#------------------------------------------------------------------------------
#$Date: 2016-04-20 09:06:48 +0300 (Wed, 20 Apr 2016) $
#$Revision: 182219 $
#$URL: svn://www.crystallography.net/cod/cif/7/22/49/7224959.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7224959
loop_
_publ_author_name
'Zhang, Min'
'Lian, Zhipeng'
'Wang, Ying'
'Pan, Shilie'
_publ_section_title
;
 Nonlinear optical and self-activated luminescent properties of A2W3O10(A
 = Rb and Cs)
;
_journal_issue                   45
_journal_name_full               'RSC Adv.'
_journal_page_first              39234
_journal_paper_doi               10.1039/C6RA03407A
_journal_volume                  6
_journal_year                    2016
_chemical_formula_sum            'O10 Rb2 W3'
_chemical_formula_weight         882.49
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           82
_symmetry_cell_setting           tetragonal
_symmetry_space_group_name_Hall  'I -4'
_symmetry_space_group_name_H-M   'I -4'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2016-02-05 deposited with the CCDC.
2016-04-12 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   15.9516(9)
_cell_length_b                   15.9516(9)
_cell_length_c                   10.0565(11)
_cell_measurement_temperature    296(2)
_cell_volume                     2558.9(3)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0691
_diffrn_reflns_av_sigmaI/netI    0.0769
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       12
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_number            7864
_diffrn_reflns_theta_full        27.45
_diffrn_reflns_theta_max         27.45
_diffrn_reflns_theta_min         2.39
_exptl_absorpt_coefficient_mu    34.491
_exptl_crystal_density_diffrn    4.581
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             3008
_refine_diff_density_max         6.969
_refine_diff_density_min         -3.977
_refine_diff_density_rms         0.635
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.00
_refine_ls_extinction_coef       0.00057(4)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.041
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     211
_refine_ls_number_reflns         2886
_refine_ls_number_restraints     31
_refine_ls_restrained_S_all      1.035
_refine_ls_R_factor_all          0.0534
_refine_ls_R_factor_gt           0.0488
_refine_ls_shift/su_max          1.566
_refine_ls_shift/su_mean         0.012
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0515P)²+187.7496P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1136
_refine_ls_wR_factor_ref         0.1174
_reflns_number_gt                2671
_reflns_number_total             2886
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c6ra03407a2.cif
_cod_data_source_block           rb
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Tetragonal' changed to 'tetragonal'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4268 2015-11-12 08:31:59Z antanas 
;
_cod_original_sg_symbol_H-M      I-4
_cod_database_code               7224959
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'y, -x, -z'
'-y, x, -z'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, -y+1/2, z+1/2'
'y+1/2, -x+1/2, -z+1/2'
'-y+1/2, x+1/2, -z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
W1 W 0.96197(5) 0.39142(5) 1.11644(8) 0.0075(2) Uani 1 1 d .
W2 W 0.73808(6) 0.51560(6) 0.66497(9) 0.0127(2) Uani 1 1 d .
W3 W 0.86894(6) 0.18280(6) 1.14652(9) 0.0120(2) Uani 1 1 d .
W4 W 0.85201(6) 0.72083(6) 0.58726(9) 0.0123(2) Uani 1 1 d .
Rb1 Rb 1.0000 0.0000 1.5000 0.097(4) Uani 0.9081(10) 4 d SPDU
Rb2 Rb 1.0000 0.5000 0.7500 0.087(4) Uani 1 4 d S
Rb3 Rb 0.9102(2) 0.2936(3) 1.4941(4) 0.0495(10) Uani 1 1 d .
Rb4 Rb 0.5000 0.5000 0.5000 0.080(4) Uani 1 4 d S
Rb5 Rb 1.11491(18) 0.21591(18) 1.2176(3) 0.0260(6) Uani 1 1 d .
O1 O 0.9079(10) 0.2966(9) 1.1876(14) 0.009(3) Uani 1 1 d .
O2 O 1.0144(9) 0.3347(9) 0.9893(16) 0.006(3) Uani 1 1 d .
O3 O 0.7997(9) 0.6101(11) 0.6894(14) 0.009(3) Uani 1 1 d .
O4 O 0.8630(9) 0.4107(8) 1.0116(15) 0.002(3) Uani 1 1 d .
O5 O 0.6853(10) 0.5618(11) 0.5064(19) 0.017(4) Uani 1 1 d .
O6 O 0.7581(11) 0.7139(9) 0.4821(18) 0.014(4) Uani 1 1 d .
O7 O 1.0429(9) 0.3924(9) 1.2429(16) 0.007(3) Uani 1 1 d .
O8 O 0.8107(11) 0.0903(10) 1.0841(16) 0.016(4) Uani 1 1 d .
O9 O 0.7985(10) 0.4448(10) 0.7748(15) 0.013(4) Uani 1 1 d .
O10 O 1.0000 0.5000 1.056(2) 0.007(4) Uani 1 2 d S
O11 O 0.9002(12) 0.8097(11) 0.513(2) 0.024(4) Uani 1 1 d .
O12 O 0.7813(10) 0.2058(11) 1.2735(16) 0.013(3) Uani 1 1 d .
O13 O 0.9385(13) 0.1328(11) 1.255(2) 0.025(4) Uani 1 1 d .
O14 O 0.6503(11) 0.5350(13) 0.770(2) 0.023(4) Uani 1 1 d .
W5 W 0.9010(6) 0.0500(5) 1.3764(10) 0.0078(19) Uani 0.0917(14) 1 d PDU
O16 O 1.0000 0.0000 1.669(2) 0.02(6) Uani 0.0919(14) 2 d SPDU
O15 O 0.903(3) -0.028(11) 1.506(16) 0.03(5) Uani 0.0919(14) 1 d PDU
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O2 W1 O7 100.1(7) . .
O2 W1 O1 94.6(6) . .
O7 W1 O1 93.8(7) . .
O2 W1 O4 94.2(7) . .
O7 W1 O4 165.5(6) . .
O1 W1 O4 87.8(7) . .
O2 W1 O10 94.7(6) . .
O7 W1 O10 89.4(7) . .
O1 W1 O10 169.5(5) . .
O4 W1 O10 86.7(5) . .
O2 W1 O7 175.7(7) . 7_567
O7 W1 O7 84.1(6) . 7_567
O1 W1 O7 84.4(6) . 7_567
O4 W1 O7 81.6(6) . 7_567
O10 W1 O7 86.0(6) . 7_567
O2 W1 Rb3 52.3(5) . 8_647
O7 W1 Rb3 60.5(5) . 8_647
O1 W1 Rb3 127.0(5) . 8_647
O4 W1 Rb3 128.7(4) . 8_647
O10 W1 Rb3 63.07(10) . 8_647
O7 W1 Rb3 131.3(4) 7_567 8_647
O2 W1 Rb2 60.0(5) . .
O7 W1 Rb2 121.3(5) . .
O1 W1 Rb2 138.2(5) . .
O4 W1 Rb2 64.1(5) . .
O10 W1 Rb2 45.2(6) . .
O7 W1 Rb2 118.4(4) 7_567 .
Rb3 W1 Rb2 65.36(5) 8_647 .
O2 W1 Rb3 123.8(5) . .
O7 W1 Rb3 60.5(5) . .
O1 W1 Rb3 42.7(5) . .
O4 W1 Rb3 113.3(5) . .
O10 W1 Rb3 132.9(6) . .
O7 W1 Rb3 57.7(4) 7_567 .
Rb3 W1 Rb3 117.68(6) 8_647 .
Rb2 W1 Rb3 175.97(6) . .
O2 W1 Rb5 134.7(5) . 7_567
O7 W1 Rb5 112.4(5) . 7_567
O1 W1 Rb5 53.9(5) . 7_567
O4 W1 Rb5 57.5(4) . 7_567
O10 W1 Rb5 115.65(17) . 7_567
O7 W1 Rb5 41.9(4) 7_567 7_567
Rb3 W1 Rb5 172.32(7) 8_647 7_567
Rb2 W1 Rb5 119.72(4) . 7_567
Rb3 W1 Rb5 56.97(7) . 7_567
O2 W1 Rb3 118.9(5) . 7_567
O7 W1 Rb3 128.3(5) . 7_567
O1 W1 Rb3 113.8(5) . 7_567
O4 W1 Rb3 39.4(4) . 7_567
O10 W1 Rb3 56.97(9) . 7_567
O7 W1 Rb3 58.1(4) 7_567 7_567
Rb3 W1 Rb3 118.33(8) 8_647 7_567
Rb2 W1 Rb3 63.30(6) . 7_567
Rb3 W1 Rb3 112.68(5) . 7_567
Rb5 W1 Rb3 62.84(8) 7_567 7_567
O14 W2 O3 101.6(8) . .
O14 W2 O9 99.2(8) . .
O3 W2 O9 98.3(7) . .
O14 W2 O5 94.7(8) . .
O3 W2 O5 91.7(7) . .
O9 W2 O5 160.8(8) . .
O14 W2 O8 94.7(8) . 6_654
O3 W2 O8 162.2(7) . 6_654
O9 W2 O8 86.0(7) . 6_654
O5 W2 O8 79.7(7) . 6_654
O14 W2 O2 171.8(8) . 7_566
O3 W2 O2 84.2(6) . 7_566
O9 W2 O2 85.7(7) . 7_566
O5 W2 O2 79.1(6) . 7_566
O8 W2 O2 79.0(6) 6_654 7_566
O14 W2 Rb3 65.5(7) . 7_567
O3 W2 Rb3 59.0(5) . 7_567
O9 W2 Rb3 61.4(5) . 7_567
O5 W2 Rb3 137.2(6) . 7_567
O8 W2 Rb3 136.3(4) 6_654 7_567
O2 W2 Rb3 122.7(4) 7_566 7_567
O14 W2 Rb5 50.5(6) . 5_454
O3 W2 Rb5 64.0(5) . 5_454
O9 W2 Rb5 134.6(6) . 5_454
O5 W2 Rb5 64.6(6) . 5_454
O8 W2 Rb5 124.0(5) 6_654 5_454
O2 W2 Rb5 129.4(4) 7_566 5_454
Rb3 W2 Rb5 74.18(7) 7_567 5_454
O14 W2 Rb4 61.9(7) . .
O3 W2 Rb4 126.8(5) . .
O9 W2 Rb4 132.7(5) . .
O5 W2 Rb4 45.6(5) . .
O8 W2 Rb4 55.9(5) 6_654 .
O2 W2 Rb4 109.9(4) 7_566 .
Rb3 W2 Rb4 127.08(7) 7_567 .
Rb5 W2 Rb4 68.40(5) 5_454 .
O14 W2 Rb2 131.2(7) . .
O3 W2 Rb2 59.5(5) . .
O9 W2 Rb2 48.4(5) . .
O5 W2 Rb2 127.5(5) . .
O8 W2 Rb2 114.0(5) 6_654 .
O2 W2 Rb2 56.8(4) 7_566 .
Rb3 W2 Rb2 66.59(7) 7_567 .
Rb5 W2 Rb2 121.90(5) 5_454 .
Rb4 W2 Rb2 166.20(3) . .
O13 W3 O8 99.6(9) . .
O13 W3 O5 98.5(9) . 8_646
O8 W3 O5 91.9(7) . 8_646
O13 W3 O12 97.6(8) . .
O8 W3 O12 90.7(8) . .
O5 W3 O12 163.0(7) 8_646 .
O13 W3 O1 95.1(8) . .
O8 W3 O1 165.1(7) . .
O5 W3 O1 88.1(7) 8_646 .
O12 W3 O1 85.1(7) . .
O13 W3 O6 174.1(8) . 8_646
O8 W3 O6 86.2(7) . 8_646
O5 W3 O6 82.0(7) 8_646 8_646
O12 W3 O6 81.4(7) . 8_646
O1 W3 O6 79.0(6) . 8_646
O13 W3 Rb4 63.5(6) . 5_545
O8 W3 Rb4 62.8(5) . 5_545
O5 W3 Rb4 52.6(5) 8_646 5_545
O12 W3 Rb4 141.7(5) . 5_545
O1 W3 Rb4 127.2(5) . 5_545
O6 W3 Rb4 120.6(4) 8_646 5_545
O13 W3 Rb3 63.1(6) . .
O8 W3 Rb3 137.4(5) . .
O5 W3 Rb3 127.5(6) 8_646 .
O12 W3 Rb3 56.8(5) . .
O1 W3 Rb3 49.5(4) . .
O6 W3 Rb3 111.9(5) 8_646 .
Rb4 W3 Rb3 125.42(6) 5_545 .
O13 W3 Rb5 48.0(7) . .
O8 W3 Rb5 130.8(5) . .
O5 W3 Rb5 64.7(6) 8_646 .
O12 W3 Rb5 124.4(5) . .
O1 W3 Rb5 62.1(5) . .
O6 W3 Rb5 128.1(4) 8_646 .
Rb4 W3 Rb5 68.93(4) 5_545 .
Rb3 W3 Rb5 67.89(7) . .
O13 W3 Rb5 130.9(6) . 4_647
O8 W3 Rb5 46.6(5) . 4_647
O5 W3 Rb5 57.8(6) 8_646 4_647
O12 W3 Rb5 114.0(5) . 4_647
O1 W3 Rb5 122.9(4) . 4_647
O6 W3 Rb5 54.2(4) 8_646 4_647
Rb4 W3 Rb5 68.64(4) 5_545 4_647
Rb3 W3 Rb5 165.87(8) . 4_647
Rb5 W3 Rb5 121.43(6) . 4_647
O13 W3 Rb5 120.4(6) . 7_567
O8 W3 Rb5 115.1(5) . 7_567
O5 W3 Rb5 125.3(5) 8_646 7_567
O12 W3 Rb5 39.7(5) . 7_567
O1 W3 Rb5 54.2(5) . 7_567
O6 W3 Rb5 55.5(4) 8_646 7_567
Rb4 W3 Rb5 176.09(5) 5_545 7_567
Rb3 W3 Rb5 58.46(7) . 7_567
Rb5 W3 Rb5 113.67(7) . 7_567
Rb5 W3 Rb5 107.47(5) 4_647 7_567
O11 W4 O6 99.2(8) . .
O11 W4 O4 97.4(7) . 7_566
O6 W4 O4 93.3(6) . 7_566
O11 W4 O12 96.4(8) . 4_657
O6 W4 O12 93.3(7) . 4_657
O4 W4 O12 163.5(7) 7_566 4_657
O11 W4 O9 95.2(8) . 7_566
O6 W4 O9 165.6(7) . 7_566
O4 W4 O9 83.9(6) 7_566 7_566
O12 W4 O9 85.9(7) 4_657 7_566
O11 W4 O3 175.9(8) . .
O6 W4 O3 84.9(6) . .
O4 W4 O3 82.4(6) 7_566 .
O12 W4 O3 83.2(7) 4_657 .
O9 W4 O3 80.7(6) 7_566 .
O11 W4 Rb5 48.2(6) . 2_764
O6 W4 Rb5 64.9(5) . 2_764
O4 W4 Rb5 67.5(4) 7_566 2_764
O12 W4 Rb5 128.9(5) 4_657 2_764
O9 W4 Rb5 126.0(5) 7_566 2_764
O3 W4 Rb5 134.7(4) . 2_764
O11 W4 Rb3 63.4(6) . 4_657
O6 W4 Rb3 55.9(5) . 4_657
O4 W4 Rb3 136.5(5) 7_566 4_657
O12 W4 Rb3 58.8(5) 4_657 4_657
O9 W4 Rb3 133.5(4) 7_566 4_657
O3 W4 Rb3 119.5(4) . 4_657
Rb5 W4 Rb3 71.28(7) 2_764 4_657
O11 W4 Rb3 61.8(6) . 2_764
O6 W4 Rb3 130.5(5) . 2_764
O4 W4 Rb3 50.2(4) 7_566 2_764
O12 W4 Rb3 131.7(5) 4_657 2_764
O9 W4 Rb3 56.9(5) 7_566 2_764
O3 W4 Rb3 115.5(4) . 2_764
Rb5 W4 Rb3 69.81(8) 2_764 2_764
Rb3 W4 Rb3 124.95(12) 4_657 2_764
O11 W4 Rb5 124.2(6) . 5_454
O6 W4 Rb5 54.3(5) . 5_454
O4 W4 Rb5 128.3(4) 7_566 5_454
O12 W4 Rb5 47.3(5) 4_657 5_454
O9 W4 Rb5 117.2(5) 7_566 5_454
O3 W4 Rb5 58.3(4) . 5_454
Rb5 W4 Rb5 116.51(6) 2_764 5_454
Rb3 W4 Rb5 61.37(7) 4_657 5_454
Rb3 W4 Rb5 173.10(8) 2_764 5_454
O15 Rb1 O15 176(10) 3_668 4_648
O15 Rb1 O15 90.1(5) 3_668 .
O15 Rb1 O15 90.1(6) 4_648 .
O15 Rb1 O15 90.1(6) 3_668 2_755
O15 Rb1 O15 90.1(5) 4_648 2_755
O15 Rb1 O15 176(10) . 2_755
O15 Rb1 O16 92(6) 3_668 .
O15 Rb1 O16 92(6) 4_648 .
O15 Rb1 O16 88(6) . .
O15 Rb1 O16 88(6) 2_755 .
O15 Rb1 O16 88(6) 3_668 3_668
O15 Rb1 O16 88(6) 4_648 3_668
O15 Rb1 O16 92(6) . 3_668
O15 Rb1 O16 92(6) 2_755 3_668
O16 Rb1 O16 179.998(4) . 3_668
O15 Rb1 W5 54.8(8) 3_668 3_668
O15 Rb1 W5 128(9) 4_648 3_668
O15 Rb1 W5 122(9) . 3_668
O15 Rb1 W5 54.6(11) 2_755 3_668
O16 Rb1 W5 54.9(3) . 3_668
O16 Rb1 W5 125.1(3) 3_668 3_668
O15 Rb1 W5 128(9) 3_668 4_648
O15 Rb1 W5 54.8(8) 4_648 4_648
O15 Rb1 W5 54.6(11) . 4_648
O15 Rb1 W5 122(9) 2_755 4_648
O16 Rb1 W5 54.9(3) . 4_648
O16 Rb1 W5 125.1(3) 3_668 4_648
W5 Rb1 W5 109.8(6) 3_668 4_648
O15 Rb1 W5 54.6(11) 3_668 .
O15 Rb1 W5 122(9) 4_648 .
O15 Rb1 W5 54.8(8) . .
O15 Rb1 W5 128(9) 2_755 .
O16 Rb1 W5 125.1(3) . .
O16 Rb1 W5 54.9(3) 3_668 .
W5 Rb1 W5 109.3(3) 3_668 .
W5 Rb1 W5 109.3(3) 4_648 .
O15 Rb1 W5 122(9) 3_668 2_755
O15 Rb1 W5 54.6(11) 4_648 2_755
O15 Rb1 W5 128(9) . 2_755
O15 Rb1 W5 54.8(8) 2_755 2_755
O16 Rb1 W5 125.1(3) . 2_755
O16 Rb1 W5 54.9(3) 3_668 2_755
W5 Rb1 W5 109.3(3) 3_668 2_755
W5 Rb1 W5 109.3(3) 4_648 2_755
W5 Rb1 W5 109.8(6) . 2_755
O15 Rb1 O14 45(6) 3_668 8_647
O15 Rb1 O14 139(6) 4_648 8_647
O15 Rb1 O14 91(9) . 8_647
O15 Rb1 O14 86.3(11) 2_755 8_647
O16 Rb1 O14 46.8(3) . 8_647
O16 Rb1 O14 133.2(4) 3_668 8_647
W5 Rb1 O14 31.7(4) 3_668 8_647
W5 Rb1 O14 93.7(4) 4_648 8_647
W5 Rb1 O14 90.6(5) . 8_647
W5 Rb1 O14 140.9(4) 2_755 8_647
O15 Rb1 O14 139(6) 3_668 7_557
O15 Rb1 O14 45(6) 4_648 7_557
O15 Rb1 O14 86.3(11) . 7_557
O15 Rb1 O14 91(9) 2_755 7_557
O16 Rb1 O14 46.8(3) . 7_557
O16 Rb1 O14 133.2(4) 3_668 7_557
W5 Rb1 O14 93.7(4) 3_668 7_557
W5 Rb1 O14 31.7(4) 4_648 7_557
W5 Rb1 O14 140.9(4) . 7_557
W5 Rb1 O14 90.6(5) 2_755 7_557
O14 Rb1 O14 93.7(7) 8_647 7_557
O10 Rb2 O10 179.999(1) . 7_566
O10 Rb2 O9 94.3(3) . 7_566
O10 Rb2 O9 85.7(3) 7_566 7_566
O10 Rb2 O9 94.3(3) . 8_646
O10 Rb2 O9 85.7(3) 7_566 8_646
O9 Rb2 O9 171.5(5) 7_566 8_646
O10 Rb2 O9 85.7(3) . .
O10 Rb2 O9 94.3(3) 7_566 .
O9 Rb2 O9 90.32(4) 7_566 .
O9 Rb2 O9 90.32(4) 8_646 .
O10 Rb2 O9 85.7(3) . 2_765
O10 Rb2 O9 94.3(3) 7_566 2_765
O9 Rb2 O9 90.32(4) 7_566 2_765
O9 Rb2 O9 90.32(4) 8_646 2_765
O9 Rb2 O9 171.5(5) . 2_765
O10 Rb2 O2 47.7(3) . 2_765
O10 Rb2 O2 132.3(3) 7_566 2_765
O9 Rb2 O2 47.5(4) 7_566 2_765
O9 Rb2 O2 140.9(4) 8_646 2_765
O9 Rb2 O2 94.7(4) . 2_765
O9 Rb2 O2 79.5(3) 2_765 2_765
O10 Rb2 O2 47.7(3) . .
O10 Rb2 O2 132.3(3) 7_566 .
O9 Rb2 O2 140.9(4) 7_566 .
O9 Rb2 O2 47.5(4) 8_646 .
O9 Rb2 O2 79.5(3) . .
O9 Rb2 O2 94.7(4) 2_765 .
O2 Rb2 O2 95.4(5) 2_765 .
O10 Rb2 O2 132.3(3) . 7_566
O10 Rb2 O2 47.7(3) 7_566 7_566
O9 Rb2 O2 79.5(3) 7_566 7_566
O9 Rb2 O2 94.7(4) 8_646 7_566
O9 Rb2 O2 47.5(4) . 7_566
O9 Rb2 O2 140.9(4) 2_765 7_566
O2 Rb2 O2 116.9(3) 2_765 7_566
O2 Rb2 O2 116.9(3) . 7_566
O10 Rb2 O2 132.3(3) . 8_646
O10 Rb2 O2 47.7(3) 7_566 8_646
O9 Rb2 O2 94.7(4) 7_566 8_646
O9 Rb2 O2 79.5(3) 8_646 8_646
O9 Rb2 O2 140.9(4) . 8_646
O9 Rb2 O2 47.5(4) 2_765 8_646
O2 Rb2 O2 116.9(3) 2_765 8_646
O2 Rb2 O2 116.9(3) . 8_646
O2 Rb2 O2 95.4(5) 7_566 8_646
O10 Rb2 W1 26.474(12) . 2_765
O10 Rb2 W1 153.525(12) 7_566 2_765
O9 Rb2 W1 72.6(2) 7_566 2_765
O9 Rb2 W1 115.6(3) 8_646 2_765
O9 Rb2 W1 100.7(3) . 2_765
O9 Rb2 W1 71.4(2) 2_765 2_765
O2 Rb2 W1 25.5(2) 2_765 2_765
O2 Rb2 W1 72.4(3) . 2_765
O2 Rb2 W1 137.5(2) 7_566 2_765
O2 Rb2 W1 117.8(2) 8_646 2_765
O10 Rb2 W1 26.474(12) . .
O10 Rb2 W1 153.527(12) 7_566 .
O9 Rb2 W1 115.6(3) 7_566 .
O9 Rb2 W1 72.6(2) 8_646 .
O9 Rb2 W1 71.4(2) . .
O9 Rb2 W1 100.7(3) 2_765 .
O2 Rb2 W1 72.4(3) 2_765 .
O2 Rb2 W1 25.5(2) . .
O2 Rb2 W1 117.8(2) 7_566 .
O2 Rb2 W1 137.5(2) 8_646 .
W1 Rb2 W1 52.95(2) 2_765 .
O4 Rb3 O1 89.2(4) 8_647 .
O4 Rb3 O3 95.8(4) 8_647 8_647
O1 Rb3 O3 173.0(4) . 8_647
O4 Rb3 O6 172.8(5) 8_647 3_567
O1 Rb3 O6 93.8(5) . 3_567
O3 Rb3 O6 80.6(5) 8_647 3_567
O4 Rb3 O9 49.3(4) 8_647 8_647
O1 Rb3 O9 135.8(4) . 8_647
O3 Rb3 O9 50.6(4) 8_647 8_647
O6 Rb3 O9 129.3(4) 3_567 8_647
O4 Rb3 O15 94(3) 8_647 3_668
O1 Rb3 O15 91(3) . 3_668
O3 Rb3 O15 93(3) 8_647 3_668
O6 Rb3 O15 93(3) 3_567 3_668
O9 Rb3 O15 79.1(5) 8_647 3_668
O4 Rb3 O2 90.3(4) 8_647 7_567
O1 Rb3 O2 91.8(4) . 7_567
O3 Rb3 O2 83.4(4) 8_647 7_567
O6 Rb3 O2 83.1(4) 3_567 7_567
O9 Rb3 O2 101.5(4) 8_647 7_567
O15 Rb3 O2 175(4) 3_668 7_567
O4 Rb3 O12 135.6(4) 8_647 .
O1 Rb3 O12 48.2(4) . .
O3 Rb3 O12 127.7(4) 8_647 .
O6 Rb3 O12 49.3(4) 3_567 .
O9 Rb3 O12 156.4(4) 8_647 .
O15 Rb3 O12 77.5(6) 3_668 .
O2 Rb3 O12 101.5(4) 7_567 .
O4 Rb3 O14 90.9(4) 8_647 8_647
O1 Rb3 O14 135.1(4) . 8_647
O3 Rb3 O14 49.8(4) 8_647 8_647
O6 Rb3 O14 91.5(5) 3_567 8_647
O9 Rb3 O14 48.8(4) 8_647 8_647
O15 Rb3 O14 44(3) 3_668 8_647
O2 Rb3 O14 133.0(4) 7_567 8_647
O12 Rb3 O14 109.8(5) . 8_647
O4 Rb3 O11 49.9(4) 8_647 2_766
O1 Rb3 O11 94.2(5) . 2_766
O3 Rb3 O11 92.7(5) 8_647 2_766
O6 Rb3 O11 136.1(4) 3_567 2_766
O9 Rb3 O11 49.7(5) 8_647 2_766
O15 Rb3 O11 44(3) 3_668 2_766
O2 Rb3 O11 139.6(4) 7_567 2_766
O12 Rb3 O11 112.2(4) . 2_766
O14 Rb3 O11 54.2(5) 8_647 2_766
O4 Rb3 O11 138.5(4) 8_647 3_567
O1 Rb3 O11 89.3(5) . 3_567
O3 Rb3 O11 90.1(4) 8_647 3_567
O6 Rb3 O11 48.1(4) 3_567 3_567
O9 Rb3 O11 111.1(4) 8_647 3_567
O15 Rb3 O11 45(3) 3_668 3_567
O2 Rb3 O11 131.1(4) 7_567 3_567
O12 Rb3 O11 47.9(5) . 3_567
O14 Rb3 O11 62.4(5) 8_647 3_567
O11 Rb3 O11 88.9(6) 2_766 3_567
O4 Rb3 O13 97.5(5) 8_647 .
O1 Rb3 O13 48.3(4) . .
O3 Rb3 O13 135.1(4) 8_647 .
O6 Rb3 O13 89.4(5) 3_567 .
O9 Rb3 O13 114.0(5) 8_647 .
O15 Rb3 O13 43(2) 3_668 .
O2 Rb3 O13 139.0(4) 7_567 .
O12 Rb3 O13 47.4(4) . .
O14 Rb3 O13 87.3(5) 8_647 .
O11 Rb3 O13 65.2(5) 2_766 .
O11 Rb3 O13 53.2(5) 3_567 .
O5 Rb4 O5 177.6(7) 2_665 .
O5 Rb4 O5 90.024(16) 2_665 4_656
O5 Rb4 O5 90.025(17) . 4_656
O5 Rb4 O5 90.025(18) 2_665 3_566
O5 Rb4 O5 90.024(15) . 3_566
O5 Rb4 O5 177.6(7) 4_656 3_566
O5 Rb4 O16 91.2(3) 2_665 5_453
O5 Rb4 O16 91.2(3) . 5_453
O5 Rb4 O16 88.8(3) 4_656 5_453
O5 Rb4 O16 88.8(3) 3_566 5_453
O5 Rb4 O16 88.8(3) 2_665 7_567
O5 Rb4 O16 88.8(3) . 7_567
O5 Rb4 O16 91.2(3) 4_656 7_567
O5 Rb4 O16 91.2(3) 3_566 7_567
O16 Rb4 O16 179.998(2) 5_453 7_567
O5 Rb4 O8 132.7(4) 2_665 7_566
O5 Rb4 O8 48.1(4) . 7_566
O5 Rb4 O8 45.4(4) 4_656 7_566
O5 Rb4 O8 133.8(4) 3_566 7_566
O16 Rb4 O8 75.8(3) 5_453 7_566
O16 Rb4 O8 104.2(3) 7_567 7_566
O5 Rb4 O8 48.1(4) 2_665 8_546
O5 Rb4 O8 132.7(4) . 8_546
O5 Rb4 O8 133.8(4) 4_656 8_546
O5 Rb4 O8 45.4(4) 3_566 8_546
O16 Rb4 O8 75.8(3) 5_453 8_546
O16 Rb4 O8 104.2(3) 7_567 8_546
O8 Rb4 O8 151.6(5) 7_566 8_546
O5 Rb4 O8 45.4(4) 2_665 5_454
O5 Rb4 O8 133.8(4) . 5_454
O5 Rb4 O8 48.1(4) 4_656 5_454
O5 Rb4 O8 132.7(4) 3_566 5_454
O16 Rb4 O8 104.2(3) 5_453 5_454
O16 Rb4 O8 75.8(3) 7_567 5_454
O8 Rb4 O8 93.44(13) 7_566 5_454
O8 Rb4 O8 93.44(13) 8_546 5_454
O5 Rb4 O8 133.8(4) 2_665 6_654
O5 Rb4 O8 45.4(4) . 6_654
O5 Rb4 O8 132.7(4) 4_656 6_654
O5 Rb4 O8 48.1(4) 3_566 6_654
O16 Rb4 O8 104.2(3) 5_453 6_654
O16 Rb4 O8 75.8(3) 7_567 6_654
O8 Rb4 O8 93.44(13) 7_566 6_654
O8 Rb4 O8 93.44(13) 8_546 6_654
O8 Rb4 O8 151.6(5) 5_454 6_654
O5 Rb4 O13 84.8(5) 2_665 5_454
O5 Rb4 O13 93.4(5) . 5_454
O5 Rb4 O13 49.2(5) 4_656 5_454
O5 Rb4 O13 133.1(5) 3_566 5_454
O16 Rb4 O13 137.7(3) 5_453 5_454
O16 Rb4 O13 42.3(3) 7_567 5_454
O8 Rb4 O13 76.4(4) 7_566 5_454
O8 Rb4 O13 126.7(4) 8_546 5_454
O8 Rb4 O13 46.9(4) 5_454 5_454
O8 Rb4 O13 108.7(4) 6_654 5_454
O5 Rb4 O13 93.4(5) 2_665 6_654
O5 Rb4 O13 84.8(5) . 6_654
O5 Rb4 O13 133.1(5) 4_656 6_654
O5 Rb4 O13 49.2(5) 3_566 6_654
O16 Rb4 O13 137.7(3) 5_453 6_654
O16 Rb4 O13 42.3(3) 7_567 6_654
O8 Rb4 O13 126.7(4) 7_566 6_654
O8 Rb4 O13 76.4(4) 8_546 6_654
O8 Rb4 O13 108.7(4) 5_454 6_654
O8 Rb4 O13 46.9(4) 6_654 6_654
O13 Rb4 O13 84.5(6) 5_454 6_654
O14 Rb5 O11 73.1(5) 5_545 2_766
O14 Rb5 O12 98.5(5) 5_545 8_647
O11 Rb5 O12 95.3(5) 2_766 8_647
O14 Rb5 O7 161.3(5) 5_545 .
O11 Rb5 O7 90.7(5) 2_766 .
O12 Rb5 O7 92.0(4) 8_647 .
O14 Rb5 O8 93.8(5) 5_545 3_667
O11 Rb5 O8 160.3(5) 2_766 3_667
O12 Rb5 O8 101.3(4) 8_647 3_667
O7 Rb5 O8 99.3(4) . 3_667
O14 Rb5 O13 74.9(5) 5_545 .
O11 Rb5 O13 75.6(5) 2_766 .
O12 Rb5 O13 169.9(5) 8_647 .
O7 Rb5 O13 92.4(4) . .
O8 Rb5 O13 87.0(5) 3_667 .
O14 Rb5 O6 89.3(4) 5_545 5_545
O11 Rb5 O6 139.9(5) 2_766 5_545
O12 Rb5 O6 51.1(5) 8_647 5_545
O7 Rb5 O6 109.3(4) . 5_545
O8 Rb5 O6 51.7(4) 3_667 5_545
O13 Rb5 O6 135.0(5) . 5_545
O14 Rb5 O2 138.7(5) 5_545 .
O11 Rb5 O2 135.1(4) 2_766 .
O12 Rb5 O2 105.9(4) 8_647 .
O7 Rb5 O2 50.3(4) . .
O8 Rb5 O2 49.5(4) 3_667 .
O13 Rb5 O2 83.9(4) . .
O6 Rb5 O2 81.1(4) 5_545 .
O14 Rb5 O3 51.2(4) 5_545 5_545
O11 Rb5 O3 94.8(5) 2_766 5_545
O12 Rb5 O3 50.2(4) 8_647 5_545
O7 Rb5 O3 142.1(4) . 5_545
O8 Rb5 O3 87.7(4) 3_667 5_545
O13 Rb5 O3 125.2(4) . 5_545
O6 Rb5 O3 48.3(4) 5_545 5_545
O2 Rb5 O3 129.1(4) . 5_545
O14 Rb5 O5 50.0(5) 5_545 5_545
O11 Rb5 O5 122.6(5) 2_766 5_545
O12 Rb5 O5 87.5(4) 8_647 5_545
O7 Rb5 O5 146.6(4) . 5_545
O8 Rb5 O5 48.4(4) 3_667 5_545
O13 Rb5 O5 93.8(5) . 5_545
O6 Rb5 O5 47.3(4) 5_545 5_545
O2 Rb5 O5 97.8(4) . 5_545
O3 Rb5 O5 46.5(4) 5_545 5_545
O14 Rb5 O1 136.0(5) 5_545 8_647
O11 Rb5 O1 83.2(4) 2_766 8_647
O12 Rb5 O1 46.7(4) 8_647 8_647
O7 Rb5 O1 47.3(4) . 8_647
O8 Rb5 O1 116.0(4) 3_667 8_647
O13 Rb5 O1 134.3(4) . 8_647
O6 Rb5 O1 85.7(4) 5_545 8_647
O2 Rb5 O1 83.4(4) . 8_647
O3 Rb5 O1 96.2(4) 5_545 8_647
O5 Rb5 O1 131.4(4) 5_545 8_647
O14 Rb5 O6 93.7(5) 5_545 2_766
O11 Rb5 O6 49.0(5) 2_766 2_766
O12 Rb5 O6 47.9(4) 8_647 2_766
O7 Rb5 O6 82.0(4) . 2_766
O8 Rb5 O6 149.1(4) 3_667 2_766
O13 Rb5 O6 123.9(5) . 2_766
O6 Rb5 O6 98.47(11) 5_545 2_766
O2 Rb5 O6 127.3(4) . 2_766
O3 Rb5 O6 73.9(4) 5_545 2_766
O5 Rb5 O6 120.4(4) 5_545 2_766
O1 Rb5 O6 44.4(4) 8_647 2_766
W1 O1 W3 143.9(8) . .
W1 O1 Rb3 112.8(6) . .
W3 O1 Rb3 101.5(5) . .
W1 O1 Rb5 100.4(6) . 7_567
W3 O1 Rb5 98.8(6) . 7_567
Rb3 O1 Rb5 75.2(4) . 7_567
W1 O1 Rb5 84.1(5) . .
W3 O1 Rb5 88.7(5) . .
Rb3 O1 Rb5 84.2(4) . .
Rb5 O1 Rb5 159.1(5) 7_567 .
W1 O2 W2 138.5(8) . 8_646
W1 O2 Rb3 102.4(6) . 8_647
W2 O2 Rb3 119.0(6) 8_646 8_647
W1 O2 Rb5 91.1(6) . .
W2 O2 Rb5 100.7(5) 8_646 .
Rb3 O2 Rb5 74.3(3) 8_647 .
W1 O2 Rb2 94.5(5) . .
W2 O2 Rb2 91.6(5) 8_646 .
Rb3 O2 Rb2 79.9(3) 8_647 .
Rb5 O2 Rb2 154.2(5) . .
W2 O3 W4 143.7(8) . .
W2 O3 Rb3 92.0(6) . 7_567
W4 O3 Rb3 123.7(6) . 7_567
W2 O3 Rb5 87.4(5) . 5_454
W4 O3 Rb5 88.2(5) . 5_454
Rb3 O3 Rb5 86.6(4) 7_567 5_454
W4 O4 W1 141.4(7) 8_646 .
W4 O4 Rb3 101.2(5) 8_646 7_567
W1 O4 Rb3 117.2(6) . 7_567
W4 O4 Rb5 83.2(5) 8_646 7_567
W1 O4 Rb5 95.8(5) . 7_567
Rb3 O4 Rb5 83.4(3) 7_567 7_567
W3 O5 W2 153.4(10) 7_566 .
W3 O5 Rb4 98.5(6) 7_566 .
W2 O5 Rb4 107.9(7) . .
W3 O5 Rb5 94.5(6) 7_566 5_454
W2 O5 Rb5 84.6(6) . 5_454
Rb4 O5 Rb5 85.9(4) . 5_454
W4 O6 W3 144.9(8) . 7_566
W4 O6 Rb3 96.1(6) . 4_657
W3 O6 Rb3 118.9(6) 7_566 4_657
W4 O6 Rb5 98.7(7) . 5_454
W3 O6 Rb5 92.8(6) 7_566 5_454
Rb3 O6 Rb5 76.2(4) 4_657 5_454
W4 O6 Rb5 87.0(6) . 2_764
W3 O6 Rb5 93.5(6) 7_566 2_764
Rb3 O6 Rb5 84.0(4) 4_657 2_764
Rb5 O6 Rb5 159.8(5) 5_454 2_764
W1 O7 W1 147.2(8) . 8_647
W1 O7 Rb5 101.6(6) . .
W1 O7 Rb5 111.0(6) 8_647 .
W1 O7 Rb3 93.0(6) . 8_647
W1 O7 Rb3 92.5(5) 8_647 8_647
Rb5 O7 Rb3 75.0(3) . 8_647
W3 O8 W2 136.0(9) . 6_655
W3 O8 Rb5 107.5(7) . 4_647
W2 O8 Rb5 116.5(6) 6_655 4_647
W3 O8 Rb4 88.7(6) . 5_545
W2 O8 Rb4 94.9(6) 6_655 5_545
Rb5 O8 Rb4 86.1(4) 4_647 5_545
W2 O9 W4 140.0(9) . 8_646
W2 O9 Rb3 88.9(6) . 7_567
W4 O9 Rb3 91.5(6) 8_646 7_567
W2 O9 Rb2 107.2(6) . .
W4 O9 Rb2 112.6(5) 8_646 .
Rb3 O9 Rb2 83.7(4) 7_567 .
W1 O10 W1 143.4(11) . 2_765
W1 O10 Rb2 108.3(6) . .
W1 O10 Rb2 108.3(6) 2_765 .
W1 O10 Rb3 96.47(8) . 7_567
W1 O10 Rb3 88.54(6) 2_765 7_567
Rb2 O10 Rb3 82.0(3) . 7_567
W1 O10 Rb3 88.54(6) . 8_647
W1 O10 Rb3 96.47(8) 2_765 8_647
Rb2 O10 Rb3 82.0(3) . 8_647
Rb3 O10 Rb3 164.0(6) 7_567 8_647
W4 O11 W5 121.5(12) . 4_657
W4 O11 Rb5 105.7(8) . 2_764
W5 O11 Rb5 132.8(9) 4_657 2_764
W4 O11 Rb1 157.5(10) . 1_564
W5 O11 Rb1 36.0(5) 4_657 1_564
Rb5 O11 Rb1 96.8(6) 2_764 1_564
W4 O11 Rb3 91.3(7) . 2_764
W5 O11 Rb3 91.8(7) 4_657 2_764
Rb5 O11 Rb3 87.1(5) 2_764 2_764
Rb1 O11 Rb3 90.8(4) 1_564 2_764
W4 O11 Rb3 89.5(7) . 4_657
W5 O11 Rb3 91.7(7) 4_657 4_657
Rb5 O11 Rb3 88.3(5) 2_764 4_657
Rb1 O11 Rb3 90.2(4) 1_564 4_657
Rb3 O11 Rb3 175.4(7) 2_764 4_657
W3 O12 W4 138.6(9) . 3_567
W3 O12 Rb5 116.5(7) . 7_567
W4 O12 Rb5 104.8(5) 3_567 7_567
W3 O12 Rb3 94.2(6) . .
W4 O12 Rb3 91.5(6) 3_567 .
Rb5 O12 Rb3 78.3(4) 7_567 .
W3 O13 W5 121.3(12) . .
W3 O13 Rb5 107.5(8) . .
W5 O13 Rb5 131.1(10) . .
W3 O13 Rb4 89.7(8) . 5_545
W5 O13 Rb4 98.0(7) . 5_545
Rb5 O13 Rb4 85.1(5) . 5_545
W3 O13 Rb3 90.8(7) . .
W5 O13 Rb3 91.7(8) . .
Rb5 O13 Rb3 83.7(5) . .
Rb4 O13 Rb3 168.4(7) 5_545 .
W2 O14 W5 123.1(11) . 6_654
W2 O14 Rb5 102.1(8) . 5_454
W5 O14 Rb5 134.7(9) 6_654 5_454
W2 O14 Rb1 159.4(9) . 5_454
W5 O14 Rb1 36.5(4) 6_654 5_454
Rb5 O14 Rb1 98.4(5) 5_454 5_454
W2 O14 Rb3 86.0(7) . 7_567
W5 O14 Rb3 94.7(8) 6_654 7_567
Rb5 O14 Rb3 90.1(5) 5_454 7_567
Rb1 O14 Rb3 92.5(5) 5_454 7_567
O15 W5 O15 78.2(11) 3_668 .
O15 W5 O16 78(5) 3_668 3_668
O15 W5 O16 82(5) . 3_668
O15 W5 O13 86(6) 3_668 .
O15 W5 O13 160.0(11) . .
O16 W5 O13 82.6(8) 3_668 .
O15 W5 O14 158.6(11) 3_668 6_655
O15 W5 O14 86(6) . 6_655
O16 W5 O14 85.5(8) 3_668 6_655
O13 W5 O14 105.8(11) . 6_655
O15 W5 O11 86(6) 3_668 3_567
O15 W5 O11 84(6) . 3_567
O16 W5 O11 160.7(11) 3_668 3_567
O13 W5 O11 108.1(9) . 3_567
O14 W5 O11 106.2(9) 6_655 3_567
O15 W5 Rb1 46.7(7) 3_668 .
O15 W5 Rb1 46.7(7) . .
O16 W5 Rb1 49.6(7) 3_668 .
O13 W5 Rb1 113.3(8) . .
O14 W5 Rb1 111.9(7) 6_655 .
O11 W5 Rb1 111.1(8) 3_567 .
O15 W5 Rb3 120(7) 3_668 4_648
O15 W5 Rb3 53.3(8) . 4_648
O16 W5 Rb3 120.3(4) 3_668 4_648
O13 W5 Rb3 146.7(8) . 4_648
O14 W5 Rb3 57.2(7) 6_655 4_648
O11 W5 Rb3 58.6(6) 3_567 4_648
Rb1 W5 Rb3 99.9(3) . 4_648
O15 W5 Rb3 52.5(8) 3_668 .
O15 W5 Rb3 117(7) . .
O16 W5 Rb3 117.3(4) 3_668 .
O13 W5 Rb3 60.6(6) . .
O14 W5 Rb3 148.9(7) 6_655 .
O11 W5 Rb3 58.9(6) 3_567 .
Rb1 W5 Rb3 99.2(3) . .
Rb3 W5 Rb3 117.5(2) 4_648 .
O15 W5 Rb4 116(8) 3_668 5_545
O15 W5 Rb4 121(7) . 5_545
O16 W5 Rb4 50.4(7) 3_668 5_545
O13 W5 Rb4 55.4(6) . 5_545
O14 W5 Rb4 61.3(7) 6_655 5_545
O11 W5 Rb4 148.8(7) 3_567 5_545
Rb1 W5 Rb4 100.1(3) . 5_545
Rb3 W5 Rb4 118.5(2) 4_648 5_545
Rb3 W5 Rb4 115.6(2) . 5_545
Rb1 O16 W5 75.5(7) . 3_668
Rb1 O16 W5 75.5(7) . 4_648
W5 O16 W5 151.0(14) 3_668 4_648
Rb1 O16 Rb4 180.0 . 5_546
W5 O16 Rb4 104.5(7) 3_668 5_546
W5 O16 Rb4 104.5(7) 4_648 5_546
Rb1 O15 W5 78.6(11) . 4_648
Rb1 O15 W5 78.5(9) . .
W5 O15 W5 157(3) 4_648 .
Rb1 O15 Rb3 177(10) . 4_648
W5 O15 Rb3 101.9(12) 4_648 4_648
W5 O15 Rb3 100.7(10) . 4_648
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
W1 O2 1.775(16) .
W1 O7 1.812(15) .
W1 O1 1.882(14) .
W1 O4 1.922(14) .
W1 O10 1.933(6) .
W1 O7 2.081(15) 7_567
W1 Rb3 4.066(4) 8_647
W1 Rb2 4.1168(9) .
W1 Rb3 4.188(4) .
W1 Rb5 4.266(3) 7_567
W1 Rb3 4.297(4) 7_567
W2 O14 1.783(18) .
W2 O3 1.816(16) .
W2 O9 1.850(13) .
W2 O5 1.948(16) .
W2 O8 2.031(16) 6_654
W2 O2 2.239(16) 7_566
W2 Rb3 3.734(4) 7_567
W2 Rb5 3.788(3) 5_454
W2 Rb4 4.1517(10) .
W2 Rb2 4.2720(10) .
W3 O13 1.75(2) .
W3 O8 1.853(15) .
W3 O5 1.894(17) 8_646
W3 O12 1.929(14) .
W3 O1 1.963(15) .
W3 O6 2.206(18) 8_646
W3 Rb4 3.8787(9) 5_545
W3 Rb3 3.971(4) .
W3 Rb5 4.023(3) .
W3 Rb5 4.051(3) 4_647
W3 Rb5 4.271(3) 7_567
W4 O11 1.78(2) .
W4 O6 1.836(18) .
W4 O4 1.912(15) 7_566
W4 O12 1.934(15) 4_657
W4 O9 2.052(14) 7_566
W4 O3 2.208(16) .
W4 Rb5 3.888(3) 2_764
W4 Rb3 3.897(4) 4_657
W4 Rb3 3.914(4) 2_764
W4 Rb5 4.003(3) 5_454
Rb1 O15 1.60(2) 3_668
Rb1 O15 1.60(2) 4_648
Rb1 O15 1.60(2) .
Rb1 O15 1.60(2) 2_755
Rb1 O16 1.70(2) .
Rb1 O16 1.70(2) 3_668
Rb1 W5 2.161(9) 3_668
Rb1 W5 2.161(9) 4_648
Rb1 W5 2.161(9) .
Rb1 W5 2.161(9) 2_755
Rb1 O14 3.375(18) 8_647
Rb1 O14 3.375(18) 7_557
Rb2 O10 3.08(2) .
Rb2 O10 3.08(2) 7_566
Rb2 O9 3.342(16) 7_566
Rb2 O9 3.342(16) 8_646
Rb2 O9 3.342(16) .
Rb2 O9 3.342(16) 2_765
Rb2 O2 3.577(14) 2_765
Rb2 O2 3.577(14) .
Rb2 O2 3.577(14) 7_566
Rb2 O2 3.577(14) 8_646
Rb2 W1 4.1168(9) 2_765
Rb3 O4 3.065(13) 8_647
Rb3 O1 3.082(15) .
Rb3 O3 3.201(15) 8_647
Rb3 O6 3.247(15) 3_567
Rb3 O9 3.281(18) 8_647
Rb3 O15 3.29(2) 3_668
Rb3 O2 3.295(15) 7_567
Rb3 O12 3.333(18) .
Rb3 O14 3.41(2) 8_647
Rb3 O11 3.449(19) 2_766
Rb3 O11 3.484(19) 3_567
Rb3 O13 3.54(2) .
Rb4 O5 3.116(17) 2_665
Rb4 O5 3.116(17) .
Rb4 O5 3.116(17) 4_656
Rb4 O5 3.116(17) 3_566
Rb4 O16 3.33(2) 5_453
Rb4 O16 3.33(2) 7_567
Rb4 O8 3.451(17) 7_566
Rb4 O8 3.451(17) 8_546
Rb4 O8 3.451(17) 5_454
Rb4 O8 3.451(17) 6_654
Rb4 O13 3.47(2) 5_454
Rb4 O13 3.47(2) 6_654
Rb5 O14 2.99(2) 5_545
Rb5 O11 3.01(2) 2_766
Rb5 O12 3.046(17) 8_647
Rb5 O7 3.052(15) .
Rb5 O8 3.088(16) 3_667
Rb5 O13 3.13(2) .
Rb5 O6 3.290(17) 5_545
Rb5 O2 3.382(16) .
Rb5 O3 3.408(15) 5_545
Rb5 O5 3.437(19) 5_545
Rb5 O1 3.505(16) 8_647
Rb5 O6 3.526(17) 2_766
O1 Rb5 3.505(16) 7_567
O2 W2 2.239(16) 8_646
O2 Rb3 3.295(15) 8_647
O3 Rb3 3.201(15) 7_567
O3 Rb5 3.408(15) 5_454
O4 W4 1.912(15) 8_646
O4 Rb3 3.065(13) 7_567
O4 Rb5 3.618(15) 7_567
O5 W3 1.894(17) 7_566
O5 Rb5 3.437(19) 5_454
O6 W3 2.206(18) 7_566
O6 Rb3 3.247(15) 4_657
O6 Rb5 3.290(17) 5_454
O6 Rb5 3.526(17) 2_764
O7 W1 2.080(15) 8_647
O7 Rb3 3.545(17) 8_647
O8 W2 2.030(16) 6_655
O8 Rb5 3.088(16) 4_647
O8 Rb4 3.451(17) 5_545
O9 W4 2.052(14) 8_646
O9 Rb3 3.281(18) 7_567
O10 W1 1.933(6) 2_765
O10 Rb3 3.626(5) 7_567
O10 Rb3 3.626(5) 8_647
O11 W5 2.00(2) 4_657
O11 Rb5 3.01(2) 2_764
O11 Rb1 3.430(19) 1_564
O11 Rb3 3.449(19) 2_764
O11 Rb3 3.484(19) 4_657
O12 W4 1.934(15) 3_567
O12 Rb5 3.046(16) 7_567
O13 W5 1.89(2) .
O13 Rb4 3.47(2) 5_545
O14 W5 1.91(2) 6_654
O14 Rb5 2.99(2) 5_454
O14 Rb1 3.375(18) 5_454
O14 Rb3 3.41(2) 7_567
W5 O15 1.80(3) 3_668
W5 O15 1.80(2) .
W5 O16 1.827(11) 3_668
W5 O14 1.91(2) 6_655
W5 O11 2.00(2) 3_567
W5 Rb3 4.038(11) 4_648
W5 Rb4 4.178(11) 5_545
O16 W5 1.827(11) 3_668
O16 W5 1.827(11) 4_648
O16 Rb4 3.33(2) 5_546
O15 W5 1.80(3) 4_648
O15 Rb3 3.29(2) 4_648
