#------------------------------------------------------------------------------
#$Date: 2016-11-08 21:32:10 +0200 (Tue, 08 Nov 2016) $
#$Revision: 188092 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/22/65/7226505.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7226505
loop_
_publ_author_name
'Hu, Yue-Qiao'
'Li, Mu-Qing'
'Li, Teng'
'Wang, Yan-Yan'
'Zheng, Zhiping'
'Zheng, Yan-Zhen'
_publ_section_title
;
 An alkali-ion insertion approach to structurally transform metal--organic
 frameworks
;
_journal_issue                   40
_journal_name_full               CrystEngComm
_journal_page_first              7680
_journal_paper_doi               10.1039/C6CE00540C
_journal_volume                  18
_journal_year                    2016
_chemical_formula_sum            'C51 H32 Cs0 Cu8 I8 N10 O31 Pr4'
_chemical_formula_weight         3368.03
_chemical_name_common            7
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           60
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2n 2ab'
_symmetry_space_group_name_H-M   'P b c n'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2015-08-20 deposited with the CCDC.
2016-09-08 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   42.221(5)
_cell_length_b                   30.379(4)
_cell_length_c                   27.178(3)
_cell_measurement_temperature    293(2)
_cell_volume                     34859(7)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.987
_diffrn_measured_fraction_theta_max 0.987
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0393
_diffrn_reflns_av_sigmaI/netI    0.0408
_diffrn_reflns_limit_h_max       49
_diffrn_reflns_limit_h_min       -49
_diffrn_reflns_limit_k_max       35
_diffrn_reflns_limit_k_min       -35
_diffrn_reflns_limit_l_max       31
_diffrn_reflns_limit_l_min       -31
_diffrn_reflns_number            198242
_diffrn_reflns_theta_full        24.78
_diffrn_reflns_theta_max         24.78
_diffrn_reflns_theta_min         0.83
_exptl_absorpt_coefficient_mu    3.504
_exptl_crystal_colour            YELLOW
_exptl_crystal_density_diffrn    1.283
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       BLOCK
_exptl_crystal_F_000             12384
_exptl_crystal_size_max          0.065
_exptl_crystal_size_mid          0.063
_exptl_crystal_size_min          0.035
_refine_diff_density_max         1.531
_refine_diff_density_min         -0.892
_refine_diff_density_rms         0.136
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.041
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     997
_refine_ls_number_reflns         29558
_refine_ls_number_restraints     28
_refine_ls_restrained_S_all      1.048
_refine_ls_R_factor_all          0.1046
_refine_ls_R_factor_gt           0.0639
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1118P)²+50.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1834
_refine_ls_wR_factor_ref         0.2025
_reflns_number_gt                17474
_reflns_number_total             29558
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c6ce00540c2.cif
_cod_data_source_block           7
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Orthorhombic' changed to
'orthorhombic' according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4268 2015-11-12 08:31:59Z antanas 

 Adding full bibliography for 7226499--7226505.cif.
;
_cod_original_sg_symbol_H-M      Pbcn
_cod_database_code               7226505
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y+1/2, z+1/2'
'x+1/2, -y+1/2, -z'
'-x, y, -z+1/2'
'-x, -y, -z'
'x-1/2, y-1/2, -z-1/2'
'-x-1/2, y-1/2, z'
'x, -y, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Pr1 Pr 0.422492(12) 0.310049(16) 0.47847(2) 0.05787(16) Uani 1 1 d .
Pr2 Pr 0.331262(12) 0.281912(16) 0.52319(2) 0.05894(16) Uani 1 1 d .
Pr3 Pr 0.325413(17) 0.15736(2) 0.42012(3) 0.0980(3) Uani 1 1 d .
Pr4 Pr 0.431616(15) 0.18114(2) 0.38552(3) 0.0825(2) Uani 1 1 d .
I1 I 0.163882(18) 0.36845(2) 0.27715(3) 0.0811(2) Uani 1 1 d .
I2 I 0.12467(2) 0.37852(3) 0.42761(3) 0.0995(3) Uani 1 1 d .
I3 I 0.11033(2) 0.25220(2) 0.34143(3) 0.0907(3) Uani 1 1 d .
I4 I 0.057192(18) 0.37123(2) 0.29662(3) 0.0860(2) Uani 1 1 d .
I5 I 0.358628(18) 0.29438(2) 0.17154(3) 0.0890(3) Uani 1 1 d .
I6 I 0.307658(16) 0.42494(3) 0.18138(3) 0.0857(2) Uani 1 1 d .
I7 I 0.126080(18) 0.10578(3) 0.55288(3) 0.0825(2) Uani 1 1 d .
I8 I 0.412660(15) 0.42225(2) 0.20285(3) 0.0730(2) Uani 1 1 d .
Cu1 Cu 0.14675(4) 0.32430(5) 0.35923(6) 0.0884(4) Uani 1 1 d .
Cu2 Cu 0.11394(4) 0.39462(4) 0.33104(6) 0.0881(4) Uani 1 1 d .
Cu3 Cu 0.08548(4) 0.32886(5) 0.37163(6) 0.0907(4) Uani 1 1 d .
Cu4 Cu 0.10995(3) 0.32262(4) 0.28124(5) 0.0768(4) Uani 1 1 d .
Cu5 Cu 0.35732(3) 0.37704(5) 0.20927(5) 0.0809(4) Uani 1 1 d .
Cu6 Cu 0.16448(3) 0.13932(5) 0.62050(6) 0.0928(5) Uani 1 1 d .
Cu7 Cu 0.36432(3) 0.56495(4) 0.64153(5) 0.0763(4) Uani 1 1 d .
Cu8 Cu 0.60426(3) 0.35883(4) 0.36316(5) 0.0750(4) Uani 1 1 d .
O1 O 0.2807(2) 0.2050(3) 0.4226(5) 0.157(5) Uani 1 1 d .
O2 O 0.2851(2) 0.2582(3) 0.4759(3) 0.110(3) Uani 1 1 d .
O3 O 0.3519(3) 0.1155(3) 0.3570(4) 0.140(4) Uani 1 1 d .
O4 O 0.4044(2) 0.1225(3) 0.3438(4) 0.128(4) Uani 1 1 d .
O5 O 0.46814(18) 0.2608(3) 0.4811(3) 0.088(2) Uani 1 1 d .
O6 O 0.4670(3) 0.1910(4) 0.4543(5) 0.168(6) Uani 1 1 d .
O7 O 0.38738(16) 0.26575(19) 0.5432(2) 0.0615(16) Uani 1 1 d .
O8 O 0.43537(14) 0.2852(2) 0.5661(3) 0.081(2) Uani 1 1 d .
O9 O 0.36674(15) 0.31614(18) 0.4565(2) 0.0574(15) Uani 1 1 d .
O10 O 0.3165(2) 0.3361(3) 0.4529(3) 0.107(3) Uani 1 1 d .
O11 O 0.31435(19) 0.2122(3) 0.5559(3) 0.095(2) Uani 1 1 d .
O12 O 0.3096(2) 0.1546(3) 0.5060(4) 0.121(3) Uani 1 1 d .
O13 O 0.35086(19) 0.3512(2) 0.5527(3) 0.087(2) Uani 1 1 d .
O14 O 0.40119(19) 0.3632(2) 0.5376(3) 0.084(2) Uani 1 1 d .
O15 O 0.44424(18) 0.3094(3) 0.3980(3) 0.086(2) Uani 1 1 d .
O16 O 0.46044(19) 0.2467(3) 0.3632(3) 0.110(3) Uani 1 1 d .
O17 O 0.40337(14) 0.23906(18) 0.4431(2) 0.0601(16) Uani 1 1 d .
O18 O 0.37939(18) 0.1777(3) 0.4224(4) 0.115(3) Uani 1 1 d .
O19 O 0.35199(16) 0.2267(2) 0.4625(3) 0.0668(18) Uani 1 1 d .
O20 O 0.32994(14) 0.2801(3) 0.6115(3) 0.105(3) Uani 1 1 d D
O23 O 0.28373(17) 0.3208(2) 0.5538(3) 0.091(2) Uani 1 1 d .
O26 O 0.2928(6) 0.0878(5) 0.4312(9) 0.349(16) Uani 1 1 d .
O24 O 0.3320(3) 0.2094(4) 0.3526(5) 0.169(5) Uani 1 1 d .
O27 O 0.3529(4) 0.0921(5) 0.4609(7) 0.214(7) Uani 1 1 d .
O29 O 0.4749(4) 0.1275(5) 0.3750(7) 0.232(7) Uani 1 1 d U
O21 O 0.41602(18) 0.3850(3) 0.4349(4) 0.118(3) Uani 1 1 d .
O22 O 0.46940(18) 0.3562(2) 0.4995(3) 0.091(2) Uani 1 1 d .
O28 O 0.4312(4) 0.1123(4) 0.4430(5) 0.219(7) Uani 1 1 d .
O25 O 0.2835(4) 0.1330(7) 0.3610(9) 0.311(14) Uani 1 1 d .
O30 O 0.4376(5) 0.1903(6) 0.2923(7) 0.262(8) Uani 1 1 d U
O31 O 0.3990(3) 0.2202(3) 0.3206(6) 0.181(6) Uani 1 1 d .
N1 N 0.1870(3) 0.2989(3) 0.3840(4) 0.091(3) Uani 1 1 d .
N2 N 0.3849(2) -0.0391(3) 0.3299(4) 0.090(3) Uani 1 1 d .
N3 N 0.5505(3) 0.1853(3) 0.5816(4) 0.103(3) Uani 1 1 d .
N4 N 0.3959(2) 0.2035(3) 0.7141(3) 0.077(3) Uani 1 1 d .
N5 N 0.3547(2) 0.3669(3) 0.2820(3) 0.079(3) Uani 1 1 d .
N6 N 0.2049(2) 0.1579(3) 0.5887(4) 0.100(3) Uani 1 1 d .
N7 N 0.36749(18) 0.5021(3) 0.6185(3) 0.073(2) Uani 1 1 d .
N8 N 0.56141(19) 0.3320(3) 0.3748(3) 0.066(2) Uani 1 1 d .
N9 N 0.3777(2) 0.2164(4) 0.4422(5) 0.109(4) Uani 1 1 d .
N12 N 0.33109(15) 0.2911(3) 0.6975(4) 0.121(4) Uani 1 1 d DU
C1 C 0.1994(3) 0.2638(5) 0.3663(5) 0.102(4) Uani 1 1 d .
H1A H 0.1889 0.2508 0.3399 0.122 Uiso 1 1 calc R
C2 C 0.2268(3) 0.2432(5) 0.3825(5) 0.114(5) Uani 1 1 d .
H2A H 0.2343 0.2176 0.3675 0.136 Uiso 1 1 calc R
C3 C 0.2421(3) 0.2616(4) 0.4206(5) 0.079(3) Uani 1 1 d .
C4 C 0.2298(4) 0.2962(5) 0.4377(7) 0.161(8) Uani 1 1 d .
H4A H 0.2408 0.3096 0.4633 0.193 Uiso 1 1 calc R
C5 C 0.2021(4) 0.3169(5) 0.4236(7) 0.132(6) Uani 1 1 d .
H5A H 0.1942 0.3414 0.4401 0.158 Uiso 1 1 calc R
C6 C 0.2711(4) 0.2409(4) 0.4407(5) 0.114(5) Uani 1 1 d .
C7 C 0.3571(4) -0.0184(4) 0.3365(8) 0.171(9) Uani 1 1 d .
H7A H 0.3387 -0.0351 0.3372 0.205 Uiso 1 1 calc R
C8 C 0.3546(4) 0.0271(4) 0.3422(7) 0.137(6) Uani 1 1 d .
H8A H 0.3351 0.0405 0.3472 0.164 Uiso 1 1 calc R
C9 C 0.3811(3) 0.0508(3) 0.3403(5) 0.088(4) Uani 1 1 d .
C10 C 0.4076(4) 0.0315(5) 0.3324(8) 0.168(9) Uani 1 1 d .
H10A H 0.4256 0.0486 0.3277 0.202 Uiso 1 1 calc R
C11 C 0.4104(4) -0.0141(4) 0.3305(8) 0.152(7) Uani 1 1 d .
H11A H 0.4303 -0.0270 0.3296 0.182 Uiso 1 1 calc R
C12 C 0.3797(4) 0.1002(5) 0.3480(6) 0.114(5) Uani 1 1 d .
C13 C 0.5337(3) 0.2229(5) 0.5883(5) 0.104(4) Uani 1 1 d .
H13A H 0.5385 0.2410 0.6149 0.125 Uiso 1 1 calc R
C14 C 0.5100(4) 0.2350(4) 0.5572(5) 0.103(4) Uani 1 1 d .
H14A H 0.4987 0.2607 0.5635 0.123 Uiso 1 1 calc R
C15 C 0.5021(3) 0.2097(4) 0.5162(5) 0.088(3) Uani 1 1 d .
C16 C 0.5200(4) 0.1712(6) 0.5108(7) 0.157(8) Uani 1 1 d .
H16A H 0.5151 0.1522 0.4850 0.188 Uiso 1 1 calc R
C17 C 0.5444(5) 0.1600(6) 0.5417(7) 0.162(8) Uani 1 1 d .
H17A H 0.5567 0.1353 0.5353 0.194 Uiso 1 1 calc R
C18 C 0.4775(3) 0.2220(5) 0.4798(5) 0.107(4) Uani 1 1 d .
C19 C 0.3800(3) 0.1925(3) 0.6751(5) 0.081(3) Uani 1 1 d .
H19A H 0.3651 0.1702 0.6786 0.098 Uiso 1 1 calc R
C20 C 0.3832(2) 0.2106(3) 0.6293(4) 0.068(3) Uani 1 1 d .
H20A H 0.3709 0.2004 0.6033 0.081 Uiso 1 1 calc R
C21 C 0.4046(2) 0.2439(3) 0.6221(4) 0.063(3) Uani 1 1 d .
C22 C 0.4202(3) 0.2573(5) 0.6641(6) 0.113(5) Uani 1 1 d .
H22A H 0.4334 0.2817 0.6625 0.135 Uiso 1 1 calc R
C23 C 0.4170(3) 0.2362(5) 0.7078(5) 0.109(5) Uani 1 1 d .
H23A H 0.4297 0.2446 0.7341 0.131 Uiso 1 1 calc R
C24 C 0.4098(2) 0.2675(3) 0.5742(3) 0.057(2) Uani 1 1 d .
C25 C 0.3713(2) 0.3351(4) 0.3056(5) 0.088(4) Uani 1 1 d .
H25A H 0.3853 0.3183 0.2869 0.105 Uiso 1 1 calc R
C26 C 0.3692(2) 0.3260(3) 0.3538(4) 0.075(3) Uani 1 1 d .
H26A H 0.3821 0.3041 0.3670 0.090 Uiso 1 1 calc R
C27 C 0.3492(2) 0.3476(3) 0.3835(4) 0.071(3) Uani 1 1 d .
C28 C 0.3304(3) 0.3811(4) 0.3613(5) 0.097(4) Uani 1 1 d .
H28A H 0.3156 0.3967 0.3797 0.116 Uiso 1 1 calc R
C29 C 0.3348(3) 0.3898(4) 0.3118(6) 0.114(5) Uani 1 1 d .
H29A H 0.3234 0.4129 0.2981 0.136 Uiso 1 1 calc R
C30 C 0.3425(3) 0.3348(3) 0.4340(4) 0.072(3) Uani 1 1 d .
C31 C 0.2211(3) 0.1929(4) 0.6043(6) 0.116(5) Uani 1 1 d .
H31A H 0.2117 0.2118 0.6269 0.139 Uiso 1 1 calc R
C32 C 0.2515(3) 0.2019(4) 0.5880(5) 0.101(4) Uani 1 1 d .
H32A H 0.2624 0.2264 0.5994 0.122 Uiso 1 1 calc R
C33 C 0.2647(3) 0.1742(4) 0.5555(5) 0.090(4) Uani 1 1 d .
C34 C 0.2491(3) 0.1396(4) 0.5387(5) 0.120(6) Uani 1 1 d .
H34A H 0.2587 0.1190 0.5183 0.145 Uiso 1 1 calc R
C35 C 0.2164(3) 0.1354(5) 0.5534(6) 0.125(5) Uani 1 1 d .
H35A H 0.2033 0.1158 0.5367 0.150 Uiso 1 1 calc R
C36 C 0.3007(3) 0.1812(5) 0.5366(6) 0.096(4) Uani 1 1 d .
C37 C 0.3431(3) 0.4734(4) 0.6215(4) 0.094(4) Uani 1 1 d .
H37A H 0.3241 0.4823 0.6356 0.113 Uiso 1 1 calc R
C38 C 0.3463(2) 0.4316(3) 0.6041(5) 0.085(4) Uani 1 1 d .
H38A H 0.3298 0.4118 0.6086 0.101 Uiso 1 1 calc R
C39 C 0.3733(3) 0.4179(3) 0.5801(4) 0.078(3) Uani 1 1 d .
C40 C 0.3974(3) 0.4477(4) 0.5771(5) 0.094(4) Uani 1 1 d .
H40A H 0.4159 0.4406 0.5605 0.112 Uiso 1 1 calc R
C41 C 0.3939(3) 0.4878(3) 0.5986(5) 0.097(4) Uani 1 1 d .
H41A H 0.4115 0.5063 0.5993 0.117 Uiso 1 1 calc R
C42 C 0.3762(3) 0.3731(3) 0.5547(4) 0.069(3) Uani 1 1 d .
C43 C 0.5370(2) 0.3600(3) 0.3873(4) 0.069(3) Uani 1 1 d .
H43A H 0.5412 0.3894 0.3940 0.083 Uiso 1 1 calc R
C44 C 0.5056(2) 0.3441(3) 0.3898(4) 0.070(3) Uani 1 1 d .
H44A H 0.4892 0.3630 0.3988 0.084 Uiso 1 1 calc R
C45 C 0.4990(3) 0.3004(3) 0.3788(4) 0.074(3) Uani 1 1 d .
C46 C 0.5247(3) 0.2736(3) 0.3673(5) 0.097(4) Uani 1 1 d .
H46A H 0.5216 0.2444 0.3582 0.116 Uiso 1 1 calc R
C47 C 0.5535(3) 0.2902(4) 0.3694(5) 0.104(4) Uani 1 1 d .
H47A H 0.5701 0.2702 0.3667 0.125 Uiso 1 1 calc R
C48 C 0.4651(3) 0.2845(5) 0.3804(4) 0.090(4) Uani 1 1 d .
C49 C 0.3364(3) 0.2970(5) 0.6463(4) 0.236(8) Uani 1 1 d D
H49A H 0.3486 0.3219 0.6403 0.284 Uiso 1 1 calc R
C50 C 0.3131(3) 0.2553(5) 0.7173(7) 0.236(8) Uani 1 1 d D
H50A H 0.3046 0.2380 0.6909 0.355 Uiso 1 1 calc R
H50B H 0.2960 0.2668 0.7369 0.355 Uiso 1 1 calc R
H50C H 0.3265 0.2373 0.7375 0.355 Uiso 1 1 calc R
C51 C 0.3451(3) 0.3237(5) 0.7317(6) 0.236(8) Uani 1 1 d D
H51A H 0.3571 0.3448 0.7133 0.355 Uiso 1 1 calc R
H51B H 0.3587 0.3089 0.7547 0.355 Uiso 1 1 calc R
H51C H 0.3284 0.3385 0.7492 0.355 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cs Cs -0.3680 2.1192 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pr Pr -0.2180 2.8214 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O15 Pr1 O9 98.5(2) . .
O15 Pr1 O5 73.5(3) . .
O9 Pr1 O5 144.8(2) . .
O15 Pr1 O14 138.8(3) . .
O9 Pr1 O14 75.9(2) . .
O5 Pr1 O14 132.4(3) . .
O15 Pr1 O22 84.7(3) . .
O9 Pr1 O22 141.4(2) . .
O5 Pr1 O22 73.2(3) . .
O14 Pr1 O22 76.7(3) . .
O15 Pr1 O17 76.3(2) . .
O9 Pr1 O17 70.02(19) . .
O5 Pr1 O17 74.8(2) . .
O14 Pr1 O17 134.7(2) . .
O22 Pr1 O17 146.2(2) . .
O15 Pr1 O8 140.7(3) . .
O9 Pr1 O8 117.2(2) . .
O5 Pr1 O8 67.9(2) . .
O14 Pr1 O8 70.3(3) . .
O22 Pr1 O8 77.5(2) . .
O17 Pr1 O8 99.9(2) . .
O15 Pr1 O21 68.0(3) . .
O9 Pr1 O21 73.6(2) . .
O5 Pr1 O21 129.6(3) . .
O14 Pr1 O21 71.3(3) . .
O22 Pr1 O21 72.1(2) . .
O17 Pr1 O21 123.5(3) . .
O8 Pr1 O21 135.3(3) . .
O15 Pr1 O7 145.0(2) . .
O9 Pr1 O7 70.3(2) . .
O5 Pr1 O7 96.4(2) . .
O14 Pr1 O7 72.3(2) . .
O22 Pr1 O7 125.1(2) . .
O17 Pr1 O7 68.75(19) . .
O8 Pr1 O7 49.80(19) . .
O21 Pr1 O7 133.6(2) . .
O15 Pr1 C24 151.5(3) . .
O9 Pr1 C24 94.2(3) . .
O5 Pr1 C24 81.3(3) . .
O14 Pr1 C24 69.2(3) . .
O22 Pr1 C24 100.9(3) . .
O17 Pr1 C24 84.4(2) . .
O8 Pr1 C24 24.4(2) . .
O21 Pr1 C24 140.4(3) . .
O7 Pr1 C24 25.4(2) . .
O15 Pr1 Pr2 129.13(18) . .
O9 Pr1 Pr2 35.56(14) . .
O5 Pr1 Pr2 126.97(19) . .
O14 Pr1 Pr2 66.48(18) . .
O22 Pr1 Pr2 142.19(19) . .
O17 Pr1 Pr2 68.44(13) . .
O8 Pr1 Pr2 82.13(13) . .
O21 Pr1 Pr2 102.64(18) . .
O7 Pr1 Pr2 35.12(15) . .
C24 Pr1 Pr2 58.7(2) . .
O13 Pr2 O11 138.7(3) . .
O13 Pr2 O20 72.2(3) . .
O11 Pr2 O20 66.6(3) . .
O13 Pr2 O2 135.2(3) . .
O11 Pr2 O2 72.4(3) . .
O20 Pr2 O2 120.0(3) . .
O13 Pr2 O23 75.4(3) . .
O11 Pr2 O23 93.2(3) . .
O20 Pr2 O23 69.9(2) . .
O2 Pr2 O23 70.8(3) . .
O13 Pr2 O7 76.8(2) . .
O11 Pr2 O7 91.6(2) . .
O20 Pr2 O7 78.41(19) . .
O2 Pr2 O7 145.0(2) . .
O23 Pr2 O7 142.8(2) . .
O13 Pr2 O19 133.3(2) . .
O11 Pr2 O19 76.0(3) . .
O20 Pr2 O19 130.5(2) . .
O2 Pr2 O19 74.6(3) . .
O23 Pr2 O19 145.4(2) . .
O7 Pr2 O19 71.2(2) . .
O13 Pr2 O9 71.3(2) . .
O11 Pr2 O9 142.2(3) . .
O20 Pr2 O9 136.7(2) . .
O2 Pr2 O9 102.3(3) . .
O23 Pr2 O9 121.1(2) . .
O7 Pr2 O9 71.20(19) . .
O19 Pr2 O9 66.67(19) . .
O13 Pr2 O10 76.8(3) . .
O11 Pr2 O10 139.4(3) . .
O20 Pr2 O10 138.0(3) . .
O2 Pr2 O10 67.0(3) . .
O23 Pr2 O10 75.5(3) . .
O7 Pr2 O10 121.0(2) . .
O19 Pr2 O10 91.4(3) . .
O9 Pr2 O10 50.6(2) . .
O13 Pr2 C30 75.0(3) . .
O11 Pr2 C30 146.3(3) . .
O20 Pr2 C30 147.0(3) . .
O2 Pr2 C30 81.7(3) . .
O23 Pr2 C30 98.4(3) . .
O7 Pr2 C30 97.7(3) . .
O19 Pr2 C30 76.6(3) . .
O9 Pr2 C30 26.6(3) . .
O10 Pr2 C30 24.2(3) . .
O13 Pr2 Pr1 66.10(18) . .
O11 Pr2 Pr1 124.6(2) . .
O20 Pr2 Pr1 108.70(15) . .
O2 Pr2 Pr1 130.6(2) . .
O23 Pr2 Pr1 139.23(19) . .
O7 Pr2 Pr1 38.18(13) . .
O19 Pr2 Pr1 67.66(14) . .
O9 Pr2 Pr1 33.41(13) . .
O10 Pr2 Pr1 82.87(19) . .
C30 Pr2 Pr1 59.6(3) . .
O18 Pr3 O1 127.3(3) . .
O18 Pr3 O3 73.1(3) . .
O1 Pr3 O3 135.2(4) . .
O18 Pr3 O12 104.4(3) . .
O1 Pr3 O12 77.1(4) . .
O3 Pr3 O12 142.4(4) . .
O18 Pr3 O24 74.9(4) . .
O1 Pr3 O24 73.6(4) . .
O3 Pr3 O24 75.7(4) . .
O12 Pr3 O24 141.0(3) . .
O18 Pr3 O25 140.9(6) . .
O1 Pr3 O25 68.7(4) . .
O3 Pr3 O25 73.4(5) . .
O12 Pr3 O25 114.4(7) . .
O24 Pr3 O25 77.8(7) . .
O18 Pr3 O26 137.5(7) . .
O1 Pr3 O26 94.2(7) . .
O3 Pr3 O26 84.1(4) . .
O12 Pr3 O26 73.0(5) . .
O24 Pr3 O26 133.7(7) . .
O25 Pr3 O26 56.4(8) . .
O18 Pr3 O27 75.7(4) . .
O1 Pr3 O27 145.3(5) . .
O3 Pr3 O27 71.8(5) . .
O12 Pr3 O27 71.4(4) . .
O24 Pr3 O27 141.1(4) . .
O25 Pr3 O27 111.8(7) . .
O26 Pr3 O27 63.2(8) . .
O18 Pr3 O19 51.1(2) . .
O1 Pr3 O19 80.8(3) . .
O3 Pr3 O19 122.2(3) . .
O12 Pr3 O19 74.1(2) . .
O24 Pr3 O19 76.3(3) . .
O25 Pr3 O19 144.5(5) . .
O26 Pr3 O19 147.1(5) . .
O27 Pr3 O19 103.6(4) . .
O18 Pr3 N9 25.9(3) . .
O1 Pr3 N9 102.8(3) . .
O3 Pr3 N9 96.9(4) . .
O12 Pr3 N9 91.8(3) . .
O24 Pr3 N9 70.6(3) . .
O25 Pr3 N9 148.4(7) . .
O26 Pr3 N9 154.2(8) . .
O27 Pr3 N9 92.5(4) . .
O19 Pr3 N9 25.6(3) . .
O4 Pr4 O16 137.2(3) . .
O4 Pr4 O6 138.9(4) . .
O16 Pr4 O6 77.3(4) . .
O4 Pr4 O18 74.2(3) . .
O16 Pr4 O18 126.8(3) . .
O6 Pr4 O18 104.4(4) . .
O4 Pr4 O29 79.1(5) . .
O16 Pr4 O29 98.1(5) . .
O6 Pr4 O29 73.3(5) . .
O18 Pr4 O29 134.0(5) . .
O4 Pr4 O31 76.0(3) . .
O16 Pr4 O31 73.3(3) . .
O6 Pr4 O31 145.0(4) . .
O18 Pr4 O31 79.2(4) . .
O29 Pr4 O31 129.2(6) . .
O4 Pr4 O30 70.2(5) . .
O16 Pr4 O30 67.1(4) . .
O6 Pr4 O30 133.8(6) . .
O18 Pr4 O30 120.2(5) . .
O29 Pr4 O30 83.3(7) . .
O31 Pr4 O30 46.7(6) . .
O4 Pr4 O28 71.7(4) . .
O16 Pr4 O28 144.6(4) . .
O6 Pr4 O28 68.9(5) . .
O18 Pr4 O28 73.3(5) . .
O29 Pr4 O28 62.9(6) . .
O31 Pr4 O28 142.0(4) . .
O30 Pr4 O28 132.8(6) . .
O4 Pr4 O17 123.9(3) . .
O16 Pr4 O17 80.0(2) . .
O6 Pr4 O17 74.8(3) . .
O18 Pr4 O17 51.1(2) . .
O29 Pr4 O17 147.6(4) . .
O31 Pr4 O17 81.7(4) . .
O30 Pr4 O17 124.0(5) . .
O28 Pr4 O17 100.2(4) . .
O4 Pr4 N9 98.4(3) . .
O16 Pr4 N9 102.8(3) . .
O6 Pr4 N9 91.6(4) . .
O18 Pr4 N9 25.5(2) . .
O29 Pr4 N9 150.8(5) . .
O31 Pr4 N9 76.9(4) . .
O30 Pr4 N9 123.6(6) . .
O28 Pr4 N9 88.5(5) . .
O17 Pr4 N9 25.8(2) . .
Cu4 I1 Cu2 57.50(4) . .
Cu4 I1 Cu1 58.58(5) . .
Cu2 I1 Cu1 59.13(5) . .
Cu1 I2 Cu3 58.34(5) . .
Cu1 I2 Cu2 59.46(5) . .
Cu3 I2 Cu2 56.88(5) . .
Cu3 I3 Cu4 59.60(5) . .
Cu3 I3 Cu1 57.84(5) . .
Cu4 I3 Cu1 58.11(4) . .
Cu2 I4 Cu3 57.53(5) . .
Cu2 I4 Cu4 57.33(4) . .
Cu3 I4 Cu4 59.36(5) . .
Cu6 I5 Cu8 58.16(4) 2_554 4_655
Cu6 I5 Cu5 58.91(5) 2_554 .
Cu8 I5 Cu5 57.90(4) 4_655 .
Cu7 I6 Cu5 57.83(4) 8_565 .
Cu7 I6 Cu6 57.45(4) 8_565 2_554
Cu5 I6 Cu6 57.29(5) . 2_554
Cu6 I7 Cu8 57.83(4) . 3_456
Cu6 I7 Cu7 58.30(5) . 7_655
Cu8 I7 Cu7 58.99(4) 3_456 7_655
Cu7 I8 Cu5 56.96(4) 8_565 .
Cu7 I8 Cu8 59.41(4) 8_565 4_655
Cu5 I8 Cu8 57.31(4) . 4_655
N1 Cu1 Cu3 145.6(3) . .
N1 Cu1 Cu4 140.6(3) . .
Cu3 Cu1 Cu4 61.30(6) . .
N1 Cu1 I2 107.7(3) . .
Cu3 Cu1 I2 61.87(5) . .
Cu4 Cu1 I2 111.67(6) . .
N1 Cu1 Cu2 148.9(3) . .
Cu3 Cu1 Cu2 58.57(5) . .
Cu4 Cu1 Cu2 58.35(5) . .
I2 Cu1 Cu2 61.30(5) . .
N1 Cu1 I1 104.1(3) . .
Cu3 Cu1 I1 110.20(6) . .
Cu4 Cu1 I1 60.14(5) . .
I2 Cu1 I1 111.36(6) . .
Cu2 Cu1 I1 60.18(5) . .
N1 Cu1 I3 103.4(3) . .
Cu3 Cu1 I3 60.38(5) . .
Cu4 Cu1 I3 60.44(5) . .
I2 Cu1 I3 115.21(6) . .
Cu2 Cu1 I3 107.53(6) . .
I1 Cu1 I3 113.85(6) . .
N2 Cu2 Cu4 147.3(3) 7_665 .
N2 Cu2 Cu3 142.4(3) 7_665 .
Cu4 Cu2 Cu3 62.42(5) . .
N2 Cu2 Cu1 142.6(3) 7_665 .
Cu4 Cu2 Cu1 60.23(5) . .
Cu3 Cu2 Cu1 59.82(6) . .
N2 Cu2 I4 106.5(3) 7_665 .
Cu4 Cu2 I4 62.06(5) . .
Cu3 Cu2 I4 61.67(5) . .
Cu1 Cu2 I4 110.79(6) . .
N2 Cu2 I1 105.5(3) 7_665 .
Cu4 Cu2 I1 60.93(5) . .
Cu3 Cu2 I1 111.69(6) . .
Cu1 Cu2 I1 60.69(5) . .
I4 Cu2 I1 115.77(6) . .
N2 Cu2 I2 101.0(3) 7_665 .
Cu4 Cu2 I2 111.50(6) . .
Cu3 Cu2 I2 61.54(5) . .
Cu1 Cu2 I2 59.23(5) . .
I4 Cu2 I2 116.23(6) . .
I1 Cu2 I2 110.08(6) . .
N3 Cu3 Cu2 141.7(3) 3_456 .
N3 Cu3 Cu1 143.5(4) 3_456 .
Cu2 Cu3 Cu1 61.61(6) . .
N3 Cu3 Cu4 148.9(4) 3_456 .
Cu2 Cu3 Cu4 58.77(5) . .
Cu1 Cu3 Cu4 59.64(5) . .
N3 Cu3 I3 107.3(3) 3_456 .
Cu2 Cu3 I3 111.05(7) . .
Cu1 Cu3 I3 61.78(5) . .
Cu4 Cu3 I3 60.39(5) . .
N3 Cu3 I4 104.9(4) 3_456 .
Cu2 Cu3 I4 60.80(5) . .
Cu1 Cu3 I4 111.54(6) . .
Cu4 Cu3 I4 60.59(5) . .
I3 Cu3 I4 110.92(6) . .
N3 Cu3 I2 102.4(4) 3_456 .
Cu2 Cu3 I2 61.58(5) . .
Cu1 Cu3 I2 59.79(5) . .
Cu4 Cu3 I2 108.66(6) . .
I3 Cu3 I2 114.62(6) . .
I4 Cu3 I2 115.51(6) . .
N4 Cu4 Cu2 145.2(3) 2_554 .
N4 Cu4 Cu1 144.5(3) 2_554 .
Cu2 Cu4 Cu1 61.42(6) . .
N4 Cu4 I1 105.9(3) 2_554 .
Cu2 Cu4 I1 61.57(5) . .
Cu1 Cu4 I1 61.29(5) . .
N4 Cu4 Cu3 144.8(3) 2_554 .
Cu2 Cu4 Cu3 58.82(5) . .
Cu1 Cu4 Cu3 59.06(6) . .
I1 Cu4 Cu3 109.32(6) . .
N4 Cu4 I3 103.8(3) 2_554 .
Cu2 Cu4 I3 110.78(6) . .
Cu1 Cu4 I3 61.45(5) . .
I1 Cu4 I3 115.74(6) . .
Cu3 Cu4 I3 60.01(5) . .
N4 Cu4 I4 104.8(3) 2_554 .
Cu2 Cu4 I4 60.62(5) . .
Cu1 Cu4 I4 110.58(6) . .
I1 Cu4 I4 115.08(5) . .
Cu3 Cu4 I4 60.05(5) . .
I3 Cu4 I4 110.16(5) . .
N5 Cu5 Cu7 145.1(3) . 8_565
N5 Cu5 Cu8 138.2(2) . 4_655
Cu7 Cu5 Cu8 62.15(5) 8_565 4_655
N5 Cu5 Cu6 149.0(3) . 2_554
Cu7 Cu5 Cu6 60.77(5) 8_565 2_554
Cu8 Cu5 Cu6 59.04(6) 4_655 2_554
N5 Cu5 I6 108.8(2) . .
Cu7 Cu5 I6 60.72(4) 8_565 .
Cu8 Cu5 I6 112.99(6) 4_655 .
Cu6 Cu5 I6 64.30(5) 2_554 .
N5 Cu5 I5 103.4(2) . .
Cu7 Cu5 I5 111.24(7) 8_565 .
Cu8 Cu5 I5 60.40(5) 4_655 .
Cu6 Cu5 I5 59.03(5) 2_554 .
I6 Cu5 I5 114.47(6) . .
N5 Cu5 I8 100.8(3) . .
Cu7 Cu5 I8 60.49(4) 8_565 .
Cu8 Cu5 I8 61.57(4) 4_655 .
Cu6 Cu5 I8 109.74(6) 2_554 .
I6 Cu5 I8 112.51(5) . .
I5 Cu5 I8 115.23(5) . .
N6 Cu6 Cu8 155.6(4) . 3_456
N6 Cu6 Cu7 137.2(3) . 7_655
Cu8 Cu6 Cu7 61.69(5) 3_456 7_655
N6 Cu6 Cu5 138.6(3) . 2
Cu8 Cu6 Cu5 60.10(5) 3_456 2
Cu7 Cu6 Cu5 58.41(5) 7_655 2
N6 Cu6 I5 109.2(3) . 2
Cu8 Cu6 I5 61.82(5) 3_456 2
Cu7 Cu6 I5 111.80(6) 7_655 2
Cu5 Cu6 I5 62.06(5) 2 2
N6 Cu6 I7 109.4(3) . .
Cu8 Cu6 I7 61.70(5) 3_456 .
Cu7 Cu6 I7 62.49(5) 7_655 .
Cu5 Cu6 I7 110.42(6) 2 .
I5 Cu6 I7 115.59(6) 2 .
N6 Cu6 I6 95.4(4) . 2
Cu8 Cu6 I6 108.99(6) 3_456 2
Cu7 Cu6 I6 57.97(5) 7_655 2
Cu5 Cu6 I6 58.41(5) 2 2
I5 Cu6 I6 112.05(6) 2 2
I7 Cu6 I6 113.32(6) . 2
N7 Cu7 Cu5 151.9(3) . 8_566
N7 Cu7 Cu6 141.1(3) . 7_665
Cu5 Cu7 Cu6 60.82(6) 8_566 7_665
N7 Cu7 I6 107.3(2) . 8_566
Cu5 Cu7 I6 61.45(4) 8_566 8_566
Cu6 Cu7 I6 64.57(5) 7_665 8_566
N7 Cu7 I8 106.4(3) . 8_566
Cu5 Cu7 I8 62.54(5) 8_566 8_566
Cu6 Cu7 I8 111.41(6) 7_665 8_566
I6 Cu7 I8 114.84(6) 8_566 8_566
N7 Cu7 Cu8 140.7(2) . 5_666
Cu5 Cu7 Cu8 59.74(5) 8_566 5_666
Cu6 Cu7 Cu8 58.30(5) 7_665 5_666
I6 Cu7 Cu8 111.60(5) 8_566 5_666
I8 Cu7 Cu8 61.49(4) 8_566 5_666
N7 Cu7 I7 98.4(3) . 7_665
Cu5 Cu7 I7 109.69(6) 8_566 7_665
Cu6 Cu7 I7 59.21(5) 7_665 7_665
I6 Cu7 I7 116.20(6) 8_566 7_665
I8 Cu7 I7 111.75(5) 8_566 7_665
Cu8 Cu7 I7 59.48(5) 5_666 7_665
N8 Cu8 Cu6 150.3(2) . 3_556
N8 Cu8 Cu5 139.8(2) . 4_655
Cu6 Cu8 Cu5 60.86(6) 3_556 4_655
N8 Cu8 Cu7 143.7(2) . 5_666
Cu6 Cu8 Cu7 60.01(5) 3_556 5_666
Cu5 Cu8 Cu7 58.11(5) 4_655 5_666
N8 Cu8 I5 106.6(2) . 4_655
Cu6 Cu8 I5 60.03(4) 3_556 4_655
Cu5 Cu8 I5 61.70(5) 4_655 4_655
Cu7 Cu8 I5 109.03(5) 5_666 4_655
N8 Cu8 I7 109.7(2) . 3_556
Cu6 Cu8 I7 60.47(5) 3_556 3_556
Cu5 Cu8 I7 110.04(6) 4_655 3_556
Cu7 Cu8 I7 61.52(5) 5_666 3_556
I5 Cu8 I7 113.01(5) 4_655 3_556
N8 Cu8 I8 98.9(2) . 4_655
Cu6 Cu8 I8 110.83(6) 3_556 4_655
Cu5 Cu8 I8 61.12(5) 4_655 4_655
Cu7 Cu8 I8 59.11(4) 5_666 4_655
I5 Cu8 I8 115.96(6) 4_655 4_655
I7 Cu8 I8 111.46(5) 3_556 4_655
C6 O1 Pr3 142.3(11) . .
C6 O2 Pr2 155.6(10) . .
C12 O3 Pr3 138.6(10) . .
C12 O4 Pr4 139.3(9) . .
C18 O5 Pr1 146.2(9) . .
C18 O6 Pr4 138.0(10) . .
C24 O7 Pr2 148.2(6) . .
C24 O7 Pr1 90.2(5) . .
Pr2 O7 Pr1 106.7(2) . .
C24 O8 Pr1 96.3(6) . .
C30 O9 Pr1 153.6(6) . .
C30 O9 Pr2 92.8(5) . .
Pr1 O9 Pr2 111.0(2) . .
C30 O10 Pr2 94.3(6) . .
C36 O11 Pr2 131.2(9) . .
C36 O12 Pr3 135.8(9) . .
C42 O13 Pr2 140.3(7) . .
C42 O14 Pr1 138.3(7) . .
C48 O15 Pr1 128.9(8) . .
C48 O16 Pr4 137.7(7) . .
N9 O17 Pr1 138.1(7) . .
N9 O17 Pr4 90.6(7) . .
Pr1 O17 Pr4 131.2(2) . .
N9 O18 Pr3 101.3(6) . .
N9 O18 Pr4 100.5(6) . .
Pr3 O18 Pr4 151.4(4) . .
N9 O19 Pr2 139.1(7) . .
N9 O19 Pr3 88.7(7) . .
Pr2 O19 Pr3 132.0(3) . .
C49 O20 Pr2 146.7(11) . .
C1 N1 C5 116.0(12) . .
C1 N1 Cu1 123.1(9) . .
C5 N1 Cu1 120.8(9) . .
C11 N2 C7 116.2(11) . .
C11 N2 Cu2 123.7(9) . 7_655
C7 N2 Cu2 119.3(9) . 7_655
C17 N3 C13 119.2(12) . .
C17 N3 Cu3 121.8(10) . 3_556
C13 N3 Cu3 118.9(9) . 3_556
C19 N4 C23 115.2(10) . .
C19 N4 Cu4 125.4(7) . 2
C23 N4 Cu4 119.4(8) . 2
C25 N5 C29 113.7(10) . .
C25 N5 Cu5 123.3(8) . .
C29 N5 Cu5 123.0(8) . .
C35 N6 C31 118.2(11) . .
C35 N6 Cu6 119.9(8) . .
C31 N6 Cu6 121.8(8) . .
C41 N7 C37 117.4(9) . .
C41 N7 Cu7 119.8(7) . .
C37 N7 Cu7 122.8(7) . .
C47 N8 C43 115.6(9) . .
C47 N8 Cu8 126.9(8) . .
C43 N8 Cu8 117.4(6) . .
O19 N9 O17 125.9(12) . .
O19 N9 O18 117.1(9) . .
O17 N9 O18 116.7(10) . .
O19 N9 Pr3 65.7(5) . .
O17 N9 Pr3 167.4(9) . .
O18 N9 Pr3 52.8(5) . .
O19 N9 Pr4 170.3(9) . .
O17 N9 Pr4 63.5(6) . .
O18 N9 Pr4 53.9(6) . .
Pr3 N9 Pr4 104.8(4) . .
C49 N12 C50 123.3(7) . .
C49 N12 C51 117.8(7) . .
C50 N12 C51 118.9(7) . .
N1 C1 C2 126.7(12) . .
N1 C1 H1A 116.7 . .
C2 C1 H1A 116.6 . .
C3 C2 C1 117.2(12) . .
C3 C2 H2A 121.4 . .
C1 C2 H2A 121.4 . .
C4 C3 C2 115.8(12) . .
C4 C3 C6 124.0(13) . .
C2 C3 C6 120.3(11) . .
C3 C4 C5 128.7(15) . .
C3 C4 H4A 115.6 . .
C5 C4 H4A 115.6 . .
N1 C5 C4 115.5(14) . .
N1 C5 H5A 122.2 . .
C4 C5 H5A 122.2 . .
O2 C6 O1 120.7(17) . .
O2 C6 C3 119.9(12) . .
O1 C6 C3 119.3(13) . .
N2 C7 C8 123.1(14) . .
N2 C7 H7A 118.4 . .
C8 C7 H7A 118.4 . .
C9 C8 C7 117.8(14) . .
C9 C8 H8A 121.1 . .
C7 C8 H8A 121.1 . .
C10 C9 C8 119.6(12) . .
C10 C9 C12 120.8(12) . .
C8 C9 C12 119.6(13) . .
C9 C10 C11 122.4(16) . .
C9 C10 H10A 118.8 . .
C11 C10 H10A 118.8 . .
N2 C11 C10 120.3(14) . .
N2 C11 H11A 119.8 . .
C10 C11 H11A 119.8 . .
O4 C12 O3 125.6(13) . .
O4 C12 C9 119.5(13) . .
O3 C12 C9 114.9(13) . .
N3 C13 C14 121.8(12) . .
N3 C13 H13A 119.1 . .
C14 C13 H13A 119.1 . .
C13 C14 C15 121.5(13) . .
C13 C14 H14A 119.2 . .
C15 C14 H14A 119.2 . .
C14 C15 C16 114.6(12) . .
C14 C15 C18 124.0(12) . .
C16 C15 C18 121.4(13) . .
C17 C16 C15 123.2(14) . .
C17 C16 H16A 118.4 . .
C15 C16 H16A 118.4 . .
N3 C17 C16 119.4(15) . .
N3 C17 H17A 120.3 . .
C16 C17 H17A 120.3 . .
O5 C18 O6 128.0(13) . .
O5 C18 C15 116.4(13) . .
O6 C18 C15 115.4(13) . .
N4 C19 C20 126.2(10) . .
N4 C19 H19A 116.9 . .
C20 C19 H19A 116.9 . .
C19 C20 C21 119.4(10) . .
C19 C20 H20A 120.3 . .
C21 C20 H20A 120.3 . .
C20 C21 C22 114.3(10) . .
C20 C21 C24 124.9(10) . .
C22 C21 C24 120.6(9) . .
C23 C22 C21 122.6(12) . .
C23 C22 H22A 118.7 . .
C21 C22 H22A 118.7 . .
N4 C23 C22 121.8(12) . .
N4 C23 H23A 119.1 . .
C22 C23 H23A 119.1 . .
O8 C24 O7 123.7(8) . .
O8 C24 C21 119.5(9) . .
O7 C24 C21 116.7(9) . .
O8 C24 Pr1 59.3(5) . .
O7 C24 Pr1 64.4(4) . .
C21 C24 Pr1 176.8(7) . .
C26 C25 N5 125.1(10) . .
C26 C25 H25A 117.4 . .
N5 C25 H25A 117.4 . .
C27 C26 C25 121.9(10) . .
C27 C26 H26A 119.0 . .
C25 C26 H26A 119.0 . .
C26 C27 C28 116.5(11) . .
C26 C27 C30 124.2(10) . .
C28 C27 C30 118.7(9) . .
C29 C28 C27 118.2(11) . .
C29 C28 H28A 120.9 . .
C27 C28 H28A 120.9 . .
N5 C29 C28 124.4(11) . .
N5 C29 H29A 117.8 . .
C28 C29 H29A 117.8 . .
O10 C30 O9 121.2(8) . .
O10 C30 C27 124.7(11) . .
O9 C30 C27 113.6(9) . .
O10 C30 Pr2 61.5(5) . .
O9 C30 Pr2 60.6(4) . .
C27 C30 Pr2 162.4(7) . .
N6 C31 C32 122.1(11) . .
N6 C31 H31A 119.0 . .
C32 C31 H31A 119.0 . .
C33 C32 C31 118.2(10) . .
C33 C32 H32A 120.9 . .
C31 C32 H32A 120.9 . .
C34 C33 C32 121.3(12) . .
C34 C33 C36 117.5(13) . .
C32 C33 C36 121.1(11) . .
C33 C34 C35 116.7(12) . .
C33 C34 H34A 121.6 . .
C35 C34 H34A 121.6 . .
N6 C35 C34 121.6(12) . .
N6 C35 H35A 119.2 . .
C34 C35 H35A 119.2 . .
O12 C36 O11 131.3(13) . .
O12 C36 C33 114.6(12) . .
O11 C36 C33 114.0(12) . .
N7 C37 C38 120.4(11) . .
N7 C37 H37A 119.8 . .
C38 C37 H37A 119.8 . .
C37 C38 C39 121.8(10) . .
C37 C38 H38A 119.1 . .
C39 C38 H38A 119.1 . .
C40 C39 C38 116.5(9) . .
C40 C39 C42 120.1(11) . .
C38 C39 C42 123.3(10) . .
C41 C40 C39 119.2(11) . .
C41 C40 H40A 120.4 . .
C39 C40 H40A 120.4 . .
N7 C41 C40 124.3(11) . .
N7 C41 H41A 117.9 . .
C40 C41 H41A 117.9 . .
O14 C42 O13 127.1(10) . .
O14 C42 C39 118.1(10) . .
O13 C42 C39 114.7(11) . .
N8 C43 C44 120.2(9) . .
N8 C43 H43A 119.9 . .
C44 C43 H43A 119.9 . .
C45 C44 C43 120.1(9) . .
C45 C44 H44A 119.9 . .
C43 C44 H44A 119.9 . .
C44 C45 C46 117.0(9) . .
C44 C45 C48 119.2(11) . .
C46 C45 C48 123.8(11) . .
C47 C46 C45 119.0(10) . .
C47 C46 H46A 120.5 . .
C45 C46 H46A 120.5 . .
C46 C47 N8 127.3(12) . .
C46 C47 H47A 116.3 . .
N8 C47 H47A 116.3 . .
O15 C48 O16 125.8(11) . .
O15 C48 C45 118.8(11) . .
O16 C48 C45 115.4(13) . .
O20 C49 N12 137.6(15) . .
O20 C49 H49A 111.2 . .
N12 C49 H49A 111.2 . .
N12 C50 H50A 109.5 . .
N12 C50 H50B 109.5 . .
H50A C50 H50B 109.5 . .
N12 C50 H50C 109.5 . .
H50A C50 H50C 109.5 . .
H50B C50 H50C 109.5 . .
N12 C51 H51A 109.5 . .
N12 C51 H51B 109.5 . .
H51A C51 H51B 109.5 . .
N12 C51 H51C 109.5 . .
H51A C51 H51C 109.5 . .
H51B C51 H51C 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Pr1 O15 2.371(8) .
Pr1 O9 2.436(6) .
Pr1 O5 2.440(7) .
Pr1 O14 2.450(7) .
Pr1 O22 2.493(7) .
Pr1 O17 2.495(6) .
Pr1 O8 2.557(8) .
Pr1 O21 2.580(9) .
Pr1 O7 2.664(6) .
Pr1 C24 2.955(8) .
Pr1 Pr2 4.1284(9) .
Pr2 O13 2.400(7) .
Pr2 O11 2.404(7) .
Pr2 O20 2.400(9) .
Pr2 O2 2.442(9) .
Pr2 O23 2.473(7) .
Pr2 O7 2.480(7) .
Pr2 O19 2.511(6) .
Pr2 O9 2.572(6) .
Pr2 O10 2.598(8) .
Pr2 C30 2.948(8) .
Pr3 O18 2.362(8) .
Pr3 O1 2.377(9) .
Pr3 O3 2.410(10) .
Pr3 O12 2.428(11) .
Pr3 O24 2.437(15) .
Pr3 O25 2.501(14) .
Pr3 O26 2.539(11) .
Pr3 O27 2.553(14) .
Pr3 O19 2.649(6) .
Pr3 N9 2.907(11) .
Pr4 O4 2.404(9) .
Pr4 O16 2.411(8) .
Pr4 O6 2.410(11) .
Pr4 O18 2.424(8) .
Pr4 O29 2.466(13) .
Pr4 O31 2.533(10) .
Pr4 O30 2.561(19) .
Pr4 O28 2.611(11) .
Pr4 O17 2.640(5) .
Pr4 N9 2.949(12) .
I1 Cu4 2.6712(15) .
I1 Cu2 2.6877(17) .
I1 Cu1 2.7015(18) .
I2 Cu1 2.6527(17) .
I2 Cu3 2.7071(18) .
I2 Cu2 2.7080(19) .
I3 Cu3 2.6831(17) .
I3 Cu4 2.6931(16) .
I3 Cu1 2.7195(17) .
I4 Cu2 2.6682(17) .
I4 Cu3 2.6905(18) .
I4 Cu4 2.7052(16) .
I5 Cu6 2.6331(16) 2_554
I5 Cu8 2.6791(15) 4_655
I5 Cu5 2.7128(17) .
I6 Cu7 2.6438(14) 8_565
I6 Cu5 2.6625(14) .
I6 Cu6 2.8163(19) 2_554
I7 Cu6 2.6542(16) .
I7 Cu8 2.6856(16) 3_456
I7 Cu7 2.7402(17) 7_655
I8 Cu7 2.6636(15) 8_565
I8 Cu5 2.7159(15) .
I8 Cu8 2.7276(16) 4_655
Cu1 N1 1.983(11) .
Cu1 Cu3 2.613(2) .
Cu1 Cu4 2.629(2) .
Cu1 Cu2 2.659(2) .
Cu2 N2 2.015(9) 7_665
Cu2 Cu4 2.5777(18) .
Cu2 Cu3 2.579(2) .
Cu3 N3 1.996(10) 3_456
Cu3 Cu4 2.672(2) .
Cu4 N4 2.005(9) 2_554
Cu5 N5 2.002(9) .
Cu5 Cu7 2.5657(18) 8_565
Cu5 Cu8 2.6101(19) 4_655
Cu5 Cu6 2.630(2) 2_554
Cu6 N6 1.995(10) .
Cu6 Cu8 2.5820(18) 3_456
Cu6 Cu7 2.6286(19) 7_655
Cu6 Cu5 2.630(2) 2
Cu6 I5 2.6331(17) 2
Cu6 I6 2.8163(19) 2
Cu7 N7 2.015(7) .
Cu7 Cu5 2.5657(18) 8_566
Cu7 Cu6 2.6286(19) 7_665
Cu7 I6 2.6438(14) 8_566
Cu7 I8 2.6636(15) 8_566
Cu7 Cu8 2.6719(18) 5_666
Cu7 I7 2.7402(17) 7_665
Cu8 N8 2.009(8) .
Cu8 Cu6 2.5820(18) 3_556
Cu8 Cu5 2.6101(19) 4_655
Cu8 Cu7 2.6719(18) 5_666
Cu8 I5 2.6791(15) 4_655
Cu8 I7 2.6856(16) 3_556
Cu8 I8 2.7276(16) 4_655
O1 C6 1.265(14) .
O2 C6 1.243(15) .
O3 C12 1.286(15) .
O4 C12 1.250(15) .
O5 C18 1.244(15) .
O6 C18 1.253(16) .
O7 C24 1.269(11) .
O8 C24 1.227(11) .
O9 C30 1.320(12) .
O10 C30 1.213(12) .
O11 C36 1.221(15) .
O12 C36 1.221(15) .
O13 C42 1.260(12) .
O14 C42 1.191(12) .
O15 C48 1.256(15) .
O16 C48 1.256(14) .
O17 N9 1.284(11) .
O18 N9 1.293(13) .
O19 N9 1.258(12) .
O20 C49 1.111(9) .
N1 C1 1.283(15) .
N1 C5 1.365(16) .
N2 C11 1.319(15) .
N2 C7 1.341(16) .
N2 Cu2 2.015(9) 7_655
N3 C17 1.354(18) .
N3 C13 1.357(15) .
N3 Cu3 1.996(10) 3_556
N4 C19 1.298(14) .
N4 C23 1.345(14) .
N4 Cu4 2.005(9) 2
N5 C25 1.354(12) .
N5 C29 1.361(15) .
N6 C35 1.274(16) .
N6 C31 1.332(13) .
N7 C41 1.314(12) .
N7 C37 1.350(13) .
N8 C47 1.321(14) .
N8 C43 1.379(12) .
N12 C49 1.421(9) .
N12 C50 1.431(9) .
N12 C51 1.481(9) .
C1 C2 1.387(17) .
C1 H1A 0.9300 .
C2 C3 1.343(15) .
C2 H2A 0.9300 .
C3 C4 1.261(18) .
C3 C6 1.481(19) .
C4 C5 1.383(19) .
C4 H4A 0.9300 .
C5 H5A 0.9300 .
C7 C8 1.395(17) .
C7 H7A 0.9300 .
C8 C9 1.331(17) .
C8 H8A 0.9300 .
C9 C10 1.279(18) .
C9 C12 1.517(17) .
C10 C11 1.390(19) .
C10 H10A 0.9300 .
C11 H11A 0.9300 .
C13 C14 1.360(17) .
C13 H13A 0.9300 .
C14 C15 1.394(16) .
C14 H14A 0.9300 .
C15 C16 1.400(17) .
C15 C18 1.483(17) .
C16 C17 1.37(2) .
C16 H16A 0.9300 .
C17 H17A 0.9300 .
C19 C20 1.366(14) .
C19 H19A 0.9300 .
C20 C21 1.374(12) .
C20 H20A 0.9300 .
C21 C22 1.379(16) .
C21 C24 1.500(13) .
C22 C23 1.355(17) .
C22 H22A 0.9300 .
C23 H23A 0.9300 .
C25 C26 1.343(15) .
C25 H25A 0.9300 .
C26 C27 1.339(13) .
C26 H26A 0.9300 .
C27 C28 1.425(13) .
C27 C30 1.453(14) .
C28 C29 1.384(17) .
C28 H28A 0.9300 .
C29 H29A 0.9300 .
C31 C32 1.383(16) .
C31 H31A 0.9300 .
C32 C33 1.341(16) .
C32 H32A 0.9300 .
C33 C34 1.322(15) .
C33 C36 1.622(17) .
C34 C35 1.444(17) .
C34 H34A 0.9300 .
C35 H35A 0.9300 .
C37 C38 1.361(14) .
C37 H37A 0.9300 .
C38 C39 1.378(15) .
C38 H38A 0.9300 .
C39 C40 1.364(14) .
C39 C42 1.534(14) .
C40 C41 1.359(14) .
C40 H40A 0.9300 .
C41 H41A 0.9300 .
C43 C44 1.415(13) .
C43 H43A 0.9300 .
C44 C45 1.389(13) .
C44 H44A 0.9300 .
C45 C46 1.393(16) .
C45 C48 1.514(15) .
C46 C47 1.317(17) .
C46 H46A 0.9300 .
C47 H47A 0.9300 .
C49 H49A 0.9300 .
C50 H50A 0.9600 .
C50 H50B 0.9600 .
C50 H50C 0.9600 .
C51 H51A 0.9600 .
C51 H51B 0.9600 .
C51 H51C 0.9600 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O15 Pr1 Pr2 O13 -128.1(4) . .
O9 Pr1 Pr2 O13 -92.1(3) . .
O5 Pr1 Pr2 O13 133.1(3) . .
O14 Pr1 Pr2 O13 6.7(3) . .
O22 Pr1 Pr2 O13 20.8(4) . .
O17 Pr1 Pr2 O13 -177.5(3) . .
O8 Pr1 Pr2 O13 78.5(3) . .
O21 Pr1 Pr2 O13 -56.2(3) . .
O7 Pr1 Pr2 O13 99.1(3) . .
C24 Pr1 Pr2 O13 85.8(3) . .
O15 Pr1 Pr2 O11 98.1(4) . .
O9 Pr1 Pr2 O11 134.1(3) . .
O5 Pr1 Pr2 O11 -0.7(3) . .
O14 Pr1 Pr2 O11 -127.1(3) . .
O22 Pr1 Pr2 O11 -113.0(4) . .
O17 Pr1 Pr2 O11 48.7(3) . .
O8 Pr1 Pr2 O11 -55.3(3) . .
O21 Pr1 Pr2 O11 170.0(3) . .
O7 Pr1 Pr2 O11 -34.7(3) . .
C24 Pr1 Pr2 O11 -48.0(3) . .
O15 Pr1 Pr2 O20 172.1(3) . .
O9 Pr1 Pr2 O20 -151.9(3) . .
O5 Pr1 Pr2 O20 73.3(3) . .
O14 Pr1 Pr2 O20 -53.1(3) . .
O22 Pr1 Pr2 O20 -39.0(4) . .
O17 Pr1 Pr2 O20 122.7(3) . .
O8 Pr1 Pr2 O20 18.7(3) . .
O21 Pr1 Pr2 O20 -116.0(3) . .
O7 Pr1 Pr2 O20 39.3(3) . .
C24 Pr1 Pr2 O20 26.0(3) . .
O15 Pr1 Pr2 O2 1.9(4) . .
O9 Pr1 Pr2 O2 37.9(4) . .
O5 Pr1 Pr2 O2 -97.0(4) . .
O14 Pr1 Pr2 O2 136.6(3) . .
O22 Pr1 Pr2 O2 150.8(4) . .
O17 Pr1 Pr2 O2 -47.6(3) . .
O8 Pr1 Pr2 O2 -151.5(3) . .
O21 Pr1 Pr2 O2 73.7(4) . .
O7 Pr1 Pr2 O2 -130.9(4) . .
C24 Pr1 Pr2 O2 -144.3(4) . .
O15 Pr1 Pr2 O23 -107.3(4) . .
O9 Pr1 Pr2 O23 -71.3(4) . .
O5 Pr1 Pr2 O23 153.9(4) . .
O14 Pr1 Pr2 O23 27.5(4) . .
O22 Pr1 Pr2 O23 41.6(4) . .
O17 Pr1 Pr2 O23 -156.7(3) . .
O8 Pr1 Pr2 O23 99.3(3) . .
O21 Pr1 Pr2 O23 -35.4(4) . .
O7 Pr1 Pr2 O23 119.9(4) . .
C24 Pr1 Pr2 O23 106.6(4) . .
O15 Pr1 Pr2 O7 132.8(4) . .
O9 Pr1 Pr2 O7 168.8(3) . .
O5 Pr1 Pr2 O7 34.0(3) . .
O14 Pr1 Pr2 O7 -92.4(3) . .
O22 Pr1 Pr2 O7 -78.3(4) . .
O17 Pr1 Pr2 O7 83.4(3) . .
O8 Pr1 Pr2 O7 -20.6(3) . .
O21 Pr1 Pr2 O7 -155.4(3) . .
C24 Pr1 Pr2 O7 -13.3(3) . .
O15 Pr1 Pr2 O19 45.1(3) . .
O9 Pr1 Pr2 O19 81.1(3) . .
O5 Pr1 Pr2 O19 -53.7(3) . .
O14 Pr1 Pr2 O19 179.8(3) . .
O22 Pr1 Pr2 O19 -166.0(3) . .
O17 Pr1 Pr2 O19 -4.4(2) . .
O8 Pr1 Pr2 O19 -108.3(2) . .
O21 Pr1 Pr2 O19 116.9(3) . .
O7 Pr1 Pr2 O19 -87.7(3) . .
C24 Pr1 Pr2 O19 -101.1(3) . .
O15 Pr1 Pr2 O9 -36.0(4) . .
O5 Pr1 Pr2 O9 -134.9(3) . .
O14 Pr1 Pr2 O9 98.7(3) . .
O22 Pr1 Pr2 O9 112.9(4) . .
O17 Pr1 Pr2 O9 -85.5(3) . .
O8 Pr1 Pr2 O9 170.6(3) . .
O21 Pr1 Pr2 O9 35.8(3) . .
O7 Pr1 Pr2 O9 -168.8(3) . .
C24 Pr1 Pr2 O9 177.8(3) . .
O15 Pr1 Pr2 O10 -49.4(3) . .
O9 Pr1 Pr2 O10 -13.4(3) . .
O5 Pr1 Pr2 O10 -148.2(3) . .
O14 Pr1 Pr2 O10 85.4(3) . .
O22 Pr1 Pr2 O10 99.5(4) . .
O17 Pr1 Pr2 O10 -98.8(3) . .
O8 Pr1 Pr2 O10 157.2(3) . .
O21 Pr1 Pr2 O10 22.4(3) . .
O7 Pr1 Pr2 O10 177.8(3) . .
C24 Pr1 Pr2 O10 164.5(3) . .
O15 Pr1 Pr2 C30 -42.0(4) . .
O9 Pr1 Pr2 C30 -6.0(3) . .
O5 Pr1 Pr2 C30 -140.9(3) . .
O14 Pr1 Pr2 C30 92.7(3) . .
O22 Pr1 Pr2 C30 106.9(4) . .
O17 Pr1 Pr2 C30 -91.5(3) . .
O8 Pr1 Pr2 C30 164.6(3) . .
O21 Pr1 Pr2 C30 29.8(3) . .
O7 Pr1 Pr2 C30 -174.8(3) . .
C24 Pr1 Pr2 C30 171.8(3) . .
Cu3 I2 Cu1 N1 -144.2(3) . .
Cu2 I2 Cu1 N1 148.2(3) . .
Cu2 I2 Cu1 Cu3 -67.58(6) . .
Cu3 I2 Cu1 Cu4 37.03(6) . .
Cu2 I2 Cu1 Cu4 -30.55(6) . .
Cu3 I2 Cu1 Cu2 67.58(6) . .
Cu3 I2 Cu1 I1 102.20(7) . .
Cu2 I2 Cu1 I1 34.62(5) . .
Cu3 I2 Cu1 I3 -29.42(6) . .
Cu2 I2 Cu1 I3 -96.99(7) . .
Cu4 I1 Cu1 N1 140.7(3) . .
Cu2 I1 Cu1 N1 -150.9(3) . .
Cu4 I1 Cu1 Cu3 -36.74(6) . .
Cu2 I1 Cu1 Cu3 31.64(6) . .
Cu2 I1 Cu1 Cu4 68.39(5) . .
Cu4 I1 Cu1 I2 -103.45(7) . .
Cu2 I1 Cu1 I2 -35.06(5) . .
Cu4 I1 Cu1 Cu2 -68.39(5) . .
Cu4 I1 Cu1 I3 28.86(5) . .
Cu2 I1 Cu1 I3 97.25(7) . .
Cu3 I3 Cu1 N1 147.2(3) . .
Cu4 I3 Cu1 N1 -141.0(3) . .
Cu4 I3 Cu1 Cu3 71.78(6) . .
Cu3 I3 Cu1 Cu4 -71.78(6) . .
Cu3 I3 Cu1 I2 29.89(6) . .
Cu4 I3 Cu1 I2 101.67(7) . .
Cu3 I3 Cu1 Cu2 -36.04(7) . .
Cu4 I3 Cu1 Cu2 35.74(6) . .
Cu3 I3 Cu1 I1 -100.54(7) . .
Cu4 I3 Cu1 I1 -28.76(5) . .
N1 Cu1 Cu2 N2 -10.7(8) . 7_665
Cu3 Cu1 Cu2 N2 138.5(5) . 7_665
Cu4 Cu1 Cu2 N2 -148.0(5) . 7_665
I2 Cu1 Cu2 N2 65.7(5) . 7_665
I1 Cu1 Cu2 N2 -76.7(5) . 7_665
I3 Cu1 Cu2 N2 175.4(5) . 7_665
N1 Cu1 Cu2 Cu4 137.3(6) . .
Cu3 Cu1 Cu2 Cu4 -73.47(6) . .
I2 Cu1 Cu2 Cu4 -146.30(7) . .
I1 Cu1 Cu2 Cu4 71.28(5) . .
I3 Cu1 Cu2 Cu4 -36.64(6) . .
N1 Cu1 Cu2 Cu3 -149.2(6) . .
Cu4 Cu1 Cu2 Cu3 73.47(6) . .
I2 Cu1 Cu2 Cu3 -72.82(6) . .
I1 Cu1 Cu2 Cu3 144.76(7) . .
I3 Cu1 Cu2 Cu3 36.83(6) . .
N1 Cu1 Cu2 I4 174.7(6) . .
Cu3 Cu1 Cu2 I4 -36.09(6) . .
Cu4 Cu1 Cu2 I4 37.39(6) . .
I2 Cu1 Cu2 I4 -108.91(7) . .
I1 Cu1 Cu2 I4 108.67(7) . .
I3 Cu1 Cu2 I4 0.74(9) . .
N1 Cu1 Cu2 I1 66.0(6) . .
Cu3 Cu1 Cu2 I1 -144.76(7) . .
Cu4 Cu1 Cu2 I1 -71.28(5) . .
I2 Cu1 Cu2 I1 142.42(6) . .
I3 Cu1 Cu2 I1 -107.93(6) . .
N1 Cu1 Cu2 I2 -76.4(6) . .
Cu3 Cu1 Cu2 I2 72.82(6) . .
Cu4 Cu1 Cu2 I2 146.30(7) . .
I1 Cu1 Cu2 I2 -142.42(6) . .
I3 Cu1 Cu2 I2 109.66(7) . .
Cu3 I4 Cu2 N2 -141.2(3) . 7_665
Cu4 I4 Cu2 N2 146.8(3) . 7_665
Cu3 I4 Cu2 Cu4 71.97(6) . .
Cu4 I4 Cu2 Cu3 -71.97(6) . .
Cu3 I4 Cu2 Cu1 35.34(7) . .
Cu4 I4 Cu2 Cu1 -36.63(6) . .
Cu3 I4 Cu2 I1 101.88(7) . .
Cu4 I4 Cu2 I1 29.91(5) . .
Cu3 I4 Cu2 I2 -29.64(6) . .
Cu4 I4 Cu2 I2 -101.61(7) . .
Cu4 I1 Cu2 N2 -147.7(3) . 7_665
Cu1 I1 Cu2 N2 142.2(3) . 7_665
Cu1 I1 Cu2 Cu4 -70.16(6) . .
Cu4 I1 Cu2 Cu3 37.70(7) . .
Cu1 I1 Cu2 Cu3 -32.47(7) . .
Cu4 I1 Cu2 Cu1 70.16(6) . .
Cu4 I1 Cu2 I4 -30.27(6) . .
Cu1 I1 Cu2 I4 -100.43(7) . .
Cu4 I1 Cu2 I2 104.08(6) . .
Cu1 I1 Cu2 I2 33.92(5) . .
Cu1 I2 Cu2 N2 -145.7(3) . 7_665
Cu3 I2 Cu2 N2 144.4(3) . 7_665
Cu1 I2 Cu2 Cu4 31.18(6) . .
Cu3 I2 Cu2 Cu4 -38.77(6) . .
Cu1 I2 Cu2 Cu3 69.95(6) . .
Cu3 I2 Cu2 Cu1 -69.95(6) . .
Cu1 I2 Cu2 I4 99.62(7) . .
Cu3 I2 Cu2 I4 29.68(6) . .
Cu1 I2 Cu2 I1 -34.49(5) . .
Cu3 I2 Cu2 I1 -104.44(6) . .
N2 Cu2 Cu3 N3 3.5(8) 7_665 3_456
Cu4 Cu2 Cu3 N3 -148.0(6) . 3_456
Cu1 Cu2 Cu3 N3 142.1(6) . 3_456
I4 Cu2 Cu3 N3 -76.6(6) . 3_456
I1 Cu2 Cu3 N3 174.9(6) . 3_456
I2 Cu2 Cu3 N3 73.1(6) . 3_456
N2 Cu2 Cu3 Cu1 -138.7(5) 7_665 .
Cu4 Cu2 Cu3 Cu1 69.87(6) . .
I4 Cu2 Cu3 Cu1 141.27(7) . .
I1 Cu2 Cu3 Cu1 32.79(7) . .
I2 Cu2 Cu3 Cu1 -69.03(5) . .
N2 Cu2 Cu3 Cu4 151.4(5) 7_665 .
Cu1 Cu2 Cu3 Cu4 -69.87(6) . .
I4 Cu2 Cu3 Cu4 71.40(5) . .
I1 Cu2 Cu3 Cu4 -37.09(6) . .
I2 Cu2 Cu3 Cu4 -138.90(7) . .
N2 Cu2 Cu3 I3 -177.1(5) 7_665 .
Cu4 Cu2 Cu3 I3 31.49(7) . .
Cu1 Cu2 Cu3 I3 -38.38(6) . .
I4 Cu2 Cu3 I3 102.89(7) . .
I1 Cu2 Cu3 I3 -5.59(10) . .
I2 Cu2 Cu3 I3 -107.41(7) . .
N2 Cu2 Cu3 I4 80.0(5) 7_665 .
Cu4 Cu2 Cu3 I4 -71.40(5) . .
Cu1 Cu2 Cu3 I4 -141.27(7) . .
I1 Cu2 Cu3 I4 -108.48(7) . .
I2 Cu2 Cu3 I4 149.70(6) . .
N2 Cu2 Cu3 I2 -69.7(5) 7_665 .
Cu4 Cu2 Cu3 I2 138.90(7) . .
Cu1 Cu2 Cu3 I2 69.03(5) . .
I4 Cu2 Cu3 I2 -149.70(6) . .
I1 Cu2 Cu3 I2 101.82(7) . .
N1 Cu1 Cu3 N3 11.9(8) . 3_456
Cu4 Cu1 Cu3 N3 151.3(5) . 3_456
I2 Cu1 Cu3 N3 -68.4(5) . 3_456
Cu2 Cu1 Cu3 N3 -140.2(5) . 3_456
I1 Cu1 Cu3 N3 -172.5(5) . 3_456
I3 Cu1 Cu3 N3 80.9(5) . 3_456
N1 Cu1 Cu3 Cu2 152.1(5) . .
Cu4 Cu1 Cu3 Cu2 -68.50(6) . .
I2 Cu1 Cu3 Cu2 71.86(6) . .
I1 Cu1 Cu3 Cu2 -32.24(6) . .
I3 Cu1 Cu3 Cu2 -138.89(7) . .
N1 Cu1 Cu3 Cu4 -139.4(5) . .
I2 Cu1 Cu3 Cu4 140.35(6) . .
Cu2 Cu1 Cu3 Cu4 68.50(6) . .
I1 Cu1 Cu3 Cu4 36.26(6) . .
I3 Cu1 Cu3 Cu4 -70.39(5) . .
N1 Cu1 Cu3 I3 -69.0(5) . .
Cu4 Cu1 Cu3 I3 70.39(5) . .
I2 Cu1 Cu3 I3 -149.26(6) . .
Cu2 Cu1 Cu3 I3 138.89(7) . .
I1 Cu1 Cu3 I3 106.65(6) . .
N1 Cu1 Cu3 I4 -171.9(5) . .
Cu4 Cu1 Cu3 I4 -32.54(6) . .
I2 Cu1 Cu3 I4 107.81(7) . .
Cu2 Cu1 Cu3 I4 35.95(6) . .
I1 Cu1 Cu3 I4 3.72(9) . .
I3 Cu1 Cu3 I4 -102.93(7) . .
N1 Cu1 Cu3 I2 80.3(5) . .
Cu4 Cu1 Cu3 I2 -140.35(6) . .
Cu2 Cu1 Cu3 I2 -71.86(6) . .
I1 Cu1 Cu3 I2 -104.09(6) . .
I3 Cu1 Cu3 I2 149.26(6) . .
Cu4 I3 Cu3 N3 148.7(4) . 3_456
Cu1 I3 Cu3 N3 -142.0(4) . 3_456
Cu4 I3 Cu3 Cu2 -30.92(6) . .
Cu1 I3 Cu3 Cu2 38.31(7) . .
Cu4 I3 Cu3 Cu1 -69.23(6) . .
Cu1 I3 Cu3 Cu4 69.23(6) . .
Cu4 I3 Cu3 I4 34.72(5) . .
Cu1 I3 Cu3 I4 103.94(7) . .
Cu4 I3 Cu3 I2 -98.30(7) . .
Cu1 I3 Cu3 I2 -29.07(6) . .
Cu2 I4 Cu3 N3 141.4(3) . 3_456
Cu4 I4 Cu3 N3 -150.1(3) . 3_456
Cu4 I4 Cu3 Cu2 68.48(5) . .
Cu2 I4 Cu3 Cu1 -36.28(6) . .
Cu4 I4 Cu3 Cu1 32.20(6) . .
Cu2 I4 Cu3 Cu4 -68.48(5) . .
Cu2 I4 Cu3 I3 -103.12(7) . .
Cu4 I4 Cu3 I3 -34.64(5) . .
Cu2 I4 Cu3 I2 29.45(6) . .
Cu4 I4 Cu3 I2 97.93(7) . .
Cu1 I2 Cu3 N3 145.5(3) . 3_456
Cu2 I2 Cu3 N3 -142.6(3) . 3_456
Cu1 I2 Cu3 Cu2 -71.92(6) . .
Cu2 I2 Cu3 Cu1 71.92(6) . .
Cu1 I2 Cu3 Cu4 -35.53(6) . .
Cu2 I2 Cu3 Cu4 36.39(6) . .
Cu1 I2 Cu3 I3 29.70(6) . .
Cu2 I2 Cu3 I3 101.62(7) . .
Cu1 I2 Cu3 I4 -101.12(7) . .
Cu2 I2 Cu3 I4 -29.21(6) . .
N2 Cu2 Cu4 N4 -3.9(7) 7_665 2_554
Cu3 Cu2 Cu4 N4 143.5(4) . 2_554
Cu1 Cu2 Cu4 N4 -147.3(4) . 2_554
I4 Cu2 Cu4 N4 72.7(4) . 2_554
I1 Cu2 Cu4 N4 -76.4(4) . 2_554
I2 Cu2 Cu4 N4 -178.1(4) . 2_554
N2 Cu2 Cu4 Cu1 143.4(5) 7_665 .
Cu3 Cu2 Cu4 Cu1 -69.22(7) . .
I4 Cu2 Cu4 Cu1 -140.02(7) . .
I1 Cu2 Cu4 Cu1 70.90(5) . .
I2 Cu2 Cu4 Cu1 -30.83(6) . .
N2 Cu2 Cu4 I1 72.5(5) 7_665 .
Cu3 Cu2 Cu4 I1 -140.13(7) . .
Cu1 Cu2 Cu4 I1 -70.90(5) . .
I4 Cu2 Cu4 I1 149.08(6) . .
I2 Cu2 Cu4 I1 -101.73(7) . .
N2 Cu2 Cu4 Cu3 -147.4(5) 7_665 .
Cu1 Cu2 Cu4 Cu3 69.22(7) . .
I4 Cu2 Cu4 Cu3 -70.79(5) . .
I1 Cu2 Cu4 Cu3 140.13(7) . .
I2 Cu2 Cu4 Cu3 38.40(6) . .
N2 Cu2 Cu4 I3 -178.7(5) 7_665 .
Cu3 Cu2 Cu4 I3 -31.30(6) . .
Cu1 Cu2 Cu4 I3 37.93(6) . .
I4 Cu2 Cu4 I3 -102.09(6) . .
I1 Cu2 Cu4 I3 108.83(6) . .
I2 Cu2 Cu4 I3 7.10(9) . .
N2 Cu2 Cu4 I4 -76.6(5) 7_665 .
Cu3 Cu2 Cu4 I4 70.79(5) . .
Cu1 Cu2 Cu4 I4 140.02(7) . .
I1 Cu2 Cu4 I4 -149.08(6) . .
I2 Cu2 Cu4 I4 109.19(7) . .
N1 Cu1 Cu4 N4 1.4(7) . 2_554
Cu3 Cu1 Cu4 N4 -143.2(5) . 2_554
I2 Cu1 Cu4 N4 179.5(5) . 2_554
Cu2 Cu1 Cu4 N4 147.9(5) . 2_554
I1 Cu1 Cu4 N4 76.6(5) . 2_554
I3 Cu1 Cu4 N4 -72.9(5) . 2_554
N1 Cu1 Cu4 Cu2 -146.5(5) . .
Cu3 Cu1 Cu4 Cu2 68.85(6) . .
I2 Cu1 Cu4 Cu2 31.58(6) . .
I1 Cu1 Cu4 Cu2 -71.36(5) . .
I3 Cu1 Cu4 Cu2 139.14(7) . .
N1 Cu1 Cu4 I1 -75.2(5) . .
Cu3 Cu1 Cu4 I1 140.20(6) . .
I2 Cu1 Cu4 I1 102.94(7) . .
Cu2 Cu1 Cu4 I1 71.36(5) . .
I3 Cu1 Cu4 I1 -149.51(6) . .
N1 Cu1 Cu4 Cu3 144.6(5) . .
I2 Cu1 Cu4 Cu3 -37.26(6) . .
Cu2 Cu1 Cu4 Cu3 -68.85(6) . .
I1 Cu1 Cu4 Cu3 -140.20(6) . .
I3 Cu1 Cu4 Cu3 70.29(5) . .
N1 Cu1 Cu4 I3 74.3(5) . .
Cu3 Cu1 Cu4 I3 -70.29(5) . .
I2 Cu1 Cu4 I3 -107.56(7) . .
Cu2 Cu1 Cu4 I3 -139.14(7) . .
I1 Cu1 Cu4 I3 149.51(6) . .
N1 Cu1 Cu4 I4 176.7(5) . .
Cu3 Cu1 Cu4 I4 32.11(6) . .
I2 Cu1 Cu4 I4 -5.15(9) . .
Cu2 Cu1 Cu4 I4 -36.73(6) . .
I1 Cu1 Cu4 I4 -108.09(6) . .
I3 Cu1 Cu4 I4 102.41(6) . .
Cu2 I1 Cu4 N4 144.8(3) . 2_554
Cu1 I1 Cu4 N4 -144.1(3) . 2_554
Cu1 I1 Cu4 Cu2 71.11(6) . .
Cu2 I1 Cu4 Cu1 -71.11(6) . .
Cu2 I1 Cu4 Cu3 -35.54(6) . .
Cu1 I1 Cu4 Cu3 35.57(6) . .
Cu2 I1 Cu4 I3 -100.77(7) . .
Cu1 I1 Cu4 I3 -29.66(5) . .
Cu2 I1 Cu4 I4 29.62(6) . .
Cu1 I1 Cu4 I4 100.73(7) . .
N3 Cu3 Cu4 N4 -3.5(8) 3_456 2_554
Cu2 Cu3 Cu4 N4 -143.9(5) . 2_554
Cu1 Cu3 Cu4 N4 142.9(5) . 2_554
I3 Cu3 Cu4 N4 70.2(5) . 2_554
I4 Cu3 Cu4 N4 -72.2(5) . 2_554
I2 Cu3 Cu4 N4 178.5(5) . 2_554
N3 Cu3 Cu4 Cu2 140.5(7) 3_456 .
Cu1 Cu3 Cu4 Cu2 -73.19(6) . .
I3 Cu3 Cu4 Cu2 -145.89(7) . .
I4 Cu3 Cu4 Cu2 71.75(5) . .
I2 Cu3 Cu4 Cu2 -37.60(6) . .
N3 Cu3 Cu4 Cu1 -146.4(6) 3_456 .
Cu2 Cu3 Cu4 Cu1 73.19(6) . .
I3 Cu3 Cu4 Cu1 -72.70(5) . .
I4 Cu3 Cu4 Cu1 144.94(6) . .
I2 Cu3 Cu4 Cu1 35.59(6) . .
N3 Cu3 Cu4 I1 177.1(6) 3_456 .
Cu2 Cu3 Cu4 I1 36.69(6) . .
Cu1 Cu3 Cu4 I1 -36.50(6) . .
I3 Cu3 Cu4 I1 -109.20(6) . .
I4 Cu3 Cu4 I1 108.44(6) . .
I2 Cu3 Cu4 I1 -0.91(8) . .
N3 Cu3 Cu4 I3 -73.7(6) 3_456 .
Cu2 Cu3 Cu4 I3 145.89(7) . .
Cu1 Cu3 Cu4 I3 72.70(5) . .
I4 Cu3 Cu4 I3 -142.36(5) . .
I2 Cu3 Cu4 I3 108.29(7) . .
N3 Cu3 Cu4 I4 68.7(6) 3_456 .
Cu2 Cu3 Cu4 I4 -71.75(5) . .
Cu1 Cu3 Cu4 I4 -144.94(6) . .
I3 Cu3 Cu4 I4 142.36(5) . .
I2 Cu3 Cu4 I4 -109.35(6) . .
Cu3 I3 Cu4 N4 -146.1(3) . 2_554
Cu1 I3 Cu4 N4 145.1(3) . 2_554
Cu3 I3 Cu4 Cu2 30.87(6) . .
Cu1 I3 Cu4 Cu2 -37.91(6) . .
Cu3 I3 Cu4 Cu1 68.78(6) . .
Cu3 I3 Cu4 I1 98.39(7) . .
Cu1 I3 Cu4 I1 29.61(6) . .
Cu1 I3 Cu4 Cu3 -68.78(6) . .
Cu3 I3 Cu4 I4 -34.31(5) . .
Cu1 I3 Cu4 I4 -103.09(6) . .
Cu2 I4 Cu4 N4 -145.7(3) . 2_554
Cu3 I4 Cu4 N4 145.4(3) . 2_554
Cu3 I4 Cu4 Cu2 -68.82(6) . .
Cu2 I4 Cu4 Cu1 37.07(6) . .
Cu3 I4 Cu4 Cu1 -31.75(6) . .
Cu2 I4 Cu4 I1 -29.92(6) . .
Cu3 I4 Cu4 I1 -98.74(7) . .
Cu2 I4 Cu4 Cu3 68.82(6) . .
Cu2 I4 Cu4 I3 103.11(7) . .
Cu3 I4 Cu4 I3 34.30(5) . .
Cu7 I6 Cu5 N5 143.3(3) 8_565 .
Cu6 I6 Cu5 N5 -147.3(3) 2_554 .
Cu6 I6 Cu5 Cu7 69.43(6) 2_554 8_565
Cu7 I6 Cu5 Cu8 -34.95(6) 8_565 4_655
Cu6 I6 Cu5 Cu8 34.48(6) 2_554 4_655
Cu7 I6 Cu5 Cu6 -69.43(6) 8_565 2_554
Cu7 I6 Cu5 I5 -101.60(7) 8_565 .
Cu6 I6 Cu5 I5 -32.17(5) 2_554 .
Cu7 I6 Cu5 I8 32.48(6) 8_565 .
Cu6 I6 Cu5 I8 101.90(7) 2_554 .
Cu6 I5 Cu5 N5 152.2(3) 2_554 .
Cu8 I5 Cu5 N5 -138.2(3) 4_655 .
Cu6 I5 Cu5 Cu7 -32.42(6) 2_554 8_565
Cu8 I5 Cu5 Cu7 37.15(6) 4_655 8_565
Cu6 I5 Cu5 Cu8 -69.57(6) 2_554 4_655
Cu8 I5 Cu5 Cu6 69.57(5) 4_655 2_554
Cu6 I5 Cu5 I6 34.02(5) 2_554 .
Cu8 I5 Cu5 I6 103.59(7) 4_655 .
Cu6 I5 Cu5 I8 -98.78(7) 2_554 .
Cu8 I5 Cu5 I8 -29.21(5) 4_655 .
Cu7 I8 Cu5 N5 -148.3(2) 8_565 .
Cu8 I8 Cu5 N5 139.4(2) 4_655 .
Cu8 I8 Cu5 Cu7 -72.30(6) 4_655 8_565
Cu7 I8 Cu5 Cu8 72.30(6) 8_565 4_655
Cu7 I8 Cu5 Cu6 36.95(6) 8_565 2_554
Cu8 I8 Cu5 Cu6 -35.35(6) 4_655 2_554
Cu7 I8 Cu5 I6 -32.56(6) 8_565 .
Cu8 I8 Cu5 I6 -104.86(7) 4_655 .
Cu7 I8 Cu5 I5 101.15(7) 8_565 .
Cu8 I8 Cu5 I5 28.85(5) 4_655 .
Cu8 I7 Cu6 N6 -155.1(4) 3_456 .
Cu7 I7 Cu6 N6 133.9(4) 7_655 .
Cu7 I7 Cu6 Cu8 -70.92(5) 7_655 3_456
Cu8 I7 Cu6 Cu7 70.92(5) 3_456 7_655
Cu8 I7 Cu6 Cu5 36.42(6) 3_456 2
Cu7 I7 Cu6 Cu5 -34.50(6) 7_655 2
Cu8 I7 Cu6 I5 -31.48(6) 3_456 2
Cu7 I7 Cu6 I5 -102.41(7) 7_655 2
Cu8 I7 Cu6 I6 99.80(7) 3_456 2
Cu7 I7 Cu6 I6 28.88(5) 7_655 2
O18 Pr3 O1 C6 -34(2) . .
O3 Pr3 O1 C6 -138.1(17) . .
O12 Pr3 O1 C6 64.6(19) . .
O24 Pr3 O1 C6 -89.4(19) . .
O25 Pr3 O1 C6 -172(2) . .
O26 Pr3 O1 C6 136(2) . .
O27 Pr3 O1 C6 90(2) . .
O19 Pr3 O1 C6 -11.1(18) . .
N9 Pr3 O1 C6 -24(2) . .
O13 Pr2 O2 C6 120(2) . .
O11 Pr2 O2 C6 -97(2) . .
O20 Pr2 O2 C6 -145(2) . .
O23 Pr2 O2 C6 163(2) . .
O7 Pr2 O2 C6 -30(3) . .
O19 Pr2 O2 C6 -17(2) . .
O9 Pr2 O2 C6 45(2) . .
O10 Pr2 O2 C6 82(2) . .
C30 Pr2 O2 C6 61(2) . .
Pr1 Pr2 O2 C6 24(3) . .
O18 Pr3 O3 C12 27.3(15) . .
O1 Pr3 O3 C12 153.6(15) . .
O12 Pr3 O3 C12 -64.5(17) . .
O24 Pr3 O3 C12 105.5(16) . .
O25 Pr3 O3 C12 -173.2(18) . .
O26 Pr3 O3 C12 -116.5(17) . .
O27 Pr3 O3 C12 -52.8(16) . .
O19 Pr3 O3 C12 42.1(17) . .
N9 Pr3 O3 C12 37.6(16) . .
O16 Pr4 O4 C12 -139.6(16) . .
O6 Pr4 O4 C12 82.0(18) . .
O18 Pr4 O4 C12 -11.9(16) . .
O29 Pr4 O4 C12 130.2(18) . .
O31 Pr4 O4 C12 -94.5(17) . .
O30 Pr4 O4 C12 -143.1(18) . .
O28 Pr4 O4 C12 65.3(17) . .
O17 Pr4 O4 C12 -24.8(18) . .
N9 Pr4 O4 C12 -20.3(17) . .
O15 Pr1 O5 C18 -98.6(16) . .
O9 Pr1 O5 C18 -17.3(17) . .
O14 Pr1 O5 C18 119.0(15) . .
O22 Pr1 O5 C18 172.0(16) . .
O17 Pr1 O5 C18 -18.7(15) . .
O8 Pr1 O5 C18 88.9(16) . .
O21 Pr1 O5 C18 -139.8(15) . .
O7 Pr1 O5 C18 47.2(16) . .
C24 Pr1 O5 C18 67.8(16) . .
Pr2 Pr1 O5 C18 28.3(16) . .
O4 Pr4 O6 C18 -167.2(16) . .
O16 Pr4 O6 C18 40.3(18) . .
O18 Pr4 O6 C18 -84.9(19) . .
O29 Pr4 O6 C18 143(2) . .
O31 Pr4 O6 C18 7(2) . .
O30 Pr4 O6 C18 80.1(19) . .
O28 Pr4 O6 C18 -150(2) . .
O17 Pr4 O6 C18 -42.7(18) . .
N9 Pr4 O6 C18 -62.5(18) . .
O13 Pr2 O7 C24 51.3(11) . .
O11 Pr2 O7 C24 -88.6(11) . .
O20 Pr2 O7 C24 -22.9(11) . .
O2 Pr2 O7 C24 -149.6(11) . .
O23 Pr2 O7 C24 8.8(12) . .
O19 Pr2 O7 C24 -163.2(11) . .
O9 Pr2 O7 C24 125.8(11) . .
O10 Pr2 O7 C24 116.8(11) . .
C30 Pr2 O7 C24 123.9(11) . .
Pr1 Pr2 O7 C24 119.4(11) . .
O13 Pr2 O7 Pr1 -68.0(3) . .
O11 Pr2 O7 Pr1 152.1(3) . .
O20 Pr2 O7 Pr1 -142.2(3) . .
O2 Pr2 O7 Pr1 91.1(5) . .
O23 Pr2 O7 Pr1 -110.5(4) . .
O19 Pr2 O7 Pr1 77.4(2) . .
O9 Pr2 O7 Pr1 6.48(19) . .
O10 Pr2 O7 Pr1 -2.6(4) . .
C30 Pr2 O7 Pr1 4.5(3) . .
O15 Pr1 O7 C24 124.2(6) . .
O9 Pr1 O7 C24 -159.5(5) . .
O5 Pr1 O7 C24 54.0(5) . .
O14 Pr1 O7 C24 -78.6(5) . .
O22 Pr1 O7 C24 -19.8(6) . .
O17 Pr1 O7 C24 125.0(5) . .
O8 Pr1 O7 C24 0.2(5) . .
O21 Pr1 O7 C24 -118.5(6) . .
Pr2 Pr1 O7 C24 -152.6(6) . .
O15 Pr1 O7 Pr2 -83.2(5) . .
O9 Pr1 O7 Pr2 -6.9(2) . .
O5 Pr1 O7 Pr2 -153.3(3) . .
O14 Pr1 O7 Pr2 74.1(3) . .
O22 Pr1 O7 Pr2 132.8(3) . .
O17 Pr1 O7 Pr2 -82.4(2) . .
O8 Pr1 O7 Pr2 152.9(4) . .
O21 Pr1 O7 Pr2 34.2(4) . .
C24 Pr1 O7 Pr2 152.6(6) . .
O15 Pr1 O8 C24 -131.6(6) . .
O9 Pr1 O8 C24 21.3(6) . .
O5 Pr1 O8 C24 -120.2(6) . .
O14 Pr1 O8 C24 82.9(6) . .
O22 Pr1 O8 C24 163.1(6) . .
O17 Pr1 O8 C24 -51.2(6) . .
O21 Pr1 O8 C24 115.2(6) . .
O7 Pr1 O8 C24 -0.2(5) . .
Pr2 Pr1 O8 C24 15.2(6) . .
O15 Pr1 O9 C30 -54.4(14) . .
O5 Pr1 O9 C30 -127.8(13) . .
O14 Pr1 O9 C30 83.9(14) . .
O22 Pr1 O9 C30 37.8(15) . .
O17 Pr1 O9 C30 -126.4(14) . .
O8 Pr1 O9 C30 142.5(13) . .
O21 Pr1 O9 C30 9.6(13) . .
O7 Pr1 O9 C30 159.8(14) . .
C24 Pr1 O9 C30 151.2(14) . .
Pr2 Pr1 O9 C30 153.0(15) . .
O15 Pr1 O9 Pr2 152.6(3) . .
O5 Pr1 O9 Pr2 79.1(4) . .
O14 Pr1 O9 Pr2 -69.1(3) . .
O22 Pr1 O9 Pr2 -115.2(3) . .
O17 Pr1 O9 Pr2 80.6(2) . .
O8 Pr1 O9 Pr2 -10.5(3) . .
O21 Pr1 O9 Pr2 -143.5(3) . .
O7 Pr1 O9 Pr2 6.80(19) . .
C24 Pr1 O9 Pr2 -1.9(3) . .
O13 Pr2 O9 C30 -93.7(6) . .
O11 Pr2 O9 C30 117.3(6) . .
O20 Pr2 O9 C30 -127.7(6) . .
O2 Pr2 O9 C30 40.2(6) . .
O23 Pr2 O9 C30 -34.6(6) . .
O7 Pr2 O9 C30 -175.6(6) . .
O19 Pr2 O9 C30 107.3(6) . .
O10 Pr2 O9 C30 -5.6(6) . .
Pr1 Pr2 O9 C30 -168.3(6) . .
O13 Pr2 O9 Pr1 74.7(3) . .
O11 Pr2 O9 Pr1 -74.4(4) . .
O20 Pr2 O9 Pr1 40.6(4) . .
O2 Pr2 O9 Pr1 -151.5(3) . .
O23 Pr2 O9 Pr1 133.8(3) . .
O7 Pr2 O9 Pr1 -7.3(2) . .
O19 Pr2 O9 Pr1 -84.4(3) . .
O10 Pr2 O9 Pr1 162.7(4) . .
C30 Pr2 O9 Pr1 168.3(6) . .
O13 Pr2 O10 C30 82.7(8) . .
O11 Pr2 O10 C30 -121.6(8) . .
O20 Pr2 O10 C30 125.8(7) . .
O2 Pr2 O10 C30 -124.3(8) . .
O23 Pr2 O10 C30 160.8(8) . .
O7 Pr2 O10 C30 17.2(8) . .
O19 Pr2 O10 C30 -51.6(7) . .
O9 Pr2 O10 C30 6.1(6) . .
Pr1 Pr2 O10 C30 15.6(7) . .
O13 Pr2 O11 C36 168.7(10) . .
O20 Pr2 O11 C36 163.7(12) . .
O2 Pr2 O11 C36 28.6(11) . .
O23 Pr2 O11 C36 97.2(12) . .
O7 Pr2 O11 C36 -119.7(11) . .
O19 Pr2 O11 C36 -49.5(11) . .
O9 Pr2 O11 C36 -58.9(13) . .
O10 Pr2 O11 C36 26.0(13) . .
C30 Pr2 O11 C36 -13.1(14) . .
Pr1 Pr2 O11 C36 -99.0(11) . .
O18 Pr3 O12 C36 83.7(14) . .
O1 Pr3 O12 C36 -41.9(13) . .
O3 Pr3 O12 C36 164.6(12) . .
O24 Pr3 O12 C36 0.1(16) . .
O25 Pr3 O12 C36 -101.0(14) . .
O26 Pr3 O12 C36 -140.4(15) . .
O27 Pr3 O12 C36 152.9(14) . .
O19 Pr3 O12 C36 42.1(13) . .
N9 Pr3 O12 C36 60.8(14) . .
O11 Pr2 O13 C42 106.8(11) . .
O20 Pr2 O13 C42 111.6(12) . .
O2 Pr2 O13 C42 -133.4(11) . .
O23 Pr2 O13 C42 -175.2(12) . .
O7 Pr2 O13 C42 29.7(11) . .
O19 Pr2 O13 C42 -17.8(13) . .
O9 Pr2 O13 C42 -44.6(11) . .
O10 Pr2 O13 C42 -97.1(12) . .
C30 Pr2 O13 C42 -72.1(12) . .
Pr1 Pr2 O13 C42 -9.1(11) . .
O15 Pr1 O14 C42 109.1(12) . .
O9 Pr1 O14 C42 22.2(11) . .
O5 Pr1 O14 C42 -133.5(11) . .
O22 Pr1 O14 C42 174.7(12) . .
O17 Pr1 O14 C42 -19.7(13) . .
O8 Pr1 O14 C42 -104.0(12) . .
O21 Pr1 O14 C42 99.4(12) . .
O7 Pr1 O14 C42 -51.3(11) . .
C24 Pr1 O14 C42 -78.0(12) . .
Pr2 Pr1 O14 C42 -14.2(11) . .
O9 Pr1 O15 C48 -134.1(9) . .
O5 Pr1 O15 C48 10.7(9) . .
O14 Pr1 O15 C48 147.6(8) . .
O22 Pr1 O15 C48 84.6(9) . .
O17 Pr1 O15 C48 -67.2(9) . .
O8 Pr1 O15 C48 21.7(11) . .
O21 Pr1 O15 C48 157.5(10) . .
O7 Pr1 O15 C48 -66.5(10) . .
C24 Pr1 O15 C48 -18.5(12) . .
Pr2 Pr1 O15 C48 -113.9(9) . .
O4 Pr4 O16 C48 147.4(13) . .
O6 Pr4 O16 C48 -59.1(14) . .
O18 Pr4 O16 C48 39.5(16) . .
O29 Pr4 O16 C48 -129.8(15) . .
O31 Pr4 O16 C48 101.6(15) . .
O30 Pr4 O16 C48 151.0(16) . .
O28 Pr4 O16 C48 -76.2(16) . .
O17 Pr4 O16 C48 17.4(14) . .
N9 Pr4 O16 C48 29.7(15) . .
O15 Pr1 O17 N9 -137.8(10) . .
O9 Pr1 O17 N9 -33.2(10) . .
O5 Pr1 O17 N9 145.9(10) . .
O14 Pr1 O17 N9 10.3(11) . .
O22 Pr1 O17 N9 164.6(9) . .
O8 Pr1 O17 N9 82.2(10) . .
O21 Pr1 O17 N9 -86.3(10) . .
O7 Pr1 O17 N9 42.7(10) . .
C24 Pr1 O17 N9 63.4(10) . .
Pr2 Pr1 O17 N9 4.9(9) . .
O15 Pr1 O17 Pr4 38.6(4) . .
O9 Pr1 O17 Pr4 143.2(4) . .
O5 Pr1 O17 Pr4 -37.7(3) . .
O14 Pr1 O17 Pr4 -173.3(3) . .
O22 Pr1 O17 Pr4 -19.0(6) . .
O8 Pr1 O17 Pr4 -101.3(3) . .
O21 Pr1 O17 Pr4 90.1(4) . .
O7 Pr1 O17 Pr4 -140.9(4) . .
C24 Pr1 O17 Pr4 -120.2(4) . .
Pr2 Pr1 O17 Pr4 -178.7(4) . .
O4 Pr4 O17 N9 10.3(7) . .
O16 Pr4 O17 N9 151.5(6) . .
O6 Pr4 O17 N9 -129.0(7) . .
O18 Pr4 O17 N9 -5.7(6) . .
O29 Pr4 O17 N9 -118.9(10) . .
O31 Pr4 O17 N9 77.1(6) . .
O30 Pr4 O17 N9 98.0(8) . .
O28 Pr4 O17 N9 -64.4(7) . .
O4 Pr4 O17 Pr1 -167.3(4) . .
O16 Pr4 O17 Pr1 -26.1(4) . .
O6 Pr4 O17 Pr1 53.4(5) . .
O18 Pr4 O17 Pr1 176.7(5) . .
O29 Pr4 O17 Pr1 63.5(9) . .
O31 Pr4 O17 Pr1 -100.5(4) . .
O30 Pr4 O17 Pr1 -79.6(6) . .
O28 Pr4 O17 Pr1 118.0(5) . .
N9 Pr4 O17 Pr1 -177.6(8) . .
O1 Pr3 O18 N9 21.6(10) . .
O3 Pr3 O18 N9 156.0(9) . .
O12 Pr3 O18 N9 -63.0(9) . .
O24 Pr3 O18 N9 76.6(8) . .
O25 Pr3 O18 N9 123.9(11) . .
O26 Pr3 O18 N9 -143.5(10) . .
O27 Pr3 O18 N9 -129.0(9) . .
O19 Pr3 O18 N9 -7.8(7) . .
O1 Pr3 O18 Pr4 -117.4(9) . .
O3 Pr3 O18 Pr4 17.0(9) . .
O12 Pr3 O18 Pr4 158.0(9) . .
O24 Pr3 O18 Pr4 -62.4(10) . .
O25 Pr3 O18 Pr4 -15.1(14) . .
O26 Pr3 O18 Pr4 77.5(13) . .
O27 Pr3 O18 Pr4 91.9(10) . .
O19 Pr3 O18 Pr4 -146.8(12) . .
N9 Pr3 O18 Pr4 -139.0(16) . .
O4 Pr4 O18 N9 -160.5(9) . .
O16 Pr4 O18 N9 -22.7(10) . .
O6 Pr4 O18 N9 62.1(9) . .
O29 Pr4 O18 N9 142.5(9) . .
O31 Pr4 O18 N9 -82.2(8) . .
O30 Pr4 O18 N9 -105.4(9) . .
O28 Pr4 O18 N9 124.3(9) . .
O17 Pr4 O18 N9 5.7(7) . .
O4 Pr4 O18 Pr3 -21.3(9) . .
O16 Pr4 O18 Pr3 116.5(9) . .
O6 Pr4 O18 Pr3 -158.8(9) . .
O29 Pr4 O18 Pr3 -78.3(12) . .
O31 Pr4 O18 Pr3 57.0(9) . .
O30 Pr4 O18 Pr3 33.7(11) . .
O28 Pr4 O18 Pr3 -96.5(10) . .
O17 Pr4 O18 Pr3 144.9(11) . .
N9 Pr4 O18 Pr3 139.2(16) . .
O13 Pr2 O19 N9 18.9(12) . .
O11 Pr2 O19 N9 -127.1(11) . .
O20 Pr2 O19 N9 -85.7(10) . .
O2 Pr2 O19 N9 157.7(11) . .
O23 Pr2 O19 N9 158.1(10) . .
O7 Pr2 O19 N9 -30.4(10) . .
O9 Pr2 O19 N9 46.6(10) . .
O10 Pr2 O19 N9 92.0(10) . .
C30 Pr2 O19 N9 72.7(10) . .
Pr1 Pr2 O19 N9 10.3(10) . .
O13 Pr2 O19 Pr3 -168.2(3) . .
O11 Pr2 O19 Pr3 45.8(4) . .
O20 Pr2 O19 Pr3 87.2(4) . .
O2 Pr2 O19 Pr3 -29.5(4) . .
O23 Pr2 O19 Pr3 -29.0(6) . .
O7 Pr2 O19 Pr3 142.5(4) . .
O9 Pr2 O19 Pr3 -140.5(4) . .
O10 Pr2 O19 Pr3 -95.1(4) . .
C30 Pr2 O19 Pr3 -114.4(5) . .
Pr1 Pr2 O19 Pr3 -176.8(4) . .
O18 Pr3 O19 N9 7.8(7) . .
O1 Pr3 O19 N9 -148.8(7) . .
O3 Pr3 O19 N9 -10.5(8) . .
O12 Pr3 O19 N9 132.1(7) . .
O24 Pr3 O19 N9 -73.6(7) . .
O25 Pr3 O19 N9 -118.0(12) . .
O26 Pr3 O19 N9 127.7(13) . .
O27 Pr3 O19 N9 66.3(7) . .
O18 Pr3 O19 Pr2 -167.5(6) . .
O1 Pr3 O19 Pr2 35.8(5) . .
O3 Pr3 O19 Pr2 174.1(4) . .
O12 Pr3 O19 Pr2 -43.3(4) . .
O24 Pr3 O19 Pr2 111.0(5) . .
O25 Pr3 O19 Pr2 66.6(11) . .
O26 Pr3 O19 Pr2 -47.7(13) . .
O27 Pr3 O19 Pr2 -109.0(5) . .
N9 Pr3 O19 Pr2 -175.3(9) . .
O13 Pr2 O20 C49 -7.0(7) . .
O11 Pr2 O20 C49 169.6(8) . .
O2 Pr2 O20 C49 -139.5(7) . .
O23 Pr2 O20 C49 -87.6(8) . .
O7 Pr2 O20 C49 72.7(7) . .
O19 Pr2 O20 C49 125.3(7) . .
O9 Pr2 O20 C49 26.9(9) . .
O10 Pr2 O20 C49 -51.3(9) . .
C30 Pr2 O20 C49 -13.6(10) . .
Pr1 Pr2 O20 C49 49.1(8) . .
Cu3 Cu1 N1 C1 95.6(12) . .
Cu4 Cu1 N1 C1 -20.4(14) . .
I2 Cu1 N1 C1 161.4(10) . .
Cu2 Cu1 N1 C1 -135.0(9) . .
I1 Cu1 N1 C1 -80.2(11) . .
I3 Cu1 N1 C1 39.0(11) . .
Cu3 Cu1 N1 C5 -80.0(13) . .
Cu4 Cu1 N1 C5 164.0(10) . .
I2 Cu1 N1 C5 -14.2(12) . .
Cu2 Cu1 N1 C5 49.4(14) . .
I1 Cu1 N1 C5 104.2(11) . .
I3 Cu1 N1 C5 -136.6(11) . .
Cu7 Cu5 N5 C25 -132.0(8) 8_565 .
Cu8 Cu5 N5 C25 -19.9(12) 4_655 .
Cu6 Cu5 N5 C25 91.4(10) 2_554 .
I6 Cu5 N5 C25 162.6(9) . .
I5 Cu5 N5 C25 40.5(10) . .
I8 Cu5 N5 C25 -79.0(9) . .
Cu7 Cu5 N5 C29 51.8(12) 8_565 .
Cu8 Cu5 N5 C29 163.9(8) 4_655 .
Cu6 Cu5 N5 C29 -84.8(11) 2_554 .
I6 Cu5 N5 C29 -13.7(11) . .
I5 Cu5 N5 C29 -135.8(10) . .
I8 Cu5 N5 C29 104.8(10) . .
Cu8 Cu6 N6 C35 -99.8(13) 3_456 .
Cu7 Cu6 N6 C35 34.1(16) 7_655 .
Cu5 Cu6 N6 C35 127.5(12) 2 .
I5 Cu6 N6 C35 -163.4(12) 2 .
I7 Cu6 N6 C35 -36.0(14) . .
I6 Cu6 N6 C35 81.0(13) 2 .
Cu8 Cu6 N6 C31 82.3(15) 3_456 .
Cu7 Cu6 N6 C31 -143.9(10) 7_655 .
Cu5 Cu6 N6 C31 -50.4(14) 2 .
I5 Cu6 N6 C31 18.7(13) 2 .
I7 Cu6 N6 C31 146.1(11) . .
I6 Cu6 N6 C31 -96.9(12) 2 .
Cu5 Cu7 N7 C41 -116.3(9) 8_566 .
Cu6 Cu7 N7 C41 111.6(9) 7_665 .
I6 Cu7 N7 C41 -177.7(9) 8_566 .
I8 Cu7 N7 C41 -54.3(10) 8_566 .
Cu8 Cu7 N7 C41 10.5(12) 5_666 .
I7 Cu7 N7 C41 61.4(10) 7_665 .
Cu5 Cu7 N7 C37 65.2(11) 8_566 .
Cu6 Cu7 N7 C37 -67.0(11) 7_665 .
I6 Cu7 N7 C37 3.8(10) 8_566 .
I8 Cu7 N7 C37 127.2(9) 8_566 .
Cu8 Cu7 N7 C37 -168.1(7) 5_666 .
I7 Cu7 N7 C37 -117.1(9) 7_665 .
Cu6 Cu8 N8 C47 -54.2(12) 3_556 .
Cu5 Cu8 N8 C47 69.3(11) 4_655 .
Cu7 Cu8 N8 C47 172.7(8) 5_666 .
I5 Cu8 N8 C47 3.8(10) 4_655 .
I7 Cu8 N8 C47 -118.9(10) 3_556 .
I8 Cu8 N8 C47 124.4(10) 4_655 .
Cu6 Cu8 N8 C43 129.5(7) 3_556 .
Cu5 Cu8 N8 C43 -106.9(7) 4_655 .
Cu7 Cu8 N8 C43 -3.6(10) 5_666 .
I5 Cu8 N8 C43 -172.5(7) 4_655 .
I7 Cu8 N8 C43 64.8(7) 3_556 .
I8 Cu8 N8 C43 -51.9(7) 4_655 .
Pr2 O19 N9 O17 -11.1(18) . .
Pr3 O19 N9 O17 174.2(11) . .
Pr2 O19 N9 O18 162.1(8) . .
Pr3 O19 N9 O18 -12.6(11) . .
Pr2 O19 N9 Pr3 174.7(10) . .
Pr2 O19 N9 Pr4 -177(4) . .
Pr3 O19 N9 Pr4 8(5) . .
Pr1 O17 N9 O19 -0.1(18) . .
Pr4 O17 N9 O19 -177.4(11) . .
Pr1 O17 N9 O18 -173.4(8) . .
Pr4 O17 N9 O18 9.3(11) . .
Pr1 O17 N9 Pr3 155(3) . .
Pr4 O17 N9 Pr3 -23(3) . .
Pr1 O17 N9 Pr4 177.3(9) . .
Pr3 O18 N9 O19 14.4(13) . .
Pr4 O18 N9 O19 175.8(9) . .
Pr3 O18 N9 O17 -171.7(8) . .
Pr4 O18 N9 O17 -10.3(12) . .
Pr4 O18 N9 Pr3 161.4(8) . .
Pr3 O18 N9 Pr4 -161.4(8) . .
O18 Pr3 N9 O19 -165.9(12) . .
O1 Pr3 N9 O19 31.6(7) . .
O3 Pr3 N9 O19 171.0(6) . .
O12 Pr3 N9 O19 -45.6(6) . .
O24 Pr3 N9 O19 98.8(6) . .
O25 Pr3 N9 O19 101.6(10) . .
O26 Pr3 N9 O19 -98.4(11) . .
O27 Pr3 N9 O19 -117.0(7) . .
O18 Pr3 N9 O17 36(3) . .
O1 Pr3 N9 O17 -126(3) . .
O3 Pr3 N9 O17 13(3) . .
O12 Pr3 N9 O17 157(3) . .
O24 Pr3 N9 O17 -59(3) . .
O25 Pr3 N9 O17 -56(4) . .
O26 Pr3 N9 O17 104(3) . .
O27 Pr3 N9 O17 85(3) . .
O19 Pr3 N9 O17 -158(4) . .
O1 Pr3 N9 O18 -162.5(9) . .
O3 Pr3 N9 O18 -23.1(9) . .
O12 Pr3 N9 O18 120.3(9) . .
O24 Pr3 N9 O18 -95.3(9) . .
O25 Pr3 N9 O18 -92.5(11) . .
O26 Pr3 N9 O18 67.5(14) . .
O27 Pr3 N9 O18 48.9(9) . .
O19 Pr3 N9 O18 165.9(12) . .
O18 Pr3 N9 Pr4 15.5(7) . .
O1 Pr3 N9 Pr4 -147.0(4) . .
O3 Pr3 N9 Pr4 -7.6(4) . .
O12 Pr3 N9 Pr4 135.8(4) . .
O24 Pr3 N9 Pr4 -79.8(4) . .
O25 Pr3 N9 Pr4 -77.0(8) . .
O26 Pr3 N9 Pr4 83.0(11) . .
O27 Pr3 N9 Pr4 64.4(5) . .
O19 Pr3 N9 Pr4 -178.6(8) . .
O4 Pr4 N9 O19 -4(5) . .
O16 Pr4 N9 O19 139(5) . .
O6 Pr4 N9 O19 -144(5) . .
O18 Pr4 N9 O19 -23(4) . .
O29 Pr4 N9 O19 -87(5) . .
O31 Pr4 N9 O19 70(5) . .
O30 Pr4 N9 O19 68(5) . .
O28 Pr4 N9 O19 -75(5) . .
O17 Pr4 N9 O19 168(5) . .
O4 Pr4 N9 O17 -171.4(6) . .
O16 Pr4 N9 O17 -28.8(6) . .
O6 Pr4 N9 O17 48.6(6) . .
O18 Pr4 N9 O17 169.7(12) . .
O29 Pr4 N9 O17 106.0(10) . .
O31 Pr4 N9 O17 -98.0(6) . .
O30 Pr4 N9 O17 -99.6(7) . .
O28 Pr4 N9 O17 117.4(7) . .
O4 Pr4 N9 O18 18.9(9) . .
O16 Pr4 N9 O18 161.5(8) . .
O6 Pr4 N9 O18 -121.1(9) . .
O29 Pr4 N9 O18 -63.8(13) . .
O31 Pr4 N9 O18 92.3(8) . .
O30 Pr4 N9 O18 90.7(9) . .
O28 Pr4 N9 O18 -52.3(9) . .
O17 Pr4 N9 O18 -169.7(12) . .
O4 Pr4 N9 Pr3 3.7(4) . .
O16 Pr4 N9 Pr3 146.3(3) . .
O6 Pr4 N9 Pr3 -136.4(4) . .
O18 Pr4 N9 Pr3 -15.3(7) . .
O29 Pr4 N9 Pr3 -79.0(10) . .
O31 Pr4 N9 Pr3 77.1(3) . .
O30 Pr4 N9 Pr3 75.4(6) . .
O28 Pr4 N9 Pr3 -67.6(4) . .
O17 Pr4 N9 Pr3 175.0(8) . .
C5 N1 C1 C2 -2(2) . .
Cu1 N1 C1 C2 -177.7(12) . .
N1 C1 C2 C3 0(2) . .
C1 C2 C3 C4 0(2) . .
C1 C2 C3 C6 178.6(13) . .
C2 C3 C4 C5 2(3) . .
C6 C3 C4 C5 -176.3(18) . .
C1 N1 C5 C4 4(2) . .
Cu1 N1 C5 C4 179.5(13) . .
C3 C4 C5 N1 -4(3) . .
Pr2 O2 C6 O1 42(3) . .
Pr2 O2 C6 C3 -140.0(19) . .
Pr3 O1 C6 O2 -16(3) . .
Pr3 O1 C6 C3 165.7(12) . .
C4 C3 C6 O2 -2(2) . .
C2 C3 C6 O2 179.8(14) . .
C4 C3 C6 O1 176.5(17) . .
C2 C3 C6 O1 -2(2) . .
C11 N2 C7 C8 2(3) . .
Cu2 N2 C7 C8 172.0(16) 7_655 .
N2 C7 C8 C9 1(3) . .
C7 C8 C9 C10 1(3) . .
C7 C8 C9 C12 -177.9(16) . .
C8 C9 C10 C11 -7(3) . .
C12 C9 C10 C11 172.8(18) . .
C7 N2 C11 C10 -7(3) . .
Cu2 N2 C11 C10 -176.4(15) 7_655 .
C9 C10 C11 N2 10(3) . .
Pr4 O4 C12 O3 47(3) . .
Pr4 O4 C12 C9 -135.6(12) . .
Pr3 O3 C12 O4 -60(3) . .
Pr3 O3 C12 C9 122.7(12) . .
C10 C9 C12 O4 4(3) . .
C8 C9 C12 O4 -176.5(16) . .
C10 C9 C12 O3 -178.1(18) . .
C8 C9 C12 O3 1(2) . .
C17 N3 C13 C14 3(2) . .
Cu3 N3 C13 C14 178.7(10) 3_556 .
N3 C13 C14 C15 -1(2) . .
C13 C14 C15 C16 1(2) . .
C13 C14 C15 C18 -177.3(13) . .
C14 C15 C16 C17 -3(3) . .
C18 C15 C16 C17 175.5(18) . .
C13 N3 C17 C16 -5(3) . .
Cu3 N3 C17 C16 179.8(15) 3_556 .
C15 C16 C17 N3 5(3) . .
Pr1 O5 C18 O6 38(3) . .
Pr1 O5 C18 C15 -136.1(12) . .
Pr4 O6 C18 O5 12(3) . .
Pr4 O6 C18 C15 -174.0(11) . .
C14 C15 C18 O5 15(2) . .
C16 C15 C18 O5 -163.9(15) . .
C14 C15 C18 O6 -159.8(15) . .
C16 C15 C18 O6 22(2) . .
C23 N4 C19 C20 0.8(18) . .
Cu4 N4 C19 C20 178.5(9) 2 .
N4 C19 C20 C21 -0.7(18) . .
C19 C20 C21 C22 -3.0(15) . .
C19 C20 C21 C24 -178.1(10) . .
C20 C21 C22 C23 7(2) . .
C24 C21 C22 C23 -178.0(13) . .
C19 N4 C23 C22 3(2) . .
Cu4 N4 C23 C22 -174.9(12) 2 .
C21 C22 C23 N4 -7(2) . .
Pr1 O8 C24 O7 0.4(10) . .
Pr1 O8 C24 C21 176.6(7) . .
Pr2 O7 C24 O8 -123.8(10) . .
Pr1 O7 C24 O8 -0.4(10) . .
Pr2 O7 C24 C21 59.9(14) . .
Pr1 O7 C24 C21 -176.7(7) . .
Pr2 O7 C24 Pr1 -123.4(10) . .
C20 C21 C24 O8 -155.3(10) . .
C22 C21 C24 O8 29.9(15) . .
C20 C21 C24 O7 21.2(14) . .
C22 C21 C24 O7 -153.7(11) . .
C20 C21 C24 Pr1 -88(14) . .
C22 C21 C24 Pr1 97(14) . .
O15 Pr1 C24 O8 82.3(8) . .
O9 Pr1 C24 O8 -161.1(6) . .
O5 Pr1 C24 O8 54.1(6) . .
O14 Pr1 C24 O8 -87.9(6) . .
O22 Pr1 C24 O8 -16.8(6) . .
O17 Pr1 C24 O8 129.5(6) . .
O21 Pr1 C24 O8 -91.8(7) . .
O7 Pr1 C24 O8 179.6(9) . .
Pr2 Pr1 C24 O8 -162.4(6) . .
O15 Pr1 C24 O7 -97.3(7) . .
O9 Pr1 C24 O7 19.3(5) . .
O5 Pr1 C24 O7 -125.5(5) . .
O14 Pr1 C24 O7 92.4(5) . .
O22 Pr1 C24 O7 163.6(5) . .
O17 Pr1 C24 O7 -50.1(5) . .
O8 Pr1 C24 O7 -179.6(9) . .
O21 Pr1 C24 O7 88.5(6) . .
Pr2 Pr1 C24 O7 18.0(4) . .
O15 Pr1 C24 C21 13(15) . .
O9 Pr1 C24 C21 130(14) . .
O5 Pr1 C24 C21 -15(14) . .
O14 Pr1 C24 C21 -157(14) . .
O22 Pr1 C24 C21 -86(14) . .
O17 Pr1 C24 C21 60(14) . .
O8 Pr1 C24 C21 -69(14) . .
O21 Pr1 C24 C21 -161(14) . .
O7 Pr1 C24 C21 110(14) . .
Pr2 Pr1 C24 C21 129(14) . .
C29 N5 C25 C26 -0.4(18) . .
Cu5 N5 C25 C26 -176.9(10) . .
N5 C25 C26 C27 2(2) . .
C25 C26 C27 C28 -0.6(18) . .
C25 C26 C27 C30 170.3(12) . .
C26 C27 C28 C29 -2.0(19) . .
C30 C27 C28 C29 -173.4(12) . .
C25 N5 C29 C28 -2(2) . .
Cu5 N5 C29 C28 174.1(11) . .
C27 C28 C29 N5 4(2) . .
Pr2 O10 C30 O9 -10.9(11) . .
Pr2 O10 C30 C27 160.7(9) . .
Pr1 O9 C30 O10 -144.0(10) . .
Pr2 O9 C30 O10 11.0(11) . .
Pr1 O9 C30 C27 43.6(18) . .
Pr2 O9 C30 C27 -161.4(8) . .
Pr1 O9 C30 Pr2 -154.9(14) . .
C26 C27 C30 O10 -140.3(12) . .
C28 C27 C30 O10 30.4(17) . .
C26 C27 C30 O9 31.8(15) . .
C28 C27 C30 O9 -157.5(10) . .
C26 C27 C30 Pr2 -35(3) . .
C28 C27 C30 Pr2 136(3) . .
O13 Pr2 C30 O10 -91.1(8) . .
O11 Pr2 C30 O10 90.1(9) . .
O20 Pr2 C30 O10 -84.6(9) . .
O2 Pr2 C30 O10 50.2(8) . .
O23 Pr2 C30 O10 -18.8(8) . .
O7 Pr2 C30 O10 -165.2(7) . .
O19 Pr2 C30 O10 126.3(8) . .
O9 Pr2 C30 O10 -169.4(11) . .
Pr1 Pr2 C30 O10 -161.9(8) . .
O13 Pr2 C30 O9 78.2(5) . .
O11 Pr2 C30 O9 -100.6(7) . .
O20 Pr2 C30 O9 84.7(7) . .
O2 Pr2 C30 O9 -140.4(6) . .
O23 Pr2 C30 O9 150.6(5) . .
O7 Pr2 C30 O9 4.2(5) . .
O19 Pr2 C30 O9 -64.3(5) . .
O10 Pr2 C30 O9 169.4(11) . .
Pr1 Pr2 C30 O9 7.4(4) . .
O13 Pr2 C30 C27 153(3) . .
O11 Pr2 C30 C27 -25(3) . .
O20 Pr2 C30 C27 160(3) . .
O2 Pr2 C30 C27 -65(3) . .
O23 Pr2 C30 C27 -134(3) . .
O7 Pr2 C30 C27 79(3) . .
O19 Pr2 C30 C27 11(3) . .
O9 Pr2 C30 C27 75(3) . .
O10 Pr2 C30 C27 -115(3) . .
Pr1 Pr2 C30 C27 83(3) . .
C35 N6 C31 C32 -9(2) . .
Cu6 N6 C31 C32 169.2(12) . .
N6 C31 C32 C33 0(2) . .
C31 C32 C33 C34 1(2) . .
C31 C32 C33 C36 -177.1(13) . .
C32 C33 C34 C35 6(2) . .
C36 C33 C34 C35 -176.2(13) . .
C31 N6 C35 C34 16(2) . .
Cu6 N6 C35 C34 -162.0(12) . .
C33 C34 C35 N6 -15(3) . .
Pr3 O12 C36 O11 -66(2) . .
Pr3 O12 C36 C33 115.0(11) . .
Pr2 O11 C36 O12 70(2) . .
Pr2 O11 C36 C33 -110.8(11) . .
C34 C33 C36 O12 3.8(19) . .
C32 C33 C36 O12 -177.9(14) . .
C34 C33 C36 O11 -175.7(13) . .
C32 C33 C36 O11 2.5(19) . .
C41 N7 C37 C38 -0.4(18) . .
Cu7 N7 C37 C38 178.2(9) . .
N7 C37 C38 C39 -4(2) . .
C37 C38 C39 C40 3.6(19) . .
C37 C38 C39 C42 -172.5(11) . .
C38 C39 C40 C41 1.8(19) . .
C42 C39 C40 C41 178.0(12) . .
C37 N7 C41 C40 6(2) . .
Cu7 N7 C41 C40 -172.4(11) . .
C39 C40 C41 N7 -7(2) . .
Pr1 O14 C42 O13 14(2) . .
Pr1 O14 C42 C39 -162.6(7) . .
Pr2 O13 C42 O14 3(2) . .
Pr2 O13 C42 C39 -179.6(8) . .
C40 C39 C42 O14 8.7(17) . .
C38 C39 C42 O14 -175.4(12) . .
C40 C39 C42 O13 -168.6(11) . .
C38 C39 C42 O13 7.3(16) . .
C47 N8 C43 C44 -4.8(15) . .
Cu8 N8 C43 C44 171.9(8) . .
N8 C43 C44 C45 -1.2(16) . .
C43 C44 C45 C46 2.2(16) . .
C43 C44 C45 C48 -178.4(10) . .
C44 C45 C46 C47 2.8(18) . .
C48 C45 C46 C47 -176.5(12) . .
C45 C46 C47 N8 -10(2) . .
C43 N8 C47 C46 11.0(19) . .
Cu8 N8 C47 C46 -165.4(11) . .
Pr1 O15 C48 O16 83.2(15) . .
Pr1 O15 C48 C45 -97.5(11) . .
Pr4 O16 C48 O15 -45(2) . .
Pr4 O16 C48 C45 135.3(10) . .
C44 C45 C48 O15 -9.5(16) . .
C46 C45 C48 O15 169.8(12) . .
C44 C45 C48 O16 169.9(11) . .
C46 C45 C48 O16 -10.8(17) . .
Pr2 O20 C49 N12 174.3(6) . .
C50 N12 C49 O20 0.00(3) . .
