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#$Date: 2016-03-26 16:55:42 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180363 $
#$URL: svn://www.crystallography.net/cod/cif/7/20/32/7203240.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7203240
loop_
_publ_author_name
'Adeline Y. Robin'
'Jorge L. Sagué'
'Katharina M. Fromm'
_publ_section_title
;
 Part 1. Solubility effect on the formation of coordination polymer
 networks between AgNO<small>₃</small> and
 <strong>L</strong>                (<strong>L</strong>                = ethanediyl
 bis(isonicotinate) as a function of solvent
;
_journal_issue                   5
_journal_name_full               CrystEngComm
_journal_page_first              403
_journal_paper_doi               10.1039/b517191a
_journal_volume                  8
_journal_year                    2006
_chemical_formula_moiety         '[Ag(C14H12N2O4)NO3]'
_chemical_formula_sum            'C14 H12 Ag N3 O7'
_chemical_formula_weight         442.14
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                93.15(2)
_cell_angle_beta                 99.898(16)
_cell_angle_gamma                91.43(2)
_cell_formula_units_Z            2
_cell_length_a                   6.1591(13)
_cell_length_b                   8.895(3)
_cell_length_c                   14.439(3)
_cell_measurement_temperature    293(2)
_cell_volume                     777.6(4)
_computing_cell_refinement       Xred
_computing_data_collection       Stoe
_computing_data_reduction        Xred
_computing_molecular_graphics    Schakal
_computing_publication_material  Word
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.439
_diffrn_measured_fraction_theta_max 0.439
_diffrn_measurement_device_type  'Stoe IPDS'
_diffrn_measurement_method       'Omega scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0213
_diffrn_reflns_av_sigmaI/netI    0.0216
_diffrn_reflns_limit_h_max       7
_diffrn_reflns_limit_h_min       -7
_diffrn_reflns_limit_k_max       1
_diffrn_reflns_limit_k_min       -8
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            1565
_diffrn_reflns_theta_full        27.01
_diffrn_reflns_theta_max         27.01
_diffrn_reflns_theta_min         2.87
_exptl_absorpt_coefficient_mu    1.341
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.888
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             440
_refine_diff_density_max         0.189
_refine_diff_density_min         -0.216
_refine_diff_density_rms         0.040
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.070
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     226
_refine_ls_number_reflns         1494
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.070
_refine_ls_R_factor_all          0.0408
_refine_ls_R_factor_gt           0.0312
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0334P)²+0.7275P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0686
_refine_ls_wR_factor_ref         0.0732
_reflns_number_gt                1291
_reflns_number_total             1494
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b517191a.txt
_cod_data_source_block           '[AgLNO3]'
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7203240
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.37808(6) 0.85718(7) 0.88967(3) 0.04882(19) Uani 1 1 d . . .
N1 N 0.4261(6) 0.7603(7) 1.0271(3) 0.0433(18) Uani 1 1 d . . .
C1 C 0.2640(7) 0.7678(9) 1.0784(4) 0.044(2) Uani 1 1 d . . .
H1 H 0.1390 0.8207 1.0565 0.053 Uiso 1 1 calc R . .
C2 C 0.2768(7) 0.6994(9) 1.1629(4) 0.0441(19) Uani 1 1 d . . .
H2 H 0.1599 0.7038 1.1959 0.053 Uiso 1 1 calc R . .
C3 C 0.6036(7) 0.6821(9) 1.0603(4) 0.047(2) Uani 1 1 d . . .
H3 H 0.7158 0.6755 1.0247 0.056 Uiso 1 1 calc R . .
C4 C 0.6300(7) 0.6112(8) 1.1433(4) 0.0392(19) Uani 1 1 d . . .
H4 H 0.7542 0.5560 1.1627 0.047 Uiso 1 1 calc R . .
C5 C 0.4635(6) 0.6248(8) 1.1977(3) 0.0354(17) Uani 1 1 d . . .
C6 C 0.4813(7) 0.5602(8) 1.2918(3) 0.0338(17) Uani 1 1 d . . .
O1 O 0.3504(5) 0.5801(6) 1.3440(2) 0.0483(16) Uani 1 1 d . . .
O2 O 0.6664(5) 0.4857(6) 1.3125(2) 0.0388(13) Uani 1 1 d . . .
C7 C 0.6991(7) 0.4117(8) 1.3993(3) 0.0370(16) Uani 1 1 d . . .
H7A H 0.5849 0.3346 1.3993 0.044 Uiso 1 1 calc R . .
H7B H 0.7001 0.4832 1.4526 0.044 Uiso 1 1 calc R . .
C8 C 0.9208(7) 0.3434(8) 1.4021(3) 0.0393(18) Uani 1 1 d . . .
H8A H 0.9164 0.2691 1.3500 0.047 Uiso 1 1 calc R . .
H8B H 1.0321 0.4206 1.3979 0.047 Uiso 1 1 calc R . .
O3 O 0.9710(5) 0.2733(6) 1.4909(2) 0.0392(13) Uani 1 1 d . . .
C9 C 1.1566(7) 0.1982(8) 1.5032(3) 0.0351(17) Uani 1 1 d . . .
O4 O 1.2742(6) 0.1850(7) 1.4446(3) 0.0549(18) Uani 1 1 d . . .
C10 C 0.2027(7) 1.1288(8) 0.5949(3) 0.0316(15) Uani 1 1 d . . .
C11 C 0.0568(7) 1.1285(8) 0.6592(3) 0.0407(19) Uani 1 1 d . . .
H11 H -0.0772 1.1756 0.6461 0.049 Uiso 1 1 calc R . .
C12 C 0.1128(7) 1.0589(9) 0.7408(4) 0.0406(18) Uani 1 1 d . . .
H12 H 0.0142 1.0606 0.7830 0.049 Uiso 1 1 calc R . .
C13 C 0.4018(7) 1.0595(8) 0.6197(3) 0.0408(18) Uani 1 1 d . . .
H13 H 0.5054 1.0600 0.5799 0.049 Uiso 1 1 calc R . .
C14 C 0.4455(7) 0.9904(8) 0.7031(3) 0.0379(18) Uani 1 1 d . . .
H14 H 0.5793 0.9436 0.7181 0.045 Uiso 1 1 calc R . .
N2 N 0.3037(6) 0.9872(7) 0.7644(3) 0.0389(16) Uani 1 1 d . . .
N3 N 0.8575(6) 0.7523(8) 0.8492(3) 0.0396(17) Uani 1 1 d . . .
O5 O 0.6661(6) 0.7028(8) 0.8165(3) 0.063(2) Uani 1 1 d . . .
O6 O 1.0157(6) 0.6753(10) 0.8340(4) 0.077(3) Uani 1 1 d . . .
O7 O 0.8869(6) 0.8723(10) 0.8943(3) 0.065(2) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1 Ag1 N2 169.8(2) . . ?
N1 Ag1 O5 98.02(18) . . ?
N2 Ag1 O5 91.59(17) . . ?
N1 Ag1 O6 89.6(2) . 1_455 ?
N2 Ag1 O6 92.1(2) . 1_455 ?
O5 Ag1 O6 99.91(17) . 1_455 ?
N1 Ag1 O7 90.63(15) . . ?
N2 Ag1 O7 94.21(15) . . ?
O5 Ag1 O7 42.67(19) . . ?
O6 Ag1 O7 142.13(17) 1_455 . ?
N1 Ag1 Ag1 64.40(18) . 2_677 ?
N2 Ag1 Ag1 108.30(17) . 2_677 ?
O5 Ag1 Ag1 115.91(12) . 2_677 ?
O6 Ag1 Ag1 137.42(10) 1_455 2_677 ?
O7 Ag1 Ag1 74.79(12) . 2_677 ?
N1 Ag1 Ag1 90.63(10) . 1_655 ?
N2 Ag1 Ag1 94.62(9) . 1_655 ?
O5 Ag1 Ag1 40.04(13) . 1_655 ?
O6 Ag1 Ag1 139.45(12) 1_455 1_655 ?
O7 Ag1 Ag1 2.68(14) . 1_655 ?
Ag1 Ag1 Ag1 77.19(2) 2_677 1_655 ?
N1 Ag1 Ag1 164.53(11) . 1_464 ?
N2 Ag1 Ag1 8.19(9) . 1_464 ?
O5 Ag1 Ag1 97.24(12) . 1_464 ?
O6 Ag1 Ag1 85.29(14) 1_455 1_464 ?
O7 Ag1 Ag1 102.38(12) . 1_464 ?
Ag1 Ag1 Ag1 110.67(3) 2_677 1_464 ?
Ag1 Ag1 Ag1 102.755(17) 1_655 1_464 ?
C1 N1 C3 117.5(4) . . ?
C1 N1 Ag1 119.1(3) . . ?
C3 N1 Ag1 123.1(3) . . ?
N1 C1 C2 122.1(4) . . ?
N1 C1 H1 118.9 . . ?
C2 C1 H1 118.9 . . ?
C5 C2 C1 119.6(4) . . ?
C5 C2 H2 120.2 . . ?
C1 C2 H2 120.2 . . ?
N1 C3 C4 124.1(3) . . ?
N1 C3 H3 117.9 . . ?
C4 C3 H3 117.9 . . ?
C3 C4 C5 117.7(4) . . ?
C3 C4 H4 121.2 . . ?
C5 C4 H4 121.2 . . ?
C2 C5 C4 118.8(4) . . ?
C2 C5 C6 119.0(3) . . ?
C4 C5 C6 122.2(4) . . ?
O1 C6 O2 124.7(4) . . ?
O1 C6 C5 124.1(4) . . ?
O2 C6 C5 111.1(3) . . ?
C6 O2 C7 116.9(3) . . ?
O2 C7 C8 103.4(3) . . ?
O2 C7 H7A 111.1 . . ?
C8 C7 H7A 111.1 . . ?
O2 C7 H7B 111.1 . . ?
C8 C7 H7B 111.1 . . ?
H7A C7 H7B 109.0 . . ?
O3 C8 C7 106.6(3) . . ?
O3 C8 H8A 110.4 . . ?
C7 C8 H8A 110.4 . . ?
O3 C8 H8B 110.4 . . ?
C7 C8 H8B 110.4 . . ?
H8A C8 H8B 108.6 . . ?
C9 O3 C8 115.0(3) . . ?
O4 C9 O3 123.5(5) . . ?
O4 C9 C10 123.1(4) . 1_646 ?
O3 C9 C10 113.4(3) . 1_646 ?
C13 C10 C11 117.3(4) . . ?
C13 C10 C9 118.8(3) . 1_464 ?
C11 C10 C9 123.9(4) . 1_464 ?
C12 C11 C10 119.3(4) . . ?
C12 C11 H11 120.3 . . ?
C10 C11 H11 120.3 . . ?
N2 C12 C11 123.7(3) . . ?
N2 C12 H12 118.1 . . ?
C11 C12 H12 118.1 . . ?
C14 C13 C10 119.8(3) . . ?
C14 C13 H13 120.1 . . ?
C10 C13 H13 120.1 . . ?
N2 C14 C13 123.0(4) . . ?
N2 C14 H14 118.5 . . ?
C13 C14 H14 118.5 . . ?
C14 N2 C12 116.6(4) . . ?
C14 N2 Ag1 119.9(3) . . ?
C12 N2 Ag1 123.3(3) . . ?
O7 N3 O6 121.2(5) . . ?
O7 N3 O5 120.4(5) . . ?
O6 N3 O5 118.4(7) . . ?
N3 O5 Ag1 110.5(5) . . ?
N3 O6 Ag1 105.3(5) . 1_655 ?
N3 O7 Ag1 89.3(3) . 1_655 ?
N3 O7 Ag1 85.3(3) . . ?
Ag1 O7 Ag1 174.6(3) 1_655 . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 N1 2.183(4) . ?
Ag1 N2 2.189(4) . ?
Ag1 O5 2.599(5) . ?
Ag1 O6 2.703(7) 1_455 ?
Ag1 O7 3.122(4) . ?
Ag1 Ag1 4.0170(17) 2_677 ?
Ag1 Ag1 6.1591(13) 1_655 ?
Ag1 Ag1 17.659(4) 1_464 ?
N1 C1 1.342(5) . ?
N1 C3 1.343(7) . ?
C1 C2 1.384(7) . ?
C1 H1 0.9300 . ?
C2 C5 1.375(6) . ?
C2 H2 0.9300 . ?
C3 C4 1.372(7) . ?
C3 H3 0.9300 . ?
C4 C5 1.398(5) . ?
C4 H4 0.9300 . ?
C5 C6 1.493(6) . ?
C6 O1 1.204(5) . ?
C6 O2 1.331(5) . ?
O2 C7 1.434(5) . ?
C7 C8 1.503(6) . ?
C7 H7A 0.9700 . ?
C7 H7B 0.9700 . ?
C8 O3 1.445(5) . ?
C8 H8A 0.9700 . ?
C8 H8B 0.9700 . ?
O3 C9 1.329(6) . ?
C9 O4 1.208(5) . ?
C9 C10 1.479(7) 1_646 ?
C10 C13 1.386(6) . ?
C10 C11 1.398(5) . ?
C10 C9 1.479(7) 1_464 ?
C11 C12 1.358(7) . ?
C11 H11 0.9300 . ?
C12 N2 1.352(6) . ?
C12 H12 0.9300 . ?
C13 C14 1.370(7) . ?
C13 H13 0.9300 . ?
C14 N2 1.347(5) . ?
C14 H14 0.9300 . ?
N3 O7 1.213(10) . ?
N3 O6 1.248(7) . ?
N3 O5 1.251(7) . ?
O6 Ag1 2.703(7) 1_655 ?
O7 Ag1 3.044(4) 1_655 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
C11 H11 O1 0.93 2.79 3.648(7) 153.2 2_577
C8 H8B O1 0.97 2.64 3.580(7) 163.4 1_655
C13 H13 O4 0.93 2.63 3.195(7) 119.3 2_767
C14 H14 O4 0.93 2.85 3.316(6) 112.3 2_767
C7 H7A O4 0.97 2.50 3.436(7) 161.9 1_455
C1 H1 O7 0.93 2.65 3.403(7) 138.9 1_455
C12 H12 O7 0.93 2.58 3.309(8) 135.3 1_455
C1 H1 O7 0.93 2.80 3.377(11) 121.3 2_677
C4 H4 O6 0.93 2.53 3.390(8) 154.7 2_767
C8 H8A O6 0.97 2.83 3.494(7) 126.5 2_767
C14 H14 O5 0.93 2.65 3.308(9) 128.3 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
N2 Ag1 N1 C1 41.6(14) . . . . ?
O5 Ag1 N1 C1 -157.7(6) . . . . ?
O6 Ag1 N1 C1 -57.8(6) 1_455 . . . ?
O7 Ag1 N1 C1 160.1(6) . . . . ?
Ag1 Ag1 N1 C1 87.3(6) 2_677 . . . ?
Ag1 Ag1 N1 C1 162.8(6) 1_655 . . . ?
Ag1 Ag1 N1 C1 12.6(11) 1_464 . . . ?
N2 Ag1 N1 C3 -143.9(9) . . . . ?
O5 Ag1 N1 C3 16.7(6) . . . . ?
O6 Ag1 N1 C3 116.6(6) 1_455 . . . ?
O7 Ag1 N1 C3 -25.5(6) . . . . ?
Ag1 Ag1 N1 C3 -98.3(6) 2_677 . . . ?
Ag1 Ag1 N1 C3 -22.8(6) 1_655 . . . ?
Ag1 Ag1 N1 C3 -173.0(5) 1_464 . . . ?
C3 N1 C1 C2 0.5(11) . . . . ?
Ag1 N1 C1 C2 175.3(6) . . . . ?
N1 C1 C2 C5 2.1(12) . . . . ?
C1 N1 C3 C4 -0.7(11) . . . . ?
Ag1 N1 C3 C4 -175.2(6) . . . . ?
N1 C3 C4 C5 -1.7(11) . . . . ?
C1 C2 C5 C4 -4.4(11) . . . . ?
C1 C2 C5 C6 176.0(7) . . . . ?
C3 C4 C5 C2 4.2(11) . . . . ?
C3 C4 C5 C6 -176.3(6) . . . . ?
C2 C5 C6 O1 -6.8(11) . . . . ?
C4 C5 C6 O1 173.6(7) . . . . ?
C2 C5 C6 O2 176.8(6) . . . . ?
C4 C5 C6 O2 -2.7(10) . . . . ?
O1 C6 O2 C7 6.5(10) . . . . ?
C5 C6 O2 C7 -177.1(6) . . . . ?
C6 O2 C7 C8 -178.6(5) . . . . ?
O2 C7 C8 O3 176.9(5) . . . . ?
C7 C8 O3 C9 175.9(5) . . . . ?
C8 O3 C9 O4 -1.8(9) . . . . ?
C8 O3 C9 C10 179.7(6) . . . 1_646 ?
C13 C10 C11 C12 -1.4(11) . . . . ?
C9 C10 C11 C12 178.6(7) 1_464 . . . ?
C10 C11 C12 N2 -0.5(11) . . . . ?
C11 C10 C13 C14 2.0(10) . . . . ?
C9 C10 C13 C14 -178.0(7) 1_464 . . . ?
C10 C13 C14 N2 -0.7(11) . . . . ?
C13 C14 N2 C12 -1.2(11) . . . . ?
C13 C14 N2 Ag1 174.8(5) . . . . ?
C11 C12 N2 C14 1.8(11) . . . . ?
C11 C12 N2 Ag1 -174.0(6) . . . . ?
N1 Ag1 N2 C14 142.8(9) . . . . ?
O5 Ag1 N2 C14 -18.0(6) . . . . ?
O6 Ag1 N2 C14 -118.0(6) 1_455 . . . ?
O7 Ag1 N2 C14 24.7(6) . . . . ?
Ag1 Ag1 N2 C14 100.0(6) 2_677 . . . ?
Ag1 Ag1 N2 C14 22.0(6) 1_655 . . . ?
Ag1 Ag1 N2 C14 -151.8(16) 1_464 . . . ?
N1 Ag1 N2 C12 -41.5(13) . . . . ?
O5 Ag1 N2 C12 157.7(5) . . . . ?
O6 Ag1 N2 C12 57.7(5) 1_455 . . . ?
O7 Ag1 N2 C12 -159.7(5) . . . . ?
Ag1 Ag1 N2 C12 -84.3(5) 2_677 . . . ?
Ag1 Ag1 N2 C12 -162.3(5) 1_655 . . . ?
Ag1 Ag1 N2 C12 23.9(8) 1_464 . . . ?
O7 N3 O5 Ag1 -12.4(8) . . . . ?
O6 N3 O5 Ag1 167.7(4) . . . . ?
N1 Ag1 O5 N3 -76.1(5) . . . . ?
N2 Ag1 O5 N3 100.6(4) . . . . ?
O6 Ag1 O5 N3 -167.0(4) 1_455 . . . ?
O7 Ag1 O5 N3 6.1(4) . . . . ?
Ag1 Ag1 O5 N3 -10.7(5) 2_677 . . . ?
Ag1 Ag1 O5 N3 5.3(3) 1_655 . . . ?
Ag1 Ag1 O5 N3 106.5(4) 1_464 . . . ?
O7 N3 O6 Ag1 -10.6(7) . . . 1_655 ?
O5 N3 O6 Ag1 169.3(4) . . . 1_655 ?
O6 N3 O7 Ag1 9.0(6) . . . 1_655 ?
O5 N3 O7 Ag1 -170.8(5) . . . 1_655 ?
O6 N3 O7 Ag1 -170.5(5) . . . . ?
O5 N3 O7 Ag1 9.6(6) . . . . ?
N1 Ag1 O7 N3 95.3(4) . . . . ?
N2 Ag1 O7 N3 -93.7(5) . . . . ?
O5 Ag1 O7 N3 -5.9(4) . . . . ?
O6 Ag1 O7 N3 5.2(6) 1_455 . . . ?
Ag1 Ag1 O7 N3 158.5(4) 2_677 . . . ?
Ag1 Ag1 O7 N3 5(2) 1_655 . . . ?
Ag1 Ag1 O7 N3 -93.1(4) 1_464 . . . ?
N1 Ag1 O7 Ag1 90(2) . . . 1_655 ?
N2 Ag1 O7 Ag1 -99(2) . . . 1_655 ?
O5 Ag1 O7 Ag1 -11(2) . . . 1_655 ?
O6 Ag1 O7 Ag1 0(2) 1_455 . . 1_655 ?
Ag1 Ag1 O7 Ag1 153(2) 2_677 . . 1_655 ?
Ag1 Ag1 O7 Ag1 -98(2) 1_464 . . 1_655 ?
