#------------------------------------------------------------------------------
#$Date: 2021-04-26 20:55:38 +0300 (Mon, 26 Apr 2021) $
#$Revision: 264550 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/21/92/7219229.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7219229
loop_
_publ_author_name
'Gonçalves, R. F.'
'Cavalcante, L. S.'
'Nogueira, I. C.'
'Longo, E.'
'Godinho, M. J.'
'Sczancoski, J. C.'
'Mastelaro, V. R.'
'Pinatti, I. M.'
'Rosa, I. L. V.'
'Marques, A. P. A.'
_publ_section_title
;
 Rietveld refinement, cluster modelling, growth mechanism and
 photoluminescence properties of CaWO4:Eu3+microcrystals
;
_journal_issue                   7
_journal_name_full               CrystEngComm
_journal_page_first              1654
_journal_paper_doi               10.1039/C4CE02279C
_journal_volume                  17
_journal_year                    2015
_chemical_compound_source        Scheelite
_chemical_formula_analytical     'Ca O4 W'
_chemical_formula_moiety         'Ca O4 W'
_chemical_formula_structural     'Ca O4 W'
_chemical_formula_sum            'Ca O4 W'
_chemical_formula_weight         287.93
_chemical_melting_point          1893
_chemical_name_common            'Calcium tungstate'
_space_group_IT_number           88
_symmetry_cell_setting           tetragonal
_symmetry_space_group_name_Hall  '-I 4ad'
_symmetry_space_group_name_H-M   'I 41/a :2'
_audit_creation_date             2014-08-13T15:00
_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_update_record
;
2014-12-23 deposited with the CCDC.
2015-01-05 downloaded from the CCDC.
;
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_formula_units_Z            4
_cell_length_a                   5.244797(30)
_cell_length_b                   5.244797
_cell_length_c                   11.38130(13)
_cell_measurement_temperature    298
_cell_volume                     313.076(4)
_computing_data_collection       Jade
_computing_data_reduction        Jade
_computing_structure_refinement  GSAS
_computing_structure_solution    xx
_diffrn_ambient_temperature      298
_diffrn_detector                 scintillation
_diffrn_detector_type            scintillation
_diffrn_measurement_device_type  'Rigaku AFC-7R'
_diffrn_radiation_monochromator  xx
_diffrn_radiation_polarisn_ratio 0.5
_diffrn_radiation_probe          x-ray
_diffrn_source                   Cu
_diffrn_source_target            Cu
_diffrn_source_type              Copper
_exptl_absorpt_correction_T_max  0.97047
_exptl_absorpt_correction_T_min  0.42588
_exptl_absorpt_process_details
;   GSAS Absorption/surface roughness correction: function number 3
 Surface roughness abs. correction (Suortti)
Terms =     0.78784E-01    0.19374    
Correction is refined.
;
_exptl_crystal_density_diffrn    6.12
_exptl_crystal_density_meas      6.12
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             276
_pd_block_id                     2014-08-13T15:00|CW_130|Icamira|Rigaku
_pd_calc_method                  'Rietveld Refinement'
_pd_char_colour                  white
_pd_char_particle_morphology     irregular
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.02
_pd_meas_2theta_range_max        110.0
_pd_meas_2theta_range_min        10.0
_pd_meas_number_of_points        5001
_pd_meas_scan_method             disp
_pd_phase_name
'from C:/Ref_CaWO4/CW_130minn/EntryWithCollCode18135.cif'
_pd_prep_cool_rate               1
_pd_prep_pressure                100
_pd_prep_temperature             298
_pd_proc_2theta_range_inc        0.02
_pd_proc_2theta_range_max        110.0
_pd_proc_2theta_range_min        10.0
_pd_proc_info_data_reduction     Jade
_pd_proc_info_datetime           2013-03-13T15:00:52
_pd_proc_info_excluded_regions   ' ?'
_pd_proc_ls_background_function
;   GSAS Background function number 1 with 10 terms.
 Shifted Chebyshev function of 1st kind
      1:    247.831     2:   -123.827     3:    66.6697     4:   -3.80814    
      5:   -3.97580     6:    19.1322     7:    10.8374     8:   -26.3550    
      9:    30.7727    10:   -20.1864    
;
_pd_proc_ls_peak_cutoff          0.00030
_pd_proc_ls_profile_function
;
 CW Profile function number 4 with  17 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 Microstrain broadening by P.W. Stephens,  (1999). J. Appl. Cryst.,32,281-289.
 Peak tails are ignored  where the intensity is below 0.0003 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_number_of_points        5001
_pd_spec_mounting                ' ?'
_refine_ls_goodness_of_fit_all   1.95
_refine_ls_goodness_of_fit_ref   1.95
_refine_ls_matrix_type           full
_refine_ls_number_parameters     19
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0500
_refine_ls_R_factor_gt           0.0342
_refine_ls_R_Fsqd_factor         0.02583
_refine_ls_shift/su_max          0.07
_refine_ls_shift/su_mean         0.02
_refine_ls_wR_factor_gt          0.0666
_reflns_d_resolution_high        0.943
_reflns_d_resolution_low         4.763
_reflns_limit_h_max              5
_reflns_limit_h_min              0
_reflns_limit_k_max              5
_reflns_limit_k_min              0
_reflns_limit_l_max              12
_reflns_limit_l_min              0
_reflns_number_total             204
_cod_data_source_file            c4ce02279c2.cif
_cod_data_source_block           CW_130_publ
_cod_depositor_comments
;
The following automatic conversions were performed:

'_geom_bond_publ_flag' value 'N' changed to 'n' according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26 (22
times).

'_geom_angle_publ_flag' value 'N' changed to 'n' according
to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26 (48
times).

Automatic conversion script
Id: cif_fix_values 2935 2014-11-11 08:27:57Z andrius 

 Adding full bibliography for 7219229--7219232.cif.

 Removed the _chemical_name_systematic data item since
 it had an incorrect value 'xx'.

 Antanas Vaitkus,
 2021-04-26
;
_cod_original_cell_volume        313.076(5)
_cod_original_sg_symbol_Hall     -I4ad
_cod_original_sg_symbol_H-M      'I 41/a'
_cod_database_code               7219229
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 -y+3/4,+x+1/4,+z+1/4
3 -x+1/2,-y,+z+1/2
4 +y+3/4,-x+3/4,+z+3/4
-1 -x,-y,-z
-2 +y+1/4,-x+3/4,-z+3/4
-3 +x+1/2,+y,-z+1/2
-4 -y+1/4,+x+1/4,-z+1/4
101 +x+1/2,+y+1/2,+z+1/2
102 -y+1/4,+x+3/4,+z+3/4
103 -x,-y+1/2,+z
104 +y+1/4,-x+1/4,+z+1/4
-101 -x+1/2,-y+1/2,-z+1/2
-102 +y+3/4,-x+1/4,-z+1/4
-103 +x,+y+1/2,-z
-104 -y+3/4,+x+3/4,-z+3/4
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Ca Ca1 0.0 0.25 0.625 1.0 Uiso 0.01225 4
W W1 0.0 0.25 0.125 1.0 Uiso 0.01098 4
O O1 0.15202 0.01135 0.20864 1.0 Uiso 0.02571 16
loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
Ca 4.0 0.000 0.000 15.6348 -0.0074 7.95180 0.60890 8.43720 10.3116 0.85370
25.9905 -14.875 International_Tables_Vol_C
W 4.0 0.000 0.000 29.4936 1.42755 19.3763 0.10462 13.0544 5.93667 5.06412
11.1972 1.01074 International_Tables_Vol_C
O 16.0 0.000 0.000 3.76936 15.0797 2.53342 6.30430 1.91579 40.3445 1.55094
0.31291 0.22789 International_Tables_Vol_C
loop_
_diffrn_radiation_wavelength
_diffrn_radiation_wavelength_wt
_diffrn_radiation_type
_diffrn_radiation_wavelength_id
1.540500 1.000 CuK\a 1
1.544300 0.500 CuK\a 2
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ca1 Ca1 Ca1 85.3305(7) 2_455 2_555 n
Ca1 Ca1 Ca1 122.7315(4) 2_455 4_444 n
Ca1 Ca1 Ca1 122.7315(4) 2_455 4_454 n
Ca1 Ca1 O1 100.8119(7) 2_455 2_455 n
Ca1 Ca1 O1 102.5389(5) 2_455 3_555 n
Ca1 Ca1 O1 38.50820(30) 2_455 -1_556 n
Ca1 Ca1 O1 131.19920(10) 2_455 -2_555 n
Ca1 Ca1 O1 38.4473 2_455 101_455 n
Ca1 Ca1 O1 84.6867(5) 2_455 -104_445 n
Ca1 Ca1 Ca1 122.7315(4) 2_555 4_444 n
Ca1 Ca1 Ca1 122.7315(4) 2_555 4_454 n
Ca1 Ca1 O1 160.02991(10) 2_555 2_455 n
Ca1 Ca1 O1 38.4473 2_555 3_555 n
Ca1 Ca1 O1 69.8220(6) 2_555 -1_556 n
Ca1 Ca1 O1 84.6867(5) 2_555 -2_555 n
Ca1 Ca1 O1 102.5389(5) 2_555 101_455 n
Ca1 Ca1 O1 131.19920(10) 2_555 -104_445 n
Ca1 Ca1 Ca1 85.3305(7) 4_444 4_454 n
Ca1 Ca1 O1 69.8220(6) 4_444 2_455 n
Ca1 Ca1 O1 84.6867(5) 4_444 3_555 n
Ca1 Ca1 O1 100.8119(7) 4_444 -1_556 n
Ca1 Ca1 O1 102.5389(5) 4_444 -2_555 n
Ca1 Ca1 O1 131.19920(10) 4_444 101_455 n
Ca1 Ca1 O1 38.4473 4_444 -104_445 n
Ca1 Ca1 O1 38.50820(30) 4_454 2_455 n
Ca1 Ca1 O1 131.19920(10) 4_454 3_555 n
Ca1 Ca1 O1 160.02991(10) 4_454 -1_556 n
Ca1 Ca1 O1 38.4473 4_454 -2_555 n
Ca1 Ca1 O1 84.6867(5) 4_454 101_455 n
Ca1 Ca1 O1 69.8220(6) 4_454 104_333 n
Ca1 Ca1 O1 102.5389(5) 4_454 -104_445 n
O1 Ca1 O1 76.95560(30) 2_455 -2_555 n
O1 Ca1 O1 72.9359(6) 2_455 101_455 n
O1 Ca1 O1 68.62470(30) 2_455 -104_445 n
O1 Ca1 O1 68.62470(30) 3_555 -1_556 n
O1 Ca1 O1 98.52040(20) 3_555 -2_555 n
O1 Ca1 O1 134.7229(5) 3_555 101_455 n
O1 Ca1 O1 98.52030(20) 3_555 -104_445 n
O1 Ca1 O1 152.08270(10) -1_556 -2_555 n
O1 Ca1 O1 76.95560(30) -1_556 101_455 n
O1 Ca1 O1 72.9359(6) -1_556 -104_445 n
O1 Ca1 O1 98.52040(20) -2_555 101_455 n
O1 Ca1 O1 134.7229(5) -2_555 -104_445 n
O1 Ca1 O1 98.52030(20) 101_455 -104_445 n
O1 W1 O1 106.94830(30) 1_555 -4_555 n
Ca1 O1 Ca1 103.04440(30) 3_554 4_444 n
Ca1 O1 W1 121.2923(6) 3_554 1_555 n
Ca1 O1 W1 131.44780(20) 4_444 1_555 n
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ca1 Ca1 3.869480(30) 2_455 n
Ca1 Ca1 3.869480(30) 2_555 n
Ca1 Ca1 3.869480(30) 4_444 n
Ca1 Ca1 3.869480(30) 4_454 n
Ca1 W1 3.708630(20) 3_455 n
Ca1 W1 3.708630(20) 3_465 n
Ca1 W1 3.708630(20) 3_555 n
Ca1 W1 3.708630(20) 3_565 n
Ca1 O1 2.469750(20) 2_455 n
Ca1 O1 2.469750(20) -1_556 n
Ca1 O1 2.473060(10) 101_455 n
Ca1 O1 2.469750(20) 104_555 n
W1 Ca1 3.708630(20) 3_454 n
W1 Ca1 3.708630(20) 3_464 n
W1 Ca1 3.708630(20) 3_554 n
W1 Ca1 3.708630(20) 3_564 n
W1 O1 1.763090(10) 1_555 n
W1 O1 1.763090(10) -4_555 n
W1 O1 1.763090(10) 103_555 n
O1 Ca1 2.473060(10) 3_554 n
O1 Ca1 2.469750(20) 4_444 n
O1 W1 1.763090(10) 1_555 n
loop_
_pd_meas_counts_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
455.0 0.002198 507.17932 507.10483
432.0 0.002315 505.11984 505.04611
442.0 0.002262 503.07730 503.00436
480.0 0.002083 501.05154 500.97937
461.0 0.002169 499.04266 498.97125
477.0 0.002096 497.05038 496.97974
482.0 0.002075 495.07480 495.00488
481.0 0.002079 493.11557 493.04642
435.0 0.002299 491.17288 491.10446
480.0 0.002083 489.24652 489.17883
438.0 0.002283 487.33643 487.26950
467.0 0.002141 485.44238 485.37616
438.0 0.002283 483.56458 483.49905
467.0 0.002141 481.70267 481.63788
454.0 0.002203 479.85675 479.79266
462.0 0.002165 478.02658 477.96320
455.0 0.002198 476.21225 476.14960
417.0 0.002398 474.41351 474.35153
437.0 0.002288 472.63043 472.56915
447.0 0.002237 470.86279 470.80222
480.0 0.002083 469.11063 469.05072
470.0 0.002128 467.37372 467.31451
459.0 0.002179 465.65219 465.59366
429.0 0.002331 463.94577 463.88788
448.0 0.002232 462.25446 462.19724
438.0 0.002283 460.57809 460.52155
439.0 0.002278 458.91672 458.86081
465.0 0.002151 457.27026 457.21500
461.0 0.002169 455.63846 455.58383
455.0 0.002198 454.02145 453.96747
440.0 0.002273 452.41901 452.36566
413.0 0.002421 450.83115 450.77841
452.0 0.002212 449.25772 449.20563
448.0 0.002232 447.69870 447.64725
423.0 0.002364 446.15390 446.10306
436.0 0.002294 444.62341 444.57318
453.0 0.002208 443.10703 443.05740
428.0 0.002336 441.60480 441.55576
414.0 0.002415 440.11646 440.06802
448.0 0.002232 438.64209 438.59427
401.0 0.002494 437.18155 437.13431
426.0 0.002347 435.73483 435.68817
418.0 0.002392 434.30170 434.25562
452.0 0.002212 432.88226 432.83676
418.0 0.002392 431.47632 431.43140
462.0 0.002165 430.08392 430.03955
443.0 0.002257 428.70480 428.66101
454.0 0.002203 427.33905 427.29581
464.0 0.002155 425.98654 425.94385
442.0 0.002262 424.64722 424.60510
385.0 0.002597 423.32098 423.27939
425.0 0.002353 422.00772 421.96667
419.0 0.002387 420.70746 420.66696
419.0 0.002387 419.42004 419.38007
409.0 0.002445 418.14548 418.10605
401.0 0.002494 416.88358 416.84467
405.0 0.002469 415.63440 415.59601
407.0 0.002457 414.39777 414.35989
429.0 0.002331 413.17371 413.13635
422.0 0.002370 411.96201 411.92517
430.0 0.002326 410.76276 410.72644
419.0 0.002387 409.57574 409.53995
423.0 0.002364 408.40103 408.36572
452.0 0.002212 407.23846 407.20364
412.0 0.002427 406.08795 406.05362
408.0 0.002451 404.94949 404.91565
424.0 0.002358 403.82300 403.78964
383.0 0.002611 402.70837 402.67551
403.0 0.002481 401.60559 401.57321
396.0 0.002525 400.51453 400.48257
428.0 0.002336 399.43515 399.40369
428.0 0.002336 398.36737 398.33636
421.0 0.002375 397.31119 397.28067
422.0 0.002370 396.26642 396.23633
442.0 0.002262 395.23309 395.20349
446.0 0.002242 394.21112 394.18195
387.0 0.002584 393.20035 393.17163
426.0 0.002347 392.20090 392.17261
400.0 0.002500 391.21249 391.18466
415.0 0.002410 390.23523 390.20782
391.0 0.002558 389.26898 389.24200
385.0 0.002597 388.31369 388.28714
438.0 0.002283 387.36920 387.34308
393.0 0.002545 386.43558 386.40988
421.0 0.002375 385.51273 385.48743
431.0 0.002320 384.60056 384.57568
395.0 0.002532 383.69894 383.67447
415.0 0.002410 382.80798 382.78394
419.0 0.002387 381.92746 381.90381
406.0 0.002463 381.05740 381.03415
390.0 0.002564 380.19766 380.17480
409.0 0.002445 379.34827 379.32581
417.0 0.002398 378.50909 378.48703
392.0 0.002551 377.68011 377.65845
415.0 0.002410 376.86124 376.83994
391.0 0.002558 376.05243 376.03152
433.0 0.002309 375.25360 375.23309
428.0 0.002336 374.46472 374.44458
369.0 0.002710 373.68573 373.66595
391.0 0.002558 372.91656 372.89716
386.0 0.002591 372.15707 372.13800
351.0 0.002849 371.40729 371.38861
364.0 0.002747 370.66718 370.64883
394.0 0.002538 369.93655 369.91858
359.0 0.002786 369.21552 369.19791
418.0 0.002392 368.50391 368.48663
409.0 0.002445 367.80173 367.78479
370.0 0.002703 367.10876 367.09219
370.0 0.002703 366.42517 366.40894
430.0 0.002326 365.75073 365.73483
380.0 0.002632 365.08551 365.06995
358.0 0.002793 364.42932 364.41409
407.0 0.002457 363.78220 363.76730
392.0 0.002551 363.14404 363.12949
404.0 0.002475 362.51486 362.50058
382.0 0.002618 361.89447 361.88055
362.0 0.002762 361.28293 361.26932
377.0 0.002653 360.68011 360.66681
370.0 0.002703 360.08600 360.07300
390.0 0.002564 359.50052 359.48782
349.0 0.002865 358.92365 358.91125
394.0 0.002538 358.35526 358.34317
425.0 0.002353 357.79535 357.78357
374.0 0.002674 357.24387 357.23239
393.0 0.002545 356.70078 356.68958
369.0 0.002710 356.16592 356.15503
384.0 0.002604 355.63934 355.62872
398.0 0.002513 355.12097 355.11066
386.0 0.002591 354.61072 354.60068
375.0 0.002667 354.10858 354.09882
371.0 0.002695 353.61444 353.60495
369.0 0.002710 353.12830 353.11908
358.0 0.002793 352.65005 352.64111
368.0 0.002717 352.17972 352.17105
365.0 0.002740 351.71716 351.70877
372.0 0.002688 351.26239 351.25424
325.0 0.003077 350.81534 350.80746
377.0 0.002653 350.37592 350.36832
386.0 0.002591 349.94409 349.93674
387.0 0.002584 349.51987 349.51276
373.0 0.002681 349.10312 349.09628
341.0 0.002933 348.69385 348.68726
340.0 0.002941 348.29193 348.28558
379.0 0.002639 347.89740 347.89130
400.0 0.002500 347.51013 347.50427
384.0 0.002604 347.13013 347.12451
356.0 0.002809 346.75732 346.75195
376.0 0.002660 346.39169 346.38654
346.0 0.002890 346.03311 346.02820
347.0 0.002882 345.68158 345.67691
364.0 0.002747 345.33707 345.33258
337.0 0.002967 344.99945 344.99521
351.0 0.002849 344.66876 344.66476
337.0 0.002967 344.34494 344.34113
322.0 0.003106 344.02789 344.02432
350.0 0.002857 343.71759 343.71423
346.0 0.002890 343.41400 343.41086
365.0 0.002740 343.11707 343.11414
342.0 0.002924 342.82675 342.82404
386.0 0.002591 342.54297 342.54047
378.0 0.002646 342.26569 342.26340
344.0 0.002907 341.99487 341.99277
372.0 0.002688 341.73050 341.72861
362.0 0.002762 341.47247 341.47076
314.0 0.003185 341.22079 341.21927
378.0 0.002646 340.97534 340.97400
353.0 0.002833 340.73615 340.73502
361.0 0.002770 340.50311 340.50217
339.0 0.002950 340.27621 340.27545
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608.0 0.001645 169.13895 584.03027
515.0 0.001942 169.13795 561.06519
532.0 0.001880 169.13707 537.93054
553.0 0.001808 169.13626 514.67200
492.0 0.002033 169.13554 491.48993
464.0 0.002155 169.13492 468.69830
455.0 0.002198 169.13437 446.65152
448.0 0.002232 169.13391 425.67923
384.0 0.002604 169.13353 406.04523
412.0 0.002427 169.13324 387.93472
350.0 0.002857 169.13303 371.45880
378.0 0.002646 169.13290 356.66702
367.0 0.002725 169.13286 343.56143
351.0 0.002849 169.13289 332.10776
373.0 0.002681 169.13301 322.24460
354.0 0.002825 169.13322 313.88950
338.0 0.002959 169.13350 306.94571
328.0 0.003049 169.13387 301.30695
313.0 0.003195 169.13432 296.86215
303.0 0.003300 169.13484 293.49994
321.0 0.003115 169.13545 291.11356
321.0 0.003115 169.13614 289.60355
326.0 0.003067 169.13689 288.95822
352.0 0.002841 169.13774 288.95023
322.0 0.003106 169.13866 289.59662
339.0 0.002950 169.13965 290.85568
303.0 0.003300 169.14072 292.70450
323.0 0.003096 169.14188 295.14020
363.0 0.002755 169.14310 298.18402
347.0 0.002882 169.14439 301.88275
389.0 0.002571 169.14577 306.31439
360.0 0.002778 169.14722 311.59378
368.0 0.002717 169.14874 317.88013
404.0 0.002475 169.15034 325.38507
396.0 0.002525 169.15201 334.38342
440.0 0.002273 169.15376 345.22238
433.0 0.002309 169.15558 358.36960
454.0 0.002203 169.15746 374.26752
461.0 0.002169 169.15942 393.56708
480.0 0.002083 169.16145 416.97324
527.0 0.001898 169.16354 445.27518
544.0 0.001838 169.16573 479.32956
646.0 0.001548 169.16795 520.03418
619.0 0.001616 169.17027 568.29077
671.0 0.001490 169.17264 624.96088
707.0 0.001414 169.17509 690.81030
785.0 0.001274 169.17760 766.44812
854.0 0.001171 169.18018 852.26270
881.0 0.001135 169.18283 948.35107
992.0 0.001008 169.18553 1054.44690
1157.0 0.000864 169.18831 1169.83984
1235.0 0.000810 169.19116 1293.28857
1414.0 0.000707 169.19406 1422.92004
1625.0 0.000615 169.19704 1556.14404
1687.0 0.000593 169.20007 1689.60046
1803.0 0.000555 169.20317 1819.22937
2016.0 0.000496 169.20633 1940.53613
2170.0 0.000461 169.20955 2049.10742
2173.0 0.000460 169.21283 2141.30518
2338.0 0.000428 169.21617 2214.90503
2283.0 0.000438 169.21959 2269.37744
2305.0 0.000434 169.22305 2305.65161
2351.0 0.000425 169.22658 2325.47510
2378.0 0.000421 169.23016 2330.66260
2371.0 0.000422 169.23380 2322.56250
2238.0 0.000447 169.23750 2301.88403
2183.0 0.000458 169.24126 2268.83423
2281.0 0.000438 169.24507 2223.43555
2227.0 0.000449 169.24895 2165.84131
1965.0 0.000509 169.25287 2096.58545
2039.0 0.000490 169.25685 2016.73816
2017.0 0.000496 169.26089 1927.94519
1784.0 0.000561 169.26498 1832.32581
1757.0 0.000569 169.26913 1732.22412
1685.0 0.000593 169.27333 1629.88489
1589.0 0.000629 169.27759 1527.18689
1450.0 0.000690 169.28189 1425.53491
1304.0 0.000767 169.28624 1325.91589
1183.0 0.000845 169.29065 1229.07471
1186.0 0.000843 169.29510 1135.69067
1097.0 0.000912 169.29962 1046.47681
968.0 0.001033 169.30418 962.17358
859.0 0.001164 169.30878 883.54498
804.0 0.001244 169.31343 810.98010
730.0 0.001370 169.31815 744.89240
720.0 0.001389 169.32289 685.39917
645.0 0.001550 169.32770 632.42249
630.0 0.001587 169.33253 585.72681
557.0 0.001795 169.33742 544.96533
544.0 0.001838 169.34236 509.71866
508.0 0.001969 169.34734 479.52737
500.0 0.002000 169.35237 453.91867
470.0 0.002128 169.35744 432.42487
486.0 0.002058 169.36255 414.59909
508.0 0.001969 169.36769 400.02682
454.0 0.002203 169.37289 388.33463
424.0 0.002358 169.37813 379.23642
439.0 0.002278 169.38341 372.38617
425.0 0.002353 169.38872 367.61243
408.0 0.002451 169.39409 364.77084
410.0 0.002439 169.39948 363.78687
450.0 0.002222 169.40492 364.66068
434.0 0.002304 169.41039 367.47183
433.0 0.002309 169.41591 372.38376
470.0 0.002128 169.42145 379.64719
439.0 0.002278 169.42703 389.60275
487.0 0.002053 169.43265 402.67993
508.0 0.001969 169.43831 419.39258
503.0 0.001988 169.44400 440.32907
555.0 0.001802 169.44972 466.13614
576.0 0.001736 169.45549 497.49521
604.0 0.001656 169.46127 535.09033
601.0 0.001664 169.46710 579.57068
634.0 0.001577 169.47296 631.50385
699.0 0.001431 169.47884 691.22333
751.0 0.001332 169.48476 759.18860
858.0 0.001166 169.49071 835.30896
909.0 0.001100 169.49669 919.30206
1004.0 0.000996 169.50269 1010.53271
1024.0 0.000977 169.50873 1107.94922
1170.0 0.000855 169.51479 1210.01379
1256.0 0.000796 169.52087 1314.63074
1448.0 0.000691 169.52699 1419.08203
1576.0 0.000635 169.53313 1520.01855
1710.0 0.000585 169.53931 1613.10168
1850.0 0.000541 169.54549 1695.12866
1964.0 0.000509 169.55171 1761.77771
1964.0 0.000509 169.55795 1810.09949
2023.0 0.000494 169.56421 1838.64343
1963.0 0.000509 169.57050 1847.74377
1867.0 0.000536 169.57681 1839.35339
1838.0 0.000544 169.58313 1816.49304
1786.0 0.000560 169.58948 1782.54004
1675.0 0.000597 169.59586 1740.59180
1626.0 0.000615 169.60225 1693.03809
1562.0 0.000640 169.60866 1641.37134
1534.0 0.000652 169.61508 1586.20239
1484.0 0.000674 169.62152 1527.44739
1422.0 0.000703 169.62798 1464.64807
1390.0 0.000719 169.63446 1397.37366
1371.0 0.000729 169.64096 1325.58374
1349.0 0.000741 169.64746 1249.84485
1179.0 0.000848 169.65399 1171.31848
1134.0 0.000882 169.66052 1091.56714
999.0 0.001001 169.66708 1012.27325
961.0 0.001041 169.67365 935.00024
866.0 0.001155 169.68022 861.04236
801.0 0.001248 169.68681 791.37274
739.0 0.001353 169.69341 726.65717
685.0 0.001460 169.70001 667.29663
608.0 0.001645 169.70663 613.47729
549.0 0.001821 169.71327 565.25610
489.0 0.002045 169.71991 522.42706
503.0 0.001988 169.72655 484.80515
481.0 0.002079 169.73320 452.08127
397.0 0.002519 169.73987 423.88651
421.0 0.002375 169.74654 399.81311
415.0 0.002410 169.75320 379.43387
386.0 0.002591 169.75989 362.31876
402.0 0.002488 169.76657 348.05057
365.0 0.002740 169.77325 336.23648
355.0 0.002817 169.77994 326.51703
397.0 0.002519 169.78664 318.57220
326.0 0.003067 169.79332 312.12378
365.0 0.002740 169.80002 306.93570
347.0 0.002882 169.80672 302.81287
357.0 0.002801 169.81342 299.62033
334.0 0.002994 169.82011 297.19299
324.0 0.003086 169.82680 295.46207
320.0 0.003125 169.83350 294.36545
364.0 0.002747 169.84018 293.86740
363.0 0.002755 169.84688 293.95721
393.0 0.002545 169.85355 294.64948
348.0 0.002874 169.86023 295.98566
398.0 0.002513 169.86691 298.03683
398.0 0.002513 169.87357 300.90887
344.0 0.002907 169.88023 304.74762
359.0 0.002786 169.88689 309.74625
372.0 0.002688 169.89354 316.15210
410.0 0.002439 169.90018 324.27386
389.0 0.002571 169.90681 334.48758
445.0 0.002247 169.91344 347.23947
461.0 0.002169 169.92004 363.04544
433.0 0.002309 169.92665 382.48547
490.0 0.002041 169.93324 406.19058
528.0 0.001894 169.93982 434.82388
517.0 0.001934 169.94640 469.05106
548.0 0.001825 169.95294 509.50616
581.0 0.001721 169.95949 556.74780
639.0 0.001565 169.96602 611.21136
654.0 0.001529 169.97253 673.15863
737.0 0.001357 169.97902 742.62476
845.0 0.001183 169.98550 819.36731
880.0 0.001136 169.99197 902.81348
943.0 0.001060 169.99841 992.00604
1067.0 0.000937 170.00484 1085.54443
1163.0 0.000860 170.01125 1181.52539
1301.0 0.000769 170.01764 1277.48474
1440.0 0.000694 170.02402 1370.38708
1547.0 0.000646 170.03036 1456.70032
1652.0 0.000605 170.03670 1532.63831
1742.0 0.000574 170.04300 1594.60315
1799.0 0.000556 170.04929 1639.78308
1814.0 0.000551 170.05554 1666.72205
1747.0 0.000572 170.06178 1675.63062
1812.0 0.000552 170.06799 1668.26855
1684.0 0.000594 170.07419 1647.45142
1570.0 0.000637 170.08035 1616.38599
1540.0 0.000649 170.08649 1578.06946
1499.0 0.000667 170.09261 1534.87476
1427.0 0.000701 170.09868 1488.35742
1313.0 0.000762 170.10474 1439.23120
1348.0 0.000742 170.11076 1387.49524
1324.0 0.000755 170.11676 1332.68079
1257.0 0.000796 170.12273 1274.19958
1175.0 0.000851 170.12866 1211.70801
1161.0 0.000861 170.13457 1145.37891
1115.0 0.000897 170.14044 1076.41724
993.0 0.001007 170.14629 1005.20679
986.0 0.001014 170.15210 933.65906
844.0 0.001185 170.15787 863.23657
814.0 0.001229 170.16362 795.21112
686.0 0.001458 170.16933 730.58325
581.0 0.001721 170.17499 670.07629
559.0 0.001789 170.18062 614.16345
567.0 0.001764 170.18622 563.11029
468.0 0.002137 170.19179 517.01385
442.0 0.002262 170.19730 475.83319
417.0 0.002398 170.20279 439.41556
392.0 0.002551 170.20824 407.51941
366.0 0.002732 170.21364 379.83472
370.0 0.002703 170.21899 356.21948
336.0 0.002976 170.22432 335.85342
385.0 0.002597 170.22960 318.55197
328.0 0.003049 170.23483 303.91962
296.0 0.003378 170.24002 291.57748
291.0 0.003436 170.24518 281.17404
288.0 0.003472 170.25029 272.39203
289.0 0.003460 170.25534 264.95154
287.0 0.003484 170.26036 258.61148
228.0 0.00439 170.26532 253.16844
265.0 0.00377 170.27025 248.45393
256.0 0.00391 170.27512 244.33057
289.0 0.003460 170.27995 240.68810
274.0 0.00365 170.28473 237.43889
202.0 0.00495 170.28946 234.51411
250.0 0.00400 170.29413 231.85977
221.0 0.00452 170.29877 229.43378
237.0 0.00422 170.30334 227.20314
234.0 0.00427 170.30786 225.14191
209.0 0.00478 170.31233 223.22939
206.0 0.00485 170.31676 221.44902
214.0 0.00467 170.32112 219.78699
246.0 0.00407 170.32542 218.23195
215.0 0.00465 170.32968 216.77440
210.0 0.00476 170.33389 215.40581
214.0 0.00467 170.33803 214.11913
211.0 0.00474 170.34212 212.90778
215.0 0.00465 170.34615 211.76639
208.0 0.00481 170.35013 210.68968
211.0 0.00474 170.35403 209.67325
190.0 0.00526 170.35789 208.71269
206.0 0.00485 170.36168 207.80461
211.0 0.00474 170.36542 206.94545
217.0 0.00461 170.36909 206.13200
211.0 0.00474 170.37270 205.36168
204.0 0.00490 170.37625 204.63179
200.0 0.00500 170.37973 203.94005
193.0 0.00518 170.38316 203.28427
183.0 0.00546 170.38652 202.66275
187.0 0.00535 170.38982 202.07343
180.0 0.00556 170.39304 201.51486
221.0 0.00452 170.39619 200.98573
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172.0 0.00581 170.40233 200.01073
189.0 0.00529 170.40529 199.56299
178.0 0.00562 170.40817 199.14078
180.0 0.00556 170.41100 198.74361
192.0 0.00521 170.41376 198.37138
174.0 0.00575 170.41643 198.02422
200.0 0.00500 170.41905 197.70282
183.0 0.00546 170.42159 197.40797
180.0 0.00556 170.42406 197.14127
170.0 0.00588 170.42645 196.90474
176.0 0.00568 170.42877 196.70125
187.0 0.00535 170.43102 196.53452
168.0 0.00595 170.43320 196.40854
175.0 0.00571 170.43530 196.32858
184.0 0.00543 170.43732 196.30034
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190.0 0.00526 170.44115 196.42554
220.0 0.00455 170.44293 196.59271
183.0 0.00546 170.44464 196.83875
172.0 0.00581 170.44629 197.16977
179.0 0.00559 170.44785 197.59088
177.0 0.00565 170.44933 198.10551
170.0 0.00588 170.45071 198.71478
195.0 0.00513 170.45203 199.41728
184.0 0.00543 170.45328 200.20831
159.0 0.00629 170.45442 201.07918
212.0 0.00472 170.45549 202.01703
204.0 0.00490 170.45648 203.00365
189.0 0.00529 170.45738 204.01527
197.0 0.00508 170.45821 205.02161
188.0 0.00532 170.45894 205.98669
188.0 0.00532 170.45959 206.86954
201.0 0.00498 170.46014 207.62788
178.0 0.00562 170.46063 208.22363
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184.0 0.00543 170.46132 208.83376
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189.0 0.00529 170.45787 203.48209
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178.0 0.00562 170.45598 202.06253
178.0 0.00562 170.45490 201.32190
167.0 0.00599 170.45372 200.58090
196.0 0.00510 170.45244 199.85655
169.0 0.00592 170.45107 199.16399
166.0 0.00602 170.44958 198.51585
180.0 0.00556 170.44801 197.92183
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150.0 0.00667 170.44456 196.92049
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174.0 0.00575 170.43864 195.92332
182.0 0.00549 170.43646 195.72516
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175.0 0.00571 170.43179 195.51802
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158.0 0.00633 170.42671 195.54156
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183.0 0.00546 170.41829 195.94968
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209.0 0.00478 170.40892 196.73621
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197.0 0.00508 170.39491 198.30418
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189.0 0.00529 170.37914 200.48579
183.0 0.00546 170.37492 201.14059
160.0 0.00625 170.37059 201.84506
152.0 0.00658 170.36615 202.60298
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199.0 0.00503 170.35690 204.29680
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189.0 0.00529 170.33705 208.55608
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197.0 0.00508 170.32095 212.76834
197.0 0.00508 170.31534 214.43158
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232.0 0.00431 170.30377 218.26833
200.0 0.00500 170.29782 220.50223
223.0 0.00448 170.29173 223.00119
201.0 0.00498 170.28554 225.82062
215.0 0.00465 170.27922 228.84785
232.0 0.00431 170.27277 232.53973
220.0 0.00455 170.26620 236.82347
281.0 0.00356 170.25952 241.83720
252.0 0.00397 170.25270 247.74911
260.0 0.00385 170.24577 254.75981
277.0 0.00361 170.23872 263.10413
257.0 0.00389 170.23154 273.04956
323.0 0.003096 170.22423 284.89279
292.0 0.003425 170.21681 298.95285
318.0 0.003145 170.20924 315.56049
318.0 0.003145 170.20157 334.94852
387.0 0.002584 170.19376 357.62454
347.0 0.002882 170.18582 383.76743
376.0 0.002660 170.17776 413.59595
424.0 0.002358 170.16957 447.24948
462.0 0.002165 170.16125 484.76474
548.0 0.001825 170.15282 526.05847
580.0 0.001724 170.14424 570.88068
580.0 0.001724 170.13554 618.82507
681.0 0.001468 170.12671 669.27820
712.0 0.001404 170.11774 721.39587
737.0 0.001357 170.10864 774.07324
832.0 0.001202 170.09943 825.92474
875.0 0.001143 170.09006 875.29706
904.0 0.001106 170.08058 920.33484
1008.0 0.000992 170.07095 959.13861
1013.0 0.000987 170.06120 990.00751
997.0 0.001003 170.05132 1011.72638
992.0 0.001008 170.04131 1023.81006
999.0 0.001001 170.03116 1026.59387
989.0 0.001011 170.02086 1021.13519
973.0 0.001028 170.01044 1008.95374
907.0 0.001103 169.99988 991.72791
847.0 0.001181 169.98920 970.99078
802.0 0.001247 169.97838 947.98511
854.0 0.001171 169.96741 923.54291
843.0 0.001186 169.95631 898.07532
763.0 0.001311 169.94507 871.61670
838.0 0.001193 169.93370 843.92072
719.0 0.001391 169.92218 814.60687
759.0 0.001318 169.91054 783.33289
697.0 0.001435 169.89876 749.95459
664.0 0.001506 169.88683 714.62012
639.0 0.001565 169.87476 677.77185
598.0 0.001672 169.86255 640.06403
618.0 0.001618 169.85020 602.24091
573.0 0.001745 169.83772 565.02332
524.0 0.001908 169.82510 529.03442
473.0 0.002114 169.81233 494.76688
434.0 0.002304 169.79942 462.58154
394.0 0.002538 169.78638 432.72015
382.0 0.002618 169.77318 405.32596
363.0 0.002755 169.75986 380.46011
359.0 0.002786 169.74637 358.11765
354.0 0.002825 169.73276 338.25571
322.0 0.003106 169.71899 320.73785
316.0 0.003165 169.70509 305.44241
285.0 0.00351 169.69104 292.20538
261.0 0.00383 169.67685 280.84592
251.0 0.00398 169.66251 271.17380
250.0 0.00400 169.64803 262.99731
269.0 0.00372 169.63341 256.13025
247.0 0.00405 169.61862 250.39604
229.0 0.00437 169.60371 245.63240
212.0 0.00472 169.58864 241.69385
238.0 0.00420 169.57343 238.45323
245.0 0.00408 169.55807 235.80147
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225.0 0.00444 169.51111 230.55557
222.0 0.00450 169.49516 229.51492
221.0 0.00452 169.47906 228.76593
219.0 0.00457 169.46283 228.28992
220.0 0.00455 169.44643 228.07912
201.0 0.00498 169.42989 228.13699
199.0 0.00503 169.41321 228.47757
215.0 0.00465 169.39636 229.12567
236.0 0.00424 169.37938 230.11826
216.0 0.00463 169.36223 231.50410
219.0 0.00457 169.34494 233.34517
222.0 0.00450 169.32750 235.71628
238.0 0.00420 169.30991 238.70598
210.0 0.00476 169.29216 242.41524
258.0 0.00388 169.27428 246.95647
249.0 0.00402 169.25623 252.45094
227.0 0.00441 169.23802 259.02603
295.0 0.003390 169.21968 266.81012
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593.0 0.001686 197.09065 602.69202
631.0 . . .
