#------------------------------------------------------------------------------
#$Date: 2016-03-26 20:55:11 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180455 $
#$URL: svn://www.crystallography.net/cod/cif/7/21/24/7212484.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7212484
loop_
_publ_author_name
'Luo, Feng'
'Ning, Yang'
'Luo, Ming-biao'
'Huang, Guo-lin'
_publ_section_title
;
 Chiral or achiral camphorate-based complexes controlled by the
 conformational rigidity of N-donor co-ligands
;
_journal_issue                   10
_journal_name_full               CrystEngComm
_journal_page_first              2769
_journal_paper_doi               10.1039/c000734j
_journal_volume                  12
_journal_year                    2010
_chemical_formula_sum            'C32 H34 N6 O8 Zn3'
_chemical_formula_weight         826.76
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                107.17(3)
_cell_angle_beta                 104.62(3)
_cell_angle_gamma                93.42(3)
_cell_formula_units_Z            1
_cell_length_a                   9.0548(18)
_cell_length_b                   9.1122(18)
_cell_length_c                   11.912(2)
_cell_measurement_reflns_used    5283
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.50
_cell_measurement_theta_min      3.08
_cell_volume                     899.0(4)
_computing_cell_refinement       'Bruker XSCANS'
_computing_data_collection       'Bruker XSCANS'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.986
_diffrn_measured_fraction_theta_max 0.986
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0825
_diffrn_reflns_av_sigmaI/netI    0.1097
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_number            8802
_diffrn_reflns_theta_full        27.50
_diffrn_reflns_theta_max         27.50
_diffrn_reflns_theta_min         3.08
_exptl_absorpt_coefficient_mu    2.041
_exptl_absorpt_correction_T_max  0.7773
_exptl_absorpt_correction_T_min  0.6857
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            Colorless
_exptl_crystal_density_diffrn    1.527
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             422
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.13
_refine_diff_density_max         1.081
_refine_diff_density_min         -1.319
_refine_diff_density_rms         0.147
_refine_ls_extinction_coef       0.043(6)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.048
_refine_ls_hydrogen_treatment    refU
_refine_ls_matrix_type           full
_refine_ls_number_parameters     238
_refine_ls_number_reflns         4074
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.048
_refine_ls_R_factor_all          0.1131
_refine_ls_R_factor_gt           0.0731
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1016P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1797
_refine_ls_wR_factor_ref         0.2070
_reflns_number_gt                2538
_reflns_number_total             4074
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c000734j.txt
_cod_data_source_block           3
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from
2011-04-26.

'_exptl_absorpt_correction_type' value 'Multi-scan'
changed to 'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.2 from
2011-04-26.

'_refine_ls_hydrogen_treatment' value 'refu' changed to
'refU' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_cell_volume        899.0(3)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7212484
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.5932(8) 0.3030(7) 0.7334(6) 0.0441(15) Uani 1 1 d . . .
C2 C 0.6014(8) 0.4615(8) 0.7567(6) 0.0467(16) Uani 1 1 d . . .
C3 C 0.6503(12) 0.5689(9) 0.8763(8) 0.078(3) Uani 1 1 d . . .
H3 H 0.6599 0.6757 0.8916 0.094 Uiso 1 1 calc R . .
C4 C 0.6826(14) 0.5038(10) 0.9682(8) 0.097(4) Uani 1 1 d . . .
H4 H 0.7129 0.5690 1.0490 0.117 Uiso 1 1 calc R . .
C5 C 0.6720(13) 0.3448(10) 0.9458(8) 0.088(3) Uani 1 1 d . . .
H5 H 0.6960 0.3082 1.0124 0.106 Uiso 1 1 calc R . .
C6 C 0.6282(9) 0.2402(8) 0.8312(7) 0.058(2) Uani 1 1 d . . .
H6 H 0.6215 0.1338 0.8176 0.070 Uiso 1 1 calc R . .
C7 C 0.3346(7) -0.1155(7) 0.6879(6) 0.0404(14) Uani 1 1 d . A .
C8 C 0.2213(7) -0.0403(7) 0.7532(6) 0.0387(14) Uani 1 1 d . . .
C9 C 0.1841(8) 0.1102(7) 0.7259(9) 0.061(2) Uani 1 1 d . A .
H9A H 0.2566 0.1984 0.7849 0.073 Uiso 1 1 calc R . .
H9B H 0.1898 0.1037 0.6444 0.073 Uiso 1 1 calc R . .
C10 C 0.0209(8) 0.1272(8) 0.7353(8) 0.0548(19) Uani 1 1 d . . .
H10A H -0.0427 0.1402 0.6611 0.066 Uiso 1 1 calc R A .
H10B H 0.0226 0.2175 0.8040 0.066 Uiso 1 1 calc R . .
C11 C -0.0447(7) -0.0207(7) 0.7539(6) 0.0372(13) Uani 1 1 d . A .
C12 C 0.2973(15) 0.0023(16) 0.8858(13) 0.043(4) Uani 0.467(13) 1 d P A 1
H12A H 0.3269 -0.0886 0.9055 0.064 Uiso 0.467(13) 1 calc PR A 1
H12B H 0.2271 0.0458 0.9306 0.064 Uiso 0.467(13) 1 calc PR A 1
H12C H 0.3873 0.0774 0.9077 0.064 Uiso 0.467(13) 1 calc PR A 1
C13 C 0.0611(7) -0.1441(6) 0.7085(6) 0.0387(14) Uani 1 1 d . A .
C14 C 0.0080(8) -0.2125(9) 0.5690(7) 0.0572(19) Uani 1 1 d . . .
H14A H 0.0779 -0.2805 0.5418 0.086 Uiso 1 1 calc R A .
H14B H 0.0064 -0.1301 0.5340 0.086 Uiso 1 1 calc R . .
H14C H -0.0937 -0.2699 0.5435 0.086 Uiso 1 1 calc R . .
C15 C 0.0598(9) -0.2742(9) 0.7640(8) 0.061(2) Uani 1 1 d . . .
H15A H -0.0444 -0.3230 0.7450 0.092 Uiso 1 1 calc R A .
H15B H 0.1027 -0.2323 0.8513 0.092 Uiso 1 1 calc R . .
H15C H 0.1203 -0.3495 0.7308 0.092 Uiso 1 1 calc R . .
C16 C -0.2129(7) -0.0790(6) 0.6835(6) 0.0350(13) Uani 1 1 d . . .
C12' C -0.0236(16) 0.014(2) 0.8886(14) 0.067(5) Uani 0.533(13) 1 d P A 2
H12D H -0.0864 0.0912 0.9151 0.100 Uiso 0.533(13) 1 calc PR A 2
H12E H 0.0828 0.0532 0.9323 0.100 Uiso 0.533(13) 1 calc PR A 2
H12F H -0.0535 -0.0786 0.9045 0.100 Uiso 0.533(13) 1 calc PR A 2
N1 N 0.5585(7) 0.4862(6) 0.6455(5) 0.0466(14) Uani 1 1 d . . .
N3 N 0.5253(5) 0.3466(5) 0.5607(4) 0.0366(12) Uani 1 1 d . . .
N4 N 0.5461(6) 0.2341(5) 0.6116(5) 0.0375(12) Uani 1 1 d . . .
O1 O 0.3748(6) -0.2395(5) 0.7052(5) 0.0557(13) Uani 1 1 d . . .
O2 O 0.3893(6) -0.0550(5) 0.6226(5) 0.0534(12) Uani 1 1 d . . .
O3 O -0.2736(5) -0.1847(5) 0.7140(4) 0.0501(12) Uani 1 1 d . . .
O4 O -0.2799(5) -0.0260(5) 0.6033(4) 0.0458(11) Uani 1 1 d . . .
Zn1 Zn 0.5000 0.0000 0.5000 0.0355(3) Uani 1 2 d S . .
Zn2 Zn 0.52926(8) -0.30704(7) 0.62099(7) 0.0372(3) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N4 C1 C2 108.1(5) . .
N4 C1 C6 131.3(6) . .
C2 C1 C6 120.6(6) . .
N1 C2 C1 107.1(6) . .
N1 C2 C3 130.1(6) . .
C1 C2 C3 122.7(6) . .
C4 C3 C2 114.9(7) . .
C4 C3 H3 122.6 . .
C2 C3 H3 122.6 . .
C3 C4 C5 122.8(8) . .
C3 C4 H4 118.6 . .
C5 C4 H4 118.6 . .
C6 C5 C4 123.0(8) . .
C6 C5 H5 118.5 . .
C4 C5 H5 118.5 . .
C5 C6 C1 115.9(6) . .
C5 C6 H6 122.0 . .
C1 C6 H6 122.0 . .
O2 C7 O1 121.5(6) . .
O2 C7 C8 121.4(5) . .
O1 C7 C8 117.0(6) . .
C12 C8 C7 106.9(7) . .
C12 C8 C9 107.3(8) . .
C7 C8 C9 111.7(5) . .
C12 C8 C13 114.7(7) . .
C7 C8 C13 112.3(5) . .
C9 C8 C13 103.9(5) . .
C10 C9 C8 106.3(5) . .
C10 C9 H9A 110.5 . .
C8 C9 H9A 110.5 . .
C10 C9 H9B 110.5 . .
C8 C9 H9B 110.5 . .
H9A C9 H9B 108.7 . .
C9 C10 C11 107.7(5) . .
C9 C10 H10A 110.2 . .
C11 C10 H10A 110.2 . .
C9 C10 H10B 110.2 . .
C11 C10 H10B 110.2 . .
H10A C10 H10B 108.5 . .
C12' C11 C16 110.2(7) . .
C12' C11 C10 107.2(8) . .
C16 C11 C10 114.2(5) . .
C12' C11 C13 110.4(7) . .
C16 C11 C13 110.7(5) . .
C10 C11 C13 104.0(5) . .
C8 C12 H12A 109.5 . .
C8 C12 H12B 109.5 . .
C8 C12 H12C 109.5 . .
C15 C13 C14 109.5(6) . .
C15 C13 C8 112.9(6) . .
C14 C13 C8 111.1(5) . .
C15 C13 C11 112.0(5) . .
C14 C13 C11 110.0(5) . .
C8 C13 C11 101.2(4) . .
C13 C14 H14A 109.5 . .
C13 C14 H14B 109.5 . .
H14A C14 H14B 109.5 . .
C13 C14 H14C 109.5 . .
H14A C14 H14C 109.5 . .
H14B C14 H14C 109.5 . .
C13 C15 H15A 109.5 . .
C13 C15 H15B 109.5 . .
H15A C15 H15B 109.5 . .
C13 C15 H15C 109.5 . .
H15A C15 H15C 109.5 . .
H15B C15 H15C 109.5 . .
O4 C16 O3 125.0(6) . .
O4 C16 C11 121.0(5) . .
O3 C16 C11 114.0(5) . .
C11 C12' H12D 109.5 . .
C11 C12' H12E 109.5 . .
H12D C12' H12E 109.5 . .
C11 C12' H12F 109.5 . .
H12D C12' H12F 109.5 . .
H12E C12' H12F 109.5 . .
N3 N1 C2 106.3(5) . .
N3 N1 Zn2 127.9(4) . 1_565
C2 N1 Zn2 125.4(4) . 1_565
N1 N3 N4 111.3(5) . .
N1 N3 Zn2 125.1(4) . 2_656
N4 N3 Zn2 123.3(4) . 2_656
N3 N4 C1 107.1(5) . .
N3 N4 Zn1 120.0(4) . .
C1 N4 Zn1 132.9(4) . .
C7 O1 Zn2 109.6(4) . .
C7 O2 Zn1 167.4(4) . .
C16 O3 Zn2 123.0(4) . 1_455
C16 O4 Zn1 144.3(4) . 1_455
N4 Zn1 N4 180.00(14) . 2_656
N4 Zn1 O2 90.69(19) . 2_656
N4 Zn1 O2 89.31(19) 2_656 2_656
N4 Zn1 O2 89.31(19) . .
N4 Zn1 O2 90.69(19) 2_656 .
O2 Zn1 O2 180.000(1) 2_656 .
N4 Zn1 O4 92.99(18) . 2_556
N4 Zn1 O4 87.01(18) 2_656 2_556
O2 Zn1 O4 92.22(18) 2_656 2_556
O2 Zn1 O4 87.78(18) . 2_556
N4 Zn1 O4 87.01(18) . 1_655
N4 Zn1 O4 92.99(18) 2_656 1_655
O2 Zn1 O4 87.78(18) 2_656 1_655
O2 Zn1 O4 92.22(18) . 1_655
O4 Zn1 O4 180.0(3) 2_556 1_655
O3 Zn2 O1 109.7(2) 1_655 .
O3 Zn2 N3 115.6(2) 1_655 2_656
O1 Zn2 N3 118.3(2) . 2_656
O3 Zn2 N1 102.0(2) 1_655 1_545
O1 Zn2 N1 102.7(2) . 1_545
N3 Zn2 N1 106.16(19) 2_656 1_545
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 N4 1.341(8) .
C1 C2 1.381(9) .
C1 C6 1.420(9) .
C2 N1 1.372(8) .
C2 C3 1.411(11) .
C3 C4 1.371(11) .
C3 H3 0.9300 .
C4 C5 1.386(11) .
C4 H4 0.9300 .
C5 C6 1.358(11) .
C5 H5 0.9300 .
C6 H6 0.9300 .
C7 O2 1.253(7) .
C7 O1 1.266(7) .
C7 C8 1.516(8) .
C8 C12 1.475(15) .
C8 C9 1.537(8) .
C8 C13 1.560(8) .
C9 C10 1.524(9) .
C9 H9A 0.9700 .
C9 H9B 0.9700 .
C10 C11 1.538(8) .
C10 H10A 0.9700 .
C10 H10B 0.9700 .
C11 C12' 1.499(15) .
C11 C16 1.517(8) .
C11 C13 1.583(7) .
C12 H12A 0.9600 .
C12 H12B 0.9600 .
C12 H12C 0.9600 .
C13 C15 1.519(8) .
C13 C14 1.526(9) .
C14 H14A 0.9600 .
C14 H14B 0.9600 .
C14 H14C 0.9600 .
C15 H15A 0.9600 .
C15 H15B 0.9600 .
C15 H15C 0.9600 .
C16 O4 1.237(7) .
C16 O3 1.267(7) .
C12' H12D 0.9600 .
C12' H12E 0.9600 .
C12' H12F 0.9600 .
N1 N3 1.331(7) .
N1 Zn2 2.013(5) 1_565
N3 N4 1.336(6) .
N3 Zn2 2.009(5) 2_656
N4 Zn1 2.105(5) .
O1 Zn2 1.946(5) .
O2 Zn1 2.121(5) .
O3 Zn2 1.922(5) 1_455
O4 Zn1 2.129(4) 1_455
Zn1 N4 2.105(5) 2_656
Zn1 O2 2.121(5) 2_656
Zn1 O4 2.129(4) 2_556
Zn1 O4 2.129(4) 1_655
Zn2 O3 1.922(5) 1_655
Zn2 N3 2.009(5) 2_656
Zn2 N1 2.013(5) 1_545
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
N4 C1 C2 N1 -0.3(8) . .
C6 C1 C2 N1 -178.7(7) . .
N4 C1 C2 C3 -178.8(8) . .
C6 C1 C2 C3 2.8(12) . .
N1 C2 C3 C4 179.1(9) . .
C1 C2 C3 C4 -2.8(14) . .
C2 C3 C4 C5 1.6(18) . .
C3 C4 C5 C6 0(2) . .
C4 C5 C6 C1 0.1(16) . .
N4 C1 C6 C5 -179.4(8) . .
C2 C1 C6 C5 -1.3(12) . .
O2 C7 C8 C12 -115.8(8) . .
O1 C7 C8 C12 62.1(9) . .
O2 C7 C8 C9 1.2(9) . .
O1 C7 C8 C9 179.1(6) . .
O2 C7 C8 C13 117.5(7) . .
O1 C7 C8 C13 -64.6(8) . .
C12 C8 C9 C10 -92.2(8) . .
C7 C8 C9 C10 150.9(6) . .
C13 C8 C9 C10 29.6(8) . .
C8 C9 C10 C11 -6.1(8) . .
C9 C10 C11 C12' 97.6(8) . .
C9 C10 C11 C16 -140.0(6) . .
C9 C10 C11 C13 -19.3(7) . .
C12 C8 C13 C15 -43.7(9) . .
C7 C8 C13 C15 78.7(7) . .
C9 C8 C13 C15 -160.4(6) . .
C12 C8 C13 C14 -167.1(7) . .
C7 C8 C13 C14 -44.8(7) . .
C9 C8 C13 C14 76.1(6) . .
C12 C8 C13 C11 76.2(8) . .
C7 C8 C13 C11 -161.5(5) . .
C9 C8 C13 C11 -40.6(6) . .
C12' C11 C13 C15 42.4(10) . .
C16 C11 C13 C15 -79.8(7) . .
C10 C11 C13 C15 157.1(6) . .
C12' C11 C13 C14 164.4(8) . .
C16 C11 C13 C14 42.2(7) . .
C10 C11 C13 C14 -80.9(6) . .
C12' C11 C13 C8 -78.1(8) . .
C16 C11 C13 C8 159.7(5) . .
C10 C11 C13 C8 36.6(6) . .
C12' C11 C16 O4 132.4(9) . .
C10 C11 C16 O4 11.7(8) . .
C13 C11 C16 O4 -105.3(6) . .
C12' C11 C16 O3 -48.3(9) . .
C10 C11 C16 O3 -169.0(5) . .
C13 C11 C16 O3 74.1(6) . .
C1 C2 N1 N3 0.5(7) . .
C3 C2 N1 N3 178.9(9) . .
C1 C2 N1 Zn2 174.1(5) . 1_565
C3 C2 N1 Zn2 -7.6(12) . 1_565
C2 N1 N3 N4 -0.6(7) . .
Zn2 N1 N3 N4 -173.9(4) 1_565 .
C2 N1 N3 Zn2 -175.0(4) . 2_656
Zn2 N1 N3 Zn2 11.7(8) 1_565 2_656
N1 N3 N4 C1 0.5(7) . .
Zn2 N3 N4 C1 175.0(4) 2_656 .
N1 N3 N4 Zn1 179.3(4) . .
Zn2 N3 N4 Zn1 -6.2(6) 2_656 .
C2 C1 N4 N3 -0.1(7) . .
C6 C1 N4 N3 178.1(7) . .
C2 C1 N4 Zn1 -178.7(5) . .
C6 C1 N4 Zn1 -0.5(12) . .
O2 C7 O1 Zn2 1.4(8) . .
C8 C7 O1 Zn2 -176.5(4) . .
O1 C7 O2 Zn1 13(3) . .
C8 C7 O2 Zn1 -169.3(18) . .
O4 C16 O3 Zn2 11.4(8) . 1_455
C11 C16 O3 Zn2 -167.9(4) . 1_455
O3 C16 O4 Zn1 20.6(11) . 1_455
C11 C16 O4 Zn1 -160.2(5) . 1_455
N3 N4 Zn1 N4 -126(100) . 2_656
C1 N4 Zn1 N4 52(100) . 2_656
N3 N4 Zn1 O2 43.3(4) . 2_656
C1 N4 Zn1 O2 -138.3(6) . 2_656
N3 N4 Zn1 O2 -136.7(4) . .
C1 N4 Zn1 O2 41.7(6) . .
N3 N4 Zn1 O4 -49.0(4) . 2_556
C1 N4 Zn1 O4 129.4(6) . 2_556
N3 N4 Zn1 O4 131.0(4) . 1_655
C1 N4 Zn1 O4 -50.6(6) . 1_655
C7 O2 Zn1 N4 -149(2) . .
C7 O2 Zn1 N4 31(2) . 2_656
C7 O2 Zn1 O2 59(100) . 2_656
C7 O2 Zn1 O4 118(2) . 2_556
C7 O2 Zn1 O4 -62(2) . 1_655
C7 O1 Zn2 O3 77.9(5) . 1_655
C7 O1 Zn2 N3 -57.7(5) . 2_656
C7 O1 Zn2 N1 -174.2(4) . 1_545
