#------------------------------------------------------------------------------
#$Date: 2016-02-16 03:10:39 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176453 $
#$URL: svn://www.crystallography.net/cod/cif/7/21/04/7210494.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7210494
loop_
_publ_author_name
'Wu, Jing-Yun'
'Huang, Sheng-Ming'
_publ_section_title
;
 Homochiral transition-metal camphorate coordination architectures
 containing "piperazine--pyridine" ligands
;
_journal_issue                   6
_journal_name_full               CrystEngComm
_journal_page_first              2062
_journal_page_last               2070
_journal_paper_doi               10.1039/c0ce00552e
_journal_volume                  13
_journal_year                    2011
_chemical_formula_sum            'C34 H47 Co2 N4 O9.5'
_chemical_formula_weight         781.62
_chemical_name_systematic
;
?
;
_space_group_IT_number           4
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 112.40(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   10.568(2)
_cell_length_b                   13.363(3)
_cell_length_c                   13.111(3)
_cell_measurement_reflns_used    4857
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      25.05
_cell_measurement_theta_min      3.21
_cell_volume                     1711.8(7)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0229
_diffrn_reflns_av_sigmaI/netI    0.0387
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            11006
_diffrn_reflns_theta_full        25.05
_diffrn_reflns_theta_max         25.05
_diffrn_reflns_theta_min         1.68
_exptl_absorpt_coefficient_mu    1.031
_exptl_absorpt_correction_T_max  0.7452
_exptl_absorpt_correction_T_min  0.6685
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'Bruker SADABS, 1996'
_exptl_crystal_colour            blue
_exptl_crystal_density_diffrn    1.516
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             818
_exptl_crystal_size_max          0.10
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.05
_refine_diff_density_max         0.451
_refine_diff_density_min         -0.551
_refine_diff_density_rms         0.146
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.02(2)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.122
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     457
_refine_ls_number_reflns         5105
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.122
_refine_ls_R_factor_all          0.0440
_refine_ls_R_factor_gt           0.0355
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0573P)²+0.5477P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0913
_refine_ls_wR_factor_ref         0.1054
_reflns_number_gt                4456
_reflns_number_total             5105
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c0ce00552e.txt
_cod_data_source_block           cpd1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to the built-in table from CIF Core dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_cell_volume        1711.8(6)
_cod_original_sg_symbol_H-M      P2(1)
_cod_original_formula_sum        'C34 H47 Co2 N4 O9.50'
_cod_database_code               7210494
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Co1 Co 0.35946(6) 0.09851(4) 0.19068(5) 0.0193(2) Uani 1 1 d .
Co2 Co 0.64647(6) 0.05874(4) 0.31701(5) 0.0199(2) Uani 1 1 d .
O1 O 0.7410(4) 0.4754(3) -0.1015(3) 0.0244(9) Uani 1 1 d .
O2 O 0.5220(3) 0.4543(3) -0.1983(3) 0.0206(9) Uani 1 1 d .
O3 O 0.4291(3) 0.1493(3) 0.0767(3) 0.0222(9) Uani 1 1 d .
O4 O 0.6487(3) 0.1090(3) 0.1734(2) 0.0218(9) Uani 1 1 d .
O5 O 0.3563(3) 0.0459(3) 0.3347(3) 0.0215(9) Uani 1 1 d .
O6 O 0.5760(4) 0.0106(3) 0.4299(3) 0.0229(9) Uani 1 1 d .
O7 O 0.2559(4) -0.3120(3) 0.6022(3) 0.0253(9) Uani 1 1 d .
O8 O 0.4772(4) -0.3011(3) 0.6933(3) 0.0227(9) Uani 1 1 d .
N1 N 0.0444(5) 0.4813(4) 0.2312(3) 0.0240(11) Uani 1 1 d .
N2 N -0.0540(5) 0.6695(4) 0.2757(3) 0.0230(11) Uani 1 1 d .
N3 N 0.2229(4) 0.2139(4) 0.1802(3) 0.0217(11) Uani 1 1 d .
N4 N -0.2226(4) 0.9417(4) 0.3247(3) 0.0205(11) Uani 1 1 d .
C1 C 0.6509(5) 0.3084(5) -0.1047(4) 0.0208(12) Uani 1 1 d .
C2 C 0.6310(6) 0.2926(5) 0.0072(4) 0.0260(13) Uani 1 1 d .
C3 C 0.5957(5) 0.1793(5) -0.0025(4) 0.0224(13) Uani 1 1 d .
H3 H 0.6769 0.1416 0.0012 0.027 Uiso 1 1 calc R
C4 C 0.4873(6) 0.1698(5) -0.1187(4) 0.0350(15) Uani 1 1 d .
H4A H 0.3975 0.1875 -0.1203 0.042 Uiso 1 1 calc R
H4B H 0.4841 0.1022 -0.1465 0.042 Uiso 1 1 calc R
C5 C 0.5346(6) 0.2448(5) -0.1869(5) 0.0345(15) Uani 1 1 d .
H5A H 0.5674 0.2091 -0.2364 0.041 Uiso 1 1 calc R
H5B H 0.4590 0.2873 -0.2305 0.041 Uiso 1 1 calc R
C6 C 0.6364(6) 0.4189(5) -0.1370(4) 0.0218(13) Uani 1 1 d .
C7 C 0.5544(6) 0.1443(5) 0.0886(4) 0.0218(13) Uani 1 1 d .
C8 C 0.7906(5) 0.2722(4) -0.0988(5) 0.0417(14) Uani 1 1 d .
H8A H 0.7945 0.2765 -0.1706 0.062 Uiso 1 1 calc R
H8B H 0.8040 0.2040 -0.0740 0.062 Uiso 1 1 calc R
H8C H 0.8611 0.3133 -0.0481 0.062 Uiso 1 1 calc R
C9 C 0.7622(5) 0.3122(5) 0.1084(4) 0.0424(16) Uani 1 1 d .
H9A H 0.7948 0.3785 0.1041 0.064 Uiso 1 1 calc R
H9B H 0.8308 0.2642 0.1103 0.064 Uiso 1 1 calc R
H9C H 0.7433 0.3061 0.1741 0.064 Uiso 1 1 calc R
C10 C 0.5201(6) 0.3565(5) 0.0131(5) 0.0319(14) Uani 1 1 d .
H10A H 0.5004 0.3380 0.0763 0.048 Uiso 1 1 calc R
H10B H 0.4395 0.3479 -0.0526 0.048 Uiso 1 1 calc R
H10C H 0.5482 0.4253 0.0196 0.048 Uiso 1 1 calc R
C11 C 0.4175(5) -0.0155(5) 0.5177(4) 0.0209(13) Uani 1 1 d .
C12 C 0.3536(5) -0.1225(5) 0.4998(4) 0.0224(13) Uani 1 1 d .
C13 C 0.3604(5) -0.1495(5) 0.6183(4) 0.0211(13) Uani 1 1 d .
H13 H 0.2782 -0.1226 0.6259 0.025 Uiso 1 1 calc R
C14 C 0.4866(6) -0.0910(5) 0.6990(4) 0.0262(14) Uani 1 1 d .
H14A H 0.4600 -0.0494 0.7481 0.031 Uiso 1 1 calc R
H14B H 0.5569 -0.1373 0.7431 0.031 Uiso 1 1 calc R
C15 C 0.5399(6) -0.0262(5) 0.6277(4) 0.0288(14) Uani 1 1 d .
H15A H 0.6161 -0.0585 0.6170 0.035 Uiso 1 1 calc R
H15B H 0.5695 0.0387 0.6615 0.035 Uiso 1 1 calc R
C16 C 0.4539(5) 0.0167(5) 0.4193(4) 0.0203(12) Uani 1 1 d .
C17 C 0.3645(6) -0.2605(5) 0.6391(4) 0.0208(13) Uani 1 1 d .
C18 C 0.3219(5) 0.0654(4) 0.5339(4) 0.0337(12) Uani 1 1 d .
H18A H 0.3012 0.0489 0.5971 0.051 Uiso 1 1 calc R
H18B H 0.2386 0.0681 0.4695 0.051 Uiso 1 1 calc R
H18C H 0.3665 0.1294 0.5450 0.051 Uiso 1 1 calc R
C19 C 0.2048(5) -0.1278(5) 0.4160(4) 0.0414(16) Uani 1 1 d .
H19A H 0.2006 -0.1052 0.3453 0.062 Uiso 1 1 calc R
H19B H 0.1480 -0.0859 0.4404 0.062 Uiso 1 1 calc R
H19C H 0.1728 -0.1956 0.4100 0.062 Uiso 1 1 calc R
C20 C 0.4399(6) -0.1968(5) 0.4631(4) 0.0294(14) Uani 1 1 d .
H20A H 0.4011 -0.2626 0.4566 0.044 Uiso 1 1 calc R
H20B H 0.5320 -0.1977 0.5168 0.044 Uiso 1 1 calc R
H20C H 0.4402 -0.1764 0.3930 0.044 Uiso 1 1 calc R
C21 C 0.0479(7) 0.5044(5) 0.3402(5) 0.0393(17) Uani 1 1 d .
H21A H 0.1381 0.5292 0.3856 0.047 Uiso 1 1 calc R
H21B H 0.0321 0.4436 0.3740 0.047 Uiso 1 1 calc R
C22 C -0.0563(6) 0.5802(5) 0.3373(5) 0.0376(17) Uani 1 1 d .
H22A H -0.1463 0.5500 0.3049 0.045 Uiso 1 1 calc R
H22B H -0.0416 0.5991 0.4123 0.045 Uiso 1 1 calc R
C23 C -0.0587(6) 0.6434(5) 0.1657(4) 0.0313(14) Uani 1 1 d .
H23A H -0.0481 0.7037 0.1286 0.038 Uiso 1 1 calc R
H23B H -0.1475 0.6148 0.1226 0.038 Uiso 1 1 calc R
C24 C 0.0515(6) 0.5699(6) 0.1706(5) 0.0402(18) Uani 1 1 d .
H24A H 0.0410 0.5513 0.0962 0.048 Uiso 1 1 calc R
H24B H 0.1405 0.6010 0.2059 0.048 Uiso 1 1 calc R
C25 C 0.1766(5) 0.2257(5) 0.2623(4) 0.0255(14) Uani 1 1 d .
H25 H 0.1844 0.1713 0.3086 0.031 Uiso 1 1 calc R
C26 C 0.1193(5) 0.3110(5) 0.2831(5) 0.0249(13) Uani 1 1 d .
H26 H 0.0928 0.3142 0.3430 0.030 Uiso 1 1 calc R
C27 C 0.1012(5) 0.3934(5) 0.2130(4) 0.0215(13) Uani 1 1 d .
C28 C 0.1458(5) 0.3810(5) 0.1265(4) 0.0221(13) Uani 1 1 d .
H28 H 0.1364 0.4333 0.0774 0.026 Uiso 1 1 calc R
C29 C 0.2032(5) 0.2930(5) 0.1132(4) 0.0245(14) Uani 1 1 d .
H29 H 0.2304 0.2876 0.0538 0.029 Uiso 1 1 calc R
C30 C -0.1754(5) 0.9294(5) 0.2441(4) 0.0257(14) Uani 1 1 d .
H30 H -0.1813 0.9833 0.1976 0.031 Uiso 1 1 calc R
C31 C -0.1196(6) 0.8431(5) 0.2266(4) 0.0272(14) Uani 1 1 d .
H31 H -0.0873 0.8402 0.1699 0.033 Uiso 1 1 calc R
C32 C -0.1091(5) 0.7575(5) 0.2921(4) 0.0197(13) Uani 1 1 d .
C33 C -0.1541(5) 0.7716(5) 0.3793(4) 0.0221(13) Uani 1 1 d .
H33 H -0.1458 0.7202 0.4292 0.027 Uiso 1 1 calc R
C34 C -0.2104(5) 0.8617(4) 0.3903(4) 0.0196(13) Uani 1 1 d .
H34 H -0.2423 0.8678 0.4470 0.023 Uiso 1 1 calc R
O9 O -0.0037(5) 0.0202(5) 0.0997(4) 0.0706(18) Uani 1 1 d .
H101 H -0.0448 0.0485 0.1411 0.106 Uiso 1 1 d R
H102 H 0.0709 0.0474 0.1021 0.106 Uiso 1 1 d R
O10 O 0.9885(7) 0.1418(7) 0.3914(6) 0.0303(19) Uani 0.50 1 d P
H103 H 0.9272 0.1726 0.4066 0.045 Uiso 0.50 1 d PR
H104 H 0.9515 0.0913 0.3476 0.045 Uiso 0.50 1 d PR
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O3 Co1 O5 161.16(14) . .
O3 Co1 O1 95.89(15) . 2_645
O5 Co1 O1 93.64(15) . 2_645
O3 Co1 N3 98.14(18) . .
O5 Co1 N3 93.51(16) . .
O1 Co1 N3 111.07(17) 2_645 .
O3 Co1 O8 84.16(14) . 2_656
O5 Co1 O8 81.85(14) . 2_656
O1 Co1 O8 162.28(15) 2_645 2_656
N3 Co1 O8 86.38(16) . 2_656
O3 Co1 O2 88.12(15) . 2_645
O5 Co1 O2 82.52(15) . 2_645
O1 Co1 O2 60.40(14) 2_645 2_645
N3 Co1 O2 170.10(16) . 2_645
O8 Co1 O2 101.94(13) 2_656 2_645
O3 Co1 C6 93.64(17) . 2_645
O5 Co1 C6 86.43(17) . 2_645
O1 Co1 C6 30.37(16) 2_645 2_645
N3 Co1 C6 140.99(18) . 2_645
O8 Co1 C6 131.92(16) 2_656 2_645
O2 Co1 C6 30.08(15) 2_645 2_645
O3 Co1 Co2 83.53(10) . .
O5 Co1 Co2 77.83(10) . .
O1 Co1 Co2 112.23(11) 2_645 .
N3 Co1 Co2 136.25(12) . .
O8 Co1 Co2 50.10(10) 2_656 .
O2 Co1 Co2 51.84(9) 2_645 .
C6 Co1 Co2 81.87(13) 2_645 .
O6 Co2 O4 160.48(14) . .
O6 Co2 N4 98.74(18) . 1_645
O4 Co2 N4 92.98(16) . 1_645
O6 Co2 O7 98.17(16) . 2_656
O4 Co2 O7 91.09(16) . 2_656
N4 Co2 O7 114.24(17) 1_645 2_656
O6 Co2 O8 86.60(15) . 2_656
O4 Co2 O8 83.10(15) . 2_656
N4 Co2 O8 173.11(16) 1_645 2_656
O7 Co2 O8 60.38(14) 2_656 2_656
O6 Co2 O2 84.06(14) . 2_645
O4 Co2 O2 81.55(14) . 2_645
N4 Co2 O2 84.60(15) 1_645 2_645
O7 Co2 O2 160.23(15) 2_656 2_645
O8 Co2 O2 100.35(13) 2_656 2_645
O6 Co2 C17 94.43(17) . 2_656
O4 Co2 C17 84.87(17) . 2_656
N4 Co2 C17 144.20(18) 1_645 2_656
O7 Co2 C17 30.44(15) 2_656 2_656
O8 Co2 C17 30.03(15) 2_656 2_656
O2 Co2 C17 130.00(16) 2_645 2_656
O6 Co2 Co1 83.00(10) . .
O4 Co2 Co1 77.67(9) . .
N4 Co2 Co1 134.63(12) 1_645 .
O7 Co2 Co1 110.28(11) 2_656 .
O8 Co2 Co1 50.06(10) 2_656 .
O2 Co2 Co1 50.28(10) 2_645 .
C17 Co2 Co1 79.84(13) 2_656 .
C6 O1 Co1 94.5(3) . 2_655
C6 O2 Co1 84.9(3) . 2_655
C6 O2 Co2 162.4(4) . 2_655
Co1 O2 Co2 77.88(13) 2_655 2_655
C7 O3 Co1 123.1(3) . .
C7 O4 Co2 131.4(3) . .
C16 O5 Co1 129.2(3) . .
C16 O6 Co2 123.9(4) . .
C17 O7 Co2 93.1(3) . 2_646
C17 O8 Co1 163.0(4) . 2_646
C17 O8 Co2 85.5(3) . 2_646
Co1 O8 Co2 79.83(14) 2_646 2_646
C27 N1 C24 119.0(4) . .
C27 N1 C21 120.2(5) . .
C24 N1 C21 112.4(5) . .
C32 N2 C22 121.6(4) . .
C32 N2 C23 120.2(5) . .
C22 N2 C23 110.6(5) . .
C29 N3 C25 114.7(5) . .
C29 N3 Co1 124.0(4) . .
C25 N3 Co1 119.2(4) . .
C30 N4 C34 115.6(5) . .
C30 N4 Co2 119.9(4) . 1_465
C34 N4 Co2 122.1(4) . 1_465
C8 C1 C6 108.2(5) . .
C8 C1 C5 110.9(5) . .
C6 C1 C5 111.7(5) . .
C8 C1 C2 112.3(4) . .
C6 C1 C2 110.7(5) . .
C5 C1 C2 102.9(5) . .
C10 C2 C9 109.2(5) . .
C10 C2 C3 113.4(5) . .
C9 C2 C3 110.3(5) . .
C10 C2 C1 111.2(5) . .
C9 C2 C1 112.7(4) . .
C3 C2 C1 99.7(5) . .
C7 C3 C4 115.9(5) . .
C7 C3 C2 112.0(5) . .
C4 C3 C2 103.2(5) . .
C3 C4 C5 103.8(5) . .
C1 C5 C4 107.4(4) . .
O2 C6 O1 120.0(6) . .
O2 C6 C1 120.6(5) . .
O1 C6 C1 119.4(5) . .
O2 C6 Co1 65.0(3) . 2_655
O1 C6 Co1 55.2(3) . 2_655
C1 C6 Co1 173.2(4) . 2_655
O4 C7 O3 124.0(5) . .
O4 C7 C3 116.5(5) . .
O3 C7 C3 119.4(5) . .
C15 C11 C16 115.0(4) . .
C15 C11 C18 107.3(4) . .
C16 C11 C18 107.7(4) . .
C15 C11 C12 102.5(4) . .
C16 C11 C12 111.2(4) . .
C18 C11 C12 113.1(4) . .
C19 C12 C20 108.2(5) . .
C19 C12 C11 114.5(5) . .
C20 C12 C11 111.3(4) . .
C19 C12 C13 110.2(4) . .
C20 C12 C13 110.6(5) . .
C11 C12 C13 102.0(4) . .
C17 C13 C14 114.3(5) . .
C17 C13 C12 113.2(5) . .
C14 C13 C12 105.1(4) . .
C15 C14 C13 106.7(4) . .
C14 C15 C11 104.6(4) . .
O6 C16 O5 125.9(5) . .
O6 C16 C11 117.7(5) . .
O5 C16 C11 116.4(4) . .
O8 C17 O7 120.6(6) . .
O8 C17 C13 119.0(5) . .
O7 C17 C13 120.4(5) . .
O8 C17 Co2 64.5(3) . 2_646
O7 C17 Co2 56.4(3) . 2_646
C13 C17 Co2 173.9(4) . 2_646
N1 C21 C22 112.3(5) . .
N2 C22 C21 114.0(5) . .
N2 C23 C24 112.2(5) . .
N1 C24 C23 110.9(5) . .
N3 C25 C26 125.5(6) . .
C25 C26 C27 119.0(5) . .
N1 C27 C28 123.1(5) . .
N1 C27 C26 121.0(5) . .
C28 C27 C26 115.9(6) . .
C29 C28 C27 120.7(6) . .
N3 C29 C28 124.2(5) . .
N4 C30 C31 123.7(6) . .
C30 C31 C32 121.7(5) . .
N2 C32 C33 122.6(5) . .
N2 C32 C31 122.8(5) . .
C33 C32 C31 114.5(5) . .
C34 C33 C32 119.7(5) . .
N4 C34 C33 124.6(5) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Co1 O3 2.019(4) .
Co1 O5 2.027(3) .
Co1 O1 2.063(4) 2_645
Co1 N3 2.080(5) .
Co1 O8 2.257(4) 2_656
Co1 O2 2.280(4) 2_645
Co1 C6 2.506(6) 2_645
Co1 Co2 2.8976(12) .
Co2 O6 2.000(3) .
Co2 O4 2.007(3) .
Co2 N4 2.065(5) 1_645
Co2 O7 2.082(4) 2_656
Co2 O8 2.259(4) 2_656
Co2 O2 2.330(4) 2_645
Co2 C17 2.496(6) 2_656
O1 C6 1.271(7) .
O1 Co1 2.063(4) 2_655
O2 C6 1.261(6) .
O2 Co1 2.280(4) 2_655
O2 Co2 2.330(4) 2_655
O3 C7 1.274(6) .
O4 C7 1.268(6) .
O5 C16 1.254(6) .
O6 C16 1.247(6) .
O7 C17 1.266(7) .
O7 Co2 2.082(4) 2_646
O8 C17 1.253(6) .
O8 Co1 2.257(4) 2_646
O8 Co2 2.259(4) 2_646
N1 C27 1.381(8) .
N1 C24 1.445(8) .
N1 C21 1.448(7) .
N2 C32 1.366(7) .
N2 C22 1.446(8) .
N2 C23 1.467(7) .
N3 C29 1.339(7) .
N3 C25 1.351(7) .
N4 C30 1.339(7) .
N4 C34 1.347(7) .
N4 Co2 2.065(5) 1_465
C1 C8 1.528(7) .
C1 C6 1.528(8) .
C1 C5 1.544(9) .
C1 C2 1.573(7) .
C2 C10 1.477(9) .
C2 C9 1.533(7) .
C2 C3 1.553(8) .
C3 C7 1.494(7) .
C3 C4 1.523(7) .
C4 C5 1.547(8) .
C6 Co1 2.506(6) 2_655
C11 C15 1.533(7) .
C11 C16 1.542(7) .
C11 C18 1.549(7) .
C11 C12 1.560(9) .
C12 C19 1.540(7) .
C12 C20 1.544(8) .
C12 C13 1.569(7) .
C13 C17 1.507(8) .
C13 C14 1.560(7) .
C14 C15 1.531(8) .
C17 Co2 2.496(6) 2_646
C21 C22 1.485(8) .
C23 C24 1.506(8) .
C25 C26 1.365(8) .
C26 C27 1.400(8) .
C27 C28 1.394(7) .
C28 C29 1.365(9) .
C30 C31 1.355(9) .
C31 C32 1.409(8) .
C32 C33 1.407(7) .
C33 C34 1.375(8) .
