_publ_section_title
;
 Coinage metal complexes of multidentate Pacman phosphane ligands.
;
_journal_issue                   35
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              5245
_journal_page_last               5248
_journal_paper_doi               10.1039/d3cc01174g
_journal_volume                  59
_journal_year                    2023
_chemical_formula_moiety         'C58 H58 Ag N8 P2 +, C F3 O3 S -, 2(C4 H8 O)'
_chemical_formula_sum            'C67 H74 Ag F3 N8 O5 P2 S'
_chemical_formula_weight         1330.21
_space_group_crystal_system      monoclinic
_space_group_IT_number           7
_space_group_name_Hall           'P -2yc'
_space_group_name_H-M_alt        'P 1 c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2022-12-14 deposited with the CCDC.	2023-04-03 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 104.971(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   20.6611(12)
_cell_length_b                   19.3470(12)
_cell_length_c                   16.2836(11)
_cell_measurement_reflns_used    9895
_cell_measurement_temperature    123(2)
_cell_measurement_theta_max      32.47
_cell_measurement_theta_min      2.80
_cell_volume                     6288.1(7)
_computing_cell_refinement       'Bruker Apex V7.51A'
_computing_data_collection       'Bruker Apex V7.51A'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'ORTEP-3v2.01 (Farrugia, 2012)'
_computing_publication_material  'SHELXL-2014/7 (Sheldrick, 2015)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2015)'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      123(2)
_diffrn_detector_area_resol_mean 10.4167
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker D8 QUEST diffractometer'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0419
_diffrn_reflns_av_unetI/netI     0.0352
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       31
_diffrn_reflns_limit_h_min       -31
_diffrn_reflns_limit_k_max       29
_diffrn_reflns_limit_k_min       -29
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            250644
_diffrn_reflns_point_group_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         32.500
_diffrn_reflns_theta_min         2.041
_diffrn_source                   'microfocus sealed tube'
_exptl_absorpt_coefficient_mu    0.471
_exptl_absorpt_correction_T_max  0.7464
_exptl_absorpt_correction_T_min  0.6730
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS-2016/2; Sheldrick, 2015)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.405
_exptl_crystal_description       block
_exptl_crystal_F_000             2768
_exptl_crystal_size_max          0.390
_exptl_crystal_size_mid          0.360
_exptl_crystal_size_min          0.240
_refine_diff_density_max         0.643
_refine_diff_density_min         -0.556
_refine_diff_density_rms         0.061
_refine_ls_abs_structure_details
;
 Refined as an inversion twin.
;
_refine_ls_abs_structure_Flack   0.489(9)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.032
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1648
_refine_ls_number_reflns         44710
_refine_ls_number_restraints     414
_refine_ls_restrained_S_all      1.044
_refine_ls_R_factor_all          0.0395
_refine_ls_R_factor_gt           0.0337
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0422P)²+2.2940P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0823
_refine_ls_wR_factor_ref         0.0860
_reflns_Friedel_coverage         0.999
_reflns_Friedel_fraction_full    0.998
_reflns_Friedel_fraction_max     0.999
_reflns_number_gt                41005
_reflns_number_total             44710
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d3cc01174g10.cif
_cod_data_source_block           is_lo22b
_cod_depositor_comments
'Adding full bibliography for 7131503--7131510.cif.'
_cod_original_sg_symbol_H-M      'P c'
_cod_database_code               7131510
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.838
_shelx_estimated_absorpt_t_max   0.895
loop_
_space_group_symop_operation_xyz
'x, y, z'
'x, -y, z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.21503(4) 0.71149(2) 0.55168(8) 0.02556(19) Uani 0.901(6) 1 d . . P A 1
Ag2 Ag 0.77882(3) 0.79402(3) 0.21007(7) 0.01972(18) Uani 0.904(8) 1 d . . P B 1
Ag1B Ag 0.2034(2) 0.71484(15) 0.5276(4) 0.0152(8) Uiso 0.099(6) 1 d . . P A 2
Ag2B Ag 0.7874(3) 0.7892(3) 0.2308(6) 0.0239(10) Uiso 0.096(8) 1 d . . P B 2
S1 S 0.26255(6) 0.77934(4) 0.07688(8) 0.0433(2) Uani 1 1 d . . . . .
S2A S 0.75828(6) 0.29571(4) 0.20438(8) 0.0333(2) Uani 0.893(3) 1 d D U P C 1
O4A O 0.7749(3) 0.3129(3) 0.1270(3) 0.0388(8) Uani 0.893(3) 1 d D U P C 1
O5A O 0.78971(19) 0.33992(19) 0.2751(2) 0.0583(8) Uani 0.893(3) 1 d D U P C 1
O6A O 0.7571(3) 0.22461(18) 0.2266(3) 0.0838(14) Uani 0.893(3) 1 d D U P C 1
C118 C 0.6706(2) 0.3238(3) 0.1831(3) 0.0486(9) Uani 0.893(3) 1 d D U P C 1
F4A F 0.63152(16) 0.2864(2) 0.1204(2) 0.0760(11) Uani 0.893(3) 1 d D U P C 1
F5A F 0.6477(2) 0.3156(3) 0.2524(3) 0.0812(14) Uani 0.893(3) 1 d D U P C 1
F6A F 0.66430(16) 0.39015(17) 0.1614(2) 0.0650(8) Uani 0.893(3) 1 d D U P C 1
S2B S 0.7312(7) 0.2760(7) 0.1850(8) 0.058(2) Uiso 0.107(3) 1 d D U P C 2
O4B O 0.767(3) 0.306(3) 0.128(3) 0.051(5) Uiso 0.107(3) 1 d D U P C 2
O5B O 0.7833(13) 0.2941(16) 0.2709(15) 0.057(4) Uiso 0.107(3) 1 d D U P C 2
O6B O 0.7034(16) 0.2174(12) 0.166(2) 0.067(5) Uiso 0.107(3) 1 d D U P C 2
C139 C 0.6691(13) 0.3404(14) 0.194(2) 0.053(3) Uiso 0.107(3) 1 d D U P C 2
F4B F 0.6215(13) 0.3417(17) 0.1237(17) 0.076(4) Uiso 0.107(3) 1 d D U P C 2
F5B F 0.6295(17) 0.329(2) 0.245(2) 0.062(5) Uiso 0.107(3) 1 d D U P C 2
F6B F 0.6946(14) 0.4014(12) 0.2036(18) 0.062(4) Uiso 0.107(3) 1 d D U P C 2
P1 P 0.14345(4) 0.77623(3) 0.61641(7) 0.01800(11) Uani 1 1 d . . . . .
P2 P 0.26749(4) 0.63668(3) 0.47021(7) 0.01657(10) Uani 1 1 d . . . . .
P3 P 0.72913(4) 0.87074(3) 0.29460(7) 0.01693(11) Uani 1 1 d . . . . .
P4 P 0.85485(4) 0.72186(3) 0.15896(7) 0.01805(11) Uani 1 1 d . . . . .
F1 F 0.35039(14) 0.73398(15) 0.21433(16) 0.0627(7) Uani 1 1 d . . . . .
F2 F 0.37618(14) 0.71028(14) 0.0999(2) 0.0645(7) Uani 1 1 d . . . . .
F3 F 0.3875(2) 0.81354(18) 0.1484(3) 0.0977(13) Uani 1 1 d . . . . .
O1 O 0.22950(16) 0.71308(15) 0.0690(2) 0.0543(7) Uani 1 1 d . . . . .
O2 O 0.2726(2) 0.80734(19) -0.00050(19) 0.0767(11) Uani 1 1 d . . . . .
O3 O 0.2392(2) 0.8261(2) 0.1311(2) 0.0844(14) Uani 1 1 d . . . . .
O7 O 0.96324(13) 0.52291(14) 0.41988(18) 0.0442(5) Uani 1 1 d . . . . .
O8 O 0.51143(16) 0.52665(15) 0.2438(2) 0.0531(7) Uani 1 1 d . . . . .
O9 O 0.48817(18) 0.99808(16) 1.0268(2) 0.0581(8) Uani 1 1 d . . . . .
N1 N 0.12328(11) 0.75100(11) 0.70920(15) 0.0202(4) Uani 1 1 d . . . . .
N2 N 0.26353(11) 0.76530(11) 0.73401(15) 0.0233(4) Uani 1 1 d . . . . .
N3 N 0.33161(12) 0.67929(11) 0.64662(15) 0.0226(4) Uani 1 1 d . . . . .
N4 N 0.28924(11) 0.55951(10) 0.52627(14) 0.0182(4) Uani 1 1 d . . . . .
N5 N 0.23357(10) 0.59955(10) 0.37184(14) 0.0178(4) Uani 1 1 d . . . . .
N6 N 0.23353(11) 0.74364(11) 0.36767(15) 0.0211(4) Uani 1 1 d . . . . .
N7 N 0.15577(11) 0.82257(11) 0.45118(15) 0.0226(4) Uani 1 1 d . . . . .
N8 N 0.06176(10) 0.78096(11) 0.55249(15) 0.0186(4) Uani 1 1 d . . . . .
N9 N 0.76577(11) 0.90917(10) 0.39142(14) 0.0193(4) Uani 1 1 d . . . . .
N10 N 0.74917(11) 0.76916(11) 0.39731(15) 0.0203(4) Uani 1 1 d . . . . .
N11 N 0.82470(11) 0.68382(11) 0.31768(14) 0.0201(4) Uani 1 1 d . . . . .
N12 N 0.93267(11) 0.70773(10) 0.23054(15) 0.0195(4) Uani 1 1 d . . . . .
N13 N 0.88475(10) 0.74045(11) 0.07176(15) 0.0207(4) Uani 1 1 d . . . . .
N14 N 0.74169(11) 0.74156(11) 0.02907(15) 0.0204(4) Uani 1 1 d . . . . .
N15 N 0.66950(11) 0.82894(11) 0.10982(14) 0.0208(4) Uani 1 1 d . . . . .
N16 N 0.71355(11) 0.94819(10) 0.23579(14) 0.0189(4) Uani 1 1 d . . . . .
C1 C 0.16981(14) 0.75345(14) 0.78939(17) 0.0252(5) Uani 1 1 d . . . . .
C2 C 0.23989(14) 0.76360(13) 0.79943(18) 0.0260(5) Uani 1 1 d . . . . .
H2 H 0.2690 0.7691 0.8547 0.031 Uiso 1 1 calc R U . . .
C3 C 0.33273(13) 0.77660(13) 0.74288(17) 0.0226(4) Uani 1 1 d . . . . .
C4 C 0.36856(14) 0.82963(13) 0.79305(18) 0.0269(5) Uani 1 1 d . . . . .
H4 H 0.3462 0.8585 0.8242 0.032 Uiso 1 1 calc R U . . .
C5 C 0.43648(14) 0.84148(13) 0.79871(18) 0.0277(5) Uani 1 1 d . . . . .
C6 C 0.46958(14) 0.79894(13) 0.75342(19) 0.0270(5) Uani 1 1 d . . . . .
C7 C 0.43424(14) 0.74513(14) 0.70498(18) 0.0265(5) Uani 1 1 d . . . . .
H7 H 0.4569 0.7157 0.6749 0.032 Uiso 1 1 calc R U . . .
C8 C 0.36639(13) 0.73309(13) 0.69917(16) 0.0226(5) Uani 1 1 d . . . . .
C9 C 0.35388(14) 0.61739(13) 0.66183(17) 0.0232(5) Uani 1 1 d . . . . .
H9 H 0.3893 0.6103 0.7115 0.028 Uiso 1 1 calc R U . . .
C10 C 0.32982(14) 0.55820(13) 0.61020(17) 0.0224(5) Uani 1 1 d . . . . .
C11 C 0.34111(17) 0.48967(15) 0.63339(19) 0.0295(6) Uani 1 1 d . . . . .
H11 H 0.3677 0.4733 0.6864 0.035 Uiso 1 1 calc R U . . .
C12 C 0.30670(16) 0.44855(13) 0.56561(19) 0.0284(5) Uani 1 1 d . . . . .
H12 H 0.3048 0.3995 0.5650 0.034 Uiso 1 1 calc R U . . .
C13 C 0.27595(13) 0.49187(12) 0.49972(17) 0.0203(4) Uani 1 1 d . . . . .
C14 C 0.23080(13) 0.47281(12) 0.41474(18) 0.0219(4) Uani 1 1 d . . . . .
C15 C 0.22610(12) 0.53017(12) 0.35032(17) 0.0200(4) Uani 1 1 d . . . . .
C16 C 0.21221(14) 0.52533(13) 0.26308(18) 0.0269(5) Uani 1 1 d . . . . .
H16 H 0.2041 0.4838 0.2309 0.032 Uiso 1 1 calc R U . . .
C17 C 0.21218(14) 0.59274(14) 0.22966(18) 0.0265(5) Uani 1 1 d . . . . .
H17 H 0.2046 0.6045 0.1713 0.032 Uiso 1 1 calc R U . . .
C18 C 0.22500(13) 0.63813(12) 0.29639(17) 0.0201(4) Uani 1 1 d . . . . .
C19 C 0.22802(13) 0.71198(12) 0.29734(18) 0.0201(4) Uani 1 1 d . . . . .
H19 H 0.2260 0.7371 0.2466 0.024 Uiso 1 1 calc R U . . .
C20 C 0.24056(12) 0.81655(12) 0.37160(16) 0.0190(4) Uani 1 1 d . . . . .
C21 C 0.28874(13) 0.84987(13) 0.33940(18) 0.0237(5) Uani 1 1 d . . . . .
H21 H 0.3154 0.8234 0.3114 0.028 Uiso 1 1 calc R U . . .
C22 C 0.29872(13) 0.92109(13) 0.34734(17) 0.0241(5) Uani 1 1 d . . . . .
C23 C 0.25799(14) 0.96054(13) 0.38591(18) 0.0254(5) Uani 1 1 d . . . . .
C24 C 0.20912(14) 0.92726(13) 0.41628(17) 0.0242(5) Uani 1 1 d . . . . .
H24 H 0.1807 0.9541 0.4412 0.029 Uiso 1 1 calc R U . . .
C25 C 0.20060(12) 0.85555(12) 0.41122(16) 0.0208(4) Uani 1 1 d . . . . .
C26 C 0.09329(13) 0.83720(13) 0.42879(17) 0.0230(5) Uani 1 1 d . . . . .
H26 H 0.0775 0.8661 0.3806 0.028 Uiso 1 1 calc R U . . .
C27 C 0.04568(13) 0.81249(13) 0.47220(17) 0.0223(4) Uani 1 1 d . . . . .
C28 C -0.02325(14) 0.81263(16) 0.44315(19) 0.0301(5) Uani 1 1 d . . . . .
H28 H -0.0484 0.8317 0.3909 0.036 Uiso 1 1 calc R U . . .
C29 C -0.04970(13) 0.77981(16) 0.50411(19) 0.0298(5) Uani 1 1 d . . . . .
H29 H -0.0959 0.7721 0.4998 0.036 Uiso 1 1 calc R U . . .
C30 C 0.00263(12) 0.76069(13) 0.57116(17) 0.0217(4) Uani 1 1 d . . . . .
C31 C 0.00056(13) 0.72086(14) 0.64950(19) 0.0249(5) Uani 1 1 d . . . . .
C32 C 0.06120(13) 0.73394(12) 0.72126(17) 0.0225(4) Uani 1 1 d . . . . .
C33 C 0.06897(15) 0.72544(15) 0.80734(19) 0.0291(5) Uani 1 1 d . . . . .
H33 H 0.0345 0.7130 0.8335 0.035 Uiso 1 1 calc R U . . .
C34 C 0.13636(16) 0.73829(16) 0.85008(19) 0.0314(6) Uani 1 1 d . . . . .
H34 H 0.1552 0.7368 0.9098 0.038 Uiso 1 1 calc R U . . .
C35 C 0.47351(16) 0.89819(15) 0.8547(2) 0.0380(7) Uani 1 1 d . . . . .
H35A H 0.4881 0.9330 0.8196 0.057 Uiso 1 1 calc R U . . .
H35B H 0.5127 0.8788 0.8955 0.057 Uiso 1 1 calc R U . . .
H35C H 0.4438 0.9198 0.8855 0.057 Uiso 1 1 calc R U . . .
C36 C 0.54229(15) 0.81029(17) 0.7556(2) 0.0359(6) Uani 1 1 d . . . . .
H36A H 0.5542 0.7814 0.7122 0.054 Uiso 1 1 calc R U . . .
H36B H 0.5705 0.7978 0.8118 0.054 Uiso 1 1 calc R U . . .
H36C H 0.5494 0.8590 0.7441 0.054 Uiso 1 1 calc R U . . .
C37 C 0.16022(15) 0.45643(16) 0.4265(2) 0.0327(6) Uani 1 1 d . . . . .
H37A H 0.1299 0.4457 0.3702 0.039 Uiso 1 1 calc R U . . .
H37B H 0.1633 0.4145 0.4622 0.039 Uiso 1 1 calc R U . . .
C38 C 0.12940(17) 0.51412(18) 0.4669(3) 0.0407(7) Uani 1 1 d . . . . .
H38A H 0.0837 0.5012 0.4679 0.061 Uiso 1 1 calc R U . . .
H38B H 0.1281 0.5566 0.4338 0.061 Uiso 1 1 calc R U . . .
H38C H 0.1564 0.5218 0.5252 0.061 Uiso 1 1 calc R U . . .
C39 C 0.25758(16) 0.40634(13) 0.38153(19) 0.0287(5) Uani 1 1 d . . . . .
H39A H 0.2585 0.3687 0.4230 0.034 Uiso 1 1 calc R U . . .
H39B H 0.2257 0.3926 0.3274 0.034 Uiso 1 1 calc R U . . .
C40 C 0.32721(16) 0.41286(16) 0.3665(2) 0.0339(6) Uani 1 1 d . . . . .
H40A H 0.3413 0.3679 0.3494 0.051 Uiso 1 1 calc R U . . .
H40B H 0.3591 0.4281 0.4190 0.051 Uiso 1 1 calc R U . . .
H40C H 0.3260 0.4468 0.3214 0.051 Uiso 1 1 calc R U . . .
C41 C 0.35360(15) 0.95402(15) 0.3151(2) 0.0325(6) Uani 1 1 d . . . . .
H41A H 0.3697 0.9210 0.2792 0.049 Uiso 1 1 calc R U . . .
H41B H 0.3907 0.9673 0.3634 0.049 Uiso 1 1 calc R U . . .
H41C H 0.3361 0.9952 0.2817 0.049 Uiso 1 1 calc R U . . .
C42 C 0.26746(18) 1.03749(15) 0.3968(2) 0.0349(6) Uani 1 1 d . . . . .
H42A H 0.3147 1.0476 0.4235 0.052 Uiso 1 1 calc R U . . .
H42B H 0.2398 1.0550 0.4329 0.052 Uiso 1 1 calc R U . . .
H42C H 0.2541 1.0600 0.3410 0.052 Uiso 1 1 calc R U . . .
C43 C -0.06392(15) 0.74025(19) 0.6766(2) 0.0377(7) Uani 1 1 d . . . . .
H43A H -0.1033 0.7282 0.6296 0.045 Uiso 1 1 calc R U . . .
H43B H -0.0659 0.7116 0.7263 0.045 Uiso 1 1 calc R U . . .
C44 C -0.06953(19) 0.8156(2) 0.6994(2) 0.0469(8) Uani 1 1 d . . . . .
H44A H -0.1124 0.8233 0.7133 0.070 Uiso 1 1 calc R U . . .
H44B H -0.0672 0.8447 0.6510 0.070 Uiso 1 1 calc R U . . .
H44C H -0.0326 0.8275 0.7486 0.070 Uiso 1 1 calc R U . . .
C45 C -0.00396(17) 0.64186(16) 0.6301(2) 0.0388(7) Uani 1 1 d . . . . .
H45A H -0.0125 0.6175 0.6797 0.047 Uiso 1 1 calc R U . . .
H45B H -0.0430 0.6336 0.5811 0.047 Uiso 1 1 calc R U . . .
C46 C 0.05730(19) 0.61004(16) 0.6104(3) 0.0417(7) Uani 1 1 d . . . . .
H46A H 0.0480 0.5616 0.5937 0.063 Uiso 1 1 calc R U . . .
H46B H 0.0952 0.6124 0.6610 0.063 Uiso 1 1 calc R U . . .
H46C H 0.0683 0.6355 0.5638 0.063 Uiso 1 1 calc R U . . .
C47 C 0.16164(12) 0.86732(12) 0.63781(16) 0.0190(4) Uani 1 1 d . . . . .
C48 C 0.11806(13) 0.90755(13) 0.67017(19) 0.0257(5) Uani 1 1 d . . . . .
H48 H 0.0794 0.8872 0.6814 0.031 Uiso 1 1 calc R U . . .
C49 C 0.13099(15) 0.97763(13) 0.6861(2) 0.0321(6) Uani 1 1 d . . . . .
H49 H 0.1017 1.0047 0.7094 0.039 Uiso 1 1 calc R U . . .
C50 C 0.18670(17) 1.00793(14) 0.6679(2) 0.0345(6) Uani 1 1 d . . . . .
H50 H 0.1950 1.0559 0.6775 0.041 Uiso 1 1 calc R U . . .
C51 C 0.23000(16) 0.96799(16) 0.63562(19) 0.0323(6) Uani 1 1 d . . . . .
H51 H 0.2678 0.9889 0.6227 0.039 Uiso 1 1 calc R U . . .
C52 C 0.21858(13) 0.89729(14) 0.62191(17) 0.0249(5) Uani 1 1 d . . . . .
H52 H 0.2494 0.8698 0.6019 0.030 Uiso 1 1 calc R U . . .
C53 C 0.34984(12) 0.66109(12) 0.45875(16) 0.0194(4) Uani 1 1 d . . . . .
C54 C 0.37811(13) 0.72507(14) 0.48547(18) 0.0248(5) Uani 1 1 d . . . . .
H54 H 0.3540 0.7580 0.5092 0.030 Uiso 1 1 calc R U . . .
C55 C 0.44194(15) 0.74081(17) 0.4773(2) 0.0366(6) Uani 1 1 d . . . . .
H55 H 0.4616 0.7843 0.4964 0.044 Uiso 1 1 calc R U . . .
C56 C 0.47672(16) 0.6938(2) 0.4420(3) 0.0431(8) Uani 1 1 d . . . . .
H56 H 0.5203 0.7049 0.4367 0.052 Uiso 1 1 calc R U . . .
C57 C 0.44849(16) 0.63003(19) 0.4139(3) 0.0413(7) Uani 1 1 d . . . . .
H57 H 0.4724 0.5978 0.3889 0.050 Uiso 1 1 calc R U . . .
C58 C 0.38514(14) 0.61372(15) 0.4226(2) 0.0300(5) Uani 1 1 d . . . . .
H58 H 0.3658 0.5701 0.4038 0.036 Uiso 1 1 calc R U . . .
C59 C 0.3476(2) 0.75807(18) 0.1381(2) 0.0427(7) Uani 1 1 d . . . . .
C60 C 0.77725(14) 0.87328(13) 0.46871(18) 0.0238(5) Uani 1 1 d . . . . .
C61 C 0.76590(14) 0.80020(13) 0.46905(18) 0.0221(5) Uani 1 1 d . . . . .
H61 H 0.7707 0.7757 0.5208 0.027 Uiso 1 1 calc R U . . .
C62 C 0.73691(12) 0.69756(12) 0.39303(16) 0.0191(4) Uani 1 1 d . . . . .
C63 C 0.68774(12) 0.66682(14) 0.42607(17) 0.0233(5) Uani 1 1 d . . . . .
H63 H 0.6615 0.6952 0.4527 0.028 Uiso 1 1 calc R U . . .
C64 C 0.67613(13) 0.59608(14) 0.42107(17) 0.0249(5) Uani 1 1 d . . . . .
C65 C 0.71455(13) 0.55373(13) 0.38228(18) 0.0243(5) Uani 1 1 d . . . . .
C66 C 0.76350(13) 0.58407(13) 0.34960(17) 0.0226(4) Uani 1 1 d . . . . .
H66 H 0.7898 0.5556 0.3233 0.027 Uiso 1 1 calc R U . . .
C67 C 0.77510(12) 0.65496(12) 0.35422(16) 0.0187(4) Uani 1 1 d . . . . .
C68 C 0.88461(13) 0.66091(13) 0.34577(17) 0.0225(4) Uani 1 1 d . . . . .
H68 H 0.8936 0.6319 0.3945 0.027 Uiso 1 1 calc R U . . .
C69 C 0.93869(12) 0.67583(13) 0.30916(18) 0.0230(5) Uani 1 1 d . . . . .
C70 C 1.00573(13) 0.66165(15) 0.3438(2) 0.0308(5) Uani 1 1 d . . . . .
H70 H 1.0242 0.6395 0.3967 0.037 Uiso 1 1 calc R U . . .
C71 C 1.04168(13) 0.68550(17) 0.2878(2) 0.0310(5) Uani 1 1 d . . . . .
H71 H 1.0889 0.6832 0.2963 0.037 Uiso 1 1 calc R U . . .
C72 C 0.99637(12) 0.71298(13) 0.21768(18) 0.0237(5) Uani 1 1 d . . . . .
C73 C 1.01065(12) 0.74904(15) 0.14338(17) 0.0245(5) Uani 1 1 d . . . . .
C74 C 0.95074(12) 0.75066(14) 0.06740(18) 0.0237(4) Uani 1 1 d . . . . .
C75 C 0.94990(14) 0.76361(15) -0.01585(18) 0.0270(5) Uani 1 1 d . . . . .
H75 H 0.9880 0.7728 -0.0365 0.032 Uiso 1 1 calc R U . . .
C76 C 0.88301(14) 0.76096(14) -0.06540(18) 0.0252(5) Uani 1 1 d . . . . .
H76 H 0.8681 0.7677 -0.1251 0.030 Uiso 1 1 calc R U . . .
C77 C 0.84325(13) 0.74671(13) -0.01131(17) 0.0222(4) Uani 1 1 d . . . . .
C78 C 0.77163(13) 0.74290(12) -0.03052(17) 0.0210(4) Uani 1 1 d . . . . .
H78 H 0.7461 0.7413 -0.0881 0.025 Uiso 1 1 calc R U . . .
C79 C 0.67132(12) 0.73532(11) 0.00978(16) 0.0170(4) Uani 1 1 d . . . . .
C80 C 0.63620(12) 0.68588(12) -0.04739(16) 0.0210(4) Uani 1 1 d . . . . .
H80 H 0.6603 0.6563 -0.0754 0.025 Uiso 1 1 calc R U . . .
C81 C 0.56685(12) 0.67885(12) -0.06441(16) 0.0213(4) Uani 1 1 d . . . . .
C82 C 0.53088(12) 0.72322(12) -0.02467(16) 0.0206(4) Uani 1 1 d . . . . .
C83 C 0.56565(12) 0.77249(12) 0.03265(16) 0.0204(4) Uani 1 1 d . . . . .
H83 H 0.5413 0.8024 0.0600 0.024 Uiso 1 1 calc R U . . .
C84 C 0.63495(12) 0.77906(12) 0.05089(15) 0.0184(4) Uani 1 1 d . . . . .
C85 C 0.64786(13) 0.89157(12) 0.09885(16) 0.0209(4) Uani 1 1 d . . . . .
H85 H 0.6123 0.9002 0.0499 0.025 Uiso 1 1 calc R U . . .
C86 C 0.67189(14) 0.94931(13) 0.15277(17) 0.0218(4) Uani 1 1 d . . . . .
C87 C 0.66074(17) 1.01796(14) 0.12902(19) 0.0291(6) Uani 1 1 d . . . . .
H87 H 0.6337 1.0342 0.0762 0.035 Uiso 1 1 calc R U . . .
C88 C 0.69652(17) 1.05943(13) 0.19687(19) 0.0288(5) Uani 1 1 d . . . . .
H88 H 0.6987 1.1085 0.1977 0.035 Uiso 1 1 calc R U . . .
C89 C 0.72774(14) 1.01559(12) 0.26186(17) 0.0214(4) Uani 1 1 d . . . . .
C90 C 0.77590(14) 1.03390(12) 0.34486(18) 0.0236(5) Uani 1 1 d . . . . .
C91 C 0.78273(13) 0.97808(12) 0.40977(18) 0.0234(5) Uani 1 1 d . . . . .
C92 C 0.80565(18) 0.98402(15) 0.4971(2) 0.0355(7) Uani 1 1 d . . . . .
H92 H 0.8215 1.0252 0.5274 0.043 Uiso 1 1 calc R U . . .
C93 C 0.80156(18) 0.91856(15) 0.53381(19) 0.0343(6) Uani 1 1 d . . . . .
H93 H 0.8135 0.9080 0.5928 0.041 Uiso 1 1 calc R U . . .
C94 C 0.70316(17) 0.47714(15) 0.3751(2) 0.0365(6) Uani 1 1 d . . . . .
H94A H 0.7287 0.4575 0.3376 0.055 Uiso 1 1 calc R U . . .
H94B H 0.6553 0.4679 0.3513 0.055 Uiso 1 1 calc R U . . .
H94C H 0.7180 0.4560 0.4315 0.055 Uiso 1 1 calc R U . . .
C95 C 0.62240(14) 0.56464(17) 0.4574(2) 0.0334(6) Uani 1 1 d . . . . .
H95A H 0.5900 0.5399 0.4124 0.050 Uiso 1 1 calc R U . . .
H95B H 0.5994 0.6014 0.4802 0.050 Uiso 1 1 calc R U . . .
H95C H 0.6430 0.5323 0.5030 0.050 Uiso 1 1 calc R U . . .
C96 C 1.03339(15) 0.82389(16) 0.1710(2) 0.0337(6) Uani 1 1 d . . . . .
H96A H 1.0715 0.8216 0.2223 0.040 Uiso 1 1 calc R U . . .
H96B H 1.0498 0.8458 0.1253 0.040 Uiso 1 1 calc R U . . .
C97 C 0.97924(18) 0.86978(16) 0.1903(2) 0.0378(6) Uani 1 1 d . . . . .
H97A H 0.9985 0.9149 0.2106 0.057 Uiso 1 1 calc R U . . .
H97B H 0.9614 0.8480 0.2342 0.057 Uiso 1 1 calc R U . . .
H97C H 0.9430 0.8760 0.1385 0.057 Uiso 1 1 calc R U . . .
C98 C 1.07002(14) 0.71234(18) 0.1184(2) 0.0353(7) Uani 1 1 d . . . . .
H98A H 1.0809 0.7387 0.0716 0.042 Uiso 1 1 calc R U . . .
H98B H 1.1098 0.7142 0.1677 0.042 Uiso 1 1 calc R U . . .
C99 C 1.05761(17) 0.6378(2) 0.0908(2) 0.0477(9) Uani 1 1 d . . . . .
H99A H 1.0963 0.6200 0.0730 0.072 Uiso 1 1 calc R U . . .
H99B H 1.0175 0.6349 0.0432 0.072 Uiso 1 1 calc R U . . .
H99C H 1.0511 0.6101 0.1385 0.072 Uiso 1 1 calc R U . . .
C100 C 0.53139(14) 0.62390(14) -0.1254(2) 0.0309(6) Uani 1 1 d . . . . .
H10A H 0.4996 0.6458 -0.1736 0.046 Uiso 1 1 calc R U . . .
H10B H 0.5071 0.5929 -0.0961 0.046 Uiso 1 1 calc R U . . .
H10C H 0.5644 0.5973 -0.1460 0.046 Uiso 1 1 calc R U . . .
C101 C 0.45609(13) 0.71720(14) -0.0403(2) 0.0282(5) Uani 1 1 d . . . . .
H10D H 0.4390 0.7572 -0.0155 0.042 Uiso 1 1 calc R U . . .
H10E H 0.4452 0.6747 -0.0140 0.042 Uiso 1 1 calc R U . . .
H10F H 0.4354 0.7158 -0.1016 0.042 Uiso 1 1 calc R U . . .
C102 C 0.84506(16) 1.04942(17) 0.3274(2) 0.0359(6) Uani 1 1 d . . . . .
H10G H 0.8407 1.0913 0.2915 0.043 Uiso 1 1 calc R U . . .
H10H H 0.8777 1.0598 0.3822 0.043 Uiso 1 1 calc R U . . .
C103 C 0.87301(19) 0.9911(2) 0.2838(3) 0.0467(9) Uani 1 1 d . . . . .
H10I H 0.9178 1.0037 0.2789 0.070 Uiso 1 1 calc R U . . .
H10J H 0.8434 0.9834 0.2269 0.070 Uiso 1 1 calc R U . . .
H10K H 0.8758 0.9487 0.3174 0.070 Uiso 1 1 calc R U . . .
C104 C 0.75148(16) 1.10080(13) 0.37996(19) 0.0287(5) Uani 1 1 d . . . . .
H10L H 0.7853 1.1148 0.4323 0.034 Uiso 1 1 calc R U . . .
H10M H 0.7486 1.1382 0.3376 0.034 Uiso 1 1 calc R U . . .
C105 C 0.68398(17) 1.09404(15) 0.4003(2) 0.0319(6) Uani 1 1 d . . . . .
H10N H 0.6704 1.1391 0.4176 0.048 Uiso 1 1 calc R U . . .
H10O H 0.6875 1.0608 0.4466 0.048 Uiso 1 1 calc R U . . .
H10P H 0.6505 1.0779 0.3497 0.048 Uiso 1 1 calc R U . . .
C106 C 0.64381(12) 0.85547(12) 0.30283(16) 0.0195(4) Uani 1 1 d . . . . .
C107 C 0.60899(14) 0.79658(13) 0.26851(18) 0.0235(5) Uani 1 1 d . . . . .
H10Q H 0.6298 0.7625 0.2420 0.028 Uiso 1 1 calc R U . . .
C108 C 0.54284(14) 0.78793(15) 0.2734(2) 0.0314(6) Uani 1 1 d . . . . .
H10R H 0.5184 0.7480 0.2493 0.038 Uiso 1 1 calc R U . . .
C109 C 0.51281(15) 0.83709(18) 0.3130(2) 0.0365(6) Uani 1 1 d . . . . .
H10S H 0.4679 0.8307 0.3162 0.044 Uiso 1 1 calc R U . . .
C110 C 0.54793(16) 0.89564(17) 0.3479(2) 0.0362(6) Uani 1 1 d . . . . .
H11A H 0.5273 0.9293 0.3753 0.043 Uiso 1 1 calc R U . . .
C111 C 0.61350(14) 0.90500(14) 0.3428(2) 0.0287(5) Uani 1 1 d . . . . .
H11B H 0.6377 0.9451 0.3666 0.034 Uiso 1 1 calc R U . . .
C112 C 0.82641(12) 0.63269(12) 0.14052(17) 0.0199(4) Uani 1 1 d . . . . .
C113 C 0.87119(14) 0.58062(13) 0.13350(19) 0.0276(5) Uani 1 1 d . . . . .
H11C H 0.9161 0.5919 0.1341 0.033 Uiso 1 1 calc R U . . .
C114 C 0.85005(16) 0.51184(14) 0.1256(2) 0.0340(6) Uani 1 1 d . . . . .
H11D H 0.8807 0.4763 0.1214 0.041 Uiso 1 1 calc R U . . .
C115 C 0.78464(17) 0.49533(14) 0.1238(2) 0.0331(6) Uani 1 1 d . . . . .
H11E H 0.7701 0.4486 0.1168 0.040 Uiso 1 1 calc R U . . .
C116 C 0.74057(14) 0.54655(14) 0.13215(18) 0.0277(5) Uani 1 1 d . . . . .
H11F H 0.6959 0.5349 0.1320 0.033 Uiso 1 1 calc R U . . .
C117 C 0.76090(12) 0.61527(13) 0.14079(17) 0.0211(4) Uani 1 1 d . . . . .
H11G H 0.7303 0.6503 0.1469 0.025 Uiso 1 1 calc R U . . .
C119 C 0.9539(2) 0.4871(2) 0.3416(3) 0.0546(10) Uani 1 1 d . . . . .
H11H H 0.9951 0.4888 0.3214 0.065 Uiso 1 1 calc R U . . .
H11I H 0.9165 0.5076 0.2977 0.065 Uiso 1 1 calc R U . . .
C120 C 0.9379(3) 0.4143(2) 0.3602(3) 0.0615(11) Uani 1 1 d . . . . .
H11J H 0.9792 0.3878 0.3860 0.074 Uiso 1 1 calc R U . . .
H11K H 0.9126 0.3903 0.3080 0.074 Uiso 1 1 calc R U . . .
C121 C 0.89546(19) 0.42348(19) 0.4226(3) 0.0455(8) Uani 1 1 d . . . . .
H12C H 0.9009 0.3841 0.4626 0.055 Uiso 1 1 calc R U . . .
H12D H 0.8475 0.4286 0.3928 0.055 Uiso 1 1 calc R U . . .
C122 C 0.92378(17) 0.49034(16) 0.4685(2) 0.0371(6) Uani 1 1 d . . . . .
H12E H 0.8868 0.5212 0.4736 0.045 Uiso 1 1 calc R U . . .
H12F H 0.9517 0.4798 0.5263 0.045 Uiso 1 1 calc R U . . .
C123 C 0.5221(2) 0.5987(2) 0.2312(3) 0.0517(9) Uani 1 1 d . . . . .
H12G H 0.5487 0.6200 0.2846 0.062 Uiso 1 1 calc R U . . .
H12H H 0.4787 0.6233 0.2128 0.062 Uiso 1 1 calc R U . . .
C124 C 0.5591(3) 0.6022(3) 0.1639(3) 0.0704(13) Uani 1 1 d . . . . .
H12I H 0.6080 0.5981 0.1884 0.084 Uiso 1 1 calc R U . . .
H12J H 0.5493 0.6457 0.1311 0.084 Uiso 1 1 calc R U . . .
C125 C 0.5312(3) 0.5399(3) 0.1093(3) 0.0731(14) Uani 1 1 d . . . . .
H12K H 0.4873 0.5503 0.0693 0.088 Uiso 1 1 calc R U . . .
H12L H 0.5626 0.5233 0.0769 0.088 Uiso 1 1 calc R U . . .
C126 C 0.5241(2) 0.4878(2) 0.1764(3) 0.0561(10) Uani 1 1 d . . . . .
H12M H 0.4865 0.4557 0.1530 0.067 Uiso 1 1 calc R U . . .
H12N H 0.5657 0.4606 0.1963 0.067 Uiso 1 1 calc R U . . .
C127 C 0.4727(3) 1.0656(3) 1.0492(4) 0.0806(18) Uani 1 1 d . . . . .
H12O H 0.4636 1.0964 0.9990 0.097 Uiso 1 1 calc R U . . .
H12P H 0.5105 1.0850 1.0936 0.097 Uiso 1 1 calc R U . . .
C128 C 0.4113(3) 1.0587(2) 1.0822(3) 0.0607(11) Uani 1 1 d . . . . .
H04E H 0.3698 1.0610 1.0353 0.073 Uiso 1 1 calc R U . . .
H04F H 0.4099 1.0951 1.1244 0.073 Uiso 1 1 calc R U . . .
C129 C 0.4204(3) 0.9877(3) 1.1229(3) 0.0688(13) Uani 1 1 d . . . . .
H04M H 0.4383 0.9914 1.1853 0.083 Uiso 1 1 calc R U . . .
H04N H 0.3772 0.9625 1.1106 0.083 Uiso 1 1 calc R U . . .
C130 C 0.4698(3) 0.9509(3) 1.0836(3) 0.0701(14) Uani 1 1 d . . . . .
H04K H 0.5099 0.9366 1.1283 0.084 Uiso 1 1 calc R U . . .
H04L H 0.4490 0.9092 1.0526 0.084 Uiso 1 1 calc R U . . .
O10A O 0.0503(2) 1.0080(2) 0.3726(2) 0.0555(10) Uani 0.862(7) 1 d D U P D 1
C131 C 0.0316(3) 0.9945(2) 0.4501(3) 0.0472(11) Uani 0.862(7) 1 d D . P D 1
H04G H 0.0638 0.9623 0.4867 0.057 Uiso 0.862(7) 1 calc R U P D 1
H04H H -0.0137 0.9739 0.4379 0.057 Uiso 0.862(7) 1 calc R U P D 1
C132 C 0.0328(2) 1.06363(19) 0.4931(3) 0.0405(9) Uani 0.862(7) 1 d D . P D 1
H04C H 0.0416 1.0587 0.5556 0.049 Uiso 0.862(7) 1 calc R U P D 1
H04D H -0.0097 1.0892 0.4711 0.049 Uiso 0.862(7) 1 calc R U P D 1
C133 C 0.0917(2) 1.0991(2) 0.4679(3) 0.0428(10) Uani 0.862(7) 1 d D . P D 1
H04A H 0.0891 1.1501 0.4716 0.051 Uiso 0.862(7) 1 calc R U P D 1
H04B H 0.1355 1.0831 0.5036 0.051 Uiso 0.862(7) 1 calc R U P D 1
C134 C 0.0803(3) 1.0751(3) 0.3767(3) 0.0579(14) Uani 0.862(7) 1 d D . P D 1
H04I H 0.0501 1.1074 0.3376 0.070 Uiso 0.862(7) 1 calc R U P D 1
H04J H 0.1233 1.0726 0.3606 0.070 Uiso 0.862(7) 1 calc R U P D 1
O10B O 0.0291(13) 0.9932(11) 0.3888(16) 0.054(4) Uiso 0.138(7) 1 d D U P D 2
C135 C 0.0453(17) 1.0176(15) 0.4747(15) 0.056(4) Uiso 0.138(7) 1 d D U P D 2
H13A H 0.0793 0.9870 0.5111 0.067 Uiso 0.138(7) 1 calc R U P D 2
H13B H 0.0048 1.0170 0.4964 0.067 Uiso 0.138(7) 1 calc R U P D 2
C136 C 0.072(2) 1.0891(15) 0.4777(18) 0.053(4) Uiso 0.138(7) 1 d D U P D 2
H13C H 0.1116 1.0949 0.5264 0.063 Uiso 0.138(7) 1 calc R U P D 2
H13D H 0.0373 1.1232 0.4828 0.063 Uiso 0.138(7) 1 calc R U P D 2
C137 C 0.091(2) 1.0979(16) 0.394(2) 0.059(4) Uiso 0.138(7) 1 d D U P D 2
H13E H 0.0741 1.1427 0.3670 0.071 Uiso 0.138(7) 1 calc R U P D 2
H13F H 0.1397 1.0959 0.4025 0.071 Uiso 0.138(7) 1 calc R U P D 2
C138 C 0.0572(16) 1.0387(15) 0.3388(14) 0.052(4) Uiso 0.138(7) 1 d D U P D 2
H13G H 0.0216 1.0564 0.2904 0.063 Uiso 0.138(7) 1 calc R U P D 2
H13H H 0.0904 1.0137 0.3157 0.063 Uiso 0.138(7) 1 calc R U P D 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
P1 Ag1 P2 168.95(6) . . ?
P1 Ag1 N3 116.88(8) . . ?
P2 Ag1 N3 72.59(6) . . ?
P4 Ag2 P3 164.10(8) . . ?
P4 Ag2 N15 119.27(8) . . ?
P3 Ag2 N15 76.29(6) . . ?
P2 Ag1B P1 165.9(2) . . ?
P2 Ag1B N7 121.9(2) . . ?
P1 Ag1B N7 72.17(11) . . ?
P3 Ag2B P4 171.1(3) . . ?
P3 Ag2B N11 114.3(3) . . ?
P4 Ag2B N11 72.61(18) . . ?
O3 S1 O2 116.8(2) . . ?
O3 S1 O1 112.9(3) . . ?
O2 S1 O1 115.5(2) . . ?
O3 S1 C59 103.63(18) . . ?
O2 S1 C59 103.2(2) . . ?
O1 S1 C59 102.38(17) . . ?
O6A S2A O4A 118.2(3) . . ?
O6A S2A O5A 113.7(2) . . ?
O4A S2A O5A 113.8(3) . . ?
O6A S2A C118 104.6(3) . . ?
O4A S2A C118 102.4(3) . . ?
O5A S2A C118 101.1(2) . . ?
F6A C118 F4A 108.7(4) . . ?
F6A C118 F5A 107.8(4) . . ?
F4A C118 F5A 107.7(4) . . ?
F6A C118 S2A 111.1(3) . . ?
F4A C118 S2A 110.8(4) . . ?
F5A C118 S2A 110.6(4) . . ?
O6B S2B O4B 118(3) . . ?
O6B S2B O5B 125(2) . . ?
O4B S2B O5B 98(3) . . ?
O6B S2B C139 110.3(18) . . ?
O4B S2B C139 105(3) . . ?
O5B S2B C139 96.4(15) . . ?
F6B C139 F4B 106(3) . . ?
F6B C139 F5B 112(3) . . ?
F4B C139 F5B 96(3) . . ?
F6B C139 S2B 111(2) . . ?
F4B C139 S2B 109(2) . . ?
F5B C139 S2B 120(2) . . ?
N1 P1 N8 96.97(10) . . ?
N1 P1 C47 100.95(11) . . ?
N8 P1 C47 100.61(11) . . ?
N1 P1 Ag1 123.56(8) . . ?
N8 P1 Ag1 112.33(8) . . ?
C47 P1 Ag1 118.27(8) . . ?
N1 P1 Ag1B 130.59(13) . . ?
N8 P1 Ag1B 103.49(16) . . ?
C47 P1 Ag1B 118.28(11) . . ?
N5 P2 N4 96.71(10) . . ?
N5 P2 C53 100.28(11) . . ?
N4 P2 C53 98.87(10) . . ?
N5 P2 Ag1B 119.93(17) . . ?
N4 P2 Ag1B 115.87(14) . . ?
C53 P2 Ag1B 120.64(12) . . ?
N5 P2 Ag1 128.96(8) . . ?
N4 P2 Ag1 108.55(8) . . ?
C53 P2 Ag1 117.84(8) . . ?
N9 P3 N16 96.04(10) . . ?
N9 P3 C106 101.89(11) . . ?
N16 P3 C106 97.65(11) . . ?
N9 P3 Ag2B 122.1(3) . . ?
N16 P3 Ag2B 111.6(2) . . ?
C106 P3 Ag2B 122.11(15) . . ?
N9 P3 Ag2 129.07(9) . . ?
N16 P3 Ag2 104.87(8) . . ?
C106 P3 Ag2 120.05(8) . . ?
N13 P4 N12 96.79(11) . . ?
N13 P4 C112 103.33(11) . . ?
N12 P4 C112 99.44(10) . . ?
N13 P4 Ag2 124.62(9) . . ?
N12 P4 Ag2 115.52(9) . . ?
C112 P4 Ag2 113.25(8) . . ?
N13 P4 Ag2B 131.2(2) . . ?
N12 P4 Ag2B 107.9(3) . . ?
C112 P4 Ag2B 112.82(13) . . ?
C119 O7 C122 108.6(3) . . ?
C126 O8 C123 110.0(3) . . ?
C127 O9 C130 108.0(4) . . ?
C32 N1 C1 108.2(2) . . ?
C32 N1 P1 128.93(18) . . ?
C1 N1 P1 122.49(18) . . ?
C2 N2 C3 120.7(2) . . ?
C9 N3 C8 117.9(2) . . ?
C9 N3 Ag1 124.99(18) . . ?
C8 N3 Ag1 115.66(16) . . ?
C13 N4 C10 107.9(2) . . ?
C13 N4 P2 129.92(18) . . ?
C10 N4 P2 122.09(17) . . ?
C15 N5 C18 108.2(2) . . ?
C15 N5 P2 128.92(17) . . ?
C18 N5 P2 121.13(16) . . ?
C19 N6 C20 120.1(2) . . ?
C26 N7 C25 120.1(2) . . ?
C26 N7 Ag1B 124.48(19) . . ?
C25 N7 Ag1B 112.65(17) . . ?
C30 N8 C27 108.5(2) . . ?
C30 N8 P1 128.72(18) . . ?
C27 N8 P1 122.65(17) . . ?
C91 N9 C60 107.9(2) . . ?
C91 N9 P3 129.35(18) . . ?
C60 N9 P3 122.51(17) . . ?
C61 N10 C62 120.7(2) . . ?
C68 N11 C67 116.6(2) . . ?
C68 N11 Ag2B 127.9(2) . . ?
C67 N11 Ag2B 114.08(19) . . ?
C72 N12 C69 107.9(2) . . ?
C72 N12 P4 129.25(19) . . ?
C69 N12 P4 121.96(17) . . ?
C74 N13 C77 107.4(2) . . ?
C74 N13 P4 129.22(18) . . ?
C77 N13 P4 123.36(17) . . ?
C78 N14 C79 120.4(2) . . ?
C85 N15 C84 116.8(2) . . ?
C85 N15 Ag2 124.37(17) . . ?
C84 N15 Ag2 117.88(15) . . ?
C89 N16 C86 108.1(2) . . ?
C89 N16 P3 129.94(18) . . ?
C86 N16 P3 121.14(16) . . ?
C34 C1 N1 108.0(2) . . ?
C34 C1 C2 129.0(3) . . ?
N1 C1 C2 122.7(2) . . ?
N2 C2 C1 120.1(2) . . ?
N2 C2 H2 120.0 . . ?
C1 C2 H2 120.0 . . ?
C8 C3 C4 118.8(2) . . ?
C8 C3 N2 118.5(2) . . ?
C4 C3 N2 122.7(2) . . ?
C3 C4 C5 121.9(2) . . ?
C3 C4 H4 119.0 . . ?
C5 C4 H4 119.0 . . ?
C6 C5 C4 119.2(2) . . ?
C6 C5 C35 120.6(3) . . ?
C4 C5 C35 120.2(3) . . ?
C7 C6 C5 118.9(3) . . ?
C7 C6 C36 119.6(3) . . ?
C5 C6 C36 121.5(2) . . ?
C6 C7 C8 122.1(3) . . ?
C6 C7 H7 118.9 . . ?
C8 C7 H7 118.9 . . ?
C3 C8 C7 119.1(2) . . ?
C3 C8 N3 120.5(2) . . ?
C7 C8 N3 120.3(2) . . ?
N3 C9 C10 125.5(2) . . ?
N3 C9 H9 117.3 . . ?
C10 C9 H9 117.3 . . ?
C11 C10 N4 107.4(2) . . ?
C11 C10 C9 126.8(2) . . ?
N4 C10 C9 125.8(2) . . ?
C10 C11 C12 108.4(2) . . ?
C10 C11 H11 125.8 . . ?
C12 C11 H11 125.8 . . ?
C13 C12 C11 107.8(2) . . ?
C13 C12 H12 126.1 . . ?
C11 C12 H12 126.1 . . ?
C12 C13 N4 108.5(2) . . ?
C12 C13 C14 128.2(2) . . ?
N4 C13 C14 123.1(2) . . ?
C13 C14 C15 111.8(2) . . ?
C13 C14 C39 109.4(2) . . ?
C15 C14 C39 109.3(2) . . ?
C13 C14 C37 108.4(2) . . ?
C15 C14 C37 110.0(2) . . ?
C39 C14 C37 107.8(2) . . ?
C16 C15 N5 107.8(2) . . ?
C16 C15 C14 128.6(2) . . ?
N5 C15 C14 123.5(2) . . ?
C15 C16 C17 108.3(2) . . ?
C15 C16 H16 125.9 . . ?
C17 C16 H16 125.9 . . ?
C18 C17 C16 107.8(2) . . ?
C18 C17 H17 126.1 . . ?
C16 C17 H17 126.1 . . ?
C17 C18 N5 107.9(2) . . ?
C17 C18 C19 130.4(2) . . ?
N5 C18 C19 121.6(2) . . ?
N6 C19 C18 118.8(2) . . ?
N6 C19 H19 120.6 . . ?
C18 C19 H19 120.6 . . ?
C25 C20 C21 119.3(2) . . ?
C25 C20 N6 119.6(2) . . ?
C21 C20 N6 121.1(2) . . ?
C22 C21 C20 121.6(2) . . ?
C22 C21 H21 119.2 . . ?
C20 C21 H21 119.2 . . ?
C21 C22 C23 119.3(2) . . ?
C21 C22 C41 119.4(2) . . ?
C23 C22 C41 121.3(2) . . ?
C24 C23 C22 118.9(2) . . ?
C24 C23 C42 120.0(3) . . ?
C22 C23 C42 121.1(2) . . ?
C23 C24 C25 122.0(2) . . ?
C23 C24 H24 119.0 . . ?
C25 C24 H24 119.0 . . ?
C20 C25 C24 118.9(2) . . ?
C20 C25 N7 120.4(2) . . ?
C24 C25 N7 120.5(2) . . ?
N7 C26 C27 123.8(2) . . ?
N7 C26 H26 118.1 . . ?
C27 C26 H26 118.1 . . ?
C28 C27 N8 107.2(2) . . ?
C28 C27 C26 127.5(2) . . ?
N8 C27 C26 125.3(2) . . ?
C27 C28 C29 108.2(2) . . ?
C27 C28 H28 125.9 . . ?
C29 C28 H28 125.9 . . ?
C30 C29 C28 108.3(2) . . ?
C30 C29 H29 125.9 . . ?
C28 C29 H29 125.9 . . ?
C29 C30 N8 107.8(2) . . ?
C29 C30 C31 128.6(2) . . ?
N8 C30 C31 123.4(2) . . ?
C32 C31 C30 112.0(2) . . ?
C32 C31 C43 110.1(2) . . ?
C30 C31 C43 109.4(2) . . ?
C32 C31 C45 108.5(2) . . ?
C30 C31 C45 110.2(2) . . ?
C43 C31 C45 106.5(2) . . ?
C33 C32 N1 107.7(2) . . ?
C33 C32 C31 128.8(2) . . ?
N1 C32 C31 123.2(2) . . ?
C32 C33 C34 108.8(2) . . ?
C32 C33 H33 125.6 . . ?
C34 C33 H33 125.6 . . ?
C1 C34 C33 107.4(2) . . ?
C1 C34 H34 126.3 . . ?
C33 C34 H34 126.3 . . ?
C5 C35 H35A 109.5 . . ?
C5 C35 H35B 109.5 . . ?
H35A C35 H35B 109.5 . . ?
C5 C35 H35C 109.5 . . ?
H35A C35 H35C 109.5 . . ?
H35B C35 H35C 109.5 . . ?
C6 C36 H36A 109.5 . . ?
C6 C36 H36B 109.5 . . ?
H36A C36 H36B 109.5 . . ?
C6 C36 H36C 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
C38 C37 C14 114.6(2) . . ?
C38 C37 H37A 108.6 . . ?
C14 C37 H37A 108.6 . . ?
C38 C37 H37B 108.6 . . ?
C14 C37 H37B 108.6 . . ?
H37A C37 H37B 107.6 . . ?
C37 C38 H38A 109.5 . . ?
C37 C38 H38B 109.5 . . ?
H38A C38 H38B 109.5 . . ?
C37 C38 H38C 109.5 . . ?
H38A C38 H38C 109.5 . . ?
H38B C38 H38C 109.5 . . ?
C40 C39 C14 115.0(2) . . ?
C40 C39 H39A 108.5 . . ?
C14 C39 H39A 108.5 . . ?
C40 C39 H39B 108.5 . . ?
C14 C39 H39B 108.5 . . ?
H39A C39 H39B 107.5 . . ?
C39 C40 H40A 109.5 . . ?
C39 C40 H40B 109.5 . . ?
H40A C40 H40B 109.5 . . ?
C39 C40 H40C 109.5 . . ?
H40A C40 H40C 109.5 . . ?
H40B C40 H40C 109.5 . . ?
C22 C41 H41A 109.5 . . ?
C22 C41 H41B 109.5 . . ?
H41A C41 H41B 109.5 . . ?
C22 C41 H41C 109.5 . . ?
H41A C41 H41C 109.5 . . ?
H41B C41 H41C 109.5 . . ?
C23 C42 H42A 109.5 . . ?
C23 C42 H42B 109.5 . . ?
H42A C42 H42B 109.5 . . ?
C23 C42 H42C 109.5 . . ?
H42A C42 H42C 109.5 . . ?
H42B C42 H42C 109.5 . . ?
C44 C43 C31 115.3(3) . . ?
C44 C43 H43A 108.5 . . ?
C31 C43 H43A 108.5 . . ?
C44 C43 H43B 108.5 . . ?
C31 C43 H43B 108.5 . . ?
H43A C43 H43B 107.5 . . ?
C43 C44 H44A 109.5 . . ?
C43 C44 H44B 109.5 . . ?
H44A C44 H44B 109.5 . . ?
C43 C44 H44C 109.5 . . ?
H44A C44 H44C 109.5 . . ?
H44B C44 H44C 109.5 . . ?
C46 C45 C31 115.6(2) . . ?
C46 C45 H45A 108.4 . . ?
C31 C45 H45A 108.4 . . ?
C46 C45 H45B 108.4 . . ?
C31 C45 H45B 108.4 . . ?
H45A C45 H45B 107.4 . . ?
C45 C46 H46A 109.5 . . ?
C45 C46 H46B 109.5 . . ?
H46A C46 H46B 109.5 . . ?
C45 C46 H46C 109.5 . . ?
H46A C46 H46C 109.5 . . ?
H46B C46 H46C 109.5 . . ?
C48 C47 C52 119.8(2) . . ?
C48 C47 P1 119.52(19) . . ?
C52 C47 P1 120.69(19) . . ?
C47 C48 C49 120.2(3) . . ?
C47 C48 H48 119.9 . . ?
C49 C48 H48 119.9 . . ?
C50 C49 C48 120.0(3) . . ?
C50 C49 H49 120.0 . . ?
C48 C49 H49 120.0 . . ?
C51 C50 C49 119.8(2) . . ?
C51 C50 H50 120.1 . . ?
C49 C50 H50 120.1 . . ?
C50 C51 C52 120.6(3) . . ?
C50 C51 H51 119.7 . . ?
C52 C51 H51 119.7 . . ?
C47 C52 C51 119.6(3) . . ?
C47 C52 H52 120.2 . . ?
C51 C52 H52 120.2 . . ?
C54 C53 C58 119.7(2) . . ?
C54 C53 P2 121.80(19) . . ?
C58 C53 P2 118.54(19) . . ?
C53 C54 C55 119.8(3) . . ?
C53 C54 H54 120.1 . . ?
C55 C54 H54 120.1 . . ?
C56 C55 C54 120.4(3) . . ?
C56 C55 H55 119.8 . . ?
C54 C55 H55 119.8 . . ?
C55 C56 C57 120.3(3) . . ?
C55 C56 H56 119.8 . . ?
C57 C56 H56 119.8 . . ?
C58 C57 C56 119.6(3) . . ?
C58 C57 H57 120.2 . . ?
C56 C57 H57 120.2 . . ?
C57 C58 C53 120.2(3) . . ?
C57 C58 H58 119.9 . . ?
C53 C58 H58 119.9 . . ?
F1 C59 F2 106.2(3) . . ?
F1 C59 F3 107.0(3) . . ?
F2 C59 F3 106.3(4) . . ?
F1 C59 S1 113.4(3) . . ?
F2 C59 S1 112.3(3) . . ?
F3 C59 S1 111.2(3) . . ?
C93 C60 N9 108.8(2) . . ?
C93 C60 C61 131.1(3) . . ?
N9 C60 C61 120.1(2) . . ?
N10 C61 C60 117.7(2) . . ?
N10 C61 H61 121.1 . . ?
C60 C61 H61 121.1 . . ?
C63 C62 C67 118.3(2) . . ?
C63 C62 N10 122.6(2) . . ?
C67 C62 N10 119.1(2) . . ?
C64 C63 C62 121.9(2) . . ?
C64 C63 H63 119.1 . . ?
C62 C63 H63 119.1 . . ?
C63 C64 C65 119.6(2) . . ?
C63 C64 C95 120.4(3) . . ?
C65 C64 C95 120.0(2) . . ?
C66 C65 C64 118.7(2) . . ?
C66 C65 C94 120.2(3) . . ?
C64 C65 C94 121.2(2) . . ?
C65 C66 C67 121.9(2) . . ?
C65 C66 H66 119.1 . . ?
C67 C66 H66 119.1 . . ?
C66 C67 C62 119.7(2) . . ?
C66 C67 N11 119.7(2) . . ?
C62 C67 N11 120.5(2) . . ?
N11 C68 C69 124.7(2) . . ?
N11 C68 H68 117.6 . . ?
C69 C68 H68 117.6 . . ?
C70 C69 N12 107.7(2) . . ?
C70 C69 C68 126.9(3) . . ?
N12 C69 C68 125.4(2) . . ?
C69 C70 C71 108.3(2) . . ?
C69 C70 H70 125.8 . . ?
C71 C70 H70 125.8 . . ?
C72 C71 C70 107.8(2) . . ?
C72 C71 H71 126.1 . . ?
C70 C71 H71 126.1 . . ?
C71 C72 N12 108.3(2) . . ?
C71 C72 C73 128.1(2) . . ?
N12 C72 C73 123.4(2) . . ?
C72 C73 C74 112.5(2) . . ?
C72 C73 C96 108.0(2) . . ?
C74 C73 C96 110.0(2) . . ?
C72 C73 C98 109.4(2) . . ?
C74 C73 C98 109.3(2) . . ?
C96 C73 C98 107.5(2) . . ?
C75 C74 N13 108.2(2) . . ?
C75 C74 C73 127.7(2) . . ?
N13 C74 C73 124.1(2) . . ?
C74 C75 C76 108.6(2) . . ?
C74 C75 H75 125.7 . . ?
C76 C75 H75 125.7 . . ?
C77 C76 C75 107.4(2) . . ?
C77 C76 H76 126.3 . . ?
C75 C76 H76 126.3 . . ?
C76 C77 N13 108.4(2) . . ?
C76 C77 C78 128.5(2) . . ?
N13 C77 C78 122.9(2) . . ?
N14 C78 C77 120.7(2) . . ?
N14 C78 H78 119.7 . . ?
C77 C78 H78 119.7 . . ?
C80 C79 C84 118.5(2) . . ?
C80 C79 N14 122.3(2) . . ?
C84 C79 N14 119.2(2) . . ?
C81 C80 C79 121.9(2) . . ?
C81 C80 H80 119.0 . . ?
C79 C80 H80 119.0 . . ?
C80 C81 C82 119.3(2) . . ?
C80 C81 C100 119.9(2) . . ?
C82 C81 C100 120.7(2) . . ?
C83 C82 C81 119.0(2) . . ?
C83 C82 C101 119.6(2) . . ?
C81 C82 C101 121.3(2) . . ?
C84 C83 C82 121.9(2) . . ?
C84 C83 H83 119.0 . . ?
C82 C83 H83 119.0 . . ?
C83 C84 C79 119.3(2) . . ?
C83 C84 N15 121.2(2) . . ?
C79 C84 N15 119.5(2) . . ?
N15 C85 C86 126.7(2) . . ?
N15 C85 H85 116.7 . . ?
C86 C85 H85 116.7 . . ?
C87 C86 N16 107.5(2) . . ?
C87 C86 C85 124.9(2) . . ?
N16 C86 C85 127.6(2) . . ?
C86 C87 C88 108.1(2) . . ?
C86 C87 H87 125.9 . . ?
C88 C87 H87 125.9 . . ?
C89 C88 C87 107.3(2) . . ?
C89 C88 H88 126.3 . . ?
C87 C88 H88 126.3 . . ?
N16 C89 C88 109.0(2) . . ?
N16 C89 C90 122.7(2) . . ?
C88 C89 C90 128.0(2) . . ?
C91 C90 C89 112.8(2) . . ?
C91 C90 C104 108.9(2) . . ?
C89 C90 C104 109.0(2) . . ?
C91 C90 C102 110.2(2) . . ?
C89 C90 C102 107.9(2) . . ?
C104 C90 C102 107.9(2) . . ?
C92 C91 N9 107.5(2) . . ?
C92 C91 C90 127.8(2) . . ?
N9 C91 C90 124.7(2) . . ?
C91 C92 C93 108.6(2) . . ?
C91 C92 H92 125.7 . . ?
C93 C92 H92 125.7 . . ?
C60 C93 C92 107.3(2) . . ?
C60 C93 H93 126.4 . . ?
C92 C93 H93 126.4 . . ?
C65 C94 H94A 109.5 . . ?
C65 C94 H94B 109.5 . . ?
H94A C94 H94B 109.5 . . ?
C65 C94 H94C 109.5 . . ?
H94A C94 H94C 109.5 . . ?
H94B C94 H94C 109.5 . . ?
C64 C95 H95A 109.5 . . ?
C64 C95 H95B 109.5 . . ?
H95A C95 H95B 109.5 . . ?
C64 C95 H95C 109.5 . . ?
H95A C95 H95C 109.5 . . ?
H95B C95 H95C 109.5 . . ?
C97 C96 C73 114.8(2) . . ?
C97 C96 H96A 108.6 . . ?
C73 C96 H96A 108.6 . . ?
C97 C96 H96B 108.6 . . ?
C73 C96 H96B 108.6 . . ?
H96A C96 H96B 107.5 . . ?
C96 C97 H97A 109.5 . . ?
C96 C97 H97B 109.5 . . ?
H97A C97 H97B 109.5 . . ?
C96 C97 H97C 109.5 . . ?
H97A C97 H97C 109.5 . . ?
H97B C97 H97C 109.5 . . ?
C99 C98 C73 115.3(2) . . ?
C99 C98 H98A 108.5 . . ?
C73 C98 H98A 108.5 . . ?
C99 C98 H98B 108.5 . . ?
C73 C98 H98B 108.5 . . ?
H98A C98 H98B 107.5 . . ?
C98 C99 H99A 109.5 . . ?
C98 C99 H99B 109.5 . . ?
H99A C99 H99B 109.5 . . ?
C98 C99 H99C 109.5 . . ?
H99A C99 H99C 109.5 . . ?
H99B C99 H99C 109.5 . . ?
C81 C100 H10A 109.5 . . ?
C81 C100 H10B 109.5 . . ?
H10A C100 H10B 109.5 . . ?
C81 C100 H10C 109.5 . . ?
H10A C100 H10C 109.5 . . ?
H10B C100 H10C 109.5 . . ?
C82 C101 H10D 109.5 . . ?
C82 C101 H10E 109.5 . . ?
H10D C101 H10E 109.5 . . ?
C82 C101 H10F 109.5 . . ?
H10D C101 H10F 109.5 . . ?
H10E C101 H10F 109.5 . . ?
C103 C102 C90 114.7(2) . . ?
C103 C102 H10G 108.6 . . ?
C90 C102 H10G 108.6 . . ?
C103 C102 H10H 108.6 . . ?
C90 C102 H10H 108.6 . . ?
H10G C102 H10H 107.6 . . ?
C102 C103 H10I 109.5 . . ?
C102 C103 H10J 109.5 . . ?
H10I C103 H10J 109.5 . . ?
C102 C103 H10K 109.5 . . ?
H10I C103 H10K 109.5 . . ?
H10J C103 H10K 109.5 . . ?
C105 C104 C90 114.4(2) . . ?
C105 C104 H10L 108.7 . . ?
C90 C104 H10L 108.7 . . ?
C105 C104 H10M 108.7 . . ?
C90 C104 H10M 108.7 . . ?
H10L C104 H10M 107.6 . . ?
C104 C105 H10N 109.5 . . ?
C104 C105 H10O 109.5 . . ?
H10N C105 H10O 109.5 . . ?
C104 C105 H10P 109.5 . . ?
H10N C105 H10P 109.5 . . ?
H10O C105 H10P 109.5 . . ?
C107 C106 C111 120.3(2) . . ?
C107 C106 P3 120.91(19) . . ?
C111 C106 P3 118.78(19) . . ?
C106 C107 C108 119.2(3) . . ?
C106 C107 H10Q 120.4 . . ?
C108 C107 H10Q 120.4 . . ?
C109 C108 C107 120.4(3) . . ?
C109 C108 H10R 119.8 . . ?
C107 C108 H10R 119.8 . . ?
C108 C109 C110 120.2(3) . . ?
C108 C109 H10S 119.9 . . ?
C110 C109 H10S 119.9 . . ?
C109 C110 C111 119.8(3) . . ?
C109 C110 H11A 120.1 . . ?
C111 C110 H11A 120.1 . . ?
C110 C111 C106 120.0(3) . . ?
C110 C111 H11B 120.0 . . ?
C106 C111 H11B 120.0 . . ?
C113 C112 C117 119.4(2) . . ?
C113 C112 P4 120.37(19) . . ?
C117 C112 P4 119.98(18) . . ?
C112 C113 C114 119.9(3) . . ?
C112 C113 H11C 120.0 . . ?
C114 C113 H11C 120.0 . . ?
C115 C114 C113 120.2(3) . . ?
C115 C114 H11D 119.9 . . ?
C113 C114 H11D 119.9 . . ?
C116 C115 C114 120.0(2) . . ?
C116 C115 H11E 120.0 . . ?
C114 C115 H11E 120.0 . . ?
C115 C116 C117 120.5(3) . . ?
C115 C116 H11F 119.7 . . ?
C117 C116 H11F 119.7 . . ?
C116 C117 C112 119.9(2) . . ?
C116 C117 H11G 120.1 . . ?
C112 C117 H11G 120.1 . . ?
O7 C119 C120 105.4(3) . . ?
O7 C119 H11H 110.7 . . ?
C120 C119 H11H 110.7 . . ?
O7 C119 H11I 110.7 . . ?
C120 C119 H11I 110.7 . . ?
H11H C119 H11I 108.8 . . ?
C119 C120 C121 102.8(3) . . ?
C119 C120 H11J 111.2 . . ?
C121 C120 H11J 111.2 . . ?
C119 C120 H11K 111.2 . . ?
C121 C120 H11K 111.2 . . ?
H11J C120 H11K 109.1 . . ?
C120 C121 C122 102.3(3) . . ?
C120 C121 H12C 111.3 . . ?
C122 C121 H12C 111.3 . . ?
C120 C121 H12D 111.3 . . ?
C122 C121 H12D 111.3 . . ?
H12C C121 H12D 109.2 . . ?
O7 C122 C121 107.7(3) . . ?
O7 C122 H12E 110.2 . . ?
C121 C122 H12E 110.2 . . ?
O7 C122 H12F 110.2 . . ?
C121 C122 H12F 110.2 . . ?
H12E C122 H12F 108.5 . . ?
O8 C123 C124 106.0(4) . . ?
O8 C123 H12G 110.5 . . ?
C124 C123 H12G 110.5 . . ?
O8 C123 H12H 110.5 . . ?
C124 C123 H12H 110.5 . . ?
H12G C123 H12H 108.7 . . ?
C123 C124 C125 101.8(4) . . ?
C123 C124 H12I 111.4 . . ?
C125 C124 H12I 111.4 . . ?
C123 C124 H12J 111.4 . . ?
C125 C124 H12J 111.4 . . ?
H12I C124 H12J 109.3 . . ?
C126 C125 C124 101.3(4) . . ?
C126 C125 H12K 111.5 . . ?
C124 C125 H12K 111.5 . . ?
C126 C125 H12L 111.5 . . ?
C124 C125 H12L 111.5 . . ?
H12K C125 H12L 109.3 . . ?
O8 C126 C125 106.2(4) . . ?
O8 C126 H12M 110.5 . . ?
C125 C126 H12M 110.5 . . ?
O8 C126 H12N 110.5 . . ?
C125 C126 H12N 110.5 . . ?
H12M C126 H12N 108.7 . . ?
O9 C127 C128 106.1(4) . . ?
O9 C127 H12O 110.5 . . ?
C128 C127 H12O 110.5 . . ?
O9 C127 H12P 110.5 . . ?
C128 C127 H12P 110.5 . . ?
H12O C127 H12P 108.7 . . ?
C127 C128 C129 102.5(4) . . ?
C127 C128 H04E 111.3 . . ?
C129 C128 H04E 111.3 . . ?
C127 C128 H04F 111.3 . . ?
C129 C128 H04F 111.3 . . ?
H04E C128 H04F 109.2 . . ?
C130 C129 C128 105.1(4) . . ?
C130 C129 H04M 110.7 . . ?
C128 C129 H04M 110.7 . . ?
C130 C129 H04N 110.7 . . ?
C128 C129 H04N 110.7 . . ?
H04M C129 H04N 108.8 . . ?
O9 C130 C129 107.3(4) . . ?
O9 C130 H04K 110.3 . . ?
C129 C130 H04K 110.3 . . ?
O9 C130 H04L 110.3 . . ?
C129 C130 H04L 110.3 . . ?
H04K C130 H04L 108.5 . . ?
C134 O10A C131 109.5(3) . . ?
O10A C131 C132 105.8(4) . . ?
O10A C131 H04G 110.6 . . ?
C132 C131 H04G 110.6 . . ?
O10A C131 H04H 110.6 . . ?
C132 C131 H04H 110.6 . . ?
H04G C131 H04H 108.7 . . ?
C131 C132 C133 101.0(3) . . ?
C131 C132 H04C 111.6 . . ?
C133 C132 H04C 111.6 . . ?
C131 C132 H04D 111.6 . . ?
C133 C132 H04D 111.6 . . ?
H04C C132 H04D 109.4 . . ?
C134 C133 C132 101.0(4) . . ?
C134 C133 H04A 111.6 . . ?
C132 C133 H04A 111.6 . . ?
C134 C133 H04B 111.6 . . ?
C132 C133 H04B 111.6 . . ?
H04A C133 H04B 109.4 . . ?
O10A C134 C133 106.2(5) . . ?
O10A C134 H04I 110.5 . . ?
C133 C134 H04I 110.5 . . ?
O10A C134 H04J 110.5 . . ?
C133 C134 H04J 110.5 . . ?
H04I C134 H04J 108.7 . . ?
C138 O10B C135 109.2(13) . . ?
O10B C135 C136 109.3(13) . . ?
O10B C135 H13A 109.8 . . ?
C136 C135 H13A 109.8 . . ?
O10B C135 H13B 109.8 . . ?
C136 C135 H13B 109.8 . . ?
H13A C135 H13B 108.3 . . ?
C135 C136 C137 104.5(13) . . ?
C135 C136 H13C 110.8 . . ?
C137 C136 H13C 110.8 . . ?
C135 C136 H13D 110.8 . . ?
C137 C136 H13D 110.8 . . ?
H13C C136 H13D 108.9 . . ?
C138 C137 C136 105.4(13) . . ?
C138 C137 H13E 110.7 . . ?
C136 C137 H13E 110.7 . . ?
C138 C137 H13F 110.7 . . ?
C136 C137 H13F 110.7 . . ?
H13E C137 H13F 108.8 . . ?
O10B C138 C137 108.8(13) . . ?
O10B C138 H13G 109.9 . . ?
C137 C138 H13G 109.9 . . ?
O10B C138 H13H 109.9 . . ?
C137 C138 H13H 109.9 . . ?
H13G C138 H13H 108.3 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 P1 2.3817(7) . ?
Ag1 P2 2.4025(7) . ?
Ag1 N3 2.580(3) . ?
Ag2 P4 2.4053(7) . ?
Ag2 P3 2.4252(8) . ?
Ag2 N15 2.514(3) . ?
Ag1B P2 2.356(3) . ?
Ag1B P1 2.442(4) . ?
Ag1B N7 2.496(5) . ?
Ag2B P3 2.380(5) . ?
Ag2B P4 2.418(5) . ?
Ag2B N11 2.488(9) . ?
S1 O3 1.433(3) . ?
S1 O2 1.435(3) . ?
S1 O1 1.442(3) . ?
S1 C59 1.829(4) . ?
S2A O6A 1.424(3) . ?
S2A O4A 1.429(4) . ?
S2A O5A 1.446(3) . ?
S2A C118 1.836(5) . ?
C118 F6A 1.329(6) . ?
C118 F4A 1.339(5) . ?
C118 F5A 1.341(5) . ?
S2B O6B 1.27(2) . ?
S2B O4B 1.45(2) . ?
S2B O5B 1.57(2) . ?
S2B C139 1.82(2) . ?
C139 F6B 1.28(2) . ?
C139 F4B 1.30(3) . ?
C139 F5B 1.33(2) . ?
P1 N1 1.738(2) . ?
P1 N8 1.742(2) . ?
P1 C47 1.817(2) . ?
P2 N5 1.730(2) . ?
P2 N4 1.747(2) . ?
P2 C53 1.821(2) . ?
P3 N9 1.731(2) . ?
P3 N16 1.763(2) . ?
P3 C106 1.826(2) . ?
P4 N13 1.726(2) . ?
P4 N12 1.746(2) . ?
P4 C112 1.822(2) . ?
F1 C59 1.313(4) . ?
F2 C59 1.335(4) . ?
F3 C59 1.338(5) . ?
O7 C119 1.419(5) . ?
O7 C122 1.422(4) . ?
O8 C126 1.408(5) . ?
O8 C123 1.433(5) . ?
O9 C127 1.415(6) . ?
O9 C130 1.419(6) . ?
N1 C32 1.387(3) . ?
N1 C1 1.408(3) . ?
N2 C2 1.282(4) . ?
N2 C3 1.416(3) . ?
N3 C9 1.284(3) . ?
N3 C8 1.419(3) . ?
N4 C13 1.383(3) . ?
N4 C10 1.407(3) . ?
N5 C15 1.386(3) . ?
N5 C18 1.409(3) . ?
N6 C19 1.278(3) . ?
N6 C20 1.418(3) . ?
N7 C26 1.279(3) . ?
N7 C25 1.414(3) . ?
N8 C30 1.389(3) . ?
N8 C27 1.403(3) . ?
N9 C91 1.391(3) . ?
N9 C60 1.403(3) . ?
N10 C61 1.279(3) . ?
N10 C62 1.407(3) . ?
N11 C68 1.283(3) . ?
N11 C67 1.425(3) . ?
N12 C72 1.389(3) . ?
N12 C69 1.397(3) . ?
N13 C74 1.398(3) . ?
N13 C77 1.407(3) . ?
N14 C78 1.279(3) . ?
N14 C79 1.411(3) . ?
N15 C85 1.288(3) . ?
N15 C84 1.417(3) . ?
N16 C89 1.379(3) . ?
N16 C86 1.403(3) . ?
C1 C34 1.376(4) . ?
C1 C2 1.428(4) . ?
C2 H2 0.9500 . ?
C3 C8 1.398(4) . ?
C3 C4 1.398(4) . ?
C4 C5 1.401(4) . ?
C4 H4 0.9500 . ?
C5 C6 1.396(4) . ?
C5 C35 1.503(4) . ?
C6 C7 1.393(4) . ?
C6 C36 1.510(4) . ?
C7 C8 1.400(4) . ?
C7 H7 0.9500 . ?
C9 C10 1.432(4) . ?
C9 H9 0.9500 . ?
C10 C11 1.382(4) . ?
C11 C12 1.397(4) . ?
C11 H11 0.9500 . ?
C12 C13 1.380(4) . ?
C12 H12 0.9500 . ?
C13 C14 1.501(4) . ?
C14 C15 1.513(4) . ?
C14 C39 1.551(4) . ?
C14 C37 1.552(4) . ?
C15 C16 1.378(4) . ?
C16 C17 1.413(4) . ?
C16 H16 0.9500 . ?
C17 C18 1.369(4) . ?
C17 H17 0.9500 . ?
C18 C19 1.430(3) . ?
C19 H19 0.9500 . ?
C20 C25 1.394(3) . ?
C20 C21 1.397(3) . ?
C21 C22 1.394(4) . ?
C21 H21 0.9500 . ?
C22 C23 1.399(4) . ?
C22 C41 1.508(4) . ?
C23 C24 1.392(4) . ?
C23 C42 1.506(4) . ?
C24 C25 1.398(3) . ?
C24 H24 0.9500 . ?
C26 C27 1.434(4) . ?
C26 H26 0.9500 . ?
C27 C28 1.380(4) . ?
C28 C29 1.403(4) . ?
C28 H28 0.9500 . ?
C29 C30 1.374(4) . ?
C29 H29 0.9500 . ?
C30 C31 1.500(4) . ?
C31 C32 1.498(4) . ?
C31 C43 1.554(4) . ?
C31 C45 1.559(4) . ?
C32 C33 1.379(4) . ?
C33 C34 1.409(4) . ?
C33 H33 0.9500 . ?
C34 H34 0.9500 . ?
C35 H35A 0.9800 . ?
C35 H35B 0.9800 . ?
C35 H35C 0.9800 . ?
C36 H36A 0.9800 . ?
C36 H36B 0.9800 . ?
C36 H36C 0.9800 . ?
C37 C38 1.517(5) . ?
C37 H37A 0.9900 . ?
C37 H37B 0.9900 . ?
C38 H38A 0.9800 . ?
C38 H38B 0.9800 . ?
C38 H38C 0.9800 . ?
C39 C40 1.526(5) . ?
C39 H39A 0.9900 . ?
C39 H39B 0.9900 . ?
C40 H40A 0.9800 . ?
C40 H40B 0.9800 . ?
C40 H40C 0.9800 . ?
C41 H41A 0.9800 . ?
C41 H41B 0.9800 . ?
C41 H41C 0.9800 . ?
C42 H42A 0.9800 . ?
C42 H42B 0.9800 . ?
C42 H42C 0.9800 . ?
C43 C44 1.515(5) . ?
C43 H43A 0.9900 . ?
C43 H43B 0.9900 . ?
C44 H44A 0.9800 . ?
C44 H44B 0.9800 . ?
C44 H44C 0.9800 . ?
C45 C46 1.515(5) . ?
C45 H45A 0.9900 . ?
C45 H45B 0.9900 . ?
C46 H46A 0.9800 . ?
C46 H46B 0.9800 . ?
C46 H46C 0.9800 . ?
C47 C48 1.393(3) . ?
C47 C52 1.394(4) . ?
C48 C49 1.393(4) . ?
C48 H48 0.9500 . ?
C49 C50 1.390(5) . ?
C49 H49 0.9500 . ?
C50 C51 1.384(5) . ?
C50 H50 0.9500 . ?
C51 C52 1.396(4) . ?
C51 H51 0.9500 . ?
C52 H52 0.9500 . ?
C53 C54 1.390(4) . ?
C53 C58 1.393(4) . ?
C54 C55 1.393(4) . ?
C54 H54 0.9500 . ?
C55 C56 1.375(5) . ?
C55 H55 0.9500 . ?
C56 C57 1.390(5) . ?
C56 H56 0.9500 . ?
C57 C58 1.389(4) . ?
C57 H57 0.9500 . ?
C58 H58 0.9500 . ?
C60 C93 1.367(4) . ?
C60 C61 1.433(4) . ?
C61 H61 0.9500 . ?
C62 C63 1.399(3) . ?
C62 C67 1.400(3) . ?
C63 C64 1.388(4) . ?
C63 H63 0.9500 . ?
C64 C65 1.400(4) . ?
C64 C95 1.514(4) . ?
C65 C66 1.389(4) . ?
C65 C94 1.500(4) . ?
C66 C67 1.391(3) . ?
C66 H66 0.9500 . ?
C68 C69 1.425(4) . ?
C68 H68 0.9500 . ?
C69 C70 1.381(4) . ?
C70 C71 1.396(4) . ?
C70 H70 0.9500 . ?
C71 C72 1.382(4) . ?
C71 H71 0.9500 . ?
C72 C73 1.491(4) . ?
C73 C74 1.507(4) . ?
C73 C96 1.553(4) . ?
C73 C98 1.559(4) . ?
C74 C75 1.374(4) . ?
C75 C76 1.410(4) . ?
C75 H75 0.9500 . ?
C76 C77 1.379(4) . ?
C76 H76 0.9500 . ?
C77 C78 1.433(3) . ?
C78 H78 0.9500 . ?
C79 C80 1.400(3) . ?
C79 C84 1.410(3) . ?
C80 C81 1.394(3) . ?
C80 H80 0.9500 . ?
C81 C82 1.399(3) . ?
C81 C100 1.509(3) . ?
C82 C83 1.396(3) . ?
C82 C101 1.504(3) . ?
C83 C84 1.391(3) . ?
C83 H83 0.9500 . ?
C85 C86 1.428(3) . ?
C85 H85 0.9500 . ?
C86 C87 1.386(4) . ?
C87 C88 1.410(4) . ?
C87 H87 0.9500 . ?
C88 C89 1.379(4) . ?
C88 H88 0.9500 . ?
C89 C90 1.499(4) . ?
C90 C91 1.492(4) . ?
C90 C104 1.551(4) . ?
C90 C102 1.556(4) . ?
C91 C92 1.383(4) . ?
C92 C93 1.412(4) . ?
C92 H92 0.9500 . ?
C93 H93 0.9500 . ?
C94 H94A 0.9800 . ?
C94 H94B 0.9800 . ?
C94 H94C 0.9800 . ?
C95 H95A 0.9800 . ?
C95 H95B 0.9800 . ?
C95 H95C 0.9800 . ?
C96 C97 1.523(5) . ?
C96 H96A 0.9900 . ?
C96 H96B 0.9900 . ?
C97 H97A 0.9800 . ?
C97 H97B 0.9800 . ?
C97 H97C 0.9800 . ?
C98 C99 1.513(5) . ?
C98 H98A 0.9900 . ?
C98 H98B 0.9900 . ?
C99 H99A 0.9800 . ?
C99 H99B 0.9800 . ?
C99 H99C 0.9800 . ?
C100 H10A 0.9800 . ?
C100 H10B 0.9800 . ?
C100 H10C 0.9800 . ?
C101 H10D 0.9800 . ?
C101 H10E 0.9800 . ?
C101 H10F 0.9800 . ?
C102 C103 1.524(5) . ?
C102 H10G 0.9900 . ?
C102 H10H 0.9900 . ?
C103 H10I 0.9800 . ?
C103 H10J 0.9800 . ?
C103 H10K 0.9800 . ?
C104 C105 1.520(5) . ?
C104 H10L 0.9900 . ?
C104 H10M 0.9900 . ?
C105 H10N 0.9800 . ?
C105 H10O 0.9800 . ?
C105 H10P 0.9800 . ?
C106 C107 1.386(3) . ?
C106 C111 1.395(4) . ?
C107 C108 1.399(4) . ?
C107 H10Q 0.9500 . ?
C108 C109 1.383(5) . ?
C108 H10R 0.9500 . ?
C109 C110 1.386(5) . ?
C109 H10S 0.9500 . ?
C110 C111 1.390(4) . ?
C110 H11A 0.9500 . ?
C111 H11B 0.9500 . ?
C112 C113 1.392(3) . ?
C112 C117 1.396(3) . ?
C113 C114 1.396(4) . ?
C113 H11C 0.9500 . ?
C114 C115 1.382(5) . ?
C114 H11D 0.9500 . ?
C115 C116 1.376(4) . ?
C115 H11E 0.9500 . ?
C116 C117 1.391(3) . ?
C116 H11F 0.9500 . ?
C117 H11G 0.9500 . ?
C119 C120 1.495(6) . ?
C119 H11H 0.9900 . ?
C119 H11I 0.9900 . ?
C120 C121 1.514(6) . ?
C120 H11J 0.9900 . ?
C120 H11K 0.9900 . ?
C121 C122 1.533(5) . ?
C121 H12C 0.9900 . ?
C121 H12D 0.9900 . ?
C122 H12E 0.9900 . ?
C122 H12F 0.9900 . ?
C123 C124 1.491(6) . ?
C123 H12G 0.9900 . ?
C123 H12H 0.9900 . ?
C124 C125 1.521(8) . ?
C124 H12I 0.9900 . ?
C124 H12J 0.9900 . ?
C125 C126 1.521(7) . ?
C125 H12K 0.9900 . ?
C125 H12L 0.9900 . ?
C126 H12M 0.9900 . ?
C126 H12N 0.9900 . ?
C127 C128 1.506(8) . ?
C127 H12O 0.9900 . ?
C127 H12P 0.9900 . ?
C128 C129 1.517(7) . ?
C128 H04E 0.9900 . ?
C128 H04F 0.9900 . ?
C129 C130 1.516(6) . ?
C129 H04M 0.9900 . ?
C129 H04N 0.9900 . ?
C130 H04K 0.9900 . ?
C130 H04L 0.9900 . ?
O10A C134 1.432(9) . ?
O10A C131 1.436(6) . ?
C131 C132 1.507(5) . ?
C131 H04G 0.9900 . ?
C131 H04H 0.9900 . ?
C132 C133 1.543(6) . ?
C132 H04C 0.9900 . ?
C132 H04D 0.9900 . ?
C133 C134 1.516(6) . ?
C133 H04A 0.9900 . ?
C133 H04B 0.9900 . ?
C134 H04I 0.9900 . ?
C134 H04J 0.9900 . ?
O10B C138 1.420(15) . ?
O10B C135 1.432(14) . ?
C135 C136 1.483(15) . ?
C135 H13A 0.9900 . ?
C135 H13B 0.9900 . ?
C136 C137 1.525(15) . ?
C136 H13C 0.9900 . ?
C136 H13D 0.9900 . ?
C137 C138 1.505(15) . ?
C137 H13E 0.9900 . ?
C137 H13F 0.9900 . ?
C138 H13G 0.9900 . ?
C138 H13H 0.9900 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O6A S2A C118 F6A 180.0(3) . . . . ?
O4A S2A C118 F6A -56.1(4) . . . . ?
O5A S2A C118 F6A 61.5(4) . . . . ?
O6A S2A C118 F4A -59.0(4) . . . . ?
O4A S2A C118 F4A 64.9(4) . . . . ?
O5A S2A C118 F4A -177.4(3) . . . . ?
O6A S2A C118 F5A 60.3(4) . . . . ?
O4A S2A C118 F5A -175.8(4) . . . . ?
O5A S2A C118 F5A -58.1(4) . . . . ?
O6B S2B C139 F6B -172(3) . . . . ?
O4B S2B C139 F6B -44(4) . . . . ?
O5B S2B C139 F6B 56(3) . . . . ?
O6B S2B C139 F4B -55(3) . . . . ?
O4B S2B C139 F4B 73(3) . . . . ?
O5B S2B C139 F4B 173(2) . . . . ?
O6B S2B C139 F5B 54(3) . . . . ?
O4B S2B C139 F5B -177(4) . . . . ?
O5B S2B C139 F5B -78(3) . . . . ?
N8 P1 N1 C32 5.8(2) . . . . ?
C47 P1 N1 C32 108.1(2) . . . . ?
Ag1 P1 N1 C32 -116.9(2) . . . . ?
Ag1B P1 N1 C32 -108.6(3) . . . . ?
N8 P1 N1 C1 -165.7(2) . . . . ?
C47 P1 N1 C1 -63.4(2) . . . . ?
Ag1 P1 N1 C1 71.6(2) . . . . ?
Ag1B P1 N1 C1 79.8(3) . . . . ?
N5 P2 N4 C13 -6.1(2) . . . . ?
C53 P2 N4 C13 -107.6(2) . . . . ?
Ag1B P2 N4 C13 121.9(3) . . . . ?
Ag1 P2 N4 C13 128.9(2) . . . . ?
N5 P2 N4 C10 169.4(2) . . . . ?
C53 P2 N4 C10 67.8(2) . . . . ?
Ag1B P2 N4 C10 -62.6(3) . . . . ?
Ag1 P2 N4 C10 -55.6(2) . . . . ?
N4 P2 N5 C15 1.7(2) . . . . ?
C53 P2 N5 C15 102.0(2) . . . . ?
Ag1B P2 N5 C15 -123.4(2) . . . . ?
Ag1 P2 N5 C15 -118.8(2) . . . . ?
N4 P2 N5 C18 -161.29(19) . . . . ?
C53 P2 N5 C18 -61.0(2) . . . . ?
Ag1B P2 N5 C18 73.6(2) . . . . ?
Ag1 P2 N5 C18 78.2(2) . . . . ?
N1 P1 N8 C30 -7.8(2) . . . . ?
C47 P1 N8 C30 -110.3(2) . . . . ?
Ag1 P1 N8 C30 122.9(2) . . . . ?
Ag1B P1 N8 C30 126.9(2) . . . . ?
N1 P1 N8 C27 167.16(19) . . . . ?
C47 P1 N8 C27 64.6(2) . . . . ?
Ag1 P1 N8 C27 -62.1(2) . . . . ?
Ag1B P1 N8 C27 -58.1(2) . . . . ?
N16 P3 N9 C91 -6.4(2) . . . . ?
C106 P3 N9 C91 -105.6(2) . . . . ?
Ag2B P3 N9 C91 113.8(3) . . . . ?
Ag2 P3 N9 C91 108.3(2) . . . . ?
N16 P3 N9 C60 166.8(2) . . . . ?
C106 P3 N9 C60 67.6(2) . . . . ?
Ag2B P3 N9 C60 -73.0(3) . . . . ?
Ag2 P3 N9 C60 -78.5(2) . . . . ?
N13 P4 N12 C72 1.8(2) . . . . ?
C112 P4 N12 C72 106.6(2) . . . . ?
Ag2 P4 N12 C72 -131.9(2) . . . . ?
Ag2B P4 N12 C72 -135.5(2) . . . . ?
N13 P4 N12 C69 -165.8(2) . . . . ?
C112 P4 N12 C69 -61.0(2) . . . . ?
Ag2 P4 N12 C69 60.5(2) . . . . ?
Ag2B P4 N12 C69 56.8(2) . . . . ?
N12 P4 N13 C74 -8.5(2) . . . . ?
C112 P4 N13 C74 -109.9(2) . . . . ?
Ag2 P4 N13 C74 119.0(2) . . . . ?
Ag2B P4 N13 C74 112.5(3) . . . . ?
N12 P4 N13 C77 170.2(2) . . . . ?
C112 P4 N13 C77 68.8(2) . . . . ?
Ag2 P4 N13 C77 -62.3(2) . . . . ?
Ag2B P4 N13 C77 -68.7(3) . . . . ?
N9 P3 N16 C89 0.6(2) . . . . ?
C106 P3 N16 C89 103.5(2) . . . . ?
Ag2B P3 N16 C89 -127.4(3) . . . . ?
Ag2 P3 N16 C89 -132.5(2) . . . . ?
N9 P3 N16 C86 -167.8(2) . . . . ?
C106 P3 N16 C86 -64.9(2) . . . . ?
Ag2B P3 N16 C86 64.1(3) . . . . ?
Ag2 P3 N16 C86 59.0(2) . . . . ?
C32 N1 C1 C34 -0.3(3) . . . . ?
P1 N1 C1 C34 172.84(19) . . . . ?
C32 N1 C1 C2 174.3(2) . . . . ?
P1 N1 C1 C2 -12.6(3) . . . . ?
C3 N2 C2 C1 178.8(2) . . . . ?
C34 C1 C2 N2 167.6(3) . . . . ?
N1 C1 C2 N2 -5.7(4) . . . . ?
C2 N2 C3 C8 132.5(3) . . . . ?
C2 N2 C3 C4 -47.9(4) . . . . ?
C8 C3 C4 C5 1.9(4) . . . . ?
N2 C3 C4 C5 -177.8(2) . . . . ?
C3 C4 C5 C6 -0.4(4) . . . . ?
C3 C4 C5 C35 -178.8(3) . . . . ?
C4 C5 C6 C7 -1.1(4) . . . . ?
C35 C5 C6 C7 177.4(3) . . . . ?
C4 C5 C6 C36 178.6(3) . . . . ?
C35 C5 C6 C36 -2.9(4) . . . . ?
C5 C6 C7 C8 1.1(4) . . . . ?
C36 C6 C7 C8 -178.6(3) . . . . ?
C4 C3 C8 C7 -1.8(4) . . . . ?
N2 C3 C8 C7 177.8(2) . . . . ?
C4 C3 C8 N3 -179.1(2) . . . . ?
N2 C3 C8 N3 0.5(3) . . . . ?
C6 C7 C8 C3 0.4(4) . . . . ?
C6 C7 C8 N3 177.7(2) . . . . ?
C9 N3 C8 C3 -124.1(3) . . . . ?
Ag1 N3 C8 C3 42.7(3) . . . . ?
C9 N3 C8 C7 58.7(3) . . . . ?
Ag1 N3 C8 C7 -134.5(2) . . . . ?
C8 N3 C9 C10 -172.9(3) . . . . ?
Ag1 N3 C9 C10 21.7(4) . . . . ?
C13 N4 C10 C11 0.4(3) . . . . ?
P2 N4 C10 C11 -175.9(2) . . . . ?
C13 N4 C10 C9 -178.7(3) . . . . ?
P2 N4 C10 C9 4.9(4) . . . . ?
N3 C9 C10 C11 -164.0(3) . . . . ?
N3 C9 C10 N4 15.0(4) . . . . ?
N4 C10 C11 C12 -1.4(3) . . . . ?
C9 C10 C11 C12 177.8(3) . . . . ?
C10 C11 C12 C13 1.9(4) . . . . ?
C11 C12 C13 N4 -1.6(3) . . . . ?
C11 C12 C13 C14 -177.1(3) . . . . ?
C10 N4 C13 C12 0.7(3) . . . . ?
P2 N4 C13 C12 176.7(2) . . . . ?
C10 N4 C13 C14 176.5(2) . . . . ?
P2 N4 C13 C14 -7.5(4) . . . . ?
C12 C13 C14 C15 -160.8(3) . . . . ?
N4 C13 C14 C15 24.3(3) . . . . ?
C12 C13 C14 C39 -39.4(4) . . . . ?
N4 C13 C14 C39 145.6(2) . . . . ?
C12 C13 C14 C37 77.8(3) . . . . ?
N4 C13 C14 C37 -97.1(3) . . . . ?
C18 N5 C15 C16 -0.8(3) . . . . ?
P2 N5 C15 C16 -165.49(19) . . . . ?
C18 N5 C15 C14 -179.0(2) . . . . ?
P2 N5 C15 C14 16.3(4) . . . . ?
C13 C14 C15 C16 153.5(3) . . . . ?
C39 C14 C15 C16 32.1(4) . . . . ?
C37 C14 C15 C16 -86.0(3) . . . . ?
C13 C14 C15 N5 -28.7(3) . . . . ?
C39 C14 C15 N5 -150.1(2) . . . . ?
C37 C14 C15 N5 91.8(3) . . . . ?
N5 C15 C16 C17 1.0(3) . . . . ?
C14 C15 C16 C17 179.1(2) . . . . ?
C15 C16 C17 C18 -0.9(3) . . . . ?
C16 C17 C18 N5 0.4(3) . . . . ?
C16 C17 C18 C19 -177.4(3) . . . . ?
C15 N5 C18 C17 0.2(3) . . . . ?
P2 N5 C18 C17 166.36(18) . . . . ?
C15 N5 C18 C19 178.3(2) . . . . ?
P2 N5 C18 C19 -15.6(3) . . . . ?
C20 N6 C19 C18 176.3(2) . . . . ?
C17 C18 C19 N6 172.2(3) . . . . ?
N5 C18 C19 N6 -5.4(4) . . . . ?
C19 N6 C20 C25 131.7(3) . . . . ?
C19 N6 C20 C21 -50.9(3) . . . . ?
C25 C20 C21 C22 1.2(4) . . . . ?
N6 C20 C21 C22 -176.2(2) . . . . ?
C20 C21 C22 C23 -2.2(4) . . . . ?
C20 C21 C22 C41 177.1(2) . . . . ?
C21 C22 C23 C24 0.8(4) . . . . ?
C41 C22 C23 C24 -178.5(3) . . . . ?
C21 C22 C23 C42 179.3(3) . . . . ?
C41 C22 C23 C42 -0.1(4) . . . . ?
C22 C23 C24 C25 1.6(4) . . . . ?
C42 C23 C24 C25 -176.9(3) . . . . ?
C21 C20 C25 C24 1.1(4) . . . . ?
N6 C20 C25 C24 178.6(2) . . . . ?
C21 C20 C25 N7 -174.2(2) . . . . ?
N6 C20 C25 N7 3.3(3) . . . . ?
C23 C24 C25 C20 -2.5(4) . . . . ?
C23 C24 C25 N7 172.8(2) . . . . ?
C26 N7 C25 C20 -123.2(3) . . . . ?
Ag1B N7 C25 C20 38.8(3) . . . . ?
C26 N7 C25 C24 61.5(3) . . . . ?
Ag1B N7 C25 C24 -136.5(2) . . . . ?
C25 N7 C26 C27 -172.5(2) . . . . ?
Ag1B N7 C26 C27 27.7(4) . . . . ?
C30 N8 C27 C28 1.3(3) . . . . ?
P1 N8 C27 C28 -174.56(19) . . . . ?
C30 N8 C27 C26 -176.7(2) . . . . ?
P1 N8 C27 C26 7.5(3) . . . . ?
N7 C26 C27 C28 -164.7(3) . . . . ?
N7 C26 C27 N8 12.9(4) . . . . ?
N8 C27 C28 C29 -1.5(3) . . . . ?
C26 C27 C28 C29 176.5(3) . . . . ?
C27 C28 C29 C30 1.1(3) . . . . ?
C28 C29 C30 N8 -0.3(3) . . . . ?
C28 C29 C30 C31 -176.4(3) . . . . ?
C27 N8 C30 C29 -0.6(3) . . . . ?
P1 N8 C30 C29 174.91(19) . . . . ?
C27 N8 C30 C31 175.7(2) . . . . ?
P1 N8 C30 C31 -8.7(4) . . . . ?
C29 C30 C31 C32 -157.4(3) . . . . ?
N8 C30 C31 C32 27.1(3) . . . . ?
C29 C30 C31 C43 -35.0(4) . . . . ?
N8 C30 C31 C43 149.4(2) . . . . ?
C29 C30 C31 C45 81.7(3) . . . . ?
N8 C30 C31 C45 -93.8(3) . . . . ?
C1 N1 C32 C33 -0.4(3) . . . . ?
P1 N1 C32 C33 -172.90(19) . . . . ?
C1 N1 C32 C31 -174.8(2) . . . . ?
P1 N1 C32 C31 12.7(4) . . . . ?
C30 C31 C32 C33 157.9(3) . . . . ?
C43 C31 C32 C33 35.9(4) . . . . ?
C45 C31 C32 C33 -80.2(3) . . . . ?
C30 C31 C32 N1 -29.0(3) . . . . ?
C43 C31 C32 N1 -151.0(2) . . . . ?
C45 C31 C32 N1 92.9(3) . . . . ?
N1 C32 C33 C34 0.9(3) . . . . ?
C31 C32 C33 C34 174.8(3) . . . . ?
N1 C1 C34 C33 0.8(3) . . . . ?
C2 C1 C34 C33 -173.3(3) . . . . ?
C32 C33 C34 C1 -1.1(3) . . . . ?
C13 C14 C37 C38 56.0(3) . . . . ?
C15 C14 C37 C38 -66.5(3) . . . . ?
C39 C14 C37 C38 174.4(3) . . . . ?
C13 C14 C39 C40 -62.1(3) . . . . ?
C15 C14 C39 C40 60.7(3) . . . . ?
C37 C14 C39 C40 -179.8(2) . . . . ?
C32 C31 C43 C44 62.0(3) . . . . ?
C30 C31 C43 C44 -61.5(3) . . . . ?
C45 C31 C43 C44 179.5(3) . . . . ?
C32 C31 C45 C46 -55.9(4) . . . . ?
C30 C31 C45 C46 67.1(4) . . . . ?
C43 C31 C45 C46 -174.4(3) . . . . ?
N1 P1 C47 C48 -46.4(2) . . . . ?
N8 P1 C47 C48 52.9(2) . . . . ?
Ag1 P1 C47 C48 175.59(18) . . . . ?
Ag1B P1 C47 C48 164.7(2) . . . . ?
N1 P1 C47 C52 133.8(2) . . . . ?
N8 P1 C47 C52 -126.9(2) . . . . ?
Ag1 P1 C47 C52 -4.2(2) . . . . ?
Ag1B P1 C47 C52 -15.1(3) . . . . ?
C52 C47 C48 C49 0.5(4) . . . . ?
P1 C47 C48 C49 -179.3(2) . . . . ?
C47 C48 C49 C50 1.4(4) . . . . ?
C48 C49 C50 C51 -1.4(4) . . . . ?
C49 C50 C51 C52 -0.6(4) . . . . ?
C48 C47 C52 C51 -2.4(4) . . . . ?
P1 C47 C52 C51 177.4(2) . . . . ?
C50 C51 C52 C47 2.5(4) . . . . ?
N5 P2 C53 C54 136.1(2) . . . . ?
N4 P2 C53 C54 -125.3(2) . . . . ?
Ag1B P2 C53 C54 1.9(3) . . . . ?
Ag1 P2 C53 C54 -8.8(2) . . . . ?
N5 P2 C53 C58 -44.3(2) . . . . ?
N4 P2 C53 C58 54.3(2) . . . . ?
Ag1B P2 C53 C58 -178.5(3) . . . . ?
Ag1 P2 C53 C58 170.78(19) . . . . ?
C58 C53 C54 C55 -1.2(4) . . . . ?
P2 C53 C54 C55 178.4(2) . . . . ?
C53 C54 C55 C56 0.9(5) . . . . ?
C54 C55 C56 C57 0.0(5) . . . . ?
C55 C56 C57 C58 -0.7(6) . . . . ?
C56 C57 C58 C53 0.4(5) . . . . ?
C54 C53 C58 C57 0.6(4) . . . . ?
P2 C53 C58 C57 -179.1(3) . . . . ?
O3 S1 C59 F1 55.0(3) . . . . ?
O2 S1 C59 F1 177.2(3) . . . . ?
O1 S1 C59 F1 -62.6(3) . . . . ?
O3 S1 C59 F2 175.4(3) . . . . ?
O2 S1 C59 F2 -62.5(3) . . . . ?
O1 S1 C59 F2 57.8(3) . . . . ?
O3 S1 C59 F3 -65.6(4) . . . . ?
O2 S1 C59 F3 56.6(3) . . . . ?
O1 S1 C59 F3 176.8(3) . . . . ?
C91 N9 C60 C93 -0.7(3) . . . . ?
P3 N9 C60 C93 -175.2(2) . . . . ?
C91 N9 C60 C61 -178.1(2) . . . . ?
P3 N9 C60 C61 7.4(4) . . . . ?
C62 N10 C61 C60 -179.6(2) . . . . ?
C93 C60 C61 N10 -172.7(3) . . . . ?
N9 C60 C61 N10 4.1(4) . . . . ?
C61 N10 C62 C63 58.8(3) . . . . ?
C61 N10 C62 C67 -121.2(3) . . . . ?
C67 C62 C63 C64 -0.1(4) . . . . ?
N10 C62 C63 C64 179.8(2) . . . . ?
C62 C63 C64 C65 0.2(4) . . . . ?
C62 C63 C64 C95 -179.9(2) . . . . ?
C63 C64 C65 C66 -0.1(4) . . . . ?
C95 C64 C65 C66 -180.0(2) . . . . ?
C63 C64 C65 C94 -179.5(2) . . . . ?
C95 C64 C65 C94 0.6(4) . . . . ?
C64 C65 C66 C67 -0.2(4) . . . . ?
C94 C65 C66 C67 179.3(2) . . . . ?
C65 C66 C67 C62 0.3(4) . . . . ?
C65 C66 C67 N11 -178.3(2) . . . . ?
C63 C62 C67 C66 -0.1(3) . . . . ?
N10 C62 C67 C66 180.0(2) . . . . ?
C63 C62 C67 N11 178.4(2) . . . . ?
N10 C62 C67 N11 -1.5(3) . . . . ?
C68 N11 C67 C66 -58.4(3) . . . . ?
Ag2B N11 C67 C66 134.0(3) . . . . ?
C68 N11 C67 C62 123.0(3) . . . . ?
Ag2B N11 C67 C62 -44.5(3) . . . . ?
C67 N11 C68 C69 170.5(2) . . . . ?
Ag2B N11 C68 C69 -23.9(4) . . . . ?
C72 N12 C69 C70 -0.1(3) . . . . ?
P4 N12 C69 C70 169.87(19) . . . . ?
C72 N12 C69 C68 -180.0(2) . . . . ?
P4 N12 C69 C68 -10.0(3) . . . . ?
N11 C68 C69 C70 169.2(3) . . . . ?
N11 C68 C69 N12 -10.9(4) . . . . ?
N12 C69 C70 C71 0.9(3) . . . . ?
C68 C69 C70 C71 -179.3(3) . . . . ?
C69 C70 C71 C72 -1.3(4) . . . . ?
C70 C71 C72 N12 1.3(3) . . . . ?
C70 C71 C72 C73 175.5(3) . . . . ?
C69 N12 C72 C71 -0.7(3) . . . . ?
P4 N12 C72 C71 -169.7(2) . . . . ?
C69 N12 C72 C73 -175.3(2) . . . . ?
P4 N12 C72 C73 15.7(4) . . . . ?
C71 C72 C73 C74 160.9(3) . . . . ?
N12 C72 C73 C74 -25.7(3) . . . . ?
C71 C72 C73 C96 -77.6(3) . . . . ?
N12 C72 C73 C96 95.9(3) . . . . ?
C71 C72 C73 C98 39.2(4) . . . . ?
N12 C72 C73 C98 -147.4(2) . . . . ?
C77 N13 C74 C75 0.6(3) . . . . ?
P4 N13 C74 C75 179.5(2) . . . . ?
C77 N13 C74 C73 179.2(2) . . . . ?
P4 N13 C74 C73 -1.9(4) . . . . ?
C72 C73 C74 C75 -162.5(3) . . . . ?
C96 C73 C74 C75 77.0(3) . . . . ?
C98 C73 C74 C75 -40.8(4) . . . . ?
C72 C73 C74 N13 19.2(4) . . . . ?
C96 C73 C74 N13 -101.3(3) . . . . ?
C98 C73 C74 N13 141.0(3) . . . . ?
N13 C74 C75 C76 -0.6(3) . . . . ?
C73 C74 C75 C76 -179.1(3) . . . . ?
C74 C75 C76 C77 0.4(3) . . . . ?
C75 C76 C77 N13 0.0(3) . . . . ?
C75 C76 C77 C78 176.0(2) . . . . ?
C74 N13 C77 C76 -0.4(3) . . . . ?
P4 N13 C77 C76 -179.37(18) . . . . ?
C74 N13 C77 C78 -176.6(2) . . . . ?
P4 N13 C77 C78 4.4(3) . . . . ?
C79 N14 C78 C77 -177.7(2) . . . . ?
C76 C77 C78 N14 -167.2(3) . . . . ?
N13 C77 C78 N14 8.2(4) . . . . ?
C78 N14 C79 C80 47.7(3) . . . . ?
C78 N14 C79 C84 -134.0(2) . . . . ?
C84 C79 C80 C81 -0.1(3) . . . . ?
N14 C79 C80 C81 178.3(2) . . . . ?
C79 C80 C81 C82 1.3(4) . . . . ?
C79 C80 C81 C100 -178.9(2) . . . . ?
C80 C81 C82 C83 -1.4(4) . . . . ?
C100 C81 C82 C83 178.7(2) . . . . ?
C80 C81 C82 C101 -179.4(2) . . . . ?
C100 C81 C82 C101 0.8(4) . . . . ?
C81 C82 C83 C84 0.5(4) . . . . ?
C101 C82 C83 C84 178.4(2) . . . . ?
C82 C83 C84 C79 0.7(4) . . . . ?
C82 C83 C84 N15 -179.4(2) . . . . ?
C80 C79 C84 C83 -0.9(3) . . . . ?
N14 C79 C84 C83 -179.3(2) . . . . ?
C80 C79 C84 N15 179.2(2) . . . . ?
N14 C79 C84 N15 0.8(3) . . . . ?
C85 N15 C84 C83 -51.2(3) . . . . ?
Ag2 N15 C84 C83 139.46(19) . . . . ?
C85 N15 C84 C79 128.6(2) . . . . ?
Ag2 N15 C84 C79 -40.7(3) . . . . ?
C84 N15 C85 C86 175.9(2) . . . . ?
Ag2 N15 C85 C86 -15.6(4) . . . . ?
C89 N16 C86 C87 -0.3(3) . . . . ?
P3 N16 C86 C87 170.4(2) . . . . ?
C89 N16 C86 C85 176.1(3) . . . . ?
P3 N16 C86 C85 -13.2(4) . . . . ?
N15 C85 C86 C87 161.9(3) . . . . ?
N15 C85 C86 N16 -13.9(5) . . . . ?
N16 C86 C87 C88 1.0(3) . . . . ?
C85 C86 C87 C88 -175.5(3) . . . . ?
C86 C87 C88 C89 -1.4(4) . . . . ?
C86 N16 C89 C88 -0.6(3) . . . . ?
P3 N16 C89 C88 -170.2(2) . . . . ?
C86 N16 C89 C90 -174.6(2) . . . . ?
P3 N16 C89 C90 15.8(4) . . . . ?
C87 C88 C89 N16 1.2(3) . . . . ?
C87 C88 C89 C90 174.8(3) . . . . ?
N16 C89 C90 C91 -25.4(4) . . . . ?
C88 C89 C90 C91 161.8(3) . . . . ?
N16 C89 C90 C104 -146.4(2) . . . . ?
C88 C89 C90 C104 40.8(4) . . . . ?
N16 C89 C90 C102 96.6(3) . . . . ?
C88 C89 C90 C102 -76.2(4) . . . . ?
C60 N9 C91 C92 1.2(3) . . . . ?
P3 N9 C91 C92 175.2(2) . . . . ?
C60 N9 C91 C90 -178.2(3) . . . . ?
P3 N9 C91 C90 -4.2(4) . . . . ?
C89 C90 C91 C92 -159.2(3) . . . . ?
C104 C90 C91 C92 -38.0(4) . . . . ?
C102 C90 C91 C92 80.2(4) . . . . ?
C89 C90 C91 N9 20.1(4) . . . . ?
C104 C90 C91 N9 141.3(3) . . . . ?
C102 C90 C91 N9 -100.5(3) . . . . ?
N9 C91 C92 C93 -1.3(4) . . . . ?
C90 C91 C92 C93 178.1(3) . . . . ?
N9 C60 C93 C92 -0.1(4) . . . . ?
C61 C60 C93 C92 176.9(3) . . . . ?
C91 C92 C93 C60 0.9(4) . . . . ?
C72 C73 C96 C97 -67.2(3) . . . . ?
C74 C73 C96 C97 56.0(3) . . . . ?
C98 C73 C96 C97 174.8(3) . . . . ?
C72 C73 C98 C99 61.9(3) . . . . ?
C74 C73 C98 C99 -61.7(3) . . . . ?
C96 C73 C98 C99 179.0(3) . . . . ?
C91 C90 C102 C103 67.4(4) . . . . ?
C89 C90 C102 C103 -56.2(4) . . . . ?
C104 C90 C102 C103 -173.9(3) . . . . ?
C91 C90 C104 C105 -60.4(3) . . . . ?
C89 C90 C104 C105 63.0(3) . . . . ?
C102 C90 C104 C105 180.0(3) . . . . ?
N9 P3 C106 C107 -143.4(2) . . . . ?
N16 P3 C106 C107 118.7(2) . . . . ?
Ag2B P3 C106 C107 -2.8(4) . . . . ?
Ag2 P3 C106 C107 6.6(2) . . . . ?
N9 P3 C106 C111 37.9(2) . . . . ?
N16 P3 C106 C111 -59.9(2) . . . . ?
Ag2B P3 C106 C111 178.5(4) . . . . ?
Ag2 P3 C106 C111 -172.06(19) . . . . ?
C111 C106 C107 C108 0.9(4) . . . . ?
P3 C106 C107 C108 -177.7(2) . . . . ?
C106 C107 C108 C109 -0.9(4) . . . . ?
C107 C108 C109 C110 0.3(5) . . . . ?
C108 C109 C110 C111 0.2(5) . . . . ?
C109 C110 C111 C106 -0.2(5) . . . . ?
C107 C106 C111 C110 -0.4(4) . . . . ?
P3 C106 C111 C110 178.2(2) . . . . ?
N13 P4 C112 C113 60.0(2) . . . . ?
N12 P4 C112 C113 -39.4(2) . . . . ?
Ag2 P4 C112 C113 -162.5(2) . . . . ?
Ag2B P4 C112 C113 -153.5(3) . . . . ?
N13 P4 C112 C117 -125.6(2) . . . . ?
N12 P4 C112 C117 135.0(2) . . . . ?
Ag2 P4 C112 C117 11.9(2) . . . . ?
Ag2B P4 C112 C117 20.9(4) . . . . ?
C117 C112 C113 C114 0.9(4) . . . . ?
P4 C112 C113 C114 175.3(2) . . . . ?
C112 C113 C114 C115 0.7(5) . . . . ?
C113 C114 C115 C116 -1.8(5) . . . . ?
C114 C115 C116 C117 1.2(4) . . . . ?
C115 C116 C117 C112 0.4(4) . . . . ?
C113 C112 C117 C116 -1.4(4) . . . . ?
P4 C112 C117 C116 -175.9(2) . . . . ?
C122 O7 C119 C120 -28.6(4) . . . . ?
O7 C119 C120 C121 37.1(5) . . . . ?
C119 C120 C121 C122 -30.7(4) . . . . ?
C119 O7 C122 C121 8.3(4) . . . . ?
C120 C121 C122 O7 14.7(4) . . . . ?
C126 O8 C123 C124 -14.3(5) . . . . ?
O8 C123 C124 C125 32.6(5) . . . . ?
C123 C124 C125 C126 -37.4(5) . . . . ?
C123 O8 C126 C125 -10.4(5) . . . . ?
C124 C125 C126 O8 30.1(5) . . . . ?
C130 O9 C127 C128 -32.9(6) . . . . ?
O9 C127 C128 C129 32.2(6) . . . . ?
C127 C128 C129 C130 -19.7(6) . . . . ?
C127 O9 C130 C129 19.6(6) . . . . ?
C128 C129 C130 O9 1.2(6) . . . . ?
C134 O10A C131 C132 15.9(5) . . . . ?
O10A C131 C132 C133 -34.7(5) . . . . ?
C131 C132 C133 C134 39.5(4) . . . . ?
C131 O10A C134 C133 10.3(6) . . . . ?
C132 C133 C134 O10A -31.3(5) . . . . ?
C138 O10B C135 C136 13(4) . . . . ?
O10B C135 C136 C137 -17(4) . . . . ?
C135 C136 C137 C138 15(4) . . . . ?
C135 O10B C138 C137 -3(4) . . . . ?
C136 C137 C138 O10B -7(4) . . . . ?
