#------------------------------------------------------------------------------
#$Date: 2016-03-26 18:26:27 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180429 $
#$URL: svn://www.crystallography.net/cod/cif/7/20/98/7209862.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7209862
loop_
_publ_author_name
'Zhao, Lang'
'Wu, Jianfeng'
'Ke, Hongshan'
'Tang, Jinkui'
_publ_section_title
;
 Three dinuclear lanthanide(iii) compounds of a polydentate Schiff base
 ligand: Slow magnetic relaxation behaviour of the DyIII derivative
;
_journal_issue                   26
_journal_name_full               CrystEngComm
_journal_page_first              5301
_journal_paper_doi               10.1039/c3ce40153g
_journal_volume                  15
_journal_year                    2013
_chemical_formula_sum            'C60 H66 N8 O12 Tb2'
_chemical_formula_weight         1409.07
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                105.5600(10)
_cell_angle_beta                 102.8740(10)
_cell_angle_gamma                101.8150(10)
_cell_formula_units_Z            1
_cell_length_a                   10.5341(4)
_cell_length_b                   11.3689(5)
_cell_length_c                   12.8170(6)
_cell_measurement_temperature    191(2)
_cell_volume                     1383.19(10)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      191(2)
_diffrn_measured_fraction_theta_full 0.985
_diffrn_measured_fraction_theta_max 0.985
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0206
_diffrn_reflns_av_sigmaI/netI    0.0454
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -7
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            7686
_diffrn_reflns_theta_full        26.08
_diffrn_reflns_theta_max         26.08
_diffrn_reflns_theta_min         1.73
_exptl_absorpt_coefficient_mu    2.608
_exptl_absorpt_correction_T_max  0.6957
_exptl_absorpt_correction_T_min  0.6104
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_density_diffrn    1.692
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             708
_exptl_crystal_size_max          0.21
_exptl_crystal_size_mid          0.19
_exptl_crystal_size_min          0.15
_refine_diff_density_max         0.702
_refine_diff_density_min         -0.713
_refine_diff_density_rms         0.111
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.054
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     502
_refine_ls_number_reflns         5385
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.054
_refine_ls_R_factor_all          0.0359
_refine_ls_R_factor_gt           0.0300
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0348P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0666
_refine_ls_wR_factor_ref         0.0698
_reflns_number_gt                4779
_reflns_number_total             5385
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3ce40153g.txt
_cod_data_source_block           1b
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7209862
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
C1 C 0.1031(4) 0.4347(4) 0.1449(3) 0.0243(9) Uani 1 1 d
C2 C -0.0119(4) 0.3637(4) 0.0493(3) 0.0268(9) Uani 1 1 d
C3 C 0.0024(5) 0.3230(4) -0.0602(4) 0.0330(10) Uani 1 1 d
H3 H -0.074(4) 0.284(4) -0.116(4) 0.019(11) Uiso 1 1 d
C4 C 0.1264(5) 0.3468(5) -0.0779(4) 0.0394(12) Uani 1 1 d
H4 H 0.132(5) 0.315(4) -0.150(4) 0.040(13) Uiso 1 1 d
C5 C 0.2414(5) 0.4148(5) 0.0145(4) 0.0358(11) Uani 1 1 d
H5 H 0.332(5) 0.431(5) 0.009(4) 0.051(15) Uiso 1 1 d
C6 C 0.2309(4) 0.4583(4) 0.1227(4) 0.0298(10) Uani 1 1 d
C7 C 0.3694(6) 0.6520(5) 0.2560(5) 0.0414(12) Uani 1 1 d
H7A H 0.290(5) 0.672(4) 0.264(4) 0.034(13) Uiso 1 1 d
H7B H 0.398(5) 0.697(5) 0.200(4) 0.047(14) Uiso 1 1 d
H7C H 0.444(5) 0.682(5) 0.317(4) 0.040(14) Uiso 1 1 d
C8 C -0.1480(4) 0.3404(4) 0.0601(3) 0.0243(9) Uani 1 1 d
H8 H -0.224(4) 0.316(4) -0.016(4) 0.037(13) Uiso 1 1 d
C9 C -0.3234(4) 0.3427(4) 0.1440(3) 0.0247(9) Uani 1 1 d
H9A H -0.380(4) 0.336(4) 0.063(3) 0.017(10) Uiso 1 1 d
H9B H -0.364(4) 0.270(4) 0.167(3) 0.015(10) Uiso 1 1 d
C10 C -0.3294(4) 0.4624(4) 0.2256(3) 0.0245(9) Uani 1 1 d
H10A H -0.287(4) 0.537(4) 0.211(3) 0.019(10) Uiso 1 1 d
H10B H -0.425(4) 0.463(4) 0.221(4) 0.030(12) Uiso 1 1 d
C11 C -0.3500(4) 0.4033(4) 0.3934(4) 0.0259(9) Uani 1 1 d
H11A H -0.344(4) 0.329(4) 0.386(4) 0.026(12) Uiso 1 1 d
H11B H -0.448(4) 0.399(4) 0.353(4) 0.027(11) Uiso 1 1 d
C12 C -0.3100(4) 0.4814(4) 0.5182(4) 0.0243(9) Uani 1 1 d
H12A H -0.392(4) 0.493(4) 0.538(4) 0.037(13) Uiso 1 1 d
H12B H -0.274(4) 0.441(4) 0.563(3) 0.019(11) Uiso 1 1 d
C13 C -0.2390(4) 0.6111(4) 0.4141(3) 0.0216(8) Uani 1 1 d
H13 H -0.325(4) 0.635(3) 0.385(3) 0.015(10) Uiso 1 1 d
C14 C -0.1268(4) 0.7068(4) 0.4033(3) 0.0213(8) Uani 1 1 d
C15 C -0.1532(4) 0.8077(4) 0.3681(3) 0.0266(9) Uani 1 1 d
H15 H -0.246(4) 0.811(4) 0.345(3) 0.017(10) Uiso 1 1 d
C16 C -0.0509(5) 0.8991(4) 0.3619(4) 0.0329(11) Uani 1 1 d
H16 H -0.066(4) 0.963(4) 0.338(3) 0.022(11) Uiso 1 1 d
C17 C 0.0825(5) 0.8931(4) 0.3918(4) 0.0297(10) Uani 1 1 d
H17 H 0.156(4) 0.958(4) 0.389(4) 0.032(12) Uiso 1 1 d
C18 C 0.1104(4) 0.7939(4) 0.4276(3) 0.0236(9) Uani 1 1 d
C19 C 0.0074(4) 0.6982(4) 0.4339(3) 0.0205(8) Uani 1 1 d
C20 C 0.3493(5) 0.8920(5) 0.4897(5) 0.0426(13) Uani 1 1 d
H20A H 0.333(5) 0.951(5) 0.544(5) 0.051(17) Uiso 1 1 d
H20B H 0.350(5) 0.918(5) 0.421(4) 0.051(15) Uiso 1 1 d
H20C H 0.427(5) 0.872(5) 0.527(4) 0.046(15) Uiso 1 1 d
C21 C -0.2610(4) 0.7163(4) 0.5949(3) 0.0244(9) Uani 1 1 d
H21A H -0.220(4) 0.792(4) 0.580(3) 0.016(10) Uiso 1 1 d
H21B H -0.358(4) 0.697(4) 0.568(3) 0.028(11) Uiso 1 1 d
C22 C -0.2064(4) 0.7471(4) 0.7210(4) 0.0259(9) Uani 1 1 d
H22A H -0.236(4) 0.818(4) 0.754(4) 0.031(12) Uiso 1 1 d
H22B H -0.232(4) 0.676(4) 0.744(3) 0.021(11) Uiso 1 1 d
C23 C 0.0076(4) 0.8929(4) 0.8204(3) 0.0244(9) Uani 1 1 d
H23 H -0.041(3) 0.939(3) 0.855(3) 0.008(9) Uiso 1 1 d
C24 C 0.1530(4) 0.9514(4) 0.8530(3) 0.0271(9) Uani 1 1 d
C25 C 0.2073(5) 1.0671(4) 0.9438(4) 0.0342(11) Uani 1 1 d
H25 H 0.148(3) 1.100(3) 0.984(3) 0.009(9) Uiso 1 1 d
C26 C 0.3414(5) 1.1301(5) 0.9751(4) 0.0421(12) Uani 1 1 d
H26 H 0.377(4) 1.202(4) 1.033(4) 0.023(11) Uiso 1 1 d
C27 C 0.4254(5) 1.0821(4) 0.9148(4) 0.0365(11) Uani 1 1 d
H27 H 0.521(4) 1.121(4) 0.935(4) 0.030(12) Uiso 1 1 d
C28 C 0.3740(4) 0.9724(4) 0.8234(4) 0.0284(9) Uani 1 1 d
C29 C 0.2345(4) 0.9003(4) 0.7892(3) 0.0238(9) Uani 1 1 d
C30 C 0.5840(5) 0.9927(5) 0.7818(5) 0.0420(12) Uani 1 1 d
H30A H 0.583(5) 1.066(5) 0.769(4) 0.050(16) Uiso 1 1 d
H30B H 0.615(5) 0.942(5) 0.728(4) 0.048(15) Uiso 1 1 d
H30C H 0.644(5) 1.010(4) 0.863(4) 0.041(13) Uiso 1 1 d
N1 N -0.1805(3) 0.3547(3) 0.1519(3) 0.0233(7) Uani 1 1 d
N2 N -0.2596(3) 0.4782(3) 0.3448(3) 0.0199(7) Uani 1 1 d
N3 N -0.2201(3) 0.6081(3) 0.5314(3) 0.0207(7) Uani 1 1 d
N4 N -0.0581(3) 0.7820(3) 0.7505(3) 0.0226(7) Uani 1 1 d
O1 O 0.0955(3) 0.4753(3) 0.2487(2) 0.0238(6) Uani 1 1 d
O2 O 0.3485(3) 0.5193(3) 0.2122(3) 0.0347(7) Uani 1 1 d
O3 O 0.0353(2) 0.6028(2) 0.4692(2) 0.0178(5) Uani 1 1 d
O4 O 0.2396(3) 0.7817(3) 0.4607(3) 0.0302(7) Uani 1 1 d
O5 O 0.1882(3) 0.7964(3) 0.7022(2) 0.0239(6) Uani 1 1 d
O6 O 0.4499(3) 0.9197(3) 0.7596(3) 0.0358(7) Uani 1 1 d
Tb1 Tb -0.032129(18) 0.391685(17) 0.345863(15) 0.01835(7) Uani 1 1 d
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Tb Tb -0.1723 4.1537 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 C1 C2 123.3(4) . .
O1 C1 C6 120.5(4) . .
C2 C1 C6 116.1(4) . .
C3 C2 C1 120.8(4) . .
C3 C2 C8 117.8(4) . .
C1 C2 C8 121.2(4) . .
C4 C3 C2 121.3(5) . .
C4 C3 H3 123(3) . .
C2 C3 H3 116(3) . .
C3 C4 C5 119.2(4) . .
C3 C4 H4 119(3) . .
C5 C4 H4 122(3) . .
C6 C5 C4 121.1(4) . .
C6 C5 H5 115(3) . .
C4 C5 H5 124(3) . .
C5 C6 O2 118.9(4) . .
C5 C6 C1 121.5(4) . .
O2 C6 C1 119.5(4) . .
O2 C7 H7A 112(3) . .
O2 C7 H7B 111(3) . .
H7A C7 H7B 105(4) . .
O2 C7 H7C 106(3) . .
H7A C7 H7C 119(4) . .
H7B C7 H7C 104(4) . .
N1 C8 C2 126.6(4) . .
N1 C8 H8 119(2) . .
C2 C8 H8 114(2) . .
N1 C9 C10 107.1(3) . .
N1 C9 H9A 112(2) . .
C10 C9 H9A 107(2) . .
N1 C9 H9B 111(2) . .
C10 C9 H9B 108(2) . .
H9A C9 H9B 111(3) . .
N2 C10 C9 112.0(3) . .
N2 C10 H10A 107(2) . .
C9 C10 H10A 112(2) . .
N2 C10 H10B 107(2) . .
C9 C10 H10B 111(2) . .
H10A C10 H10B 107(3) . .
N2 C11 C12 104.9(3) . .
N2 C11 H11A 115(3) . .
C12 C11 H11A 110(3) . .
N2 C11 H11B 107(2) . .
C12 C11 H11B 111(2) . .
H11A C11 H11B 109(4) . .
N3 C12 C11 106.4(3) . .
N3 C12 H12A 109(3) . .
C11 C12 H12A 109(3) . .
N3 C12 H12B 115(3) . .
C11 C12 H12B 112(3) . .
H12A C12 H12B 106(4) . .
N2 C13 N3 104.6(3) . .
N2 C13 C14 115.1(3) . .
N3 C13 C14 113.3(3) . .
N2 C13 H13 107(2) . .
N3 C13 H13 112(2) . .
C14 C13 H13 105(2) . .
C15 C14 C19 120.1(4) . .
C15 C14 C13 120.3(4) . .
C19 C14 C13 119.6(3) . .
C16 C15 C14 121.1(4) . .
C16 C15 H15 120(2) . .
C14 C15 H15 119(2) . .
C15 C16 C17 120.0(4) . .
C15 C16 H16 122(3) . .
C17 C16 H16 118(3) . .
C18 C17 C16 119.5(4) . .
C18 C17 H17 120(3) . .
C16 C17 H17 121(3) . .
O4 C18 C17 123.4(4) . .
O4 C18 C19 114.8(3) . .
C17 C18 C19 121.8(4) . .
O3 C19 C18 121.4(3) . .
O3 C19 C14 121.1(3) . .
C18 C19 C14 117.5(4) . .
O4 C20 H20A 105(3) . .
O4 C20 H20B 110(3) . .
H20A C20 H20B 112(4) . .
O4 C20 H20C 105(3) . .
H20A C20 H20C 106(5) . .
H20B C20 H20C 119(4) . .
N3 C21 C22 111.7(3) . .
N3 C21 H21A 108(2) . .
C22 C21 H21A 105(2) . .
N3 C21 H21B 108(2) . .
C22 C21 H21B 114(2) . .
H21A C21 H21B 110(3) . .
N4 C22 C21 107.7(3) . .
N4 C22 H22A 111(3) . .
C21 C22 H22A 105(3) . .
N4 C22 H22B 106(2) . .
C21 C22 H22B 112(3) . .
H22A C22 H22B 115(4) . .
N4 C23 C24 126.8(4) . .
N4 C23 H23 117(2) . .
C24 C23 H23 116(2) . .
C25 C24 C29 121.2(4) . .
C25 C24 C23 117.4(4) . .
C29 C24 C23 121.1(4) . .
C26 C25 C24 120.5(4) . .
C26 C25 H25 121(2) . .
C24 C25 H25 119(2) . .
C25 C26 C27 119.9(4) . .
C25 C26 H26 121(3) . .
C27 C26 H26 119(3) . .
C28 C27 C26 120.8(4) . .
C28 C27 H27 116(3) . .
C26 C27 H27 123(3) . .
C27 C28 O6 124.2(4) . .
C27 C28 C29 121.5(4) . .
O6 C28 C29 114.3(3) . .
O5 C29 C24 123.6(4) . .
O5 C29 C28 120.3(4) . .
C24 C29 C28 116.0(4) . .
O6 C30 H30A 110(3) . .
O6 C30 H30B 103(3) . .
H30A C30 H30B 110(5) . .
O6 C30 H30C 114(3) . .
H30A C30 H30C 110(4) . .
H30B C30 H30C 111(4) . .
C8 N1 C9 117.1(3) . .
C8 N1 Tb1 128.3(3) . .
C9 N1 Tb1 114.6(2) . .
C13 N2 C10 107.8(3) . .
C13 N2 C11 103.1(3) . .
C10 N2 C11 111.2(3) . .
C13 N2 Tb1 117.7(2) . .
C10 N2 Tb1 107.7(2) . .
C11 N2 Tb1 109.4(2) . .
C21 N3 C13 107.5(3) . .
C21 N3 C12 113.0(3) . .
C13 N3 C12 104.7(3) . .
C21 N3 Tb1 109.7(2) . 2_566
C13 N3 Tb1 118.6(2) . 2_566
C12 N3 Tb1 103.4(2) . 2_566
C23 N4 C22 117.6(3) . .
C23 N4 Tb1 128.8(3) . 2_566
C22 N4 Tb1 113.6(2) . 2_566
C1 O1 Tb1 133.5(3) . .
C6 O2 C7 113.2(4) . .
C19 O3 Tb1 122.0(2) . .
C19 O3 Tb1 118.5(2) . 2_566
Tb1 O3 Tb1 110.74(10) . 2_566
C18 O4 C20 117.0(4) . .
C29 O5 Tb1 135.7(2) . 2_566
C28 O6 C30 116.7(4) . .
O5 Tb1 O1 131.86(9) 2_566 .
O5 Tb1 O3 142.13(9) 2_566 .
O1 Tb1 O3 83.63(9) . .
O5 Tb1 O3 82.44(9) 2_566 2_566
O1 Tb1 O3 142.68(9) . 2_566
O3 Tb1 O3 69.26(10) . 2_566
O5 Tb1 N1 73.93(10) 2_566 .
O1 Tb1 N1 71.22(10) . .
O3 Tb1 N1 115.18(9) . .
O3 Tb1 N1 143.35(10) 2_566 .
O5 Tb1 N4 71.27(10) 2_566 2_566
O1 Tb1 N4 73.79(10) . 2_566
O3 Tb1 N4 142.75(10) . 2_566
O3 Tb1 N4 113.28(9) 2_566 2_566
N1 Tb1 N4 85.38(10) . 2_566
O5 Tb1 N3 112.03(10) 2_566 2_566
O1 Tb1 N3 81.15(9) . 2_566
O3 Tb1 N3 82.27(9) . 2_566
O3 Tb1 N3 70.48(9) 2_566 2_566
N1 Tb1 N3 144.58(10) . 2_566
N4 Tb1 N3 65.50(10) 2_566 2_566
O5 Tb1 N2 81.24(9) 2_566 .
O1 Tb1 N2 112.55(9) . .
O3 Tb1 N2 71.10(9) . .
O3 Tb1 N2 83.07(9) 2_566 .
N1 Tb1 N2 66.16(10) . .
N4 Tb1 N2 145.05(10) 2_566 .
N3 Tb1 N2 147.79(9) 2_566 .
O5 Tb1 Tb1 113.48(7) 2_566 2_566
O1 Tb1 Tb1 114.65(7) . 2_566
O3 Tb1 Tb1 34.72(6) . 2_566
O3 Tb1 Tb1 34.54(6) 2_566 2_566
N1 Tb1 Tb1 138.29(7) . 2_566
N4 Tb1 Tb1 136.32(7) 2_566 2_566
N3 Tb1 Tb1 73.44(6) 2_566 2_566
N2 Tb1 Tb1 74.34(6) . 2_566
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 O1 1.313(4) .
C1 C2 1.424(6) .
C1 C6 1.425(6) .
C2 C3 1.408(6) .
C2 C8 1.448(6) .
C3 C4 1.361(7) .
C3 H3 0.88(4) .
C4 C5 1.397(7) .
C4 H4 0.91(5) .
C5 C6 1.379(6) .
C5 H5 0.95(5) .
C6 O2 1.385(5) .
C7 O2 1.412(6) .
C7 H7A 0.94(4) .
C7 H7B 1.05(5) .
C7 H7C 0.91(5) .
C8 N1 1.276(5) .
C8 H8 1.04(5) .
C9 N1 1.461(5) .
C9 C10 1.501(6) .
C9 H9A 1.04(4) .
C9 H9B 1.00(4) .
C10 N2 1.485(5) .
C10 H10A 0.96(4) .
C10 H10B 1.00(4) .
C11 N2 1.495(5) .
C11 C12 1.519(6) .
C11 H11A 0.84(4) .
C11 H11B 1.03(4) .
C12 N3 1.497(5) .
C12 H12A 0.98(4) .
C12 H12B 0.89(4) .
C13 N2 1.476(5) .
C13 N3 1.483(5) .
C13 C14 1.493(5) .
C13 H13 1.02(4) .
C14 C15 1.396(6) .
C14 C19 1.411(5) .
C15 C16 1.368(6) .
C15 H15 0.97(4) .
C16 C17 1.393(6) .
C16 H16 0.89(4) .
C17 C18 1.386(6) .
C17 H17 0.97(4) .
C18 O4 1.380(5) .
C18 C19 1.404(5) .
C19 O3 1.342(4) .
C20 O4 1.418(5) .
C20 H20A 0.90(5) .
C20 H20B 1.01(5) .
C20 H20C 0.96(5) .
C21 N3 1.482(5) .
C21 C22 1.506(6) .
C21 H21A 0.97(4) .
C21 H21B 0.96(4) .
C22 N4 1.464(5) .
C22 H22A 0.95(4) .
C22 H22B 0.94(4) .
C23 N4 1.278(5) .
C23 C24 1.453(6) .
C23 H23 0.91(3) .
C24 C25 1.409(6) .
C24 C29 1.417(5) .
C25 C26 1.359(7) .
C25 H25 0.97(3) .
C26 C27 1.398(7) .
C26 H26 0.89(4) .
C27 C28 1.370(6) .
C27 H27 0.96(4) .
C28 O6 1.376(5) .
C28 C29 1.431(6) .
C29 O5 1.301(5) .
C30 O6 1.407(6) .
C30 H30A 0.89(6) .
C30 H30B 0.94(5) .
C30 H30C 1.03(5) .
N1 Tb1 2.497(3) .
N2 Tb1 2.769(3) .
N3 Tb1 2.769(3) 2_566
N4 Tb1 2.512(3) 2_566
O1 Tb1 2.263(3) .
O3 Tb1 2.351(2) .
O3 Tb1 2.362(2) 2_566
O5 Tb1 2.249(3) 2_566
Tb1 O5 2.249(3) 2_566
Tb1 O3 2.362(2) 2_566
Tb1 N4 2.512(3) 2_566
Tb1 N3 2.769(3) 2_566
Tb1 Tb1 3.8782(4) 2_566
