#------------------------------------------------------------------------------
#$Date: 2016-03-26 17:20:13 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180388 $
#$URL: svn://www.crystallography.net/cod/cif/7/20/57/7205704.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7205704
loop_
_publ_author_name
'Zhang, Jun'
'Xue, Yun-Shan'
'Li, Yi-Zhi'
'Du, Hong-Bin'
'You, Xiao-Zeng'
_publ_section_title
;
 Cuprous iodide coordination polymers (CuI)x(L)y·z(solvent)
 built on linear thioether linkers
;
_journal_issue                   7
_journal_name_full               CrystEngComm
_journal_page_first              2578
_journal_paper_doi               10.1039/c0ce00685h
_journal_volume                  13
_journal_year                    2011
_chemical_formula_moiety         'C60 H84 Cu12 I12 S12'
_chemical_formula_sum            'C60 H84 Cu12 I12 S12'
_chemical_formula_weight         3475.27
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                107.4560(10)
_cell_angle_beta                 90.016(2)
_cell_angle_gamma                95.2510(10)
_cell_formula_units_Z            2
_cell_length_a                   11.1804(9)
_cell_length_b                   17.3956(14)
_cell_length_c                   25.706(2)
_cell_measurement_reflns_used    4585
_cell_measurement_temperature    291(2)
_cell_measurement_theta_max      23.507
_cell_measurement_theta_min      2.312
_cell_volume                     4747.3(7)
_computing_cell_refinement       SMART
_computing_data_collection       'SMART (Bruker, 2000)'
_computing_data_reduction        'SAINT (Bruker, 2000)'
_computing_molecular_graphics    SHELXTL
_computing_publication_material  SHELXTL
_computing_structure_refinement  SHELXTL
_computing_structure_solution    'SHELXTL (Bruker, 2000)'
_diffrn_ambient_temperature      291(2)
_diffrn_measured_fraction_theta_full 0.981
_diffrn_measured_fraction_theta_max 0.981
_diffrn_measurement_device_type  'Bruker Smart Apex CCD'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0216
_diffrn_reflns_av_sigmaI/netI    0.0463
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       31
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            26254
_diffrn_reflns_theta_full        26.00
_diffrn_reflns_theta_max         26.00
_diffrn_reflns_theta_min         1.66
_exptl_absorpt_coefficient_mu    6.827
_exptl_absorpt_correction_T_max  0.3421
_exptl_absorpt_correction_T_min  0.3151
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS; Bruker, 2000'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.431
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             3240
_exptl_crystal_size_max          0.22
_exptl_crystal_size_mid          0.21
_exptl_crystal_size_min          0.20
_refine_diff_density_max         0.720
_refine_diff_density_min         -1.821
_refine_diff_density_rms         0.195
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.023
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           fullcycle
_refine_ls_number_parameters     877
_refine_ls_number_reflns         18334
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.023
_refine_ls_R_factor_all          0.0804
_refine_ls_R_factor_gt           0.0597
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0962P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1428
_refine_ls_wR_factor_ref         0.1489
_reflns_number_gt                13807
_reflns_number_total             18334
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c0ce00685h.txt
_cod_data_source_block           MSF-7
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1555 2011-01-17 13:19:09Z saulius 
;
_cod_original_cell_volume        4747.2(7)
_cod_original_sg_symbol_H-M      'P-1 '
_cod_database_code               7205704
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C -0.2509(9) 0.0817(8) 0.0699(4) 0.066(3) Uani 1 1 d . . .
H1A H -0.2572 0.0459 0.0332 0.100 Uiso 1 1 calc R . .
H1B H -0.2373 0.1367 0.0692 0.100 Uiso 1 1 calc R . .
H1C H -0.3241 0.0750 0.0882 0.100 Uiso 1 1 calc R . .
C2 C -0.1466(11) 0.0620(8) 0.1001(4) 0.065(3) Uani 1 1 d . . .
H2A H -0.1721 0.0576 0.1353 0.078 Uiso 1 1 calc R . .
H2B H -0.0813 0.1047 0.1062 0.078 Uiso 1 1 calc R . .
C3 C 0.0439(9) -0.0312(7) 0.0957(4) 0.050(2) Uani 1 1 d . . .
C4 C 0.1499(8) -0.0061(6) 0.0753(4) 0.046(2) Uani 1 1 d . . .
H4 H 0.1495 0.0084 0.0433 0.056 Uiso 1 1 calc R . .
C5 C 0.2568(8) -0.0031(5) 0.1035(4) 0.0397(18) Uani 1 1 d . . .
H5 H 0.3294 0.0121 0.0900 0.048 Uiso 1 1 calc R . .
C6 C 0.2549(8) -0.0232(5) 0.1526(3) 0.0400(18) Uani 1 1 d . . .
C7 C 0.1461(10) -0.0488(8) 0.1724(4) 0.060(3) Uani 1 1 d . . .
H7 H 0.1435 -0.0600 0.2055 0.072 Uiso 1 1 calc R . .
C8 C 0.0473(9) -0.0562(6) 0.1422(4) 0.051(2) Uani 1 1 d . . .
H8 H -0.0234 -0.0794 0.1526 0.061 Uiso 1 1 calc R . .
C9 C 0.5130(8) 0.0231(7) 0.1606(4) 0.051(2) Uani 1 1 d . . .
H9A H 0.5878 0.0110 0.1741 0.061 Uiso 1 1 calc R . .
H9B H 0.5094 -0.0014 0.1214 0.061 Uiso 1 1 calc R . .
C10 C 0.5161(12) 0.1111(8) 0.1722(5) 0.071(3) Uani 1 1 d . . .
H10A H 0.4779 0.1232 0.1425 0.107 Uiso 1 1 calc R . .
H10B H 0.5981 0.1345 0.1766 0.107 Uiso 1 1 calc R . .
H10C H 0.4744 0.1334 0.2052 0.107 Uiso 1 1 calc R . .
C11 C -0.0895(10) 0.0038(7) 0.2908(5) 0.066(3) Uani 1 1 d . . .
H11A H -0.0786 0.0615 0.2987 0.099 Uiso 1 1 calc R . .
H11B H -0.1644 -0.0167 0.2711 0.099 Uiso 1 1 calc R . .
H11C H -0.0248 -0.0199 0.2692 0.099 Uiso 1 1 calc R . .
C12 C -0.0908(9) -0.0183(8) 0.3450(5) 0.061(3) Uani 1 1 d . . .
H12A H -0.0590 -0.0701 0.3396 0.074 Uiso 1 1 calc R . .
H12B H -0.1723 -0.0220 0.3576 0.074 Uiso 1 1 calc R . .
C13 C 0.0127(12) -0.0540(7) 0.4518(4) 0.063(3) Uani 1 1 d . . .
H13 H 0.0221 -0.0921 0.4182 0.075 Uiso 1 1 calc R . .
C14 C -0.0016(9) 0.0265(6) 0.4536(4) 0.049(2) Uani 1 1 d . . .
C15 C -0.0134(7) 0.0773(6) 0.5032(4) 0.042(2) Uani 1 1 d . . .
H15 H -0.0224 0.1312 0.5067 0.051 Uiso 1 1 calc R . .
C16 C 0.3599(10) 0.3871(7) 0.4851(4) 0.056(3) Uani 1 1 d . . .
H16A H 0.3039 0.3448 0.4900 0.084 Uiso 1 1 calc R . .
H16B H 0.3264 0.4381 0.4983 0.084 Uiso 1 1 calc R . .
H16C H 0.4334 0.3892 0.5050 0.084 Uiso 1 1 calc R . .
C17 C 0.3855(8) 0.3699(7) 0.4240(4) 0.051(2) Uani 1 1 d . . .
H17A H 0.4079 0.4221 0.4185 0.061 Uiso 1 1 calc R . .
H17B H 0.3093 0.3494 0.4046 0.061 Uiso 1 1 calc R . .
C18 C 0.6228(9) 0.3323(6) 0.4340(4) 0.048(2) Uani 1 1 d . . .
C19 C 0.7050(11) 0.3934(6) 0.4275(5) 0.059(3) Uani 1 1 d . . .
H19 H 0.6896 0.4194 0.4018 0.071 Uiso 1 1 calc R . .
C20 C 0.8103(10) 0.4157(6) 0.4594(4) 0.059(3) Uani 1 1 d . . .
H20 H 0.8653 0.4566 0.4550 0.071 Uiso 1 1 calc R . .
C21 C 0.8333(8) 0.3768(4) 0.4978(4) 0.0391(19) Uani 1 1 d . . .
C22 C 0.7511(10) 0.3157(6) 0.5044(5) 0.058(3) Uani 1 1 d . . .
H22 H 0.7665 0.2897 0.5301 0.070 Uiso 1 1 calc R . .
C23 C 0.6459(10) 0.2934(7) 0.4725(5) 0.064(3) Uani 1 1 d . . .
H23 H 0.5909 0.2525 0.4768 0.076 Uiso 1 1 calc R . .
C24 C 1.0414(8) 0.3108(6) 0.5089(4) 0.045(2) Uani 1 1 d . . .
H24A H 1.1183 0.3161 0.5276 0.054 Uiso 1 1 calc R . .
H24B H 0.9905 0.2679 0.5170 0.054 Uiso 1 1 calc R . .
C25 C 1.0598(10) 0.2882(7) 0.4477(4) 0.059(3) Uani 1 1 d . . .
H25A H 0.9888 0.2574 0.4287 0.088 Uiso 1 1 calc R . .
H25B H 1.1269 0.2565 0.4387 0.088 Uiso 1 1 calc R . .
H25C H 1.0753 0.3366 0.4372 0.088 Uiso 1 1 calc R . .
C26 C 0.9418(9) 0.2624(6) 0.8060(4) 0.046(2) Uani 1 1 d . . .
H26A H 0.9655 0.3191 0.8220 0.070 Uiso 1 1 calc R . .
H26B H 0.9429 0.2355 0.8336 0.070 Uiso 1 1 calc R . .
H26C H 0.8622 0.2552 0.7902 0.070 Uiso 1 1 calc R . .
C27 C 1.0288(9) 0.2265(6) 0.7617(4) 0.047(2) Uani 1 1 d . . .
H27A H 0.9842 0.2028 0.7274 0.056 Uiso 1 1 calc R . .
H27B H 1.0651 0.1834 0.7708 0.056 Uiso 1 1 calc R . .
C28 C 1.2304(8) 0.2382(5) 0.7050(3) 0.0364(17) Uani 1 1 d . . .
C29 C 1.3338(9) 0.2069(5) 0.7208(3) 0.043(2) Uani 1 1 d . . .
H29 H 1.3566 0.2242 0.7576 0.052 Uiso 1 1 calc R . .
C30 C 1.3990(8) 0.1557(5) 0.6874(3) 0.0371(18) Uani 1 1 d . . .
H30 H 1.4599 0.1329 0.7005 0.045 Uiso 1 1 calc R . .
C31 C 1.3751(8) 0.1372(5) 0.6338(3) 0.0399(19) Uani 1 1 d . . .
C32 C 1.2817(8) 0.1610(6) 0.6113(4) 0.046(2) Uani 1 1 d . . .
H32 H 1.2654 0.1436 0.5739 0.055 Uiso 1 1 calc R . .
C33 C 1.2072(9) 0.2161(6) 0.6494(3) 0.048(2) Uani 1 1 d . . .
H33 H 1.1438 0.2364 0.6360 0.058 Uiso 1 1 calc R . .
C34 C 1.5841(7) 0.1500(5) 0.5741(4) 0.0402(19) Uani 1 1 d . . .
H34A H 1.5454 0.1902 0.5627 0.048 Uiso 1 1 calc R . .
H34B H 1.6274 0.1768 0.6084 0.048 Uiso 1 1 calc R . .
C35 C 1.6684(10) 0.1105(7) 0.5320(4) 0.058(3) Uani 1 1 d . . .
H35A H 1.7065 0.0710 0.5437 0.087 Uiso 1 1 calc R . .
H35B H 1.7284 0.1507 0.5270 0.087 Uiso 1 1 calc R . .
H35C H 1.6249 0.0845 0.4982 0.087 Uiso 1 1 calc R . .
C36 C 1.1002(9) 0.7666(6) 0.6953(4) 0.045(2) Uani 1 1 d . . .
H36A H 1.0309 0.7521 0.7136 0.068 Uiso 1 1 calc R . .
H36B H 1.0825 0.7510 0.6567 0.068 Uiso 1 1 calc R . .
H36C H 1.1207 0.8241 0.7086 0.068 Uiso 1 1 calc R . .
C37 C 1.2011(8) 0.7250(5) 0.7056(3) 0.0379(18) Uani 1 1 d . . .
H37A H 1.2714 0.7635 0.7176 0.045 Uiso 1 1 calc R . .
H37B H 1.2200 0.6845 0.6723 0.045 Uiso 1 1 calc R . .
C38 C 1.3030(8) 0.6673(6) 0.7839(4) 0.046(2) Uani 1 1 d . . .
C39 C 1.3144(8) 0.6783(6) 0.8410(3) 0.043(2) Uani 1 1 d . . .
H39 H 1.2484 0.6862 0.8634 0.052 Uiso 1 1 calc R . .
C40 C 1.4353(9) 0.6766(6) 0.8628(4) 0.054(2) Uani 1 1 d . . .
H40 H 1.4456 0.6841 0.9000 0.064 Uiso 1 1 calc R . .
C41 C 1.5280(8) 0.6650(6) 0.8323(4) 0.046(2) Uani 1 1 d . . .
C42 C 1.5218(10) 0.6498(6) 0.7733(4) 0.054(2) Uani 1 1 d . . .
H42 H 1.5881 0.6386 0.7514 0.065 Uiso 1 1 calc R . .
C43 C 1.4037(9) 0.6538(6) 0.7518(5) 0.058(3) Uani 1 1 d . . .
H43 H 1.3946 0.6471 0.7147 0.070 Uiso 1 1 calc R . .
C44 C 1.7934(10) 0.6928(8) 0.8283(5) 0.063(3) Uani 1 1 d . . .
H44A H 1.8680 0.6822 0.8429 0.076 Uiso 1 1 calc R . .
H44B H 1.7882 0.6634 0.7896 0.076 Uiso 1 1 calc R . .
C45 C 1.7964(11) 0.7818(7) 0.8352(5) 0.065(3) Uani 1 1 d . . .
H45A H 1.7192 0.7998 0.8464 0.097 Uiso 1 1 calc R . .
H45B H 1.8154 0.7916 0.8012 0.097 Uiso 1 1 calc R . .
H45C H 1.8563 0.8108 0.8625 0.097 Uiso 1 1 calc R . .
C46 C 0.5460(10) 0.4226(6) 0.6487(5) 0.056(3) Uani 1 1 d . . .
H46A H 0.5150 0.4741 0.6638 0.084 Uiso 1 1 calc R . .
H46B H 0.4951 0.3901 0.6186 0.084 Uiso 1 1 calc R . .
H46C H 0.6258 0.4306 0.6363 0.084 Uiso 1 1 calc R . .
C47 C 0.5491(9) 0.3810(7) 0.6912(5) 0.055(2) Uani 1 1 d . . .
H47A H 0.5807 0.3290 0.6760 0.066 Uiso 1 1 calc R . .
H47B H 0.4682 0.3713 0.7029 0.066 Uiso 1 1 calc R . .
C48 C 0.6414(8) 0.3803(5) 0.7939(4) 0.0424(19) Uani 1 1 d . . .
C49 C 0.6220(9) 0.2963(6) 0.7748(4) 0.046(2) Uani 1 1 d . . .
H49 H 0.6072 0.2704 0.7378 0.055 Uiso 1 1 calc R . .
C50 C 0.6248(8) 0.2511(6) 0.8111(4) 0.047(2) Uani 1 1 d . . .
H50 H 0.6118 0.1950 0.7984 0.057 Uiso 1 1 calc R . .
C51 C 0.6469(9) 0.2899(5) 0.8664(4) 0.044(2) Uani 1 1 d . . .
C52 C 0.6662(9) 0.3738(6) 0.8855(4) 0.049(2) Uani 1 1 d . . .
H52 H 0.6810 0.3998 0.9225 0.059 Uiso 1 1 calc R . .
C53 C 0.6635(10) 0.4190(6) 0.8492(4) 0.051(2) Uani 1 1 d . . .
H53 H 0.6765 0.4752 0.8620 0.061 Uiso 1 1 calc R . .
C54 C 0.7524(9) 0.2806(5) 0.9643(4) 0.047(2) Uani 1 1 d . . .
H54A H 0.8297 0.2852 0.9478 0.056 Uiso 1 1 calc R . .
H54B H 0.7312 0.3349 0.9823 0.056 Uiso 1 1 calc R . .
C55 C 0.7627(10) 0.2372(7) 1.0056(4) 0.055(3) Uani 1 1 d . . .
H55A H 0.7027 0.2526 1.0324 0.083 Uiso 1 1 calc R . .
H55B H 0.8411 0.2511 1.0230 0.083 Uiso 1 1 calc R . .
H55C H 0.7512 0.1799 0.9880 0.083 Uiso 1 1 calc R . .
C56 C 0.3584(11) 0.4446(9) 0.8579(5) 0.077(4) Uani 1 1 d . . .
H56A H 0.3365 0.3873 0.8436 0.116 Uiso 1 1 calc R . .
H56B H 0.4415 0.4542 0.8695 0.116 Uiso 1 1 calc R . .
H56C H 0.3460 0.4697 0.8300 0.116 Uiso 1 1 calc R . .
C57 C 0.2810(11) 0.4802(6) 0.9062(5) 0.060(3) Uani 1 1 d . . .
H57A H 0.2441 0.5260 0.9013 0.071 Uiso 1 1 calc R . .
H57B H 0.3298 0.4986 0.9396 0.071 Uiso 1 1 calc R . .
C58 C 0.1195(11) 0.4899(7) 1.0115(5) 0.065(3) Uani 1 1 d . . .
H58 H 0.1991 0.4853 1.0197 0.078 Uiso 1 1 calc R . .
C59 C 0.0724(9) 0.4562(6) 0.9613(4) 0.048(2) Uani 1 1 d . . .
C60 C -0.0422(9) 0.4659(6) 0.9471(4) 0.050(2) Uani 1 1 d . . .
H60 H -0.0701 0.4442 0.9111 0.060 Uiso 1 1 calc R . .
Cu1 Cu 0.43341(10) 0.00920(7) 0.37687(5) 0.0449(2) Uani 1 1 d . . .
Cu2 Cu 0.20351(10) 0.06686(7) 0.36745(5) 0.0445(2) Uani 1 1 d . . .
Cu3 Cu 0.36588(10) 0.04147(7) 0.28187(5) 0.0446(2) Uani 1 1 d . . .
Cu4 Cu 0.41684(10) 0.17027(7) 0.37244(5) 0.0450(2) Uani 1 1 d . . .
Cu5 Cu 0.96038(10) 0.42734(7) 0.62688(5) 0.0456(2) Uani 1 1 d . . .
Cu6 Cu 0.83766(10) 0.45080(7) 0.71944(5) 0.0461(2) Uani 1 1 d . . .
Cu7 Cu 1.05334(10) 0.38699(7) 0.71601(5) 0.0456(2) Uani 1 1 d . . .
Cu8 Cu 1.05871(10) 0.54852(7) 0.71947(5) 0.0463(2) Uani 1 1 d . . .
Cu9 Cu 0.44955(10) 0.23339(7) 0.94952(5) 0.0455(2) Uani 1 1 d . . .
Cu10 Cu 0.24893(10) 0.31106(7) 0.94820(5) 0.0458(2) Uani 1 1 d . . .
Cu11 Cu 0.21580(10) 0.15588(7) 0.95613(5) 0.0455(2) Uani 1 1 d . . .
Cu12 Cu 0.32242(10) 0.27537(7) 1.04517(5) 0.0458(2) Uani 1 1 d . . .
I1 I 0.25080(5) -0.08317(3) 0.31442(2) 0.04401(13) Uani 1 1 d . . .
I2 I 0.34010(5) 0.12688(3) 0.45747(2) 0.04389(13) Uani 1 1 d . . .
I3 I 0.23086(5) 0.16395(3) 0.30348(2) 0.04423(13) Uani 1 1 d . . .
I4 I 0.59127(5) 0.07947(4) 0.32423(2) 0.04486(14) Uani 1 1 d . . .
I5 I 0.86590(5) 0.29894(3) 0.65138(2) 0.04456(13) Uani 1 1 d . . .
I6 I 0.98868(5) 0.50158(4) 0.80480(2) 0.04561(14) Uani 1 1 d . . .
I7 I 0.86077(5) 0.56453(4) 0.66566(2) 0.04601(14) Uani 1 1 d . . .
I8 I 1.20182(5) 0.44957(3) 0.65456(2) 0.04480(14) Uani 1 1 d . . .
I9 I 0.41251(5) 0.13229(4) 1.01077(2) 0.04501(14) Uani 1 1 d . . .
I10 I 0.44432(5) 0.38922(3) 1.00729(2) 0.04518(13) Uani 1 1 d . . .
I11 I 0.29382(5) 0.17985(4) 0.86470(2) 0.04451(13) Uani 1 1 d . . .
I12 I 0.09165(5) 0.27036(4) 1.01737(2) 0.04600(14) Uani 1 1 d . . .
S1 S -0.0948(2) -0.03621(16) 0.05778(10) 0.0539(6) Uani 1 1 d . . .
S2 S 0.38665(19) -0.02540(14) 0.19021(9) 0.0420(4) Uani 1 1 d . . .
S3 S 0.0044(2) 0.06327(15) 0.39586(11) 0.0523(5) Uani 1 1 d . . .
S4 S 0.4939(2) 0.30391(15) 0.38908(10) 0.0540(6) Uani 1 1 d . . .
S5 S 0.9727(2) 0.40490(13) 0.53360(9) 0.0444(5) Uani 1 1 d . . .
S6 S 1.1484(2) 0.30092(14) 0.75297(9) 0.0436(5) Uani 1 1 d . . .
S7 S 1.46991(17) 0.07103(12) 0.58274(8) 0.0351(4) Uani 1 1 d . . .
S8 S 1.1622(2) 0.67646(15) 0.75835(10) 0.0497(5) Uani 1 1 d . . .
S9 S 1.6662(2) 0.65475(16) 0.86245(10) 0.0524(5) Uani 1 1 d . . .
S10 S 0.6433(2) 0.44230(16) 0.74992(11) 0.0538(6) Uani 1 1 d . . .
S11 S 0.6394(2) 0.22884(14) 0.91079(9) 0.0469(5) Uani 1 1 d . . .
S12 S 0.16171(19) 0.39815(14) 0.91001(10) 0.0439(5) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C2 C1 H1A 109.5 . . ?
C2 C1 H1B 109.5 . . ?
H1A C1 H1B 109.5 . . ?
C2 C1 H1C 109.5 . . ?
H1A C1 H1C 109.5 . . ?
H1B C1 H1C 109.5 . . ?
C1 C2 S1 108.5(8) . . ?
C1 C2 H2A 110.0 . . ?
S1 C2 H2A 110.0 . . ?
C1 C2 H2B 110.0 . . ?
S1 C2 H2B 110.0 . . ?
H2A C2 H2B 108.4 . . ?
C4 C3 C8 119.7(9) . . ?
C4 C3 S1 118.0(7) . . ?
C8 C3 S1 122.2(8) . . ?
C3 C4 C5 118.6(8) . . ?
C3 C4 H4 120.7 . . ?
C5 C4 H4 120.7 . . ?
C4 C5 C6 119.7(8) . . ?
C4 C5 H5 120.2 . . ?
C6 C5 H5 120.2 . . ?
C7 C6 C5 120.5(8) . . ?
C7 C6 S2 116.1(7) . . ?
C5 C6 S2 123.2(7) . . ?
C8 C7 C6 117.7(9) . . ?
C8 C7 H7 121.1 . . ?
C6 C7 H7 121.1 . . ?
C7 C8 C3 123.3(9) . . ?
C7 C8 H8 118.4 . . ?
C3 C8 H8 118.4 . . ?
C10 C9 S2 115.8(7) . . ?
C10 C9 H9A 108.3 . . ?
S2 C9 H9A 108.3 . . ?
C10 C9 H9B 108.3 . . ?
S2 C9 H9B 108.3 . . ?
H9A C9 H9B 107.4 . . ?
C9 C10 H10A 109.5 . . ?
C9 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C9 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C12 C11 H11A 109.5 . . ?
C12 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
C12 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C11 C12 S3 107.3(7) . . ?
C11 C12 H12A 110.3 . . ?
S3 C12 H12A 110.3 . . ?
C11 C12 H12B 110.3 . . ?
S3 C12 H12B 110.3 . . ?
H12A C12 H12B 108.5 . . ?
C15 C13 C14 122.0(10) 2_556 . ?
C15 C13 H13 119.0 2_556 . ?
C14 C13 H13 119.0 . . ?
C15 C14 C13 115.3(10) . . ?
C15 C14 S3 120.0(8) . . ?
C13 C14 S3 124.6(8) . . ?
C14 C15 C13 122.7(10) . 2_556 ?
C14 C15 H15 118.7 . . ?
C13 C15 H15 118.7 2_556 . ?
C17 C16 H16A 109.5 . . ?
C17 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
C17 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
C16 C17 S4 123.9(8) . . ?
C16 C17 H17A 106.4 . . ?
S4 C17 H17A 106.4 . . ?
C16 C17 H17B 106.4 . . ?
S4 C17 H17B 106.4 . . ?
H17A C17 H17B 106.4 . . ?
C23 C18 C19 120.0(9) . . ?
C23 C18 S4 122.8(7) . . ?
C19 C18 S4 117.1(8) . . ?
C20 C19 C18 120.0(9) . . ?
C20 C19 H19 120.0 . . ?
C18 C19 H19 120.0 . . ?
C21 C20 C19 120.0(8) . . ?
C21 C20 H20 120.0 . . ?
C19 C20 H20 120.0 . . ?
C20 C21 C22 120.0(9) . . ?
C20 C21 S5 116.8(7) . . ?
C22 C21 S5 123.1(8) . . ?
C21 C22 C23 120.0(10) . . ?
C21 C22 H22 120.0 . . ?
C23 C22 H22 120.0 . . ?
C18 C23 C22 120.0(9) . . ?
C18 C23 H23 120.0 . . ?
C22 C23 H23 120.0 . . ?
C25 C24 S5 111.6(7) . . ?
C25 C24 H24A 109.3 . . ?
S5 C24 H24A 109.3 . . ?
C25 C24 H24B 109.3 . . ?
S5 C24 H24B 109.3 . . ?
H24A C24 H24B 108.0 . . ?
C24 C25 H25A 109.5 . . ?
C24 C25 H25B 109.5 . . ?
H25A C25 H25B 109.5 . . ?
C24 C25 H25C 109.5 . . ?
H25A C25 H25C 109.5 . . ?
H25B C25 H25C 109.5 . . ?
C27 C26 H26A 109.5 . . ?
C27 C26 H26B 109.5 . . ?
H26A C26 H26B 109.5 . . ?
C27 C26 H26C 109.5 . . ?
H26A C26 H26C 109.5 . . ?
H26B C26 H26C 109.5 . . ?
C26 C27 S6 113.4(7) . . ?
C26 C27 H27A 108.9 . . ?
S6 C27 H27A 108.9 . . ?
C26 C27 H27B 108.9 . . ?
S6 C27 H27B 108.9 . . ?
H27A C27 H27B 107.7 . . ?
C33 C28 C29 114.9(8) . . ?
C33 C28 S6 124.5(7) . . ?
C29 C28 S6 120.6(6) . . ?
C30 C29 C28 125.0(8) . . ?
C30 C29 H29 117.5 . . ?
C28 C29 H29 117.5 . . ?
C29 C30 C31 117.9(8) . . ?
C29 C30 H30 121.0 . . ?
C31 C30 H30 121.0 . . ?
C30 C31 C32 125.0(8) . . ?
C30 C31 S7 121.2(6) . . ?
C32 C31 S7 113.8(6) . . ?
C31 C32 C33 116.1(8) . . ?
C31 C32 H32 122.0 . . ?
C33 C32 H32 122.0 . . ?
C28 C33 C32 120.6(8) . . ?
C28 C33 H33 119.7 . . ?
C32 C33 H33 119.7 . . ?
C35 C34 S7 108.3(6) . . ?
C35 C34 H34A 110.0 . . ?
S7 C34 H34A 110.0 . . ?
C35 C34 H34B 110.0 . . ?
S7 C34 H34B 110.0 . . ?
H34A C34 H34B 108.4 . . ?
C34 C35 H35A 109.5 . . ?
C34 C35 H35B 109.5 . . ?
H35A C35 H35B 109.5 . . ?
C34 C35 H35C 109.5 . . ?
H35A C35 H35C 109.5 . . ?
H35B C35 H35C 109.5 . . ?
C37 C36 H36A 109.5 . . ?
C37 C36 H36B 109.5 . . ?
H36A C36 H36B 109.5 . . ?
C37 C36 H36C 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
C36 C37 S8 109.7(6) . . ?
C36 C37 H37A 109.7 . . ?
S8 C37 H37A 109.7 . . ?
C36 C37 H37B 109.7 . . ?
S8 C37 H37B 109.7 . . ?
H37A C37 H37B 108.2 . . ?
C43 C38 C39 119.7(9) . . ?
C43 C38 S8 123.0(8) . . ?
C39 C38 S8 117.3(7) . . ?
C38 C39 C40 116.8(9) . . ?
C38 C39 H39 121.6 . . ?
C40 C39 H39 121.6 . . ?
C41 C40 C39 122.6(10) . . ?
C41 C40 H40 118.7 . . ?
C39 C40 H40 118.7 . . ?
C40 C41 C42 123.4(10) . . ?
C40 C41 S9 118.1(8) . . ?
C42 C41 S9 118.0(7) . . ?
C43 C42 C41 114.3(10) . . ?
C43 C42 H42 122.9 . . ?
C41 C42 H42 122.9 . . ?
C38 C43 C42 123.2(11) . . ?
C38 C43 H43 118.4 . . ?
C42 C43 H43 118.4 . . ?
C45 C44 S9 113.0(9) . . ?
C45 C44 H44A 109.0 . . ?
S9 C44 H44A 109.0 . . ?
C45 C44 H44B 109.0 . . ?
S9 C44 H44B 109.0 . . ?
H44A C44 H44B 107.8 . . ?
C44 C45 H45A 109.5 . . ?
C44 C45 H45B 109.5 . . ?
H45A C45 H45B 109.5 . . ?
C44 C45 H45C 109.5 . . ?
H45A C45 H45C 109.5 . . ?
H45B C45 H45C 109.5 . . ?
C47 C46 H46A 109.5 . . ?
C47 C46 H46B 109.5 . . ?
H46A C46 H46B 109.5 . . ?
C47 C46 H46C 109.5 . . ?
H46A C46 H46C 109.5 . . ?
H46B C46 H46C 109.5 . . ?
C46 C47 S10 110.6(8) . . ?
C46 C47 H47A 109.5 . . ?
S10 C47 H47A 109.5 . . ?
C46 C47 H47B 109.5 . . ?
S10 C47 H47B 109.5 . . ?
H47A C47 H47B 108.1 . . ?
C53 C48 C49 120.0(9) . . ?
C53 C48 S10 117.2(7) . . ?
C49 C48 S10 122.8(7) . . ?
C50 C49 C48 120.0(8) . . ?
C50 C49 H49 120.0 . . ?
C48 C49 H49 120.0 . . ?
C49 C50 C51 120.0(9) . . ?
C49 C50 H50 120.0 . . ?
C51 C50 H50 120.0 . . ?
C52 C51 C50 120.0(9) . . ?
C52 C51 S11 122.4(7) . . ?
C50 C51 S11 117.4(7) . . ?
C53 C52 C51 120.0(9) . . ?
C53 C52 H52 120.0 . . ?
C51 C52 H52 120.0 . . ?
C52 C53 C48 120.0(9) . . ?
C52 C53 H53 120.0 . . ?
C48 C53 H53 120.0 . . ?
C55 C54 S11 112.2(7) . . ?
C55 C54 H54A 109.2 . . ?
S11 C54 H54A 109.2 . . ?
C55 C54 H54B 109.2 . . ?
S11 C54 H54B 109.2 . . ?
H54A C54 H54B 107.9 . . ?
C54 C55 H55A 109.5 . . ?
C54 C55 H55B 109.5 . . ?
H55A C55 H55B 109.5 . . ?
C54 C55 H55C 109.5 . . ?
H55A C55 H55C 109.5 . . ?
H55B C55 H55C 109.5 . . ?
C57 C56 H56A 109.5 . . ?
C57 C56 H56B 109.5 . . ?
H56A C56 H56B 109.5 . . ?
C57 C56 H56C 109.5 . . ?
H56A C56 H56C 109.5 . . ?
H56B C56 H56C 109.5 . . ?
C56 C57 S12 107.6(8) . . ?
C56 C57 H57A 110.2 . . ?
S12 C57 H57A 110.2 . . ?
C56 C57 H57B 110.2 . . ?
S12 C57 H57B 110.2 . . ?
H57A C57 H57B 108.5 . . ?
C59 C58 C60 117.5(10) . 2_567 ?
C59 C58 H58 121.2 . . ?
C60 C58 H58 121.2 2_567 . ?
C58 C59 C60 122.7(10) . . ?
C58 C59 S12 119.1(8) . . ?
C60 C59 S12 118.2(8) . . ?
C59 C60 C58 119.7(9) . 2_567 ?
C59 C60 H60 120.2 . . ?
C58 C60 H60 120.2 2_567 . ?
S7 Cu1 I4 109.50(7) 2_756 . ?
S7 Cu1 I1 107.91(7) 2_756 . ?
I4 Cu1 I1 114.71(5) . . ?
S7 Cu1 I2 107.95(7) 2_756 . ?
I4 Cu1 I2 108.45(4) . . ?
I1 Cu1 I2 108.14(4) . . ?
S7 Cu1 Cu3 148.49(8) 2_756 . ?
I4 Cu1 Cu3 59.25(4) . . ?
I1 Cu1 Cu3 60.74(4) . . ?
I2 Cu1 Cu3 103.56(5) . . ?
S7 Cu1 Cu4 145.53(7) 2_756 . ?
I4 Cu1 Cu4 58.20(4) . . ?
I1 Cu1 Cu4 106.30(5) . . ?
I2 Cu1 Cu4 56.30(4) . . ?
Cu3 Cu1 Cu4 57.61(4) . . ?
S7 Cu1 Cu2 142.39(7) 2_756 . ?
I4 Cu1 Cu2 108.01(5) . . ?
I1 Cu1 Cu2 57.01(3) . . ?
I2 Cu1 Cu2 56.42(3) . . ?
Cu3 Cu1 Cu2 59.47(4) . . ?
Cu4 Cu1 Cu2 59.11(4) . . ?
S3 Cu2 I2 106.23(8) . . ?
S3 Cu2 I1 108.65(8) . . ?
I2 Cu2 I1 110.93(4) . . ?
S3 Cu2 I3 108.92(8) . . ?
I2 Cu2 I3 110.51(4) . . ?
I1 Cu2 I3 111.43(5) . . ?
S3 Cu2 Cu3 148.99(9) . . ?
I2 Cu2 Cu3 104.74(5) . . ?
I1 Cu2 Cu3 60.63(4) . . ?
I3 Cu2 Cu3 57.52(4) . . ?
S3 Cu2 Cu4 143.56(8) . . ?
I2 Cu2 Cu4 57.38(4) . . ?
I1 Cu2 Cu4 107.71(5) . . ?
I3 Cu2 Cu4 58.63(3) . . ?
Cu3 Cu2 Cu4 57.66(4) . . ?
S3 Cu2 Cu1 143.83(8) . . ?
I2 Cu2 Cu1 58.83(4) . . ?
I1 Cu2 Cu1 57.71(4) . . ?
I3 Cu2 Cu1 107.23(5) . . ?
Cu3 Cu2 Cu1 58.57(4) . . ?
Cu4 Cu2 Cu1 60.12(4) . . ?
S2 Cu3 I3 115.56(7) . . ?
S2 Cu3 I4 105.33(7) . . ?
I3 Cu3 I4 114.89(5) . . ?
S2 Cu3 Cu4 151.75(8) . . ?
I3 Cu3 Cu4 60.51(4) . . ?
I4 Cu3 Cu4 59.58(4) . . ?
S2 Cu3 I1 99.72(7) . . ?
I3 Cu3 I1 109.44(4) . . ?
I4 Cu3 I1 110.84(4) . . ?
Cu4 Cu3 I1 107.93(5) . . ?
S2 Cu3 Cu1 132.77(8) . . ?
I3 Cu3 Cu1 111.25(5) . . ?
I4 Cu3 Cu1 57.96(4) . . ?
Cu4 Cu3 Cu1 62.62(4) . . ?
I1 Cu3 Cu1 57.77(4) . . ?
S2 Cu3 Cu2 143.67(8) . . ?
I3 Cu3 Cu2 58.91(4) . . ?
I4 Cu3 Cu2 109.00(5) . . ?
Cu4 Cu3 Cu2 61.57(4) . . ?
I1 Cu3 Cu2 56.98(3) . . ?
Cu1 Cu3 Cu2 61.95(4) . . ?
S4 Cu4 I2 116.69(8) . . ?
S4 Cu4 I4 106.29(9) . . ?
I2 Cu4 I4 110.01(4) . . ?
S4 Cu4 I3 100.13(8) . . ?
I2 Cu4 I3 110.41(4) . . ?
I4 Cu4 I3 113.05(5) . . ?
S4 Cu4 Cu3 135.38(9) . . ?
I2 Cu4 Cu3 107.71(5) . . ?
I4 Cu4 Cu3 59.64(4) . . ?
I3 Cu4 Cu3 58.40(4) . . ?
S4 Cu4 Cu2 144.22(9) . . ?
I2 Cu4 Cu2 57.89(4) . . ?
I4 Cu4 Cu2 108.42(5) . . ?
I3 Cu4 Cu2 58.02(3) . . ?
Cu3 Cu4 Cu2 60.77(4) . . ?
S4 Cu4 Cu1 151.87(9) . . ?
I2 Cu4 Cu1 59.23(4) . . ?
I4 Cu4 Cu1 57.03(4) . . ?
I3 Cu4 Cu1 107.26(5) . . ?
Cu3 Cu4 Cu1 59.77(4) . . ?
Cu2 Cu4 Cu1 60.76(4) . . ?
S5 Cu5 I5 112.46(7) . . ?
S5 Cu5 I7 106.24(8) . . ?
I5 Cu5 I7 118.39(5) . . ?
S5 Cu5 Cu6 152.69(8) . . ?
I5 Cu5 Cu6 62.06(4) . . ?
I7 Cu5 Cu6 61.51(4) . . ?
S5 Cu5 I8 99.28(7) . . ?
I5 Cu5 I8 108.31(4) . . ?
I7 Cu5 I8 110.50(5) . . ?
Cu6 Cu5 I8 107.85(5) . . ?
S5 Cu5 Cu8 134.62(8) . . ?
I5 Cu5 Cu8 111.83(5) . . ?
I7 Cu5 Cu8 59.02(4) . . ?
Cu6 Cu5 Cu8 62.87(4) . . ?
I8 Cu5 Cu8 57.20(4) . . ?
S5 Cu5 Cu7 143.86(8) . . ?
I5 Cu5 Cu7 59.77(4) . . ?
I7 Cu5 Cu7 107.82(5) . . ?
Cu6 Cu5 Cu7 59.58(4) . . ?
I8 Cu5 Cu7 57.33(4) . . ?
Cu8 Cu5 Cu7 59.27(4) . . ?
S10 Cu6 I6 108.94(8) . . ?
S10 Cu6 Cu5 141.24(9) . . ?
I6 Cu6 Cu5 109.82(5) . . ?
S10 Cu6 I7 109.09(8) . . ?
I6 Cu6 I7 107.00(4) . . ?
Cu5 Cu6 I7 58.42(4) . . ?
S10 Cu6 Cu7 143.20(9) . . ?
I6 Cu6 Cu7 59.96(4) . . ?
Cu5 Cu6 Cu7 62.48(4) . . ?
I7 Cu6 Cu7 107.70(5) . . ?
S10 Cu6 I5 105.01(8) . . ?
I6 Cu6 I5 114.88(5) . . ?
Cu5 Cu6 I5 57.90(4) . . ?
I7 Cu6 I5 111.80(5) . . ?
Cu7 Cu6 I5 59.47(4) . . ?
S10 Cu6 Cu8 148.21(9) . . ?
I6 Cu6 Cu8 57.38(4) . . ?
Cu5 Cu6 Cu8 60.58(4) . . ?
I7 Cu6 Cu8 57.37(4) . . ?
Cu7 Cu6 Cu8 59.41(4) . . ?
I5 Cu6 Cu8 106.77(5) . . ?
S6 Cu7 I8 111.35(7) . . ?
S6 Cu7 I6 103.11(7) . . ?
I8 Cu7 I6 111.79(5) . . ?
S6 Cu7 I5 108.05(7) . . ?
I8 Cu7 I5 108.18(4) . . ?
I6 Cu7 I5 114.28(5) . . ?
S6 Cu7 Cu6 139.68(8) . . ?
I8 Cu7 Cu6 108.89(5) . . ?
I6 Cu7 Cu6 58.39(4) . . ?
I5 Cu7 Cu6 60.38(4) . . ?
S6 Cu7 Cu8 141.80(8) . . ?
I8 Cu7 Cu8 58.43(4) . . ?
I6 Cu7 Cu8 58.05(4) . . ?
I5 Cu7 Cu8 110.05(5) . . ?
Cu6 Cu7 Cu8 62.67(4) . . ?
S6 Cu7 Cu5 151.77(8) . . ?
I8 Cu7 Cu5 60.21(4) . . ?
I6 Cu7 Cu5 104.95(5) . . ?
I5 Cu7 Cu5 56.73(4) . . ?
Cu6 Cu7 Cu5 57.94(4) . . ?
Cu8 Cu7 Cu5 60.25(4) . . ?
S8 Cu8 I6 104.01(8) . . ?
S8 Cu8 I8 110.28(8) . . ?
I6 Cu8 I8 113.23(5) . . ?
S8 Cu8 I7 109.10(7) . . ?
I6 Cu8 I7 107.90(5) . . ?
I8 Cu8 I7 111.96(5) . . ?
S8 Cu8 Cu7 143.03(8) . . ?
I6 Cu8 Cu7 59.31(4) . . ?
I8 Cu8 Cu7 58.76(4) . . ?
I7 Cu8 Cu7 107.54(5) . . ?
S8 Cu8 Cu5 149.64(8) . . ?
I6 Cu8 Cu5 106.10(5) . . ?
I8 Cu8 Cu5 60.40(4) . . ?
I7 Cu8 Cu5 57.45(4) . . ?
Cu7 Cu8 Cu5 60.49(4) . . ?
S8 Cu8 Cu6 144.21(9) . . ?
I6 Cu8 Cu6 57.12(4) . . ?
I8 Cu8 Cu6 105.33(5) . . ?
I7 Cu8 Cu6 58.68(4) . . ?
Cu7 Cu8 Cu6 57.92(4) . . ?
Cu5 Cu8 Cu6 56.55(4) . . ?
S11 Cu9 I11 104.93(7) . . ?
S11 Cu9 I10 103.84(7) . . ?
I11 Cu9 I10 115.20(5) . . ?
S11 Cu9 I9 112.90(7) . . ?
I11 Cu9 I9 106.94(4) . . ?
I10 Cu9 I9 112.89(5) . . ?
S11 Cu9 Cu10 137.50(8) . . ?
I11 Cu9 Cu10 60.23(4) . . ?
I10 Cu9 Cu10 59.26(4) . . ?
I9 Cu9 Cu10 109.59(5) . . ?
S11 Cu9 Cu12 146.10(8) . . ?
I11 Cu9 Cu12 108.93(5) . . ?
I10 Cu9 Cu12 59.75(4) . . ?
I9 Cu9 Cu12 58.37(4) . . ?
Cu10 Cu9 Cu12 63.08(4) . . ?
S11 Cu9 Cu11 149.45(8) . . ?
I11 Cu9 Cu11 56.97(4) . . ?
I10 Cu9 Cu11 106.28(5) . . ?
I9 Cu9 Cu11 58.94(4) . . ?
Cu10 Cu9 Cu11 59.15(4) . . ?
Cu12 Cu9 Cu11 58.85(4) . . ?
S12 Cu10 I10 109.15(7) . . ?
S12 Cu10 I12 108.06(8) . . ?
I10 Cu10 I12 107.31(5) . . ?
S12 Cu10 I11 106.76(8) . . ?
I10 Cu10 I11 114.10(5) . . ?
I12 Cu10 I11 111.31(4) . . ?
S12 Cu10 Cu9 143.96(8) . . ?
I10 Cu10 Cu9 59.44(4) . . ?
I12 Cu10 Cu9 107.98(5) . . ?
I11 Cu10 Cu9 58.85(4) . . ?
S12 Cu10 Cu11 141.51(8) . . ?
I10 Cu10 Cu11 109.30(5) . . ?
I12 Cu10 Cu11 57.96(4) . . ?
I11 Cu10 Cu11 57.78(4) . . ?
Cu9 Cu10 Cu11 62.79(4) . . ?
S12 Cu10 Cu12 148.19(8) . . ?
I10 Cu10 Cu12 58.49(4) . . ?
I12 Cu10 Cu12 56.93(4) . . ?
I11 Cu10 Cu12 104.96(5) . . ?
Cu9 Cu10 Cu12 59.30(4) . . ?
Cu11 Cu10 Cu12 58.78(4) . . ?
S1 Cu11 I11 113.31(8) 2_556 . ?
S1 Cu11 I12 105.70(9) 2_556 . ?
I11 Cu11 I12 115.25(5) . . ?
S1 Cu11 I9 103.00(8) 2_556 . ?
I11 Cu11 I9 106.62(4) . . ?
I12 Cu11 I9 112.39(5) . . ?
S1 Cu11 Cu10 149.37(9) 2_556 . ?
I11 Cu11 Cu10 60.16(4) . . ?
I12 Cu11 Cu10 59.88(4) . . ?
I9 Cu11 Cu10 107.51(5) . . ?
S1 Cu11 Cu12 136.27(9) 2_556 . ?
I11 Cu11 Cu12 110.02(5) . . ?
I12 Cu11 Cu12 58.88(4) . . ?
I9 Cu11 Cu12 58.02(4) . . ?
Cu10 Cu11 Cu12 62.79(4) . . ?
S1 Cu11 Cu9 147.70(10) 2_556 . ?
I11 Cu11 Cu9 57.95(4) . . ?
I12 Cu11 Cu9 105.75(5) . . ?
I9 Cu11 Cu9 57.58(4) . . ?
Cu10 Cu11 Cu9 58.07(4) . . ?
Cu12 Cu11 Cu9 59.12(4) . . ?
S9 Cu12 I12 104.24(8) 2_767 . ?
S9 Cu12 I9 118.85(8) 2_767 . ?
I12 Cu12 I9 113.94(5) . . ?
S9 Cu12 I10 98.79(8) 2_767 . ?
I12 Cu12 I10 106.99(4) . . ?
I9 Cu12 I10 112.41(5) . . ?
S9 Cu12 Cu11 151.48(9) 2_767 . ?
I12 Cu12 Cu11 58.23(4) . . ?
I9 Cu12 Cu11 60.36(4) . . ?
I10 Cu12 Cu11 107.65(5) . . ?
S9 Cu12 Cu9 145.10(8) 2_767 . ?
I12 Cu12 Cu9 107.54(5) . . ?
I9 Cu12 Cu9 59.30(4) . . ?
I10 Cu12 Cu9 58.30(4) . . ?
Cu11 Cu12 Cu9 62.03(4) . . ?
S9 Cu12 Cu10 134.97(9) 2_767 . ?
I12 Cu12 Cu10 58.11(4) . . ?
I9 Cu12 Cu10 105.91(5) . . ?
I10 Cu12 Cu10 56.94(4) . . ?
Cu11 Cu12 Cu10 58.43(4) . . ?
Cu9 Cu12 Cu10 57.61(4) . . ?
Cu2 I1 Cu1 65.28(4) . . ?
Cu2 I1 Cu3 62.40(4) . . ?
Cu1 I1 Cu3 61.50(4) . . ?
Cu4 I2 Cu2 64.73(4) . . ?
Cu4 I2 Cu1 64.48(4) . . ?
Cu2 I2 Cu1 64.74(4) . . ?
Cu3 I3 Cu2 63.57(4) . . ?
Cu3 I3 Cu4 61.09(4) . . ?
Cu2 I3 Cu4 63.35(4) . . ?
Cu1 I4 Cu4 64.77(4) . . ?
Cu1 I4 Cu3 62.79(4) . . ?
Cu4 I4 Cu3 60.78(4) . . ?
Cu5 I5 Cu7 63.49(4) . . ?
Cu5 I5 Cu6 60.04(4) . . ?
Cu7 I5 Cu6 60.16(4) . . ?
Cu6 I6 Cu8 65.50(4) . . ?
Cu6 I6 Cu7 61.66(4) . . ?
Cu8 I6 Cu7 62.65(4) . . ?
Cu5 I7 Cu8 63.53(4) . . ?
Cu5 I7 Cu6 60.06(4) . . ?
Cu8 I7 Cu6 63.95(4) . . ?
Cu8 I8 Cu7 62.81(4) . . ?
Cu8 I8 Cu5 62.41(4) . . ?
Cu7 I8 Cu5 62.46(4) . . ?
Cu12 I9 Cu9 62.33(4) . . ?
Cu12 I9 Cu11 61.62(4) . . ?
Cu9 I9 Cu11 63.48(4) . . ?
Cu10 I10 Cu9 61.30(4) . . ?
Cu10 I10 Cu12 64.57(4) . . ?
Cu9 I10 Cu12 61.94(4) . . ?
Cu11 I11 Cu9 65.08(4) . . ?
Cu11 I11 Cu10 62.06(4) . . ?
Cu9 I11 Cu10 60.92(4) . . ?
Cu11 I12 Cu12 62.89(4) . . ?
Cu11 I12 Cu10 62.16(4) . . ?
Cu12 I12 Cu10 64.96(4) . . ?
C3 S1 C2 97.7(5) . . ?
C3 S1 Cu11 114.0(4) . 2_556 ?
C2 S1 Cu11 120.6(4) . 2_556 ?
C6 S2 C9 106.8(4) . . ?
C6 S2 Cu3 110.3(3) . . ?
C9 S2 Cu3 111.9(4) . . ?
C14 S3 C12 101.4(5) . . ?
C14 S3 Cu2 108.3(3) . . ?
C12 S3 Cu2 110.0(4) . . ?
C18 S4 C17 103.9(5) . . ?
C18 S4 Cu4 113.8(3) . . ?
C17 S4 Cu4 109.7(3) . . ?
C21 S5 C24 100.0(4) . . ?
C21 S5 Cu5 114.2(3) . . ?
C24 S5 Cu5 104.7(3) . . ?
C28 S6 C27 99.6(4) . . ?
C28 S6 Cu7 111.0(3) . . ?
C27 S6 Cu7 105.5(3) . . ?
C34 S7 C31 98.8(4) . . ?
C34 S7 Cu1 107.2(3) . 2_756 ?
C31 S7 Cu1 109.6(3) . 2_756 ?
C38 S8 C37 102.4(5) . . ?
C38 S8 Cu8 110.5(3) . . ?
C37 S8 Cu8 110.5(3) . . ?
C41 S9 C44 110.1(5) . . ?
C41 S9 Cu12 111.3(3) . 2_767 ?
C44 S9 Cu12 109.4(4) . 2_767 ?
C48 S10 C47 103.6(5) . . ?
C48 S10 Cu6 106.6(3) . . ?
C47 S10 Cu6 106.7(4) . . ?
C51 S11 C54 103.7(4) . . ?
C51 S11 Cu9 108.4(3) . . ?
C54 S11 Cu9 108.7(3) . . ?
C59 S12 C57 99.5(5) . . ?
C59 S12 Cu10 106.1(4) . . ?
C57 S12 Cu10 108.2(4) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 C2 1.521(16) . ?
C1 H1A 0.9600 . ?
C1 H1B 0.9600 . ?
C1 H1C 0.9600 . ?
C2 S1 1.872(13) . ?
C2 H2A 0.9700 . ?
C2 H2B 0.9700 . ?
C3 C4 1.383(13) . ?
C3 C8 1.390(13) . ?
C3 S1 1.814(10) . ?
C4 C5 1.386(12) . ?
C4 H4 0.9300 . ?
C5 C6 1.408(12) . ?
C5 H5 0.9300 . ?
C6 C7 1.404(13) . ?
C6 S2 1.771(9) . ?
C7 C8 1.324(13) . ?
C7 H7 0.9300 . ?
C8 H8 0.9300 . ?
C9 C10 1.466(16) . ?
C9 S2 1.859(9) . ?
C9 H9A 0.9700 . ?
C9 H9B 0.9700 . ?
C10 H10A 0.9600 . ?
C10 H10B 0.9600 . ?
C10 H10C 0.9600 . ?
C11 C12 1.550(15) . ?
C11 H11A 0.9600 . ?
C11 H11B 0.9600 . ?
C11 H11C 0.9600 . ?
C12 S3 1.862(12) . ?
C12 H12A 0.9700 . ?
C12 H12B 0.9700 . ?
C13 C15 1.336(13) 2_556 ?
C13 C14 1.411(14) . ?
C13 H13 0.9300 . ?
C14 C15 1.329(13) . ?
C14 S3 1.784(11) . ?
C15 C13 1.336(13) 2_556 ?
C15 H15 0.9300 . ?
C16 C17 1.540(14) . ?
C16 H16A 0.9600 . ?
C16 H16B 0.9600 . ?
C16 H16C 0.9600 . ?
C17 S4 1.797(12) . ?
C17 H17A 0.9700 . ?
C17 H17B 0.9700 . ?
C18 C23 1.390(14) . ?
C18 C19 1.390(13) . ?
C18 S4 1.784(10) . ?
C19 C20 1.390(15) . ?
C19 H19 0.9300 . ?
C20 C21 1.390(13) . ?
C20 H20 0.9300 . ?
C21 C22 1.390(11) . ?
C21 S5 1.762(9) . ?
C22 C23 1.390(14) . ?
C22 H22 0.9300 . ?
C23 H23 0.9300 . ?
C24 C25 1.521(14) . ?
C24 S5 1.810(10) . ?
C24 H24A 0.9700 . ?
C24 H24B 0.9700 . ?
C25 H25A 0.9600 . ?
C25 H25B 0.9600 . ?
C25 H25C 0.9600 . ?
C26 C27 1.521(12) . ?
C26 H26A 0.9600 . ?
C26 H26B 0.9600 . ?
C26 H26C 0.9600 . ?
C27 S6 1.837(9) . ?
C27 H27A 0.9700 . ?
C27 H27B 0.9700 . ?
C28 C33 1.381(11) . ?
C28 C29 1.429(12) . ?
C28 S6 1.712(9) . ?
C29 C30 1.313(12) . ?
C29 H29 0.9300 . ?
C30 C31 1.339(11) . ?
C30 H30 0.9300 . ?
C31 C32 1.348(13) . ?
C31 S7 1.868(8) . ?
C32 C33 1.468(12) . ?
C32 H32 0.9300 . ?
C33 H33 0.9300 . ?
C34 C35 1.484(12) . ?
C34 S7 1.851(8) . ?
C34 H34A 0.9700 . ?
C34 H34B 0.9700 . ?
C35 H35A 0.9600 . ?
C35 H35B 0.9600 . ?
C35 H35C 0.9600 . ?
C36 C37 1.461(12) . ?
C36 H36A 0.9600 . ?
C36 H36B 0.9600 . ?
C36 H36C 0.9600 . ?
C37 S8 1.833(8) . ?
C37 H37A 0.9700 . ?
C37 H37B 0.9700 . ?
C38 C43 1.392(14) . ?
C38 C39 1.426(12) . ?
C38 S8 1.746(9) . ?
C39 C40 1.469(13) . ?
C39 H39 0.9300 . ?
C40 C41 1.293(14) . ?
C40 H40 0.9300 . ?
C41 C42 1.461(14) . ?
C41 S9 1.775(10) . ?
C42 C43 1.447(15) . ?
C42 H42 0.9300 . ?
C43 H43 0.9300 . ?
C44 C45 1.500(17) . ?
C44 S9 1.847(11) . ?
C44 H44A 0.9700 . ?
C44 H44B 0.9700 . ?
C45 H45A 0.9600 . ?
C45 H45B 0.9600 . ?
C45 H45C 0.9600 . ?
C46 C47 1.483(14) . ?
C46 H46A 0.9600 . ?
C46 H46B 0.9600 . ?
C46 H46C 0.9600 . ?
C47 S10 1.831(11) . ?
C47 H47A 0.9700 . ?
C47 H47B 0.9700 . ?
C48 C53 1.390(13) . ?
C48 C49 1.390(13) . ?
C48 S10 1.781(10) . ?
C49 C50 1.390(14) . ?
C49 H49 0.9300 . ?
C50 C51 1.390(13) . ?
C50 H50 0.9300 . ?
C51 C52 1.390(13) . ?
C51 S11 1.774(9) . ?
C52 C53 1.390(14) . ?
C52 H52 0.9300 . ?
C53 H53 0.9300 . ?
C54 C55 1.484(13) . ?
C54 S11 1.829(10) . ?
C54 H54A 0.9700 . ?
C54 H54B 0.9700 . ?
C55 H55A 0.9600 . ?
C55 H55B 0.9600 . ?
C55 H55C 0.9600 . ?
C56 C57 1.520(16) . ?
C56 H56A 0.9600 . ?
C56 H56B 0.9600 . ?
C56 H56C 0.9600 . ?
C57 S12 1.887(10) . ?
C57 H57A 0.9700 . ?
C57 H57B 0.9700 . ?
C58 C59 1.334(14) . ?
C58 C60 1.450(14) 2_567 ?
C58 H58 0.9300 . ?
C59 C60 1.370(13) . ?
C59 S12 1.772(10) . ?
C60 C58 1.450(14) 2_567 ?
C60 H60 0.9300 . ?
Cu1 S7 2.311(2) 2_756 ?
Cu1 I4 2.6530(13) . ?
Cu1 I1 2.6791(13) . ?
Cu1 I2 2.7238(14) . ?
Cu1 Cu3 2.7834(16) . ?
Cu1 Cu4 2.8608(16) . ?
Cu1 Cu2 2.8790(16) . ?
Cu2 S3 2.345(3) . ?
Cu2 I2 2.6522(13) . ?
Cu2 I1 2.6585(14) . ?
Cu2 I3 2.6873(13) . ?
Cu2 Cu3 2.8099(17) . ?
Cu2 Cu4 2.8314(16) . ?
Cu3 S2 2.316(3) . ?
Cu3 I3 2.6469(13) . ?
Cu3 I4 2.6897(13) . ?
Cu3 Cu4 2.7205(17) . ?
Cu3 I1 2.7631(13) . ?
Cu4 S4 2.316(3) . ?
Cu4 I2 2.6373(13) . ?
Cu4 I4 2.6878(14) . ?
Cu4 I3 2.7050(13) . ?
Cu5 S5 2.317(3) . ?
Cu5 I5 2.6293(13) . ?
Cu5 I7 2.6437(13) . ?
Cu5 Cu6 2.6891(17) . ?
Cu5 I8 2.7542(13) . ?
Cu5 Cu8 2.8074(17) . ?
Cu5 Cu7 2.8140(16) . ?
Cu6 S10 2.317(3) . ?
Cu6 I6 2.6473(13) . ?
Cu6 I7 2.7274(13) . ?
Cu6 Cu7 2.7360(16) . ?
Cu6 I5 2.7420(14) . ?
Cu6 Cu8 2.8684(17) . ?
Cu7 S6 2.328(3) . ?
Cu7 I8 2.6717(13) . ?
Cu7 I6 2.6910(14) . ?
Cu7 I5 2.7170(13) . ?
Cu7 Cu8 2.7795(17) . ?
Cu8 S8 2.342(3) . ?
Cu8 I6 2.6552(14) . ?
Cu8 I8 2.6625(14) . ?
Cu8 I7 2.6890(13) . ?
Cu9 S11 2.342(3) . ?
Cu9 I11 2.6713(13) . ?
Cu9 I10 2.6779(14) . ?
Cu9 I9 2.6965(13) . ?
Cu9 Cu10 2.7277(16) . ?
Cu9 Cu12 2.7775(17) . ?
Cu9 Cu11 2.8583(17) . ?
Cu10 S12 2.318(3) . ?
Cu10 I10 2.6727(13) . ?
Cu10 I12 2.6991(13) . ?
Cu10 I11 2.7093(14) . ?
Cu10 Cu11 2.7592(16) . ?
Cu10 Cu12 2.8802(17) . ?
Cu11 S1 2.308(3) 2_556 ?
Cu11 I11 2.6422(13) . ?
Cu11 I12 2.6452(14) . ?
Cu11 I9 2.7363(13) . ?
Cu11 Cu12 2.7697(17) . ?
Cu12 S9 2.318(3) 2_767 ?
Cu12 I12 2.6638(13) . ?
Cu12 I9 2.6703(13) . ?
Cu12 I10 2.7189(13) . ?
S1 Cu11 2.308(3) 2_556 ?
S7 Cu1 2.311(2) 2_756 ?
S9 Cu12 2.318(3) 2_767 ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C8 C3 C4 C5 -3.0(16) . . . . ?
S1 C3 C4 C5 -179.1(7) . . . . ?
C3 C4 C5 C6 -1.8(14) . . . . ?
C4 C5 C6 C7 2.1(14) . . . . ?
C4 C5 C6 S2 177.3(7) . . . . ?
C5 C6 C7 C8 2.6(17) . . . . ?
S2 C6 C7 C8 -172.9(9) . . . . ?
C6 C7 C8 C3 -7.8(19) . . . . ?
C4 C3 C8 C7 8.2(18) . . . . ?
S1 C3 C8 C7 -175.9(10) . . . . ?
C15 C13 C14 C15 0.5(18) 2_556 . . . ?
C15 C13 C14 S3 176.6(9) 2_556 . . . ?
C13 C14 C15 C13 -0.5(18) . . . 2_556 ?
S3 C14 C15 C13 -176.8(9) . . . 2_556 ?
C23 C18 C19 C20 0.0(19) . . . . ?
S4 C18 C19 C20 -176.9(10) . . . . ?
C18 C19 C20 C21 0.0(19) . . . . ?
C19 C20 C21 C22 0.0(17) . . . . ?
C19 C20 C21 S5 176.4(10) . . . . ?
C20 C21 C22 C23 0.0(17) . . . . ?
S5 C21 C22 C23 -176.2(9) . . . . ?
C19 C18 C23 C22 0.0(19) . . . . ?
S4 C18 C23 C22 176.7(10) . . . . ?
C21 C22 C23 C18 0.0(19) . . . . ?
C33 C28 C29 C30 -5.5(15) . . . . ?
S6 C28 C29 C30 176.8(8) . . . . ?
C28 C29 C30 C31 7.2(15) . . . . ?
C29 C30 C31 C32 -6.8(16) . . . . ?
C29 C30 C31 S7 175.5(8) . . . . ?
C30 C31 C32 C33 4.7(16) . . . . ?
S7 C31 C32 C33 -177.4(8) . . . . ?
C29 C28 C33 C32 3.2(14) . . . . ?
S6 C28 C33 C32 -179.2(8) . . . . ?
C31 C32 C33 C28 -2.9(15) . . . . ?
C43 C38 C39 C40 1.5(14) . . . . ?
S8 C38 C39 C40 -175.5(7) . . . . ?
C38 C39 C40 C41 -0.7(15) . . . . ?
C39 C40 C41 C42 -2.1(17) . . . . ?
C39 C40 C41 S9 -174.2(8) . . . . ?
C40 C41 C42 C43 3.7(15) . . . . ?
S9 C41 C42 C43 175.8(7) . . . . ?
C39 C38 C43 C42 0.3(15) . . . . ?
S8 C38 C43 C42 177.1(8) . . . . ?
C41 C42 C43 C38 -2.7(15) . . . . ?
C53 C48 C49 C50 0.0(14) . . . . ?
S10 C48 C49 C50 178.3(7) . . . . ?
C48 C49 C50 C51 0.0(14) . . . . ?
C49 C50 C51 C52 0.0(15) . . . . ?
C49 C50 C51 S11 176.0(7) . . . . ?
C50 C51 C52 C53 0.0(16) . . . . ?
S11 C51 C52 C53 -175.8(8) . . . . ?
C51 C52 C53 C48 0.0(16) . . . . ?
C49 C48 C53 C52 0.0(15) . . . . ?
S10 C48 C53 C52 -178.4(8) . . . . ?
C60 C58 C59 C60 4(2) 2_567 . . . ?
C60 C58 C59 S12 -177.5(9) 2_567 . . . ?
C58 C59 C60 C58 -4(2) . . . 2_567 ?
S12 C59 C60 C58 177.4(9) . . . 2_567 ?
S7 Cu1 Cu2 S3 1.1(2) 2_756 . . . ?
I4 Cu1 Cu2 S3 -174.68(14) . . . . ?
I1 Cu1 Cu2 S3 77.08(14) . . . . ?
I2 Cu1 Cu2 S3 -74.11(14) . . . . ?
Cu3 Cu1 Cu2 S3 149.99(15) . . . . ?
Cu4 Cu1 Cu2 S3 -141.84(15) . . . . ?
S7 Cu1 Cu2 I2 75.19(12) 2_756 . . . ?
I4 Cu1 Cu2 I2 -100.57(5) . . . . ?
I1 Cu1 Cu2 I2 151.19(5) . . . . ?
Cu3 Cu1 Cu2 I2 -135.90(5) . . . . ?
Cu4 Cu1 Cu2 I2 -67.73(4) . . . . ?
S7 Cu1 Cu2 I1 -76.00(12) 2_756 . . . ?
I4 Cu1 Cu2 I1 108.24(5) . . . . ?
I2 Cu1 Cu2 I1 -151.19(5) . . . . ?
Cu3 Cu1 Cu2 I1 72.91(4) . . . . ?
Cu4 Cu1 Cu2 I1 141.08(5) . . . . ?
S7 Cu1 Cu2 I3 179.14(11) 2_756 . . . ?
I4 Cu1 Cu2 I3 3.38(6) . . . . ?
I1 Cu1 Cu2 I3 -104.86(5) . . . . ?
I2 Cu1 Cu2 I3 103.95(5) . . . . ?
Cu3 Cu1 Cu2 I3 -31.95(4) . . . . ?
Cu4 Cu1 Cu2 I3 36.22(4) . . . . ?
S7 Cu1 Cu2 Cu3 -148.91(13) 2_756 . . . ?
I4 Cu1 Cu2 Cu3 35.32(4) . . . . ?
I1 Cu1 Cu2 Cu3 -72.91(4) . . . . ?
I2 Cu1 Cu2 Cu3 135.90(5) . . . . ?
Cu4 Cu1 Cu2 Cu3 68.17(4) . . . . ?
S7 Cu1 Cu2 Cu4 142.92(13) 2_756 . . . ?
I4 Cu1 Cu2 Cu4 -32.85(4) . . . . ?
I1 Cu1 Cu2 Cu4 -141.08(5) . . . . ?
I2 Cu1 Cu2 Cu4 67.73(4) . . . . ?
Cu3 Cu1 Cu2 Cu4 -68.17(4) . . . . ?
S7 Cu1 Cu3 S2 4.28(19) 2_756 . . . ?
I4 Cu1 Cu3 S2 81.13(10) . . . . ?
I1 Cu1 Cu3 S2 -71.86(10) . . . . ?
I2 Cu1 Cu3 S2 -175.27(9) . . . . ?
Cu4 Cu1 Cu3 S2 150.72(11) . . . . ?
Cu2 Cu1 Cu3 S2 -138.65(11) . . . . ?
S7 Cu1 Cu3 I3 176.33(13) 2_756 . . . ?
I4 Cu1 Cu3 I3 -106.82(5) . . . . ?
I1 Cu1 Cu3 I3 100.19(5) . . . . ?
I2 Cu1 Cu3 I3 -3.22(6) . . . . ?
Cu4 Cu1 Cu3 I3 -37.23(5) . . . . ?
Cu2 Cu1 Cu3 I3 33.40(4) . . . . ?
S7 Cu1 Cu3 I4 -76.85(14) 2_756 . . . ?
I1 Cu1 Cu3 I4 -152.98(5) . . . . ?
I2 Cu1 Cu3 I4 103.61(5) . . . . ?
Cu4 Cu1 Cu3 I4 69.59(4) . . . . ?
Cu2 Cu1 Cu3 I4 140.22(5) . . . . ?
S7 Cu1 Cu3 Cu4 -146.45(14) 2_756 . . . ?
I4 Cu1 Cu3 Cu4 -69.59(4) . . . . ?
I1 Cu1 Cu3 Cu4 137.42(5) . . . . ?
I2 Cu1 Cu3 Cu4 34.01(4) . . . . ?
Cu2 Cu1 Cu3 Cu4 70.63(5) . . . . ?
S7 Cu1 Cu3 I1 76.13(14) 2_756 . . . ?
I4 Cu1 Cu3 I1 152.98(5) . . . . ?
I2 Cu1 Cu3 I1 -103.41(4) . . . . ?
Cu4 Cu1 Cu3 I1 -137.42(5) . . . . ?
Cu2 Cu1 Cu3 I1 -66.79(4) . . . . ?
S7 Cu1 Cu3 Cu2 142.93(15) 2_756 . . . ?
I4 Cu1 Cu3 Cu2 -140.22(5) . . . . ?
I1 Cu1 Cu3 Cu2 66.79(4) . . . . ?
I2 Cu1 Cu3 Cu2 -36.62(4) . . . . ?
Cu4 Cu1 Cu3 Cu2 -70.63(5) . . . . ?
S3 Cu2 Cu3 S2 -20.0(2) . . . . ?
I2 Cu2 Cu3 S2 163.06(12) . . . . ?
I1 Cu2 Cu3 S2 57.05(13) . . . . ?
I3 Cu2 Cu3 S2 -91.75(13) . . . . ?
Cu4 Cu2 Cu3 S2 -162.65(14) . . . . ?
Cu1 Cu2 Cu3 S2 125.06(14) . . . . ?
S3 Cu2 Cu3 I3 71.76(16) . . . . ?
I2 Cu2 Cu3 I3 -105.19(5) . . . . ?
I1 Cu2 Cu3 I3 148.80(4) . . . . ?
Cu4 Cu2 Cu3 I3 -70.90(4) . . . . ?
Cu1 Cu2 Cu3 I3 -143.19(5) . . . . ?
S3 Cu2 Cu3 I4 179.95(15) . . . . ?
I2 Cu2 Cu3 I4 3.01(6) . . . . ?
I1 Cu2 Cu3 I4 -103.00(5) . . . . ?
I3 Cu2 Cu3 I4 108.19(5) . . . . ?
Cu4 Cu2 Cu3 I4 37.30(4) . . . . ?
Cu1 Cu2 Cu3 I4 -35.00(4) . . . . ?
S3 Cu2 Cu3 Cu4 142.65(16) . . . . ?
I2 Cu2 Cu3 Cu4 -34.29(4) . . . . ?
I1 Cu2 Cu3 Cu4 -140.30(5) . . . . ?
I3 Cu2 Cu3 Cu4 70.90(4) . . . . ?
Cu1 Cu2 Cu3 Cu4 -72.30(4) . . . . ?
S3 Cu2 Cu3 I1 -77.05(16) . . . . ?
I2 Cu2 Cu3 I1 106.01(5) . . . . ?
I3 Cu2 Cu3 I1 -148.80(4) . . . . ?
Cu4 Cu2 Cu3 I1 140.30(5) . . . . ?
Cu1 Cu2 Cu3 I1 68.00(4) . . . . ?
S3 Cu2 Cu3 Cu1 -145.05(16) . . . . ?
I2 Cu2 Cu3 Cu1 38.01(4) . . . . ?
I1 Cu2 Cu3 Cu1 -68.00(4) . . . . ?
I3 Cu2 Cu3 Cu1 143.19(5) . . . . ?
Cu4 Cu2 Cu3 Cu1 72.30(4) . . . . ?
S2 Cu3 Cu4 S4 18.9(2) . . . . ?
I3 Cu3 Cu4 S4 -70.77(13) . . . . ?
I4 Cu3 Cu4 S4 82.48(13) . . . . ?
I1 Cu3 Cu4 S4 -173.41(12) . . . . ?
Cu1 Cu3 Cu4 S4 149.61(13) . . . . ?
Cu2 Cu3 Cu4 S4 -139.16(13) . . . . ?
S2 Cu3 Cu4 I2 -166.81(15) . . . . ?
I3 Cu3 Cu4 I2 103.50(5) . . . . ?
I4 Cu3 Cu4 I2 -103.25(5) . . . . ?
I1 Cu3 Cu4 I2 0.86(6) . . . . ?
Cu1 Cu3 Cu4 I2 -36.12(4) . . . . ?
Cu2 Cu3 Cu4 I2 35.11(4) . . . . ?
S2 Cu3 Cu4 I4 -63.56(16) . . . . ?
I3 Cu3 Cu4 I4 -153.25(4) . . . . ?
I1 Cu3 Cu4 I4 104.11(5) . . . . ?
Cu1 Cu3 Cu4 I4 67.13(4) . . . . ?
Cu2 Cu3 Cu4 I4 138.36(5) . . . . ?
S2 Cu3 Cu4 I3 89.69(16) . . . . ?
I4 Cu3 Cu4 I3 153.25(4) . . . . ?
I1 Cu3 Cu4 I3 -102.64(5) . . . . ?
Cu1 Cu3 Cu4 I3 -139.62(5) . . . . ?
Cu2 Cu3 Cu4 I3 -68.39(4) . . . . ?
S2 Cu3 Cu4 Cu2 158.08(17) . . . . ?
I3 Cu3 Cu4 Cu2 68.39(4) . . . . ?
I4 Cu3 Cu4 Cu2 -138.36(5) . . . . ?
I1 Cu3 Cu4 Cu2 -34.26(4) . . . . ?
Cu1 Cu3 Cu4 Cu2 -71.23(4) . . . . ?
S2 Cu3 Cu4 Cu1 -130.68(17) . . . . ?
I3 Cu3 Cu4 Cu1 139.62(5) . . . . ?
I4 Cu3 Cu4 Cu1 -67.13(4) . . . . ?
I1 Cu3 Cu4 Cu1 36.98(4) . . . . ?
Cu2 Cu3 Cu4 Cu1 71.23(4) . . . . ?
S3 Cu2 Cu4 S4 -20.0(2) . . . . ?
I2 Cu2 Cu4 S4 -92.08(14) . . . . ?
I1 Cu2 Cu4 S4 163.97(13) . . . . ?
I3 Cu2 Cu4 S4 59.23(14) . . . . ?
Cu3 Cu2 Cu4 S4 128.22(14) . . . . ?
Cu1 Cu2 Cu4 S4 -162.15(15) . . . . ?
S3 Cu2 Cu4 I2 72.06(14) . . . . ?
I1 Cu2 Cu4 I2 -103.94(5) . . . . ?
I3 Cu2 Cu4 I2 151.31(5) . . . . ?
Cu3 Cu2 Cu4 I2 -139.69(5) . . . . ?
Cu1 Cu2 Cu4 I2 -70.06(4) . . . . ?
S3 Cu2 Cu4 I4 174.57(14) . . . . ?
I2 Cu2 Cu4 I4 102.52(5) . . . . ?
I1 Cu2 Cu4 I4 -1.42(6) . . . . ?
I3 Cu2 Cu4 I4 -106.17(5) . . . . ?
Cu3 Cu2 Cu4 I4 -37.18(4) . . . . ?
Cu1 Cu2 Cu4 I4 32.45(4) . . . . ?
S3 Cu2 Cu4 I3 -79.26(14) . . . . ?
I2 Cu2 Cu4 I3 -151.31(5) . . . . ?
I1 Cu2 Cu4 I3 104.74(5) . . . . ?
Cu3 Cu2 Cu4 I3 68.99(4) . . . . ?
Cu1 Cu2 Cu4 I3 138.62(5) . . . . ?
S3 Cu2 Cu4 Cu3 -148.25(15) . . . . ?
I2 Cu2 Cu4 Cu3 139.69(5) . . . . ?
I1 Cu2 Cu4 Cu3 35.75(4) . . . . ?
I3 Cu2 Cu4 Cu3 -68.99(4) . . . . ?
Cu1 Cu2 Cu4 Cu3 69.63(5) . . . . ?
S3 Cu2 Cu4 Cu1 142.12(15) . . . . ?
I2 Cu2 Cu4 Cu1 70.06(4) . . . . ?
I1 Cu2 Cu4 Cu1 -33.88(4) . . . . ?
I3 Cu2 Cu4 Cu1 -138.62(5) . . . . ?
Cu3 Cu2 Cu4 Cu1 -69.63(5) . . . . ?
S7 Cu1 Cu4 S4 18.2(3) 2_756 . . . ?
I4 Cu1 Cu4 S4 -59.71(19) . . . . ?
I1 Cu1 Cu4 S4 -169.04(18) . . . . ?
I2 Cu1 Cu4 S4 89.72(19) . . . . ?
Cu3 Cu1 Cu4 S4 -131.1(2) . . . . ?
Cu2 Cu1 Cu4 S4 157.7(2) . . . . ?
S7 Cu1 Cu4 I2 -71.51(13) 2_756 . . . ?
I4 Cu1 Cu4 I2 -149.43(4) . . . . ?
I1 Cu1 Cu4 I2 101.23(5) . . . . ?
Cu3 Cu1 Cu4 I2 139.18(5) . . . . ?
Cu2 Cu1 Cu4 I2 67.94(4) . . . . ?
S7 Cu1 Cu4 I4 77.92(13) 2_756 . . . ?
I1 Cu1 Cu4 I4 -109.34(5) . . . . ?
I2 Cu1 Cu4 I4 149.43(4) . . . . ?
Cu3 Cu1 Cu4 I4 -71.39(4) . . . . ?
Cu2 Cu1 Cu4 I4 -142.64(5) . . . . ?
S7 Cu1 Cu4 I3 -175.40(12) 2_756 . . . ?
I4 Cu1 Cu4 I3 106.68(5) . . . . ?
I1 Cu1 Cu4 I3 -2.66(6) . . . . ?
I2 Cu1 Cu4 I3 -103.89(5) . . . . ?
Cu3 Cu1 Cu4 I3 35.29(4) . . . . ?
Cu2 Cu1 Cu4 I3 -35.95(4) . . . . ?
S7 Cu1 Cu4 Cu3 149.31(14) 2_756 . . . ?
I4 Cu1 Cu4 Cu3 71.39(4) . . . . ?
I1 Cu1 Cu4 Cu3 -37.95(4) . . . . ?
I2 Cu1 Cu4 Cu3 -139.18(5) . . . . ?
Cu2 Cu1 Cu4 Cu3 -71.25(5) . . . . ?
S7 Cu1 Cu4 Cu2 -139.45(13) 2_756 . . . ?
I4 Cu1 Cu4 Cu2 142.64(5) . . . . ?
I1 Cu1 Cu4 Cu2 33.30(4) . . . . ?
I2 Cu1 Cu4 Cu2 -67.94(4) . . . . ?
Cu3 Cu1 Cu4 Cu2 71.25(5) . . . . ?
S5 Cu5 Cu6 S10 12.2(2) . . . . ?
I5 Cu5 Cu6 S10 -72.95(14) . . . . ?
I7 Cu5 Cu6 S10 81.24(14) . . . . ?
I8 Cu5 Cu6 S10 -174.65(13) . . . . ?
Cu8 Cu5 Cu6 S10 148.91(14) . . . . ?
Cu7 Cu5 Cu6 S10 -142.50(14) . . . . ?
S5 Cu5 Cu6 I6 -167.29(16) . . . . ?
I5 Cu5 Cu6 I6 107.57(5) . . . . ?
I7 Cu5 Cu6 I6 -98.24(5) . . . . ?
I8 Cu5 Cu6 I6 5.87(6) . . . . ?
Cu8 Cu5 Cu6 I6 -30.57(4) . . . . ?
Cu7 Cu5 Cu6 I6 38.02(5) . . . . ?
S5 Cu5 Cu6 I7 -69.05(17) . . . . ?
I5 Cu5 Cu6 I7 -154.19(4) . . . . ?
I8 Cu5 Cu6 I7 104.11(5) . . . . ?
Cu8 Cu5 Cu6 I7 67.67(4) . . . . ?
Cu7 Cu5 Cu6 I7 136.26(5) . . . . ?
S5 Cu5 Cu6 Cu7 154.69(18) . . . . ?
I5 Cu5 Cu6 Cu7 69.55(4) . . . . ?
I7 Cu5 Cu6 Cu7 -136.26(5) . . . . ?
I8 Cu5 Cu6 Cu7 -32.15(4) . . . . ?
Cu8 Cu5 Cu6 Cu7 -68.59(4) . . . . ?
S5 Cu5 Cu6 I5 85.14(17) . . . . ?
I7 Cu5 Cu6 I5 154.19(4) . . . . ?
I8 Cu5 Cu6 I5 -101.70(5) . . . . ?
Cu8 Cu5 Cu6 I5 -138.14(5) . . . . ?
Cu7 Cu5 Cu6 I5 -69.55(4) . . . . ?
S5 Cu5 Cu6 Cu8 -136.72(18) . . . . ?
I5 Cu5 Cu6 Cu8 138.14(5) . . . . ?
I7 Cu5 Cu6 Cu8 -67.67(4) . . . . ?
I8 Cu5 Cu6 Cu8 36.44(4) . . . . ?
Cu7 Cu5 Cu6 Cu8 68.59(4) . . . . ?
S10 Cu6 Cu7 S6 -9.8(2) . . . . ?
I6 Cu6 Cu7 S6 71.71(12) . . . . ?
Cu5 Cu6 Cu7 S6 -150.31(13) . . . . ?
I7 Cu6 Cu7 S6 171.51(11) . . . . ?
I5 Cu6 Cu7 S6 -83.16(12) . . . . ?
Cu8 Cu6 Cu7 S6 139.29(13) . . . . ?
S10 Cu6 Cu7 I8 173.99(14) . . . . ?
I6 Cu6 Cu7 I8 -104.48(5) . . . . ?
Cu5 Cu6 Cu7 I8 33.50(5) . . . . ?
I7 Cu6 Cu7 I8 -4.69(6) . . . . ?
I5 Cu6 Cu7 I8 100.64(5) . . . . ?
Cu8 Cu6 Cu7 I8 -36.90(4) . . . . ?
S10 Cu6 Cu7 I6 -81.53(15) . . . . ?
Cu5 Cu6 Cu7 I6 137.98(5) . . . . ?
I7 Cu6 Cu7 I6 99.79(5) . . . . ?
I5 Cu6 Cu7 I6 -154.87(4) . . . . ?
Cu8 Cu6 Cu7 I6 67.58(4) . . . . ?
S10 Cu6 Cu7 I5 73.35(15) . . . . ?
I6 Cu6 Cu7 I5 154.87(4) . . . . ?
Cu5 Cu6 Cu7 I5 -67.15(4) . . . . ?
I7 Cu6 Cu7 I5 -105.33(5) . . . . ?
Cu8 Cu6 Cu7 I5 -137.55(5) . . . . ?
S10 Cu6 Cu7 Cu8 -149.11(15) . . . . ?
I6 Cu6 Cu7 Cu8 -67.58(4) . . . . ?
Cu5 Cu6 Cu7 Cu8 70.40(5) . . . . ?
I7 Cu6 Cu7 Cu8 32.21(5) . . . . ?
I5 Cu6 Cu7 Cu8 137.55(5) . . . . ?
S10 Cu6 Cu7 Cu5 140.49(16) . . . . ?
I6 Cu6 Cu7 Cu5 -137.98(5) . . . . ?
I7 Cu6 Cu7 Cu5 -38.19(4) . . . . ?
I5 Cu6 Cu7 Cu5 67.15(4) . . . . ?
Cu8 Cu6 Cu7 Cu5 -70.40(5) . . . . ?
S5 Cu5 Cu7 S6 -23.2(2) . . . . ?
I5 Cu5 Cu7 S6 64.00(17) . . . . ?
I7 Cu5 Cu7 S6 177.01(16) . . . . ?
Cu6 Cu5 Cu7 S6 137.34(17) . . . . ?
I8 Cu5 Cu7 S6 -79.65(17) . . . . ?
Cu8 Cu5 Cu7 S6 -148.09(17) . . . . ?
S5 Cu5 Cu7 I8 56.42(12) . . . . ?
I5 Cu5 Cu7 I8 143.65(5) . . . . ?
I7 Cu5 Cu7 I8 -103.34(5) . . . . ?
Cu6 Cu5 Cu7 I8 -143.01(5) . . . . ?
Cu8 Cu5 Cu7 I8 -68.44(4) . . . . ?
S5 Cu5 Cu7 I6 163.27(12) . . . . ?
I5 Cu5 Cu7 I6 -109.50(5) . . . . ?
I7 Cu5 Cu7 I6 3.51(6) . . . . ?
Cu6 Cu5 Cu7 I6 -36.16(4) . . . . ?
I8 Cu5 Cu7 I6 106.85(5) . . . . ?
Cu8 Cu5 Cu7 I6 38.41(4) . . . . ?
S5 Cu5 Cu7 I5 -87.24(13) . . . . ?
I7 Cu5 Cu7 I5 113.00(5) . . . . ?
Cu6 Cu5 Cu7 I5 73.34(4) . . . . ?
I8 Cu5 Cu7 I5 -143.65(5) . . . . ?
Cu8 Cu5 Cu7 I5 147.91(5) . . . . ?
S5 Cu5 Cu7 Cu6 -160.58(13) . . . . ?
I5 Cu5 Cu7 Cu6 -73.34(4) . . . . ?
I7 Cu5 Cu7 Cu6 39.66(5) . . . . ?
I8 Cu5 Cu7 Cu6 143.01(5) . . . . ?
Cu8 Cu5 Cu7 Cu6 74.57(5) . . . . ?
S5 Cu5 Cu7 Cu8 124.85(13) . . . . ?
I5 Cu5 Cu7 Cu8 -147.91(5) . . . . ?
I7 Cu5 Cu7 Cu8 -34.91(5) . . . . ?
Cu6 Cu5 Cu7 Cu8 -74.57(5) . . . . ?
I8 Cu5 Cu7 Cu8 68.44(4) . . . . ?
S6 Cu7 Cu8 S8 2.4(2) . . . . ?
I8 Cu7 Cu8 S8 -82.43(14) . . . . ?
I6 Cu7 Cu8 S8 71.30(14) . . . . ?
I5 Cu7 Cu8 S8 178.05(13) . . . . ?
Cu6 Cu7 Cu8 S8 139.39(15) . . . . ?
Cu5 Cu7 Cu8 S8 -153.73(15) . . . . ?
S6 Cu7 Cu8 I6 -68.88(13) . . . . ?
I8 Cu7 Cu8 I6 -153.72(5) . . . . ?
I5 Cu7 Cu8 I6 106.75(5) . . . . ?
Cu6 Cu7 Cu8 I6 68.10(4) . . . . ?
Cu5 Cu7 Cu8 I6 134.97(5) . . . . ?
S6 Cu7 Cu8 I8 84.84(13) . . . . ?
I6 Cu7 Cu8 I8 153.72(5) . . . . ?
I5 Cu7 Cu8 I8 -99.53(5) . . . . ?
Cu6 Cu7 Cu8 I8 -138.18(5) . . . . ?
Cu5 Cu7 Cu8 I8 -71.31(4) . . . . ?
S6 Cu7 Cu8 I7 -169.67(12) . . . . ?
I8 Cu7 Cu8 I7 105.48(5) . . . . ?
I6 Cu7 Cu8 I7 -100.79(5) . . . . ?
I5 Cu7 Cu8 I7 5.95(7) . . . . ?
Cu6 Cu7 Cu8 I7 -32.70(5) . . . . ?
Cu5 Cu7 Cu8 I7 34.17(5) . . . . ?
S6 Cu7 Cu8 Cu5 156.15(14) . . . . ?
I8 Cu7 Cu8 Cu5 71.31(4) . . . . ?
I6 Cu7 Cu8 Cu5 -134.97(5) . . . . ?
I5 Cu7 Cu8 Cu5 -28.22(5) . . . . ?
Cu6 Cu7 Cu8 Cu5 -66.87(5) . . . . ?
S6 Cu7 Cu8 Cu6 -136.98(14) . . . . ?
I8 Cu7 Cu8 Cu6 138.18(5) . . . . ?
I6 Cu7 Cu8 Cu6 -68.10(4) . . . . ?
I5 Cu7 Cu8 Cu6 38.65(5) . . . . ?
Cu5 Cu7 Cu8 Cu6 66.87(5) . . . . ?
S5 Cu5 Cu8 S8 11.1(2) . . . . ?
I5 Cu5 Cu8 S8 177.86(16) . . . . ?
I7 Cu5 Cu8 S8 -71.22(17) . . . . ?
Cu6 Cu5 Cu8 S8 -142.71(17) . . . . ?
I8 Cu5 Cu8 S8 79.56(17) . . . . ?
Cu7 Cu5 Cu8 S8 148.23(17) . . . . ?
S5 Cu5 Cu8 I6 -176.45(11) . . . . ?
I5 Cu5 Cu8 I6 -9.65(6) . . . . ?
I7 Cu5 Cu8 I6 101.26(5) . . . . ?
Cu6 Cu5 Cu8 I6 29.77(4) . . . . ?
I8 Cu5 Cu8 I6 -107.95(5) . . . . ?
Cu7 Cu5 Cu8 I6 -39.29(4) . . . . ?
S5 Cu5 Cu8 I8 -68.50(11) . . . . ?
I5 Cu5 Cu8 I8 98.30(5) . . . . ?
I7 Cu5 Cu8 I8 -150.79(5) . . . . ?
Cu6 Cu5 Cu8 I8 137.72(5) . . . . ?
Cu7 Cu5 Cu8 I8 68.66(4) . . . . ?
S5 Cu5 Cu8 I7 82.29(11) . . . . ?
I5 Cu5 Cu8 I7 -110.91(5) . . . . ?
Cu6 Cu5 Cu8 I7 -71.49(4) . . . . ?
I8 Cu5 Cu8 I7 150.79(5) . . . . ?
Cu7 Cu5 Cu8 I7 -140.55(5) . . . . ?
S5 Cu5 Cu8 Cu7 -137.16(12) . . . . ?
I5 Cu5 Cu8 Cu7 29.64(5) . . . . ?
I7 Cu5 Cu8 Cu7 140.55(5) . . . . ?
Cu6 Cu5 Cu8 Cu7 69.06(5) . . . . ?
I8 Cu5 Cu8 Cu7 -68.66(4) . . . . ?
S5 Cu5 Cu8 Cu6 153.78(12) . . . . ?
I5 Cu5 Cu8 Cu6 -39.43(5) . . . . ?
I7 Cu5 Cu8 Cu6 71.49(4) . . . . ?
I8 Cu5 Cu8 Cu6 -137.72(5) . . . . ?
Cu7 Cu5 Cu8 Cu6 -69.06(5) . . . . ?
S10 Cu6 Cu8 S8 6.3(2) . . . . ?
I6 Cu6 Cu8 S8 -66.18(13) . . . . ?
Cu5 Cu6 Cu8 S8 148.43(14) . . . . ?
I7 Cu6 Cu8 S8 79.09(13) . . . . ?
Cu7 Cu6 Cu8 S8 -137.99(14) . . . . ?
I5 Cu6 Cu8 S8 -175.38(12) . . . . ?
S10 Cu6 Cu8 I6 72.47(16) . . . . ?
Cu5 Cu6 Cu8 I6 -145.38(5) . . . . ?
I7 Cu6 Cu8 I6 145.28(5) . . . . ?
Cu7 Cu6 Cu8 I6 -71.81(4) . . . . ?
I5 Cu6 Cu8 I6 -109.20(5) . . . . ?
S10 Cu6 Cu8 I8 -179.48(15) . . . . ?
I6 Cu6 Cu8 I8 108.05(5) . . . . ?
Cu5 Cu6 Cu8 I8 -37.34(4) . . . . ?
I7 Cu6 Cu8 I8 -106.68(5) . . . . ?
Cu7 Cu6 Cu8 I8 36.24(4) . . . . ?
I5 Cu6 Cu8 I8 -1.15(6) . . . . ?
S10 Cu6 Cu8 I7 -72.80(16) . . . . ?
I6 Cu6 Cu8 I7 -145.28(5) . . . . ?
Cu5 Cu6 Cu8 I7 69.34(4) . . . . ?
Cu7 Cu6 Cu8 I7 142.92(5) . . . . ?
I5 Cu6 Cu8 I7 105.53(5) . . . . ?
S10 Cu6 Cu8 Cu7 144.28(17) . . . . ?
I6 Cu6 Cu8 Cu7 71.81(4) . . . . ?
Cu5 Cu6 Cu8 Cu7 -73.57(5) . . . . ?
I7 Cu6 Cu8 Cu7 -142.92(5) . . . . ?
I5 Cu6 Cu8 Cu7 -37.39(4) . . . . ?
S10 Cu6 Cu8 Cu5 -142.15(17) . . . . ?
I6 Cu6 Cu8 Cu5 145.38(5) . . . . ?
I7 Cu6 Cu8 Cu5 -69.34(4) . . . . ?
Cu7 Cu6 Cu8 Cu5 73.57(5) . . . . ?
I5 Cu6 Cu8 Cu5 36.18(4) . . . . ?
S11 Cu9 Cu10 S12 4.3(2) . . . . ?
I11 Cu9 Cu10 S12 -75.06(14) . . . . ?
I10 Cu9 Cu10 S12 80.57(14) . . . . ?
I9 Cu9 Cu10 S12 -173.85(13) . . . . ?
Cu12 Cu9 Cu10 S12 149.75(14) . . . . ?
Cu11 Cu9 Cu10 S12 -142.11(14) . . . . ?
S11 Cu9 Cu10 I10 -76.28(12) . . . . ?
I11 Cu9 Cu10 I10 -155.62(5) . . . . ?
I9 Cu9 Cu10 I10 105.59(5) . . . . ?
Cu12 Cu9 Cu10 I10 69.18(4) . . . . ?
Cu11 Cu9 Cu10 I10 137.32(5) . . . . ?
S11 Cu9 Cu10 I12 -176.16(11) . . . . ?
I11 Cu9 Cu10 I12 104.50(5) . . . . ?
I10 Cu9 Cu10 I12 -99.88(5) . . . . ?
I9 Cu9 Cu10 I12 5.71(7) . . . . ?
Cu12 Cu9 Cu10 I12 -30.70(5) . . . . ?
Cu11 Cu9 Cu10 I12 37.44(4) . . . . ?
S11 Cu9 Cu10 I11 79.34(12) . . . . ?
I10 Cu9 Cu10 I11 155.62(5) . . . . ?
I9 Cu9 Cu10 I11 -98.79(5) . . . . ?
Cu12 Cu9 Cu10 I11 -135.19(5) . . . . ?
Cu11 Cu9 Cu10 I11 -67.06(4) . . . . ?
S11 Cu9 Cu10 Cu11 146.40(12) . . . . ?
I11 Cu9 Cu10 Cu11 67.06(4) . . . . ?
I10 Cu9 Cu10 Cu11 -137.32(5) . . . . ?
I9 Cu9 Cu10 Cu11 -31.73(5) . . . . ?
Cu12 Cu9 Cu10 Cu11 -68.13(5) . . . . ?
S11 Cu9 Cu10 Cu12 -145.46(12) . . . . ?
I11 Cu9 Cu10 Cu12 135.19(5) . . . . ?
I10 Cu9 Cu10 Cu12 -69.18(4) . . . . ?
I9 Cu9 Cu10 Cu12 36.40(5) . . . . ?
Cu11 Cu9 Cu10 Cu12 68.13(5) . . . . ?
S12 Cu10 Cu11 S1 -10.0(3) . . . 2_556 ?
I10 Cu10 Cu11 S1 167.31(17) . . . 2_556 ?
I12 Cu10 Cu11 S1 68.53(18) . . . 2_556 ?
I11 Cu10 Cu11 S1 -85.78(18) . . . 2_556 ?
Cu9 Cu10 Cu11 S1 -154.48(19) . . . 2_556 ?
Cu12 Cu10 Cu11 S1 136.60(19) . . . 2_556 ?
S12 Cu10 Cu11 I11 75.82(13) . . . . ?
I10 Cu10 Cu11 I11 -106.90(5) . . . . ?
I12 Cu10 Cu11 I11 154.32(5) . . . . ?
Cu9 Cu10 Cu11 I11 -68.69(4) . . . . ?
Cu12 Cu10 Cu11 I11 -137.62(5) . . . . ?
S12 Cu10 Cu11 I12 -78.49(13) . . . . ?
I10 Cu10 Cu11 I12 98.78(5) . . . . ?
I11 Cu10 Cu11 I12 -154.32(5) . . . . ?
Cu9 Cu10 Cu11 I12 136.99(5) . . . . ?
Cu12 Cu10 Cu11 I12 68.07(4) . . . . ?
S12 Cu10 Cu11 I9 175.32(12) . . . . ?
I10 Cu10 Cu11 I9 -7.41(7) . . . . ?
I12 Cu10 Cu11 I9 -106.19(5) . . . . ?
I11 Cu10 Cu11 I9 99.49(5) . . . . ?
Cu9 Cu10 Cu11 I9 30.80(5) . . . . ?
Cu12 Cu10 Cu11 I9 -38.13(4) . . . . ?
S12 Cu10 Cu11 Cu12 -146.56(14) . . . . ?
I10 Cu10 Cu11 Cu12 30.72(5) . . . . ?
I12 Cu10 Cu11 Cu12 -68.07(4) . . . . ?
I11 Cu10 Cu11 Cu12 137.62(5) . . . . ?
Cu9 Cu10 Cu11 Cu12 68.92(5) . . . . ?
S12 Cu10 Cu11 Cu9 144.52(14) . . . . ?
I10 Cu10 Cu11 Cu9 -38.21(5) . . . . ?
I12 Cu10 Cu11 Cu9 -136.99(5) . . . . ?
I11 Cu10 Cu11 Cu9 68.69(4) . . . . ?
Cu12 Cu10 Cu11 Cu9 -68.92(5) . . . . ?
S11 Cu9 Cu11 S1 23.1(2) . . . 2_556 ?
I11 Cu9 Cu11 S1 83.29(15) . . . 2_556 ?
I10 Cu9 Cu11 S1 -166.89(14) . . . 2_556 ?
I9 Cu9 Cu11 S1 -59.60(15) . . . 2_556 ?
Cu10 Cu9 Cu11 S1 155.74(16) . . . 2_556 ?
Cu12 Cu9 Cu11 S1 -129.04(16) . . . 2_556 ?
S11 Cu9 Cu11 I11 -60.19(15) . . . . ?
I10 Cu9 Cu11 I11 109.83(5) . . . . ?
I9 Cu9 Cu11 I11 -142.89(5) . . . . ?
Cu10 Cu9 Cu11 I11 72.45(4) . . . . ?
Cu12 Cu9 Cu11 I11 147.68(5) . . . . ?
S11 Cu9 Cu11 I12 -170.45(14) . . . . ?
I11 Cu9 Cu11 I12 -110.26(5) . . . . ?
I10 Cu9 Cu11 I12 -0.44(6) . . . . ?
I9 Cu9 Cu11 I12 106.85(5) . . . . ?
Cu10 Cu9 Cu11 I12 -37.81(4) . . . . ?
Cu12 Cu9 Cu11 I12 37.41(4) . . . . ?
S11 Cu9 Cu11 I9 82.70(15) . . . . ?
I11 Cu9 Cu11 I9 142.89(5) . . . . ?
I10 Cu9 Cu11 I9 -107.29(5) . . . . ?
Cu10 Cu9 Cu11 I9 -144.66(5) . . . . ?
Cu12 Cu9 Cu11 I9 -69.44(4) . . . . ?
S11 Cu9 Cu11 Cu10 -132.64(16) . . . . ?
I11 Cu9 Cu11 Cu10 -72.45(4) . . . . ?
I10 Cu9 Cu11 Cu10 37.37(4) . . . . ?
I9 Cu9 Cu11 Cu10 144.66(5) . . . . ?
Cu12 Cu9 Cu11 Cu10 75.22(5) . . . . ?
S11 Cu9 Cu11 Cu12 152.14(16) . . . . ?
I11 Cu9 Cu11 Cu12 -147.68(5) . . . . ?
I10 Cu9 Cu11 Cu12 -37.85(4) . . . . ?
I9 Cu9 Cu11 Cu12 69.44(4) . . . . ?
Cu10 Cu9 Cu11 Cu12 -75.22(5) . . . . ?
S1 Cu11 Cu12 S9 -22.3(2) 2_556 . . 2_767 ?
I11 Cu11 Cu12 S9 165.81(18) . . . 2_767 ?
I12 Cu11 Cu12 S9 57.73(18) . . . 2_767 ?
I9 Cu11 Cu12 S9 -96.64(19) . . . 2_767 ?
Cu10 Cu11 Cu12 S9 127.32(19) . . . 2_767 ?
Cu9 Cu11 Cu12 S9 -165.35(19) . . . 2_767 ?
S1 Cu11 Cu12 I12 -79.98(13) 2_556 . . . ?
I11 Cu11 Cu12 I12 108.08(5) . . . . ?
I9 Cu11 Cu12 I12 -154.37(5) . . . . ?
Cu10 Cu11 Cu12 I12 69.59(4) . . . . ?
Cu9 Cu11 Cu12 I12 136.92(5) . . . . ?
S1 Cu11 Cu12 I9 74.38(13) 2_556 . . . ?
I11 Cu11 Cu12 I9 -97.55(5) . . . . ?
I12 Cu11 Cu12 I9 154.37(5) . . . . ?
Cu10 Cu11 Cu12 I9 -136.04(5) . . . . ?
Cu9 Cu11 Cu12 I9 -68.72(4) . . . . ?
S1 Cu11 Cu12 I10 -179.40(12) 2_556 . . . ?
I11 Cu11 Cu12 I10 8.66(6) . . . . ?
I12 Cu11 Cu12 I10 -99.41(5) . . . . ?
I9 Cu11 Cu12 I10 106.22(5) . . . . ?
Cu10 Cu11 Cu12 I10 -29.82(5) . . . . ?
Cu9 Cu11 Cu12 I10 37.50(4) . . . . ?
S1 Cu11 Cu12 Cu9 143.10(14) 2_556 . . . ?
I11 Cu11 Cu12 Cu9 -28.84(5) . . . . ?
I12 Cu11 Cu12 Cu9 -136.92(5) . . . . ?
I9 Cu11 Cu12 Cu9 68.72(4) . . . . ?
Cu10 Cu11 Cu12 Cu9 -67.33(4) . . . . ?
S1 Cu11 Cu12 Cu10 -149.58(14) 2_556 . . . ?
I11 Cu11 Cu12 Cu10 38.49(5) . . . . ?
I12 Cu11 Cu12 Cu10 -69.59(4) . . . . ?
I9 Cu11 Cu12 Cu10 136.04(5) . . . . ?
Cu9 Cu11 Cu12 Cu10 67.33(4) . . . . ?
S11 Cu9 Cu12 S9 13.0(2) . . . 2_767 ?
I11 Cu9 Cu12 S9 -163.90(15) . . . 2_767 ?
I10 Cu9 Cu12 S9 -55.17(15) . . . 2_767 ?
I9 Cu9 Cu12 S9 97.44(15) . . . 2_767 ?
Cu10 Cu9 Cu12 S9 -123.60(16) . . . 2_767 ?
Cu11 Cu9 Cu12 S9 167.82(16) . . . 2_767 ?
S11 Cu9 Cu12 I12 167.69(13) . . . . ?
I11 Cu9 Cu12 I12 -9.23(6) . . . . ?
I10 Cu9 Cu12 I12 99.50(5) . . . . ?
I9 Cu9 Cu12 I12 -107.89(5) . . . . ?
Cu10 Cu9 Cu12 I12 31.06(4) . . . . ?
Cu11 Cu9 Cu12 I12 -37.52(4) . . . . ?
S11 Cu9 Cu12 I9 -84.42(14) . . . . ?
I11 Cu9 Cu12 I9 98.66(5) . . . . ?
I10 Cu9 Cu12 I9 -152.61(5) . . . . ?
Cu10 Cu9 Cu12 I9 138.96(5) . . . . ?
Cu11 Cu9 Cu12 I9 70.38(4) . . . . ?
S11 Cu9 Cu12 I10 68.19(14) . . . . ?
I11 Cu9 Cu12 I10 -108.72(5) . . . . ?
I9 Cu9 Cu12 I10 152.61(5) . . . . ?
Cu10 Cu9 Cu12 I10 -68.43(4) . . . . ?
Cu11 Cu9 Cu12 I10 -137.01(5) . . . . ?
S11 Cu9 Cu12 Cu11 -154.79(15) . . . . ?
I11 Cu9 Cu12 Cu11 28.29(4) . . . . ?
I10 Cu9 Cu12 Cu11 137.01(5) . . . . ?
I9 Cu9 Cu12 Cu11 -70.38(4) . . . . ?
Cu10 Cu9 Cu12 Cu11 68.58(4) . . . . ?
S11 Cu9 Cu12 Cu10 136.63(15) . . . . ?
I11 Cu9 Cu12 Cu10 -40.29(4) . . . . ?
I10 Cu9 Cu12 Cu10 68.43(4) . . . . ?
I9 Cu9 Cu12 Cu10 -138.96(5) . . . . ?
Cu11 Cu9 Cu12 Cu10 -68.58(4) . . . . ?
S12 Cu10 Cu12 S9 -8.1(2) . . . 2_767 ?
I10 Cu10 Cu12 S9 66.89(11) . . . 2_767 ?
I12 Cu10 Cu12 S9 -77.76(12) . . . 2_767 ?
I11 Cu10 Cu12 S9 176.29(11) . . . 2_767 ?
Cu9 Cu10 Cu12 S9 137.65(12) . . . 2_767 ?
Cu11 Cu10 Cu12 S9 -147.54(12) . . . 2_767 ?
S12 Cu10 Cu12 I12 69.62(15) . . . . ?
I10 Cu10 Cu12 I12 144.65(5) . . . . ?
I11 Cu10 Cu12 I12 -105.96(5) . . . . ?
Cu9 Cu10 Cu12 I12 -144.59(5) . . . . ?
Cu11 Cu10 Cu12 I12 -69.78(4) . . . . ?
S12 Cu10 Cu12 I9 178.26(14) . . . . ?
I10 Cu10 Cu12 I9 -106.71(5) . . . . ?
I12 Cu10 Cu12 I9 108.64(5) . . . . ?
I11 Cu10 Cu12 I9 2.68(6) . . . . ?
Cu9 Cu10 Cu12 I9 -35.95(4) . . . . ?
Cu11 Cu10 Cu12 I9 38.86(4) . . . . ?
S12 Cu10 Cu12 I10 -75.03(15) . . . . ?
I12 Cu10 Cu12 I10 -144.65(5) . . . . ?
I11 Cu10 Cu12 I10 109.39(5) . . . . ?
Cu9 Cu10 Cu12 I10 70.76(4) . . . . ?
Cu11 Cu10 Cu12 I10 145.57(5) . . . . ?
S12 Cu10 Cu12 Cu11 139.41(16) . . . . ?
I10 Cu10 Cu12 Cu11 -145.57(5) . . . . ?
I12 Cu10 Cu12 Cu11 69.78(4) . . . . ?
I11 Cu10 Cu12 Cu11 -36.17(4) . . . . ?
Cu9 Cu10 Cu12 Cu11 -74.81(5) . . . . ?
S12 Cu10 Cu12 Cu9 -145.79(16) . . . . ?
I10 Cu10 Cu12 Cu9 -70.76(4) . . . . ?
I12 Cu10 Cu12 Cu9 144.59(5) . . . . ?
I11 Cu10 Cu12 Cu9 38.63(4) . . . . ?
Cu11 Cu10 Cu12 Cu9 74.81(5) . . . . ?
S3 Cu2 I1 Cu1 -142.62(9) . . . . ?
I2 Cu2 I1 Cu1 -26.20(4) . . . . ?
I3 Cu2 I1 Cu1 97.38(5) . . . . ?
Cu3 Cu2 I1 Cu1 69.38(4) . . . . ?
Cu4 Cu2 I1 Cu1 34.88(4) . . . . ?
S3 Cu2 I1 Cu3 148.00(9) . . . . ?
I2 Cu2 I1 Cu3 -95.58(5) . . . . ?
I3 Cu2 I1 Cu3 28.00(4) . . . . ?
Cu4 Cu2 I1 Cu3 -34.51(4) . . . . ?
Cu1 Cu2 I1 Cu3 -69.38(4) . . . . ?
S7 Cu1 I1 Cu2 141.52(8) 2_756 . . . ?
I4 Cu1 I1 Cu2 -96.15(5) . . . . ?
I2 Cu1 I1 Cu2 24.99(4) . . . . ?
Cu3 Cu1 I1 Cu2 -70.71(4) . . . . ?
Cu4 Cu1 I1 Cu2 -34.17(5) . . . . ?
S7 Cu1 I1 Cu3 -147.78(8) 2_756 . . . ?
I4 Cu1 I1 Cu3 -25.45(4) . . . . ?
I2 Cu1 I1 Cu3 95.70(5) . . . . ?
Cu4 Cu1 I1 Cu3 36.53(4) . . . . ?
Cu2 Cu1 I1 Cu3 70.71(4) . . . . ?
S2 Cu3 I1 Cu2 -149.71(7) . . . . ?
I3 Cu3 I1 Cu2 -28.06(4) . . . . ?
I4 Cu3 I1 Cu2 99.67(5) . . . . ?
Cu4 Cu3 I1 Cu2 36.18(5) . . . . ?
Cu1 Cu3 I1 Cu2 75.34(4) . . . . ?
S2 Cu3 I1 Cu1 134.95(7) . . . . ?
I3 Cu3 I1 Cu1 -103.40(5) . . . . ?
I4 Cu3 I1 Cu1 24.33(4) . . . . ?
Cu4 Cu3 I1 Cu1 -39.16(5) . . . . ?
Cu2 Cu3 I1 Cu1 -75.34(4) . . . . ?
S4 Cu4 I2 Cu2 139.16(10) . . . . ?
I4 Cu4 I2 Cu2 -99.70(5) . . . . ?
I3 Cu4 I2 Cu2 25.75(4) . . . . ?
Cu3 Cu4 I2 Cu2 -36.34(5) . . . . ?
Cu1 Cu4 I2 Cu2 -72.70(4) . . . . ?
S4 Cu4 I2 Cu1 -148.15(10) . . . . ?
I4 Cu4 I2 Cu1 -27.01(4) . . . . ?
I3 Cu4 I2 Cu1 98.45(5) . . . . ?
Cu3 Cu4 I2 Cu1 36.36(5) . . . . ?
Cu2 Cu4 I2 Cu1 72.70(4) . . . . ?
S3 Cu2 I2 Cu4 -143.95(8) . . . . ?
I1 Cu2 I2 Cu4 98.15(5) . . . . ?
I3 Cu2 I2 Cu4 -25.95(4) . . . . ?
Cu3 Cu2 I2 Cu4 34.41(5) . . . . ?
Cu1 Cu2 I2 Cu4 72.30(4) . . . . ?
S3 Cu2 I2 Cu1 143.76(8) . . . . ?
I1 Cu2 I2 Cu1 25.86(4) . . . . ?
I3 Cu2 I2 Cu1 -98.24(5) . . . . ?
Cu3 Cu2 I2 Cu1 -37.88(4) . . . . ?
Cu4 Cu2 I2 Cu1 -72.30(4) . . . . ?
S7 Cu1 I2 Cu4 145.66(8) 2_756 . . . ?
I4 Cu1 I2 Cu4 27.11(4) . . . . ?
I1 Cu1 I2 Cu4 -97.84(5) . . . . ?
Cu3 Cu1 I2 Cu4 -34.60(4) . . . . ?
Cu2 Cu1 I2 Cu4 -72.67(4) . . . . ?
S7 Cu1 I2 Cu2 -141.67(8) 2_756 . . . ?
I4 Cu1 I2 Cu2 99.78(5) . . . . ?
I1 Cu1 I2 Cu2 -25.17(4) . . . . ?
Cu3 Cu1 I2 Cu2 38.08(4) . . . . ?
Cu4 Cu1 I2 Cu2 72.67(4) . . . . ?
S2 Cu3 I3 Cu2 138.97(9) . . . . ?
I4 Cu3 I3 Cu2 -98.01(5) . . . . ?
Cu4 Cu3 I3 Cu2 -72.68(4) . . . . ?
I1 Cu3 I3 Cu2 27.42(4) . . . . ?
Cu1 Cu3 I3 Cu2 -34.56(5) . . . . ?
S2 Cu3 I3 Cu4 -148.35(9) . . . . ?
I4 Cu3 I3 Cu4 -25.33(4) . . . . ?
I1 Cu3 I3 Cu4 100.10(5) . . . . ?
Cu1 Cu3 I3 Cu4 38.11(5) . . . . ?
Cu2 Cu3 I3 Cu4 72.68(4) . . . . ?
S3 Cu2 I3 Cu3 -148.85(9) . . . . ?
I2 Cu2 I3 Cu3 94.81(5) . . . . ?
I1 Cu2 I3 Cu3 -29.01(4) . . . . ?
Cu4 Cu2 I3 Cu3 69.24(4) . . . . ?
Cu1 Cu2 I3 Cu3 32.36(5) . . . . ?
S3 Cu2 I3 Cu4 141.91(9) . . . . ?
I2 Cu2 I3 Cu4 25.57(4) . . . . ?
I1 Cu2 I3 Cu4 -98.24(5) . . . . ?
Cu3 Cu2 I3 Cu4 -69.24(4) . . . . ?
Cu1 Cu2 I3 Cu4 -36.88(5) . . . . ?
S4 Cu4 I3 Cu3 137.65(9) . . . . ?
I2 Cu4 I3 Cu3 -98.75(5) . . . . ?
I4 Cu4 I3 Cu3 24.97(4) . . . . ?
Cu2 Cu4 I3 Cu3 -73.04(4) . . . . ?
Cu1 Cu4 I3 Cu3 -35.88(5) . . . . ?
S4 Cu4 I3 Cu2 -149.31(9) . . . . ?
I2 Cu4 I3 Cu2 -25.71(4) . . . . ?
I4 Cu4 I3 Cu2 98.00(5) . . . . ?
Cu3 Cu4 I3 Cu2 73.04(4) . . . . ?
Cu1 Cu4 I3 Cu2 37.16(5) . . . . ?
S7 Cu1 I4 Cu4 -144.05(8) 2_756 . . . ?
I1 Cu1 I4 Cu4 94.49(5) . . . . ?
I2 Cu1 I4 Cu4 -26.49(4) . . . . ?
Cu3 Cu1 I4 Cu4 68.62(4) . . . . ?
Cu2 Cu1 I4 Cu4 33.21(5) . . . . ?
S7 Cu1 I4 Cu3 147.32(8) 2_756 . . . ?
I1 Cu1 I4 Cu3 25.86(4) . . . . ?
I2 Cu1 I4 Cu3 -95.11(5) . . . . ?
Cu4 Cu1 I4 Cu3 -68.62(4) . . . . ?
Cu2 Cu1 I4 Cu3 -35.42(5) . . . . ?
S4 Cu4 I4 Cu1 154.90(8) . . . . ?
I2 Cu4 I4 Cu1 27.71(4) . . . . ?
I3 Cu4 I4 Cu1 -96.22(5) . . . . ?
Cu3 Cu4 I4 Cu1 -71.60(4) . . . . ?
Cu2 Cu4 I4 Cu1 -33.93(5) . . . . ?
S4 Cu4 I4 Cu3 -133.49(8) . . . . ?
I2 Cu4 I4 Cu3 99.32(5) . . . . ?
I3 Cu4 I4 Cu3 -24.62(4) . . . . ?
Cu2 Cu4 I4 Cu3 37.67(4) . . . . ?
Cu1 Cu4 I4 Cu3 71.60(4) . . . . ?
S2 Cu3 I4 Cu1 -131.24(8) . . . . ?
I3 Cu3 I4 Cu1 100.42(6) . . . . ?
Cu4 Cu3 I4 Cu1 74.84(4) . . . . ?
I1 Cu3 I4 Cu1 -24.28(4) . . . . ?
Cu2 Cu3 I4 Cu1 36.67(5) . . . . ?
S2 Cu3 I4 Cu4 153.93(8) . . . . ?
I3 Cu3 I4 Cu4 25.59(4) . . . . ?
I1 Cu3 I4 Cu4 -99.11(5) . . . . ?
Cu1 Cu3 I4 Cu4 -74.84(4) . . . . ?
Cu2 Cu3 I4 Cu4 -38.17(5) . . . . ?
S5 Cu5 I5 Cu7 140.40(9) . . . . ?
I7 Cu5 I5 Cu7 -95.03(6) . . . . ?
Cu6 Cu5 I5 Cu7 -69.24(4) . . . . ?
I8 Cu5 I5 Cu7 31.70(4) . . . . ?
Cu8 Cu5 I5 Cu7 -29.47(5) . . . . ?
S5 Cu5 I5 Cu6 -150.36(9) . . . . ?
I7 Cu5 I5 Cu6 -25.79(5) . . . . ?
I8 Cu5 I5 Cu6 100.95(5) . . . . ?
Cu8 Cu5 I5 Cu6 39.78(5) . . . . ?
Cu7 Cu5 I5 Cu6 69.24(4) . . . . ?
S6 Cu7 I5 Cu5 -153.44(9) . . . . ?
I8 Cu7 I5 Cu5 -32.78(4) . . . . ?
I6 Cu7 I5 Cu5 92.44(5) . . . . ?
Cu6 Cu7 I5 Cu5 69.07(4) . . . . ?
Cu8 Cu7 I5 Cu5 29.40(5) . . . . ?
S6 Cu7 I5 Cu6 137.49(8) . . . . ?
I8 Cu7 I5 Cu6 -101.85(5) . . . . ?
I6 Cu7 I5 Cu6 23.37(4) . . . . ?
Cu8 Cu7 I5 Cu6 -39.67(5) . . . . ?
Cu5 Cu7 I5 Cu6 -69.07(4) . . . . ?
S10 Cu6 I5 Cu5 141.71(9) . . . . ?
I6 Cu6 I5 Cu5 -98.64(6) . . . . ?
I7 Cu6 I5 Cu5 23.55(4) . . . . ?
Cu7 Cu6 I5 Cu5 -74.74(4) . . . . ?
Cu8 Cu6 I5 Cu5 -37.38(5) . . . . ?
S10 Cu6 I5 Cu7 -143.55(9) . . . . ?
I6 Cu6 I5 Cu7 -23.90(4) . . . . ?
Cu5 Cu6 I5 Cu7 74.74(4) . . . . ?
I7 Cu6 I5 Cu7 98.29(5) . . . . ?
Cu8 Cu6 I5 Cu7 37.36(4) . . . . ?
S10 Cu6 I6 Cu8 -147.92(9) . . . . ?
Cu5 Cu6 I6 Cu8 31.74(5) . . . . ?
I7 Cu6 I6 Cu8 -30.11(4) . . . . ?
Cu7 Cu6 I6 Cu8 70.86(4) . . . . ?
I5 Cu6 I6 Cu8 94.64(5) . . . . ?
S10 Cu6 I6 Cu7 141.22(9) . . . . ?
Cu5 Cu6 I6 Cu7 -39.13(5) . . . . ?
I7 Cu6 I6 Cu7 -100.97(5) . . . . ?
I5 Cu6 I6 Cu7 23.77(4) . . . . ?
Cu8 Cu6 I6 Cu7 -70.86(4) . . . . ?
S8 Cu8 I6 Cu6 146.53(8) . . . . ?
I8 Cu8 I6 Cu6 -93.74(5) . . . . ?
I7 Cu8 I6 Cu6 30.75(4) . . . . ?
Cu7 Cu8 I6 Cu6 -69.41(4) . . . . ?
Cu5 Cu8 I6 Cu6 -29.56(5) . . . . ?
S8 Cu8 I6 Cu7 -144.05(8) . . . . ?
I8 Cu8 I6 Cu7 -24.32(4) . . . . ?
I7 Cu8 I6 Cu7 100.17(5) . . . . ?
Cu5 Cu8 I6 Cu7 39.85(5) . . . . ?
Cu6 Cu8 I6 Cu7 69.41(4) . . . . ?
S6 Cu7 I6 Cu6 -140.89(8) . . . . ?
I8 Cu7 I6 Cu6 99.40(5) . . . . ?
I5 Cu7 I6 Cu6 -23.88(4) . . . . ?
Cu8 Cu7 I6 Cu6 75.43(4) . . . . ?
Cu5 Cu7 I6 Cu6 35.96(5) . . . . ?
S6 Cu7 I6 Cu8 143.68(8) . . . . ?
I8 Cu7 I6 Cu8 23.97(4) . . . . ?
I5 Cu7 I6 Cu8 -99.32(5) . . . . ?
Cu6 Cu7 I6 Cu8 -75.43(4) . . . . ?
Cu5 Cu7 I6 Cu8 -39.48(5) . . . . ?
S5 Cu5 I7 Cu8 -132.72(8) . . . . ?
I5 Cu5 I7 Cu8 99.71(6) . . . . ?
Cu6 Cu5 I7 Cu8 73.78(4) . . . . ?
I8 Cu5 I7 Cu8 -25.97(4) . . . . ?
Cu7 Cu5 I7 Cu8 35.01(5) . . . . ?
S5 Cu5 I7 Cu6 153.50(8) . . . . ?
I5 Cu5 I7 Cu6 25.93(5) . . . . ?
I8 Cu5 I7 Cu6 -99.75(5) . . . . ?
Cu8 Cu5 I7 Cu6 -73.78(4) . . . . ?
Cu7 Cu5 I7 Cu6 -38.77(5) . . . . ?
S8 Cu8 I7 Cu5 149.58(9) . . . . ?
I6 Cu8 I7 Cu5 -98.03(5) . . . . ?
I8 Cu8 I7 Cu5 27.23(4) . . . . ?
Cu7 Cu8 I7 Cu5 -35.44(5) . . . . ?
Cu6 Cu8 I7 Cu5 -67.85(4) . . . . ?
S8 Cu8 I7 Cu6 -142.57(9) . . . . ?
I6 Cu8 I7 Cu6 -30.18(4) . . . . ?
I8 Cu8 I7 Cu6 95.07(5) . . . . ?
Cu7 Cu8 I7 Cu6 32.40(5) . . . . ?
Cu5 Cu8 I7 Cu6 67.85(4) . . . . ?
S10 Cu6 I7 Cu5 -139.10(9) . . . . ?
I6 Cu6 I7 Cu5 103.19(5) . . . . ?
Cu7 Cu6 I7 Cu5 40.06(5) . . . . ?
I5 Cu6 I7 Cu5 -23.41(4) . . . . ?
Cu8 Cu6 I7 Cu5 73.08(5) . . . . ?
S10 Cu6 I7 Cu8 147.82(9) . . . . ?
I6 Cu6 I7 Cu8 30.11(4) . . . . ?
Cu5 Cu6 I7 Cu8 -73.08(5) . . . . ?
Cu7 Cu6 I7 Cu8 -33.01(5) . . . . ?
I5 Cu6 I7 Cu8 -96.48(5) . . . . ?
S8 Cu8 I8 Cu7 140.54(8) . . . . ?
I6 Cu8 I8 Cu7 24.47(4) . . . . ?
I7 Cu8 I8 Cu7 -97.79(5) . . . . ?
Cu5 Cu8 I8 Cu7 -71.45(4) . . . . ?
Cu6 Cu8 I8 Cu7 -35.86(4) . . . . ?
S8 Cu8 I8 Cu5 -148.00(8) . . . . ?
I6 Cu8 I8 Cu5 95.93(5) . . . . ?
I7 Cu8 I8 Cu5 -26.33(4) . . . . ?
Cu7 Cu8 I8 Cu5 71.45(4) . . . . ?
Cu6 Cu8 I8 Cu5 35.59(4) . . . . ?
S6 Cu7 I8 Cu8 -138.60(9) . . . . ?
I6 Cu7 I8 Cu8 -23.86(4) . . . . ?
I5 Cu7 I8 Cu8 102.81(5) . . . . ?
Cu6 Cu7 I8 Cu8 38.76(5) . . . . ?
Cu5 Cu7 I8 Cu8 71.37(4) . . . . ?
S6 Cu7 I8 Cu5 150.03(9) . . . . ?
I6 Cu7 I8 Cu5 -95.23(5) . . . . ?
I5 Cu7 I8 Cu5 31.44(4) . . . . ?
Cu6 Cu7 I8 Cu5 -32.61(5) . . . . ?
Cu8 Cu7 I8 Cu5 -71.37(4) . . . . ?
S5 Cu5 I8 Cu8 137.85(8) . . . . ?
I5 Cu5 I8 Cu8 -104.65(5) . . . . ?
I7 Cu5 I8 Cu8 26.53(4) . . . . ?
Cu6 Cu5 I8 Cu8 -38.97(5) . . . . ?
Cu7 Cu5 I8 Cu8 -72.00(5) . . . . ?
S5 Cu5 I8 Cu7 -150.14(8) . . . . ?
I5 Cu5 I8 Cu7 -32.64(4) . . . . ?
I7 Cu5 I8 Cu7 98.54(5) . . . . ?
Cu6 Cu5 I8 Cu7 33.03(5) . . . . ?
Cu8 Cu5 I8 Cu7 72.00(5) . . . . ?
S9 Cu12 I9 Cu9 -139.63(10) 2_767 . . . ?
I12 Cu12 I9 Cu9 96.89(5) . . . . ?
I10 Cu12 I9 Cu9 -25.05(4) . . . . ?
Cu11 Cu12 I9 Cu9 73.16(4) . . . . ?
Cu10 Cu12 I9 Cu9 35.21(4) . . . . ?
S9 Cu12 I9 Cu11 147.21(10) 2_767 . . . ?
I12 Cu12 I9 Cu11 23.73(4) . . . . ?
I10 Cu12 I9 Cu11 -98.21(5) . . . . ?
Cu9 Cu12 I9 Cu11 -73.16(4) . . . . ?
Cu10 Cu12 I9 Cu11 -37.95(4) . . . . ?
S11 Cu9 I9 Cu12 142.95(9) . . . . ?
I11 Cu9 I9 Cu12 -102.16(5) . . . . ?
I10 Cu9 I9 Cu12 25.55(4) . . . . ?
Cu10 Cu9 I9 Cu12 -38.42(5) . . . . ?
Cu11 Cu9 I9 Cu12 -70.23(4) . . . . ?
S11 Cu9 I9 Cu11 -146.82(9) . . . . ?
I11 Cu9 I9 Cu11 -31.92(4) . . . . ?
I10 Cu9 I9 Cu11 95.79(5) . . . . ?
Cu10 Cu9 I9 Cu11 31.81(5) . . . . ?
Cu12 Cu9 I9 Cu11 70.23(4) . . . . ?
S1 Cu11 I9 Cu12 -136.91(9) 2_556 . . . ?
I11 Cu11 I9 Cu12 103.58(5) . . . . ?
I12 Cu11 I9 Cu12 -23.61(4) . . . . ?
Cu10 Cu11 I9 Cu12 40.34(5) . . . . ?
Cu9 Cu11 I9 Cu12 71.32(5) . . . . ?
S1 Cu11 I9 Cu9 151.77(9) 2_556 . . . ?
I11 Cu11 I9 Cu9 32.26(4) . . . . ?
I12 Cu11 I9 Cu9 -94.93(5) . . . . ?
Cu10 Cu11 I9 Cu9 -30.98(5) . . . . ?
Cu12 Cu11 I9 Cu9 -71.32(5) . . . . ?
S12 Cu10 I10 Cu9 -142.10(9) . . . . ?
I12 Cu10 I10 Cu9 101.04(5) . . . . ?
I11 Cu10 I10 Cu9 -22.77(4) . . . . ?
Cu11 Cu10 I10 Cu9 39.70(5) . . . . ?
Cu12 Cu10 I10 Cu9 70.52(4) . . . . ?
S12 Cu10 I10 Cu12 147.38(9) . . . . ?
I12 Cu10 I10 Cu12 30.52(4) . . . . ?
I11 Cu10 I10 Cu12 -93.29(5) . . . . ?
Cu9 Cu10 I10 Cu12 -70.52(4) . . . . ?
Cu11 Cu10 I10 Cu12 -30.82(5) . . . . ?
S11 Cu9 I10 Cu10 137.47(8) . . . . ?
I11 Cu9 I10 Cu10 23.32(5) . . . . ?
I9 Cu9 I10 Cu10 -99.92(5) . . . . ?
Cu12 Cu9 I10 Cu10 -74.76(4) . . . . ?
Cu11 Cu9 I10 Cu10 -37.32(5) . . . . ?
S11 Cu9 I10 Cu12 -147.77(8) . . . . ?
I11 Cu9 I10 Cu12 98.08(5) . . . . ?
I9 Cu9 I10 Cu12 -25.16(4) . . . . ?
Cu10 Cu9 I10 Cu12 74.76(4) . . . . ?
Cu11 Cu9 I10 Cu12 37.44(4) . . . . ?
S9 Cu12 I10 Cu10 -138.82(9) 2_767 . . . ?
I12 Cu12 I10 Cu10 -30.91(4) . . . . ?
I9 Cu12 I10 Cu10 94.89(5) . . . . ?
Cu11 Cu12 I10 Cu10 30.37(5) . . . . ?
Cu9 Cu12 I10 Cu10 69.56(4) . . . . ?
S9 Cu12 I10 Cu9 151.62(9) 2_767 . . . ?
I12 Cu12 I10 Cu9 -100.47(5) . . . . ?
I9 Cu12 I10 Cu9 25.33(4) . . . . ?
Cu11 Cu12 I10 Cu9 -39.19(5) . . . . ?
Cu10 Cu12 I10 Cu9 -69.56(4) . . . . ?
S1 Cu11 I11 Cu9 -144.71(10) 2_556 . . . ?
I12 Cu11 I11 Cu9 93.37(5) . . . . ?
I9 Cu11 I11 Cu9 -32.11(4) . . . . ?
Cu10 Cu11 I11 Cu9 68.88(4) . . . . ?
Cu12 Cu11 I11 Cu9 29.24(5) . . . . ?
S1 Cu11 I11 Cu10 146.41(10) 2_556 . . . ?
I12 Cu11 I11 Cu10 24.49(4) . . . . ?
I9 Cu11 I11 Cu10 -100.99(5) . . . . ?
Cu12 Cu11 I11 Cu10 -39.64(5) . . . . ?
Cu9 Cu11 I11 Cu10 -68.88(4) . . . . ?
S11 Cu9 I11 Cu11 152.85(8) . . . . ?
I10 Cu9 I11 Cu11 -93.64(5) . . . . ?
I9 Cu9 I11 Cu11 32.70(4) . . . . ?
Cu10 Cu9 I11 Cu11 -70.56(4) . . . . ?
Cu12 Cu9 I11 Cu11 -28.93(5) . . . . ?
S11 Cu9 I11 Cu10 -136.59(8) . . . . ?
I10 Cu9 I11 Cu10 -23.08(4) . . . . ?
I9 Cu9 I11 Cu10 103.27(5) . . . . ?
Cu12 Cu9 I11 Cu10 41.63(5) . . . . ?
Cu11 Cu9 I11 Cu10 70.56(4) . . . . ?
S12 Cu10 I11 Cu11 -140.94(8) . . . . ?
I10 Cu10 I11 Cu11 98.40(5) . . . . ?
I12 Cu10 I11 Cu11 -23.23(4) . . . . ?
Cu9 Cu10 I11 Cu11 75.48(4) . . . . ?
Cu12 Cu10 I11 Cu11 36.63(4) . . . . ?
S12 Cu10 I11 Cu9 143.58(8) . . . . ?
I10 Cu10 I11 Cu9 22.91(4) . . . . ?
I12 Cu10 I11 Cu9 -98.71(5) . . . . ?
Cu11 Cu10 I11 Cu9 -75.48(4) . . . . ?
Cu12 Cu10 I11 Cu9 -38.85(5) . . . . ?
S1 Cu11 I12 Cu12 135.01(8) 2_556 . . . ?
I11 Cu11 I12 Cu12 -99.06(6) . . . . ?
I9 Cu11 I12 Cu12 23.38(4) . . . . ?
Cu10 Cu11 I12 Cu12 -74.50(4) . . . . ?
Cu9 Cu11 I12 Cu12 -37.52(4) . . . . ?
S1 Cu11 I12 Cu10 -150.50(8) 2_556 . . . ?
I11 Cu11 I12 Cu10 -24.56(4) . . . . ?
I9 Cu11 I12 Cu10 97.88(5) . . . . ?
Cu12 Cu11 I12 Cu10 74.50(4) . . . . ?
Cu9 Cu11 I12 Cu10 36.97(4) . . . . ?
S9 Cu12 I12 Cu11 -155.38(9) 2_767 . . . ?
I9 Cu12 I12 Cu11 -24.29(4) . . . . ?
I10 Cu12 I12 Cu11 100.59(5) . . . . ?
Cu9 Cu12 I12 Cu11 39.25(5) . . . . ?
Cu10 Cu12 I12 Cu11 70.12(4) . . . . ?
S9 Cu12 I12 Cu10 134.49(9) 2_767 . . . ?
I9 Cu12 I12 Cu10 -94.42(5) . . . . ?
I10 Cu12 I12 Cu10 30.46(4) . . . . ?
Cu11 Cu12 I12 Cu10 -70.12(4) . . . . ?
Cu9 Cu12 I12 Cu10 -30.87(5) . . . . ?
S12 Cu10 I12 Cu11 140.10(8) . . . . ?
I10 Cu10 I12 Cu11 -102.32(5) . . . . ?
I11 Cu10 I12 Cu11 23.18(4) . . . . ?
Cu9 Cu10 I12 Cu11 -39.62(5) . . . . ?
Cu12 Cu10 I12 Cu11 -71.21(4) . . . . ?
S12 Cu10 I12 Cu12 -148.69(8) . . . . ?
I10 Cu10 I12 Cu12 -31.11(4) . . . . ?
I11 Cu10 I12 Cu12 94.39(5) . . . . ?
Cu9 Cu10 I12 Cu12 31.59(5) . . . . ?
Cu11 Cu10 I12 Cu12 71.21(4) . . . . ?
C4 C3 S1 C2 -99.8(9) . . . . ?
C8 C3 S1 C2 84.2(10) . . . . ?
C4 C3 S1 Cu11 131.7(8) . . . 2_556 ?
C8 C3 S1 Cu11 -44.2(10) . . . 2_556 ?
C1 C2 S1 C3 168.3(8) . . . . ?
C1 C2 S1 Cu11 -67.9(9) . . . 2_556 ?
C7 C6 S2 C9 -173.0(8) . . . . ?
C5 C6 S2 C9 11.6(9) . . . . ?
C7 C6 S2 Cu3 -51.2(9) . . . . ?
C5 C6 S2 Cu3 133.4(7) . . . . ?
C10 C9 S2 C6 72.0(10) . . . . ?
C10 C9 S2 Cu3 -48.8(10) . . . . ?
I3 Cu3 S2 C6 -31.8(3) . . . . ?
I4 Cu3 S2 C6 -159.7(3) . . . . ?
Cu4 Cu3 S2 C6 -106.5(4) . . . . ?
I1 Cu3 S2 C6 85.4(3) . . . . ?
Cu1 Cu3 S2 C6 140.0(3) . . . . ?
Cu2 Cu3 S2 C6 39.8(4) . . . . ?
I3 Cu3 S2 C9 86.9(4) . . . . ?
I4 Cu3 S2 C9 -41.0(4) . . . . ?
Cu4 Cu3 S2 C9 12.2(4) . . . . ?
I1 Cu3 S2 C9 -155.9(4) . . . . ?
Cu1 Cu3 S2 C9 -101.3(4) . . . . ?
Cu2 Cu3 S2 C9 158.5(4) . . . . ?
C15 C14 S3 C12 -138.7(9) . . . . ?
C13 C14 S3 C12 45.4(11) . . . . ?
C15 C14 S3 Cu2 105.6(8) . . . . ?
C13 C14 S3 Cu2 -70.3(11) . . . . ?
C11 C12 S3 C14 -177.6(8) . . . . ?
C11 C12 S3 Cu2 -63.1(9) . . . . ?
I2 Cu2 S3 C14 -43.0(4) . . . . ?
I1 Cu2 S3 C14 76.4(4) . . . . ?
I3 Cu2 S3 C14 -162.0(3) . . . . ?
Cu3 Cu2 S3 C14 140.1(4) . . . . ?
Cu4 Cu2 S3 C14 -99.5(4) . . . . ?
Cu1 Cu2 S3 C14 16.0(4) . . . . ?
I2 Cu2 S3 C12 -152.9(4) . . . . ?
I1 Cu2 S3 C12 -33.5(4) . . . . ?
I3 Cu2 S3 C12 88.1(4) . . . . ?
Cu3 Cu2 S3 C12 30.2(4) . . . . ?
Cu4 Cu2 S3 C12 150.5(4) . . . . ?
Cu1 Cu2 S3 C12 -93.9(4) . . . . ?
C23 C18 S4 C17 93.8(11) . . . . ?
C19 C18 S4 C17 -89.4(10) . . . . ?
C23 C18 S4 Cu4 -25.4(11) . . . . ?
C19 C18 S4 Cu4 151.3(8) . . . . ?
C16 C17 S4 C18 -45.5(9) . . . . ?
C16 C17 S4 Cu4 76.6(8) . . . . ?
I2 Cu4 S4 C18 61.3(4) . . . . ?
I4 Cu4 S4 C18 -61.7(4) . . . . ?
I3 Cu4 S4 C18 -179.6(4) . . . . ?
Cu3 Cu4 S4 C18 -124.8(4) . . . . ?
Cu2 Cu4 S4 C18 132.7(4) . . . . ?
Cu1 Cu4 S4 C18 -12.7(5) . . . . ?
I2 Cu4 S4 C17 -54.6(3) . . . . ?
I4 Cu4 S4 C17 -177.6(3) . . . . ?
I3 Cu4 S4 C17 64.6(3) . . . . ?
Cu3 Cu4 S4 C17 119.3(3) . . . . ?
Cu2 Cu4 S4 C17 16.8(4) . . . . ?
Cu1 Cu4 S4 C17 -128.6(4) . . . . ?
C20 C21 S5 C24 -114.6(8) . . . . ?
C22 C21 S5 C24 61.7(9) . . . . ?
C20 C21 S5 Cu5 134.2(8) . . . . ?
C22 C21 S5 Cu5 -49.5(9) . . . . ?
C25 C24 S5 C21 63.3(7) . . . . ?
C25 C24 S5 Cu5 -178.3(6) . . . . ?
I5 Cu5 S5 C21 59.3(3) . . . . ?
I7 Cu5 S5 C21 -71.7(3) . . . . ?
Cu6 Cu5 S5 C21 -12.9(4) . . . . ?
I8 Cu5 S5 C21 173.6(3) . . . . ?
Cu8 Cu5 S5 C21 -133.9(3) . . . . ?
Cu7 Cu5 S5 C21 128.4(3) . . . . ?
I5 Cu5 S5 C24 -49.1(3) . . . . ?
I7 Cu5 S5 C24 179.9(3) . . . . ?
Cu6 Cu5 S5 C24 -121.3(3) . . . . ?
I8 Cu5 S5 C24 65.3(3) . . . . ?
Cu8 Cu5 S5 C24 117.7(3) . . . . ?
Cu7 Cu5 S5 C24 20.0(3) . . . . ?
C33 C28 S6 C27 85.8(9) . . . . ?
C29 C28 S6 C27 -96.8(8) . . . . ?
C33 C28 S6 Cu7 -25.0(9) . . . . ?
C29 C28 S6 Cu7 152.4(7) . . . . ?
C26 C27 S6 C28 176.0(7) . . . . ?
C26 C27 S6 Cu7 -68.9(7) . . . . ?
I8 Cu7 S6 C28 -44.5(3) . . . . ?
I6 Cu7 S6 C28 -164.5(3) . . . . ?
I5 Cu7 S6 C28 74.2(3) . . . . ?
Cu6 Cu7 S6 C28 139.4(3) . . . . ?
Cu8 Cu7 S6 C28 -110.1(3) . . . . ?
Cu5 Cu7 S6 C28 22.0(4) . . . . ?
I8 Cu7 S6 C27 -151.4(3) . . . . ?
I6 Cu7 S6 C27 88.6(3) . . . . ?
I5 Cu7 S6 C27 -32.7(3) . . . . ?
Cu6 Cu7 S6 C27 32.5(4) . . . . ?
Cu8 Cu7 S6 C27 143.0(3) . . . . ?
Cu5 Cu7 S6 C27 -84.9(4) . . . . ?
C35 C34 S7 C31 -177.3(7) . . . . ?
C35 C34 S7 Cu1 68.9(8) . . . 2_756 ?
C30 C31 S7 C34 -88.6(9) . . . . ?
C32 C31 S7 C34 93.4(8) . . . . ?
C30 C31 S7 Cu1 23.3(9) . . . 2_756 ?
C32 C31 S7 Cu1 -154.7(7) . . . 2_756 ?
C43 C38 S8 C37 -33.3(10) . . . . ?
C39 C38 S8 C37 143.6(8) . . . . ?
C43 C38 S8 Cu8 84.4(9) . . . . ?
C39 C38 S8 Cu8 -98.7(7) . . . . ?
C36 C37 S8 C38 -157.1(7) . . . . ?
C36 C37 S8 Cu8 85.3(7) . . . . ?
I6 Cu8 S8 C38 74.8(4) . . . . ?
I8 Cu8 S8 C38 -46.9(4) . . . . ?
I7 Cu8 S8 C38 -170.2(3) . . . . ?
Cu7 Cu8 S8 C38 17.7(4) . . . . ?
Cu5 Cu8 S8 C38 -112.6(4) . . . . ?
Cu6 Cu8 S8 C38 127.2(4) . . . . ?
I6 Cu8 S8 C37 -172.6(3) . . . . ?
I8 Cu8 S8 C37 65.7(3) . . . . ?
I7 Cu8 S8 C37 -57.7(3) . . . . ?
Cu7 Cu8 S8 C37 130.3(3) . . . . ?
Cu5 Cu8 S8 C37 0.0(4) . . . . ?
Cu6 Cu8 S8 C37 -120.2(3) . . . . ?
C40 C41 S9 C44 -149.7(9) . . . . ?
C42 C41 S9 C44 37.8(10) . . . . ?
C40 C41 S9 Cu12 -28.3(10) . . . 2_767 ?
C42 C41 S9 Cu12 159.2(7) . . . 2_767 ?
C45 C44 S9 C41 63.9(9) . . . . ?
C45 C44 S9 Cu12 -58.6(9) . . . 2_767 ?
C53 C48 S10 C47 -155.6(8) . . . . ?
C49 C48 S10 C47 26.1(9) . . . . ?
C53 C48 S10 Cu6 92.1(8) . . . . ?
C49 C48 S10 Cu6 -86.3(8) . . . . ?
C46 C47 S10 C48 -177.2(8) . . . . ?
C46 C47 S10 Cu6 -64.8(8) . . . . ?
I6 Cu6 S10 C48 -54.1(3) . . . . ?
Cu5 Cu6 S10 C48 126.5(3) . . . . ?
I7 Cu6 S10 C48 -170.5(3) . . . . ?
Cu7 Cu6 S10 C48 10.8(4) . . . . ?
I5 Cu6 S10 C48 69.5(3) . . . . ?
Cu8 Cu6 S10 C48 -112.2(3) . . . . ?
I6 Cu6 S10 C47 -164.3(4) . . . . ?
Cu5 Cu6 S10 C47 16.3(4) . . . . ?
I7 Cu6 S10 C47 79.3(4) . . . . ?
Cu7 Cu6 S10 C47 -99.4(4) . . . . ?
I5 Cu6 S10 C47 -40.7(4) . . . . ?
Cu8 Cu6 S10 C47 137.6(4) . . . . ?
C52 C51 S11 C54 -37.1(10) . . . . ?
C50 C51 S11 C54 146.9(8) . . . . ?
C52 C51 S11 Cu9 78.3(9) . . . . ?
C50 C51 S11 Cu9 -97.7(8) . . . . ?
C55 C54 S11 C51 -178.5(7) . . . . ?
C55 C54 S11 Cu9 66.3(7) . . . . ?
I11 Cu9 S11 C51 58.2(3) . . . . ?
I10 Cu9 S11 C51 -63.1(3) . . . . ?
I9 Cu9 S11 C51 174.3(3) . . . . ?
Cu10 Cu9 S11 C51 -3.8(4) . . . . ?
Cu12 Cu9 S11 C51 -118.8(3) . . . . ?
Cu11 Cu9 S11 C51 107.0(3) . . . . ?
I11 Cu9 S11 C54 170.3(3) . . . . ?
I10 Cu9 S11 C54 49.0(3) . . . . ?
I9 Cu9 S11 C54 -73.6(3) . . . . ?
Cu10 Cu9 S11 C54 108.3(3) . . . . ?
Cu12 Cu9 S11 C54 -6.7(4) . . . . ?
Cu11 Cu9 S11 C54 -140.9(3) . . . . ?
C58 C59 S12 C57 -64.3(11) . . . . ?
C60 C59 S12 C57 114.2(9) . . . . ?
C58 C59 S12 Cu10 47.8(10) . . . . ?
C60 C59 S12 Cu10 -133.6(8) . . . . ?
C56 C57 S12 C59 -172.0(9) . . . . ?
C56 C57 S12 Cu10 77.5(9) . . . . ?
I10 Cu10 S12 C59 -82.7(3) . . . . ?
I12 Cu10 S12 C59 33.7(3) . . . . ?
I11 Cu10 S12 C59 153.5(3) . . . . ?
Cu9 Cu10 S12 C59 -146.7(3) . . . . ?
Cu11 Cu10 S12 C59 94.6(4) . . . . ?
Cu12 Cu10 S12 C59 -22.0(4) . . . . ?
I10 Cu10 S12 C57 23.2(4) . . . . ?
I12 Cu10 S12 C57 139.6(4) . . . . ?
I11 Cu10 S12 C57 -100.5(4) . . . . ?
Cu9 Cu10 S12 C57 -40.8(4) . . . . ?
Cu11 Cu10 S12 C57 -159.5(4) . . . . ?
Cu12 Cu10 S12 C57 83.9(4) . . . . ?
