#------------------------------------------------------------------------------
#$Date: 2016-03-26 16:36:20 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180345 $
#$URL: svn://www.crystallography.net/cod/cif/7/20/14/7201442.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7201442
loop_
_publ_author_name
'Lee, Kwang-Ming'
'Chen, Jack C. C.'
'Huang, Chao-June'
'Lin, Ivan J. B.'
_publ_section_title
;
 Anion-controlled assemble of C--H⋯X hydrogen bonded helical
 tubes or catemers by crescent imidazolium salts
;
_journal_issue                   12
_journal_name_full               CrystEngComm
_journal_page_first              2804
_journal_paper_doi               10.1039/b911665f
_journal_volume                  11
_journal_year                    2009
_chemical_formula_sum            'C9 H10 F6 N5 O P'
_chemical_formula_weight         349.19
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 104.745(16)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   12.9852(16)
_cell_length_b                   24.937(2)
_cell_length_c                   8.9006(12)
_cell_measurement_reflns_used    21
_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      12.92
_cell_measurement_theta_min      10.01
_cell_volume                     2787.2(6)
_computing_cell_refinement       'Bruker XSCANS'
_computing_data_collection       'Bruker XSCANS'
_computing_data_reduction        'Bruker XSCANS'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'Bruker SHELXTL'
_computing_structure_solution    'Bruker SHELXS'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0282
_diffrn_reflns_av_sigmaI/netI    0.0262
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       29
_diffrn_reflns_limit_k_min       -29
_diffrn_reflns_limit_l_max       10
_diffrn_reflns_limit_l_min       -1
_diffrn_reflns_number            11693
_diffrn_reflns_theta_full        25.01
_diffrn_reflns_theta_max         25.01
_diffrn_reflns_theta_min         1.62
_diffrn_standards_decay_%        3.94
_diffrn_standards_interval_count 397
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    0.275
_exptl_absorpt_correction_T_max  0.8638
_exptl_absorpt_correction_T_min  0.7837
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            white
_exptl_crystal_density_diffrn    1.664
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       column
_exptl_crystal_F_000             1408
_exptl_crystal_size_max          0.3
_exptl_crystal_size_mid          0.3
_exptl_crystal_size_min          0.4
_refine_diff_density_max         0.291
_refine_diff_density_min         -0.287
_refine_diff_density_rms         0.041
_refine_ls_extinction_coef       0.0035(4)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.032
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     508
_refine_ls_number_reflns         4925
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.032
_refine_ls_R_factor_all          0.0609
_refine_ls_R_factor_gt           0.0432
_refine_ls_shift/su_max          0.106
_refine_ls_shift/su_mean         0.005
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0583P)²+0.9559P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1078
_refine_ls_wR_factor_ref         0.1181
_reflns_number_gt                3701
_reflns_number_total             4925
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b911665f.txt
_cod_data_source_block           2
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P2(1)/c
_cod_database_code               7201442
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
P1 P 0.36291(5) 0.34843(3) 0.49575(8) 0.0564(2) Uani 1 1 d . . .
P2 P 0.86570(5) 0.37355(3) 0.51170(7) 0.0536(2) Uani 1 1 d . . .
F1' F 0.3423(13) 0.2861(4) 0.5001(19) 0.147(5) Uani 0.448(17) 1 d P A 1
F2' F 0.2448(9) 0.3568(9) 0.496(2) 0.164(6) Uani 0.448(17) 1 d P A 1
F3' F 0.3825(11) 0.4014(5) 0.5305(17) 0.206(7) Uani 0.448(17) 1 d P A 1
F4' F 0.3930(13) 0.3304(8) 0.6690(15) 0.145(6) Uani 0.448(17) 1 d P A 1
F5' F 0.4780(7) 0.3394(7) 0.4949(17) 0.130(5) Uani 0.448(17) 1 d P A 1
F6' F 0.3285(10) 0.3661(5) 0.3242(13) 0.118(4) Uani 0.448(17) 1 d P A 1
F7' F 0.8479(9) 0.3161(4) 0.4331(15) 0.121(2) Uani 0.61(2) 1 d P B 2
F8' F 0.8916(8) 0.4305(3) 0.5524(17) 0.160(4) Uani 0.61(2) 1 d P B 2
F9' F 0.7482(6) 0.3729(5) 0.5234(11) 0.098(3) Uani 0.61(2) 1 d P B 2
F10' F 0.8960(12) 0.3588(6) 0.6885(10) 0.117(4) Uani 0.61(2) 1 d P B 2
F11' F 0.8305(6) 0.3900(4) 0.3337(9) 0.089(2) Uani 0.61(2) 1 d P B 2
F12' F 0.9836(4) 0.3673(4) 0.5023(10) 0.082(2) Uani 0.61(2) 1 d P B 2
F1 F 0.3801(8) 0.2907(3) 0.4430(11) 0.120(3) Uani 0.552(17) 1 d P A 3
F2 F 0.2476(7) 0.3382(5) 0.5030(14) 0.115(3) Uani 0.552(17) 1 d P A 3
F3 F 0.3528(9) 0.4128(3) 0.5285(8) 0.118(3) Uani 0.552(17) 1 d P A 3
F4 F 0.4061(10) 0.3454(5) 0.6771(12) 0.106(3) Uani 0.552(17) 1 d P A 3
F5 F 0.4794(6) 0.3590(6) 0.4867(15) 0.135(4) Uani 0.552(17) 1 d P A 3
F6 F 0.3210(7) 0.3531(5) 0.3147(10) 0.122(4) Uani 0.552(17) 1 d P A 3
F7 F 0.8124(17) 0.3188(8) 0.474(2) 0.134(5) Uani 0.39(2) 1 d P B 4
F8 F 0.9041(7) 0.4283(5) 0.6058(19) 0.109(4) Uani 0.39(2) 1 d P B 4
F9 F 0.7497(12) 0.3992(11) 0.5135(18) 0.120(6) Uani 0.39(2) 1 d P B 4
F10 F 0.8922(19) 0.3422(10) 0.671(2) 0.125(6) Uani 0.39(2) 1 d P B 4
F11 F 0.8422(12) 0.4020(6) 0.3531(18) 0.105(5) Uani 0.39(2) 1 d P B 4
F12 F 0.9755(10) 0.3554(7) 0.5032(17) 0.105(4) Uani 0.39(2) 1 d P B 4
O1 O 0.66454(15) 0.28261(7) 0.04826(19) 0.0639(5) Uani 1 1 d . . .
O2 O 1.10218(19) 0.21839(8) 0.5180(2) 0.0815(6) Uani 1 1 d . . .
N1 N 0.41906(13) 0.39333(7) 0.0207(2) 0.0429(4) Uani 1 1 d . . .
N2 N 0.52007(14) 0.33482(7) 0.1623(2) 0.0450(4) Uani 1 1 d . . .
N3 N 0.24232(15) 0.38770(8) -0.1121(3) 0.0617(6) Uani 1 1 d . . .
N4 N 0.34423(16) 0.46500(8) -0.1331(3) 0.0630(6) Uani 1 1 d . . .
N5 N 0.68832(18) 0.21711(8) 0.2259(2) 0.0642(6) Uani 1 1 d . . .
H10 H 0.7354 0.2010 0.1895 0.077 Uiso 1 1 calc R . .
H9 H 0.6704 0.2041 0.3051 0.077 Uiso 1 1 calc R . .
N6 N 0.88939(14) 0.09618(7) 0.5193(2) 0.0502(5) Uani 1 1 d . . .
N7 N 0.98111(16) 0.15924(8) 0.6541(2) 0.0562(5) Uani 1 1 d . . .
N8 N 0.71599(17) 0.09700(8) 0.3697(2) 0.0627(6) Uani 1 1 d . . .
N9 N 0.82320(17) 0.01906(8) 0.3845(3) 0.0658(6) Uani 1 1 d . . .
N10 N 1.15537(17) 0.27279(8) 0.7245(2) 0.0619(5) Uani 1 1 d . . .
H20 H 1.2028 0.2885 0.6881 0.074 Uiso 1 1 calc R . .
H19 H 1.1466 0.2821 0.8135 0.074 Uiso 1 1 calc R . .
C1 C 0.42696(17) 0.34213(8) 0.0660(3) 0.0455(5) Uani 1 1 d . . .
H1 H 0.3748 0.3160 0.0342 0.055 Uiso 1 1 calc R . .
C2 C 0.51207(17) 0.41901(9) 0.0931(3) 0.0559(6) Uani 1 1 d . . .
H2 H 0.5284 0.4549 0.0826 0.067 Uiso 1 1 calc R . .
C3 C 0.57443(19) 0.38243(9) 0.1815(3) 0.0609(7) Uani 1 1 d . . .
H3 H 0.6425 0.3882 0.2447 0.073 Uiso 1 1 calc R . .
C4 C 0.32842(17) 0.41710(9) -0.0827(3) 0.0464(5) Uani 1 1 d . . .
C5 C 0.1584(2) 0.41050(12) -0.2095(4) 0.0772(8) Uani 1 1 d . . .
H6 H 0.0941 0.3920 -0.2347 0.093 Uiso 1 1 calc R . .
C6 C 0.1631(2) 0.45961(12) -0.2733(4) 0.0823(9) Uani 1 1 d . . .
H5 H 0.1041 0.4747 -0.3422 0.099 Uiso 1 1 calc R . .
C7 C 0.2579(2) 0.48569(11) -0.2318(4) 0.0813(9) Uani 1 1 d . . .
H4 H 0.2632 0.5194 -0.2738 0.098 Uiso 1 1 calc R . .
C8 C 0.56198(19) 0.28435(9) 0.2354(3) 0.0513(6) Uani 1 1 d . . .
H8 H 0.5041 0.2589 0.2261 0.062 Uiso 1 1 calc R . .
H7 H 0.5939 0.2903 0.3451 0.062 Uiso 1 1 calc R . .
C9 C 0.64400(17) 0.26134(8) 0.1608(2) 0.0443(5) Uani 1 1 d . . .
C10 C 0.8887(2) 0.14772(9) 0.5606(3) 0.0519(6) Uani 1 1 d . . .
H11 H 0.8320 0.1714 0.5282 0.062 Uiso 1 1 calc R . .
C11 C 0.9869(2) 0.07515(11) 0.5926(3) 0.0712(8) Uani 1 1 d . . .
H12 H 1.0095 0.0401 0.5852 0.085 Uiso 1 1 calc R . .
C12 C 1.0432(2) 0.11453(11) 0.6763(4) 0.0767(8) Uani 1 1 d . . .
H13 H 1.1123 0.1119 0.7386 0.092 Uiso 1 1 calc R . .
C13 C 0.80322(19) 0.06886(9) 0.4173(3) 0.0505(5) Uani 1 1 d . . .
C14 C 0.6363(2) 0.07094(13) 0.2722(4) 0.0773(8) Uani 1 1 d . . .
H16 H 0.5719 0.0886 0.2336 0.093 Uiso 1 1 calc R . .
C15 C 0.6463(2) 0.01918(13) 0.2273(4) 0.0806(9) Uani 1 1 d . . .
H15 H 0.5905 0.0014 0.1592 0.097 Uiso 1 1 calc R . .
C16 C 0.7409(3) -0.00500(12) 0.2863(4) 0.0810(9) Uani 1 1 d . . .
H14 H 0.7494 -0.0402 0.2573 0.097 Uiso 1 1 calc R . .
C17 C 1.0158(2) 0.21153(10) 0.7208(3) 0.0635(7) Uani 1 1 d . . .
H17 H 1.0469 0.2079 0.8316 0.076 Uiso 1 1 calc R . .
H18 H 0.9551 0.2354 0.7056 0.076 Uiso 1 1 calc R . .
C18 C 1.0967(2) 0.23479(9) 0.6447(3) 0.0527(6) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
F3' P1 F5' 91.0(7) . . ?
F3' P1 F2 106.2(7) . . ?
F5' P1 F2 161.7(7) . . ?
F3' P1 F6' 86.5(8) . . ?
F5' P1 F6' 94.3(8) . . ?
F2 P1 F6' 92.8(7) . . ?
F3' P1 F1 159.3(6) . . ?
F5' P1 F1 69.0(6) . . ?
F2 P1 F1 94.3(5) . . ?
F6' P1 F1 89.6(6) . . ?
F3' P1 F2' 89.8(8) . . ?
F5' P1 F2' 179.1(8) . . ?
F2 P1 F2' 17.4(10) . . ?
F6' P1 F2' 85.8(8) . . ?
F1 P1 F2' 110.2(8) . . ?
F3' P1 F5 73.8(7) . . ?
F5' P1 F5 18.5(8) . . ?
F2 P1 F5 179.5(7) . . ?
F6' P1 F5 86.6(7) . . ?
F1 P1 F5 85.7(5) . . ?
F2' P1 F5 162.4(8) . . ?
F3' P1 F4' 94.0(10) . . ?
F5' P1 F4' 87.9(8) . . ?
F2 P1 F4' 84.9(8) . . ?
F6' P1 F4' 177.8(8) . . ?
F1 P1 F4' 90.7(9) . . ?
F2' P1 F4' 92.0(9) . . ?
F5 P1 F4' 95.6(8) . . ?
F3' P1 F6 99.0(7) . . ?
F5' P1 F6 95.2(7) . . ?
F2 P1 F6 88.2(6) . . ?
F6' P1 F6 12.6(8) . . ?
F1 P1 F6 78.3(6) . . ?
F2' P1 F6 84.8(8) . . ?
F5 P1 F6 91.3(6) . . ?
F4' P1 F6 166.6(8) . . ?
F3' P1 F4 79.4(7) . . ?
F5' P1 F4 84.4(8) . . ?
F2 P1 F4 92.6(7) . . ?
F6' P1 F4 165.8(6) . . ?
F1 P1 F4 103.0(6) . . ?
F2' P1 F4 95.6(8) . . ?
F5 P1 F4 87.9(7) . . ?
F4' P1 F4 15.0(10) . . ?
F6 P1 F4 178.4(6) . . ?
F3' P1 F1' 165.7(8) . . ?
F5' P1 F1' 91.6(7) . . ?
F2 P1 F1' 70.3(7) . . ?
F6' P1 F1' 107.3(9) . . ?
F1 P1 F1' 29.6(6) . . ?
F2' P1 F1' 87.6(7) . . ?
F5 P1 F1' 109.9(6) . . ?
F4' P1 F1' 72.1(12) . . ?
F6 P1 F1' 94.7(8) . . ?
F4 P1 F1' 86.9(7) . . ?
F3' P1 F3 14.8(8) . . ?
F5' P1 F3 105.7(6) . . ?
F2 P1 F3 91.9(5) . . ?
F6' P1 F3 83.1(5) . . ?
F1 P1 F3 170.7(4) . . ?
F2' P1 F3 75.2(8) . . ?
F5 P1 F3 88.1(5) . . ?
F4' P1 F3 96.8(7) . . ?
F6 P1 F3 95.0(5) . . ?
F4 P1 F3 83.6(5) . . ?
F1' P1 F3 159.4(8) . . ?
F8' P2 F12 98.1(7) . . ?
F8' P2 F7 166.0(10) . . ?
F12 P2 F7 95.8(8) . . ?
F8' P2 F11 76.2(7) . . ?
F12 P2 F11 93.5(8) . . ?
F7 P2 F11 103.8(11) . . ?
F8' P2 F9' 99.1(6) . . ?
F12 P2 F9' 162.0(6) . . ?
F7 P2 F9' 66.9(8) . . ?
F11 P2 F9' 95.5(6) . . ?
F8' P2 F12' 86.9(5) . . ?
F12 P2 F12' 11.7(8) . . ?
F7 P2 F12' 107.1(9) . . ?
F11 P2 F12' 88.0(6) . . ?
F9' P2 F12' 173.6(4) . . ?
F8' P2 F10' 89.8(6) . . ?
F12 P2 F10' 88.9(8) . . ?
F7 P2 F10' 89.6(10) . . ?
F11 P2 F10' 166.0(8) . . ?
F9' P2 F10' 86.0(7) . . ?
F12' P2 F10' 91.8(7) . . ?
F8' P2 F10 105.7(8) . . ?
F12 P2 F10 84.5(11) . . ?
F7 P2 F10 74.7(12) . . ?
F11 P2 F10 177.4(10) . . ?
F9' P2 F10 85.9(9) . . ?
F12' P2 F10 90.3(10) . . ?
F10' P2 F10 16.1(12) . . ?
F8' P2 F11' 89.2(5) . . ?
F12 P2 F11' 93.6(6) . . ?
F7 P2 F11' 90.8(8) . . ?
F11 P2 F11' 13.1(9) . . ?
F9' P2 F11' 91.8(4) . . ?
F12' P2 F11' 90.6(4) . . ?
F10' P2 F11' 177.4(6) . . ?
F10 P2 F11' 165.1(9) . . ?
F8' P2 F7' 166.4(8) . . ?
F12 P2 F7' 75.0(6) . . ?
F7 P2 F7' 24.4(6) . . ?
F11 P2 F7' 92.3(10) . . ?
F9' P2 F7' 89.1(4) . . ?
F12' P2 F7' 85.5(4) . . ?
F10' P2 F7' 101.7(8) . . ?
F10 P2 F7' 85.6(12) . . ?
F11' P2 F7' 79.7(7) . . ?
F8' P2 F8 16.6(8) . . ?
F12 P2 F8 96.3(7) . . ?
F7 P2 F8 158.8(12) . . ?
F11 P2 F8 92.8(8) . . ?
F9' P2 F8 98.8(6) . . ?
F12' P2 F8 86.3(4) . . ?
F10' P2 F8 73.2(7) . . ?
F10 P2 F8 89.1(9) . . ?
F11' P2 F8 105.8(6) . . ?
F7' P2 F8 170.1(6) . . ?
F8' P2 F9 77.0(10) . . ?
F12 P2 F9 174.1(9) . . ?
F7 P2 F9 89.1(8) . . ?
F11 P2 F9 82.0(9) . . ?
F9' P2 F9 23.7(8) . . ?
F12' P2 F9 162.7(9) . . ?
F10' P2 F9 94.5(9) . . ?
F10 P2 F9 100.1(13) . . ?
F11' P2 F9 83.0(7) . . ?
F7' P2 F9 109.0(8) . . ?
F8 P2 F9 80.1(8) . . ?
C1 N1 C2 108.26(17) . . ?
C1 N1 C4 125.45(18) . . ?
C2 N1 C4 126.28(18) . . ?
C1 N2 C3 108.83(18) . . ?
C1 N2 C8 126.34(19) . . ?
C3 N2 C8 124.82(19) . . ?
C4 N3 C5 114.0(2) . . ?
C4 N4 C7 113.4(2) . . ?
C10 N6 C11 107.9(2) . . ?
C10 N6 C13 125.2(2) . . ?
C11 N6 C13 126.95(19) . . ?
C10 N7 C12 109.1(2) . . ?
C10 N7 C17 126.5(2) . . ?
C12 N7 C17 124.4(2) . . ?
C13 N8 C14 114.4(2) . . ?
C13 N9 C16 113.5(2) . . ?
N2 C1 N1 108.62(18) . . ?
C3 C2 N1 106.7(2) . . ?
C2 C3 N2 107.6(2) . . ?
N3 C4 N4 130.1(2) . . ?
N3 C4 N1 114.8(2) . . ?
N4 C4 N1 115.11(19) . . ?
N3 C5 C6 122.7(3) . . ?
C5 C6 C7 116.9(2) . . ?
N4 C7 C6 122.9(3) . . ?
N2 C8 C9 110.96(18) . . ?
O1 C9 N5 124.5(2) . . ?
O1 C9 C8 121.55(19) . . ?
N5 C9 C8 113.98(19) . . ?
N7 C10 N6 108.5(2) . . ?
C12 C11 N6 107.0(2) . . ?
C11 C12 N7 107.6(2) . . ?
N8 C13 N9 129.6(2) . . ?
N8 C13 N6 115.2(2) . . ?
N9 C13 N6 115.2(2) . . ?
N8 C14 C15 122.2(3) . . ?
C16 C15 C14 117.0(3) . . ?
N9 C16 C15 123.4(3) . . ?
N7 C17 C18 109.9(2) . . ?
O2 C18 N10 125.7(2) . . ?
O2 C18 C17 120.0(2) . . ?
N10 C18 C17 114.3(2) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
P1 F3' 1.365(11) . ?
P1 F5' 1.514(9) . ?
P1 F2 1.537(8) . ?
P1 F6' 1.542(10) . ?
P1 F1 1.548(7) . ?
P1 F2' 1.549(12) . ?
P1 F5 1.557(9) . ?
P1 F4' 1.558(13) . ?
P1 F6 1.569(8) . ?
P1 F4 1.570(10) . ?
P1 F1' 1.578(9) . ?
P1 F3 1.642(7) . ?
P2 F8' 1.482(8) . ?
P2 F12 1.516(10) . ?
P2 F7 1.528(14) . ?
P2 F11 1.540(11) . ?
P2 F9' 1.556(8) . ?
P2 F12' 1.562(6) . ?
P2 F10' 1.565(9) . ?
P2 F10 1.577(16) . ?
P2 F11' 1.587(7) . ?
P2 F7' 1.586(9) . ?
P2 F8 1.613(11) . ?
P2 F9 1.641(13) . ?
O1 C9 1.221(3) . ?
O2 C18 1.219(3) . ?
N1 C1 1.335(3) . ?
N1 C2 1.374(3) . ?
N1 C4 1.426(3) . ?
N2 C1 1.305(3) . ?
N2 C3 1.370(3) . ?
N2 C8 1.457(3) . ?
N3 C4 1.307(3) . ?
N3 C5 1.335(3) . ?
N4 C4 1.310(3) . ?
N4 C7 1.339(3) . ?
N5 C9 1.309(3) . ?
N6 C10 1.337(3) . ?
N6 C11 1.373(3) . ?
N6 C13 1.423(3) . ?
N7 C10 1.307(3) . ?
N7 C12 1.360(3) . ?
N7 C17 1.456(3) . ?
N8 C13 1.308(3) . ?
N8 C14 1.338(3) . ?
N9 C13 1.316(3) . ?
N9 C16 1.338(3) . ?
N10 C18 1.307(3) . ?
C2 C3 1.335(3) . ?
C5 C6 1.358(4) . ?
C6 C7 1.358(4) . ?
C8 C9 1.505(3) . ?
C11 C12 1.332(4) . ?
C14 C15 1.367(4) . ?
C15 C16 1.349(4) . ?
C17 C18 1.504(3) . ?
