#------------------------------------------------------------------------------
#$Date: 2016-03-26 18:12:22 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180416 $
#$URL: svn://www.crystallography.net/cod/cif/7/20/85/7208551.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7208551
loop_
_publ_author_name
'Liu, Ying-Ying'
'Chen, Chun'
'Ma, Jian-Fang'
'Yang, Jin'
_publ_section_title
;
 A series of complexes constructed by different calix[4]arene derivatives
;
_journal_issue                   19
_journal_name_full               CrystEngComm
_journal_page_first              6201
_journal_paper_doi               10.1039/c2ce25650a
_journal_volume                  14
_journal_year                    2012
_chemical_formula_sum            'C52 H67 Na O16 Zn2'
_chemical_formula_weight         1101.79
_chemical_name_systematic
;
?
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90
_cell_angle_beta                 97.552(2)
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   24.2387(6)
_cell_length_b                   25.4087(7)
_cell_length_c                   18.6362(5)
_cell_measurement_temperature    293(2)
_cell_volume                     11378.0(5)
_computing_cell_refinement       CrysAlis
_computing_data_collection       'CrysAlis (Oxford Diffraction, 2006)'
_computing_data_reduction        CrysAlis
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 10.0
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.846
_diffrn_measurement_device_type  'Oxford Diffraction Gemini R Ultra'
_diffrn_measurement_method       'ω scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0345
_diffrn_reflns_av_sigmaI/netI    0.1279
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -32
_diffrn_reflns_limit_k_max       34
_diffrn_reflns_limit_k_min       -33
_diffrn_reflns_limit_l_max       25
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            25289
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         29.18
_diffrn_reflns_theta_min         3.01
_exptl_absorpt_coefficient_mu    0.914
_exptl_absorpt_correction_T_max  0.8676
_exptl_absorpt_correction_T_min  0.8174
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlis (Oxford Diffraction, 2006)
;
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.286
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             4624
_exptl_crystal_size_max          0.23
_exptl_crystal_size_mid          0.21
_exptl_crystal_size_min          0.16
_refine_diff_density_max         1.446
_refine_diff_density_min         -0.645
_refine_diff_density_rms         0.088
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.823
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     675
_refine_ls_number_reflns         13034
_refine_ls_number_restraints     34
_refine_ls_restrained_S_all      0.823
_refine_ls_R_factor_all          0.1350
_refine_ls_R_factor_gt           0.0619
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1052P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1593
_refine_ls_wR_factor_ref         0.1770
_reflns_number_gt                5513
_reflns_number_total             13034
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c2ce25650a.txt
_cod_data_source_block           12
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7208551
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Zn1 Zn 0.01733(2) 1.10855(2) 0.05857(3) 0.05149(18) Uani 1 1 d .
Zn2 Zn -0.04435(2) 1.01017(2) 0.11049(3) 0.05670(19) Uani 1 1 d .
Na1 Na 0.14678(6) 1.10929(6) 0.13952(8) 0.0412(4) Uani 1 1 d .
C1 C 0.24588(18) 0.99308(16) 0.0890(2) 0.0440(10) Uani 1 1 d .
H1A H 0.2069 0.9994 0.0720 0.053 Uiso 1 1 calc R
H1B H 0.2580 0.9630 0.0631 0.053 Uiso 1 1 calc R
C2 C 0.33803(18) 1.03946(18) 0.0872(2) 0.0500(11) Uani 1 1 d .
H2 H 0.3550 1.0071 0.0983 0.060 Uiso 1 1 calc R
C3 C 0.28013(16) 1.04145(16) 0.0746(2) 0.0414(10) Uani 1 1 d .
C4 C 0.25598(15) 1.09000(16) 0.0560(2) 0.0361(9) Uani 1 1 d .
C5 C 0.28793(16) 1.13532(16) 0.0538(2) 0.0375(9) Uani 1 1 d .
C6 C 0.34500(17) 1.13022(17) 0.0673(2) 0.0444(10) Uani 1 1 d .
H6 H 0.3667 1.1602 0.0649 0.053 Uiso 1 1 calc R
C7 C 0.37155(17) 1.08322(19) 0.0840(2) 0.0505(11) Uani 1 1 d .
C8 C 0.26151(16) 1.18933(15) 0.0407(2) 0.0374(9) Uani 1 1 d .
H8A H 0.2787 1.2077 0.0037 0.045 Uiso 1 1 calc R
H8B H 0.2221 1.1855 0.0237 0.045 Uiso 1 1 calc R
C9 C 0.26905(16) 1.22110(14) 0.1102(2) 0.0358(9) Uani 1 1 d .
C10 C 0.22877(16) 1.22074(14) 0.1574(2) 0.0355(9) Uani 1 1 d .
C11 C 0.23859(16) 1.24270(14) 0.2261(2) 0.0363(9) Uani 1 1 d .
C12 C 0.28844(18) 1.26951(16) 0.2444(2) 0.0440(10) Uani 1 1 d .
H12 H 0.2952 1.2850 0.2899 0.053 Uiso 1 1 calc R
C13 C 0.32883(17) 1.27428(16) 0.1980(2) 0.0419(10) Uani 1 1 d .
C14 C 0.31813(16) 1.24876(16) 0.1315(2) 0.0404(10) Uani 1 1 d .
H14 H 0.3448 1.2502 0.1001 0.048 Uiso 1 1 calc R
C15 C 0.19923(17) 1.23348(16) 0.2813(2) 0.0432(10) Uani 1 1 d .
H15A H 0.1619 1.2275 0.2568 0.052 Uiso 1 1 calc R
H15B H 0.1984 1.2643 0.3118 0.052 Uiso 1 1 calc R
C16 C 0.21840(17) 1.18576(16) 0.3278(2) 0.0422(10) Uani 1 1 d .
C17 C 0.19522(16) 1.13572(16) 0.3170(2) 0.0388(10) Uani 1 1 d .
C18 C 0.22096(18) 1.09164(16) 0.3522(2) 0.0435(10) Uani 1 1 d .
C19 C 0.26812(19) 1.10006(19) 0.4023(2) 0.0509(11) Uani 1 1 d .
H19 H 0.2855 1.0711 0.4260 0.061 Uiso 1 1 calc R
C20 C 0.29021(19) 1.1493(2) 0.4185(2) 0.0535(12) Uani 1 1 d .
C21 C 0.26453(18) 1.19136(17) 0.3806(2) 0.0476(11) Uani 1 1 d .
H21 H 0.2787 1.2250 0.3908 0.057 Uiso 1 1 calc R
C22 C 0.19871(18) 1.03631(16) 0.3379(2) 0.0490(11) Uani 1 1 d .
H22A H 0.1606 1.0383 0.3145 0.059 Uiso 1 1 calc R
H22B H 0.1986 1.0182 0.3836 0.059 Uiso 1 1 calc R
C23 C 0.21853(16) 1.00423(14) 0.2147(2) 0.0399(10) Uani 1 1 d .
C24 C 0.25355(16) 0.98197(15) 0.1694(2) 0.0401(10) Uani 1 1 d .
C25 C 0.29908(18) 0.95343(17) 0.2019(3) 0.0502(11) Uani 1 1 d .
H25 H 0.3218 0.9366 0.1724 0.060 Uiso 1 1 calc R
C26 C 0.31205(18) 0.94902(17) 0.2763(3) 0.0505(11) Uani 1 1 d .
C27 C 0.27956(18) 0.97667(16) 0.3188(2) 0.0477(11) Uani 1 1 d .
H27 H 0.2894 0.9763 0.3688 0.057 Uiso 1 1 calc R
C28 C 0.23302(17) 1.00489(15) 0.2903(2) 0.0442(10) Uani 1 1 d .
C29 C 0.4346(2) 1.0796(2) 0.1017(3) 0.0711(15) Uani 1 1 d .
C30 C 0.4517(7) 1.1118(7) 0.1721(10) 0.170(6) Uani 0.68 1 d PU
C31 C 0.4646(6) 1.1115(6) 0.0466(8) 0.148(5) Uani 0.68 1 d PU
C32 C 0.4504(6) 1.0453(6) 0.1701(8) 0.151(5) Uani 0.68 1 d PU
C34 C 0.4054(5) 0.9572(4) 0.3515(7) 0.096(3) Uani 0.68 1 d PU
C35 C 0.3802(5) 0.8759(4) 0.2560(5) 0.099(4) Uani 0.68 1 d P
C38 C 0.3840(4) 1.1947(4) 0.4504(6) 0.090(3) Uani 0.68 1 d PU
C39 C 0.3211(5) 1.1889(7) 0.5408(6) 0.126(5) Uani 0.68 1 d P
C30' C 0.4651(8) 1.1299(8) 0.1153(11) 0.084(5) Uiso 0.32 1 d P
C31' C 0.4581(7) 1.0391(7) 0.0469(10) 0.071(4) Uiso 0.32 1 d P
C32' C 0.4588(8) 1.0263(8) 0.1009(12) 0.085(5) Uiso 0.32 1 d P
C34' C 0.4144(8) 0.9505(8) 0.3185(12) 0.071(5) Uiso 0.32 1 d P
C35' C 0.4095(17) 0.9101(17) 0.254(2) 0.183(17) Uiso 0.32 1 d P
C38' C 0.3909(9) 1.1689(9) 0.4287(12) 0.087(6) Uiso 0.32 1 d P
C39' C 0.3274(17) 1.1581(14) 0.544(2) 0.141(15) Uiso 0.32 1 d P
C33 C 0.3617(2) 0.9159(2) 0.3109(3) 0.0674(14) Uani 1 1 d .
C36 C 0.3446(3) 0.8827(3) 0.3730(4) 0.104(2) Uani 1 1 d .
H36A H 0.3103 0.8648 0.3569 0.156 Uiso 1 1 calc R
H36B H 0.3397 0.9051 0.4131 0.156 Uiso 1 1 calc R
H36C H 0.3731 0.8572 0.3879 0.156 Uiso 1 1 calc R
C37 C 0.3417(2) 1.1576(2) 0.4755(3) 0.0709(15) Uani 1 1 d .
C40 C 0.3707(3) 1.1053(3) 0.5019(5) 0.139(3) Uani 1 1 d .
C41 C 0.38208(19) 1.30418(19) 0.2218(3) 0.0581(13) Uani 1 1 d .
C42 C 0.4187(2) 1.3098(3) 0.1614(3) 0.0859(18) Uani 1 1 d .
H42A H 0.4521 1.3286 0.1794 0.129 Uiso 1 1 calc R
H42B H 0.3988 1.3288 0.1217 0.129 Uiso 1 1 calc R
H42C H 0.4283 1.2755 0.1453 0.129 Uiso 1 1 calc R
C43 C 0.3687(3) 1.3606(3) 0.2424(4) 0.106(2) Uani 1 1 d .
H43A H 0.4027 1.3792 0.2579 0.159 Uiso 1 1 calc R
H43B H 0.3461 1.3600 0.2811 0.159 Uiso 1 1 calc R
H43C H 0.3488 1.3781 0.2012 0.159 Uiso 1 1 calc R
C44 C 0.4140(3) 1.2767(4) 0.2854(4) 0.150(4) Uani 1 1 d .
H44A H 0.4478 1.2956 0.3006 0.226 Uiso 1 1 calc R
H44B H 0.4227 1.2415 0.2719 0.226 Uiso 1 1 calc R
H44C H 0.3918 1.2755 0.3245 0.226 Uiso 1 1 calc R
C45 C 0.13854(17) 1.23421(17) 0.0989(3) 0.0509(11) Uani 1 1 d .
H45A H 0.1551 1.2518 0.0607 0.061 Uiso 1 1 calc R
H45B H 0.1300 1.2606 0.1333 0.061 Uiso 1 1 calc R
C46 C 0.08617(18) 1.20720(19) 0.0674(3) 0.0500(11) Uani 1 1 d .
C47 C 0.12437(17) 0.98920(16) 0.1840(3) 0.0533(12) Uani 1 1 d .
H47A H 0.1235 0.9755 0.2324 0.064 Uiso 1 1 calc R
H47B H 0.1309 0.9600 0.1527 0.064 Uiso 1 1 calc R
C48 C 0.06870(18) 1.01479(18) 0.1569(2) 0.0486(11) Uani 1 1 d .
C49 C 0.17743(17) 1.08371(19) -0.0324(2) 0.0499(11) Uani 1 1 d .
H49A H 0.2014 1.0584 -0.0519 0.060 Uiso 1 1 calc R
H49B H 0.1787 1.1162 -0.0595 0.060 Uiso 1 1 calc R
C50 C 0.11942(17) 1.06335(16) -0.0420(2) 0.0411(10) Uani 1 1 d .
C51 C 0.09748(16) 1.14974(17) 0.2881(2) 0.0457(11) Uani 1 1 d .
H51A H 0.0728 1.1594 0.2449 0.055 Uiso 1 1 calc R
H51B H 0.1070 1.1817 0.3154 0.055 Uiso 1 1 calc R
C52 C 0.06603(16) 1.11366(17) 0.3335(2) 0.0382(9) Uani 1 1 d .
O1 O 0.17715(10) 1.19704(10) 0.13431(14) 0.0373(6) Uani 1 1 d .
O2 O 0.14743(11) 1.12824(10) 0.26653(14) 0.0403(7) Uani 1 1 d .
O3 O 0.16871(10) 1.02668(10) 0.18492(15) 0.0433(7) Uani 1 1 d .
O4 O 0.19790(10) 1.09336(10) 0.04186(13) 0.0364(6) Uani 1 1 d .
O5 O 0.07607(11) 1.16329(12) 0.08982(16) 0.0497(7) Uani 1 1 d .
O6 O 0.05600(16) 1.23289(16) 0.0197(2) 0.0976(14) Uani 1 1 d .
O9 O 0.06526(11) 1.06188(11) 0.14372(15) 0.0459(7) Uani 1 1 d .
O10 O 0.02853(12) 0.98212(12) 0.1490(2) 0.0735(11) Uani 1 1 d .
O11 O 0.08969(15) 1.07215(17) 0.0050(2) 0.0856(12) Uani 1 1 d .
O12 O 0.10399(12) 1.04092(13) -0.10087(17) 0.0562(8) Uani 1 1 d .
O8 O 0.07296(12) 1.06479(12) 0.32930(17) 0.0531(8) Uani 1 1 d .
O7 O 0.03363(12) 1.13722(12) 0.36886(17) 0.0571(8) Uani 1 1 d .
O2W O -0.0099(6) 1.2461(6) 0.3140(8) 0.173(5) Uiso 0.50 1 d P
O3W O -0.0243(8) 1.2722(8) 0.1423(11) 0.221(7) Uiso 0.50 1 d P
O4W O 0.1189(3) 0.8880(3) 0.0509(4) 0.101(2) Uiso 0.60 1 d P
O4W' O 0.1597(5) 0.8660(4) 0.0182(6) 0.100(3) Uiso 0.40 1 d P
O1W O -0.01168(16) 1.1567(2) -0.0308(2) 0.0912(12) Uani 1 1 d D
H1D H -0.0402(19) 1.170(2) -0.017(4) 0.137 Uiso 1 1 d D
H1C H -0.014(3) 1.1269(16) -0.050(4) 0.137 Uiso 1 1 d D
O13 O -0.03293(15) 1.04990(16) 0.02405(18) 0.0759(11) Uani 1 1 d D
H13 H -0.024(3) 1.066(2) -0.013(2) 0.114 Uiso 1 1 d D
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O13 Zn1 O5 173.14(14) . .
O13 Zn1 O7 94.72(13) . 2
O5 Zn1 O7 91.58(12) . 2
O13 Zn1 O1W 93.04(17) . .
O5 Zn1 O1W 88.70(14) . .
O7 Zn1 O1W 98.36(16) 2 .
O13 Zn1 O9 94.20(15) . .
O5 Zn1 O9 82.95(11) . .
O7 Zn1 O9 91.29(12) 2 .
O1W Zn1 O9 167.42(13) . .
O13 Zn1 O11 91.59(14) . .
O5 Zn1 O11 81.65(12) . .
O7 Zn1 O11 165.09(14) 2 .
O1W Zn1 O11 94.78(17) . .
O9 Zn1 O11 74.76(13) . .
O13 Zn1 Zn2 36.89(10) . .
O5 Zn1 Zn2 143.87(9) . .
O7 Zn1 Zn2 74.34(9) 2 .
O1W Zn1 Zn2 125.70(10) . .
O9 Zn1 Zn2 64.71(7) . .
O11 Zn1 Zn2 103.50(11) . .
O13 Zn1 Na1 131.40(13) . .
O5 Zn1 Na1 43.31(8) . .
O7 Zn1 Na1 108.14(9) 2 .
O1W Zn1 Na1 123.76(10) . .
O9 Zn1 Na1 44.68(8) . .
O11 Zn1 Na1 58.13(10) . .
Zn2 Zn1 Na1 109.12(3) . .
O13 Zn1 H1C 74.0(13) . .
O5 Zn1 H1C 106.1(14) . .
O7 Zn1 H1C 111.7(14) 2 .
O1W Zn1 H1C 22.8(7) . .
O9 Zn1 H1C 154.6(9) . .
O11 Zn1 H1C 83.0(15) . .
Zn2 Zn1 H1C 110.0(14) . .
Na1 Zn1 H1C 129.8(18) . .
O13 Zn1 H13 25.4(16) . .
O5 Zn1 H13 151.9(17) . .
O7 Zn1 H13 111.0(17) 2 .
O1W Zn1 H13 71.7(13) . .
O9 Zn1 H13 112.3(16) . .
O11 Zn1 H13 79.8(18) . .
Zn2 Zn1 H13 62.2(15) . .
Na1 Zn1 H13 135(2) . .
H1C Zn1 H13 50.4(14) . .
O12 Zn2 O13 117.15(14) 5_575 .
O12 Zn2 O10 114.73(14) 5_575 .
O13 Zn2 O10 105.82(16) . .
O12 Zn2 O8 102.19(12) 5_575 2
O13 Zn2 O8 101.82(15) . 2
O10 Zn2 O8 114.69(14) . 2
O12 Zn2 Zn1 152.75(10) 5_575 .
O13 Zn2 Zn1 37.48(10) . .
O10 Zn2 Zn1 87.66(10) . .
O8 Zn2 Zn1 80.30(9) 2 .
O5 Na1 O3 144.99(11) . .
O5 Na1 O9 74.34(11) . .
O3 Na1 O9 70.78(10) . .
O5 Na1 O1 68.77(10) . .
O3 Na1 O1 145.24(11) . .
O9 Na1 O1 139.83(11) . .
O5 Na1 O4 103.34(11) . .
O3 Na1 O4 90.45(10) . .
O9 Na1 O4 118.06(11) . .
O1 Na1 O4 86.11(10) . .
O5 Na1 O2 100.65(11) . .
O3 Na1 O2 81.37(10) . .
O9 Na1 O2 88.07(10) . .
O1 Na1 O2 83.67(10) . .
O4 Na1 O2 148.38(11) . .
O5 Na1 O11 66.02(12) . .
O3 Na1 O11 94.77(12) . .
O9 Na1 O11 62.81(10) . .
O1 Na1 O11 113.21(12) . .
O4 Na1 O11 60.75(10) . .
O2 Na1 O11 149.95(11) . .
O5 Na1 C48 94.09(12) . .
O3 Na1 C48 50.90(11) . .
O9 Na1 C48 20.25(10) . .
O1 Na1 C48 159.44(11) . .
O4 Na1 C48 109.64(11) . .
O2 Na1 C48 88.71(11) . .
O11 Na1 C48 66.70(12) . .
O5 Na1 C46 19.90(10) . .
O3 Na1 C46 164.67(12) . .
O9 Na1 C46 94.24(12) . .
O1 Na1 C46 49.90(11) . .
O4 Na1 C46 93.99(11) . .
O2 Na1 C46 101.93(12) . .
O11 Na1 C46 74.79(13) . .
C48 Na1 C46 113.91(13) . .
O5 Na1 Zn1 37.17(7) . .
O3 Na1 Zn1 108.85(8) . .
O9 Na1 Zn1 41.45(8) . .
O1 Na1 Zn1 105.69(8) . .
O4 Na1 Zn1 102.12(8) . .
O2 Na1 Zn1 109.44(8) . .
O11 Na1 Zn1 43.57(8) . .
C48 Na1 Zn1 59.09(9) . .
C46 Na1 Zn1 55.86(9) . .
C24 C1 C3 109.0(3) . .
C24 C1 H1A 109.9 . .
C3 C1 H1A 109.9 . .
C24 C1 H1B 109.9 . .
C3 C1 H1B 109.9 . .
H1A C1 H1B 108.3 . .
C7 C2 C3 123.2(4) . .
C7 C2 H2 118.4 . .
C3 C2 H2 118.4 . .
C4 C3 C2 117.2(4) . .
C4 C3 C1 122.5(4) . .
C2 C3 C1 120.0(4) . .
C3 C4 C5 121.6(4) . .
C3 C4 O4 118.8(3) . .
C5 C4 O4 119.6(4) . .
C6 C5 C4 117.8(4) . .
C6 C5 C8 120.3(4) . .
C4 C5 C8 121.8(4) . .
C7 C6 C5 123.5(4) . .
C7 C6 H6 118.2 . .
C5 C6 H6 118.2 . .
C6 C7 C2 116.7(4) . .
C6 C7 C29 121.9(4) . .
C2 C7 C29 121.4(4) . .
C9 C8 C5 110.0(3) . .
C9 C8 H8A 109.7 . .
C5 C8 H8A 109.7 . .
C9 C8 H8B 109.7 . .
C5 C8 H8B 109.7 . .
H8A C8 H8B 108.2 . .
C14 C9 C10 117.7(4) . .
C14 C9 C8 121.0(3) . .
C10 C9 C8 121.2(3) . .
C11 C10 C9 121.9(4) . .
C11 C10 O1 119.6(3) . .
C9 C10 O1 118.5(3) . .
C10 C11 C12 117.5(3) . .
C10 C11 C15 121.2(4) . .
C12 C11 C15 121.0(4) . .
C11 C12 C13 123.2(4) . .
C11 C12 H12 118.4 . .
C13 C12 H12 118.4 . .
C14 C13 C12 116.6(4) . .
C14 C13 C41 123.2(4) . .
C12 C13 C41 120.1(4) . .
C13 C14 C9 122.8(4) . .
C13 C14 H14 118.6 . .
C9 C14 H14 118.6 . .
C11 C15 C16 109.7(3) . .
C11 C15 H15A 109.7 . .
C16 C15 H15A 109.7 . .
C11 C15 H15B 109.7 . .
C16 C15 H15B 109.7 . .
H15A C15 H15B 108.2 . .
C17 C16 C21 117.7(4) . .
C17 C16 C15 123.7(4) . .
C21 C16 C15 118.4(4) . .
C16 C17 C18 121.0(4) . .
C16 C17 O2 120.1(4) . .
C18 C17 O2 118.8(4) . .
C19 C18 C17 117.8(4) . .
C19 C18 C22 120.1(4) . .
C17 C18 C22 122.2(4) . .
C20 C19 C18 123.1(4) . .
C20 C19 H19 118.4 . .
C18 C19 H19 118.4 . .
C19 C20 C21 117.0(4) . .
C19 C20 C37 122.1(4) . .
C21 C20 C37 120.9(4) . .
C20 C21 C16 123.0(4) . .
C20 C21 H21 118.5 . .
C16 C21 H21 118.5 . .
C18 C22 C28 112.4(3) . .
C18 C22 H22A 109.1 . .
C28 C22 H22A 109.1 . .
C18 C22 H22B 109.1 . .
C28 C22 H22B 109.1 . .
H22A C22 H22B 107.9 . .
O3 C23 C24 119.5(4) . .
O3 C23 C28 119.1(3) . .
C24 C23 C28 121.3(4) . .
C25 C24 C23 117.4(4) . .
C25 C24 C1 121.0(4) . .
C23 C24 C1 121.3(4) . .
C26 C25 C24 122.7(4) . .
C26 C25 H25 118.6 . .
C24 C25 H25 118.6 . .
C27 C26 C25 117.5(4) . .
C27 C26 C33 120.7(4) . .
C25 C26 C33 121.7(4) . .
C26 C27 C28 122.8(4) . .
C26 C27 H27 118.6 . .
C28 C27 H27 118.6 . .
C27 C28 C23 117.6(4) . .
C27 C28 C22 122.0(4) . .
C23 C28 C22 120.4(4) . .
C32' C29 C30' 127.1(11) . .
C32' C29 C7 116.2(9) . .
C30' C29 C7 116.6(9) . .
C32' C29 C32 55.7(9) . .
C30' C29 C32 106.3(10) . .
C7 C29 C32 110.1(7) . .
C32' C29 C30 115.4(11) . .
C30' C29 C30 48.0(9) . .
C7 C29 C30 107.3(7) . .
C32 C29 C30 66.0(8) . .
C32' C29 C31 104.5(10) . .
C30' C29 C31 53.1(9) . .
C7 C29 C31 111.6(7) . .
C32 C29 C31 138.3(8) . .
C30 C29 C31 100.7(9) . .
C32' C29 C31' 39.8(8) . .
C30' C29 C31' 116.8(11) . .
C7 C29 C31' 109.4(7) . .
C32 C29 C31' 95.3(9) . .
C30 C29 C31' 142.8(9) . .
C31 C29 C31' 71.3(9) . .
C30' C30 C29 62.9(13) . .
C30' C30 C32 111.0(16) . .
C29 C30 C32 56.9(8) . .
C30' C31 C29 60.5(11) . .
C30' C31 C31' 109.3(14) . .
C29 C31 C31' 55.5(8) . .
C32' C32 C29 59.5(10) . .
C32' C32 C30 110.8(14) . .
C29 C32 C30 57.2(8) . .
C34' C34 C33 72(2) . .
C35' C35 C33 76(2) . .
C38' C38 C37 80.7(19) . .
C39' C39 C37 59(3) . .
C30 C30' C31 135(2) . .
C30 C30' C29 69.1(13) . .
C31 C30' C29 66.4(11) . .
C32' C31' C29 63.5(14) . .
C32' C31' C31 108.6(18) . .
C29 C31' C31 53.2(7) . .
C31' C32' C32 141(2) . .
C31' C32' C29 76.7(16) . .
C32 C32' C29 64.8(11) . .
C34 C34' C33 82(2) . .
C34 C34' C35' 146(3) . .
C33 C34' C35' 65.3(17) . .
C35 C35' C34' 117(3) . .
C35 C35' C33 63(2) . .
C34' C35' C33 56.3(16) . .
C38 C38' C37 69.5(18) . .
C39 C39' C37 90(4) . .
C39 C39' C40 139(5) . .
C37 C39' C40 52.8(14) . .
C36 C33 C26 110.1(4) . .
C36 C33 C34' 123.3(9) . .
C26 C33 C34' 108.7(8) . .
C36 C33 C35 105.5(6) . .
C26 C33 C35 111.1(5) . .
C34' C33 C35 97.2(10) . .
C36 C33 C34 103.4(6) . .
C26 C33 C34 105.7(5) . .
C34' C33 C34 25.6(7) . .
C35 C33 C34 120.6(7) . .
C36 C33 C35' 135.1(15) . .
C26 C33 C35' 110.3(15) . .
C34' C33 C35' 58.4(15) . .
C35 C33 C35' 40.6(14) . .
C34 C33 C35' 83.7(15) . .
C33 C36 H36A 109.5 . .
C33 C36 H36B 109.5 . .
H36A C36 H36B 109.5 . .
C33 C36 H36C 109.5 . .
H36A C36 H36C 109.5 . .
H36B C36 H36C 109.5 . .
C39' C37 C38 123.4(18) . .
C39' C37 C20 111.2(17) . .
C38 C37 C20 113.1(5) . .
C39' C37 C40 82.7(15) . .
C38 C37 C40 109.6(6) . .
C20 C37 C40 113.0(5) . .
C39' C37 C39 30.2(15) . .
C38 C37 C39 102.6(9) . .
C20 C37 C39 106.7(6) . .
C40 C37 C39 111.2(8) . .
C39' C37 C38' 144.2(19) . .
C38 C37 C38' 29.8(8) . .
C20 C37 C38' 104.0(9) . .
C40 C37 C38' 89.3(9) . .
C39 C37 C38' 131.6(12) . .
C37 C40 C39' 44.5(12) . .
C44 C41 C13 109.3(4) . .
C44 C41 C42 109.7(5) . .
C13 C41 C42 112.7(4) . .
C44 C41 C43 110.0(6) . .
C13 C41 C43 110.1(4) . .
C42 C41 C43 105.1(4) . .
C41 C42 H42A 109.5 . .
C41 C42 H42B 109.5 . .
H42A C42 H42B 109.5 . .
C41 C42 H42C 109.5 . .
H42A C42 H42C 109.5 . .
H42B C42 H42C 109.5 . .
C41 C43 H43A 109.5 . .
C41 C43 H43B 109.5 . .
H43A C43 H43B 109.5 . .
C41 C43 H43C 109.5 . .
H43A C43 H43C 109.5 . .
H43B C43 H43C 109.5 . .
C41 C44 H44A 109.5 . .
C41 C44 H44B 109.5 . .
H44A C44 H44B 109.5 . .
C41 C44 H44C 109.5 . .
H44A C44 H44C 109.5 . .
H44B C44 H44C 109.5 . .
O1 C45 C46 110.4(3) . .
O1 C45 H45A 109.6 . .
C46 C45 H45A 109.6 . .
O1 C45 H45B 109.6 . .
C46 C45 H45B 109.6 . .
H45A C45 H45B 108.1 . .
O5 C46 O6 126.1(4) . .
O5 C46 C45 118.7(4) . .
O6 C46 C45 115.1(4) . .
O5 C46 Na1 39.5(2) . .
O6 C46 Na1 157.1(4) . .
C45 C46 Na1 82.5(2) . .
O3 C47 C48 110.5(3) . .
O3 C47 H47A 109.6 . .
C48 C47 H47A 109.6 . .
O3 C47 H47B 109.6 . .
C48 C47 H47B 109.6 . .
H47A C47 H47B 108.1 . .
O9 C48 O10 125.7(4) . .
O9 C48 C47 121.2(4) . .
O10 C48 C47 113.0(4) . .
O9 C48 Na1 41.17(19) . .
O10 C48 Na1 163.9(4) . .
C47 C48 Na1 80.7(2) . .
O4 C49 C50 112.3(3) . .
O4 C49 H49A 109.1 . .
C50 C49 H49A 109.1 . .
O4 C49 H49B 109.1 . .
C50 C49 H49B 109.1 . .
H49A C49 H49B 107.9 . .
O11 C50 O12 125.1(4) . .
O11 C50 C49 119.1(4) . .
O12 C50 C49 115.7(4) . .
O2 C51 C52 115.5(3) . .
O2 C51 H51A 108.4 . .
C52 C51 H51A 108.4 . .
O2 C51 H51B 108.4 . .
C52 C51 H51B 108.4 . .
H51A C51 H51B 107.5 . .
O7 C52 O8 127.4(4) . .
O7 C52 C51 113.8(4) . .
O8 C52 C51 118.8(3) . .
C10 O1 C45 111.2(3) . .
C10 O1 Na1 131.6(2) . .
C45 O1 Na1 117.1(2) . .
C17 O2 C51 114.4(3) . .
C17 O2 Na1 125.6(2) . .
C51 O2 Na1 117.0(2) . .
C23 O3 C47 110.1(3) . .
C23 O3 Na1 132.2(2) . .
C47 O3 Na1 117.7(2) . .
C4 O4 C49 112.6(3) . .
C4 O4 Na1 118.7(2) . .
C49 O4 Na1 128.6(2) . .
C46 O5 Zn1 133.8(3) . .
C46 O5 Na1 120.6(3) . .
Zn1 O5 Na1 99.52(13) . .
C48 O9 Zn1 133.8(3) . .
C48 O9 Na1 118.6(3) . .
Zn1 O9 Na1 93.87(11) . .
C48 O10 Zn2 116.5(3) . .
C50 O11 Zn1 158.2(4) . .
C50 O11 Na1 115.1(3) . .
Zn1 O11 Na1 78.29(11) . .
C50 O12 Zn2 121.5(3) . 5_575
C52 O8 Zn2 127.0(3) . 2
C52 O7 Zn1 130.3(3) . 2
Zn1 O1W H1D 101(6) . .
Zn1 O1W H1C 79(6) . .
H1D O1W H1C 118(4) . .
Zn2 O13 Zn1 105.63(15) . .
Zn2 O13 H13 173(5) . .
Zn1 O13 H13 72(5) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Zn1 O13 1.978(3) .
Zn1 O5 2.021(3) .
Zn1 O7 2.080(3) 2
Zn1 O1W 2.112(5) .
Zn1 O9 2.188(3) .
Zn1 O11 2.322(4) .
Zn1 Zn2 3.1303(8) .
Zn1 Na1 3.2981(16) .
Zn1 H1C 2.12(8) .
Zn1 H13 1.90(7) .
Zn2 O12 1.934(3) 5_575
Zn2 O13 1.951(4) .
Zn2 O10 1.952(3) .
Zn2 O8 1.967(3) 2
Na1 O5 2.294(3) .
Na1 O3 2.299(3) .
Na1 O9 2.324(3) .
Na1 O1 2.354(3) .
Na1 O4 2.367(3) .
Na1 O2 2.413(3) .
Na1 O11 2.860(4) .
Na1 C48 3.100(5) .
Na1 C46 3.104(5) .
C1 C24 1.513(6) .
C1 C3 1.526(6) .
C1 H1A 0.9700 .
C1 H1B 0.9700 .
C2 C7 1.383(6) .
C2 C3 1.393(6) .
C2 H2 0.9300 .
C3 C4 1.390(6) .
C4 C5 1.391(5) .
C4 O4 1.400(4) .
C5 C6 1.379(5) .
C5 C8 1.521(5) .
C6 C7 1.373(6) .
C6 H6 0.9300 .
C7 C29 1.524(6) .
C8 C9 1.516(5) .
C8 H8A 0.9700 .
C8 H8B 0.9700 .
C9 C14 1.394(5) .
C9 C10 1.398(5) .
C10 C11 1.387(5) .
C10 O1 1.404(4) .
C11 C12 1.390(6) .
C11 C15 1.510(5) .
C12 C13 1.395(6) .
C12 H12 0.9300 .
C13 C14 1.391(6) .
C13 C41 1.513(6) .
C14 H14 0.9300 .
C15 C16 1.527(6) .
C15 H15A 0.9700 .
C15 H15B 0.9700 .
C16 C17 1.394(6) .
C16 C21 1.396(6) .
C17 C18 1.402(6) .
C17 O2 1.406(5) .
C18 C19 1.395(6) .
C18 C22 1.517(6) .
C19 C20 1.377(6) .
C19 H19 0.9300 .
C20 C21 1.384(6) .
C20 C37 1.545(7) .
C21 H21 0.9300 .
C22 C28 1.519(6) .
C22 H22A 0.9700 .
C22 H22B 0.9700 .
C23 O3 1.384(5) .
C23 C24 1.394(6) .
C23 C28 1.406(6) .
C24 C25 1.391(6) .
C25 C26 1.386(6) .
C25 H25 0.9300 .
C26 C27 1.381(6) .
C26 C33 1.539(6) .
C27 C28 1.382(6) .
C27 H27 0.9300 .
C29 C32' 1.48(2) .
C29 C30' 1.48(2) .
C29 C32 1.550(16) .
C29 C30 1.555(18) .
C29 C31 1.559(15) .
C29 C31' 1.604(18) .
C30 C30' 1.24(2) .
C30 C32 1.69(2) .
C31 C30' 1.36(2) .
C31 C31' 1.85(2) .
C32 C32' 1.42(2) .
C34 C34' 0.70(2) .
C34 C33 1.608(12) .
C35 C35' 1.13(4) .
C35 C33 1.550(10) .
C38 C38' 0.80(2) .
C38 C37 1.512(11) .
C39 C39' 0.80(4) .
C39 C37 1.589(12) .
C31' C32' 1.06(2) .
C34' C33 1.54(2) .
C34' C35' 1.58(4) .
C35' C33 1.68(4) .
C38' C37 1.59(2) .
C39' C37 1.37(4) .
C39' C40 1.93(4) .
C33 C36 1.533(8) .
C36 H36A 0.9600 .
C36 H36B 0.9600 .
C36 H36C 0.9600 .
C37 C40 1.553(9) .
C41 C44 1.499(8) .
C41 C42 1.529(7) .
C41 C43 1.530(8) .
C42 H42A 0.9600 .
C42 H42B 0.9600 .
C42 H42C 0.9600 .
C43 H43A 0.9600 .
C43 H43B 0.9600 .
C43 H43C 0.9600 .
C44 H44A 0.9600 .
C44 H44B 0.9600 .
C44 H44C 0.9600 .
C45 O1 1.429(5) .
C45 C46 1.494(6) .
C45 H45A 0.9700 .
C45 H45B 0.9700 .
C46 O5 1.228(5) .
C46 O6 1.256(5) .
C47 O3 1.434(5) .
C47 C48 1.523(6) .
C47 H47A 0.9700 .
C47 H47B 0.9700 .
C48 O9 1.222(5) .
C48 O10 1.273(5) .
C49 O4 1.429(5) .
C49 C50 1.487(6) .
C49 H49A 0.9700 .
C49 H49B 0.9700 .
C50 O11 1.226(5) .
C50 O12 1.249(5) .
C51 O2 1.433(4) .
C51 C52 1.519(5) .
C51 H51A 0.9700 .
C51 H51B 0.9700 .
C52 O7 1.244(5) .
C52 O8 1.257(5) .
O12 Zn2 1.934(3) 5_575
O8 Zn2 1.967(3) 2
O7 Zn1 2.080(3) 2
O2W O3W 1.270(19) 2
O3W O2W 1.270(19) 2
O4W O4W' 1.350(12) .
O1W H1D 0.841(19) .
O1W H1C 0.835(19) .
O13 H13 0.86(2) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O13 Zn1 Zn2 O12 -26.5(3) . 5_575
O5 Zn1 Zn2 O12 164.9(2) . 5_575
O7 Zn1 Zn2 O12 94.5(2) 2 5_575
O1W Zn1 Zn2 O12 5.4(3) . 5_575
O9 Zn1 Zn2 O12 -166.4(2) . 5_575
O11 Zn1 Zn2 O12 -100.7(2) . 5_575
Na1 Zn1 Zn2 O12 -161.3(2) . 5_575
O5 Zn1 Zn2 O13 -168.5(2) . .
O7 Zn1 Zn2 O13 121.1(2) 2 .
O1W Zn1 Zn2 O13 31.9(3) . .
O9 Zn1 Zn2 O13 -139.8(2) . .
O11 Zn1 Zn2 O13 -74.2(2) . .
Na1 Zn1 Zn2 O13 -134.8(2) . .
O13 Zn1 Zn2 O10 120.1(2) . .
O5 Zn1 Zn2 O10 -48.43(19) . .
O7 Zn1 Zn2 O10 -118.84(15) 2 .
O1W Zn1 Zn2 O10 152.0(2) . .
O9 Zn1 Zn2 O10 -19.74(14) . .
O11 Zn1 Zn2 O10 45.90(15) . .
Na1 Zn1 Zn2 O10 -14.66(12) . .
O13 Zn1 Zn2 O8 -124.4(2) . 2
O5 Zn1 Zn2 O8 67.11(17) . 2
O7 Zn1 Zn2 O8 -3.31(13) 2 2
O1W Zn1 Zn2 O8 -92.4(2) . 2
O9 Zn1 Zn2 O8 95.79(12) . 2
O11 Zn1 Zn2 O8 161.44(14) . 2
Na1 Zn1 Zn2 O8 100.88(10) . 2
O13 Zn1 Na1 O5 173.92(17) . .
O7 Zn1 Na1 O5 -72.23(16) 2 .
O1W Zn1 Na1 O5 41.5(2) . .
O9 Zn1 Na1 O5 -144.92(17) . .
O11 Zn1 Na1 O5 114.22(18) . .
Zn2 Zn1 Na1 O5 -151.46(13) . .
O13 Zn1 Na1 O3 -16.93(16) . .
O5 Zn1 Na1 O3 169.15(16) . .
O7 Zn1 Na1 O3 96.92(13) 2 .
O1W Zn1 Na1 O3 -149.32(19) . .
O9 Zn1 Na1 O3 24.24(13) . .
O11 Zn1 Na1 O3 -76.63(15) . .
Zn2 Zn1 Na1 O3 17.70(9) . .
O13 Zn1 Na1 O9 -41.17(16) . .
O5 Zn1 Na1 O9 144.92(17) . .
O7 Zn1 Na1 O9 72.68(14) 2 .
O1W Zn1 Na1 O9 -173.6(2) . .
O11 Zn1 Na1 O9 -100.87(17) . .
Zn2 Zn1 Na1 O9 -6.54(11) . .
O13 Zn1 Na1 O1 167.08(14) . .
O5 Zn1 Na1 O1 -6.83(14) . .
O7 Zn1 Na1 O1 -79.07(12) 2 .
O1W Zn1 Na1 O1 34.69(19) . .
O9 Zn1 Na1 O1 -151.75(14) . .
O11 Zn1 Na1 O1 107.38(15) . .
Zn2 Zn1 Na1 O1 -158.29(7) . .
O13 Zn1 Na1 O4 77.76(15) . .
O5 Zn1 Na1 O4 -96.16(15) . .
O7 Zn1 Na1 O4 -168.39(12) 2 .
O1W Zn1 Na1 O4 -54.64(19) . .
O9 Zn1 Na1 O4 118.92(14) . .
O11 Zn1 Na1 O4 18.06(14) . .
Zn2 Zn1 Na1 O4 112.38(8) . .
O13 Zn1 Na1 O2 -104.19(15) . .
O5 Zn1 Na1 O2 81.89(15) . .
O7 Zn1 Na1 O2 9.65(13) 2 .
O1W Zn1 Na1 O2 123.41(19) . .
O9 Zn1 Na1 O2 -63.03(13) . .
O11 Zn1 Na1 O2 -163.89(16) . .
Zn2 Zn1 Na1 O2 -69.57(8) . .
O13 Zn1 Na1 O11 59.70(18) . .
O5 Zn1 Na1 O11 -114.22(18) . .
O7 Zn1 Na1 O11 173.55(16) 2 .
O1W Zn1 Na1 O11 -72.7(2) . .
O9 Zn1 Na1 O11 100.87(17) . .
Zn2 Zn1 Na1 O11 94.33(13) . .
O13 Zn1 Na1 C48 -28.04(15) . .
O5 Zn1 Na1 C48 158.05(16) . .
O7 Zn1 Na1 C48 85.81(13) 2 .
O1W Zn1 Na1 C48 -160.4(2) . .
O9 Zn1 Na1 C48 13.13(14) . .
O11 Zn1 Na1 C48 -87.74(16) . .
Zn2 Zn1 Na1 C48 6.59(9) . .
O13 Zn1 Na1 C46 164.34(16) . .
O5 Zn1 Na1 C46 -9.57(16) . .
O7 Zn1 Na1 C46 -81.81(14) 2 .
O1W Zn1 Na1 C46 32.0(2) . .
O9 Zn1 Na1 C46 -154.49(15) . .
O11 Zn1 Na1 C46 104.65(17) . .
Zn2 Zn1 Na1 C46 -161.03(11) . .
C7 C2 C3 C4 1.9(6) . .
C7 C2 C3 C1 -171.8(4) . .
C24 C1 C3 C4 -106.8(4) . .
C24 C1 C3 C2 66.5(5) . .
C2 C3 C4 C5 -3.4(6) . .
C1 C3 C4 C5 170.2(4) . .
C2 C3 C4 O4 179.0(3) . .
C1 C3 C4 O4 -7.4(6) . .
C3 C4 C5 C6 3.1(6) . .
O4 C4 C5 C6 -179.3(3) . .
C3 C4 C5 C8 -173.9(3) . .
O4 C4 C5 C8 3.7(5) . .
C4 C5 C6 C7 -1.3(6) . .
C8 C5 C6 C7 175.8(4) . .
C5 C6 C7 C2 -0.1(6) . .
C5 C6 C7 C29 -177.4(4) . .
C3 C2 C7 C6 -0.2(6) . .
C3 C2 C7 C29 177.1(4) . .
C6 C5 C8 C9 -69.5(4) . .
C4 C5 C8 C9 107.5(4) . .
C5 C8 C9 C14 83.4(4) . .
C5 C8 C9 C10 -92.1(4) . .
C14 C9 C10 C11 -5.9(6) . .
C8 C9 C10 C11 169.8(3) . .
C14 C9 C10 O1 174.5(3) . .
C8 C9 C10 O1 -9.8(5) . .
C9 C10 C11 C12 5.6(6) . .
O1 C10 C11 C12 -174.8(3) . .
C9 C10 C11 C15 -168.7(4) . .
O1 C10 C11 C15 10.9(5) . .
C10 C11 C12 C13 -1.3(6) . .
C15 C11 C12 C13 173.0(4) . .
C11 C12 C13 C14 -2.5(6) . .
C11 C12 C13 C41 179.9(4) . .
C12 C13 C14 C9 2.1(6) . .
C41 C13 C14 C9 179.7(4) . .
C10 C9 C14 C13 1.9(6) . .
C8 C9 C14 C13 -173.8(4) . .
C10 C11 C15 C16 92.3(4) . .
C12 C11 C15 C16 -81.9(5) . .
C11 C15 C16 C17 -99.8(4) . .
C11 C15 C16 C21 74.9(5) . .
C21 C16 C17 C18 -6.9(5) . .
C15 C16 C17 C18 167.9(3) . .
C21 C16 C17 O2 177.5(3) . .
C15 C16 C17 O2 -7.7(5) . .
C16 C17 C18 C19 4.7(5) . .
O2 C17 C18 C19 -179.7(3) . .
C16 C17 C18 C22 -176.1(3) . .
O2 C17 C18 C22 -0.4(5) . .
C17 C18 C19 C20 0.0(6) . .
C22 C18 C19 C20 -179.3(4) . .
C18 C19 C20 C21 -2.1(6) . .
C18 C19 C20 C37 178.6(4) . .
C19 C20 C21 C16 -0.3(6) . .
C37 C20 C21 C16 179.0(4) . .
C17 C16 C21 C20 4.7(6) . .
C15 C16 C21 C20 -170.4(4) . .
C19 C18 C22 C28 -76.8(5) . .
C17 C18 C22 C28 104.0(4) . .
O3 C23 C24 C25 -171.1(3) . .
C28 C23 C24 C25 9.6(5) . .
O3 C23 C24 C1 15.1(5) . .
C28 C23 C24 C1 -164.2(4) . .
C3 C1 C24 C25 -83.6(4) . .
C3 C1 C24 C23 89.9(4) . .
C23 C24 C25 C26 -3.6(6) . .
C1 C24 C25 C26 170.2(4) . .
C24 C25 C26 C27 -3.4(6) . .
C24 C25 C26 C33 178.2(4) . .
C25 C26 C27 C28 4.8(6) . .
C33 C26 C27 C28 -176.8(4) . .
C26 C27 C28 C23 0.9(6) . .
C26 C27 C28 C22 -178.3(4) . .
O3 C23 C28 C27 172.3(3) . .
C24 C23 C28 C27 -8.3(6) . .
O3 C23 C28 C22 -8.5(5) . .
C24 C23 C28 C22 170.8(4) . .
C18 C22 C28 C27 86.9(5) . .
C18 C22 C28 C23 -92.2(5) . .
C6 C7 C29 C32' -165.4(10) . .
C2 C7 C29 C32' 17.5(11) . .
C6 C7 C29 C30' 12.6(11) . .
C2 C7 C29 C30' -164.5(10) . .
C6 C7 C29 C32 133.8(7) . .
C2 C7 C29 C32 -43.3(8) . .
C6 C7 C29 C30 63.7(9) . .
C2 C7 C29 C30 -113.4(8) . .
C6 C7 C29 C31 -45.7(8) . .
C2 C7 C29 C31 137.1(7) . .
C6 C7 C29 C31' -122.7(8) . .
C2 C7 C29 C31' 60.2(9) . .
C32' C29 C30 C30' 118.1(15) . .
C7 C29 C30 C30' -110.6(13) . .
C32 C29 C30 C30' 144.6(15) . .
C31 C29 C30 C30' 6.2(14) . .
C31' C29 C30 C30' 79(2) . .
C32' C29 C30 C32 -26.5(12) . .
C30' C29 C30 C32 -144.6(15) . .
C7 C29 C30 C32 104.8(8) . .
C31 C29 C30 C32 -138.4(9) . .
C31' C29 C30 C32 -65.2(17) . .
C32' C29 C31 C30' -125.8(13) . .
C7 C29 C31 C30' 107.8(11) . .
C32 C29 C31 C30' -71.6(16) . .
C30 C29 C31 C30' -5.8(13) . .
C31' C29 C31 C30' -148.2(13) . .
C32' C29 C31 C31' 22.3(11) . .
C30' C29 C31 C31' 148.2(13) . .
C7 C29 C31 C31' -104.0(8) . .
C32 C29 C31 C31' 76.6(14) . .
C30 C29 C31 C31' 142.4(10) . .
C30' C29 C32 C32' -124.2(13) . .
C7 C29 C32 C32' 108.7(11) . .
C30 C29 C32 C32' -150.8(13) . .
C31 C29 C32 C32' -72.0(16) . .
C31' C29 C32 C32' -4.2(12) . .
C32' C29 C32 C30 150.8(13) . .
C30' C29 C32 C30 26.6(11) . .
C7 C29 C32 C30 -100.6(8) . .
C31 C29 C32 C30 78.8(14) . .
C31' C29 C32 C30 146.6(10) . .
C30' C30 C32 C32' -7(2) . .
C29 C30 C32 C32' 26.7(12) . .
C30' C30 C32 C29 -33.5(14) . .
C29 C30 C30' C31 -10(2) . .
C32 C30 C30' C31 21(3) . .
C32 C30 C30' C29 31.3(12) . .
C29 C31 C30' C30 10(2) . .
C31' C31 C30' C30 -17(3) . .
C31' C31 C30' C29 -27.4(11) . .
C32' C29 C30' C30 -92.5(17) . .
C7 C29 C30' C30 89.8(13) . .
C32 C29 C30' C30 -33.4(14) . .
C31 C29 C30' C30 -172.3(17) . .
C31' C29 C30' C30 -138.3(13) . .
C32' C29 C30' C31 79.9(16) . .
C7 C29 C30' C31 -97.9(10) . .
C32 C29 C30' C31 138.9(10) . .
C30 C29 C30' C31 172.3(17) . .
C31' C29 C30' C31 34.1(14) . .
C30' C29 C31' C32' 116.7(17) . .
C7 C29 C31' C32' -108.1(15) . .
C32 C29 C31' C32' 5.4(16) . .
C30 C29 C31' C32' 62(2) . .
C31 C29 C31' C32' 144.9(16) . .
C32' C29 C31' C31 -144.9(16) . .
C30' C29 C31' C31 -28.2(12) . .
C7 C29 C31' C31 107.0(7) . .
C32 C29 C31' C31 -139.5(9) . .
C30 C29 C31' C31 -83.1(16) . .
C30' C31 C31' C32' -4(2) . .
C29 C31 C31' C32' -32.9(15) . .
C30' C31 C31' C29 29.1(12) . .
C29 C31' C32' C32 -9(3) . .
C31 C31' C32' C32 20(4) . .
C31 C31' C32' C29 29.1(12) . .
C29 C32 C32' C31' 10(3) . .
C30 C32 C32' C31' -16(4) . .
C30 C32 C32' C29 -26.0(11) . .
C30' C29 C32' C31' -88.6(19) . .
C7 C29 C32' C31' 89.2(15) . .
C32 C29 C32' C31' -173.5(19) . .
C30 C29 C32' C31' -143.9(14) . .
C31 C29 C32' C31' -34.2(16) . .
C30' C29 C32' C32 84.8(15) . .
C7 C29 C32' C32 -97.4(10) . .
C30 C29 C32' C32 29.6(13) . .
C31 C29 C32' C32 139.2(10) . .
C31' C29 C32' C32 173.5(19) . .
C33 C34 C34' C35' -17(5) . .
C33 C35 C35' C34' 18(3) . .
C34 C34' C35' C35 0(8) . .
C33 C34' C35' C35 -19(3) . .
C34 C34' C35' C33 19(5) . .
C37 C39 C39' C40 23(4) . .
C27 C26 C33 C36 46.1(6) . .
C25 C26 C33 C36 -135.6(5) . .
C27 C26 C33 C34' -91.6(10) . .
C25 C26 C33 C34' 86.7(10) . .
C27 C26 C33 C35 162.6(7) . .
C25 C26 C33 C35 -19.1(8) . .
C27 C26 C33 C34 -64.9(7) . .
C25 C26 C33 C34 113.4(6) . .
C27 C26 C33 C35' -153.9(16) . .
C25 C26 C33 C35' 24.4(17) . .
C34 C34' C33 C36 -43(2) . .
C35' C34' C33 C36 126.2(18) . .
C34 C34' C33 C26 88(2) . .
C35' C34' C33 C26 -102.9(18) . .
C34 C34' C33 C35 -157(2) . .
C35' C34' C33 C35 12.3(18) . .
C35' C34' C33 C34 170(3) . .
C34 C34' C33 C35' -170(3) . .
C35' C35 C33 C36 -144(2) . .
C35' C35 C33 C26 97(2) . .
C35' C35 C33 C34' -16(2) . .
C35' C35 C33 C34 -27(2) . .
C34' C34 C33 C36 144(2) . .
C34' C34 C33 C26 -100(2) . .
C34' C34 C33 C35 26(2) . .
C34' C34 C33 C35' 9(3) . .
C35 C35' C33 C36 54(3) . .
C34' C35' C33 C36 -107.2(19) . .
C35 C35' C33 C26 -99.1(19) . .
C34' C35' C33 C26 99.9(13) . .
C35 C35' C33 C34' 161(3) . .
C34' C35' C33 C35 -161(3) . .
C35 C35' C33 C34 156(2) . .
C34' C35' C33 C34 -4.5(13) . .
C39 C39' C37 C38 52(4) . .
C40 C39' C37 C38 -108.7(12) . .
C39 C39' C37 C20 -87(4) . .
C40 C39' C37 C20 111.9(8) . .
C39 C39' C37 C40 161(4) . .
C40 C39' C37 C39 -161(4) . .
C39 C39' C37 C38' 83(5) . .
C40 C39' C37 C38' -78(3) . .
C38' C38 C37 C39' 144(3) . .
C38' C38 C37 C20 -77.7(19) . .
C38' C38 C37 C40 49(2) . .
C38' C38 C37 C39 167.7(19) . .
C19 C20 C37 C39' -81.4(17) . .
C21 C20 C37 C39' 99.4(17) . .
C19 C20 C37 C38 134.9(6) . .
C21 C20 C37 C38 -44.3(8) . .
C19 C20 C37 C40 9.6(7) . .
C21 C20 C37 C40 -169.7(5) . .
C19 C20 C37 C39 -113.0(9) . .
C21 C20 C37 C39 67.8(9) . .
C19 C20 C37 C38' 104.9(10) . .
C21 C20 C37 C38' -74.4(10) . .
C39' C39 C37 C38 -137(4) . .
C39' C39 C37 C20 104(4) . .
C39' C39 C37 C40 -20(4) . .
C39' C39 C37 C38' -129(4) . .
C38 C38' C37 C39' -58(4) . .
C38 C38' C37 C20 112.1(17) . .
C38 C38' C37 C40 -134.3(18) . .
C38 C38' C37 C39 -16(2) . .
C38 C37 C40 C39' 122.9(18) . .
C20 C37 C40 C39' -110.0(18) . .
C39 C37 C40 C39' 10(2) . .
C38' C37 C40 C39' 145.0(19) . .
C39 C39' C40 C37 -30(6) . .
C14 C13 C41 C44 -114.1(6) . .
C12 C13 C41 C44 63.4(7) . .
C14 C13 C41 C42 8.1(7) . .
C12 C13 C41 C42 -174.5(4) . .
C14 C13 C41 C43 125.0(5) . .
C12 C13 C41 C43 -57.5(6) . .
O1 C45 C46 O5 18.7(6) . .
O1 C45 C46 O6 -162.0(4) . .
O1 C45 C46 Na1 2.6(3) . .
O3 Na1 C46 O5 12.6(7) . .
O9 Na1 C46 O5 0.6(3) . .
O1 Na1 C46 O5 -159.4(4) . .
O4 Na1 C46 O5 119.1(3) . .
O2 Na1 C46 O5 -88.4(3) . .
O11 Na1 C46 O5 60.9(3) . .
C48 Na1 C46 O5 5.6(4) . .
Zn1 Na1 C46 O5 17.2(3) . .
O5 Na1 C46 O6 -60.7(8) . .
O3 Na1 C46 O6 -48.1(11) . .
O9 Na1 C46 O6 -60.1(9) . .
O1 Na1 C46 O6 139.9(9) . .
O4 Na1 C46 O6 58.4(9) . .
O2 Na1 C46 O6 -149.1(8) . .
O11 Na1 C46 O6 0.2(8) . .
C48 Na1 C46 O6 -55.1(9) . .
Zn1 Na1 C46 O6 -43.5(8) . .
O5 Na1 C46 C45 157.5(5) . .
O3 Na1 C46 C45 170.1(4) . .
O9 Na1 C46 C45 158.0(3) . .
O1 Na1 C46 C45 -1.9(2) . .
O4 Na1 C46 C45 -83.4(3) . .
O2 Na1 C46 C45 69.1(3) . .
O11 Na1 C46 C45 -141.6(3) . .
C48 Na1 C46 C45 163.0(2) . .
Zn1 Na1 C46 C45 174.7(3) . .
O3 C47 C48 O9 -4.7(6) . .
O3 C47 C48 O10 174.2(4) . .
O3 C47 C48 Na1 3.0(3) . .
O5 Na1 C48 O9 -12.7(3) . .
O3 Na1 C48 O9 167.8(4) . .
O1 Na1 C48 O9 19.9(5) . .
O4 Na1 C48 O9 -118.4(3) . .
O2 Na1 C48 O9 87.9(3) . .
O11 Na1 C48 O9 -74.3(3) . .
C46 Na1 C48 O9 -14.6(3) . .
Zn1 Na1 C48 O9 -25.7(3) . .
O5 Na1 C48 O10 27.6(11) . .
O3 Na1 C48 O10 -151.9(12) . .
O9 Na1 C48 O10 40.3(10) . .
O1 Na1 C48 O10 60.2(13) . .
O4 Na1 C48 O10 -78.1(11) . .
O2 Na1 C48 O10 128.2(11) . .
O11 Na1 C48 O10 -34.0(11) . .
C46 Na1 C48 O10 25.7(12) . .
Zn1 Na1 C48 O10 14.5(11) . .
O5 Na1 C48 C47 177.3(3) . .
O3 Na1 C48 C47 -2.2(2) . .
O9 Na1 C48 C47 -170.1(5) . .
O1 Na1 C48 C47 -150.2(3) . .
O4 Na1 C48 C47 71.5(3) . .
O2 Na1 C48 C47 -82.1(3) . .
O11 Na1 C48 C47 115.6(3) . .
C46 Na1 C48 C47 175.4(3) . .
Zn1 Na1 C48 C47 164.2(3) . .
O4 C49 C50 O11 22.8(6) . .
O4 C49 C50 O12 -161.4(4) . .
O2 C51 C52 O7 159.6(4) . .
O2 C51 C52 O8 -23.5(5) . .
C11 C10 O1 C45 90.3(4) . .
C9 C10 O1 C45 -90.1(4) . .
C11 C10 O1 Na1 -92.8(4) . .
C9 C10 O1 Na1 86.8(4) . .
C46 C45 O1 C10 173.6(3) . .
C46 C45 O1 Na1 -3.7(4) . .
O5 Na1 O1 C10 178.1(3) . .
O3 Na1 O1 C10 9.2(4) . .
O9 Na1 O1 C10 153.5(3) . .
O4 Na1 O1 C10 -76.0(3) . .
O2 Na1 O1 C10 74.1(3) . .
O11 Na1 O1 C10 -131.8(3) . .
C48 Na1 O1 C10 142.9(4) . .
C46 Na1 O1 C10 -174.5(3) . .
Zn1 Na1 O1 C10 -177.5(3) . .
O5 Na1 O1 C45 -5.2(3) . .
O3 Na1 O1 C45 -174.1(3) . .
O9 Na1 O1 C45 -29.8(3) . .
O4 Na1 O1 C45 100.8(3) . .
O2 Na1 O1 C45 -109.2(3) . .
O11 Na1 O1 C45 45.0(3) . .
C48 Na1 O1 C45 -40.3(5) . .
C46 Na1 O1 C45 2.2(3) . .
Zn1 Na1 O1 C45 -0.8(3) . .
C16 C17 O2 C51 -71.0(4) . .
C18 C17 O2 C51 113.3(4) . .
C16 C17 O2 Na1 88.6(4) . .
C18 C17 O2 Na1 -87.1(4) . .
C52 C51 O2 C17 -87.3(4) . .
C52 C51 O2 Na1 111.2(3) . .
O5 Na1 O2 C17 -137.4(3) . .
O3 Na1 O2 C17 78.1(3) . .
O9 Na1 O2 C17 149.0(3) . .
O1 Na1 O2 C17 -70.4(3) . .
O4 Na1 O2 C17 1.5(4) . .
O11 Na1 O2 C17 162.7(3) . .
C48 Na1 O2 C17 128.7(3) . .
C46 Na1 O2 C17 -117.1(3) . .
Zn1 Na1 O2 C17 -174.9(3) . .
O5 Na1 O2 C51 21.8(3) . .
O3 Na1 O2 C51 -122.7(2) . .
O9 Na1 O2 C51 -51.9(3) . .
O1 Na1 O2 C51 88.8(2) . .
O4 Na1 O2 C51 160.7(3) . .
O11 Na1 O2 C51 -38.1(4) . .
C48 Na1 O2 C51 -72.1(3) . .
C46 Na1 O2 C51 42.1(3) . .
Zn1 Na1 O2 C51 -15.7(3) . .
C24 C23 O3 C47 94.8(4) . .
C28 C23 O3 C47 -85.8(4) . .
C24 C23 O3 Na1 -85.2(4) . .
C28 C23 O3 Na1 94.1(4) . .
C48 C47 O3 C23 175.5(4) . .
C48 C47 O3 Na1 -4.5(5) . .
O5 Na1 O3 C23 -178.2(3) . .
O9 Na1 O3 C23 -172.9(3) . .
O1 Na1 O3 C23 -16.4(4) . .
O4 Na1 O3 C23 67.4(3) . .
O2 Na1 O3 C23 -81.9(3) . .
O11 Na1 O3 C23 128.1(3) . .
C48 Na1 O3 C23 -177.3(4) . .
C46 Na1 O3 C23 174.4(5) . .
Zn1 Na1 O3 C23 170.4(3) . .
O5 Na1 O3 C47 1.8(4) . .
O9 Na1 O3 C47 7.1(3) . .
O1 Na1 O3 C47 163.6(3) . .
O4 Na1 O3 C47 -112.6(3) . .
O2 Na1 O3 C47 98.0(3) . .
O11 Na1 O3 C47 -52.0(3) . .
C48 Na1 O3 C47 2.6(3) . .
C46 Na1 O3 C47 -5.7(6) . .
Zn1 Na1 O3 C47 -9.7(3) . .
C3 C4 O4 C49 -89.0(4) . .
C5 C4 O4 C49 93.4(4) . .
C3 C4 O4 Na1 88.1(4) . .
C5 C4 O4 Na1 -89.5(4) . .
C50 C49 O4 C4 153.9(4) . .
C50 C49 O4 Na1 -22.8(5) . .
O5 Na1 O4 C4 142.9(2) . .
O3 Na1 O4 C4 -69.5(3) . .
O9 Na1 O4 C4 -137.9(2) . .
O1 Na1 O4 C4 75.8(2) . .
O2 Na1 O4 C4 4.6(4) . .
O11 Na1 O4 C4 -164.8(3) . .
C48 Na1 O4 C4 -117.7(3) . .
C46 Na1 O4 C4 125.2(3) . .
Zn1 Na1 O4 C4 -178.9(2) . .
O5 Na1 O4 C49 -40.5(3) . .
O3 Na1 O4 C49 107.0(3) . .
O9 Na1 O4 C49 38.7(3) . .
O1 Na1 O4 C49 -107.6(3) . .
O2 Na1 O4 C49 -178.8(3) . .
O11 Na1 O4 C49 11.8(3) . .
C48 Na1 O4 C49 58.9(3) . .
C46 Na1 O4 C49 -58.3(3) . .
Zn1 Na1 O4 C49 -2.4(3) . .
O6 C46 O5 Zn1 8.7(8) . .
C45 C46 O5 Zn1 -172.1(3) . .
Na1 C46 O5 Zn1 -146.5(5) . .
O6 C46 O5 Na1 155.1(4) . .
C45 C46 O5 Na1 -25.7(6) . .
O13 Zn1 O5 C46 109.4(12) . .
O7 Zn1 O5 C46 -93.7(4) 2 .
O1W Zn1 O5 C46 4.6(4) . .
O9 Zn1 O5 C46 175.2(4) . .
O11 Zn1 O5 C46 99.7(4) . .
Zn2 Zn1 O5 C46 -158.9(3) . .
Na1 Zn1 O5 C46 151.2(5) . .
O13 Zn1 O5 Na1 -41.7(12) . .
O7 Zn1 O5 Na1 115.13(13) 2 .
O1W Zn1 O5 Na1 -146.54(17) . .
O9 Zn1 O5 Na1 24.03(11) . .
O11 Zn1 O5 Na1 -51.52(14) . .
Zn2 Zn1 O5 Na1 49.96(19) . .
O3 Na1 O5 C46 -174.2(3) . .
O9 Na1 O5 C46 -179.4(4) . .
O1 Na1 O5 C46 16.8(3) . .
O4 Na1 O5 C46 -63.6(4) . .
O2 Na1 O5 C46 95.6(3) . .
O11 Na1 O5 C46 -112.7(4) . .
C48 Na1 O5 C46 -174.9(3) . .
Zn1 Na1 O5 C46 -156.1(4) . .
O3 Na1 O5 Zn1 -18.1(3) . .
O9 Na1 O5 Zn1 -23.28(11) . .
O1 Na1 O5 Zn1 172.94(14) . .
O4 Na1 O5 Zn1 92.55(12) . .
O2 Na1 O5 Zn1 -108.21(12) . .
O11 Na1 O5 Zn1 43.47(12) . .
C48 Na1 O5 Zn1 -18.76(13) . .
C46 Na1 O5 Zn1 156.1(4) . .
O10 C48 O9 Zn1 -38.3(7) . .
C47 C48 O9 Zn1 140.4(4) . .
Na1 C48 O9 Zn1 128.9(4) . .
O10 C48 O9 Na1 -167.2(4) . .
C47 C48 O9 Na1 11.5(5) . .
O13 Zn1 O9 C48 13.5(4) . .
O5 Zn1 O9 C48 -160.2(4) . .
O7 Zn1 O9 C48 108.4(4) 2 .
O1W Zn1 O9 C48 -111.4(8) . .
O11 Zn1 O9 C48 -77.0(4) . .
Zn2 Zn1 O9 C48 36.4(3) . .
Na1 Zn1 O9 C48 -136.8(4) . .
O13 Zn1 O9 Na1 150.33(12) . .
O5 Zn1 O9 Na1 -23.40(11) . .
O7 Zn1 O9 Na1 -114.84(12) 2 .
O1W Zn1 O9 Na1 25.4(7) . .
O11 Zn1 O9 Na1 59.82(12) . .
Zn2 Zn1 O9 Na1 173.17(11) . .
O5 Na1 O9 C48 166.9(3) . .
O3 Na1 O9 C48 -10.0(3) . .
O1 Na1 O9 C48 -169.3(3) . .
O4 Na1 O9 C48 69.9(3) . .
O2 Na1 O9 C48 -91.5(3) . .
O11 Na1 O9 C48 96.2(3) . .
C46 Na1 O9 C48 166.7(3) . .
Zn1 Na1 O9 C48 145.7(4) . .
O5 Na1 O9 Zn1 21.14(10) . .
O3 Na1 O9 Zn1 -155.71(13) . .
O1 Na1 O9 Zn1 44.9(2) . .
O4 Na1 O9 Zn1 -75.87(13) . .
O2 Na1 O9 Zn1 122.77(10) . .
O11 Na1 O9 Zn1 -49.56(12) . .
C48 Na1 O9 Zn1 -145.7(4) . .
C46 Na1 O9 Zn1 20.94(13) . .
O9 C48 O10 Zn2 1.4(6) . .
C47 C48 O10 Zn2 -177.5(3) . .
Na1 C48 O10 Zn2 -30.3(13) . .
O12 Zn2 O10 C48 -179.2(3) 5_575 .
O13 Zn2 O10 C48 50.1(4) . .
O8 Zn2 O10 C48 -61.3(4) 2 .
Zn1 Zn2 O10 C48 16.9(3) . .
O12 C50 O11 Zn1 -64.7(11) . .
C49 C50 O11 Zn1 110.6(8) . .
O12 C50 O11 Na1 170.6(3) . .
C49 C50 O11 Na1 -14.1(5) . .
O13 Zn1 O11 C50 89.9(9) . .
O5 Zn1 O11 C50 -91.3(9) . .
O7 Zn1 O11 C50 -155.0(7) 2 .
O1W Zn1 O11 C50 -3.3(9) . .
O9 Zn1 O11 C50 -176.2(9) . .
Zn2 Zn1 O11 C50 125.2(9) . .
Na1 Zn1 O11 C50 -130.5(9) . .
O13 Zn1 O11 Na1 -139.62(14) . .
O5 Zn1 O11 Na1 39.22(10) . .
O7 Zn1 O11 Na1 -24.5(6) 2 .
O1W Zn1 O11 Na1 127.20(13) . .
O9 Zn1 O11 Na1 -45.70(10) . .
Zn2 Zn1 O11 Na1 -104.32(7) . .
O5 Na1 O11 C50 124.7(4) . .
O3 Na1 O11 C50 -85.7(4) . .
O9 Na1 O11 C50 -151.2(4) . .
O1 Na1 O11 C50 73.2(4) . .
O4 Na1 O11 C50 2.2(3) . .
O2 Na1 O11 C50 -166.7(3) . .
C48 Na1 O11 C50 -129.2(4) . .
C46 Na1 O11 C50 105.8(4) . .
Zn1 Na1 O11 C50 161.8(4) . .
O5 Na1 O11 Zn1 -37.09(10) . .
O3 Na1 O11 Zn1 112.49(12) . .
O9 Na1 O11 Zn1 46.97(10) . .
O1 Na1 O11 Zn1 -88.63(12) . .
O4 Na1 O11 Zn1 -159.67(16) . .
O2 Na1 O11 Zn1 31.5(3) . .
C48 Na1 O11 Zn1 68.97(12) . .
C46 Na1 O11 Zn1 -56.08(12) . .
O11 C50 O12 Zn2 -28.5(6) . 5_575
C49 C50 O12 Zn2 156.0(3) . 5_575
O7 C52 O8 Zn2 -11.0(6) . 2
C51 C52 O8 Zn2 172.6(3) . 2
O8 C52 O7 Zn1 5.5(7) . 2
C51 C52 O7 Zn1 -177.9(3) . 2
O12 Zn2 O13 Zn1 166.71(14) 5_575 .
O10 Zn2 O13 Zn1 -64.0(2) . .
O8 Zn2 O13 Zn1 56.24(19) 2 .
O5 Zn1 O13 Zn2 100.9(11) . .
O7 Zn1 O13 Zn2 -55.86(19) 2 .
O1W Zn1 O13 Zn2 -154.5(2) . .
O9 Zn1 O13 Zn2 35.78(18) . .
O11 Zn1 O13 Zn2 110.61(18) . .
Na1 Zn1 O13 Zn2 63.43(19) . .
