#------------------------------------------------------------------------------
#$Date: 2016-03-26 20:56:05 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180456 $
#$URL: svn://www.crystallography.net/cod/cif/7/21/25/7212597.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7212597
loop_
_publ_author_name
'Visinescu, Diana'
'Fabelo, Oscar'
'Ruiz-Pérez, Catalina'
'Lloret, Francesc'
'Julve, Miguel'
_publ_section_title
;
 [Fe(phen)(CN)4]−: a suitable metalloligand unit to build 3d--4f
 heterobimetallic complexes with mixed bpym-cyano bridges (phen =
 1,10-phenantroline, bpym = 2,2′-bipyrimidine)
;
_journal_issue                   8
_journal_name_full               CrystEngComm
_journal_page_first              2454
_journal_paper_doi               10.1039/c002305a
_journal_volume                  12
_journal_year                    2010
_chemical_formula_sum            'C72 H66 Dy2 Fe4 N30 O20'
_chemical_formula_weight         2219.95
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                94.664(5)
_cell_angle_beta                 104.432(6)
_cell_angle_gamma                92.157(10)
_cell_formula_units_Z            1
_cell_length_a                   10.0660(10)
_cell_length_b                   15.0110(13)
_cell_length_c                   16.5870(7)
_cell_measurement_temperature    293(2)
_cell_volume                     2414.8(3)
_computing_cell_refinement       'EvalCCD (Duisenberg & Schreurs 1990-2000)'
_computing_data_collection       'Collect (Bruker AXS BV, 1997-2004)'
_computing_data_reduction        'EvalCCD (Duisenberg & Schreurs 1990-2000)'
_computing_molecular_graphics    'Ortep-3 for Windows (Farrugia, 1997)'
_computing_publication_material  'WinGX publication routines (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXL-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector                 'CCD plate'
_diffrn_detector_area_resol_mean 9
_diffrn_measured_fraction_theta_full 0.982
_diffrn_measured_fraction_theta_max 0.982
_diffrn_measurement_device       '95mm CCD camera on κ-goniostat'
_diffrn_measurement_device_type  KappaCCD
_diffrn_measurement_method       'CCD rotation images, thick slices'
_diffrn_radiation_monochromator  'horizonally mounted graphite crystal'
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0282
_diffrn_reflns_av_sigmaI/netI    0.0242
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            48282
_diffrn_reflns_theta_full        27.50
_diffrn_reflns_theta_max         27.50
_diffrn_reflns_theta_min         6.44
_diffrn_source                   'Enraf Nonius FR590'
_exptl_absorpt_coefficient_mu    2.189
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            Brown
_exptl_crystal_density_diffrn    1.527
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Prism
_exptl_crystal_F_000             1104
_exptl_crystal_size_max          0.11
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.08
_refine_diff_density_max         1.220
_refine_diff_density_min         -0.560
_refine_diff_density_rms         0.087
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.123
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     577
_refine_ls_number_reflns         10873
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.123
_refine_ls_R_factor_all          0.0346
_refine_ls_R_factor_gt           0.0264
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0360P)²+2.6588P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0729
_refine_ls_wR_factor_ref         0.0791
_reflns_number_gt                9647
_reflns_number_total             10873
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c002305a.txt
_cod_data_source_block           compound31
_cod_database_code               7212597
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Dy1 Dy 0.706791(12) 0.662685(8) 0.128405(8) 0.02593(5) Uani 1 1 d .
Fe1 Fe 1.12671(4) 0.45350(3) 0.27006(2) 0.02956(9) Uani 1 1 d .
Fe2 Fe 0.37405(4) 0.91557(3) 0.20791(3) 0.03742(11) Uani 1 1 d .
C1 C 0.7943(3) 0.4718(2) 0.0304(2) 0.0366(7) Uani 1 1 d .
H1 H 0.8812 0.4958 0.0594 0.044 Uiso 1 1 calc R
C2 C 0.7829(3) 0.3941(2) -0.0207(2) 0.0487(9) Uani 1 1 d .
H2 H 0.8605 0.3656 -0.0274 0.058 Uiso 1 1 calc R
C3 C 0.6537(3) 0.3596(2) -0.0618(2) 0.0443(8) Uani 1 1 d .
H3 H 0.6439 0.3068 -0.0967 0.053 Uiso 1 1 calc R
C4 C 0.5616(3) 0.47620(18) -0.00405(16) 0.0250(5) Uani 1 1 d .
C5 C 0.9832(3) 0.5315(2) 0.23151(18) 0.0319(6) Uani 1 1 d .
C6 C 0.4985(3) 0.8255(2) 0.19687(19) 0.0339(6) Uani 1 1 d .
C7 C 1.0994(3) 0.4047(2) 0.15674(19) 0.0392(7) Uani 1 1 d .
C8 C 1.2664(3) 0.5374(2) 0.25195(19) 0.0389(7) Uani 1 1 d .
C9 C 0.9844(4) 0.3684(2) 0.2830(2) 0.0455(8) Uani 1 1 d .
C10 C 0.3990(4) 0.8879(3) 0.3215(3) 0.0570(10) Uani 1 1 d .
C11 C 0.5264(4) 1.0052(3) 0.2427(3) 0.0531(9) Uani 1 1 d .
C12 C 0.2228(3) 0.8241(2) 0.1716(2) 0.0376(7) Uani 1 1 d .
C13 C 1.3268(4) 0.3087(3) 0.2717(3) 0.0520(9) Uani 1 1 d .
H13 H 1.2958 0.3007 0.2137 0.062 Uiso 1 1 calc R
C14 C 1.4282(5) 0.2551(4) 0.3120(4) 0.0757(14) Uani 1 1 d .
H14 H 1.4635 0.2117 0.2811 0.091 Uiso 1 1 calc R
C15 C 1.4752(6) 0.2667(5) 0.3970(4) 0.096(2) Uani 1 1 d .
H15 H 1.5418 0.2305 0.4243 0.115 Uiso 1 1 calc R
C16 C 1.4237(5) 0.3327(4) 0.4431(3) 0.0815(16) Uani 1 1 d .
C17 C 1.3203(4) 0.3838(3) 0.3982(2) 0.0530(9) Uani 1 1 d .
C18 C 1.4668(7) 0.3546(7) 0.5323(4) 0.126(3) Uani 1 1 d .
H18 H 1.5342 0.3222 0.5642 0.151 Uiso 1 1 calc R
C19 C 1.4118(8) 0.4209(7) 0.5707(4) 0.133(3) Uani 1 1 d .
H19 H 1.4434 0.4334 0.6283 0.160 Uiso 1 1 calc R
C20 C 1.3081(6) 0.4719(5) 0.5264(3) 0.0899(18) Uani 1 1 d .
C21 C 1.2631(4) 0.4521(3) 0.4386(2) 0.0554(10) Uani 1 1 d .
C22 C 1.1107(5) 0.5642(3) 0.4257(2) 0.0600(10) Uani 1 1 d .
H22 H 1.0450 0.5967 0.3924 0.072 Uiso 1 1 calc R
C23 C 1.1497(7) 0.5867(4) 0.5128(3) 0.0885(17) Uani 1 1 d .
H23 H 1.1085 0.6328 0.5366 0.106 Uiso 1 1 calc R
C24 C 1.2453(7) 0.5421(5) 0.5611(3) 0.107(2) Uani 1 1 d .
H24 H 1.2710 0.5575 0.6185 0.128 Uiso 1 1 calc R
C25 C 0.1932(5) 1.0403(3) 0.2778(3) 0.0727(13) Uani 1 1 d .
H25 H 0.2249 1.0175 0.3291 0.087 Uiso 1 1 calc R
C26 C 0.0965(6) 1.1068(4) 0.2696(5) 0.0895(18) Uani 1 1 d .
H26 H 0.0662 1.1282 0.3157 0.107 Uiso 1 1 calc R
C27 C 0.0471(5) 1.1396(3) 0.1942(5) 0.0871(18) Uani 1 1 d .
H27 H -0.0176 1.1827 0.1888 0.104 Uiso 1 1 calc R
C28 C 0.0940(4) 1.1083(3) 0.1250(4) 0.0666(13) Uani 1 1 d .
C29 C 0.1915(4) 1.0435(2) 0.1381(3) 0.0522(9) Uani 1 1 d .
C30 C 0.0500(5) 1.1365(3) 0.0432(4) 0.0746(15) Uani 1 1 d .
H30 H -0.0148 1.1795 0.0336 0.090 Uiso 1 1 calc R
C31 C 0.0988(5) 1.1033(3) -0.0205(4) 0.0728(14) Uani 1 1 d .
H31 H 0.0673 1.1238 -0.0729 0.087 Uiso 1 1 calc R
C32 C 0.1984(4) 1.0368(3) -0.0094(3) 0.0571(10) Uani 1 1 d .
C33 C 0.2435(4) 1.0084(2) 0.0713(3) 0.0478(8) Uani 1 1 d .
C34 C 0.3866(4) 0.9103(3) 0.0274(2) 0.0487(8) Uani 1 1 d .
H34 H 0.4508 0.8670 0.0387 0.058 Uiso 1 1 calc R
C35 C 0.3464(5) 0.9352(3) -0.0531(3) 0.0606(10) Uani 1 1 d .
H35 H 0.3836 0.9088 -0.0946 0.073 Uiso 1 1 calc R
C36 C 0.2523(5) 0.9984(3) -0.0721(3) 0.0637(11) Uani 1 1 d .
H36 H 0.2250 1.0153 -0.1262 0.076 Uiso 1 1 calc R
O1A O 0.6325(3) 0.7742(2) 0.03321(17) 0.0592(7) Uani 1 1 d .
O1W O 0.8896(2) 0.67771(15) 0.06751(13) 0.0372(5) Uani 1 1 d .
O2A O 0.6223(4) 0.6621(2) -0.0562(3) 0.0779(10) Uani 1 1 d .
O2W O 0.6196(2) 0.58135(18) 0.22032(15) 0.0479(6) Uani 1 1 d .
O3A O 0.5748(4) 0.7921(3) -0.0977(2) 0.0839(11) Uani 1 1 d .
O3W O 0.8567(2) 0.76589(18) 0.22356(17) 0.0552(7) Uani 1 1 d .
O4W O 0.6237(5) 0.3997(3) 0.2081(3) 0.1033(13) Uani 1 1 d .
O5W O 1.1053(5) 0.7452(5) 0.3333(3) 0.141(2) Uani 1 1 d .
O6W O 0.8146(7) 1.1790(4) 0.3749(3) 0.138(2) Uani 1 1 d .
O7W O 0.8479(8) 0.9274(5) 0.3010(7) 0.242(5) Uani 1 1 d .
N1 N 0.6836(2) 0.51394(16) 0.03965(14) 0.0285(5) Uani 1 1 d .
N1A N 0.6077(3) 0.7427(2) -0.0431(2) 0.0526(8) Uani 1 1 d .
N2 N 0.5411(2) 0.39979(16) -0.05326(15) 0.0309(5) Uani 1 1 d .
N3 N 0.8935(3) 0.57462(19) 0.20620(16) 0.0382(6) Uani 1 1 d .
N4 N 0.5680(3) 0.76965(18) 0.18611(17) 0.0373(6) Uani 1 1 d .
N5 N 1.0877(3) 0.3733(3) 0.09014(18) 0.0571(9) Uani 1 1 d .
N6 N 1.3539(3) 0.5823(3) 0.2421(2) 0.0593(9) Uani 1 1 d .
N7 N 0.8990(5) 0.3207(3) 0.2901(3) 0.0796(12) Uani 1 1 d .
N8 N 0.4120(6) 0.8720(4) 0.3883(3) 0.0951(15) Uani 1 1 d .
N9 N 0.6158(5) 1.0569(3) 0.2634(3) 0.0856(13) Uani 1 1 d .
N10 N 0.1347(3) 0.7717(2) 0.1469(2) 0.0499(7) Uani 1 1 d .
N11 N 1.2733(3) 0.3709(2) 0.31350(17) 0.0407(6) Uani 1 1 d .
N12 N 1.1655(3) 0.4981(2) 0.39013(16) 0.0416(6) Uani 1 1 d .
N13 N 0.2400(3) 1.0099(2) 0.2128(2) 0.0522(8) Uani 1 1 d .
N14 N 0.3376(3) 0.94541(18) 0.08934(19) 0.0421(6) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_3
O1W Dy1 O3W 77.52(9) .
O1W Dy1 O2W 143.86(8) .
O3W Dy1 O2W 100.09(10) .
O1W Dy1 O1A 77.70(9) .
O3W Dy1 O1A 92.12(11) .
O2W Dy1 O1A 138.24(9) .
O1W Dy1 N4 133.87(9) .
O3W Dy1 N4 72.24(9) .
O2W Dy1 N4 76.41(9) .
O1A Dy1 N4 69.61(9) .
O1W Dy1 N3 73.09(8) .
O3W Dy1 N3 74.23(10) .
O2W Dy1 N3 71.65(9) .
O1A Dy1 N3 149.76(9) .
N4 Dy1 N3 127.96(9) .
O1W Dy1 N1 78.57(8) .
O3W Dy1 N1 145.59(8) .
O2W Dy1 N1 85.18(9) .
O1A Dy1 N1 106.52(9) .
N4 Dy1 N1 141.14(8) .
N3 Dy1 N1 75.36(8) .
O1W Dy1 N2 126.30(7) 2_665
O3W Dy1 N2 150.57(8) 2_665
O2W Dy1 N2 71.21(8) 2_665
O1A Dy1 N2 78.65(10) 2_665
N4 Dy1 N2 78.36(8) 2_665
N3 Dy1 N2 125.62(9) 2_665
N1 Dy1 N2 63.28(7) 2_665
C7 Fe1 C5 87.91(13) .
C7 Fe1 C9 89.47(15) .
C5 Fe1 C9 87.05(14) .
C7 Fe1 C8 88.13(15) .
C5 Fe1 C8 92.29(13) .
C9 Fe1 C8 177.54(14) .
C7 Fe1 N12 175.88(13) .
C5 Fe1 N12 96.21(12) .
C9 Fe1 N12 90.70(14) .
C8 Fe1 N12 91.73(13) .
C7 Fe1 N11 93.45(12) .
C5 Fe1 N11 177.95(12) .
C9 Fe1 N11 91.42(14) .
C8 Fe1 N11 89.29(13) .
N12 Fe1 N11 82.43(12) .
C6 Fe2 C10 87.06(15) .
C6 Fe2 C11 90.26(14) .
C10 Fe2 C11 90.28(19) .
C6 Fe2 C12 88.77(12) .
C10 Fe2 C12 90.22(17) .
C11 Fe2 C12 178.89(15) .
C6 Fe2 N14 95.37(12) .
C10 Fe2 N14 176.97(15) .
C11 Fe2 N14 91.52(16) .
C12 Fe2 N14 88.02(13) .
C6 Fe2 N13 176.92(14) .
C10 Fe2 N13 95.89(16) .
C11 Fe2 N13 90.62(14) .
C12 Fe2 N13 90.32(13) .
N14 Fe2 N13 81.66(13) .
N1 C1 C2 121.6(3) .
N1 C1 H1 119.2 .
C2 C1 H1 119.2 .
C1 C2 C3 117.9(3) .
C1 C2 H2 121.0 .
C3 C2 H2 121.0 .
N2 C3 C2 121.8(3) .
N2 C3 H3 119.1 .
C2 C3 H3 119.1 .
N2 C4 N1 125.9(2) .
N2 C4 C4 117.4(3) 2_665
N1 C4 C4 116.7(3) 2_665
N3 C5 Fe1 176.6(3) .
N4 C6 Fe2 176.1(3) .
N5 C7 Fe1 177.1(3) .
N6 C8 Fe1 175.7(3) .
N7 C9 Fe1 178.1(4) .
N8 C10 Fe2 179.1(4) .
N9 C11 Fe2 179.4(5) .
N10 C12 Fe2 176.9(3) .
N11 C13 C14 122.0(4) .
N11 C13 H13 119.0 .
C14 C13 H13 119.0 .
C15 C14 C13 119.5(5) .
C15 C14 H14 120.2 .
C13 C14 H14 120.2 .
C14 C15 C16 120.2(4) .
C14 C15 H15 119.9 .
C16 C15 H15 119.9 .
C15 C16 C17 117.1(4) .
C15 C16 C18 126.3(5) .
C17 C16 C18 116.6(6) .
N11 C17 C21 116.5(3) .
N11 C17 C16 122.1(4) .
C21 C17 C16 121.4(4) .
C19 C18 C16 121.7(5) .
C19 C18 H18 119.2 .
C16 C18 H18 119.2 .
C18 C19 C20 122.1(5) .
C18 C19 H19 118.9 .
C20 C19 H19 118.9 .
C24 C20 C19 126.0(5) .
C24 C20 C21 116.3(5) .
C19 C20 C21 117.7(6) .
N12 C21 C17 117.2(3) .
N12 C21 C20 122.3(4) .
C17 C21 C20 120.5(4) .
N12 C22 C23 121.5(5) .
N12 C22 H22 119.3 .
C23 C22 H22 119.3 .
C24 C23 C22 120.0(5) .
C24 C23 H23 120.0 .
C22 C23 H23 120.0 .
C23 C24 C20 120.8(4) .
C23 C24 H24 119.6 .
C20 C24 H24 119.6 .
N13 C25 C26 120.9(5) .
N13 C25 H25 119.6 .
C26 C25 H25 119.6 .
C27 C26 C25 120.2(5) .
C27 C26 H26 119.9 .
C25 C26 H26 119.9 .
C26 C27 C28 120.0(4) .
C26 C27 H27 120.0 .
C28 C27 H27 120.0 .
C29 C28 C27 116.6(5) .
C29 C28 C30 117.9(5) .
C27 C28 C30 125.4(4) .
N13 C29 C28 123.6(4) .
N13 C29 C33 116.3(3) .
C28 C29 C33 120.0(4) .
C31 C30 C28 122.3(4) .
C31 C30 H30 118.8 .
C28 C30 H30 118.8 .
C30 C31 C32 121.3(5) .
C30 C31 H31 119.4 .
C32 C31 H31 119.4 .
C36 C32 C33 118.1(4) .
C36 C32 C31 124.8(4) .
C33 C32 C31 117.2(5) .
N14 C33 C32 122.5(4) .
N14 C33 C29 116.2(4) .
C32 C33 C29 121.3(3) .
N14 C34 C35 122.8(4) .
N14 C34 H34 118.6 .
C35 C34 H34 118.6 .
C36 C35 C34 120.3(4) .
C36 C35 H35 119.9 .
C34 C35 H35 119.9 .
C35 C36 C32 118.8(4) .
C35 C36 H36 120.6 .
C32 C36 H36 120.6 .
N1A O1A Dy1 112.5(2) .
C1 N1 C4 116.3(2) .
C1 N1 Dy1 121.23(18) .
C4 N1 Dy1 122.32(17) .
O3A N1A O2A 123.8(4) .
O3A N1A O1A 119.7(4) .
O2A N1A O1A 116.5(3) .
C4 N2 C3 116.3(2) .
C4 N2 Dy1 120.27(17) 2_665
C3 N2 Dy1 123.39(19) 2_665
C5 N3 Dy1 170.6(2) .
C6 N4 Dy1 165.8(3) .
C13 N11 C17 119.1(3) .
C13 N11 Fe1 129.1(2) .
C17 N11 Fe1 111.8(2) .
C22 N12 C21 119.1(3) .
C22 N12 Fe1 128.8(3) .
C21 N12 Fe1 112.1(2) .
C25 N13 C29 118.7(4) .
C25 N13 Fe2 128.5(3) .
C29 N13 Fe2 112.8(2) .
C34 N14 C33 117.5(3) .
C34 N14 Fe2 129.5(2) .
C33 N14 Fe2 112.9(3) .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Dy1 O1W 2.321(2) .
Dy1 O3W 2.326(2) .
Dy1 O2W 2.340(2) .
Dy1 O1A 2.406(3) .
Dy1 N4 2.456(2) .
Dy1 N3 2.490(3) .
Dy1 N1 2.542(2) .
Dy1 N2 2.597(2) 2_665
Fe1 C7 1.910(3) .
Fe1 C5 1.912(3) .
Fe1 C9 1.946(4) .
Fe1 C8 1.947(4) .
Fe1 N12 1.986(3) .
Fe1 N11 1.997(3) .
Fe2 C6 1.906(3) .
Fe2 C10 1.920(5) .
Fe2 C11 1.943(4) .
Fe2 C12 1.954(3) .
Fe2 N14 2.000(3) .
Fe2 N13 2.003(3) .
C1 N1 1.338(3) .
C1 C2 1.368(4) .
C1 H1 0.9300 .
C2 C3 1.370(4) .
C2 H2 0.9300 .
C3 N2 1.336(4) .
C3 H3 0.9300 .
C4 N2 1.331(3) .
C4 N1 1.338(3) .
C4 C4 1.483(5) 2_665
C5 N3 1.144(4) .
C6 N4 1.142(4) .
C7 N5 1.141(4) .
C8 N6 1.141(5) .
C9 N7 1.134(5) .
C10 N8 1.128(6) .
C11 N9 1.130(5) .
C12 N10 1.134(4) .
C13 N11 1.327(5) .
C13 C14 1.395(6) .
C13 H13 0.9300 .
C14 C15 1.366(8) .
C14 H14 0.9300 .
C15 C16 1.397(8) .
C15 H15 0.9300 .
C16 C17 1.412(5) .
C16 C18 1.440(9) .
C17 N11 1.360(5) .
C17 C21 1.399(6) .
C18 C19 1.348(11) .
C18 H18 0.9300 .
C19 C20 1.409(9) .
C19 H19 0.9300 .
C20 C24 1.404(9) .
C20 C21 1.416(5) .
C21 N12 1.354(5) .
C22 N12 1.322(5) .
C22 C23 1.409(6) .
C22 H22 0.9300 .
C23 C24 1.330(9) .
C23 H23 0.9300 .
C24 H24 0.9300 .
C25 N13 1.334(6) .
C25 C26 1.411(7) .
C25 H25 0.9300 .
C26 C27 1.365(9) .
C26 H26 0.9300 .
C27 C28 1.399(8) .
C27 H27 0.9300 .
C28 C29 1.399(5) .
C28 C30 1.423(8) .
C29 N13 1.359(6) .
C29 C33 1.413(6) .
C30 C31 1.341(8) .
C30 H30 0.9300 .
C31 C32 1.431(6) .
C31 H31 0.9300 .
C32 C36 1.385(7) .
C32 C33 1.408(6) .
C33 N14 1.361(4) .
C34 N14 1.327(5) .
C34 C35 1.383(6) .
C34 H34 0.9300 .
C35 C36 1.365(6) .
C35 H35 0.9300 .
C36 H36 0.9300 .
O1A N1A 1.274(4) .
O2A N1A 1.234(4) .
O3A N1A 1.207(4) .
N2 Dy1 2.597(2) 2_665
