#------------------------------------------------------------------------------
#$Date: 2016-03-26 16:34:18 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180343 $
#$URL: svn://www.crystallography.net/cod/cif/7/20/12/7201206.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7201206
loop_
_publ_author_name
'Kajiwara, Takashi'
'Takahashi, Kohei'
'Hiraizumi, Tomonari'
'Takaishi, Shinya'
'Yamashita, Masahiro'
_publ_section_title
;
 Structural correlations between the crystal field and magnetic
 anisotropy of Ln--Cu single-molecule magnets
;
_journal_issue                   10
_journal_name_full               CrystEngComm
_journal_page_first              2110
_journal_paper_doi               10.1039/b906182g
_journal_volume                  11
_journal_year                    2009
_chemical_formula_sum            'C46 H64 Cu2 Dy2 N14 O32'
_chemical_formula_weight         1777.19
_chemical_name_systematic
;
?
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 99.705(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   14.4409(15)
_cell_length_b                   18.0725(19)
_cell_length_c                   23.928(2)
_cell_measurement_temperature    100(2)
_cell_volume                     6155.4(10)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'Bruker SHELXTL'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0325
_diffrn_reflns_av_sigmaI/netI    0.0417
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -20
_diffrn_reflns_limit_k_max       25
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_l_max       33
_diffrn_reflns_limit_l_min       -33
_diffrn_reflns_number            36451
_diffrn_reflns_theta_full        30.02
_diffrn_reflns_theta_max         30.02
_diffrn_reflns_theta_min         1.73
_exptl_absorpt_coefficient_mu    3.187
_exptl_absorpt_correction_T_max  0.6707
_exptl_absorpt_correction_T_min  0.5289
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
G. M. Sheldrick, SADABS. Program for Empirical Absorption
Correction of Area Detector Data; University of Gottingen,
Germany, 1996
;
_exptl_crystal_colour            green
_exptl_crystal_density_diffrn    1.918
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             3536
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.15
_refine_diff_density_max         1.836
_refine_diff_density_min         -1.026
_refine_diff_density_rms         0.116
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.945
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     443
_refine_ls_number_reflns         8989
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.945
_refine_ls_R_factor_all          0.0341
_refine_ls_R_factor_gt           0.0263
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0286P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0577
_refine_ls_wR_factor_ref         0.0592
_reflns_number_gt                7403
_reflns_number_total             8989
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b906182g.txt
_cod_data_source_block           DyCu_complex
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        6155.5(11)
_cod_original_sg_symbol_H-M      'C2/c '
_cod_database_code               7201206
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy Dy 0.112168(8) 0.007116(6) 0.144867(5) 0.01174(3) Uani 1 1 d . . .
Cu Cu 0.15479(2) -0.055287(15) 0.284668(12) 0.01183(6) Uani 1 1 d . . .
O1 O 0.07009(12) -0.11702(9) 0.10064(7) 0.0160(4) Uani 1 1 d . . .
O2 O 0.10612(12) -0.09301(9) 0.20898(7) 0.0136(3) Uani 1 1 d . . .
N1 N 0.15476(14) -0.15393(11) 0.31991(8) 0.0147(4) Uani 1 1 d . . .
C1 C 0.03914(19) -0.12890(15) 0.04051(10) 0.0202(5) Uani 1 1 d . . .
H1 H 0.0830 -0.1624 0.0260 0.030 Uiso 1 1 calc R . .
H2 H 0.0373 -0.0814 0.0205 0.030 Uiso 1 1 calc R . .
H3 H -0.0238 -0.1509 0.0343 0.030 Uiso 1 1 calc R . .
C2 C 0.07401(17) -0.17912(13) 0.13496(10) 0.0139(5) Uani 1 1 d . . .
C3 C 0.05693(17) -0.25025(13) 0.11531(10) 0.0164(5) Uani 1 1 d . . .
H4 H 0.0418 -0.2595 0.0757 0.020 Uiso 1 1 calc R . .
C4 C 0.06198(18) -0.30865(14) 0.15394(11) 0.0185(5) Uani 1 1 d . . .
H5 H 0.0476 -0.3576 0.1407 0.022 Uiso 1 1 calc R . .
C5 C 0.08759(17) -0.29557(13) 0.21091(10) 0.0161(5) Uani 1 1 d . . .
H6 H 0.0931 -0.3359 0.2367 0.019 Uiso 1 1 calc R . .
C6 C 0.10594(16) -0.22284(13) 0.23169(10) 0.0133(5) Uani 1 1 d . . .
C7 C 0.09588(16) -0.16340(13) 0.19345(10) 0.0124(5) Uani 1 1 d . . .
C8 C 0.13306(17) -0.21415(13) 0.29205(10) 0.0152(5) Uani 1 1 d . . .
H7 H 0.1352 -0.2582 0.3139 0.018 Uiso 1 1 calc R . .
C9 C 0.1792(2) -0.15951(14) 0.38231(11) 0.0257(6) Uani 1 1 d . . .
H8 H 0.1287 -0.1347 0.3985 0.031 Uiso 1 1 calc R . .
H9 H 0.2373 -0.1303 0.3941 0.031 Uiso 1 1 calc R . .
C10 C 0.1943(3) -0.23330(18) 0.40951(13) 0.0411(8) Uani 1 1 d . . .
H10 H 0.1369 -0.2628 0.4002 0.062 Uiso 1 1 calc R . .
H11 H 0.2101 -0.2273 0.4507 0.062 Uiso 1 1 calc R . .
H12 H 0.2460 -0.2586 0.3956 0.062 Uiso 1 1 calc R . .
O3 O 0.07977(12) 0.13660(9) 0.17026(7) 0.0150(3) Uani 1 1 d . . .
O4 O 0.14765(12) 0.03425(9) 0.24001(7) 0.0133(3) Uani 1 1 d . . .
N2 N 0.26199(14) -0.00720(10) 0.33948(8) 0.0123(4) Uani 1 1 d . . .
H13 H 0.2768 -0.0389 0.3703 0.015 Uiso 1 1 calc R . .
N3 N 0.08491(15) 0.02828(11) 0.38852(8) 0.0133(4) Uani 1 1 d . . .
O5 O 0.02286(12) 0.02711(10) 0.42308(7) 0.0160(4) Uani 1 1 d . . .
O6 O 0.05129(12) 0.00232(9) 0.33708(7) 0.0140(3) Uani 1 1 d . . .
C11 C 0.03067(18) 0.19170(14) 0.13264(10) 0.0188(5) Uani 1 1 d . . .
H14 H -0.0163 0.2163 0.1513 0.028 Uiso 1 1 calc R . .
H15 H -0.0006 0.1677 0.0978 0.028 Uiso 1 1 calc R . .
H16 H 0.0757 0.2284 0.1233 0.028 Uiso 1 1 calc R . .
C12 C 0.12002(17) 0.16095(13) 0.22401(10) 0.0138(5) Uani 1 1 d . . .
C13 C 0.12587(17) 0.23406(13) 0.24048(10) 0.0163(5) Uani 1 1 d . . .
H17 H 0.1011 0.2719 0.2147 0.020 Uiso 1 1 calc R . .
C14 C 0.16859(18) 0.25176(13) 0.29544(11) 0.0175(5) Uani 1 1 d . . .
H18 H 0.1735 0.3020 0.3074 0.021 Uiso 1 1 calc R . .
C15 C 0.20367(17) 0.19620(13) 0.33249(10) 0.0160(5) Uani 1 1 d . . .
H19 H 0.2332 0.2087 0.3698 0.019 Uiso 1 1 calc R . .
C16 C 0.19678(16) 0.12137(13) 0.31626(10) 0.0127(5) Uani 1 1 d . . .
C17 C 0.15540(16) 0.10330(12) 0.26131(10) 0.0124(5) Uani 1 1 d . . .
C18 C 0.23486(17) 0.06537(12) 0.36190(10) 0.0126(5) Uani 1 1 d . . .
H20 H 0.2935 0.0873 0.3839 0.015 Uiso 1 1 calc R . .
C19 C 0.34710(17) -0.00059(13) 0.31282(11) 0.0164(5) Uani 1 1 d . . .
H21 H 0.3974 0.0245 0.3393 0.020 Uiso 1 1 calc R . .
H22 H 0.3327 0.0299 0.2781 0.020 Uiso 1 1 calc R . .
C20 C 0.38100(18) -0.07614(13) 0.29782(11) 0.0186(5) Uani 1 1 d . . .
H23 H 0.3966 -0.1059 0.3323 0.028 Uiso 1 1 calc R . .
H24 H 0.4370 -0.0706 0.2801 0.028 Uiso 1 1 calc R . .
H25 H 0.3314 -0.1008 0.2714 0.028 Uiso 1 1 calc R . .
C21 C 0.16838(17) 0.05438(13) 0.40319(10) 0.0139(5) Uani 1 1 d . . .
H26 H 0.1844(18) 0.0703(14) 0.4379(11) 0.012(7) Uiso 1 1 d . . .
O7 O 0.13934(13) 0.10796(10) 0.06765(7) 0.0211(4) Uani 1 1 d . . .
O8 O 0.17774(13) -0.00557(9) 0.05666(7) 0.0193(4) Uani 1 1 d . . .
N4 N 0.17512(15) 0.06127(12) 0.03893(9) 0.0177(4) Uani 1 1 d . . .
O9 O 0.20744(13) 0.07814(11) -0.00353(8) 0.0262(4) Uani 1 1 d . . .
O10 O 0.27401(13) 0.06553(10) 0.15870(7) 0.0214(4) Uani 1 1 d . . .
O11 O 0.26786(12) -0.05362(10) 0.16536(7) 0.0202(4) Uani 1 1 d . . .
N5 N 0.31772(16) 0.00450(13) 0.16410(9) 0.0221(5) Uani 1 1 d . . .
O12 O 0.40335(14) 0.00076(12) 0.16731(10) 0.0364(6) Uani 1 1 d . . .
O13 O 0.38980(18) 0.02225(14) 0.48882(14) 0.0594(8) Uani 1 1 d . . .
O14 O 0.39151(17) -0.07782(16) 0.44287(9) 0.0501(7) Uani 1 1 d . . .
N6 N 0.39829(17) -0.04470(16) 0.48653(12) 0.0335(6) Uani 1 1 d . . .
C22 C 0.4203(2) -0.0861(2) 0.54016(13) 0.0443(9) Uani 1 1 d . . .
H27 H 0.3696 -0.1212 0.5429 0.066 Uiso 1 1 calc R . .
H28 H 0.4266 -0.0515 0.5721 0.066 Uiso 1 1 calc R . .
H29 H 0.4794 -0.1132 0.5411 0.066 Uiso 1 1 calc R . .
O15 O 0.29864(18) 0.18402(14) 0.47691(9) 0.0469(6) Uani 1 1 d . . .
O16 O 0.43374(17) 0.20480(13) 0.52866(10) 0.0445(6) Uani 1 1 d . . .
N7 N 0.35355(19) 0.17965(14) 0.52172(10) 0.0303(6) Uani 1 1 d . . .
C23 C 0.3211(2) 0.14465(17) 0.57005(12) 0.0342(7) Uani 1 1 d . . .
H30 H 0.3750 0.1346 0.5998 0.051 Uiso 1 1 calc R . .
H31 H 0.2892 0.0981 0.5579 0.051 Uiso 1 1 calc R . .
H32 H 0.2773 0.1778 0.5848 0.051 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O4 Dy O5 132.32(6) . 2 ?
O4 Dy O2 63.32(5) . . ?
O5 Dy O2 116.52(6) 2 . ?
O4 Dy O8 144.43(6) . . ?
O5 Dy O8 79.36(6) 2 . ?
O2 Dy O8 122.79(6) . . ?
O4 Dy O6 83.94(6) . 2 ?
O5 Dy O6 54.55(5) 2 2 ?
O2 Dy O6 73.81(5) . 2 ?
O8 Dy O6 131.47(6) . 2 ?
O4 Dy O11 81.67(6) . . ?
O5 Dy O11 145.72(6) 2 . ?
O2 Dy O11 70.52(6) . . ?
O8 Dy O11 70.20(6) . . ?
O6 Dy O11 144.29(6) 2 . ?
O4 Dy O3 64.94(5) . . ?
O5 Dy O3 81.69(6) 2 . ?
O2 Dy O3 121.96(5) . . ?
O8 Dy O3 114.38(5) . . ?
O6 Dy O3 76.42(5) 2 . ?
O11 Dy O3 124.89(6) . . ?
O4 Dy O1 127.24(5) . . ?
O5 Dy O1 74.44(6) 2 . ?
O2 Dy O1 63.93(5) . . ?
O8 Dy O1 69.92(6) . . ?
O6 Dy O1 82.64(5) 2 . ?
O11 Dy O1 80.47(6) . . ?
O3 Dy O1 154.60(6) . . ?
O4 Dy O10 74.65(6) . . ?
O5 Dy O10 131.79(6) 2 . ?
O2 Dy O10 111.42(6) . . ?
O8 Dy O10 70.84(6) . . ?
O6 Dy O10 151.45(6) 2 . ?
O11 Dy O10 51.11(6) . . ?
O3 Dy O10 77.47(6) . . ?
O1 Dy O10 125.41(6) . . ?
O4 Dy O7 120.33(6) . . ?
O5 Dy O7 67.51(6) 2 . ?
O2 Dy O7 171.46(5) . . ?
O8 Dy O7 49.37(5) . . ?
O6 Dy O7 113.63(5) 2 . ?
O11 Dy O7 101.84(6) . . ?
O3 Dy O7 65.28(5) . . ?
O1 Dy O7 111.80(5) . . ?
O10 Dy O7 64.30(5) . . ?
O4 Dy N3 107.11(6) . 2 ?
O5 Dy N3 27.25(5) 2 2 ?
O2 Dy N3 98.00(6) . 2 ?
O8 Dy N3 106.38(6) . 2 ?
O6 Dy N3 27.81(5) 2 2 ?
O11 Dy N3 161.08(6) . 2 ?
O3 Dy N3 73.83(6) . 2 ?
O1 Dy N3 80.93(6) . 2 ?
O10 Dy N3 146.73(6) . 2 ?
O7 Dy N3 88.32(6) . 2 ?
O4 Dy N5 78.29(6) . . ?
O5 Dy N5 144.46(6) 2 . ?
O2 Dy N5 91.88(6) . . ?
O8 Dy N5 66.88(6) . . ?
O6 Dy N5 160.93(6) 2 . ?
O11 Dy N5 25.64(6) . . ?
O3 Dy N5 101.82(6) . . ?
O1 Dy N5 102.64(6) . . ?
O10 Dy N5 25.55(6) . . ?
O7 Dy N5 81.75(6) . . ?
N3 Dy N5 170.07(6) 2 . ?
O4 Cu O2 78.58(7) . . ?
O4 Cu N1 171.74(8) . . ?
O2 Cu N1 93.16(7) . . ?
O4 Cu N2 87.87(7) . . ?
O2 Cu N2 149.12(8) . . ?
N1 Cu N2 99.47(8) . . ?
O4 Cu O6 86.83(6) . . ?
O2 Cu O6 119.20(6) . . ?
N1 Cu O6 97.25(7) . . ?
N2 Cu O6 87.15(7) . . ?
O4 Cu Dy 38.18(5) . . ?
O2 Cu Dy 40.95(5) . . ?
N1 Cu Dy 133.65(6) . . ?
N2 Cu Dy 118.03(6) . . ?
O6 Cu Dy 110.09(4) . . ?
C2 O1 C1 116.32(18) . . ?
C2 O1 Dy 119.39(13) . . ?
C1 O1 Dy 124.27(14) . . ?
C7 O2 Cu 126.91(15) . . ?
C7 O2 Dy 124.20(14) . . ?
Cu O2 Dy 106.59(7) . . ?
C8 N1 C9 117.5(2) . . ?
C8 N1 Cu 124.08(17) . . ?
C9 N1 Cu 118.44(15) . . ?
C3 C2 O1 124.5(2) . . ?
C3 C2 C7 121.6(2) . . ?
O1 C2 C7 113.9(2) . . ?
C2 C3 C4 119.5(2) . . ?
C5 C4 C3 120.2(2) . . ?
C4 C5 C6 120.8(2) . . ?
C7 C6 C5 119.3(2) . . ?
C7 C6 C8 123.5(2) . . ?
C5 C6 C8 117.2(2) . . ?
O2 C7 C6 123.9(2) . . ?
O2 C7 C2 117.8(2) . . ?
C6 C7 C2 118.3(2) . . ?
N1 C8 C6 127.8(2) . . ?
N1 C9 C10 119.8(2) . . ?
C12 O3 C11 116.27(18) . . ?
C12 O3 Dy 117.27(13) . . ?
C11 O3 Dy 126.15(14) . . ?
C17 O4 Cu 125.02(14) . . ?
C17 O4 Dy 124.27(14) . . ?
Cu O4 Dy 110.55(7) . . ?
C19 N2 C18 111.75(18) . . ?
C19 N2 Cu 110.54(15) . . ?
C18 N2 Cu 112.78(14) . . ?
C21 N3 O5 122.7(2) . . ?
C21 N3 O6 124.1(2) . . ?
O5 N3 O6 113.21(18) . . ?
C21 N3 Dy 166.20(17) . 2 ?
O5 N3 Dy 54.62(11) . 2 ?
O6 N3 Dy 60.11(11) . 2 ?
N3 O5 Dy 98.12(13) . 2 ?
N3 O6 Cu 118.96(13) . . ?
N3 O6 Dy 92.08(12) . 2 ?
Cu O6 Dy 145.17(7) . 2 ?
C13 C12 O3 124.3(2) . . ?
C13 C12 C17 122.0(2) . . ?
O3 C12 C17 113.7(2) . . ?
C12 C13 C14 119.1(2) . . ?
C15 C14 C13 119.8(2) . . ?
C14 C15 C16 121.5(2) . . ?
C17 C16 C15 119.2(2) . . ?
C17 C16 C18 124.7(2) . . ?
C15 C16 C18 116.2(2) . . ?
O4 C17 C16 124.9(2) . . ?
O4 C17 C12 116.6(2) . . ?
C16 C17 C12 118.5(2) . . ?
N2 C18 C21 110.81(19) . . ?
N2 C18 C16 114.26(19) . . ?
C21 C18 C16 111.5(2) . . ?
N2 C19 C20 110.74(19) . . ?
N3 C21 C18 122.8(2) . . ?
N4 O7 Dy 92.41(13) . . ?
N4 O8 Dy 101.66(14) . . ?
O9 N4 O7 122.5(2) . . ?
O9 N4 O8 121.1(2) . . ?
O7 N4 O8 116.5(2) . . ?
N5 O10 Dy 94.78(14) . . ?
N5 O11 Dy 97.33(14) . . ?
O12 N5 O10 122.2(2) . . ?
O12 N5 O11 121.3(2) . . ?
O10 N5 O11 116.5(2) . . ?
O12 N5 Dy 174.18(19) . . ?
O10 N5 Dy 59.67(12) . . ?
O11 N5 Dy 57.03(12) . . ?
O14 N6 O13 122.9(3) . . ?
O14 N6 C22 118.8(3) . . ?
O13 N6 C22 118.3(3) . . ?
O15 N7 O16 123.4(3) . . ?
O15 N7 C23 118.3(3) . . ?
O16 N7 C23 118.3(2) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Dy O4 2.3005(16) . ?
Dy O5 2.3467(17) 2 ?
Dy O2 2.3834(16) . ?
Dy O8 2.4654(18) . ?
Dy O6 2.4718(17) 2 ?
Dy O11 2.4756(18) . ?
Dy O3 2.4819(16) . ?
Dy O1 2.5111(16) . ?
Dy O10 2.5348(18) . ?
Dy O7 2.6709(18) . ?
Dy N3 2.849(2) 2 ?
Dy N5 2.927(2) . ?
Cu O4 1.9323(16) . ?
Cu O2 1.9517(16) . ?
Cu N1 1.972(2) . ?
Cu N2 2.046(2) . ?
Cu O6 2.3501(17) . ?
O1 C2 1.386(3) . ?
O1 C1 1.449(3) . ?
O2 C7 1.327(3) . ?
N1 C8 1.287(3) . ?
N1 C9 1.479(3) . ?
C2 C3 1.377(3) . ?
C2 C7 1.411(3) . ?
C3 C4 1.397(3) . ?
C4 C5 1.371(3) . ?
C5 C6 1.415(3) . ?
C6 C7 1.403(3) . ?
C6 C8 1.440(3) . ?
C9 C10 1.484(4) . ?
O3 C12 1.391(3) . ?
O3 C11 1.446(3) . ?
O4 C17 1.345(3) . ?
N2 C19 1.482(3) . ?
N2 C18 1.494(3) . ?
N3 C21 1.287(3) . ?
N3 O5 1.318(3) . ?
N3 O6 1.330(2) . ?
N3 Dy 2.849(2) 2 ?
O5 Dy 2.3467(17) 2 ?
O6 Dy 2.4718(17) 2 ?
C12 C13 1.377(3) . ?
C12 C17 1.411(3) . ?
C13 C14 1.393(3) . ?
C14 C15 1.378(3) . ?
C15 C16 1.406(3) . ?
C16 C17 1.388(3) . ?
C16 C18 1.522(3) . ?
C18 C21 1.502(3) . ?
C19 C20 1.514(3) . ?
O7 N4 1.253(3) . ?
O8 N4 1.279(3) . ?
N4 O9 1.226(3) . ?
O10 N5 1.267(3) . ?
O11 N5 1.277(3) . ?
N5 O12 1.228(3) . ?
O13 N6 1.218(4) . ?
O14 N6 1.194(3) . ?
N6 C22 1.473(4) . ?
O15 N7 1.224(3) . ?
O16 N7 1.229(3) . ?
N7 C23 1.463(3) . ?
