#------------------------------------------------------------------------------
#$Date: 2016-03-26 16:27:48 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180340 $
#$URL: svn://www.crystallography.net/cod/cif/7/20/09/7200938.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7200938
loop_
_publ_author_name
'Baudron, Stéphane A.'
'Salazar-Mendoza, Domingo'
'Hosseini, Mir Wais'
_publ_section_title
;
 Combination of primary amide and dipyrrin for the elaboration of
 extended architectures built upon both coordination and hydrogen
 bonding
;
_journal_issue                   7
_journal_name_full               CrystEngComm
_journal_page_first              1245
_journal_paper_doi               10.1039/b901167f
_journal_volume                  11
_journal_year                    2009
_chemical_formula_moiety         ' C32 H26 Co N5 O3, C H Cl3'
_chemical_formula_sum            'C33 H27 Cl3 Co N5 O3'
_chemical_formula_weight         706.88
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 114.3580(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   13.4382(5)
_cell_length_b                   21.1339(8)
_cell_length_c                   12.3217(4)
_cell_measurement_reflns_used    6566
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      25.25
_cell_measurement_theta_min      2.55
_cell_volume                     3187.9(2)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'Bruker SHELXTL'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0541
_diffrn_reflns_av_sigmaI/netI    0.0597
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       27
_diffrn_reflns_limit_k_min       -27
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            30856
_diffrn_reflns_theta_full        27.53
_diffrn_reflns_theta_max         27.53
_diffrn_reflns_theta_min         1.66
_exptl_absorpt_coefficient_mu    0.833
_exptl_absorpt_correction_T_max  0.8923
_exptl_absorpt_correction_T_min  0.7650
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            dark-red
_exptl_crystal_density_diffrn    1.473
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    .
_exptl_crystal_description       prism
_exptl_crystal_F_000             1448
_exptl_crystal_size_max          0.34
_exptl_crystal_size_mid          0.25
_exptl_crystal_size_min          0.14
_refine_diff_density_max         1.393
_refine_diff_density_min         -1.086
_refine_diff_density_rms         0.248
_refine_ls_extinction_coef       0.027(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.060
_refine_ls_hydrogen_treatment    riding
_refine_ls_matrix_type           full
_refine_ls_number_parameters     407
_refine_ls_number_reflns         7325
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.060
_refine_ls_R_factor_all          0.1305
_refine_ls_R_factor_gt           0.0881
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1751P)²+6.2311P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2598
_refine_ls_wR_factor_ref         0.2930
_reflns_number_gt                4826
_reflns_number_total             7325
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b901167f.txt
_cod_data_source_block           compound7CHCl3
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P2(1)/c '
_cod_database_code               7200938
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.6808(5) 0.2897(2) 0.2424(5) 0.0350(11) Uani 1 1 d . . .
H1 H 0.6284 0.3119 0.1797 0.042 Uiso 1 1 calc R . .
C2 C 0.7884(5) 0.3109(3) 0.3088(5) 0.0393(12) Uani 1 1 d . . .
H2 H 0.8189 0.3488 0.2991 0.047 Uiso 1 1 calc R . .
C3 C 0.8389(4) 0.2644(3) 0.3902(5) 0.0373(12) Uani 1 1 d . . .
H3 H 0.9115 0.2647 0.4450 0.045 Uiso 1 1 calc R . .
C4 C 0.7631(4) 0.2162(2) 0.3776(4) 0.0310(11) Uani 1 1 d . . .
C5 C 0.7698(4) 0.1648(2) 0.4518(5) 0.0314(11) Uani 1 1 d . . .
C6 C 0.6789(4) 0.1289(2) 0.4428(4) 0.0309(11) Uani 1 1 d . . .
C7 C 0.6676(5) 0.0901(3) 0.5327(5) 0.0383(12) Uani 1 1 d . . .
H7 H 0.7235 0.0756 0.6025 0.046 Uiso 1 1 calc R . .
C8 C 0.5592(5) 0.0787(3) 0.4958(5) 0.0389(12) Uani 1 1 d . . .
H8 H 0.5264 0.0561 0.5369 0.047 Uiso 1 1 calc R . .
C9 C 0.5050(5) 0.1079(2) 0.3825(5) 0.0352(11) Uani 1 1 d . . .
H9 H 0.4300 0.1066 0.3369 0.042 Uiso 1 1 calc R . .
C10 C 0.8760(4) 0.1504(3) 0.5532(5) 0.0349(11) Uani 1 1 d . . .
C11 C 0.9298(4) 0.1941(3) 0.6406(5) 0.0341(11) Uani 1 1 d . . .
H11 H 0.9018 0.2348 0.6342 0.041 Uiso 1 1 calc R . .
C12 C 1.0256(4) 0.1784(3) 0.7387(5) 0.0362(12) Uani 1 1 d . . .
H12 H 1.0613 0.2086 0.7968 0.043 Uiso 1 1 calc R . .
C13 C 1.0674(4) 0.1177(3) 0.7490(5) 0.0371(12) Uani 1 1 d . . .
C14 C 1.0150(5) 0.0735(3) 0.6612(5) 0.0457(14) Uani 1 1 d . . .
H14 H 1.0442 0.0331 0.6671 0.055 Uiso 1 1 calc R . .
C15 C 0.9191(5) 0.0891(3) 0.5642(5) 0.0447(14) Uani 1 1 d . . .
H15 H 0.8834 0.0589 0.5064 0.054 Uiso 1 1 calc R . .
C16 C 1.1700(4) 0.0963(3) 0.8544(5) 0.0419(13) Uani 1 1 d . . .
C17 C 0.3683(5) 0.2584(3) 0.1280(5) 0.0394(12) Uani 1 1 d . . .
C18 C 0.2792(5) 0.2848(4) 0.1466(6) 0.0556(17) Uani 1 1 d . . .
H18 H 0.2756 0.2790 0.2197 0.067 Uiso 1 1 calc R . .
C19 C 0.1980(7) 0.3187(5) 0.0589(8) 0.081(3) Uani 1 1 d . . .
H19 H 0.1392 0.3336 0.0728 0.097 Uiso 1 1 calc R . .
C20 C 0.2021(7) 0.3312(5) -0.0499(8) 0.084(3) Uani 1 1 d . . .
H20 H 0.1480 0.3553 -0.1074 0.100 Uiso 1 1 calc R . .
C21 C 0.2884(6) 0.3069(4) -0.0708(6) 0.0583(18) Uani 1 1 d . . .
H21 H 0.2915 0.3147 -0.1436 0.070 Uiso 1 1 calc R . .
C22 C 0.3725(5) 0.2703(3) 0.0168(5) 0.0403(13) Uani 1 1 d . . .
C23 C 0.4565(5) 0.2472(3) -0.0139(5) 0.0374(12) Uani 1 1 d . . .
H23 H 0.4567 0.2607 -0.0857 0.045 Uiso 1 1 calc R . .
C24 C 0.6145(5) 0.1898(3) 0.0064(6) 0.0455(14) Uani 1 1 d . . .
H24A H 0.6430 0.2266 -0.0182 0.055 Uiso 1 1 calc R . .
H24B H 0.5818 0.1618 -0.0616 0.055 Uiso 1 1 calc R . .
C25 C 0.7062(5) 0.1557(3) 0.1075(6) 0.0438(14) Uani 1 1 d . . .
H25A H 0.7449 0.1271 0.0767 0.053 Uiso 1 1 calc R . .
H25B H 0.7578 0.1857 0.1610 0.053 Uiso 1 1 calc R . .
C26 C 0.6475(5) 0.0597(3) 0.1669(5) 0.0423(13) Uani 1 1 d . . .
H26 H 0.7013 0.0380 0.1530 0.051 Uiso 1 1 calc R . .
C27 C 0.5653(5) 0.0238(3) 0.1861(5) 0.0408(13) Uani 1 1 d . . .
C28 C 0.5853(6) -0.0394(3) 0.2242(6) 0.0515(15) Uani 1 1 d . . .
H28 H 0.6548 -0.0564 0.2462 0.062 Uiso 1 1 calc R . .
C29 C 0.5031(7) -0.0764(3) 0.2294(6) 0.0591(19) Uani 1 1 d . . .
H29 H 0.5174 -0.1175 0.2588 0.071 Uiso 1 1 calc R . .
C30 C 0.3988(6) -0.0514(3) 0.1900(6) 0.0507(16) Uani 1 1 d . . .
H30 H 0.3422 -0.0769 0.1896 0.061 Uiso 1 1 calc R . .
C31 C 0.3768(5) 0.0105(3) 0.1512(5) 0.0459(14) Uani 1 1 d . . .
H31 H 0.3057 0.0258 0.1243 0.055 Uiso 1 1 calc R . .
C32 C 0.4606(4) 0.0508(3) 0.1519(5) 0.0355(12) Uani 1 1 d . . .
N1 N 0.6637(3) 0.23306(19) 0.2814(4) 0.0291(9) Uani 1 1 d . . .
N2 N 0.5757(3) 0.13718(19) 0.3507(4) 0.0293(9) Uani 1 1 d . . .
N3 N 1.2335(4) 0.1394(3) 0.9252(5) 0.0623(17) Uani 1 1 d . . .
H3A H 1.2911 0.1283 0.9863 0.075 Uiso 1 1 calc R . .
H3B H 1.2177 0.1788 0.9109 0.075 Uiso 1 1 calc R . .
N4 N 0.5322(4) 0.2091(2) 0.0498(4) 0.0347(10) Uani 1 1 d . . .
N5 N 0.6496(3) 0.1207(2) 0.1681(4) 0.0349(10) Uani 1 1 d . . .
O1 O 1.1889(4) 0.0391(2) 0.8708(5) 0.0656(14) Uani 1 1 d . . .
O2 O 0.4399(3) 0.22553(17) 0.2143(3) 0.0329(8) Uani 1 1 d . . .
O3 O 0.4389(3) 0.11081(17) 0.1217(3) 0.0342(8) Uani 1 1 d . . .
Co1 Co 0.54894(5) 0.17357(3) 0.19834(6) 0.0276(3) Uani 1 1 d . . .
C33 C 1.0044(18) 0.4478(9) 0.642(2) 0.226(12) Uani 1 1 d . . .
H33 H 0.9599 0.4862 0.6175 0.272 Uiso 1 1 calc R . .
Cl1 Cl 1.1385(4) 0.4701(3) 0.7333(6) 0.201(2) Uani 1 1 d . . .
Cl2 Cl 0.9609(5) 0.4016(4) 0.7501(10) 0.316(6) Uani 1 1 d . . .
Cl3 Cl 0.9857(10) 0.4104(7) 0.5311(12) 0.406(8) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1 C1 C2 111.2(5) . . ?
N1 C1 H1 124.4 . . ?
C2 C1 H1 124.4 . . ?
C3 C2 C1 106.1(5) . . ?
C3 C2 H2 127.0 . . ?
C1 C2 H2 127.0 . . ?
C2 C3 C4 108.8(5) . . ?
C2 C3 H3 125.6 . . ?
C4 C3 H3 125.6 . . ?
C5 C4 C3 130.0(5) . . ?
C5 C4 N1 121.8(4) . . ?
C3 C4 N1 107.5(4) . . ?
C4 C5 C6 123.3(5) . . ?
C4 C5 C10 119.2(5) . . ?
C6 C5 C10 117.2(5) . . ?
N2 C6 C5 122.5(4) . . ?
N2 C6 C7 108.2(4) . . ?
C5 C6 C7 127.9(5) . . ?
C8 C7 C6 106.4(5) . . ?
C8 C7 H7 126.8 . . ?
C6 C7 H7 126.8 . . ?
C7 C8 C9 107.3(5) . . ?
C7 C8 H8 126.3 . . ?
C9 C8 H8 126.3 . . ?
N2 C9 C8 110.7(5) . . ?
N2 C9 H9 124.6 . . ?
C8 C9 H9 124.6 . . ?
C11 C10 C15 118.8(5) . . ?
C11 C10 C5 122.1(5) . . ?
C15 C10 C5 119.0(5) . . ?
C10 C11 C12 121.3(5) . . ?
C10 C11 H11 119.4 . . ?
C12 C11 H11 119.4 . . ?
C13 C12 C11 119.5(5) . . ?
C13 C12 H12 120.2 . . ?
C11 C12 H12 120.2 . . ?
C14 C13 C12 119.9(5) . . ?
C14 C13 C16 117.2(5) . . ?
C12 C13 C16 122.9(5) . . ?
C13 C14 C15 120.3(5) . . ?
C13 C14 H14 119.9 . . ?
C15 C14 H14 119.9 . . ?
C14 C15 C10 120.2(5) . . ?
C14 C15 H15 119.9 . . ?
C10 C15 H15 119.9 . . ?
O1 C16 N3 122.7(5) . . ?
O1 C16 C13 118.9(5) . . ?
N3 C16 C13 118.4(5) . . ?
O2 C17 C22 125.0(5) . . ?
O2 C17 C18 117.8(5) . . ?
C22 C17 C18 117.3(5) . . ?
C19 C18 C17 121.6(6) . . ?
C19 C18 H18 119.2 . . ?
C17 C18 H18 119.2 . . ?
C18 C19 C20 121.5(7) . . ?
C18 C19 H19 119.3 . . ?
C20 C19 H19 119.3 . . ?
C21 C20 C19 118.6(7) . . ?
C21 C20 H20 120.7 . . ?
C19 C20 H20 120.7 . . ?
C20 C21 C22 121.5(6) . . ?
C20 C21 H21 119.2 . . ?
C22 C21 H21 119.2 . . ?
C23 C22 C17 123.5(5) . . ?
C23 C22 C21 117.1(5) . . ?
C17 C22 C21 119.5(6) . . ?
N4 C23 C22 124.8(5) . . ?
N4 C23 H23 117.6 . . ?
C22 C23 H23 117.6 . . ?
N4 C24 C25 108.1(5) . . ?
N4 C24 H24A 110.1 . . ?
C25 C24 H24A 110.1 . . ?
N4 C24 H24B 110.1 . . ?
C25 C24 H24B 110.1 . . ?
H24A C24 H24B 108.4 . . ?
N5 C25 C24 103.8(5) . . ?
N5 C25 H25A 111.0 . . ?
C24 C25 H25A 111.0 . . ?
N5 C25 H25B 111.0 . . ?
C24 C25 H25B 111.0 . . ?
H25A C25 H25B 109.0 . . ?
N5 C26 C27 122.7(5) . . ?
N5 C26 H26 118.6 . . ?
C27 C26 H26 118.6 . . ?
C28 C27 C32 120.9(6) . . ?
C28 C27 C26 120.1(6) . . ?
C32 C27 C26 118.5(5) . . ?
C29 C28 C27 120.6(7) . . ?
C29 C28 H28 119.7 . . ?
C27 C28 H28 119.7 . . ?
C28 C29 C30 118.9(6) . . ?
C28 C29 H29 120.5 . . ?
C30 C29 H29 120.5 . . ?
C29 C30 C31 121.5(6) . . ?
C29 C30 H30 119.2 . . ?
C31 C30 H30 119.2 . . ?
C30 C31 C32 120.9(6) . . ?
C30 C31 H31 119.6 . . ?
C32 C31 H31 119.6 . . ?
O3 C32 C31 119.7(5) . . ?
O3 C32 C27 123.3(5) . . ?
C31 C32 C27 117.0(5) . . ?
C1 N1 C4 106.4(4) . . ?
C1 N1 Co1 127.5(4) . . ?
C4 N1 Co1 123.5(3) . . ?
C9 N2 C6 107.2(4) . . ?
C9 N2 Co1 127.5(4) . . ?
C6 N2 Co1 124.6(3) . . ?
C16 N3 H3A 120.0 . . ?
C16 N3 H3B 120.0 . . ?
H3A N3 H3B 120.0 . . ?
C23 N4 C24 118.5(5) . . ?
C23 N4 Co1 126.0(4) . . ?
C24 N4 Co1 115.5(4) . . ?
C26 N5 C25 120.8(5) . . ?
C26 N5 Co1 125.0(4) . . ?
C25 N5 Co1 111.3(3) . . ?
C17 O2 Co1 124.4(3) . . ?
C32 O3 Co1 119.3(3) . . ?
N4 Co1 O2 94.60(17) . . ?
N4 Co1 N5 81.7(2) . . ?
O2 Co1 N5 174.99(17) . . ?
N4 Co1 O3 92.16(17) . . ?
O2 Co1 O3 88.87(16) . . ?
N5 Co1 O3 87.91(17) . . ?
N4 Co1 N2 176.33(18) . . ?
O2 Co1 N2 88.40(16) . . ?
N5 Co1 N2 95.44(19) . . ?
O3 Co1 N2 90.01(16) . . ?
N4 Co1 N1 90.28(18) . . ?
O2 Co1 N1 92.87(17) . . ?
N5 Co1 N1 90.52(18) . . ?
O3 Co1 N1 176.88(16) . . ?
N2 Co1 N1 87.45(17) . . ?
Cl3 C33 Cl1 118.0(18) . . ?
Cl3 C33 Cl2 112.2(12) . . ?
Cl1 C33 Cl2 102.4(13) . . ?
Cl3 C33 H33 108.0 . . ?
Cl1 C33 H33 108.0 . . ?
Cl2 C33 H33 108.0 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 N1 1.344(7) . ?
C1 C2 1.410(8) . ?
C1 H1 0.9300 . ?
C2 C3 1.368(8) . ?
C2 H2 0.9300 . ?
C3 C4 1.404(7) . ?
C3 H3 0.9300 . ?
C4 C5 1.397(7) . ?
C4 N1 1.418(6) . ?
C5 C6 1.403(7) . ?
C5 C10 1.491(7) . ?
C6 N2 1.394(6) . ?
C6 C7 1.436(7) . ?
C7 C8 1.356(8) . ?
C7 H7 0.9300 . ?
C8 C9 1.422(8) . ?
C8 H8 0.9300 . ?
C9 N2 1.321(7) . ?
C9 H9 0.9300 . ?
C10 C11 1.375(8) . ?
C10 C15 1.402(8) . ?
C11 C12 1.394(7) . ?
C11 H11 0.9300 . ?
C12 C13 1.386(8) . ?
C12 H12 0.9300 . ?
C13 C14 1.382(8) . ?
C13 C16 1.522(7) . ?
C14 C15 1.388(8) . ?
C14 H14 0.9300 . ?
C15 H15 0.9300 . ?
C16 O1 1.235(8) . ?
C16 N3 1.306(8) . ?
C17 O2 1.301(7) . ?
C17 C22 1.417(8) . ?
C17 C18 1.423(9) . ?
C18 C19 1.379(10) . ?
C18 H18 0.9300 . ?
C19 C20 1.388(12) . ?
C19 H19 0.9300 . ?
C20 C21 1.386(11) . ?
C20 H20 0.9300 . ?
C21 C22 1.427(8) . ?
C21 H21 0.9300 . ?
C22 C23 1.417(8) . ?
C23 N4 1.281(7) . ?
C23 H23 0.9300 . ?
C24 N4 1.471(7) . ?
C24 C25 1.524(9) . ?
C24 H24A 0.9700 . ?
C24 H24B 0.9700 . ?
C25 N5 1.467(7) . ?
C25 H25A 0.9700 . ?
C25 H25B 0.9700 . ?
C26 N5 1.290(7) . ?
C26 C27 1.438(8) . ?
C26 H26 0.9300 . ?
C27 C28 1.405(8) . ?
C27 C32 1.411(8) . ?
C28 C29 1.377(10) . ?
C28 H28 0.9300 . ?
C29 C30 1.385(10) . ?
C29 H29 0.9300 . ?
C30 C31 1.384(9) . ?
C30 H30 0.9300 . ?
C31 C32 1.409(8) . ?
C31 H31 0.9300 . ?
C32 O3 1.320(6) . ?
N1 Co1 1.925(4) . ?
N2 Co1 1.921(4) . ?
N3 H3A 0.8600 . ?
N3 H3B 0.8600 . ?
N4 Co1 1.903(4) . ?
N5 Co1 1.906(4) . ?
O2 Co1 1.904(4) . ?
O3 Co1 1.920(4) . ?
C33 Cl3 1.50(2) . ?
C33 Cl1 1.752(19) . ?
C33 Cl2 1.93(3) . ?
C33 H33 0.9800 . ?
