#------------------------------------------------------------------------------
#$Date: 2016-03-26 16:53:33 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180361 $
#$URL: svn://www.crystallography.net/cod/cif/7/20/30/7203095.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7203095
loop_
_publ_author_name
'Bardelang, David'
'Udachin, Konstantin A.'
'Leek, Donald M.'
'Ripmeester, John A.'
_publ_section_title
;
 Highly symmetric columnar channels in metal-free cucurbit[n]uril
 hydrate crystals (n = 6, 8)
;
_journal_issue                   11
_journal_name_full               CrystEngComm
_journal_page_first              973
_journal_paper_doi               10.1039/b711285h
_journal_volume                  9
_journal_year                    2007
_chemical_formula_sum            'C48 H168 N40 O100'
_chemical_formula_weight         2906.22
_chemical_name_systematic
;
?
;
_space_group_IT_number           139
_symmetry_cell_setting           tetragonal
_symmetry_space_group_name_Hall  '-I 4 2'
_symmetry_space_group_name_H-M   'I 4/m m m'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   24.0685(6)
_cell_length_b                   24.0685(6)
_cell_length_c                   10.9542(6)
_cell_measurement_temperature    100(2)
_cell_volume                     6345.7(4)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.928
_diffrn_measured_fraction_theta_max 0.928
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71070
_diffrn_reflns_av_R_equivalents  0.0371
_diffrn_reflns_av_sigmaI/netI    0.0074
_diffrn_reflns_limit_h_max       28
_diffrn_reflns_limit_h_min       -28
_diffrn_reflns_limit_k_max       28
_diffrn_reflns_limit_k_min       -28
_diffrn_reflns_limit_l_max       12
_diffrn_reflns_limit_l_min       -12
_diffrn_reflns_number            90650
_diffrn_reflns_theta_full        24.71
_diffrn_reflns_theta_max         24.71
_diffrn_reflns_theta_min         2.68
_exptl_absorpt_coefficient_mu    0.148
_exptl_absorpt_correction_T_max  0.9710
_exptl_absorpt_correction_T_min  0.9297
_exptl_absorpt_correction_type   multi-scal
_exptl_absorpt_process_details   sadabs
_exptl_crystal_density_diffrn    1.521
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             3072
_exptl_crystal_size_max          0.50
_exptl_crystal_size_mid          0.40
_exptl_crystal_size_min          0.20
_refine_diff_density_max         0.736
_refine_diff_density_min         -0.823
_refine_diff_density_rms         0.129
_refine_ls_extinction_coef       0.006(2)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.744
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     236
_refine_ls_number_reflns         1449
_refine_ls_number_restraints     339
_refine_ls_restrained_S_all      1.729
_refine_ls_R_factor_all          0.1262
_refine_ls_R_factor_gt           0.1181
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.2000P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.3212
_refine_ls_wR_factor_ref         0.3465
_reflns_number_gt                1233
_reflns_number_total             1449
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b711285h.txt
_cod_data_source_block           dav17
_cod_original_sg_symbol_H-M      I4/mmm
_cod_database_code               7203095
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'-y, x, z'
'y, -x, z'
'-x, y, -z'
'x, -y, -z'
'y, x, -z'
'-y, -x, -z'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, -y+1/2, z+1/2'
'-y+1/2, x+1/2, z+1/2'
'y+1/2, -x+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z+1/2'
'y+1/2, x+1/2, -z+1/2'
'-y+1/2, -x+1/2, -z+1/2'
'-x, -y, -z'
'x, y, -z'
'y, -x, -z'
'-y, x, -z'
'x, -y, z'
'-x, y, z'
'-y, -x, z'
'y, x, z'
'-x+1/2, -y+1/2, -z+1/2'
'x+1/2, y+1/2, -z+1/2'
'y+1/2, -x+1/2, -z+1/2'
'-y+1/2, x+1/2, -z+1/2'
'x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, z+1/2'
'-y+1/2, -x+1/2, z+1/2'
'y+1/2, x+1/2, z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
O1 O 0.41851(7) 0.31105(7) 0.22268(14) 0.0554(5) Uani 1 1 d U . .
N1 N 0.36312(8) 0.29209(8) 0.38946(16) 0.0460(5) Uani 1 1 d U . .
N2 N 0.44975(7) 0.26203(7) 0.38941(17) 0.0423(5) Uani 1 1 d U . .
C1 C 0.36642(13) 0.25961(12) 0.5000 0.0449(7) Uani 1 2 d SU . .
H1 H 0.3392 0.2282 0.5000 0.054 Uiso 1 2 calc SR . .
C2 C 0.42731(11) 0.23867(11) 0.5000 0.0396(7) Uani 1 2 d SU . .
H2 H 0.4294 0.1972 0.5000 0.048 Uiso 1 2 calc SR . .
C3 C 0.5000 0.24053(14) 0.3339(3) 0.0463(7) Uani 1 2 d SU . .
H3A H 0.5000 0.2501 0.2460 0.056 Uiso 1 2 calc SR . .
H3B H 0.5000 0.1995 0.3407 0.056 Uiso 1 2 calc SR . .
C4 C 0.41140(10) 0.29071(9) 0.3247(2) 0.0433(6) Uani 1 1 d U . .
C5 C 0.31172(11) 0.31172(11) 0.3373(3) 0.0516(8) Uani 1 2 d SU . .
H5A H 0.2829 0.2829 0.3487 0.062 Uiso 1 2 calc SR . .
H5B H 0.3170 0.3170 0.2484 0.062 Uiso 1 2 calc SR . .
O1M O 0.1611(2) 0.3929(2) 0.3032(7) 0.1091(18) Uani 0.50 1 d PDU A -2
O2M O 0.1926(2) 0.3295(3) 0.2116(9) 0.137(3) Uani 0.50 1 d PDU A -2
O3M O 0.1009(4) 0.3595(4) 0.1842(10) 0.164(3) Uani 0.50 1 d PDU A -2
N1M N 0.1479(3) 0.3528(4) 0.2368(13) 0.120(2) Uani 0.50 1 d PDU A -2
O1W O 0.0000 0.3893(3) 0.0000 0.144(3) Uani 1 4 d SU . .
O2W O 0.4020(7) 0.4446(7) 0.471(2) 0.197(6) Uani 0.25 1 d PDU B -33
O3W O 0.5000 0.396(3) 0.550(5) 0.186(6) Uani 0.15 2 d SPDU . .
O33W O 0.5000 0.393(2) 0.5000 0.186(6) Uani 0.30 4 d SPU . .
O4W O 0.3927(7) 0.2463(7) 0.0000 0.177(4) Uani 0.60 2 d SPU D .
O5W O 0.348(4) 0.250(3) 0.0000 0.171(5) Uani 0.12 2 d SPU . .
O6W O 0.0231(12) 0.3311(9) 0.5928(16) 0.165(8) Uani 0.13 1 d PU C -33
O66W O 0.0174(14) 0.3484(11) 0.537(2) 0.181(10) Uani 0.13 1 d PU C -33
O7W O 0.3508(7) 0.3171(8) -0.019(3) 0.180(5) Uani 0.25 1 d PU D -33
O37W O 0.3160(7) 0.2797(7) 0.021(2) 0.165(5) Uani 0.25 1 d PU D -33
O8W O 0.1723(10) 0.2615(9) 0.592(2) 0.082(4) Uani 0.10 1 d PU . -33
O81W O 0.2104(9) 0.2282(9) 0.5515(19) 0.082(4) Uani 0.10 1 d PU . -33
O9W O 0.0511(3) 0.4489(3) 0.2500 0.176(4) Uani 0.50 2 d SPU . .
O10W O 0.0000 0.4232(9) 0.048(3) 0.150(5) Uani 0.24 2 d SPU . .
O11W O 0.4205(4) 0.4205(4) 0.1176(10) 0.177(4) Uani 0.50 2 d SPU . .
O12W O 0.0963(16) 0.502(9) 0.0000 0.145(9) Uani 0.24 4 d SPU . .
O92W O 0.099(2) 0.468(2) 0.0000 0.144(8) Uani 0.12 2 d SPU . .
O13W O 0.5000 0.4082(6) 0.2456(15) 0.154(4) Uani 0.50 2 d SPU . .
O14W O 0.4425(6) 0.2595(5) 0.0000 0.235(4) Uani 1 2 d SU . .
O15W O 0.424(2) 1.038(2) 0.033(5) 0.102(10) Uani 0.05 1 d PU E -2
O16W O 0.3830(10) 0.5000 0.1214(14) 0.242(9) Uani 0.50 2 d SPU . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C4 N1 C5 122.2(2) . . ?
C4 N1 C1 112.2(2) . . ?
C5 N1 C1 123.9(2) . . ?
C4 N2 C2 112.58(19) . . ?
C4 N2 C3 122.1(2) . . ?
C2 N2 C3 121.8(2) . . ?
N1 C1 N1 114.0(2) . 18_556 ?
N1 C1 C2 103.19(17) . . ?
N1 C1 C2 103.19(17) 18_556 . ?
N2 C2 N2 114.5(2) 18_556 . ?
N2 C2 C1 103.16(15) 18_556 . ?
N2 C2 C1 103.16(15) . . ?
N2 C3 N2 113.2(3) . 22_655 ?
O1 C4 N2 125.7(2) . . ?
O1 C4 N1 125.6(2) . . ?
N2 C4 N1 108.73(19) . . ?
N1 C5 N1 113.9(3) . 24 ?
O2M N1M O1M 104.9(8) . . ?
O2M N1M O3M 136.2(12) . . ?
O1M N1M O3M 112.9(7) . . ?
O10W O1W O10W 66(3) 18 . ?
O10W O1W O15W 67(2) 18 24_455 ?
O10W O1W O15W 46(2) . 24_455 ?
O10W O1W O15W 67(2) 18 3_655 ?
O10W O1W O15W 46(2) . 3_655 ?
O15W O1W O15W 90(5) 24_455 3_655 ?
O10W O1W O15W 46(2) 18 7_455 ?
O10W O1W O15W 67(2) . 7_455 ?
O15W O1W O15W 32(5) 24_455 7_455 ?
O15W O1W O15W 98(5) 3_655 7_455 ?
O10W O1W O15W 46(2) 18 20_655 ?
O10W O1W O15W 67(2) . 20_655 ?
O15W O1W O15W 98(5) 24_455 20_655 ?
O15W O1W O15W 32(5) 3_655 20_655 ?
O15W O1W O15W 90(5) 7_455 20_655 ?
O3W O2W O33W 23(2) 19_566 19_566 ?
O3W O2W O3W 43(4) 19_566 4_565 ?
O33W O2W O3W 19.9(19) 19_566 4_565 ?
O33W O3W O3W 7(10) . 18_556 ?
O33W O3W O2W 81(3) . 7_556 ?
O3W O3W O2W 80(3) 18_556 7_556 ?
O33W O3W O2W 81(3) . 20_656 ?
O3W O3W O2W 80(3) 18_556 20_656 ?
O2W O3W O2W 156(6) 7_556 20_656 ?
O33W O3W O2W 58(3) . 24 ?
O3W O3W O2W 57.1(19) 18_556 24 ?
O2W O3W O2W 23(2) 7_556 24 ?
O2W O3W O2W 135(4) 20_656 24 ?
O33W O3W O2W 58(3) . 3_655 ?
O3W O3W O2W 57.1(19) 18_556 3_655 ?
O2W O3W O2W 135(4) 7_556 3_655 ?
O2W O3W O2W 23(2) 20_656 3_655 ?
O2W O3W O2W 113(4) 24 3_655 ?
O3W O33W O3W 167(10) . 18_556 ?
O3W O33W O2W 76(2) . 20_656 ?
O3W O33W O2W 102(3) 18_556 20_656 ?
O3W O33W O2W 76(2) . 7_556 ?
O3W O33W O2W 102(3) 18_556 7_556 ?
O2W O33W O2W 148(3) 20_656 7_556 ?
O3W O33W O2W 102(3) . 24 ?
O3W O33W O2W 76(2) 18_556 24 ?
O2W O33W O2W 162(5) 20_656 24 ?
O2W O33W O2W 26(2) 7_556 24 ?
O3W O33W O2W 102(3) . 3_655 ?
O3W O33W O2W 76(2) 18_556 3_655 ?
O2W O33W O2W 26(2) 20_656 3_655 ?
O2W O33W O2W 162(5) 7_556 3_655 ?
O2W O33W O2W 148(3) 24 3_655 ?
O5W O4W O14W 161(4) . . ?
O4W O5W O37W 140(7) . 18 ?
O4W O5W O37W 140(7) . . ?
O37W O5W O37W 24(3) 18 . ?
O4W O5W O8W 114(4) . 10_554 ?
O37W O5W O8W 91(6) 18 10_554 ?
O37W O5W O8W 70(4) . 10_554 ?
O4W O5W O8W 114(4) . 25 ?
O37W O5W O8W 70(4) 18 25 ?
O37W O5W O8W 91(6) . 25 ?
O8W O5W O8W 121(7) 10_554 25 ?
O4W O5W O81W 154(4) . 10_554 ?
O37W O5W O81W 39(3) 18 10_554 ?
O37W O5W O81W 23(2) . 10_554 ?
O8W O5W O81W 53(3) 10_554 10_554 ?
O8W O5W O81W 90(5) 25 10_554 ?
O4W O5W O81W 154(4) . 25 ?
O37W O5W O81W 23(2) 18 25 ?
O37W O5W O81W 39(3) . 25 ?
O8W O5W O81W 90(5) 10_554 25 ?
O8W O5W O81W 53(3) 25 25 ?
O81W O5W O81W 41(3) 10_554 25 ?
O4W O5W O7W 93(5) . 18 ?
O37W O5W O7W 53(3) 18 18 ?
O37W O5W O7W 49(3) . 18 ?
O8W O5W O7W 98(4) 10_554 18 ?
O8W O5W O7W 111(5) 25 18 ?
O81W O5W O7W 70(3) 10_554 18 ?
O81W O5W O7W 75(3) 25 18 ?
O4W O5W O7W 93(5) . . ?
O37W O5W O7W 49(3) 18 . ?
O37W O5W O7W 53(3) . . ?
O8W O5W O7W 111(5) 10_554 . ?
O8W O5W O7W 98(4) 25 . ?
O81W O5W O7W 75(3) 10_554 . ?
O81W O5W O7W 70(3) 25 . ?
O7W O5W O7W 15(2) 18 . ?
O6W O66W O92W 134(3) . 31 ?
O6W O66W O12W 141(3) . 27_455 ?
O92W O66W O12W 30(8) 31 27_455 ?
O6W O66W O12W 141(4) . 31 ?
O92W O66W O12W 33(8) 31 31 ?
O12W O66W O12W 3(10) 27_455 31 ?
O6W O66W O92W 134(4) . 27_455 ?
O92W O66W O92W 56(4) 31 27_455 ?
O12W O66W O92W 27(8) 27_455 27_455 ?
O12W O66W O92W 23(8) 31 27_455 ?
O37W O7W O5W 42(3) . . ?
O5W O37W O7W 86(4) . . ?
O5W O8W O81W 82(4) 25 . ?
O8W O81W O5W 45.4(19) . 25 ?
O1W O10W O15W 86(4) . 3_655 ?
O1W O10W O15W 86(4) . 24_455 ?
O15W O10W O15W 159(8) 3_655 24_455 ?
O1W O10W O10W 57.2(16) . 18 ?
O15W O10W O10W 80(4) 3_655 18 ?
O15W O10W O10W 80(4) 24_455 18 ?
O1W O10W O15W 69(3) . 20_655 ?
O15W O10W O15W 34(5) 3_655 20_655 ?
O15W O10W O15W 125(4) 24_455 20_655 ?
O10W O10W O15W 46(3) 18 20_655 ?
O1W O10W O15W 69(3) . 7_455 ?
O15W O10W O15W 125(4) 3_655 7_455 ?
O15W O10W O15W 34(5) 24_455 7_455 ?
O10W O10W O15W 46(3) 18 7_455 ?
O15W O10W O15W 91(5) 20_655 7_455 ?
O92W O12W O92W 172(10) 21_565 . ?
O92W O12W O12W 176(5) 21_565 21_565 ?
O92W O12W O12W 4(5) . 21_565 ?
O92W O12W O66W 71(9) 21_565 11_554 ?
O92W O12W O66W 101(8) . 11_554 ?
O12W O12W O66W 105(8) 21_565 11_554 ?
O92W O12W O66W 71(9) 21_565 28 ?
O92W O12W O66W 101(8) . 28 ?
O12W O12W O66W 105(8) 21_565 28 ?
O66W O12W O66W 32(2) 11_554 28 ?
O92W O12W O66W 104(9) 21_565 31_554 ?
O92W O12W O66W 68(8) . 31_554 ?
O12W O12W O66W 72(8) 21_565 31_554 ?
O66W O12W O66W 33(3) 11_554 31_554 ?
O66W O12W O66W 47(2) 28 31_554 ?
O92W O12W O66W 104(9) 21_565 16 ?
O92W O12W O66W 68(8) . 16 ?
O12W O12W O66W 72(8) 21_565 16 ?
O66W O12W O66W 47(2) 11_554 16 ?
O66W O12W O66W 33(3) 28 16 ?
O66W O12W O66W 32(2) 31_554 16 ?
O12W O92W O92W 4(5) 21_565 21_565 ?
O12W O92W O12W 0(2) 21_565 . ?
O92W O92W O12W 4(5) 21_565 . ?
O12W O92W O66W 79(5) 21_565 31_554 ?
O92W O92W O66W 75(2) 21_565 31_554 ?
O12W O92W O66W 79(5) . 31_554 ?
O12W O92W O66W 79(5) 21_565 16 ?
O92W O92W O66W 75(2) 21_565 16 ?
O12W O92W O66W 79(5) . 16 ?
O66W O92W O66W 34(2) 31_554 16 ?
O12W O92W O66W 52(5) 21_565 11_554 ?
O92W O92W O66W 48.3(17) 21_565 11_554 ?
O12W O92W O66W 52(4) . 11_554 ?
O66W O92W O66W 27(2) 31_554 11_554 ?
O66W O92W O66W 40(2) 16 11_554 ?
O12W O92W O66W 52(5) 21_565 28 ?
O92W O92W O66W 48.3(17) 21_565 28 ?
O12W O92W O66W 52(4) . 28 ?
O66W O92W O66W 40(2) 31_554 28 ?
O66W O92W O66W 27(2) 16 28 ?
O66W O92W O66W 25.8(16) 11_554 28 ?
O10W O15W O10W 55(4) 4_565 19_565 ?
O10W O15W O1W 49(3) 4_565 19_565 ?
O10W O15W O1W 45(2) 19_565 19_565 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
O1 C4 1.232(3) . ?
N1 C4 1.362(3) . ?
N1 C5 1.442(3) . ?
N1 C1 1.443(2) . ?
N2 C4 1.353(3) . ?
N2 C2 1.441(2) . ?
N2 C3 1.449(3) . ?
C1 N1 1.443(2) 18_556 ?
C1 C2 1.550(4) . ?
C2 N2 1.441(2) 18_556 ?
C3 N2 1.449(3) 22_655 ?
C5 N1 1.442(3) 24 ?
O1M N1M 1.250(11) . ?
O2M N1M 1.245(9) . ?
O3M N1M 1.280(11) . ?
O1W O10W 0.97(2) 18 ?
O1W O10W 0.97(2) . ?
O1W O15W 1.29(6) 24_455 ?
O1W O15W 1.29(6) 3_655 ?
O1W O15W 1.29(6) 7_455 ?
O1W O15W 1.29(6) 20_655 ?
O2W O3W 1.36(2) 19_566 ?
O2W O33W 1.39(2) 19_566 ?
O2W O3W 1.60(4) 4_565 ?
O3W O33W 0.56(6) . ?
O3W O3W 1.10(12) 18_556 ?
O3W O2W 1.36(2) 7_556 ?
O3W O2W 1.36(2) 20_656 ?
O3W O2W 1.60(4) 24 ?
O3W O2W 1.60(4) 3_655 ?
O33W O3W 0.56(6) 18_556 ?
O33W O2W 1.39(2) 20_656 ?
O33W O2W 1.39(2) 7_556 ?
O33W O2W 1.39(2) 24 ?
O33W O2W 1.39(2) 3_655 ?
O4W O5W 1.07(8) . ?
O4W O14W 1.242(19) . ?
O5W O37W 1.09(7) 18 ?
O5W O37W 1.09(7) . ?
O5W O8W 1.16(4) 10_554 ?
O5W O8W 1.16(4) 25 ?
O5W O81W 1.62(8) 10_554 ?
O5W O81W 1.62(8) 25 ?
O5W O7W 1.63(7) 18 ?
O5W O7W 1.63(7) . ?
O6W O66W 0.75(3) . ?
O66W O92W 1.39(6) 31 ?
O66W O12W 1.44(7) 27_455 ?
O66W O12W 1.47(8) 31 ?
O66W O92W 1.79(6) 27_455 ?
O7W O37W 1.30(2) . ?
O8W O5W 1.16(4) 25 ?
O8W O81W 1.30(4) . ?
O81W O5W 1.62(8) 25 ?
O10W O15W 0.93(6) 3_655 ?
O10W O15W 0.93(6) 24_455 ?
O10W O10W 1.05(6) 18 ?
O10W O15W 1.27(6) 20_655 ?
O10W O15W 1.27(6) 7_455 ?
O12W O92W 0.7(2) 21_565 ?
O12W O92W 0.8(2) . ?
O12W O12W 0.1(4) 21_565 ?
O12W O66W 1.44(7) 11_554 ?
O12W O66W 1.44(7) 28 ?
O12W O66W 1.47(8) 31_554 ?
O12W O66W 1.47(8) 16 ?
O92W O12W 0.7(2) 21_565 ?
O92W O92W 1.55(10) 21_565 ?
O92W O66W 1.39(6) 31_554 ?
O92W O66W 1.39(6) 16 ?
O92W O66W 1.79(6) 11_554 ?
O92W O66W 1.79(6) 28 ?
O13W O16W 1.49(2) 3_655 ?
O15W O10W 0.93(6) 4_565 ?
O15W O10W 1.27(6) 19_565 ?
O15W O1W 1.29(6) 19_565 ?
O16W O13W 1.49(2) 4_565 ?
