#------------------------------------------------------------------------------
#$Date: 2016-03-26 22:57:29 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180524 $
#$URL: svn://www.crystallography.net/cod/cif/7/21/93/7219378.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7219378
loop_
_publ_author_name
'Xue, Zhenzhen'
'Sheng, Tianlu'
'Wang, Yanlong'
'Hu, Shengmin'
'Wen, Yuehong'
'Wang, Yong'
'Li, Haoran'
'Fu, Ruibiao'
'Wu, Xintao'
_publ_section_title
;
 A series of d10coordination polymers constructed with a rigid tripodal
 imidazole ligand and varied polycarboxylates: syntheses, structures and
 luminescence properties
;
_journal_issue                   9
_journal_name_full               CrystEngComm
_journal_page_first              2004
_journal_paper_doi               10.1039/C4CE02551B
_journal_volume                  17
_journal_year                    2015
_chemical_formula_sum            'C33 H34 Cd N8 O7'
_chemical_formula_weight         767.08
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2015-01-16 deposited with the CCDC.
2015-01-20 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 114.073(4)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   11.328(4)
_cell_length_b                   24.951(7)
_cell_length_c                   13.624(5)
_cell_measurement_reflns_used    10444
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.4816
_cell_measurement_theta_min      2.1324
_cell_volume                     3516(2)
_computing_cell_refinement       'CrystalClear (Rigaku Inc., 2007)'
_computing_data_collection       'CrystalClear (Rigaku Inc., 2007)'
_computing_data_reduction        'CrystalClear (Rigaku Inc., 2007)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  Saturn724HG
_diffrn_measurement_method       CCD_Profile_fitting
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0543
_diffrn_reflns_av_sigmaI/netI    0.0531
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       32
_diffrn_reflns_limit_k_min       -27
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            30102
_diffrn_reflns_theta_full        27.49
_diffrn_reflns_theta_max         27.49
_diffrn_reflns_theta_min         2.13
_exptl_absorpt_coefficient_mu    0.679
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.8074
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            'pale yellow'
_exptl_crystal_density_diffrn    1.449
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1568
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.765
_refine_diff_density_min         -0.777
_refine_diff_density_rms         0.133
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.013
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     446
_refine_ls_number_reflns         8056
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.013
_refine_ls_R_factor_all          0.0796
_refine_ls_R_factor_gt           0.0573
_refine_ls_shift/su_max          0.008
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0857P)²+5.1007P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1418
_refine_ls_wR_factor_ref         0.1606
_reflns_number_gt                6377
_reflns_number_total             8056
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c4ce02551b2.cif
_cod_data_source_block           4
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 

 Adding full bibliography for 7219375--7219379.cif.
;
_cod_original_sg_symbol_H-M      P2(1)/n
_cod_database_code               7219378
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Cd1 Cd 0.64754(3) 0.159773(12) 0.82527(2) 0.02743(11) Uani 1 1 d .
C1 C 0.2751(4) 0.05539(17) 0.2747(4) 0.0347(10) Uani 1 1 d .
C2 C 0.1681(5) 0.07762(18) 0.1935(4) 0.0386(11) Uani 1 1 d .
H2A H 0.1345 0.0630 0.1247 0.046 Uiso 1 1 calc R
C3 C 0.1119(4) 0.12253(18) 0.2177(4) 0.0373(10) Uani 1 1 d .
C4 C 0.1618(4) 0.14499(19) 0.3187(4) 0.0376(11) Uani 1 1 d .
H4A H 0.1248 0.1757 0.3330 0.045 Uiso 1 1 calc R
C5 C 0.2684(4) 0.12108(17) 0.3992(3) 0.0326(9) Uani 1 1 d .
C6 C 0.3254(4) 0.07613(18) 0.3783(4) 0.0361(10) Uani 1 1 d .
H6A H 0.3960 0.0601 0.4325 0.043 Uiso 1 1 calc R
C7 C 0.4683(5) 0.0064(2) 0.2763(5) 0.0544(15) Uani 1 1 d .
H7A H 0.5325 0.0313 0.3129 0.065 Uiso 1 1 calc R
C8 C 0.4838(5) -0.0414(2) 0.2383(5) 0.0541(15) Uani 1 1 d .
H8A H 0.5625 -0.0552 0.2436 0.065 Uiso 1 1 calc R
C9 C 0.2823(5) -0.03404(18) 0.1990(4) 0.0374(10) Uani 1 1 d .
H9A H 0.1940 -0.0409 0.1728 0.045 Uiso 1 1 calc R
C10 C -0.0050(6) 0.2028(2) 0.1154(5) 0.0558(16) Uani 1 1 d .
H10A H 0.0482 0.2296 0.1584 0.067 Uiso 1 1 calc R
C11 C -0.1111(5) 0.2092(2) 0.0227(5) 0.0559(16) Uani 1 1 d .
H11A H -0.1429 0.2421 -0.0094 0.067 Uiso 1 1 calc R
C12 C -0.0914(4) 0.12489(19) 0.0500(4) 0.0396(11) Uani 1 1 d .
H12A H -0.1051 0.0881 0.0421 0.048 Uiso 1 1 calc R
C13 C 0.2497(5) 0.1683(2) 0.5549(4) 0.0422(11) Uani 1 1 d .
H13A H 0.1617 0.1760 0.5253 0.051 Uiso 1 1 calc R
C14 C 0.3367(5) 0.1802(2) 0.6561(4) 0.0416(11) Uani 1 1 d .
H14A H 0.3175 0.1973 0.7085 0.050 Uiso 1 1 calc R
C15 C 0.4425(4) 0.1408(2) 0.5776(4) 0.0377(10) Uani 1 1 d .
H15A H 0.5092 0.1256 0.5640 0.045 Uiso 1 1 calc R
C16 C 0.4796(4) 0.23585(18) 1.0179(4) 0.0343(10) Uani 1 1 d .
C17 C 0.4040(5) 0.2811(2) 0.9853(4) 0.0463(12) Uani 1 1 d .
H17A H 0.3900 0.2967 0.9194 0.056 Uiso 1 1 calc R
C18 C 0.3480(5) 0.3040(2) 1.0502(4) 0.0476(12) Uani 1 1 d .
H18A H 0.2999 0.3353 1.0276 0.057 Uiso 1 1 calc R
C19 C 0.3627(5) 0.2813(2) 1.1463(4) 0.0396(11) Uani 1 1 d .
C20 C 0.4656(5) 0.2099(2) 1.2836(4) 0.0523(14) Uani 1 1 d .
H20A H 0.4234 0.2225 1.3250 0.063 Uiso 1 1 calc R
C21 C 0.5479(6) 0.1676(2) 1.3198(5) 0.0592(15) Uani 1 1 d .
H21A H 0.5613 0.1518 1.3853 0.071 Uiso 1 1 calc R
C22 C 0.6116(6) 0.1480(3) 1.2604(5) 0.0609(16) Uani 1 1 d .
H22A H 0.6697 0.1198 1.2875 0.073 Uiso 1 1 calc R
C23 C 0.5909(5) 0.1691(2) 1.1628(5) 0.0478(13) Uani 1 1 d .
H23A H 0.6337 0.1548 1.1233 0.057 Uiso 1 1 calc R
C24 C 0.5040(4) 0.21305(18) 1.1202(4) 0.0357(10) Uani 1 1 d .
C25 C 0.4428(4) 0.2348(2) 1.1847(4) 0.0381(10) Uani 1 1 d .
C26 C 0.5298(4) 0.21116(19) 0.9406(4) 0.0353(10) Uani 1 1 d .
C27 C 0.2912(5) 0.3072(2) 1.2069(4) 0.0442(12) Uani 1 1 d .
C28 C 0.9427(15) -0.0727(5) 0.3509(15) 0.214(8) Uani 1 1 d .
H28A H 1.0311 -0.0727 0.3593 0.321 Uiso 1 1 calc R
H28B H 0.8891 -0.0883 0.2829 0.321 Uiso 1 1 calc R
H28C H 0.9354 -0.0932 0.4078 0.321 Uiso 1 1 calc R
C29 C 0.937(2) 0.0263(6) 0.3015(16) 0.252(11) Uani 1 1 d .
H29A H 0.8610 0.0396 0.2433 0.378 Uiso 1 1 calc R
H29B H 0.9972 0.0134 0.2739 0.378 Uiso 1 1 calc R
H29C H 0.9760 0.0546 0.3521 0.378 Uiso 1 1 calc R
C30 C 0.8321(12) -0.0095(6) 0.4162(13) 0.158(6) Uani 1 1 d .
H30A H 0.8159 -0.0374 0.4541 0.190 Uiso 1 1 calc R
C31 C -0.2962(10) -0.0840(6) 0.0090(11) 0.174(6) Uani 1 1 d .
H31A H -0.2810 -0.0463 0.0067 0.261 Uiso 1 1 calc R
H31B H -0.3493 -0.0901 0.0477 0.261 Uiso 1 1 calc R
H31C H -0.3394 -0.0975 -0.0629 0.261 Uiso 1 1 calc R
C32 C -0.1651(14) -0.1707(5) 0.0866(15) 0.199(8) Uani 1 1 d .
H32A H -0.0825 -0.1842 0.0943 0.299 Uiso 1 1 calc R
H32B H -0.2323 -0.1888 0.0283 0.299 Uiso 1 1 calc R
H32C H -0.1762 -0.1767 0.1519 0.299 Uiso 1 1 calc R
C33 C -0.0626(9) -0.0843(6) 0.0968(8) 0.114(4) Uani 1 1 d .
H33A H 0.0136 -0.1027 0.1358 0.136 Uiso 1 1 calc R
N1 N 0.3673(4) -0.06724(15) 0.1905(3) 0.0387(9) Uani 1 1 d .
N2 N 0.3391(4) 0.01123(14) 0.2504(3) 0.0351(8) Uani 1 1 d .
N3 N -0.1649(4) 0.16080(15) -0.0172(3) 0.0396(9) Uani 1 1 d .
N4 N 0.0078(4) 0.14856(15) 0.1329(3) 0.0387(10) Uani 1 1 d .
N5 N 0.4576(4) 0.16298(15) 0.6689(3) 0.0349(8) Uani 1 1 d .
N6 N 0.3177(4) 0.14270(15) 0.5053(3) 0.0348(8) Uani 1 1 d .
N7 N 0.9009(8) -0.0176(4) 0.3552(7) 0.118(3) Uani 1 1 d .
N8 N -0.1720(8) -0.1119(4) 0.0635(8) 0.130(3) Uani 1 1 d .
O1 O 0.5249(4) 0.16096(14) 0.9302(3) 0.0498(9) Uani 1 1 d .
O1W O 0.1630(4) 0.4343(2) 1.0417(4) 0.0792(14) Uani 1 1 d .
O2 O 0.5725(3) 0.24045(13) 0.8898(3) 0.0420(8) Uani 1 1 d .
O3 O 0.2794(5) 0.35687(18) 1.2035(4) 0.0647(11) Uani 1 1 d .
O4 O 0.2459(4) 0.27759(16) 1.2577(3) 0.0524(9) Uani 1 1 d .
O5 O 0.7929(9) 0.0355(5) 0.4191(8) 0.185(5) Uani 1 1 d .
O6 O -0.0535(7) -0.0347(4) 0.0799(7) 0.138(3) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cd Cd -0.8075 1.2024 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O4 Cd1 N1 131.53(14) 4_665 3_656
O4 Cd1 N3 87.30(15) 4_665 1_656
N1 Cd1 N3 95.79(14) 3_656 1_656
O4 Cd1 N5 91.59(14) 4_665 .
N1 Cd1 N5 86.82(13) 3_656 .
N3 Cd1 N5 177.26(13) 1_656 .
O4 Cd1 O1 136.72(13) 4_665 .
N1 Cd1 O1 91.74(13) 3_656 .
N3 Cd1 O1 89.01(16) 1_656 .
N5 Cd1 O1 90.08(15) . .
O4 Cd1 O2 83.31(13) 4_665 .
N1 Cd1 O2 144.93(12) 3_656 .
N3 Cd1 O2 88.87(13) 1_656 .
N5 Cd1 O2 88.51(13) . .
O1 Cd1 O2 53.50(11) . .
O4 Cd1 C26 109.62(14) 4_665 .
N1 Cd1 C26 118.85(14) 3_656 .
N3 Cd1 C26 86.63(15) 1_656 .
N5 Cd1 C26 91.38(14) . .
O1 Cd1 C26 27.10(12) . .
O2 Cd1 C26 26.56(12) . .
C2 C1 C6 121.7(4) . .
C2 C1 N2 119.1(4) . .
C6 C1 N2 119.1(4) . .
C1 C2 C3 118.1(4) . .
C1 C2 H2A 121.0 . .
C3 C2 H2A 121.0 . .
C4 C3 C2 121.6(4) . .
C4 C3 N4 119.4(4) . .
C2 C3 N4 118.8(4) . .
C3 C4 C5 118.9(4) . .
C3 C4 H4A 120.5 . .
C5 C4 H4A 120.5 . .
C6 C5 C4 121.0(4) . .
C6 C5 N6 119.6(4) . .
C4 C5 N6 119.5(4) . .
C5 C6 C1 118.7(4) . .
C5 C6 H6A 120.7 . .
C1 C6 H6A 120.7 . .
C8 C7 N2 105.9(5) . .
C8 C7 H7A 127.0 . .
N2 C7 H7A 127.0 . .
C7 C8 N1 110.4(5) . .
C7 C8 H8A 124.8 . .
N1 C8 H8A 124.8 . .
N1 C9 N2 111.3(4) . .
N1 C9 H9A 124.3 . .
N2 C9 H9A 124.3 . .
C11 C10 N4 105.7(4) . .
C11 C10 H10A 127.2 . .
N4 C10 H10A 127.2 . .
C10 C11 N3 110.5(4) . .
C10 C11 H11A 124.7 . .
N3 C11 H11A 124.7 . .
N3 C12 N4 111.0(4) . .
N3 C12 H12A 124.5 . .
N4 C12 H12A 124.5 . .
C14 C13 N6 106.3(4) . .
C14 C13 H13A 126.9 . .
N6 C13 H13A 126.9 . .
C13 C14 N5 109.4(4) . .
C13 C14 H14A 125.3 . .
N5 C14 H14A 125.3 . .
N5 C15 N6 111.7(4) . .
N5 C15 H15A 124.1 . .
N6 C15 H15A 124.1 . .
C17 C16 C24 119.4(4) . .
C17 C16 C26 117.9(4) . .
C24 C16 C26 122.6(4) . .
C16 C17 C18 120.8(5) . .
C16 C17 H17A 119.6 . .
C18 C17 H17A 119.6 . .
C19 C18 C17 121.6(5) . .
C19 C18 H18A 119.2 . .
C17 C18 H18A 119.2 . .
C18 C19 C25 119.6(4) . .
C18 C19 C27 117.4(5) . .
C25 C19 C27 123.1(5) . .
C21 C20 C25 121.4(5) . .
C21 C20 H20A 119.3 . .
C25 C20 H20A 119.3 . .
C20 C21 C22 120.7(6) . .
C20 C21 H21A 119.7 . .
C22 C21 H21A 119.7 . .
C23 C22 C21 121.0(6) . .
C23 C22 H22A 119.5 . .
C21 C22 H22A 119.5 . .
C22 C23 C24 120.7(5) . .
C22 C23 H23A 119.7 . .
C24 C23 H23A 119.7 . .
C16 C24 C23 122.0(4) . .
C16 C24 C25 120.0(4) . .
C23 C24 C25 117.9(5) . .
C20 C25 C24 118.3(5) . .
C20 C25 C19 123.2(5) . .
C24 C25 C19 118.5(4) . .
O2 C26 O1 122.5(4) . .
O2 C26 C16 119.5(4) . .
O1 C26 C16 118.0(4) . .
O2 C26 Cd1 64.2(2) . .
O1 C26 Cd1 58.9(2) . .
C16 C26 Cd1 171.9(3) . .
O3 C27 O4 122.9(5) . .
O3 C27 C19 118.5(5) . .
O4 C27 C19 118.6(5) . .
N7 C28 H28A 109.5 . .
N7 C28 H28B 109.5 . .
H28A C28 H28B 109.5 . .
N7 C28 H28C 109.5 . .
H28A C28 H28C 109.5 . .
H28B C28 H28C 109.5 . .
N7 C29 H29A 109.5 . .
N7 C29 H29B 109.5 . .
H29A C29 H29B 109.5 . .
N7 C29 H29C 109.5 . .
H29A C29 H29C 109.5 . .
H29B C29 H29C 109.5 . .
O5 C30 N7 117.6(17) . .
O5 C30 H30A 121.2 . .
N7 C30 H30A 121.2 . .
N8 C31 H31A 109.5 . .
N8 C31 H31B 109.5 . .
H31A C31 H31B 109.5 . .
N8 C31 H31C 109.5 . .
H31A C31 H31C 109.5 . .
H31B C31 H31C 109.5 . .
N8 C32 H32A 109.5 . .
N8 C32 H32B 109.5 . .
H32A C32 H32B 109.5 . .
N8 C32 H32C 109.5 . .
H32A C32 H32C 109.5 . .
H32B C32 H32C 109.5 . .
O6 C33 N8 125.3(11) . .
O6 C33 H33A 117.3 . .
N8 C33 H33A 117.3 . .
C9 N1 C8 105.1(4) . .
C9 N1 Cd1 127.6(3) . 3_656
C8 N1 Cd1 122.1(3) . 3_656
C9 N2 C7 107.2(4) . .
C9 N2 C1 125.9(4) . .
C7 N2 C1 126.8(4) . .
C12 N3 C11 105.9(4) . .
C12 N3 Cd1 136.0(3) . 1_454
C11 N3 Cd1 118.0(3) . 1_454
C12 N4 C10 106.9(4) . .
C12 N4 C3 127.2(4) . .
C10 N4 C3 125.7(4) . .
C15 N5 C14 105.9(4) . .
C15 N5 Cd1 124.7(3) . .
C14 N5 Cd1 128.7(3) . .
C15 N6 C13 106.7(4) . .
C15 N6 C5 125.8(4) . .
C13 N6 C5 127.5(4) . .
C30 N7 C28 115.9(12) . .
C30 N7 C29 122.5(12) . .
C28 N7 C29 121.5(12) . .
C33 N8 C31 119.7(11) . .
C33 N8 C32 118.5(11) . .
C31 N8 C32 121.8(9) . .
C26 O1 Cd1 94.0(3) . .
C26 O2 Cd1 89.3(3) . .
C27 O4 Cd1 101.2(3) . 4_566
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Cd1 O4 2.317(4) 4_665
Cd1 N1 2.318(4) 3_656
Cd1 N3 2.324(4) 1_656
Cd1 N5 2.331(4) .
Cd1 O1 2.365(4) .
Cd1 O2 2.481(3) .
Cd1 C26 2.756(5) .
C1 C2 1.381(6) .
C1 C6 1.389(6) .
C1 N2 1.430(6) .
C2 C3 1.393(6) .
C2 H2A 0.9300 .
C3 C4 1.376(6) .
C3 N4 1.426(5) .
C4 C5 1.392(6) .
C4 H4A 0.9300 .
C5 C6 1.380(6) .
C5 N6 1.426(5) .
C6 H6A 0.9300 .
C7 C8 1.341(7) .
C7 N2 1.363(6) .
C7 H7A 0.9300 .
C8 N1 1.372(6) .
C8 H8A 0.9300 .
C9 N1 1.311(6) .
C9 N2 1.347(6) .
C9 H9A 0.9300 .
C10 C11 1.352(7) .
C10 N4 1.372(6) .
C10 H10A 0.9300 .
C11 N3 1.362(6) .
C11 H11A 0.9300 .
C12 N3 1.309(6) .
C12 N4 1.361(6) .
C12 H12A 0.9300 .
C13 C14 1.361(7) .
C13 N6 1.373(6) .
C13 H13A 0.9300 .
C14 N5 1.378(6) .
C14 H14A 0.9300 .
C15 N5 1.308(6) .
C15 N6 1.354(6) .
C15 H15A 0.9300 .
C16 C17 1.377(7) .
C16 C24 1.424(6) .
C16 C26 1.518(6) .
C17 C18 1.403(7) .
C17 H17A 0.9300 .
C18 C19 1.374(7) .
C18 H18A 0.9300 .
C19 C25 1.433(7) .
C19 C27 1.515(7) .
C20 C21 1.360(8) .
C20 C25 1.410(7) .
C20 H20A 0.9300 .
C21 C22 1.374(9) .
C21 H21A 0.9300 .
C22 C23 1.360(8) .
C22 H22A 0.9300 .
C23 C24 1.429(7) .
C23 H23A 0.9300 .
C24 C25 1.430(6) .
C26 O2 1.233(6) .
C26 O1 1.259(5) .
C27 O3 1.247(7) .
C27 O4 1.255(7) .
C28 N7 1.463(14) .
C28 H28A 0.9600 .
C28 H28B 0.9600 .
C28 H28C 0.9600 .
C29 N7 1.463(14) .
C29 H29A 0.9600 .
C29 H29B 0.9600 .
C29 H29C 0.9600 .
C30 O5 1.213(14) .
C30 N7 1.367(16) .
C30 H30A 0.9300 .
C31 N8 1.471(13) .
C31 H31A 0.9600 .
C31 H31B 0.9600 .
C31 H31C 0.9600 .
C32 N8 1.494(14) .
C32 H32A 0.9600 .
C32 H32B 0.9600 .
C32 H32C 0.9600 .
C33 O6 1.270(13) .
C33 N8 1.325(12) .
C33 H33A 0.9300 .
N1 Cd1 2.318(4) 3_656
N3 Cd1 2.324(4) 1_454
O4 Cd1 2.317(4) 4_566
