#------------------------------------------------------------------------------
#$Date: 2016-03-26 18:26:27 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180429 $
#$URL: svn://www.crystallography.net/cod/cif/7/20/98/7209825.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7209825
loop_
_publ_author_name
'Pettinari, Claudio'
'Marchetti, Fabio'
'Orbisaglia, Serena'
'Pettinari, Riccardo'
'Ngoune, Jean'
'Gómez, Margarita'
'Santos, Carina'
'Álvarez, Eleuterio'
_publ_section_title
;
 Group 11 complexes with the bidentate di(1H-indazol-1-yl)methane and
 di(2H-indazol-2-yl)methane) ligands
;
_journal_issue                   19
_journal_name_full               CrystEngComm
_journal_page_first              3892
_journal_paper_doi               10.1039/c3ce40355f
_journal_volume                  15
_journal_year                    2013
_chemical_formula_moiety         'C30 H24 Ag N8, N O3'
_chemical_formula_sum            'C30 H24 Ag N9 O3'
_chemical_formula_weight         666.45
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 95.6670(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   11.1130(3)
_cell_length_b                   12.0540(3)
_cell_length_c                   20.2158(5)
_cell_measurement_reflns_used    7408
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      29.51
_cell_measurement_theta_min      2.60
_cell_volume                     2694.79(12)
_computing_cell_refinement       'APEX2 Software Suite (Bruker, 2007)'
_computing_data_collection       'APEX2 Software Suite (Bruker, 2007)'
_computing_data_reduction        'APEX2 Software Suite (Bruker, 2007)'
_computing_molecular_graphics    'SHELXTL (Sheldrick, 2008)'
_computing_publication_material  'SHELXTL and publCIF (Westrip, 2010)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 2008)'
_computing_structure_solution    'SIR2002 (Burla et al., 2003)'
_diffrn_ambient_temperature      173(2)
_diffrn_detector_area_resol_mean 8.26
_diffrn_measured_fraction_theta_full 0.985
_diffrn_measured_fraction_theta_max 0.985
_diffrn_measurement_device_type
;
Bruker-Nonius X8kappa APEX II CCD area detector
;
_diffrn_measurement_method       'phi and omega scans with narrow frames'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0317
_diffrn_reflns_av_sigmaI/netI    0.0257
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            23453
_diffrn_reflns_theta_full        25.25
_diffrn_reflns_theta_max         25.25
_diffrn_reflns_theta_min         1.84
_diffrn_standards_decay_%        0
_exptl_absorpt_coefficient_mu    0.801
_exptl_absorpt_correction_T_max  0.8962
_exptl_absorpt_correction_T_min  0.8826
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
APEX2 Software Suite; Bruker 2005.
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.643
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             1352
_exptl_crystal_size_max          0.16
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.14
_refine_diff_density_max         0.544
_refine_diff_density_min         -0.462
_refine_diff_density_rms         0.057
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.040
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     388
_refine_ls_number_reflns         4695
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.040
_refine_ls_R_factor_all          0.0358
_refine_ls_R_factor_gt           0.0273
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0303P)²+1.6519P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0634
_refine_ls_wR_factor_ref         0.0663
_reflns_number_gt                3968
_reflns_number_total             4695
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3ce40355f.txt
_cod_data_source_block           11
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7209825
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 0.903776(17) 0.182135(17) 0.081147(9) 0.03084(8) Uani 1 1 d .
N1 N 0.75570(16) 0.12658(15) -0.05766(9) 0.0207(4) Uani 1 1 d .
N2 N 0.86822(16) 0.11045(15) -0.02465(9) 0.0222(4) Uani 1 1 d .
N3 N 0.66429(17) 0.27823(16) -0.00403(9) 0.0226(4) Uani 1 1 d .
N4 N 0.74061(18) 0.31269(17) 0.04924(10) 0.0271(5) Uani 1 1 d .
N5 N 1.17182(17) 0.22723(16) 0.15769(9) 0.0225(4) Uani 1 1 d .
N6 N 1.11987(17) 0.21099(16) 0.09407(9) 0.0251(4) Uani 1 1 d .
N7 N 1.01884(17) 0.20038(15) 0.23327(9) 0.0214(4) Uani 1 1 d .
N8 N 0.91740(17) 0.16654(16) 0.19461(10) 0.0256(4) Uani 1 1 d .
C1 C 0.9414(2) 0.08703(18) -0.07032(11) 0.0220(5) Uani 1 1 d .
H1 H 1.0251 0.0713 -0.0611 0.026 Uiso 1 1 calc R
C2 C 0.8787(2) 0.08842(18) -0.13480(11) 0.0211(5) Uani 1 1 d .
C3 C 0.9106(2) 0.06976(19) -0.19954(12) 0.0278(6) Uani 1 1 d .
H3 H 0.9908 0.0496 -0.2071 0.033 Uiso 1 1 calc R
C4 C 0.8227(3) 0.0815(2) -0.25114(13) 0.0334(6) Uani 1 1 d .
H4 H 0.8423 0.0699 -0.2953 0.040 Uiso 1 1 calc R
C5 C 0.7033(3) 0.1105(2) -0.24022(13) 0.0343(6) Uani 1 1 d .
H5 H 0.6449 0.1194 -0.2775 0.041 Uiso 1 1 calc R
C6 C 0.6686(2) 0.12636(19) -0.17761(12) 0.0279(6) Uani 1 1 d .
H6 H 0.5875 0.1437 -0.1705 0.033 Uiso 1 1 calc R
C7 C 0.7589(2) 0.11569(17) -0.12493(11) 0.0208(5) Uani 1 1 d .
C8 C 0.7411(2) 0.4217(2) 0.04691(12) 0.0292(6) Uani 1 1 d .
H8 H 0.7857 0.4676 0.0788 0.035 Uiso 1 1 calc R
C9 C 0.6670(2) 0.4626(2) -0.00881(12) 0.0249(5) Uani 1 1 d .
C10 C 0.6356(2) 0.5676(2) -0.03571(13) 0.0315(6) Uani 1 1 d .
H10 H 0.6652 0.6335 -0.0141 0.038 Uiso 1 1 calc R
C11 C 0.5615(2) 0.5724(2) -0.09366(13) 0.0339(6) Uani 1 1 d .
H11 H 0.5409 0.6425 -0.1131 0.041 Uiso 1 1 calc R
C12 C 0.5151(2) 0.4752(2) -0.12508(13) 0.0351(6) Uani 1 1 d .
H12 H 0.4637 0.4815 -0.1653 0.042 Uiso 1 1 calc R
C13 C 0.5415(2) 0.3713(2) -0.09966(12) 0.0302(6) Uani 1 1 d .
H13 H 0.5081 0.3060 -0.1205 0.036 Uiso 1 1 calc R
C14 C 0.6202(2) 0.36733(19) -0.04141(11) 0.0221(5) Uani 1 1 d .
C15 C 0.6579(2) 0.16172(18) -0.02076(12) 0.0232(5) Uani 1 1 d .
H15A H 0.6598 0.1177 0.0207 0.028 Uiso 1 1 calc R
H15B H 0.5801 0.1466 -0.0474 0.028 Uiso 1 1 calc R
C16 C 1.2042(2) 0.16628(19) 0.06090(12) 0.0234(5) Uani 1 1 d .
H16 H 1.1927 0.1456 0.0154 0.028 Uiso 1 1 calc R
C17 C 1.3136(2) 0.15326(18) 0.10184(11) 0.0210(5) Uani 1 1 d .
C18 C 1.4306(2) 0.11519(19) 0.09239(12) 0.0249(5) Uani 1 1 d .
H18 H 1.4487 0.0875 0.0505 0.030 Uiso 1 1 calc R
C19 C 1.5173(2) 0.1194(2) 0.14534(13) 0.0290(6) Uani 1 1 d .
H19 H 1.5970 0.0949 0.1399 0.035 Uiso 1 1 calc R
C20 C 1.4909(2) 0.1593(2) 0.20787(13) 0.0299(6) Uani 1 1 d .
H20 H 1.5534 0.1606 0.2435 0.036 Uiso 1 1 calc R
C21 C 1.3780(2) 0.19635(19) 0.21883(12) 0.0254(5) Uani 1 1 d .
H21 H 1.3606 0.2228 0.2611 0.030 Uiso 1 1 calc R
C22 C 1.2897(2) 0.19310(17) 0.16443(11) 0.0201(5) Uani 1 1 d .
C23 C 0.8501(2) 0.1129(2) 0.23411(12) 0.0272(5) Uani 1 1 d .
H23 H 0.7747 0.0791 0.2199 0.033 Uiso 1 1 calc R
C24 C 0.9042(2) 0.11193(19) 0.30047(12) 0.0243(5) Uani 1 1 d .
C25 C 0.8717(2) 0.0713(2) 0.36156(13) 0.0317(6) Uani 1 1 d .
H25 H 0.7982 0.0319 0.3641 0.038 Uiso 1 1 calc R
C26 C 0.9493(2) 0.0904(2) 0.41704(13) 0.0344(6) Uani 1 1 d .
H26 H 0.9289 0.0644 0.4589 0.041 Uiso 1 1 calc R
C27 C 1.0585(2) 0.1474(2) 0.41370(13) 0.0318(6) Uani 1 1 d .
H27 H 1.1097 0.1591 0.4535 0.038 Uiso 1 1 calc R
C28 C 1.0940(2) 0.18711(19) 0.35497(12) 0.0260(5) Uani 1 1 d .
H28 H 1.1690 0.2242 0.3530 0.031 Uiso 1 1 calc R
C29 C 1.0139(2) 0.16996(18) 0.29830(11) 0.0211(5) Uani 1 1 d .
C30 C 1.1014(2) 0.27725(19) 0.20602(11) 0.0228(5) Uani 1 1 d .
H30A H 1.0544 0.3398 0.1849 0.027 Uiso 1 1 calc R
H30B H 1.1570 0.3078 0.2428 0.027 Uiso 1 1 calc R
O1 O 0.3101(2) 0.3809(2) 0.32780(11) 0.0697(8) Uani 1 1 d .
O2 O 0.2311(2) 0.46491(18) 0.40479(13) 0.0676(7) Uani 1 1 d .
O3 O 0.3737(2) 0.3555(4) 0.42756(15) 0.1175(14) Uani 1 1 d .
N9 N 0.30481(17) 0.40036(16) 0.38686(10) 0.0251(4) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
N8 Ag1 N2 152.45(7)
N8 Ag1 N6 86.38(7)
N2 Ag1 N6 103.41(6)
N8 Ag1 N4 106.95(7)
N2 Ag1 N4 86.66(7)
N6 Ag1 N4 129.87(7)
C7 N1 N2 110.93(18)
C7 N1 C15 129.6(2)
N2 N1 C15 119.18(18)
C1 N2 N1 106.56(18)
C1 N2 Ag1 131.95(15)
N1 N2 Ag1 117.57(13)
N4 N3 C14 110.80(19)
N4 N3 C15 119.45(19)
C14 N3 C15 128.6(2)
C8 N4 N3 106.22(19)
C8 N4 Ag1 130.46(16)
N3 N4 Ag1 113.53(14)
C22 N5 N6 111.18(18)
C22 N5 C30 129.56(19)
N6 N5 C30 119.25(18)
C16 N6 N5 106.30(18)
C16 N6 Ag1 129.38(16)
N5 N6 Ag1 116.38(13)
N8 N7 C29 111.02(18)
N8 N7 C30 119.32(19)
C29 N7 C30 128.5(2)
C23 N8 N7 106.58(19)
C23 N8 Ag1 131.45(16)
N7 N8 Ag1 121.08(14)
N2 C1 C2 111.1(2)
N2 C1 H1 124.4
C2 C1 H1 124.4
C7 C2 C3 119.9(2)
C7 C2 C1 105.00(19)
C3 C2 C1 135.1(2)
C4 C3 C2 117.9(2)
C4 C3 H3 121.1
C2 C3 H3 121.1
C3 C4 C5 121.3(2)
C3 C4 H4 119.3
C5 C4 H4 119.3
C6 C5 C4 122.2(2)
C6 C5 H5 118.9
C4 C5 H5 118.9
C5 C6 C7 116.4(2)
C5 C6 H6 121.8
C7 C6 H6 121.8
N1 C7 C6 131.4(2)
N1 C7 C2 106.4(2)
C6 C7 C2 122.3(2)
N4 C8 C9 111.8(2)
N4 C8 H8 124.1
C9 C8 H8 124.1
C14 C9 C10 119.3(2)
C14 C9 C8 104.4(2)
C10 C9 C8 136.2(2)
C11 C10 C9 118.4(2)
C11 C10 H10 120.8
C9 C10 H10 120.8
C10 C11 C12 121.0(2)
C10 C11 H11 119.5
C12 C11 H11 119.5
C13 C12 C11 122.4(2)
C13 C12 H12 118.8
C11 C12 H12 118.8
C12 C13 C14 116.0(2)
C12 C13 H13 122.0
C14 C13 H13 122.0
N3 C14 C13 130.5(2)
N3 C14 C9 106.7(2)
C13 C14 C9 122.8(2)
N1 C15 N3 112.65(18)
N1 C15 H15A 109.1
N3 C15 H15A 109.1
N1 C15 H15B 109.1
N3 C15 H15B 109.1
H15A C15 H15B 107.8
N6 C16 C17 111.2(2)
N6 C16 H16 124.4
C17 C16 H16 124.4
C22 C17 C18 119.5(2)
C22 C17 C16 105.20(19)
C18 C17 C16 135.2(2)
C19 C18 C17 118.0(2)
C19 C18 H18 121.0
C17 C18 H18 121.0
C18 C19 C20 121.4(2)
C18 C19 H19 119.3
C20 C19 H19 119.3
C21 C20 C19 122.1(2)
C21 C20 H20 119.0
C19 C20 H20 119.0
C20 C21 C22 116.5(2)
C20 C21 H21 121.8
C22 C21 H21 121.8
N5 C22 C21 131.3(2)
N5 C22 C17 106.1(2)
C21 C22 C17 122.5(2)
N8 C23 C24 111.4(2)
N8 C23 H23 124.3
C24 C23 H23 124.3
C25 C24 C29 119.9(2)
C25 C24 C23 135.4(2)
C29 C24 C23 104.7(2)
C26 C25 C24 117.7(2)
C26 C25 H25 121.1
C24 C25 H25 121.1
C25 C26 C27 121.5(2)
C25 C26 H26 119.2
C27 C26 H26 119.2
C28 C27 C26 122.4(2)
C28 C27 H27 118.8
C26 C27 H27 118.8
C27 C28 C29 116.3(2)
C27 C28 H28 121.8
C29 C28 H28 121.8
N7 C29 C28 131.7(2)
N7 C29 C24 106.2(2)
C28 C29 C24 122.1(2)
N5 C30 N7 113.33(18)
N5 C30 H30A 108.9
N7 C30 H30A 108.9
N5 C30 H30B 108.9
N7 C30 H30B 108.9
H30A C30 H30B 107.7
O3 N9 O2 119.4(3)
O3 N9 O1 119.7(3)
O2 N9 O1 121.0(3)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
Ag1 N8 2.292(2)
Ag1 N2 2.3045(19)
Ag1 N6 2.4150(19)
Ag1 N4 2.439(2)
N1 C7 1.370(3)
N1 N2 1.372(3)
N1 C15 1.441(3)
N2 C1 1.320(3)
N3 N4 1.368(3)
N3 C14 1.375(3)
N3 C15 1.445(3)
N4 C8 1.315(3)
N5 C22 1.367(3)
N5 N6 1.371(3)
N5 C30 1.443(3)
N6 C16 1.320(3)
N7 N8 1.369(3)
N7 C29 1.371(3)
N7 C30 1.450(3)
N8 C23 1.317(3)
C1 C2 1.416(3)
C1 H1 0.9500
C2 C7 1.404(3)
C2 C3 1.407(3)
C3 C4 1.364(4)
C3 H3 0.9500
C4 C5 1.411(4)
C4 H4 0.9500
C5 C6 1.372(4)
C5 H5 0.9500
C6 C7 1.395(3)
C6 H6 0.9500
C8 C9 1.416(3)
C8 H8 0.9500
C9 C14 1.398(3)
C9 C10 1.408(3)
C10 C11 1.365(4)
C10 H10 0.9500
C11 C12 1.406(4)
C11 H11 0.9500
C12 C13 1.374(4)
C12 H12 0.9500
C13 C14 1.397(3)
C13 H13 0.9500
C15 H15A 0.9900
C15 H15B 0.9900
C16 C17 1.410(3)
C16 H16 0.9500
C17 C22 1.403(3)
C17 C18 1.410(3)
C18 C19 1.369(3)
C18 H18 0.9500
C19 C20 1.410(3)
C19 H19 0.9500
C20 C21 1.370(3)
C20 H20 0.9500
C21 C22 1.400(3)
C21 H21 0.9500
C23 C24 1.415(3)
C23 H23 0.9500
C24 C25 1.409(3)
C24 C29 1.409(3)
C25 C26 1.366(4)
C25 H25 0.9500
C26 C27 1.401(4)
C26 H26 0.9500
C27 C28 1.374(3)
C27 H27 0.9500
C28 C29 1.395(3)
C28 H28 0.9500
C30 H30A 0.9900
C30 H30B 0.9900
O1 N9 1.224(3)
O2 N9 1.211(3)
O3 N9 1.196(3)
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
C7 N1 N2 C1 -1.4(2)
C15 N1 N2 C1 -175.45(19)
C7 N1 N2 Ag1 158.97(14)
C15 N1 N2 Ag1 -15.1(2)
N8 Ag1 N2 C1 -107.9(2)
N6 Ag1 N2 C1 0.6(2)
N4 Ag1 N2 C1 130.8(2)
N8 Ag1 N2 N1 97.73(19)
N6 Ag1 N2 N1 -153.81(14)
N4 Ag1 N2 N1 -23.56(15)
C14 N3 N4 C8 2.3(2)
C15 N3 N4 C8 171.07(19)
C14 N3 N4 Ag1 -147.47(14)
C15 N3 N4 Ag1 21.3(2)
N8 Ag1 N4 C8 84.4(2)
N2 Ag1 N4 C8 -120.0(2)
N6 Ag1 N4 C8 -15.3(2)
N8 Ag1 N4 N3 -135.11(14)
N2 Ag1 N4 N3 20.48(15)
N6 Ag1 N4 N3 125.19(14)
C22 N5 N6 C16 0.3(2)
C30 N5 N6 C16 179.04(19)
C22 N5 N6 Ag1 152.32(14)
C30 N5 N6 Ag1 -29.0(2)
N8 Ag1 N6 C16 133.9(2)
N2 Ag1 N6 C16 -20.0(2)
N4 Ag1 N6 C16 -117.0(2)
N8 Ag1 N6 N5 -10.39(15)
N2 Ag1 N6 N5 -164.32(15)
N4 Ag1 N6 N5 98.73(16)
C29 N7 N8 C23 -1.5(2)
C30 N7 N8 C23 -170.05(19)
C29 N7 N8 Ag1 -171.93(14)
C30 N7 N8 Ag1 19.5(2)
N2 Ag1 N8 C23 -40.4(3)
N6 Ag1 N8 C23 -152.8(2)
N4 Ag1 N8 C23 76.5(2)
N2 Ag1 N8 N7 127.28(17)
N6 Ag1 N8 N7 14.87(16)
N4 Ag1 N8 N7 -115.83(16)
N1 N2 C1 C2 0.7(2)
Ag1 N2 C1 C2 -155.78(15)
N2 C1 C2 C7 0.3(2)
N2 C1 C2 C3 -179.7(2)
C7 C2 C3 C4 1.4(3)
C1 C2 C3 C4 -178.5(2)
C2 C3 C4 C5 -0.5(4)
C3 C4 C5 C6 -1.3(4)
C4 C5 C6 C7 2.0(4)
N2 N1 C7 C6 -178.9(2)
C15 N1 C7 C6 -5.7(4)
N2 N1 C7 C2 1.6(2)
C15 N1 C7 C2 174.8(2)
C5 C6 C7 N1 179.5(2)
C5 C6 C7 C2 -1.0(3)
C3 C2 C7 N1 178.90(19)
C1 C2 C7 N1 -1.1(2)
C3 C2 C7 C6 -0.6(3)
C1 C2 C7 C6 179.3(2)
N3 N4 C8 C9 -1.2(3)
Ag1 N4 C8 C9 141.37(17)
N4 C8 C9 C14 -0.2(3)
N4 C8 C9 C10 -179.1(3)
C14 C9 C10 C11 -1.0(3)
C8 C9 C10 C11 177.8(3)
C9 C10 C11 C12 1.5(4)
C10 C11 C12 C13 -0.1(4)
C11 C12 C13 C14 -1.7(4)
N4 N3 C14 C13 179.4(2)
C15 N3 C14 C13 11.9(4)
N4 N3 C14 C9 -2.4(2)
C15 N3 C14 C9 -169.9(2)
C12 C13 C14 N3 -179.8(2)
C12 C13 C14 C9 2.2(4)
C10 C9 C14 N3 -179.3(2)
C8 C9 C14 N3 1.5(2)
C10 C9 C14 C13 -0.9(3)
C8 C9 C14 C13 179.9(2)
C7 N1 C15 N3 -96.0(3)
N2 N1 C15 N3 76.7(2)
N4 N3 C15 N1 -80.5(2)
C14 N3 C15 N1 86.1(3)
N5 N6 C16 C17 -0.6(3)
Ag1 N6 C16 C17 -147.61(16)
N6 C16 C17 C22 0.6(3)
N6 C16 C17 C18 -177.2(2)
C22 C17 C18 C19 -0.4(3)
C16 C17 C18 C19 177.2(2)
C17 C18 C19 C20 0.7(4)
C18 C19 C20 C21 -0.3(4)
C19 C20 C21 C22 -0.3(3)
N6 N5 C22 C21 178.0(2)
C30 N5 C22 C21 -0.5(4)
N6 N5 C22 C17 0.0(2)
C30 N5 C22 C17 -178.5(2)
C20 C21 C22 N5 -177.0(2)
C20 C21 C22 C17 0.6(3)
C18 C17 C22 N5 177.87(19)
C16 C17 C22 N5 -0.4(2)
C18 C17 C22 C21 -0.3(3)
C16 C17 C22 C21 -178.5(2)
N7 N8 C23 C24 1.3(3)
Ag1 N8 C23 C24 170.32(15)
N8 C23 C24 C25 177.5(3)
N8 C23 C24 C29 -0.6(3)
C29 C24 C25 C26 0.0(3)
C23 C24 C25 C26 -177.9(3)
C24 C25 C26 C27 -0.6(4)
C25 C26 C27 C28 -0.2(4)
C26 C27 C28 C29 1.5(4)
N8 N7 C29 C28 -179.1(2)
C30 N7 C29 C28 -11.9(4)
N8 N7 C29 C24 1.1(2)
C30 N7 C29 C24 168.3(2)
C27 C28 C29 N7 178.2(2)
C27 C28 C29 C24 -2.1(3)
C25 C24 C29 N7 -178.8(2)
C23 C24 C29 N7 -0.3(2)
C25 C24 C29 C28 1.4(3)
C23 C24 C29 C28 179.9(2)
C22 N5 C30 N7 -102.5(3)
N6 N5 C30 N7 79.1(3)
N8 N7 C30 N5 -73.0(2)
C29 N7 C30 N5 120.7(2)
