#------------------------------------------------------------------------------
#$Date: 2017-04-05 12:59:51 +0300 (Wed, 05 Apr 2017) $
#$Revision: 195138 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/22/75/7227520.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7227520
loop_
_publ_author_name
'Hu, Yue-Qiao'
'Zhang, Tao'
'Li, Mu-Qing'
'Wang, Yanyan'
'Zheng, Zhiping'
'Zheng, Yan-Zhen'
_publ_section_title
;
 Copper(i)/(ii)-redox triggered efficient and green rare-earth separation
 using a heterometallic metal--organic framework
;
_journal_issue                   5
_journal_name_full               'Green Chem.'
_journal_page_first              1250
_journal_paper_doi               10.1039/C6GC02833K
_journal_volume                  19
_journal_year                    2017
_chemical_formula_sum            'C48 H72 Cu2 Eu2 I2 N14 O23'
_chemical_formula_weight         1898.00
_chemical_name_common            1-Eu
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                92.5280(10)
_cell_angle_beta                 96.8370(10)
_cell_angle_gamma                116.2890(10)
_cell_formula_units_Z            1
_cell_length_a                   11.1874(8)
_cell_length_b                   12.6000(9)
_cell_length_c                   15.1798(11)
_cell_measurement_reflns_used    9229
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      24.81
_cell_measurement_theta_min      2.28
_cell_volume                     1893.5(2)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.966
_diffrn_measured_fraction_theta_max 0.966
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0156
_diffrn_reflns_av_sigmaI/netI    0.0205
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            15346
_diffrn_reflns_theta_full        24.82
_diffrn_reflns_theta_max         24.82
_diffrn_reflns_theta_min         1.36
_exptl_absorpt_coefficient_mu    3.076
_exptl_absorpt_correction_T_max  0.824
_exptl_absorpt_correction_T_min  0.608
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            YELLOW
_exptl_crystal_density_diffrn    1.664
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       BLOCK
_exptl_crystal_F_000             932
_exptl_crystal_size_max          0.165
_exptl_crystal_size_mid          0.150
_exptl_crystal_size_min          0.063
_refine_diff_density_max         1.301
_refine_diff_density_min         -0.427
_refine_diff_density_rms         0.125
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.020
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     412
_refine_ls_number_reflns         6315
_refine_ls_number_restraints     32
_refine_ls_restrained_S_all      1.038
_refine_ls_R_factor_all          0.0326
_refine_ls_R_factor_gt           0.0274
_refine_ls_shift/su_max          0.007
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0646P)²+3.1834P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0894
_refine_ls_wR_factor_ref         0.0975
_reflns_number_gt                5629
_reflns_number_total             6315
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c6gc02833k2.cif
_cod_data_source_block           2
_cod_depositor_comments
'Adding full bibliography for 7227519--7227529.cif.'
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7227520
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Eu1 Eu 0.29357(2) 0.889285(18) 0.963884(14) 0.02761(9) Uani 1 1 d .
I1 I 0.27501(3) 1.42813(3) 0.49164(2) 0.04524(12) Uani 1 1 d .
Cu1 Cu 0.51306(6) 1.49833(5) 0.58882(4) 0.03804(16) Uani 1 1 d .
O4 O 0.3828(3) 1.0493(3) 0.8739(2) 0.0426(8) Uani 1 1 d .
O3 O 0.6089(3) 1.1355(3) 0.8963(2) 0.0406(8) Uani 1 1 d .
O2 O 0.4892(4) 0.8842(3) 0.9304(2) 0.0435(8) Uani 1 1 d .
O1 O 0.7088(4) 0.9465(3) 0.9483(2) 0.0422(8) Uani 1 1 d .
O5 O 0.2289(4) 0.6783(3) 0.9558(3) 0.0558(10) Uani 1 1 d .
O6 O 0.1076(4) 0.8116(3) 1.0449(3) 0.0461(9) Uani 1 1 d .
N2 N 0.5043(4) 1.3605(4) 0.6622(3) 0.0397(10) Uani 1 1 d .
O8 O 0.0861(4) 0.8719(4) 0.8669(3) 0.0619(11) Uani 1 1 d .
N1 N 0.5430(4) 0.6278(4) 0.6908(3) 0.0406(10) Uani 1 1 d .
O7 O 0.1987(4) 0.7996(4) 0.8049(3) 0.0610(11) Uani 1 1 d .
C9 C 0.4989(5) 1.2029(4) 0.7875(3) 0.0356(10) Uani 1 1 d .
N4 N 0.0064(5) 0.8680(5) 1.1438(3) 0.0552(12) Uani 1 1 d .
C8 C 0.6187(5) 1.2817(5) 0.7623(4) 0.0424(12) Uani 1 1 d .
H8A H 0.7015 1.2833 0.7873 0.051 Uiso 1 1 calc R
C6 C 0.5920(5) 0.8791(4) 0.9100(3) 0.0340(10) Uani 1 1 d .
C12 C 0.4965(5) 1.1214(4) 0.8580(3) 0.0341(10) Uani 1 1 d .
N5 N 0.0997(5) 0.8232(5) 0.7988(4) 0.0609(14) Uani 1 1 d .
C3 C 0.5747(5) 0.7887(4) 0.8348(3) 0.0341(10) Uani 1 1 d .
C10 C 0.3817(6) 1.2013(6) 0.7459(4) 0.0554(16) Uani 1 1 d .
H10A H 0.2967 1.1458 0.7591 0.066 Uiso 1 1 calc R
C2 C 0.6857(5) 0.7866(5) 0.8044(4) 0.0429(12) Uani 1 1 d .
H2A H 0.7746 0.8396 0.8325 0.052 Uiso 1 1 calc R
C4 C 0.4478(5) 0.7072(5) 0.7925(4) 0.0474(13) Uani 1 1 d .
H4A H 0.3693 0.7054 0.8118 0.057 Uiso 1 1 calc R
C1 C 0.6644(5) 0.7056(5) 0.7319(4) 0.0454(12) Uani 1 1 d .
H1A H 0.7411 0.7060 0.7107 0.054 Uiso 1 1 calc R
C7 C 0.6168(5) 1.3583(5) 0.7002(4) 0.0455(13) Uani 1 1 d .
H7A H 0.7002 1.4123 0.6838 0.055 Uiso 1 1 calc R
C5 C 0.4365(5) 0.6293(5) 0.7226(4) 0.0508(14) Uani 1 1 d .
H5A H 0.3486 0.5731 0.6950 0.061 Uiso 1 1 calc R
N3 N 0.2194(6) 0.5208(4) 1.0269(4) 0.0698(15) Uani 1 1 d .
C18 C 0.1035(5) 0.8458(5) 1.1216(4) 0.0479(13) Uani 1 1 d .
H18A H 0.1750 0.8567 1.1673 0.057 Uiso 1 1 calc R
C11 C 0.3889(6) 1.2809(6) 0.6849(4) 0.0583(17) Uani 1 1 d .
H11A H 0.3070 1.2790 0.6575 0.070 Uiso 1 1 calc R
C15 C 0.1874(6) 0.6076(4) 1.0122(4) 0.0550(15) Uani 1 1 d .
H15A H 0.1277 0.6171 1.0478 0.066 Uiso 1 1 calc R
O9 O 0.0206(7) 0.7970(8) 0.7301(4) 0.132(3) Uani 1 1 d .
C17 C 0.0046(8) 0.9046(8) 1.2356(5) 0.085(2) Uani 1 1 d .
H17A H 0.0851 0.9109 1.2737 0.128 Uiso 1 1 calc R
H17B H -0.0764 0.8455 1.2560 0.128 Uiso 1 1 calc R
H17C H 0.0038 0.9822 1.2390 0.128 Uiso 1 1 calc R
C14 C 0.1610(9) 0.4359(6) 1.0917(5) 0.085(2) Uani 1 1 d .
H14A H 0.1009 0.4576 1.1218 0.127 Uiso 1 1 calc R
H14B H 0.2336 0.4381 1.1359 0.127 Uiso 1 1 calc R
H14C H 0.1095 0.3554 1.0604 0.127 Uiso 1 1 calc R
C16 C -0.1040(9) 0.8557(9) 1.0774(6) 0.099(3) Uani 1 1 d .
H16A H -0.0910 0.8309 1.0187 0.149 Uiso 1 1 calc R
H16B H -0.1068 0.9323 1.0761 0.149 Uiso 1 1 calc R
H16C H -0.1891 0.7957 1.0924 0.149 Uiso 1 1 calc R
C13 C 0.3152(14) 0.5053(11) 0.9760(10) 0.172(7) Uani 1 1 d .
H13A H 0.3471 0.5681 0.9364 0.257 Uiso 1 1 calc R
H13B H 0.2704 0.4274 0.9404 0.257 Uiso 1 1 calc R
H13C H 0.3921 0.5100 1.0174 0.257 Uiso 1 1 calc R
N6 N 0.9870(6) 0.5385(5) 0.3210(4) 0.0667(15) Uani 1 1 d .
N7 N 0.5100(8) 0.1065(6) 0.4071(5) 0.0859(19) Uani 1 1 d D
C20 C 0.9348(8) 0.4386(7) 0.3693(5) 0.078(2) Uani 1 1 d .
H20A H 0.8835 0.3663 0.3276 0.116 Uiso 1 1 calc R
H20B H 0.8754 0.4479 0.4082 0.116 Uiso 1 1 calc R
H20C H 1.0094 0.4323 0.4057 0.116 Uiso 1 1 calc R
O10 O 1.0107(8) 0.6029(6) 0.1854(5) 0.129(3) Uani 1 1 d .
C21 C 0.9654(9) 0.5246(8) 0.2343(6) 0.093(3) Uani 1 1 d .
H21A H 0.9092 0.4461 0.2063 0.111 Uiso 1 1 calc R
C19 C 1.0645(10) 0.6531(8) 0.3713(7) 0.107(3) Uani 1 1 d .
H19A H 1.0950 0.7144 0.3304 0.161 Uiso 1 1 calc R
H19B H 1.1430 0.6540 0.4084 0.161 Uiso 1 1 calc R
H19C H 1.0085 0.6691 0.4097 0.161 Uiso 1 1 calc R
O11 O 0.3460(13) -0.0358(11) 0.3163(9) 0.199(4) Uani 1 1 d DU
C24 C 0.3760(14) 0.0379(16) 0.3748(13) 0.252(11) Uani 1 1 d DU
H24A H 0.3088 0.0505 0.3998 0.303 Uiso 1 1 calc R
C22 C 0.5215(18) 0.1834(14) 0.4775(10) 0.194(6) Uani 1 1 d U
H22A H 0.6166 0.2281 0.5045 0.291 Uiso 1 1 calc R
H22B H 0.4686 0.1385 0.5220 0.291 Uiso 1 1 calc R
H22C H 0.4878 0.2390 0.4565 0.291 Uiso 1 1 calc R
C23 C 0.634(2) 0.128(2) 0.3972(15) 0.261(10) Uani 1 1 d U
H23A H 0.6311 0.0727 0.3484 0.391 Uiso 1 1 calc R
H23B H 0.6803 0.1172 0.4526 0.391 Uiso 1 1 calc R
H23C H 0.6837 0.2100 0.3831 0.391 Uiso 1 1 calc R
O1W O 0.0000 0.0000 0.5000 0.291(10) Uani 1 2 d SU
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Eu Eu -0.1578 3.6682 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O2 Eu1 O3 77.71(12) . 2_677
O2 Eu1 O4 76.68(12) . .
O3 Eu1 O4 128.97(12) 2_677 .
O2 Eu1 O6 147.32(13) . .
O3 Eu1 O6 76.64(13) 2_677 .
O4 Eu1 O6 135.80(13) . .
O2 Eu1 O5 78.41(14) . .
O3 Eu1 O5 75.74(13) 2_677 .
O4 Eu1 O5 138.72(13) . .
O6 Eu1 O5 75.90(14) . .
O2 Eu1 O1 124.15(13) . 2_677
O3 Eu1 O1 81.89(12) 2_677 2_677
O4 Eu1 O1 77.28(12) . 2_677
O6 Eu1 O1 71.43(12) . 2_677
O5 Eu1 O1 143.81(13) . 2_677
O2 Eu1 O8 132.23(13) . .
O3 Eu1 O8 147.72(13) 2_677 .
O4 Eu1 O8 77.13(14) . .
O6 Eu1 O8 71.08(14) . .
O5 Eu1 O8 96.59(15) . .
O1 Eu1 O8 87.34(13) 2_677 .
O2 Eu1 O7 84.39(14) . .
O3 Eu1 O7 145.04(13) 2_677 .
O4 Eu1 O7 73.89(14) . .
O6 Eu1 O7 105.85(15) . .
O5 Eu1 O7 71.35(14) . .
O1 Eu1 O7 132.57(13) 2_677 .
O8 Eu1 O7 50.09(14) . .
O2 Eu1 N5 108.58(15) . .
O3 Eu1 N5 157.38(14) 2_677 .
O4 Eu1 N5 73.40(14) . .
O6 Eu1 N5 88.61(15) . .
O5 Eu1 N5 84.16(15) . .
O1 Eu1 N5 109.84(14) 2_677 .
O8 Eu1 N5 24.77(14) . .
O7 Eu1 N5 25.33(14) . .
O2 Eu1 O2 78.37(12) . 2_677
O3 Eu1 O2 64.73(11) 2_677 2_677
O4 Eu1 O2 67.30(11) . 2_677
O6 Eu1 O2 108.02(11) . 2_677
O5 Eu1 O2 137.42(12) . 2_677
O1 Eu1 O2 46.02(10) 2_677 2_677
O8 Eu1 O2 125.27(13) . 2_677
O7 Eu1 O2 140.14(13) . 2_677
N5 Eu1 O2 137.27(13) . 2_677
O2 Eu1 C6 102.08(13) . 2_677
O3 Eu1 C6 69.91(12) 2_677 2_677
O4 Eu1 C6 73.38(12) . 2_677
O6 Eu1 C6 87.74(13) . 2_677
O5 Eu1 C6 144.55(13) . 2_677
O1 Eu1 C6 22.57(12) 2_677 2_677
O8 Eu1 C6 107.68(14) . 2_677
O7 Eu1 C6 144.05(13) . 2_677
N5 Eu1 C6 127.30(14) . 2_677
O2 Eu1 C6 23.71(11) 2_677 2_677
O2 Eu1 Eu1 45.20(9) . 2_677
O3 Eu1 Eu1 64.65(8) 2_677 2_677
O4 Eu1 Eu1 65.91(8) . 2_677
O6 Eu1 Eu1 133.97(9) . 2_677
O5 Eu1 Eu1 114.92(11) . 2_677
O1 Eu1 Eu1 79.07(9) 2_677 2_677
O8 Eu1 Eu1 142.54(11) . 2_677
O7 Eu1 Eu1 120.10(11) . 2_677
N5 Eu1 Eu1 135.25(12) . 2_677
O2 Eu1 Eu1 33.17(6) 2_677 2_677
C6 Eu1 Eu1 56.88(9) 2_677 2_677
Cu1 I1 Cu1 61.57(2) 2_686 .
N2 Cu1 N1 100.68(17) . 1_565
N2 Cu1 I1 109.46(12) . 2_686
N1 Cu1 I1 109.32(12) 1_565 2_686
N2 Cu1 I1 107.77(12) . .
N1 Cu1 I1 109.71(12) 1_565 .
I1 Cu1 I1 118.43(2) 2_686 .
N2 Cu1 Cu1 128.57(13) . 2_686
N1 Cu1 Cu1 130.74(13) 1_565 2_686
I1 Cu1 Cu1 59.56(2) 2_686 2_686
I1 Cu1 Cu1 58.87(2) . 2_686
C12 O4 Eu1 137.5(3) . .
C12 O3 Eu1 139.0(3) . 2_677
C6 O2 Eu1 178.0(3) . .
C6 O2 Eu1 80.2(3) . 2_677
Eu1 O2 Eu1 101.63(11) . 2_677
C6 O1 Eu1 109.3(3) . 2_677
C15 O5 Eu1 130.0(4) . .
C18 O6 Eu1 127.7(3) . .
C7 N2 C11 116.4(4) . .
C7 N2 Cu1 120.8(3) . .
C11 N2 Cu1 122.0(3) . .
N5 O8 Eu1 97.0(3) . .
C1 N1 C5 116.7(4) . .
C1 N1 Cu1 123.1(3) . 1_545
C5 N1 Cu1 120.0(3) . 1_545
N5 O7 Eu1 96.2(3) . .
C10 C9 C8 117.6(4) . .
C10 C9 C12 121.2(4) . .
C8 C9 C12 121.2(4) . .
C18 N4 C16 120.9(6) . .
C18 N4 C17 121.7(6) . .
C16 N4 C17 117.4(6) . .
C9 C8 C7 119.3(5) . .
O1 C6 O2 123.1(4) . .
O1 C6 C3 118.2(4) . .
O2 C6 C3 118.7(4) . .
O1 C6 Eu1 48.1(2) . 2_677
O2 C6 Eu1 76.0(3) . 2_677
C3 C6 Eu1 161.7(3) . 2_677
O4 C12 O3 126.8(4) . .
O4 C12 C9 116.8(4) . .
O3 C12 C9 116.4(4) . .
O9 N5 O8 121.9(6) . .
O9 N5 O7 121.4(6) . .
O8 N5 O7 116.6(5) . .
O9 N5 Eu1 179.3(7) . .
O8 N5 Eu1 58.2(3) . .
O7 N5 Eu1 58.4(3) . .
C4 C3 C2 117.9(4) . .
C4 C3 C6 121.2(4) . .
C2 C3 C6 120.9(4) . .
C9 C10 C11 119.4(5) . .
C3 C2 C1 118.7(5) . .
C5 C4 C3 119.4(5) . .
N1 C1 C2 123.7(5) . .
N2 C7 C8 123.5(5) . .
N1 C5 C4 123.6(5) . .
C15 N3 C13 119.4(6) . .
C15 N3 C14 122.7(7) . .
C13 N3 C14 117.9(6) . .
O6 C18 N4 124.0(6) . .
N2 C11 C10 123.8(5) . .
O5 C15 N3 125.3(6) . .
C21 N6 C20 120.2(7) . .
C21 N6 C19 122.4(7) . .
C20 N6 C19 117.4(7) . .
C23 N7 C22 106.5(13) . .
C23 N7 C24 144.7(14) . .
C22 N7 C24 108.8(12) . .
O10 C21 N6 126.2(8) . .
O11 C24 N7 118.8(17) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Eu1 O2 2.332(3) .
Eu1 O3 2.366(3) 2_677
Eu1 O4 2.390(3) .
Eu1 O6 2.390(4) .
Eu1 O5 2.420(4) .
Eu1 O1 2.423(3) 2_677
Eu1 O8 2.512(4) .
Eu1 O7 2.513(4) .
Eu1 N5 2.933(5) .
Eu1 O2 3.025(4) 2_677
Eu1 C6 3.071(5) 2_677
Eu1 Eu1 4.1748(5) 2_677
I1 Cu1 2.6106(7) 2_686
I1 Cu1 2.6294(7) .
Cu1 N2 2.077(4) .
Cu1 N1 2.082(4) 1_565
Cu1 I1 2.6106(7) 2_686
Cu1 Cu1 2.6818(12) 2_686
O4 C12 1.253(6) .
O3 C12 1.254(6) .
O3 Eu1 2.366(3) 2_677
O2 C6 1.253(6) .
O2 Eu1 3.025(4) 2_677
O1 C6 1.249(6) .
O1 Eu1 2.423(3) 2_677
O5 C15 1.240(7) .
O6 C18 1.237(7) .
N2 C7 1.333(6) .
N2 C11 1.334(7) .
O8 N5 1.238(6) .
N1 C1 1.328(7) .
N1 C5 1.345(7) .
N1 Cu1 2.082(4) 1_545
O7 N5 1.262(6) .
C9 C10 1.376(7) .
C9 C8 1.380(7) .
C9 C12 1.511(6) .
N4 C18 1.310(7) .
N4 C16 1.445(9) .
N4 C17 1.455(8) .
C8 C7 1.383(7) .
C6 C3 1.509(6) .
C6 Eu1 3.071(5) 2_677
N5 O9 1.213(7) .
C3 C4 1.384(7) .
C3 C2 1.386(7) .
C10 C11 1.377(7) .
C2 C1 1.389(7) .
C4 C5 1.369(7) .
N3 C15 1.312(8) .
N3 C13 1.468(11) .
N3 C14 1.471(9) .
N6 C21 1.299(10) .
N6 C20 1.413(9) .
N6 C19 1.434(10) .
N7 C23 1.323(19) .
N7 C22 1.365(15) .
N7 C24 1.369(10) .
O10 C21 1.222(10) .
O11 C24 1.159(10) .
