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#$Date: 2016-03-26 18:26:27 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180429 $
#$URL: svn://www.crystallography.net/cod/cif/7/20/98/7209863.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7209863
loop_
_publ_author_name
'Zhao, Lang'
'Wu, Jianfeng'
'Ke, Hongshan'
'Tang, Jinkui'
_publ_section_title
;
 Three dinuclear lanthanide(iii) compounds of a polydentate Schiff base
 ligand: Slow magnetic relaxation behaviour of the DyIII derivative
;
_journal_issue                   26
_journal_name_full               CrystEngComm
_journal_page_first              5301
_journal_paper_doi               10.1039/c3ce40153g
_journal_volume                  15
_journal_year                    2013
_chemical_formula_sum            'C68 H78 Dy2 N12 O12'
_chemical_formula_weight         1580.42
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 95.7800(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   12.2399(5)
_cell_length_b                   18.9948(8)
_cell_length_c                   14.4502(6)
_cell_measurement_temperature    191(2)
_cell_volume                     3342.5(2)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      191(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0263
_diffrn_reflns_av_sigmaI/netI    0.0314
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            18462
_diffrn_reflns_theta_full        26.13
_diffrn_reflns_theta_max         26.13
_diffrn_reflns_theta_min         1.78
_exptl_absorpt_coefficient_mu    2.289
_exptl_absorpt_correction_T_max  0.6574
_exptl_absorpt_correction_T_min  0.5279
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_density_diffrn    1.570
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             1596
_exptl_crystal_size_max          0.32
_exptl_crystal_size_mid          0.25
_exptl_crystal_size_min          0.20
_refine_diff_density_max         0.454
_refine_diff_density_min         -0.688
_refine_diff_density_rms         0.133
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.107
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     429
_refine_ls_number_reflns         6664
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.107
_refine_ls_R_factor_all          0.0294
_refine_ls_R_factor_gt           0.0233
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0309P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0594
_refine_ls_wR_factor_ref         0.0623
_reflns_number_gt                5713
_reflns_number_total             6664
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3ce40153g.txt
_cod_data_source_block           1c
_cod_original_sg_symbol_H-M      P2(1)/n
_cod_database_code               7209863
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Dy1 Dy 0.139398(10) 0.043335(6) 0.036088(8) 0.01648(5) Uani 1 1 d .
N1 N 0.21297(18) 0.16371(12) 0.07244(16) 0.0223(5) Uani 1 1 d .
N2 N 0.01698(18) -0.13807(11) -0.08092(15) 0.0182(5) Uani 1 1 d .
N3 N 0.18651(18) -0.08474(11) -0.03494(15) 0.0189(5) Uani 1 1 d .
N4 N 0.33504(18) 0.00735(12) 0.07451(16) 0.0226(5) Uani 1 1 d .
N5 N 0.7953(3) 0.77402(19) 0.3685(3) 0.0698(11) Uani 1 1 d .
N6 N 0.2175(4) 0.8982(3) 0.5263(3) 0.0970(15) Uani 1 1 d .
O1 O 0.22478(15) 0.08210(10) -0.08435(13) 0.0233(4) Uani 1 1 d .
O2 O 0.31873(19) 0.05938(12) -0.23899(15) 0.0360(5) Uani 1 1 d .
O3 O 0.00882(15) -0.03696(9) 0.07730(12) 0.0167(4) Uani 1 1 d .
O4 O -0.02790(18) -0.04354(10) 0.25503(14) 0.0281(5) Uani 1 1 d .
O5 O 0.17921(16) 0.04519(9) 0.19010(13) 0.0228(4) Uani 1 1 d .
O6 O 0.13443(17) 0.09603(12) 0.35025(14) 0.0347(5) Uani 1 1 d .
C1 C 0.3100(2) 0.12011(15) -0.09769(19) 0.0228(6) Uani 1 1 d .
C2 C 0.3638(2) 0.11050(15) -0.1802(2) 0.0269(7) Uani 1 1 d .
C3 C 0.4533(3) 0.15106(17) -0.1967(2) 0.0351(8) Uani 1 1 d .
H3 H 0.4878 0.1435 -0.2519 0.042 Uiso 1 1 calc R
C4 C 0.4938(3) 0.20265(18) -0.1344(2) 0.0384(8) Uani 1 1 d .
H4 H 0.5558 0.2300 -0.1467 0.046 Uiso 1 1 calc R
C5 C 0.4437(2) 0.21371(17) -0.0553(2) 0.0339(7) Uani 1 1 d .
H5 H 0.4710 0.2492 -0.0127 0.041 Uiso 1 1 calc R
C6 C 0.3525(2) 0.17353(15) -0.03597(19) 0.0248(6) Uani 1 1 d .
C7 C 0.3476(3) 0.06033(19) -0.3323(2) 0.0417(9) Uani 1 1 d .
H7A H 0.3316 0.1069 -0.3596 0.063 Uiso 1 1 calc R
H7B H 0.3048 0.0246 -0.3690 0.063 Uiso 1 1 calc R
H7C H 0.4261 0.0502 -0.3323 0.063 Uiso 1 1 calc R
C8 C 0.2936(2) 0.19552(15) 0.04069(19) 0.0247(6) Uani 1 1 d .
H8 H 0.3171 0.2381 0.0708 0.030 Uiso 1 1 calc R
C9 C 0.1516(2) 0.20289(15) 0.13791(19) 0.0235(6) Uani 1 1 d .
H9A H 0.1836 0.2503 0.1493 0.028 Uiso 1 1 calc R
H9B H 0.1538 0.1776 0.1980 0.028 Uiso 1 1 calc R
C10 C -0.0347(2) -0.20841(14) -0.0931(2) 0.0252(6) Uani 1 1 d .
H10A H -0.0345 -0.2316 -0.0317 0.030 Uiso 1 1 calc R
H10B H 0.0086 -0.2379 -0.1325 0.030 Uiso 1 1 calc R
C11 C 0.0605(2) -0.11327(15) -0.16878(19) 0.0245(6) Uani 1 1 d .
H11A H 0.0091 -0.0793 -0.2019 0.029 Uiso 1 1 calc R
H11B H 0.0707 -0.1535 -0.2106 0.029 Uiso 1 1 calc R
C12 C 0.1703(2) -0.07808(15) -0.13827(19) 0.0247(6) Uani 1 1 d .
H12A H 0.2305 -0.1019 -0.1669 0.030 Uiso 1 1 calc R
H12B H 0.1688 -0.0279 -0.1569 0.030 Uiso 1 1 calc R
C13 C 0.1168(2) -0.14556(14) -0.01446(19) 0.0198(6) Uani 1 1 d .
H13 H 0.1556 -0.1897 -0.0302 0.024 Uiso 1 1 calc R
C14 C 0.0938(2) -0.14993(14) 0.08535(19) 0.0199(6) Uani 1 1 d .
C15 C 0.1248(2) -0.21005(15) 0.1374(2) 0.0269(7) Uani 1 1 d .
H15 H 0.1604 -0.2476 0.1090 0.032 Uiso 1 1 calc R
C16 C 0.1046(2) -0.21555(16) 0.2282(2) 0.0322(7) Uani 1 1 d .
H16 H 0.1258 -0.2569 0.2625 0.039 Uiso 1 1 calc R
C17 C 0.0531(2) -0.16070(16) 0.2708(2) 0.0303(7) Uani 1 1 d .
H17 H 0.0388 -0.1646 0.3340 0.036 Uiso 1 1 calc R
C18 C 0.0228(2) -0.10039(15) 0.22069(19) 0.0236(6) Uani 1 1 d .
C19 C 0.0411(2) -0.09461(14) 0.12655(18) 0.0185(6) Uani 1 1 d .
C20 C -0.0508(3) -0.04625(17) 0.3490(2) 0.0386(8) Uani 1 1 d .
H20A H -0.0974 -0.0871 0.3582 0.058 Uiso 1 1 calc R
H20B H -0.0890 -0.0031 0.3644 0.058 Uiso 1 1 calc R
H20C H 0.0181 -0.0504 0.3894 0.058 Uiso 1 1 calc R
C21 C 0.3011(2) -0.10330(15) -0.0017(2) 0.0235(6) Uani 1 1 d .
H21A H 0.3289 -0.1379 -0.0449 0.028 Uiso 1 1 calc R
H21B H 0.3028 -0.1257 0.0603 0.028 Uiso 1 1 calc R
C22 C 0.3747(2) -0.03990(14) 0.0049(2) 0.0235(6) Uani 1 1 d .
H22A H 0.4515 -0.0541 0.0239 0.028 Uiso 1 1 calc R
H22B H 0.3720 -0.0159 -0.0562 0.028 Uiso 1 1 calc R
C23 C 0.4007(2) 0.02181(15) 0.1462(2) 0.0238(6) Uani 1 1 d .
H23 H 0.4751 0.0078 0.1450 0.029 Uiso 1 1 calc R
C24 C 0.3730(2) 0.05732(15) 0.2288(2) 0.0235(6) Uani 1 1 d .
C25 C 0.4590(3) 0.07702(16) 0.2968(2) 0.0309(7) Uani 1 1 d .
H25 H 0.5330 0.0725 0.2833 0.037 Uiso 1 1 calc R
C26 C 0.4375(3) 0.10229(17) 0.3815(2) 0.0362(8) Uani 1 1 d .
H26 H 0.4960 0.1155 0.4262 0.043 Uiso 1 1 calc R
C27 C 0.3286(3) 0.10860(16) 0.4020(2) 0.0309(7) Uani 1 1 d .
H27 H 0.3135 0.1255 0.4612 0.037 Uiso 1 1 calc R
C28 C 0.2438(2) 0.09071(15) 0.3375(2) 0.0267(7) Uani 1 1 d .
C29 C 0.2623(2) 0.06374(14) 0.24799(19) 0.0221(6) Uani 1 1 d .
C30 C 0.1081(3) 0.1152(2) 0.4400(2) 0.0472(9) Uani 1 1 d .
H30A H 0.1413 0.0815 0.4858 0.071 Uiso 1 1 calc R
H30B H 0.0281 0.1149 0.4411 0.071 Uiso 1 1 calc R
H30C H 0.1365 0.1625 0.4552 0.071 Uiso 1 1 calc R
C31 C 0.8204(3) 0.7336(2) 0.2022(3) 0.0640(12) Uani 1 1 d .
H31A H 0.8788 0.6982 0.2047 0.096 Uiso 1 1 calc R
H31B H 0.8406 0.7739 0.1651 0.096 Uiso 1 1 calc R
H31C H 0.7517 0.7131 0.1736 0.096 Uiso 1 1 calc R
C32 C 0.8058(3) 0.7568(2) 0.2954(3) 0.0503(10) Uani 1 1 d .
C33 C 0.3122(4) 0.9140(2) 0.3775(4) 0.0753(15) Uani 1 1 d .
H33A H 0.2566 0.9129 0.3238 0.113 Uiso 1 1 calc R
H33B H 0.3652 0.8759 0.3721 0.113 Uiso 1 1 calc R
H33C H 0.3505 0.9594 0.3794 0.113 Uiso 1 1 calc R
C34 C 0.2597(4) 0.9050(2) 0.4620(4) 0.0627(12) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O5 Dy1 O1 134.20(7) . .
O5 Dy1 O3 141.41(7) . 3
O1 Dy1 O3 82.04(7) . 3
O5 Dy1 O3 80.90(7) . .
O1 Dy1 O3 143.00(7) . .
O3 Dy1 O3 68.83(7) 3 .
O5 Dy1 N1 74.77(7) . .
O1 Dy1 N1 71.08(7) . .
O3 Dy1 N1 115.87(7) 3 .
O3 Dy1 N1 142.08(7) . .
O5 Dy1 N4 70.99(7) . .
O1 Dy1 N4 75.59(7) . .
O3 Dy1 N4 143.69(7) 3 .
O3 Dy1 N4 115.53(7) . .
N1 Dy1 N4 83.47(7) . .
O5 Dy1 N3 110.90(7) . .
O1 Dy1 N3 82.42(7) . .
O3 Dy1 N3 82.39(6) 3 .
O3 Dy1 N3 71.84(6) . .
N1 Dy1 N3 144.32(7) . .
N4 Dy1 N3 66.73(7) . .
O5 Dy1 N2 80.90(7) . 3
O1 Dy1 N2 110.95(7) . 3
O3 Dy1 N2 71.80(6) 3 3
O3 Dy1 N2 81.75(6) . 3
N1 Dy1 N2 66.16(7) . 3
N4 Dy1 N2 143.18(7) . 3
N3 Dy1 N2 148.35(6) . 3
O5 Dy1 Dy1 112.15(5) . 3
O1 Dy1 Dy1 113.65(5) . 3
O3 Dy1 Dy1 34.48(4) 3 3
O3 Dy1 Dy1 34.35(5) . 3
N1 Dy1 Dy1 137.98(5) . 3
N4 Dy1 Dy1 138.52(5) . 3
N3 Dy1 Dy1 74.38(5) . 3
N2 Dy1 Dy1 73.97(4) 3 3
C8 N1 C9 117.0(2) . .
C8 N1 Dy1 129.19(19) . .
C9 N1 Dy1 113.77(16) . .
C10 N2 C13 107.7(2) . .
C10 N2 C11 111.5(2) . .
C13 N2 C11 103.8(2) . .
C10 N2 Dy1 108.59(15) . 3
C13 N2 Dy1 117.24(15) . 3
C11 N2 Dy1 107.96(16) . 3
C21 N3 C13 107.2(2) . .
C21 N3 C12 111.8(2) . .
C13 N3 C12 104.2(2) . .
C21 N3 Dy1 108.69(16) . .
C13 N3 Dy1 118.19(15) . .
C12 N3 Dy1 106.83(16) . .
C23 N4 C22 117.7(2) . .
C23 N4 Dy1 129.27(19) . .
C22 N4 Dy1 113.00(17) . .
C1 O1 Dy1 137.87(18) . .
C2 O2 C7 117.0(2) . .
C19 O3 Dy1 119.90(15) . 3
C19 O3 Dy1 119.75(15) . .
Dy1 O3 Dy1 111.17(7) 3 .
C18 O4 C20 117.5(2) . .
C29 O5 Dy1 136.49(18) . .
C28 O6 C30 117.2(2) . .
O1 C1 C6 123.7(2) . .
O1 C1 C2 119.8(3) . .
C6 C1 C2 116.5(2) . .
O2 C2 C3 124.5(3) . .
O2 C2 C1 114.7(2) . .
C3 C2 C1 120.9(3) . .
C2 C3 C4 121.4(3) . .
C2 C3 H3 119.3 . .
C4 C3 H3 119.3 . .
C5 C4 C3 119.3(3) . .
C5 C4 H4 120.4 . .
C3 C4 H4 120.4 . .
C4 C5 C6 121.1(3) . .
C4 C5 H5 119.5 . .
C6 C5 H5 119.5 . .
C5 C6 C1 120.9(3) . .
C5 C6 C8 117.7(3) . .
C1 C6 C8 120.7(2) . .
O2 C7 H7A 109.5 . .
O2 C7 H7B 109.5 . .
H7A C7 H7B 109.5 . .
O2 C7 H7C 109.5 . .
H7A C7 H7C 109.5 . .
H7B C7 H7C 109.5 . .
N1 C8 C6 126.9(3) . .
N1 C8 H8 116.5 . .
C6 C8 H8 116.5 . .
N1 C9 C10 106.4(2) . 3
N1 C9 H9A 110.4 . .
C10 C9 H9A 110.4 3 .
N1 C9 H9B 110.4 . .
C10 C9 H9B 110.4 3 .
H9A C9 H9B 108.6 . .
N2 C10 C9 111.3(2) . 3
N2 C10 H10A 109.4 . .
C9 C10 H10A 109.4 3 .
N2 C10 H10B 109.4 . .
C9 C10 H10B 109.4 3 .
H10A C10 H10B 108.0 . .
N2 C11 C12 105.7(2) . .
N2 C11 H11A 110.6 . .
C12 C11 H11A 110.6 . .
N2 C11 H11B 110.6 . .
C12 C11 H11B 110.6 . .
H11A C11 H11B 108.7 . .
N3 C12 C11 106.0(2) . .
N3 C12 H12A 110.5 . .
C11 C12 H12A 110.5 . .
N3 C12 H12B 110.5 . .
C11 C12 H12B 110.5 . .
H12A C12 H12B 108.7 . .
N2 C13 N3 104.4(2) . .
N2 C13 C14 113.9(2) . .
N3 C13 C14 113.8(2) . .
N2 C13 H13 108.2 . .
N3 C13 H13 108.2 . .
C14 C13 H13 108.2 . .
C19 C14 C15 119.8(2) . .
C19 C14 C13 120.5(2) . .
C15 C14 C13 119.7(2) . .
C16 C15 C14 121.0(3) . .
C16 C15 H15 119.5 . .
C14 C15 H15 119.5 . .
C15 C16 C17 120.1(3) . .
C15 C16 H16 119.9 . .
C17 C16 H16 119.9 . .
C18 C17 C16 119.8(3) . .
C18 C17 H17 120.1 . .
C16 C17 H17 120.1 . .
O4 C18 C17 124.9(3) . .
O4 C18 C19 114.4(2) . .
C17 C18 C19 120.7(3) . .
O3 C19 C14 120.7(2) . .
O3 C19 C18 120.6(2) . .
C14 C19 C18 118.6(2) . .
O4 C20 H20A 109.5 . .
O4 C20 H20B 109.5 . .
H20A C20 H20B 109.5 . .
O4 C20 H20C 109.5 . .
H20A C20 H20C 109.5 . .
H20B C20 H20C 109.5 . .
N3 C21 C22 111.9(2) . .
N3 C21 H21A 109.2 . .
C22 C21 H21A 109.2 . .
N3 C21 H21B 109.2 . .
C22 C21 H21B 109.2 . .
H21A C21 H21B 107.9 . .
N4 C22 C21 107.2(2) . .
N4 C22 H22A 110.3 . .
C21 C22 H22A 110.3 . .
N4 C22 H22B 110.3 . .
C21 C22 H22B 110.3 . .
H22A C22 H22B 108.5 . .
N4 C23 C24 126.3(3) . .
N4 C23 H23 116.8 . .
C24 C23 H23 116.8 . .
C25 C24 C29 120.0(3) . .
C25 C24 C23 118.6(3) . .
C29 C24 C23 120.8(3) . .
C26 C25 C24 121.2(3) . .
C26 C25 H25 119.4 . .
C24 C25 H25 119.4 . .
C25 C26 C27 119.6(3) . .
C25 C26 H26 120.2 . .
C27 C26 H26 120.2 . .
C28 C27 C26 120.6(3) . .
C28 C27 H27 119.7 . .
C26 C27 H27 119.7 . .
C27 C28 O6 125.1(3) . .
C27 C28 C29 121.8(3) . .
O6 C28 C29 113.1(3) . .
O5 C29 C24 123.6(3) . .
O5 C29 C28 119.6(3) . .
C24 C29 C28 116.8(3) . .
O6 C30 H30A 109.5 . .
O6 C30 H30B 109.5 . .
H30A C30 H30B 109.5 . .
O6 C30 H30C 109.5 . .
H30A C30 H30C 109.5 . .
H30B C30 H30C 109.5 . .
C32 C31 H31A 109.5 . .
C32 C31 H31B 109.5 . .
H31A C31 H31B 109.5 . .
C32 C31 H31C 109.5 . .
H31A C31 H31C 109.5 . .
H31B C31 H31C 109.5 . .
N5 C32 C31 179.0(5) . .
C34 C33 H33A 109.5 . .
C34 C33 H33B 109.5 . .
H33A C33 H33B 109.5 . .
C34 C33 H33C 109.5 . .
H33A C33 H33C 109.5 . .
H33B C33 H33C 109.5 . .
N6 C34 C33 178.8(6) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Dy1 O5 2.2300(19) .
Dy1 O1 2.2427(17) .
Dy1 O3 2.3220(19) 3
Dy1 O3 2.3296(17) .
Dy1 N1 2.494(2) .
Dy1 N4 2.498(2) .
Dy1 N3 2.725(2) .
Dy1 N2 2.752(2) 3
Dy1 Dy1 3.8374(3) 3
N1 C8 1.281(3) .
N1 C9 1.468(3) .
N2 C10 1.481(3) .
N2 C13 1.483(3) .
N2 C11 1.501(3) .
N2 Dy1 2.752(2) 3
N3 C21 1.478(3) .
N3 C13 1.483(3) .
N3 C12 1.492(3) .
N4 C23 1.276(4) .
N4 C22 1.467(3) .
N5 C32 1.126(5) .
N6 C34 1.115(5) .
O1 C1 1.299(3) .
O2 C2 1.369(4) .
O2 C7 1.428(4) .
O3 C19 1.344(3) .
O3 Dy1 2.3220(19) 3
O4 C18 1.364(3) .
O4 C20 1.415(3) .
O5 C29 1.299(3) .
O6 C28 1.373(3) .
O6 C30 1.415(3) .
C1 C6 1.415(4) .
C1 C2 1.430(4) .
C2 C3 1.379(4) .
C3 C4 1.388(5) .
C3 H3 0.9500 .
C4 C5 1.368(4) .
C4 H4 0.9500 .
C5 C6 1.403(4) .
C5 H5 0.9500 .
C6 C8 1.443(4) .
C7 H7A 0.9800 .
C7 H7B 0.9800 .
C7 H7C 0.9800 .
C8 H8 0.9500 .
C9 C10 1.513(4) 3
C9 H9A 0.9900 .
C9 H9B 0.9900 .
C10 C9 1.513(4) 3
C10 H10A 0.9900 .
C10 H10B 0.9900 .
C11 C12 1.526(4) .
C11 H11A 0.9900 .
C11 H11B 0.9900 .
C12 H12A 0.9900 .
C12 H12B 0.9900 .
C13 C14 1.499(4) .
C13 H13 1.0000 .
C14 C19 1.397(4) .
C14 C15 1.399(4) .
C15 C16 1.364(4) .
C15 H15 0.9500 .
C16 C17 1.393(4) .
C16 H16 0.9500 .
C17 C18 1.386(4) .
C17 H17 0.9500 .
C18 C19 1.405(4) .
C20 H20A 0.9800 .
C20 H20B 0.9800 .
C20 H20C 0.9800 .
C21 C22 1.501(4) .
C21 H21A 0.9900 .
C21 H21B 0.9900 .
C22 H22A 0.9900 .
C22 H22B 0.9900 .
C23 C24 1.440(4) .
C23 H23 0.9500 .
C24 C25 1.416(4) .
C24 C29 1.416(4) .
C25 C26 1.364(4) .
C25 H25 0.9500 .
C26 C27 1.399(4) .
C26 H26 0.9500 .
C27 C28 1.366(4) .
C27 H27 0.9500 .
C28 C29 1.431(4) .
C30 H30A 0.9800 .
C30 H30B 0.9800 .
C30 H30C 0.9800 .
C31 C32 1.444(5) .
C31 H31A 0.9800 .
C31 H31B 0.9800 .
C31 H31C 0.9800 .
C33 C34 1.446(6) .
C33 H33A 0.9800 .
C33 H33B 0.9800 .
C33 H33C 0.9800 .
