#------------------------------------------------------------------------------
#$Date: 2016-03-26 20:55:11 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180455 $
#$URL: svn://www.crystallography.net/cod/cif/7/21/24/7212485.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7212485
loop_
_publ_author_name
'Luo, Feng'
'Ning, Yang'
'Luo, Ming-biao'
'Huang, Guo-lin'
_publ_section_title
;
 Chiral or achiral camphorate-based complexes controlled by the
 conformational rigidity of N-donor co-ligands
;
_journal_issue                   10
_journal_name_full               CrystEngComm
_journal_page_first              2769
_journal_paper_doi               10.1039/c000734j
_journal_volume                  12
_journal_year                    2010
_chemical_formula_sum            'C32 H34 Co3 N6 O8'
_chemical_formula_weight         807.44
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                106.73(3)
_cell_angle_beta                 103.76(3)
_cell_angle_gamma                95.01(3)
_cell_formula_units_Z            1
_cell_length_a                   9.0109(18)
_cell_length_b                   9.0814(18)
_cell_length_c                   11.788(2)
_cell_measurement_reflns_used    5524
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      27.48
_cell_measurement_theta_min      3.06
_cell_volume                     884.6(4)
_computing_cell_refinement       'Bruker XSCANS'
_computing_data_collection       'Bruker XSCANS'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0819
_diffrn_reflns_av_sigmaI/netI    0.1123
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            8817
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         3.06
_exptl_absorpt_coefficient_mu    1.447
_exptl_absorpt_correction_T_max  0.8342
_exptl_absorpt_correction_T_min  0.7607
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            Purple
_exptl_crystal_density_diffrn    1.516
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             413
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.13
_refine_diff_density_max         0.751
_refine_diff_density_min         -0.598
_refine_diff_density_rms         0.141
_refine_ls_extinction_coef       0.020(4)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.094
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     238
_refine_ls_number_reflns         4031
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.094
_refine_ls_R_factor_all          0.1150
_refine_ls_R_factor_gt           0.0700
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0560P)²+3.9354P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1756
_refine_ls_wR_factor_ref         0.1978
_reflns_number_gt                2620
_reflns_number_total             4031
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c000734j.txt
_cod_data_source_block           4
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from
2011-04-26.

'_exptl_absorpt_correction_type' value 'Multi-scan'
changed to 'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_cell_volume        884.6(3)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7212485
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.8309(7) 0.3748(8) 0.1881(6) 0.0309(14) Uani 1 1 d . A .
C2 C 0.7197(7) 0.4582(8) 0.2497(6) 0.0297(14) Uani 1 1 d . . .
C3 C 0.7949(15) 0.5066(17) 0.3856(13) 0.040(4) Uani 0.518(15) 1 d P A 1
H3A H 0.8041 0.4155 0.4109 0.059 Uiso 0.518(15) 1 calc PR A 1
H3B H 0.7327 0.5691 0.4289 0.059 Uiso 0.518(15) 1 calc PR A 1
H3C H 0.8960 0.5661 0.4042 0.059 Uiso 0.518(15) 1 calc PR A 1
C4 C 0.5468(9) 0.2293(10) 0.2706(9) 0.053(2) Uani 1 1 d . . .
H4A H 0.6081 0.1531 0.2414 0.079 Uiso 1 1 calc R A .
H4B H 0.4411 0.1798 0.2503 0.079 Uiso 1 1 calc R . .
H4C H 0.5862 0.2753 0.3584 0.079 Uiso 1 1 calc R . .
C5 C 0.5550(7) 0.3563(7) 0.2096(6) 0.0307(14) Uani 1 1 d . A .
C6 C 0.5030(9) 0.2797(10) 0.0685(7) 0.049(2) Uani 1 1 d . . .
H6A H 0.5064 0.3589 0.0296 0.074 Uiso 1 1 calc R A .
H6B H 0.3991 0.2238 0.0439 0.074 Uiso 1 1 calc R . .
H6C H 0.5711 0.2087 0.0442 0.074 Uiso 1 1 calc R . .
C7 C 0.4540(7) 0.4835(8) 0.2503(6) 0.0303(14) Uani 1 1 d . . .
C8 C 0.2846(7) 0.4279(7) 0.1816(6) 0.0294(14) Uani 1 1 d . A .
C9 C 0.5287(8) 0.6304(8) 0.2317(8) 0.0411(17) Uani 1 1 d . A .
H9A H 0.5370 0.7211 0.3022 0.049 Uiso 1 1 calc R . .
H9B H 0.4660 0.6469 0.1587 0.049 Uiso 1 1 calc R . .
C10 C 0.6908(8) 0.6055(8) 0.2172(8) 0.0445(19) Uani 1 1 d . A .
H10A H 0.6938 0.5926 0.1332 0.053 Uiso 1 1 calc R . .
H10B H 0.7685 0.6938 0.2723 0.053 Uiso 1 1 calc R . .
C11 C 1.0951(8) 0.8046(8) 0.2367(6) 0.0318(14) Uani 1 1 d . . .
C12 C 1.1295(10) 0.7426(9) 0.3359(7) 0.0477(19) Uani 1 1 d . . .
H12 H 1.1205 0.6358 0.3227 0.057 Uiso 1 1 calc R . .
C13 C 1.1760(12) 0.8471(10) 0.4503(8) 0.063(3) Uani 1 1 d . . .
H13 H 1.2035 0.8109 0.5173 0.076 Uiso 1 1 calc R . .
C14 C 1.1844(14) 1.0089(10) 0.4723(8) 0.072(3) Uani 1 1 d . . .
H14 H 1.2146 1.0753 0.5533 0.087 Uiso 1 1 calc R . .
C15 C 1.1501(12) 1.0710(9) 0.3798(8) 0.062(3) Uani 1 1 d . . .
H15 H 1.1570 1.1780 0.3947 0.074 Uiso 1 1 calc R . .
C16 C 1.1038(8) 0.9650(8) 0.2603(6) 0.0350(15) Uani 1 1 d . . .
C3' C 0.4697(16) 0.523(2) 0.3851(13) 0.045(5) Uani 0.482(15) 1 d P A 2
H3'1 H 0.4136 0.6058 0.4101 0.067 Uiso 0.482(15) 1 calc PR A 2
H3'2 H 0.5772 0.5549 0.4301 0.067 Uiso 0.482(15) 1 calc PR A 2
H3'3 H 0.4284 0.4325 0.4018 0.067 Uiso 0.482(15) 1 calc PR A 2
Co1 Co 1.0000 0.5000 0.0000 0.0248(3) Uani 1 2 d S . .
Co2 Co 0.97917(10) 0.80681(10) -0.12060(8) 0.0285(3) Uani 1 1 d . . .
N1 N 1.0468(6) 0.7352(6) 0.1131(5) 0.0267(11) Uani 1 1 d . . .
N2 N 1.0287(6) 0.8482(6) 0.0615(5) 0.0290(12) Uani 1 1 d . . .
N3 N 1.0609(7) 0.9887(6) 0.1486(5) 0.0341(13) Uani 1 1 d . . .
O1 O 0.8997(5) 0.4310(6) 0.1258(4) 0.0396(12) Uani 1 1 d . . .
O2 O 0.8607(6) 0.2473(6) 0.2069(5) 0.0453(13) Uani 1 1 d . . .
O3 O 0.2218(5) 0.4821(5) 0.0993(4) 0.0344(11) Uani 1 1 d . . .
O4 O 0.2176(5) 0.3232(6) 0.2116(5) 0.0368(11) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 C1 O2 120.0(6) . .
O1 C1 C2 121.8(6) . .
O2 C1 C2 118.0(6) . .
C3 C2 C1 106.3(7) . .
C3 C2 C10 107.4(8) . .
C1 C2 C10 112.8(6) . .
C3 C2 C5 113.3(7) . .
C1 C2 C5 112.4(5) . .
C10 C2 C5 104.6(5) . .
C2 C3 H3A 109.5 . .
C2 C3 H3B 109.5 . .
C2 C3 H3C 109.5 . .
C5 C4 H4A 109.5 . .
C5 C4 H4B 109.5 . .
H4A C4 H4B 109.5 . .
C5 C4 H4C 109.5 . .
H4A C4 H4C 109.5 . .
H4B C4 H4C 109.5 . .
C4 C5 C6 109.0(6) . .
C4 C5 C2 113.6(5) . .
C6 C5 C2 109.9(6) . .
C4 C5 C7 112.5(6) . .
C6 C5 C7 110.4(5) . .
C2 C5 C7 101.3(5) . .
C5 C6 H6A 109.5 . .
C5 C6 H6B 109.5 . .
H6A C6 H6B 109.5 . .
C5 C6 H6C 109.5 . .
H6A C6 H6C 109.5 . .
H6B C6 H6C 109.5 . .
C3' C7 C8 108.4(7) . .
C3' C7 C9 106.5(9) . .
C8 C7 C9 115.1(5) . .
C3' C7 C5 110.2(8) . .
C8 C7 C5 111.5(5) . .
C9 C7 C5 105.0(5) . .
O3 C8 O4 124.7(6) . .
O3 C8 C7 120.4(6) . .
O4 C8 C7 114.9(6) . .
C7 C9 C10 107.7(5) . .
C7 C9 H9A 110.2 . .
C10 C9 H9A 110.2 . .
C7 C9 H9B 110.2 . .
C10 C9 H9B 110.2 . .
H9A C9 H9B 108.5 . .
C2 C10 C9 105.6(6) . .
C2 C10 H10A 110.6 . .
C9 C10 H10A 110.6 . .
C2 C10 H10B 110.6 . .
C9 C10 H10B 110.6 . .
H10A C10 H10B 108.8 . .
N1 C11 C16 107.9(6) . .
N1 C11 C12 131.9(6) . .
C16 C11 C12 120.2(6) . .
C13 C12 C11 116.3(7) . .
C13 C12 H12 121.8 . .
C11 C12 H12 121.8 . .
C12 C13 C14 122.7(8) . .
C12 C13 H13 118.7 . .
C14 C13 H13 118.7 . .
C15 C14 C13 122.2(8) . .
C15 C14 H14 118.9 . .
C13 C14 H14 118.9 . .
C14 C15 C16 116.1(7) . .
C14 C15 H15 121.9 . .
C16 C15 H15 121.9 . .
N3 C16 C11 106.8(6) . .
N3 C16 C15 130.8(7) . .
C11 C16 C15 122.5(7) . .
C7 C3' H3'1 109.5 . .
C7 C3' H3'2 109.5 . .
H3'1 C3' H3'2 109.5 . .
C7 C3' H3'3 109.5 . .
H3'1 C3' H3'3 109.5 . .
H3'2 C3' H3'3 109.5 . .
O3 Co1 O3 180.0(3) 2_665 1_655
O3 Co1 N1 93.62(19) 2_665 .
O3 Co1 N1 86.38(19) 1_655 .
O3 Co1 N1 86.38(19) 2_665 2_765
O3 Co1 N1 93.62(19) 1_655 2_765
N1 Co1 N1 180.0(3) . 2_765
O3 Co1 O1 90.59(18) 2_665 2_765
O3 Co1 O1 89.41(18) 1_655 2_765
N1 Co1 O1 88.9(2) . 2_765
N1 Co1 O1 91.1(2) 2_765 2_765
O3 Co1 O1 89.41(18) 2_665 .
O3 Co1 O1 90.59(18) 1_655 .
N1 Co1 O1 91.1(2) . .
N1 Co1 O1 88.9(2) 2_765 .
O1 Co1 O1 180.0 2_765 .
O4 Co2 O2 111.2(2) 2_665 2_765
O4 Co2 N2 114.1(2) 2_665 .
O2 Co2 N2 119.9(2) 2_765 .
O4 Co2 N3 100.6(2) 2_665 2_775
O2 Co2 N3 101.9(2) 2_765 2_775
N2 Co2 N3 106.1(2) . 2_775
N2 N1 C11 107.4(5) . .
N2 N1 Co1 119.7(4) . .
C11 N1 Co1 132.9(4) . .
N1 N2 N3 110.5(5) . .
N1 N2 Co2 122.8(4) . .
N3 N2 Co2 126.5(4) . .
N2 N3 C16 107.4(5) . .
N2 N3 Co2 126.1(4) . 2_775
C16 N3 Co2 125.9(4) . 2_775
C1 O1 Co1 172.3(5) . .
C1 O2 Co2 103.1(4) . 2_765
C8 O3 Co1 140.4(4) . 1_455
C8 O4 Co2 126.1(4) . 2_665
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 O1 1.250(8) .
C1 O2 1.279(8) .
C1 C2 1.506(9) .
C2 C3 1.498(15) .
C2 C10 1.521(9) .
C2 C5 1.568(9) .
C3 H3A 0.9600 .
C3 H3B 0.9600 .
C3 H3C 0.9600 .
C4 C5 1.530(9) .
C4 H4A 0.9600 .
C4 H4B 0.9600 .
C4 H4C 0.9600 .
C5 C6 1.541(9) .
C5 C7 1.570(9) .
C6 H6A 0.9600 .
C6 H6B 0.9600 .
C6 H6C 0.9600 .
C7 C3' 1.493(15) .
C7 C8 1.511(9) .
C7 C9 1.537(9) .
C8 O3 1.252(7) .
C8 O4 1.261(8) .
C9 C10 1.539(9) .
C9 H9A 0.9700 .
C9 H9B 0.9700 .
C10 H10A 0.9700 .
C10 H10B 0.9700 .
C11 N1 1.354(8) .
C11 C16 1.393(9) .
C11 C12 1.421(9) .
C12 C13 1.349(11) .
C12 H12 0.9300 .
C13 C14 1.408(12) .
C13 H13 0.9300 .
C14 C15 1.352(12) .
C14 H14 0.9300 .
C15 C16 1.397(10) .
C15 H15 0.9300 .
C16 N3 1.366(8) .
C3' H3'1 0.9600 .
C3' H3'2 0.9600 .
C3' H3'3 0.9600 .
Co1 O3 2.108(4) 2_665
Co1 O3 2.108(4) 1_655
Co1 N1 2.110(5) .
Co1 N1 2.110(5) 2_765
Co1 O1 2.117(5) 2_765
Co1 O1 2.117(5) .
Co2 O4 1.921(5) 2_665
Co2 O2 1.973(5) 2_765
Co2 N2 1.999(5) .
Co2 N3 2.025(5) 2_775
N1 N2 1.338(7) .
N2 N3 1.344(7) .
N3 Co2 2.025(5) 2_775
O2 Co2 1.973(5) 2_765
O3 Co1 2.108(4) 1_455
O4 Co2 1.921(5) 2_665
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O1 C1 C2 C3 -111.9(9) . .
O2 C1 C2 C3 64.2(9) . .
O1 C1 C2 C10 5.5(9) . .
O2 C1 C2 C10 -178.4(6) . .
O1 C1 C2 C5 123.6(7) . .
O2 C1 C2 C5 -60.4(8) . .
C3 C2 C5 C4 -44.1(9) . .
C1 C2 C5 C4 76.5(7) . .
C10 C2 C5 C4 -160.8(6) . .
C3 C2 C5 C6 -166.6(8) . .
C1 C2 C5 C6 -46.0(7) . .
C10 C2 C5 C6 76.8(7) . .
C3 C2 C5 C7 76.7(8) . .
C1 C2 C5 C7 -162.7(5) . .
C10 C2 C5 C7 -39.9(6) . .
C4 C5 C7 C3' 40.8(10) . .
C6 C5 C7 C3' 162.8(9) . .
C2 C5 C7 C3' -80.8(9) . .
C4 C5 C7 C8 -79.6(7) . .
C6 C5 C7 C8 42.4(8) . .
C2 C5 C7 C8 158.8(5) . .
C4 C5 C7 C9 155.2(6) . .
C6 C5 C7 C9 -82.8(7) . .
C2 C5 C7 C9 33.5(6) . .
C3' C7 C8 O3 131.6(9) . .
C9 C7 C8 O3 12.5(9) . .
C5 C7 C8 O3 -106.9(7) . .
C3' C7 C8 O4 -50.3(10) . .
C9 C7 C8 O4 -169.4(6) . .
C5 C7 C8 O4 71.2(7) . .
C3' C7 C9 C10 101.4(8) . .
C8 C7 C9 C10 -138.4(6) . .
C5 C7 C9 C10 -15.5(8) . .
C3 C2 C10 C9 -89.6(8) . .
C1 C2 C10 C9 153.6(6) . .
C5 C2 C10 C9 31.1(8) . .
C7 C9 C10 C2 -9.7(8) . .
N1 C11 C12 C13 179.9(8) . .
C16 C11 C12 C13 -2.7(12) . .
C11 C12 C13 C14 2.6(15) . .
C12 C13 C14 C15 -1.7(18) . .
C13 C14 C15 C16 0.7(17) . .
N1 C11 C16 N3 -0.4(8) . .
C12 C11 C16 N3 -178.4(7) . .
N1 C11 C16 C15 179.9(8) . .
C12 C11 C16 C15 1.9(12) . .
C14 C15 C16 N3 179.5(9) . .
C14 C15 C16 C11 -0.9(14) . .
C16 C11 N1 N2 1.0(7) . .
C12 C11 N1 N2 178.7(7) . .
C16 C11 N1 Co1 -178.9(5) . .
C12 C11 N1 Co1 -1.3(12) . .
O3 Co1 N1 N2 -51.8(4) 2_665 .
O3 Co1 N1 N2 128.2(4) 1_655 .
N1 Co1 N1 N2 -122(100) 2_765 .
O1 Co1 N1 N2 38.8(4) 2_765 .
O1 Co1 N1 N2 -141.2(4) . .
O3 Co1 N1 C11 128.2(6) 2_665 .
O3 Co1 N1 C11 -51.8(6) 1_655 .
N1 Co1 N1 C11 58(100) 2_765 .
O1 Co1 N1 C11 -141.3(6) 2_765 .
O1 Co1 N1 C11 38.7(6) . .
C11 N1 N2 N3 -1.3(7) . .
Co1 N1 N2 N3 178.7(4) . .
C11 N1 N2 Co2 173.6(4) . .
Co1 N1 N2 Co2 -6.4(6) . .
O4 Co2 N2 N1 63.4(5) 2_665 .
O2 Co2 N2 N1 -72.3(5) 2_765 .
N3 Co2 N2 N1 173.3(4) 2_775 .
O4 Co2 N2 N3 -122.6(5) 2_665 .
O2 Co2 N2 N3 101.8(5) 2_765 .
N3 Co2 N2 N3 -12.7(6) 2_775 .
N1 N2 N3 C16 1.0(7) . .
Co2 N2 N3 C16 -173.7(4) . .
N1 N2 N3 Co2 -170.2(4) . 2_775
Co2 N2 N3 Co2 15.1(8) . 2_775
C11 C16 N3 N2 -0.3(7) . .
C15 C16 N3 N2 179.3(9) . .
C11 C16 N3 Co2 170.9(5) . 2_775
C15 C16 N3 Co2 -9.5(12) . 2_775
O2 C1 O1 Co1 67(4) . .
C2 C1 O1 Co1 -117(3) . .
O3 Co1 O1 C1 63(3) 2_665 .
O3 Co1 O1 C1 -117(3) 1_655 .
N1 Co1 O1 C1 157(3) . .
N1 Co1 O1 C1 -23(3) 2_765 .
O1 Co1 O1 C1 -73(100) 2_765 .
O1 C1 O2 Co2 0.6(7) . 2_765
C2 C1 O2 Co2 -175.5(5) . 2_765
O4 C8 O3 Co1 19.9(11) . 1_455
C7 C8 O3 Co1 -162.3(5) . 1_455
O3 C8 O4 Co2 13.1(9) . 2_665
C7 C8 O4 Co2 -164.9(4) . 2_665
