#------------------------------------------------------------------------------
#$Date: 2016-03-26 22:50:16 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180520 $
#$URL: svn://www.crystallography.net/cod/cif/7/21/89/7218959.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7218959
loop_
_publ_author_name
'Ji, Baoming'
'deng, dong sheng'
'Ma, Junying'
'Sun, Chaowei'
'Zhao, Bin'
_publ_section_title
;
 Two- and Three-Dimensional Lanthanide-Based Coordination Polymers
 Assembled by the Synergistic Effect of Various Lanthanide Radii and
 Flexibility of a New Binicotinate-Containing Ligand: in Situ Synthesis,
 Structures, and Properties
;
_journal_name_full               'RSC Adv.'
_journal_paper_doi               10.1039/C4RA12714E
_journal_year                    2014
_chemical_formula_sum            'C12 H9 Eu N2 O8'
_chemical_formula_weight         461.17
_chemical_name_systematic
;

 ?

;
_space_group_IT_number           9
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'C -2yc'
_symmetry_space_group_name_H-M   'C 1 c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2013-12-09 deposited with the CCDC.
2014-11-28 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 96.9570(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   17.909(3)
_cell_length_b                   10.2645(15)
_cell_length_c                   7.4561(11)
_cell_measurement_reflns_used    3412
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      28.24
_cell_measurement_theta_min      2.29
_cell_volume                     1360.5(4)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0153
_diffrn_reflns_av_sigmaI/netI    0.0324
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       9
_diffrn_reflns_limit_l_min       -8
_diffrn_reflns_number            4096
_diffrn_reflns_theta_full        25.49
_diffrn_reflns_theta_max         25.49
_diffrn_reflns_theta_min         2.29
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    4.658
_exptl_absorpt_correction_T_max  0.6049
_exptl_absorpt_correction_T_min  0.4715
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    2.251
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             888
_exptl_crystal_size_max          0.19
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.12
_refine_diff_density_max         0.431
_refine_diff_density_min         -0.889
_refine_diff_density_rms         0.091
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.017(13)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.024
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     208
_refine_ls_number_reflns         2296
_refine_ls_number_restraints     4
_refine_ls_restrained_S_all      1.023
_refine_ls_R_factor_all          0.0180
_refine_ls_R_factor_gt           0.0171
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0179P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0419
_refine_ls_wR_factor_ref         0.0425
_reflns_number_gt                2217
_reflns_number_total             2296
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c4ra12714e2.cif
_cod_data_source_block           4
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2935 2014-11-11 08:27:57Z andrius 
;
_cod_original_cell_volume        1360.5(3)
_cod_original_sg_symbol_H-M      Cc
_cod_database_code               7218959
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'x, -y, z+1/2'
'x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Eu1 Eu 0.39782(4) 0.759689(14) 0.24976(6) 0.01408(6) Uani 1 1 d .
N1 N 0.52973(18) 0.8181(3) 0.1596(4) 0.0144(7) Uani 1 1 d .
N2 N 0.5018(2) 0.5879(3) 0.2957(4) 0.0157(7) Uani 1 1 d .
O1 O 0.40783(17) 0.9687(3) 0.1124(4) 0.0283(8) Uani 1 1 d .
O2 O 0.47218(17) 1.1281(3) -0.0061(4) 0.0221(7) Uani 1 1 d .
O3 O 0.36362(19) 0.5693(3) 0.3976(5) 0.0275(7) Uani 1 1 d .
O4 O 0.38478(17) 0.3616(3) 0.4820(4) 0.0259(7) Uani 1 1 d .
O5 O 0.72555(17) 0.7128(3) 0.2234(4) 0.0273(7) Uani 1 1 d D
H5D H 0.6997 0.6042 0.2018 0.041 Uiso 1 1 d RD
O6 O 0.68171(17) 0.4958(3) 0.1496(5) 0.0313(8) Uani 1 1 d D
O7 O 0.3142(2) 0.8465(4) 0.4533(5) 0.0371(9) Uani 1 1 d .
H1W H 0.3274 0.9074 0.5223 0.056 Uiso 1 1 d R
H2W H 0.2847 0.7964 0.4962 0.056 Uiso 1 1 d R
O8 O 0.27333(19) 0.7900(4) 0.0920(5) 0.0326(8) Uani 1 1 d .
H3W H 0.2572 0.7996 -0.0165 0.049 Uiso 1 1 d R
H4W H 0.2554 0.8456 0.1550 0.049 Uiso 1 1 d R
C1 C 0.5388(2) 0.9404(4) 0.1043(6) 0.0182(9) Uani 1 1 d .
C2 C 0.6088(2) 0.9912(5) 0.0802(6) 0.0248(10) Uani 1 1 d .
H2 H 0.6134 1.0757 0.0379 0.030 Uiso 1 1 calc R
C3 C 0.6714(3) 0.9136(5) 0.1203(7) 0.0299(11) Uani 1 1 d .
H3 H 0.7189 0.9463 0.1075 0.036 Uiso 1 1 calc R
C4 C 0.6637(2) 0.7876(5) 0.1793(6) 0.0199(9) Uani 1 1 d .
C5 C 0.5898(3) 0.7375(4) 0.1924(6) 0.0178(10) Uani 1 1 d .
C6 C 0.5709(2) 0.6006(4) 0.2379(5) 0.0167(9) Uani 1 1 d .
C7 C 0.6142(2) 0.4885(5) 0.2101(6) 0.0245(10) Uani 1 1 d .
C8 C 0.5840(3) 0.3666(4) 0.2377(6) 0.0265(11) Uani 1 1 d .
H8 H 0.6109 0.2920 0.2156 0.032 Uiso 1 1 calc R
C9 C 0.5142(3) 0.3551(5) 0.2978(6) 0.0245(10) Uani 1 1 d .
H9 H 0.4936 0.2737 0.3161 0.029 Uiso 1 1 calc R
C10 C 0.4757(2) 0.4690(5) 0.3302(6) 0.0205(10) Uani 1 1 d .
C11 C 0.4686(2) 1.0208(4) 0.0673(6) 0.0196(9) Uani 1 1 d .
C12 C 0.4016(2) 0.4671(4) 0.4073(6) 0.0207(10) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Eu Eu -0.1578 3.6682 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O4 Eu1 O3 87.30(12) 2_564 .
O4 Eu1 O1 96.72(12) 2_564 .
O3 Eu1 O1 168.23(11) . .
O4 Eu1 O8 70.23(11) 2_564 .
O3 Eu1 O8 93.31(13) . .
O1 Eu1 O8 77.78(12) . .
O4 Eu1 O2 152.40(11) 2_564 2_575
O3 Eu1 O2 101.16(12) . 2_575
O1 Eu1 O2 80.32(11) . 2_575
O8 Eu1 O2 134.35(11) . 2_575
O4 Eu1 O7 136.33(12) 2_564 .
O3 Eu1 O7 78.30(12) . .
O1 Eu1 O7 91.29(11) . .
O8 Eu1 O7 69.74(12) . .
O2 Eu1 O7 71.27(11) 2_575 .
O4 Eu1 N2 75.13(11) 2_564 .
O3 Eu1 N2 65.95(11) . .
O1 Eu1 N2 125.76(11) . .
O8 Eu1 N2 140.32(11) . .
O2 Eu1 N2 84.36(11) 2_575 .
O7 Eu1 N2 131.57(12) . .
O4 Eu1 N1 84.40(11) 2_564 .
O3 Eu1 N1 127.31(11) . .
O1 Eu1 N1 64.26(10) . .
O8 Eu1 N1 131.19(12) . .
O2 Eu1 N1 69.51(10) 2_575 .
O7 Eu1 N1 136.46(11) . .
N2 Eu1 N1 61.62(11) . .
O4 Eu1 C12 79.07(11) 2_564 .
O3 Eu1 C12 18.81(11) . .
O1 Eu1 C12 172.77(12) . .
O8 Eu1 C12 105.99(12) . .
O2 Eu1 C12 100.64(11) 2_575 .
O7 Eu1 C12 95.81(12) . .
N2 Eu1 C12 47.61(11) . .
N1 Eu1 C12 109.22(11) . .
O4 Eu1 H4W 87.6 2_564 .
O3 Eu1 H4W 95.9 . .
O1 Eu1 H4W 73.4 . .
O8 Eu1 H4W 17.4 . .
O2 Eu1 H4W 117.2 2_575 .
O7 Eu1 H4W 53.9 . .
N2 Eu1 H4W 155.0 . .
N1 Eu1 H4W 135.4 . .
C12 Eu1 H4W 112.1 . .
C1 N1 C5 120.3(4) . .
C1 N1 Eu1 116.4(3) . .
C5 N1 Eu1 122.5(3) . .
C10 N2 C6 119.7(4) . .
C10 N2 Eu1 112.8(3) . .
C6 N2 Eu1 124.4(3) . .
C11 O1 Eu1 126.2(3) . .
C11 O2 Eu1 135.0(3) . 2_574
C12 O3 Eu1 123.6(3) . .
C12 O4 Eu1 145.4(3) . 2_565
C4 O5 H5D 101.6 . .
C7 O6 H5D 99.2 . .
Eu1 O7 H1W 121.0 . .
Eu1 O7 H2W 119.0 . .
H1W O7 H2W 112.2 . .
Eu1 O8 H3W 133.0 . .
Eu1 O8 H4W 102.2 . .
H3W O8 H4W 111.0 . .
N1 C1 C2 122.5(4) . .
N1 C1 C11 116.2(4) . .
C2 C1 C11 121.3(4) . .
C3 C2 C1 118.5(4) . .
C3 C2 H2 120.7 . .
C1 C2 H2 120.7 . .
C2 C3 C4 120.1(4) . .
C2 C3 H3 119.9 . .
C4 C3 H3 119.9 . .
O5 C4 C3 119.9(4) . .
O5 C4 C5 121.0(4) . .
C3 C4 C5 119.1(4) . .
N1 C5 C4 119.2(4) . .
N1 C5 C6 114.8(4) . .
C4 C5 C6 126.1(4) . .
N2 C6 C7 120.1(4) . .
N2 C6 C5 113.6(4) . .
C7 C6 C5 126.0(4) . .
O6 C7 C8 118.9(4) . .
O6 C7 C6 122.3(4) . .
C8 C7 C6 118.7(4) . .
C7 C8 C9 120.6(4) . .
C7 C8 H8 119.7 . .
C9 C8 H8 119.7 . .
C10 C9 C8 118.0(4) . .
C10 C9 H9 121.0 . .
C8 C9 H9 121.0 . .
N2 C10 C9 122.6(4) . .
N2 C10 C12 115.3(4) . .
C9 C10 C12 122.1(4) . .
O2 C11 O1 125.0(4) . .
O2 C11 C1 119.0(4) . .
O1 C11 C1 116.0(4) . .
O3 C12 O4 125.8(4) . .
O3 C12 C10 117.7(4) . .
O4 C12 C10 116.4(4) . .
O3 C12 Eu1 37.6(2) . .
O4 C12 Eu1 163.4(3) . .
C10 C12 Eu1 80.2(2) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Eu1 O4 2.340(3) 2_564
Eu1 O3 2.361(3) .
Eu1 O1 2.393(3) .
Eu1 O8 2.412(3) .
Eu1 O2 2.414(3) 2_575
Eu1 O7 2.427(3) .
Eu1 N2 2.557(3) .
Eu1 N1 2.603(3) .
Eu1 C12 3.223(4) .
Eu1 H4W 2.7098 .
N1 C1 1.337(5) .
N1 C5 1.356(6) .
N2 C10 1.343(6) .
N2 C6 1.366(5) .
O1 C11 1.294(5) .
O2 C11 1.235(5) .
O2 Eu1 2.414(3) 2_574
O3 C12 1.247(5) .
O4 C12 1.270(5) .
O4 Eu1 2.340(3) 2_565
O5 C4 1.355(6) .
O5 H5D 1.2100 .
O6 C7 1.343(5) .
O6 H5D 1.2100 .
O7 H1W 0.8261 .
O7 H2W 0.8285 .
O8 H3W 0.8314 .
O8 H4W 0.8280 .
C1 C2 1.389(6) .
C1 C11 1.501(6) .
C2 C3 1.377(6) .
C2 H2 0.9300 .
C3 C4 1.379(7) .
C3 H3 0.9300 .
C4 C5 1.433(6) .
C5 C6 1.494(6) .
C6 C7 1.417(6) .
C7 C8 1.388(7) .
C8 C9 1.382(6) .
C8 H8 0.9300 .
C9 C10 1.393(6) .
C9 H9 0.9300 .
C10 C12 1.510(6) .
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
O5 H5D O6 1.21 1.21 2.4035(12) 166.6 .
O7 H1W O1 0.83 1.98 2.709(4) 147.3 2_575
O7 H2W O5 0.83 2.11 2.779(5) 138.1 4_465
O8 H3W O5 0.83 1.96 2.778(5) 168.9 4_464
O8 H4W O6 0.83 2.03 2.740(4) 144.0 3_455
O8 H4W O7 0.83 2.34 2.766(5) 112.4 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
O4 Eu1 N1 C1 108.5(3) 2_564
O3 Eu1 N1 C1 -169.2(3) .
O1 Eu1 N1 C1 8.3(3) .
O8 Eu1 N1 C1 51.0(3) .
O2 Eu1 N1 C1 -80.6(3) 2_575
O7 Eu1 N1 C1 -53.6(3) .
N2 Eu1 N1 C1 -175.4(3) .
C12 Eu1 N1 C1 -175.1(3) .
O4 Eu1 N1 C5 -81.5(3) 2_564
O3 Eu1 N1 C5 0.8(4) .
O1 Eu1 N1 C5 178.2(3) .
O8 Eu1 N1 C5 -139.0(3) .
O2 Eu1 N1 C5 89.3(3) 2_575
O7 Eu1 N1 C5 116.3(3) .
N2 Eu1 N1 C5 -5.4(3) .
C12 Eu1 N1 C5 -5.2(3) .
O4 Eu1 N2 C10 -75.6(3) 2_564
O3 Eu1 N2 C10 18.2(3) .
O1 Eu1 N2 C10 -163.1(3) .
O8 Eu1 N2 C10 -45.8(3) .
O2 Eu1 N2 C10 123.1(3) 2_575
O7 Eu1 N2 C10 64.3(3) .
N1 Eu1 N2 C10 -167.2(3) .
C12 Eu1 N2 C10 13.1(2) .
O4 Eu1 N2 C6 84.7(3) 2_564
O3 Eu1 N2 C6 178.5(3) .
O1 Eu1 N2 C6 -2.9(4) .
O8 Eu1 N2 C6 114.5(3) .
O2 Eu1 N2 C6 -76.6(3) 2_575
O7 Eu1 N2 C6 -135.4(3) .
N1 Eu1 N2 C6 -6.9(3) .
C12 Eu1 N2 C6 173.4(4) .
O4 Eu1 O1 C11 -84.9(4) 2_564
O3 Eu1 O1 C11 165.6(5) .
O8 Eu1 O1 C11 -153.0(4) .
O2 Eu1 O1 C11 67.3(3) 2_575
O7 Eu1 O1 C11 138.1(3) .
N2 Eu1 O1 C11 -8.4(4) .
N1 Eu1 O1 C11 -4.5(3) .
C12 Eu1 O1 C11 -30.9(12) .
O4 Eu1 O3 C12 63.3(4) 2_564
O1 Eu1 O3 C12 173.6(6) .
O8 Eu1 O3 C12 133.3(4) .
O2 Eu1 O3 C12 -90.2(4) 2_575
O7 Eu1 O3 C12 -158.2(4) .
N2 Eu1 O3 C12 -11.6(3) .
N1 Eu1 O3 C12 -17.6(4) .
C5 N1 C1 C2 -0.9(6) .
Eu1 N1 C1 C2 169.3(3) .
C5 N1 C1 C11 178.5(4) .
Eu1 N1 C1 C11 -11.3(5) .
N1 C1 C2 C3 -2.1(7) .
C11 C1 C2 C3 178.6(4) .
C1 C2 C3 C4 1.3(7) .
C2 C3 C4 O5 -178.1(4) .
C2 C3 C4 C5 2.1(7) .
C1 N1 C5 C4 4.3(6) .
Eu1 N1 C5 C4 -165.2(3) .
C1 N1 C5 C6 -175.0(4) .
Eu1 N1 C5 C6 15.4(5) .
O5 C4 C5 N1 175.3(4) .
C3 C4 C5 N1 -5.0(7) .
O5 C4 C5 C6 -5.5(7) .
C3 C4 C5 C6 174.3(4) .
C10 N2 C6 C7 1.5(6) .
Eu1 N2 C6 C7 -157.5(3) .
C10 N2 C6 C5 175.8(4) .
Eu1 N2 C6 C5 16.7(5) .
N1 C5 C6 N2 -20.0(5) .
C4 C5 C6 N2 160.7(4) .
N1 C5 C6 C7 153.9(4) .
C4 C5 C6 C7 -25.4(7) .
N2 C6 C7 O6 178.5(4) .
C5 C6 C7 O6 5.0(7) .
N2 C6 C7 C8 1.9(6) .
C5 C6 C7 C8 -171.6(4) .
O6 C7 C8 C9 -179.2(4) .
C6 C7 C8 C9 -2.5(7) .
C7 C8 C9 C10 -0.2(7) .
C6 N2 C10 C9 -4.4(6) .
Eu1 N2 C10 C9 156.9(3) .
C6 N2 C10 C12 175.4(3) .
Eu1 N2 C10 C12 -23.3(4) .
C8 C9 C10 N2 3.8(7) .
C8 C9 C10 C12 -176.0(4) .
Eu1 O2 C11 O1 -44.0(6) 2_574
Eu1 O2 C11 C1 134.2(3) 2_574
Eu1 O1 C11 O2 178.8(3) .
Eu1 O1 C11 C1 0.6(5) .
N1 C1 C11 O2 -170.7(4) .
C2 C1 C11 O2 8.7(6) .
N1 C1 C11 O1 7.7(6) .
C2 C1 C11 O1 -172.9(4) .
Eu1 O3 C12 O4 -178.5(3) .
Eu1 O3 C12 C10 4.0(5) .
Eu1 O4 C12 O3 -91.5(6) 2_565
Eu1 O4 C12 C10 86.0(6) 2_565
Eu1 O4 C12 Eu1 -94.7(11) 2_565
N2 C10 C12 O3 14.6(6) .
C9 C10 C12 O3 -165.6(4) .
N2 C10 C12 O4 -163.1(4) .
C9 C10 C12 O4 16.7(6) .
N2 C10 C12 Eu1 17.1(3) .
C9 C10 C12 Eu1 -163.1(4) .
O4 Eu1 C12 O3 -114.7(4) 2_564
O1 Eu1 C12 O3 -169.7(9) .
O8 Eu1 C12 O3 -49.1(4) .
O2 Eu1 C12 O3 93.4(4) 2_575
O7 Eu1 C12 O3 21.4(4) .
N2 Eu1 C12 O3 165.5(4) .
N1 Eu1 C12 O3 165.3(4) .
O4 Eu1 C12 O4 -110.5(11) 2_564
O3 Eu1 C12 O4 4.2(9) .
O1 Eu1 C12 O4 -165.4(9) .
O8 Eu1 C12 O4 -44.9(11) .
O2 Eu1 C12 O4 97.6(10) 2_575
O7 Eu1 C12 O4 25.6(10) .
N2 Eu1 C12 O4 169.8(11) .
N1 Eu1 C12 O4 169.5(10) .
O4 Eu1 C12 C10 68.9(2) 2_564
O3 Eu1 C12 C10 -176.4(5) .
O1 Eu1 C12 C10 13.9(11) .
O8 Eu1 C12 C10 134.4(2) .
O2 Eu1 C12 C10 -83.0(2) 2_575
O7 Eu1 C12 C10 -155.0(2) .
N2 Eu1 C12 C10 -10.9(2) .
N1 Eu1 C12 C10 -11.2(2) .
