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#$Date: 2025-03-04 20:09:12 +0200 (Tue, 04 Mar 2025) $
#$Revision: 297990 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/13/40/7134096.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7134096
loop_
_publ_author_name
'Wetzel, Philipp'
'Maichle-Mössmer, Cäcilia'
'Anwander, Reiner'
_publ_section_title
;
 A homoleptic rare-earth-metal tetramethylindate.
;
_journal_issue                   10
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              2123
_journal_page_last               2126
_journal_paper_doi               10.1039/d4cc06213b
_journal_volume                  61
_journal_year                    2025
_chemical_formula_sum            'C13.5 H40.5 Al1.5 Ce In2.01'
_chemical_formula_weight         613.63
_chemical_properties_physical    Air-sensitive,Moisture-sensitive
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   mixed
_audit_creation_method           SHELXL-2019/3
_audit_update_record
;
2024-11-18 deposited with the CCDC.	2024-12-26 downloaded from the CCDC.
;
_cell_angle_alpha                102.3840(10)
_cell_angle_beta                 90.3130(10)
_cell_angle_gamma                107.7340(10)
_cell_formula_units_Z            2
_cell_length_a                   7.3339(3)
_cell_length_b                   10.2240(4)
_cell_length_c                   17.7791(7)
_cell_measurement_reflns_used    277
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      29.96
_cell_measurement_theta_min      2.168
_cell_volume                     1236.62(9)
_computing_cell_refinement       'SAINT V8.40B (Bruker Nano, Inc., 2019)'
_computing_data_collection       'APEX3 v2019.11-0'
_computing_data_reduction        'SAINT V8.40B (Bruker Nano, Inc., 2019)'
_computing_structure_refinement  'SHELXL-2019/2 (Sheldrick, 2019)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker APEX II DUO'
_diffrn_measurement_method       'omega scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0211
_diffrn_reflns_av_unetI/netI     0.0125
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.998
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       25
_diffrn_reflns_limit_l_min       -25
_diffrn_reflns_number            47233
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.998
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         30.519
_diffrn_reflns_theta_min         2.147
_diffrn_source                   'ImuS-focus sealed tube'
_exptl_absorpt_coefficient_mu    3.705
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'sadabs V2012/1 (Bruker AXS Inc.)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.648
_exptl_crystal_description       block
_exptl_crystal_F_000             594
_exptl_crystal_size_max          0.355
_exptl_crystal_size_mid          0.232
_exptl_crystal_size_min          0.140
_exptl_transmission_factor_max   0.7461
_exptl_transmission_factor_min   0.6509
_refine_diff_density_max         2.132
_refine_diff_density_min         -2.763
_refine_diff_density_rms         0.103
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.073
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     285
_refine_ls_number_reflns         7560
_refine_ls_number_restraints     27
_refine_ls_restrained_S_all      1.077
_refine_ls_R_factor_all          0.0256
_refine_ls_R_factor_gt           0.0242
_refine_ls_shift/su_max          0.039
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0197P)²+2.7009P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0561
_refine_ls_wR_factor_ref         0.0572
_reflns_Friedel_coverage         0.000
_reflns_number_gt                7278
_reflns_number_total             7560
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d4cc06213b2.cif
_cod_data_source_block           6_mo_PW145_0m_a
_cod_depositor_comments
'Adding full bibliography for 7134096--7134101.cif.'
_cod_original_formula_sum        'C13.50 H40.50 Al1.50 Ce In2.01'
_cod_database_code               7134096
_shelx_shelxl_version_number     2019/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.353
_shelx_estimated_absorpt_t_max   0.625
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.4156(3) 0.4715(2) 0.80894(12) 0.0331(5) Uani 1 1 d D . . . .
H1A H 0.4406(19) 0.468(2) 0.75570(18) 0.044(10) Uiso 1 1 d D . . . .
H1B H 0.4691(7) 0.4052(4) 0.8238(4) 0.055(11) Uiso 1 1 d D . . . .
H1C H 0.4939(14) 0.5609(5) 0.8393(5) 0.056(12) Uiso 1 1 d D . . . .
C2 C -0.0754(4) 0.4620(3) 0.82296(19) 0.0334(6) Uani 1 1 d . . . . .
H2A H -0.126(6) 0.458(4) 0.770(2) 0.046(10) Uiso 1 1 d . . . . .
H2B H -0.178(7) 0.395(5) 0.837(3) 0.073(14) Uiso 1 1 d . . . . .
H2C H -0.073(5) 0.553(4) 0.856(2) 0.044(10) Uiso 1 1 d . . . . .
C3 C 0.0392(6) 0.1579(4) 0.7630(3) 0.0620(11) Uani 1 1 d . . . . .
H3A H -0.085332 0.144777 0.736928 0.093 Uiso 1 1 calc R U . . .
H3B H 0.026396 0.083766 0.791421 0.093 Uiso 1 1 calc R U . . .
H3C H 0.133409 0.152722 0.724509 0.093 Uiso 1 1 calc R U . . .
C4 C 0.1673(7) 0.3729(5) 0.9634(2) 0.0616(11) Uani 1 1 d . . . . .
H4A H 0.048888 0.316623 0.981070 0.092 Uiso 1 1 calc R U . . .
H4B H 0.194005 0.472482 0.988945 0.092 Uiso 1 1 calc R U . . .
H4C H 0.274188 0.340845 0.976091 0.092 Uiso 1 1 calc R U . . .
C5 C 0.1428(4) 0.4895(3) 0.63068(15) 0.0311(5) Uani 1 1 d . . . . .
H53 H 0.112(6) 0.444(4) 0.578(2) 0.054(11) Uiso 1 1 d . . . . .
H52 H 0.094(5) 0.414(4) 0.660(2) 0.040(9) Uiso 1 1 d . . . . .
H51 H 0.282(5) 0.514(4) 0.635(2) 0.036(9) Uiso 1 1 d . . . . .
C6 C 0.0143(4) 0.7767(3) 0.73293(15) 0.0257(4) Uani 1 1 d . . . . .
H63 H -0.053(5) 0.832(4) 0.713(2) 0.044(10) Uiso 1 1 d . . . . .
H62 H 0.127(5) 0.850(4) 0.759(2) 0.037(9) Uiso 1 1 d . . . . .
H61 H -0.062(5) 0.742(4) 0.773(2) 0.038(9) Uiso 1 1 d . . . . .
C7 C 0.1657(5) 0.7725(3) 0.55697(19) 0.0368(6) Uani 1 1 d . . . . .
H7A H 0.180(6) 0.860(5) 0.579(2) 0.055 Uiso 1 1 d . U . . .
H7B H 0.127(6) 0.753(5) 0.509(3) 0.055 Uiso 1 1 d . U . . .
H7C H 0.290(6) 0.773(4) 0.562(2) 0.055 Uiso 1 1 d . U . . .
C8 C -0.2841(5) 0.5398(4) 0.59074(18) 0.0420(7) Uani 1 1 d . . . . .
H8A H -0.348051 0.610282 0.588389 0.063 Uiso 1 1 calc R U . . .
H8B H -0.335977 0.490137 0.631157 0.063 Uiso 1 1 calc R U . . .
H8C H -0.306482 0.471943 0.540822 0.063 Uiso 1 1 calc R U . . .
C9 C 0.5315(3) 0.8174(3) 0.74170(14) 0.0243(4) Uani 1 1 d . . . . .
H9A H 0.431(5) 0.812(4) 0.703(2) 0.044(10) Uiso 1 1 d . . . . .
H9B H 0.646(5) 0.892(4) 0.733(2) 0.039(9) Uiso 1 1 d . . . . .
H9C H 0.558(5) 0.729(4) 0.726(2) 0.039(9) Uiso 1 1 d . . . . .
C10 C 0.3026(4) 0.7992(3) 0.91534(14) 0.0277(5) Uani 1 1 d . . . . .
H10A H 0.176(5) 0.801(4) 0.905(2) 0.038(9) Uiso 1 1 d . . . . .
H10B H 0.293(5) 0.708(4) 0.927(2) 0.044(10) Uiso 1 1 d . . . . .
H10C H 0.339(6) 0.858(4) 0.965(2) 0.051(11) Uiso 1 1 d . . . . .
C11 C 0.7908(5) 0.9077(3) 0.91611(17) 0.0386(6) Uani 1 1 d . . . . .
H11A H 0.783772 0.808068 0.904232 0.058 Uiso 1 1 calc R U . . .
H11B H 0.795134 0.942011 0.972168 0.058 Uiso 1 1 calc R U . . .
H11C H 0.906913 0.962712 0.896381 0.058 Uiso 1 1 calc R U . . .
C12 C 0.5072(5) 1.1158(3) 0.86600(19) 0.0431(7) Uani 1 1 d . . . . .
H12A H 0.518511 1.134391 0.814122 0.065 Uiso 1 1 calc R U . . .
H12B H 0.602631 1.191794 0.902379 0.065 Uiso 1 1 calc R U . . .
H12C H 0.378132 1.110985 0.882003 0.065 Uiso 1 1 calc R U . . .
C13 C -0.678(3) -0.011(2) 0.4202(10) 0.169(8) Uani 0.5 1 d D U P . .
H13A H -0.807627 -0.036542 0.437714 0.254 Uiso 0.5 1 calc R U P . .
H13B H -0.670225 -0.082802 0.374937 0.254 Uiso 0.5 1 calc R U P . .
H13C H -0.647607 0.080627 0.406330 0.254 Uiso 0.5 1 calc R U P . .
C14 C -0.4720(19) 0.1504(13) 0.6208(7) 0.095(4) Uani 0.5 1 d D U P . .
H14A H -0.521703 0.094867 0.659013 0.143 Uiso 0.5 1 calc R U P . .
H14B H -0.545791 0.215161 0.618859 0.143 Uiso 0.5 1 calc R U P . .
H14C H -0.336571 0.204598 0.635298 0.143 Uiso 0.5 1 calc R U P . .
C15 C -0.2992(19) -0.1154(14) 0.5165(8) 0.100(4) Uani 0.5 1 d D U P . .
H15A H -0.188894 -0.052138 0.551318 0.150 Uiso 0.5 1 calc R U P . .
H15B H -0.254722 -0.150149 0.466485 0.150 Uiso 0.5 1 calc R U P . .
H15C H -0.364532 -0.195342 0.538933 0.150 Uiso 0.5 1 calc R U P . .
Ce1 Ce 0.22225(2) 0.63306(2) 0.77614(2) 0.01700(4) Uani 1 1 d . . . . .
In1 In 0.13518(14) 0.34947(8) 0.84600(4) 0.03048(13) Uani 0.6428(15) 1 d . . P .
.
In2 In -0.0053(5) 0.6344(3) 0.61462(13) 0.0216(2) Uani 0.3744(13) 1 d . . P . .
In3 In 0.5536(2) 0.92926(17) 0.86493(8) 0.0186(2) Uani 0.4886(19) 1 d . . P . .
Al1 Al 0.1212(13) 0.3340(8) 0.8318(4) 0.03048(13) Uani 0.3572(15) 1 d . . P . .
Al2 Al 0.0010(13) 0.6449(10) 0.6237(4) 0.0216(2) Uani 0.6256(13) 1 d . . P . .
Al3 Al 0.5458(12) 0.9224(9) 0.8638(5) 0.038(3) Uani 0.5114(19) 1 d . . P . .
In4 In -0.500000 0.000000 0.500000 0.06636(13) Uani 1 2 d S . P . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ce Ce -0.2486 2.6331 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
In In -0.7276 1.3100 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
In1 C1 Al1 6.73(19) . . ?
In1 C1 Ce1 84.39(8) . . ?
Al1 C1 Ce1 83.7(2) . . ?
Al1 C2 In1 6.79(19) . . ?
Al1 C2 Ce1 84.7(2) . . ?
In1 C2 Ce1 84.16(8) . . ?
Al1 C3 In1 3.8(3) . . ?
In1 C4 Al1 3.2(2) . . ?
In2 C5 Al2 4.5(2) . . ?
In2 C5 Ce1 86.86(10) . . ?
Al2 C5 Ce1 82.39(19) . . ?
Al2 C6 In2 1.0(3) . . ?
Al2 C6 Ce1 84.3(3) . . ?
In2 C6 Ce1 85.09(12) . . ?
In2 C7 Al2 4.7(2) . . ?
In2 C8 Al2 4.3(3) . . ?
Al3 C9 In3 1.8(3) . . ?
Al3 C9 Ce1 83.7(2) . . ?
In3 C9 Ce1 85.48(9) . . ?
Al3 C10 In3 1.3(2) . . ?
Al3 C10 Ce1 84.2(2) . . ?
In3 C10 Ce1 85.45(9) . . ?
In3 C11 Al3 1.9(3) . . ?
In3 C12 Al3 1.7(3) . . ?
C2 Ce1 C1 86.25(8) . . ?
C2 Ce1 C6 92.22(9) . . ?
C1 Ce1 C6 175.00(7) . . ?
C2 Ce1 C10 90.85(10) . . ?
C1 Ce1 C10 92.67(7) . . ?
C6 Ce1 C10 92.12(8) . . ?
C2 Ce1 C9 174.97(9) . . ?
C1 Ce1 C9 93.17(8) . . ?
C6 Ce1 C9 88.77(8) . . ?
C10 Ce1 C9 84.18(8) . . ?
C2 Ce1 C5 92.78(10) . . ?
C1 Ce1 C5 92.29(8) . . ?
C6 Ce1 C5 83.02(9) . . ?
C10 Ce1 C5 174.03(9) . . ?
C9 Ce1 C5 92.24(8) . . ?
C2 Ce1 Al2 95.30(19) . . ?
C1 Ce1 Al2 134.63(17) . . ?
C6 Ce1 Al2 40.75(17) . . ?
C10 Ce1 Al2 132.54(17) . . ?
C9 Ce1 Al2 88.67(18) . . ?
C5 Ce1 Al2 42.34(17) . . ?
C2 Ce1 Al3 132.80(16) . . ?
C1 Ce1 Al3 93.59(14) . . ?
C6 Ce1 Al3 90.94(15) . . ?
C10 Ce1 Al3 41.96(16) . . ?
C9 Ce1 Al3 42.22(16) . . ?
C5 Ce1 Al3 134.31(16) . . ?
Al2 Ce1 Al3 116.4(2) . . ?
C2 Ce1 In1 43.46(7) . . ?
C1 Ce1 In1 42.79(5) . . ?
C6 Ce1 In1 135.55(6) . . ?
C10 Ce1 In1 91.90(6) . . ?
C9 Ce1 In1 135.68(6) . . ?
C5 Ce1 In1 93.99(7) . . ?
Al2 Ce1 In1 123.61(17) . . ?
Al3 Ce1 In1 119.94(14) . . ?
C2 Ce1 Al1 42.91(18) . . ?
C1 Ce1 Al1 43.65(17) . . ?
C6 Ce1 Al1 134.16(18) . . ?
C10 Ce1 Al1 96.52(13) . . ?
C9 Ce1 Al1 136.81(17) . . ?
C5 Ce1 Al1 89.36(14) . . ?
Al2 Ce1 Al1 119.3(2) . . ?
Al3 Ce1 Al1 124.24(19) . . ?
In1 Ce1 Al1 4.68(13) . . ?
C2 Ce1 In3 133.07(8) . . ?
C1 Ce1 In3 93.68(5) . . ?
C6 Ce1 In3 90.84(6) . . ?
C10 Ce1 In3 42.23(7) . . ?
C9 Ce1 In3 41.95(6) . . ?
C5 Ce1 In3 134.03(7) . . ?
Al2 Ce1 In3 116.22(17) . . ?
Al3 Ce1 In3 0.29(18) . . ?
In1 Ce1 In3 120.17(3) . . ?
Al1 Ce1 In3 124.46(14) . . ?
C2 Ce1 In2 95.00(9) . . ?
C1 Ce1 In2 132.57(7) . . ?
C6 Ce1 In2 42.79(8) . . ?
C10 Ce1 In2 134.62(8) . . ?
C9 Ce1 In2 89.08(8) . . ?
C5 Ce1 In2 40.28(9) . . ?
Al2 Ce1 In2 2.1(2) . . ?
Al3 Ce1 In2 117.89(15) . . ?
In1 Ce1 In2 122.16(6) . . ?
Al1 Ce1 In2 117.79(14) . . ?
In3 Ce1 In2 117.65(6) . . ?
C4 In1 C3 126.40(19) . . ?
C4 In1 C1 107.43(15) . . ?
C3 In1 C1 105.93(14) . . ?
C4 In1 C2 107.32(14) . . ?
C3 In1 C2 102.81(15) . . ?
C1 In1 C2 105.19(9) . . ?
C4 In1 Ce1 118.73(13) . . ?
C3 In1 Ce1 114.81(13) . . ?
C1 In1 Ce1 52.81(6) . . ?
C2 In1 Ce1 52.38(7) . . ?
C8 In2 C7 125.4(2) . . ?
C8 In2 C5 111.9(2) . . ?
C7 In2 C5 107.68(19) . . ?
C8 In2 C6 103.62(17) . . ?
C7 In2 C6 100.84(17) . . ?
C5 In2 C6 104.90(14) . . ?
C8 In2 Ce1 122.30(16) . . ?
C7 In2 Ce1 111.34(14) . . ?
C5 In2 Ce1 52.86(9) . . ?
C6 In2 Ce1 52.12(8) . . ?
C12 In3 C11 125.13(16) . . ?
C12 In3 C9 106.64(13) . . ?
C11 In3 C9 106.42(12) . . ?
C12 In3 C10 106.87(13) . . ?
C11 In3 C10 105.32(13) . . ?
C9 In3 C10 104.89(11) . . ?
C12 In3 Ce1 118.58(11) . . ?
C11 In3 Ce1 116.29(11) . . ?
C9 In3 Ce1 52.57(7) . . ?
C10 In3 Ce1 52.32(7) . . ?
C3 Al1 C2 112.1(4) . . ?
C3 Al1 C1 113.0(4) . . ?
C2 Al1 C1 104.6(4) . . ?
C3 Al1 C4 125.8(5) . . ?
C2 Al1 C4 100.3(3) . . ?
C1 Al1 C4 98.4(3) . . ?
C3 Al1 Ce1 123.1(4) . . ?
C2 Al1 Ce1 52.39(19) . . ?
C1 Al1 Ce1 52.66(18) . . ?
C4 Al1 Ce1 111.1(3) . . ?
C8 Al2 C7 120.0(4) . . ?
C8 Al2 C6 107.0(4) . . ?
C7 Al2 C6 105.7(4) . . ?
C8 Al2 C5 108.0(4) . . ?
C7 Al2 C5 105.8(4) . . ?
C6 Al2 C5 110.1(4) . . ?
C8 Al2 Ce1 124.9(4) . . ?
C7 Al2 Ce1 115.1(3) . . ?
C6 Al2 Ce1 54.95(19) . . ?
C5 Al2 Ce1 55.3(2) . . ?
C12 Al3 C11 121.6(4) . . ?
C12 Al3 C10 107.5(4) . . ?
C11 Al3 C10 106.4(4) . . ?
C12 Al3 C9 106.3(4) . . ?
C11 Al3 C9 106.5(3) . . ?
C10 Al3 C9 107.9(4) . . ?
C12 Al3 Ce1 120.2(3) . . ?
C11 Al3 Ce1 118.2(3) . . ?
C10 Al3 Ce1 53.85(19) . . ?
C9 Al3 Ce1 54.05(19) . . ?
C13 In4 C13 180.0 2_456 . ?
C13 In4 C15 135.5(6) 2_456 2_456 ?
C13 In4 C15 44.5(6) . 2_456 ?
C13 In4 C15 44.5(6) 2_456 . ?
C13 In4 C15 135.5(6) . . ?
C15 In4 C15 180.0(7) 2_456 . ?
C13 In4 C14 122.2(7) 2_456 2_456 ?
C13 In4 C14 57.8(7) . 2_456 ?
C15 In4 C14 102.1(5) 2_456 2_456 ?
C15 In4 C14 77.9(5) . 2_456 ?
C13 In4 C14 57.8(7) 2_456 . ?
C13 In4 C14 122.2(7) . . ?
C15 In4 C14 77.9(5) 2_456 . ?
C15 In4 C14 102.1(5) . . ?
C14 In4 C14 180.0 2_456 . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 In1 2.241(2) . ?
C1 Al1 2.282(9) . ?
C1 Ce1 2.629(2) . ?
C2 Al1 2.247(10) . ?
C2 In1 2.270(3) . ?
C2 Ce1 2.614(3) . ?
C3 Al1 1.868(8) . ?
C3 In1 2.102(4) . ?
C4 In1 2.052(4) . ?
C4 Al1 2.292(9) . ?
C5 In2 2.148(5) . ?
C5 Al2 2.171(11) . ?
C5 Ce1 2.649(3) . ?
C6 Al2 2.096(7) . ?
C6 In2 2.262(3) . ?
C6 Ce1 2.629(2) . ?
C7 In2 2.043(5) . ?
C7 Al2 2.071(10) . ?
C8 In2 1.976(5) . ?
C8 Al2 2.054(9) . ?
C9 Al3 2.193(8) . ?
C9 In3 2.223(3) . ?
C9 Ce1 2.641(2) . ?
C10 Al3 2.180(9) . ?
C10 In3 2.236(3) . ?
C10 Ce1 2.632(2) . ?
C11 In3 2.050(3) . ?
C11 Al3 2.079(8) . ?
C12 In3 2.033(4) . ?
C12 Al3 2.073(9) . ?
C13 In4 1.883(16) . ?
C14 In4 2.324(11) . ?
C15 In4 2.202(12) . ?
Ce1 Al2 3.195(8) . ?
Ce1 Al3 3.243(9) . ?
Ce1 In1 3.2836(9) . ?
Ce1 Al1 3.286(9) . ?
Ce1 In3 3.3157(18) . ?
Ce1 In2 3.318(3) . ?
