#------------------------------------------------------------------------------
#$Date: 2017-05-09 04:35:02 +0300 (Tue, 09 May 2017) $
#$Revision: 196565 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/22/82/7228233.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7228233
loop_
_publ_author_name
'Fukushima, Misaki'
'Kikkawa, Shoko'
'hikawa, hidemasa'
'Azumaya, Isao'
_publ_section_title
;
 Synthesis and Solvent Vapor Induced Transformations of Crystals of 1D
 Coordination Polymer Assembled with Continuous Void Space
;
_journal_name_full               CrystEngComm
_journal_paper_doi               10.1039/C7CE00640C
_journal_year                    2017
_chemical_absolute_configuration ad
_chemical_formula_moiety         'C34 H32 Ag Cl N2 O6'
_chemical_formula_sum            'C34 H32 Ag Cl N2 O6'
_chemical_formula_weight         707.96
_space_group_crystal_system      orthorhombic
_space_group_IT_number           33
_space_group_name_Hall           'P 2c -2n'
_space_group_name_H-M_alt        'P n a 21'
_symmetry_space_group_name_Hall  'P 2c -2n'
_symmetry_space_group_name_H-M   'P n a 21'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_update_record
;
2017-01-10 deposited with the CCDC.
2017-05-08 downloaded from the CCDC.
;
_cell_angle_alpha                90.0000
_cell_angle_beta                 90.0000
_cell_angle_gamma                90.0000
_cell_formula_units_Z            4
_cell_length_a                   18.5169(19)
_cell_length_b                   14.1650(15)
_cell_length_c                   11.4339(11)
_cell_measurement_reflns_used    7027
_cell_measurement_temperature    93
_cell_measurement_theta_max      27.50
_cell_measurement_theta_min      3.10
_cell_volume                     2999.0(5)
_computing_cell_refinement       'CrystalClear-SM Expert 2.1 b29'
_computing_data_collection
'CrystalClear-SM Expert 2.1 b29 (Rigaku, 2013)'
_computing_data_reduction        'CrystalClear-SM Expert 2.1 b29'
_computing_molecular_graphics    'CrystalStructure 4.1'
_computing_publication_material  'CrystalStructure 4.1 (Rigaku, 2014)'
_computing_structure_refinement  'SHELXL2013 (Sheldrick, 2008)'
_computing_structure_solution    'Il Milione (Burla, et al., 2007)'
_diffrn_ambient_temperature      93
_diffrn_detector_area_resol_mean 5.814
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Rigaku XtaLAB P200'
_diffrn_measurement_method       ω
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71075
_diffrn_reflns_av_R_equivalents  0.0542
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_h_min       -24
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            24638
_diffrn_reflns_point_group_measured_fraction_full 0.994
_diffrn_reflns_point_group_measured_fraction_max 0.982
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.494
_diffrn_reflns_theta_min         3.176
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    0.809
_exptl_absorpt_correction_T_max  0.984
_exptl_absorpt_correction_T_min  0.863
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'REQAB (Rigaku, 1998)'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.568
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             1448.00
_exptl_crystal_size_max          0.130
_exptl_crystal_size_mid          0.070
_exptl_crystal_size_min          0.020
_refine_diff_density_max         2.27
_refine_diff_density_min         -0.82
_refine_ls_abs_structure_details
;
 Flack x determined using 2004 quotients [(I+)-(I-)]/[(I+)+(I-)]
 (Parsons and Flack (2004), Acta Cryst. A60, s61).
;
_refine_ls_abs_structure_Flack   0.022(15)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.066
_refine_ls_hydrogen_treatment    constr
_refine_ls_number_parameters     397
_refine_ls_number_reflns         6764
_refine_ls_number_restraints     67
_refine_ls_R_factor_all          0.0713
_refine_ls_R_factor_gt           0.0461
_refine_ls_shift/su_max          0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[σ²(Fo²)+(0.0278P)²+5.7829P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0832
_refine_ls_wR_factor_ref         0.0906
_reflns_number_gt                5242
_reflns_number_total             6764
_reflns_threshold_expression     F²>2.0σ(F²)
_cod_data_source_file            c7ce00640c2.cif
_cod_data_source_block           mfu106-2e-2
_cod_database_code               7228233
loop_
_symmetry_equiv_pos_site_id
_space_group_symop_operation_xyz
1 +X,+Y,+Z
2 1/2-X,1/2+Y,1/2+Z
3 1/2+X,1/2-Y,+Z
4 -X,-Y,1/2+Z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 0.79824(2) 0.97361(3) 0.34739(4) 0.02012(12) Uani 1 4 d .
Cl1 Cl 0.63130(8) 0.97519(14) 0.20734(13) 0.0223(3) Uani 1 4 d .
O1 O 0.6621(3) 1.0599(4) 0.2577(4) 0.0338(13) Uani 1 4 d .
O2 O 0.5552(3) 0.9747(5) 0.2258(6) 0.0519(17) Uani 1 4 d .
O3 O 0.6463(3) 0.9737(5) 0.0846(4) 0.0341(13) Uani 1 4 d .
O4 O 0.6640(3) 0.8946(4) 0.2632(4) 0.0292(12) Uani 1 4 d .
O5 O 0.8793(3) 0.7702(5) 0.4245(5) 0.0458(16) Uani 1 4 d .
O6 O 0.9001(5) 1.1928(6) 0.4247(7) 0.080(3) Uani 1 4 d .
N1 N 0.8142(3) 0.9748(5) 0.1590(6) 0.0149(13) Uani 1 4 d .
N2 N 0.8004(3) 0.9769(5) -0.4642(7) 0.0155(12) Uani 1 4 d .
C1 C 0.8105(5) 0.7227(5) 0.1056(6) 0.0320(19) Uani 1 4 d .
C2 C 0.8121(4) 0.8062(5) 0.1631(6) 0.0239(16) Uani 1 4 d .
C3 C 0.8124(3) 0.8929(5) 0.1002(5) 0.0159(14) Uani 1 4 d .
C4 C 0.8101(3) 0.8908(5) -0.0253(5) 0.0145(14) Uani 1 4 d .
C5 C 0.8084(4) 0.8002(5) -0.0826(6) 0.0247(16) Uani 1 4 d .
C6 C 0.8085(5) 0.7197(5) -0.0189(6) 0.0329(19) Uani 1 4 d .
C7 C 0.8104(4) 0.9775(7) -0.0853(7) 0.0143(17) Uani 1 4 d .
C8 C 0.8132(3) 1.0622(5) -0.0248(5) 0.0150(14) Uani 1 4 d .
C9 C 0.8153(4) 1.1517(5) -0.0814(5) 0.0215(16) Uani 1 4 d .
C10 C 0.8200(4) 1.2328(6) -0.0179(6) 0.0282(17) Uani 1 4 d .
C11 C 0.8218(4) 1.2278(5) 0.1073(6) 0.0275(17) Uani 1 4 d .
C12 C 0.8193(4) 1.1446(5) 0.1643(6) 0.0200(15) Uani 1 4 d .
C13 C 0.8144(3) 1.0581(5) 0.1004(5) 0.0134(13) Uani 1 4 d .
C14 C 0.8069(4) 0.9738(6) -0.2161(7) 0.0127(15) Uani 1 4 d .
C15 C 0.8708(3) 0.9713(5) -0.2833(5) 0.0178(11) Uani 1 4 d .
C16 C 0.8653(3) 0.9717(5) -0.4088(5) 0.0165(11) Uani 1 4 d .
C17 C 0.7387(3) 0.9783(5) -0.4002(5) 0.0144(11) Uani 1 4 d .
C18 C 0.7404(3) 0.9799(5) -0.2736(5) 0.0134(10) Uani 1 4 d .
C19 C 0.6739(3) 0.9844(5) -0.2111(5) 0.0172(13) Uani 1 4 d .
C20 C 0.6099(3) 0.9880(5) -0.2703(6) 0.0181(14) Uani 1 4 d .
C21 C 0.6080(4) 0.9867(5) -0.3941(6) 0.0180(15) Uani 1 4 d .
C22 C 0.6707(4) 0.9818(5) -0.4566(5) 0.0164(13) Uani 1 4 d .
C23 C 0.9406(3) 0.9634(6) -0.2316(5) 0.0236(16) Uani 1 4 d .
C24 C 1.0007(4) 0.9588(6) -0.2982(6) 0.0319(19) Uani 1 4 d .
C25 C 0.9956(4) 0.9614(6) -0.4223(6) 0.033(2) Uani 1 4 d .
C26 C 0.9299(4) 0.9668(6) -0.4757(6) 0.0252(15) Uani 1 4 d .
C27 C 0.8742(5) 0.7239(7) 0.5359(7) 0.044(2) Uani 1 4 d .
C28 C 0.9520(6) 0.6985(9) 0.5686(10) 0.070(4) Uani 1 4 d .
C29 C 0.9830(6) 0.6771(11) 0.4501(10) 0.081(4) Uani 1 4 d .
C30 C 0.9449(5) 0.7408(7) 0.3701(7) 0.049(3) Uani 1 4 d .
C31 C 0.8951(13) 1.2183(9) 0.5475(15) 0.147(9) Uani 1 4 d .
C32 C 0.9774(13) 1.2568(13) 0.5615(17) 0.162(10) Uani 1 4 d .
C33 C 0.9843(8) 1.3103(16) 0.450(2) 0.145(8) Uani 1 4 d .
C34 C 0.9450(10) 1.2532(10) 0.3804(13) 0.103(6) Uani 1 4 d .
H1 H 0.81074 0.66541 0.14879 0.0384 Uiso 1 4 calc R
H2 H 0.81313 0.80691 0.24614 0.0287 Uiso 1 4 calc R
H5 H 0.80715 0.79702 -0.1656 0.0296 Uiso 1 4 calc R
H6 H 0.80728 0.66044 -0.05769 0.0395 Uiso 1 4 calc R
H9 H 0.81342 1.15488 -0.1643 0.0258 Uiso 1 4 calc R
H10 H 0.82213 1.29222 -0.0563 0.0338 Uiso 1 4 calc R
H11 H 0.82488 1.28464 0.15123 0.0330 Uiso 1 4 calc R
H12 H 0.8207 1.14337 0.24736 0.0239 Uiso 1 4 calc R
H19 H 0.67412 0.98497 -0.12804 0.0207 Uiso 1 4 calc R
H20 H 0.56588 0.9914 -0.22769 0.0218 Uiso 1 4 calc R
H21 H 0.56296 0.98914 -0.43384 0.0216 Uiso 1 4 calc R
H22 H 0.66872 0.98083 -0.53958 0.0196 Uiso 1 4 calc R
H23 H 0.94498 0.9614 -0.14882 0.0284 Uiso 1 4 calc R
H24 H 1.04672 0.95372 -0.26201 0.0382 Uiso 1 4 calc R
H25 H 1.03824 0.9593 -0.46829 0.0396 Uiso 1 4 calc R
H26 H 0.9273 0.96729 -0.55867 0.0302 Uiso 1 4 calc R
H27A H 0.844 0.66644 0.53013 0.0529 Uiso 1 4 calc R
H27B H 0.85278 0.76666 0.595 0.0529 Uiso 1 4 calc R
H28A H 0.9771 0.75212 0.60639 0.0841 Uiso 1 4 calc R
H28B H 0.95387 0.64276 0.62072 0.0841 Uiso 1 4 calc R
H29A H 1.03563 0.68947 0.44872 0.0972 Uiso 1 4 calc R
H29B H 0.97441 0.61036 0.42855 0.0972 Uiso 1 4 calc R
H30A H 0.97537 0.79647 0.35259 0.0585 Uiso 1 4 calc R
H30B H 0.93422 0.70788 0.29574 0.0585 Uiso 1 4 calc R
H31A H 0.88524 1.16305 0.59808 0.1766 Uiso 1 4 calc R
H31B H 0.85879 1.26817 0.56183 0.1766 Uiso 1 4 calc R
H32A H 0.9827 1.29832 0.63064 0.1938 Uiso 1 4 calc R
H32B H 1.01264 1.20442 0.56639 0.1938 Uiso 1 4 calc R
H33A H 0.96315 1.3743 0.45582 0.1734 Uiso 1 4 calc R
H33B H 1.03515 1.31488 0.42383 0.1734 Uiso 1 4 calc R
H34A H 0.91701 1.29432 0.32694 0.1239 Uiso 1 4 calc R
H34B H 0.97939 1.21729 0.33134 0.1239 Uiso 1 4 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016
;
International Tables for Crystallography
(Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
H H 0.0000 0.0000
;
International Tables for Crystallography
(Vol. C, Table 6.1.1.4)
;
Ag Ag -0.8971 1.1015
;
International Tables for Crystallography
(Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
Cl Cl 0.1484 0.1585
;
International Tables for Crystallography
(Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
N N 0.0061 0.0033
;
International Tables for Crystallography
(Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
O O 0.0106 0.0060
;
International Tables for Crystallography
(Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_publ_flag
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N1 Ag1 N2 171.0(2) yes . 1_556
O1 Cl1 O2 109.6(4) yes . .
O1 Cl1 O3 109.0(3) yes . .
O1 Cl1 O4 108.4(3) yes . .
O2 Cl1 O3 109.7(4) yes . .
O2 Cl1 O4 110.2(4) yes . .
O3 Cl1 O4 110.0(3) yes . .
C27 O5 C30 108.0(7) yes . .
C31 O6 C34 104.8(11) yes . .
Ag1 N1 C3 119.1(5) yes . .
Ag1 N1 C13 119.7(5) yes . .
C3 N1 C13 120.3(6) yes . .
Ag1 N2 C16 118.7(5) yes 1_554 .
Ag1 N2 C17 121.6(5) yes 1_554 .
C16 N2 C17 119.6(7) yes . .
C2 C1 C6 120.8(7) yes . .
C1 C2 C3 120.6(6) yes . .
N1 C3 C2 119.5(6) yes . .
N1 C3 C4 121.3(6) yes . .
C2 C3 C4 119.1(6) yes . .
C3 C4 C5 118.3(6) yes . .
C3 C4 C7 118.0(6) yes . .
C5 C4 C7 123.7(6) yes . .
C4 C5 C6 120.3(6) yes . .
C1 C6 C5 120.9(7) yes . .
C4 C7 C8 120.8(7) yes . .
C4 C7 C14 117.2(8) yes . .
C8 C7 C14 122.0(8) yes . .
C7 C8 C9 123.0(6) yes . .
C7 C8 C13 117.7(6) yes . .
C9 C8 C13 119.3(6) yes . .
C8 C9 C10 120.8(6) yes . .
C9 C10 C11 119.5(7) yes . .
C10 C11 C12 121.6(7) yes . .
C11 C12 C13 120.3(6) yes . .
N1 C13 C8 121.9(6) yes . .
N1 C13 C12 119.6(6) yes . .
C8 C13 C12 118.5(6) yes . .
C7 C14 C15 120.5(7) yes . .
C7 C14 C18 120.4(7) yes . .
C15 C14 C18 118.9(7) yes . .
C14 C15 C16 118.9(6) yes . .
C14 C15 C23 122.5(6) yes . .
C16 C15 C23 118.5(5) yes . .
N2 C16 C15 121.7(6) yes . .
N2 C16 C26 119.8(6) yes . .
C15 C16 C26 118.5(5) yes . .
N2 C17 C18 121.4(6) yes . .
N2 C17 C22 120.3(6) yes . .
C18 C17 C22 118.3(5) yes . .
C14 C18 C17 119.2(6) yes . .
C14 C18 C19 121.8(6) yes . .
C17 C18 C19 118.9(5) yes . .
C18 C19 C20 120.2(6) yes . .
C19 C20 C21 121.0(6) yes . .
C20 C21 C22 120.2(6) yes . .
C17 C22 C21 121.4(6) yes . .
C15 C23 C24 121.1(6) yes . .
C23 C24 C25 120.4(6) yes . .
C24 C25 C26 120.6(6) yes . .
C16 C26 C25 120.8(6) yes . .
O5 C27 C28 105.2(8) yes . .
C27 C28 C29 100.8(9) yes . .
C28 C29 C30 104.7(10) yes . .
O5 C30 C29 108.6(7) yes . .
O6 C31 C32 96.9(14) yes . .
C31 C32 C33 99.6(15) yes . .
C32 C33 C34 98.8(16) yes . .
O6 C34 C33 120.7(15) yes . .
C2 C1 H1 119.615 no . .
C6 C1 H1 119.609 no . .
C1 C2 H2 119.697 no . .
C3 C2 H2 119.712 no . .
C4 C5 H5 119.830 no . .
C6 C5 H5 119.833 no . .
C1 C6 H6 119.558 no . .
C5 C6 H6 119.565 no . .
C8 C9 H9 119.617 no . .
C10 C9 H9 119.622 no . .
C9 C10 H10 120.261 no . .
C11 C10 H10 120.253 no . .
C10 C11 H11 119.180 no . .
C12 C11 H11 119.177 no . .
C11 C12 H12 119.838 no . .
C13 C12 H12 119.841 no . .
C18 C19 H19 119.891 no . .
C20 C19 H19 119.884 no . .
C19 C20 H20 119.482 no . .
C21 C20 H20 119.490 no . .
C20 C21 H21 119.911 no . .
C22 C21 H21 119.915 no . .
C17 C22 H22 119.313 no . .
C21 C22 H22 119.306 no . .
C15 C23 H23 119.448 no . .
C24 C23 H23 119.432 no . .
C23 C24 H24 119.773 no . .
C25 C24 H24 119.784 no . .
C24 C25 H25 119.719 no . .
C26 C25 H25 119.723 no . .
C16 C26 H26 119.591 no . .
C25 C26 H26 119.582 no . .
O5 C27 H27A 110.704 no . .
O5 C27 H27B 110.704 no . .
C28 C27 H27A 110.699 no . .
C28 C27 H27B 110.710 no . .
H27A C27 H27B 108.799 no . .
C27 C28 H28A 111.609 no . .
C27 C28 H28B 111.623 no . .
C29 C28 H28A 111.610 no . .
C29 C28 H28B 111.616 no . .
H28A C28 H28B 109.403 no . .
C28 C29 H29A 110.808 no . .
C28 C29 H29B 110.807 no . .
C30 C29 H29A 110.815 no . .
C30 C29 H29B 110.807 no . .
H29A C29 H29B 108.873 no . .
O5 C30 H30A 109.980 no . .
O5 C30 H30B 109.987 no . .
C29 C30 H30A 109.982 no . .
C29 C30 H30B 109.982 no . .
H30A C30 H30B 108.354 no . .
O6 C31 H31A 112.383 no . .
O6 C31 H31B 112.390 no . .
C32 C31 H31A 112.376 no . .
C32 C31 H31B 112.379 no . .
H31A C31 H31B 109.951 no . .
C31 C32 H32A 111.851 no . .
C31 C32 H32B 111.851 no . .
C33 C32 H32A 111.851 no . .
C33 C32 H32B 111.853 no . .
H32A C32 H32B 109.560 no . .
C32 C33 H33A 112.002 no . .
C32 C33 H33B 112.003 no . .
C34 C33 H33A 112.006 no . .
C34 C33 H33B 112.001 no . .
H33A C33 H33B 109.662 no . .
O6 C34 H34A 107.145 no . .
O6 C34 H34B 107.138 no . .
C33 C34 H34A 107.132 no . .
C33 C34 H34B 107.142 no . .
H34A C34 H34B 106.814 no . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_publ_flag
_geom_bond_site_symmetry_2
Ag1 N1 2.175(7) yes .
Ag1 N2 2.155(8) yes 1_556
Cl1 O1 1.449(6) yes .
Cl1 O2 1.426(5) yes .
Cl1 O3 1.431(5) yes .
Cl1 O4 1.441(6) yes .
O5 C27 1.436(10) yes .
O5 C30 1.426(11) yes .
O6 C31 1.452(19) yes .
O6 C34 1.296(19) yes .
N1 C3 1.341(10) yes .
N1 C13 1.357(10) yes .
N2 C16 1.361(9) yes .
N2 C17 1.356(9) yes .
C1 C2 1.353(10) yes .
C1 C6 1.425(10) yes .
C2 C3 1.424(10) yes .
C3 C4 1.435(8) yes .
C4 C5 1.441(10) yes .
C4 C7 1.407(12) yes .
C5 C6 1.353(10) yes .
C7 C8 1.385(12) yes .
C7 C14 1.497(11) yes .
C8 C9 1.424(10) yes .
C8 C13 1.434(8) yes .
C9 C10 1.361(10) yes .
C10 C11 1.434(10) yes .
C11 C12 1.349(10) yes .
C12 C13 1.429(9) yes .
C14 C15 1.411(10) yes .
C14 C18 1.399(10) yes .
C15 C16 1.439(8) yes .
C15 C23 1.427(9) yes .
C16 C26 1.421(9) yes .
C17 C18 1.448(8) yes .
C17 C22 1.415(9) yes .
C18 C19 1.425(8) yes .
C19 C20 1.366(9) yes .
C20 C21 1.417(9) yes .
C21 C22 1.366(9) yes .
C23 C24 1.350(9) yes .
C24 C25 1.422(10) yes .
C25 C26 1.362(9) yes .
C27 C28 1.531(15) yes .
C28 C29 1.503(16) yes .
C29 C30 1.466(16) yes .
C31 C32 1.63(3) yes .
C32 C33 1.49(3) yes .
C33 C34 1.35(3) yes .
C1 H1 0.950 no .
C2 H2 0.950 no .
C5 H5 0.950 no .
C6 H6 0.950 no .
C9 H9 0.950 no .
C10 H10 0.950 no .
C11 H11 0.950 no .
C12 H12 0.950 no .
C19 H19 0.950 no .
C20 H20 0.950 no .
C21 H21 0.950 no .
C22 H22 0.950 no .
C23 H23 0.950 no .
C24 H24 0.950 no .
C25 H25 0.950 no .
C26 H26 0.950 no .
C27 H27A 0.990 no .
C27 H27B 0.990 no .
C28 H28A 0.990 no .
C28 H28B 0.990 no .
C29 H29A 0.990 no .
C29 H29B 0.990 no .
C30 H30A 0.990 no .
C30 H30B 0.990 no .
C31 H31A 0.990 no .
C31 H31B 0.990 no .
C32 H32A 0.990 no .
C32 H32B 0.990 no .
C33 H33A 0.990 no .
C33 H33B 0.990 no .
C34 H34A 0.990 no .
C34 H34B 0.990 no .
loop_
_geom_contact_atom_site_label_1
_geom_contact_atom_site_label_2
_geom_contact_distance
_geom_contact_publ_flag
_geom_contact_site_symmetry_2
Ag1 C2 3.183(7) no .
Ag1 C12 3.224(7) no .
Ag1 C22 3.257(6) no 1_556
Ag1 C26 3.170(6) no 1_556
N1 C7 2.795(10) no .
N1 C24 3.588(9) no 4_775
N2 C14 2.840(11) no .
C1 C4 2.813(10) no .
C1 C17 3.580(11) no 2_645
C1 C22 3.502(10) no 2_645
C2 C5 2.812(9) no .
C3 C6 2.807(10) no .
C3 C8 2.791(9) no .
C4 C13 2.773(9) no .
C4 C15 3.356(8) no .
C4 C18 3.365(8) no .
C4 C19 3.555(9) no .
C4 C23 3.530(9) no .
C5 C14 2.894(11) no .
C5 C15 3.531(10) no .
C5 C18 3.582(9) no .
C6 C22 3.466(10) no 2_645
C7 C19 2.909(10) no .
C7 C23 2.942(10) no .
C8 C11 2.796(10) no .
C8 C15 3.395(8) no .
C8 C18 3.357(8) no .
C8 C19 3.522(9) no .
C9 C12 2.812(9) no .
C9 C14 2.957(11) no .
C9 C15 3.594(9) no .
C9 C18 3.561(9) no .
C10 C13 2.822(10) no .
C13 C25 3.540(9) no 4_775
C15 C17 2.789(8) no .
C15 C25 2.808(9) no .
C16 C18 2.785(8) no .
C16 C24 2.814(9) no .
C17 C20 2.814(9) no .
C18 C21 2.814(9) no .
C19 C22 2.807(9) no .
C23 C26 2.799(9) no .
Ag1 Cl1 3.4814(16) no .
Ag1 O1 2.983(6) no .
Ag1 O4 2.892(5) no .
Ag1 O5 3.366(7) no .
Cl1 Ag1 3.4814(16) no .
Cl1 N1 3.432(5) no .
O1 Ag1 2.983(6) no .
O1 N1 3.265(8) no .
O1 C6 3.456(9) no 2_655
O1 C12 3.323(9) no .
O1 C13 3.344(8) no .
O1 C22 3.453(8) no 1_556
O1 C27 3.505(10) no 2_654
O2 C20 3.101(8) no 4_675
O2 C21 3.362(9) no 4_675
O3 N1 3.224(8) no .
O3 C3 3.287(8) no .
O3 C4 3.488(8) no .
O3 C8 3.563(8) no .
O3 C13 3.339(8) no .
O3 C19 3.423(8) no .
O4 Ag1 2.892(5) no .
O4 N1 3.232(8) no .
O4 C2 3.226(9) no .
O4 C3 3.320(8) no .
O4 C10 3.407(9) no 2_645
O4 C22 3.437(8) no 1_556
O5 Ag1 3.366(7) no .
O5 N2 3.511(10) no 1_556
O5 C2 3.277(9) no .
O5 C16 3.442(9) no 1_556
O5 C26 3.153(10) no 1_556
O6 C12 3.402(11) no .
O6 C26 3.443(12) no 1_556
N1 Cl1 3.432(5) no .
N1 O1 3.265(8) no .
N1 O3 3.224(8) no .
N1 O4 3.232(8) no .
N2 O5 3.511(10) no 1_554
C2 O4 3.226(9) no .
C2 O5 3.277(9) no .
C2 C30 3.536(11) no .
C3 O3 3.287(8) no .
C3 O4 3.320(8) no .
C4 O3 3.488(8) no .
C6 O1 3.456(9) no 2_644
C8 O3 3.563(8) no .
C10 O4 3.407(9) no 2_654
C12 O1 3.323(9) no .
C12 O6 3.402(11) no .
C13 O1 3.344(8) no .
C13 O3 3.339(8) no .
C16 O5 3.442(9) no 1_554
C16 C27 3.570(12) no 1_554
C16 C31 3.571(15) no 1_554
C19 O3 3.423(8) no .
C20 O2 3.101(8) no 4_674
C21 O2 3.362(9) no 4_674
C22 O1 3.453(8) no 1_554
C22 O4 3.437(8) no 1_554
C26 O5 3.153(10) no 1_554
C26 O6 3.443(12) no 1_554
C26 C27 3.594(12) no 1_554
C27 O1 3.505(10) no 2_645
C27 C16 3.570(12) no 1_556
C27 C26 3.594(12) no 1_556
C30 C2 3.536(11) no .
C31 C16 3.571(15) no 1_556
Ag1 H2 2.6442 no .
Ag1 H6 3.4640 no 2_655
Ag1 H10 3.5752 no 2_645
Ag1 H12 2.6951 no .
Ag1 H22 2.7263 no 1_556
Ag1 H24 3.2964 no 4_775
Ag1 H26 2.6216 no 1_556
O5 H28A 2.7701 no .
O5 H28B 3.1939 no .
O5 H29A 3.1250 no .
O5 H29B 2.8688 no .
O6 H32A 3.1804 no .
O6 H32B 2.6442 no .
O6 H33A 2.8455 no .
O6 H33B 3.0399 no .
N1 H2 2.5782 no .
N1 H12 2.5960 no .
N1 H24 2.9111 no 4_775
N1 H25 3.2335 no 4_775
N2 H6 3.4464 no 2_654
N2 H22 2.5860 no .
N2 H26 2.5907 no .
C1 H5 3.2754 no .
C2 H6 3.2621 no .
C3 H1 3.2704 no .
C3 H5 3.3299 no .
C3 H25 3.5562 no 4_775
C4 H2 3.3238 no .
C4 H6 3.2847 no .
C4 H19 3.0826 no .
C4 H23 3.0379 no .
C4 H25 3.5797 no 4_775
C5 H1 3.2636 no .
C5 H23 3.4901 no .
C6 H2 3.2735 no .
C6 H22 3.4183 no 2_645
C7 H5 2.7170 no .
C7 H9 2.6703 no .
C7 H19 2.5722 no .
C7 H23 2.6057 no .
C7 H25 3.2325 no 4_775
C8 H10 3.2827 no .
C8 H12 3.3210 no .
C8 H19 3.0369 no .
C8 H23 3.1620 no .
C8 H25 2.8416 no 4_775
C9 H11 3.2634 no .
C9 H19 3.5637 no .
C9 H25 3.3905 no 4_775
C10 H12 3.2870 no .
C10 H22 3.5282 no 2_655
C11 H9 3.2768 no .
C12 H10 3.2773 no .
C12 H24 2.9675 no 4_775
C12 H25 3.3802 no 4_775
C13 H9 3.3228 no .
C13 H11 3.2669 no .
C13 H24 3.0193 no 4_775
C13 H25 2.8504 no 4_775
C14 H5 2.5703 no .
C14 H9 2.6347 no .
C14 H19 2.6613 no .
C14 H23 2.6760 no .
C15 H5 3.0483 no .
C15 H9 3.1214 no .
C15 H24 3.2762 no .
C15 H26 3.3186 no .
C16 H23 3.3220 no .
C16 H25 3.2778 no .
C17 H1 2.8594 no 2_654
C17 H6 3.2590 no 2_654
C17 H10 3.3767 no 2_644
C17 H11 3.0429 no 2_644
C17 H19 3.3355 no .
C17 H21 3.2805 no .
C18 H1 2.9311 no 2_654
C18 H5 3.1243 no .
C18 H9 3.0883 no .
C18 H11 3.1378 no 2_644
C18 H20 3.2777 no .
C18 H22 3.3180 no .
C19 H1 3.0364 no 2_654
C19 H9 3.5764 no .
C19 H11 3.2381 no 2_644
C19 H21 3.2726 no .
C20 H1 3.0553 no 2_654
C20 H11 3.2500 no 2_644
C20 H22 3.2680 no .
C21 H1 2.9860 no 2_654
C21 H6 3.4668 no 2_654
C21 H10 3.5635 no 2_644
C21 H11 3.1627 no 2_644
C21 H19 3.2796 no .
C22 H1 2.8862 no 2_654
C22 H6 2.8111 no 2_654
C22 H10 2.9210 no 2_644
C22 H11 3.0543 no 2_644
C22 H20 3.2616 no .
C23 H5 3.4978 no .
C23 H25 3.2550 no .
C23 H25 3.2270 no 4_775
C23 H26 3.2940 no 4_775
C24 H26 3.2757 no .
C24 H26 3.2213 no 4_775
C25 H23 3.2639 no .
C25 H23 3.0198 no 4_774
C26 H23 3.2124 no 4_774
C26 H24 3.2682 no .
C26 H24 3.4889 no 4_774
C27 H29A 3.1889 no .
C27 H29B 2.7458 no .
C27 H30A 2.9930 no .
C27 H30B 2.9710 no .
C28 H30A 2.8659 no .
C28 H30B 3.1398 no .
C29 H27A 2.7362 no .
C29 H27B 3.1891 no .
C30 H27A 2.8189 no .
C30 H27B 3.1070 no .
C30 H28A 2.7711 no .
C30 H28B 3.1885 no .
C31 H33A 2.7512 no .
C31 H33B 3.2546 no .
C31 H34A 2.7717 no .
C31 H34B 2.9224 no .
C32 H34A 2.9542 no .
C32 H34B 2.6912 no .
C33 H31A 3.2529 no .
C33 H31B 2.7189 no .
C34 H31A 3.0083 no .
C34 H31B 2.6257 no .
C34 H32A 3.0139 no .
C34 H32B 2.5635 no .
H1 H2 2.2931 no .
H1 H6 2.3628 no .
H1 H9 3.1425 no 2_645
H1 H21 3.5491 no 2_645
H1 H22 3.4087 no 2_645
H2 H9 3.3432 no 2_645
H2 H10 3.3792 no 2_645
H5 H6 2.2946 no .
H5 H11 3.2240 no 2_644
H5 H12 3.3663 no 2_644
H5 H23 3.4601 no .
H6 H12 3.2624 no 2_644
H6 H22 2.5910 no 2_645
H9 H10 2.3099 no .
H9 H19 3.5522 no .
H10 H11 2.3759 no .
H10 H22 2.6838 no 2_655
H11 H12 2.2844 no .
H11 H22 3.5351 no 2_655
H12 H24 2.8160 no 4_775
H19 H20 2.3073 no .
H20 H21 2.3579 no .
H21 H22 2.3045 no .
H23 H24 2.2882 no .
H23 H25 2.3705 no 4_775
H23 H26 2.7705 no 4_775
H24 H25 2.3651 no .
H24 H26 2.6247 no 4_775
H25 H26 2.3023 no .
H27A H28A 2.8823 no .
H27A H28B 2.3075 no .
H27A H29B 2.7949 no .
H27A H30B 3.2121 no .
H27B H28A 2.3149 no .
H27B H28B 2.5827 no .
H28A H29A 2.2830 no .
H28A H29B 2.8582 no .
H28A H30A 2.9693 no .
H28B H29A 2.5685 no .
H28B H29B 2.2767 no .
H29A H30A 2.1795 no .
H29A H30B 2.5795 no .
H29B H30A 2.7757 no .
H29B H30B 2.1836 no .
H31A H32A 2.6584 no .
H31A H32B 2.4576 no .
H31A H34B 3.5960 no .
H31B H32A 2.4629 no .
H31B H32B 2.9890 no .
H31B H33A 2.7319 no .
H31B H34A 2.9176 no .
H31B H34B 3.5287 no .
H32A H33A 2.2989 no .
H32A H33B 2.5671 no .
H32B H33A 2.8686 no .
H32B H33B 2.2976 no .
H32B H34A 3.5004 no .
H32B H34B 2.7632 no .
H33A H34A 2.0457 no .
H33A H34B 2.6576 no .
H33B H34A 2.4693 no .
H33B H34B 2.0237 no .
Cl1 H22 2.9766 no 1_556
Cl1 H27A 3.4137 no 2_654
Cl1 H28B 3.0170 no 2_654
Cl1 H31B 3.3765 no 2_644
Cl1 H32A 3.3915 no 2_644
O1 H5 3.5170 no 2_655
O1 H6 2.6080 no 2_655
O1 H12 3.1673 no .
O1 H22 2.5773 no 1_556
O1 H27A 3.0100 no 2_654
O1 H27B 3.4801 no 2_654
O1 H28B 2.9058 no 2_654
O1 H33B 3.5042 no 3_475
O2 H20 2.3528 no 4_675
O2 H21 2.8944 no 4_675
O2 H22 3.4097 no 1_556
O2 H28B 2.6716 no 2_654
O2 H29A 3.4693 no 3_465
O2 H29B 3.0102 no 3_465
O2 H30B 3.5134 no 3_465
O2 H32A 2.8140 no 2_644
O2 H33A 3.4158 no 2_644
O3 H19 2.4906 no .
O3 H27A 2.8057 no 2_654
O3 H28B 3.0564 no 2_654
O3 H29B 3.4530 no 2_654
O3 H31B 2.9249 no 2_644
O3 H32A 3.4862 no 2_644
O3 H33A 2.8735 no 2_644
O4 H2 3.0344 no .
O4 H9 3.5201 no 2_645
O4 H10 2.5356 no 2_645
O4 H22 2.5665 no 1_556
O4 H29A 3.4010 no 3_465
O4 H31B 2.9468 no 2_644
O4 H32A 3.3959 no 2_644
O5 H2 2.4348 no .
O5 H26 2.9366 no 1_556
O6 H12 2.6011 no .
O6 H24 3.1363 no 4_775
O6 H26 3.2396 no 1_556
N2 H27B 3.2039 no 1_554
N2 H31A 3.1519 no 1_554
C1 H30B 3.1648 no .
C1 H31B 3.2396 no 2_644
C1 H32B 3.4623 no 4_774
C1 H33B 3.5734 no 4_774
C2 H30B 3.0578 no .
C2 H31B 3.4129 no 2_644
C2 H32B 3.4310 no 4_774
C3 H32B 3.5425 no 4_774
C5 H31B 3.5382 no 2_644
C5 H33B 3.3251 no 4_774
C6 H31B 3.3048 no 2_644
C6 H33B 3.0079 no 4_774
C8 H27A 3.3246 no 2_654
C9 H27A 3.2207 no 2_654
C9 H29A 3.5772 no 4_774
C10 H27A 3.2267 no 2_654
C10 H27B 3.4839 no 2_654
C10 H29A 2.9155 no 4_774
C11 H27A 3.3111 no 2_654
C11 H27B 3.2825 no 2_654
C11 H29A 3.4100 no 4_774
C11 H34A 3.2093 no .
C12 H27A 3.4043 no 2_654
C12 H34A 3.3517 no .
C13 H27A 3.4063 no 2_654
C15 H27B 3.2325 no 1_554
C15 H31A 3.0481 no 1_554
C16 H27B 2.9143 no 1_554
C16 H31A 2.7363 no 1_554
C19 H33A 3.5380 no 2_644
C19 H34A 3.2053 no 2_644
C20 H29B 3.2570 no 2_654
C20 H30B 3.3073 no 2_654
C20 H33A 3.3322 no 2_644
C20 H34A 3.0014 no 2_644
C21 H28B 3.3962 no 3_464
C21 H29A 3.3539 no 3_464
C21 H29B 3.4811 no 3_464
C23 H28A 3.5841 no 1_554
C23 H31A 3.5838 no 1_554
C23 H34B 3.0432 no 4_774
C24 H28A 3.1541 no 1_554
C24 H34B 2.9239 no 4_774
C25 H28A 3.0015 no 1_554
C25 H30A 3.4959 no 1_554
C25 H31A 3.5197 no 1_554
C25 H32B 3.4599 no 1_554
C26 H27B 3.2757 no 1_554
C26 H28A 3.3001 no 1_554
C26 H30A 3.2224 no 1_554
C26 H31A 3.0207 no 1_554
C28 H21 3.3600 no 3_566
C28 H34B 3.4734 no 4_775
C29 H20 3.4455 no 2_645
C29 H21 3.0819 no 3_566
C30 H2 2.9729 no .
C30 H26 3.3256 no 1_556
C30 H32A 3.0990 no 4_774
C32 H30A 3.5226 no 4_775
C32 H30B 3.1783 no 4_775
C33 H20 3.4020 no 2_655
C33 H21 3.4578 no 3_576
C34 H11 3.4652 no .
C34 H12 3.1669 no .
C34 H20 3.5985 no 2_655
C34 H24 3.3568 no 4_775
C34 H28A 3.4502 no 4_774
H1 H30B 2.9005 no .
H2 O4 3.0344 no .
H2 O5 2.4348 no .
H2 C30 2.9729 no .
H2 H30A 3.2447 no .
H2 H30B 2.7050 no .
H5 O1 3.5170 no 2_644
H5 H27B 2.8968 no 1_554
H5 H33B 3.4764 no 4_774
H6 O1 2.6080 no 2_644
H6 H33B 2.9462 no 4_774
H9 O4 3.5201 no 2_654
H9 H31A 3.0272 no 1_554
H10 O4 2.5356 no 2_654
H10 H29A 2.6472 no 4_774
H11 C34 3.4652 no .
H11 H27B 3.3616 no 2_654
H11 H29A 3.4882 no 4_774
H11 H34A 2.6392 no .
H12 O1 3.1673 no .
H12 O6 2.6011 no .
H12 C34 3.1669 no .
H12 H34A 2.9292 no .
H12 H34B 3.2639 no .
H19 O3 2.4906 no .
H19 H27A 3.1608 no 2_654
H19 H29B 3.3373 no 2_654
H19 H33A 3.1365 no 2_644
H19 H34A 3.2257 no 2_644
H20 O2 2.3528 no 4_674
H20 C29 3.4455 no 2_654
H20 C33 3.4020 no 2_644
H20 C34 3.5985 no 2_644
H20 H28B 3.3042 no 3_464
H20 H29B 2.5666 no 2_654
H20 H30B 3.0781 no 2_654
H20 H33A 2.7282 no 2_644
H20 H33B 3.5712 no 2_644
H20 H34A 2.8782 no 2_644
H21 O2 2.8944 no 4_674
H21 C28 3.3600 no 3_464
H21 C29 3.0819 no 3_464
H21 C33 3.4578 no 3_474
H21 H28B 2.8214 no 3_464
H21 H29A 2.9086 no 3_464
H21 H29B 2.6741 no 3_464
H21 H32A 3.4375 no 3_474
H21 H33A 2.9579 no 3_474
H21 H33B 3.2588 no 3_474
H22 Cl1 2.9766 no 1_554
H22 O1 2.5773 no 1_554
H22 O2 3.4097 no 1_554
H22 O4 2.5665 no 1_554
H22 H29A 3.4511 no 3_464
H23 H32B 3.4911 no 4_774
H23 H34B 2.9016 no 4_774
H24 O6 3.1363 no 4_774
H24 C34 3.3568 no 4_774
H24 H28A 3.4758 no 1_554
H24 H34B 2.6909 no 4_774
H25 H28A 3.2593 no 1_554
H25 H30A 3.2969 no 1_554
H25 H32B 3.5267 no 1_554
H26 O5 2.9366 no 1_554
H26 O6 3.2396 no 1_554
H26 C30 3.3256 no 1_554
H26 H30A 2.7707 no 1_554
H26 H31A 3.3923 no 1_554
H27A Cl1 3.4137 no 2_645
H27A O1 3.0100 no 2_645
H27A O3 2.8057 no 2_645
H27A C8 3.3246 no 2_645
H27A C9 3.2207 no 2_645
H27A C10 3.2267 no 2_645
H27A C11 3.3111 no 2_645
H27A C12 3.4043 no 2_645
H27A C13 3.4063 no 2_645
H27A H19 3.1608 no 2_645
H27B O1 3.4801 no 2_645
H27B N2 3.2039 no 1_556
H27B C10 3.4839 no 2_645
H27B C11 3.2825 no 2_645
H27B C15 3.2325 no 1_556
H27B C16 2.9143 no 1_556
H27B C26 3.2757 no 1_556
H27B H5 2.8968 no 1_556
H27B H11 3.3616 no 2_645
H28A C23 3.5841 no 1_556
H28A C24 3.1541 no 1_556
H28A C25 3.0015 no 1_556
H28A C26 3.3001 no 1_556
H28A C34 3.4502 no 4_775
H28A H24 3.4758 no 1_556
H28A H25 3.2593 no 1_556
H28A H34A 3.2614 no 4_775
H28A H34B 2.7299 no 4_775
H28B Cl1 3.0170 no 2_645
H28B O1 2.9058 no 2_645
H28B O2 2.6716 no 2_645
H28B O3 3.0564 no 2_645
H28B C21 3.3962 no 3_566
H28B H20 3.3042 no 3_566
H28B H21 2.8214 no 3_566
H28B H33B 3.5232 no 4_775
H28B H34A 3.4743 no 4_775
H28B H34B 3.3551 no 4_775
H29A O2 3.4693 no 3_565
H29A O4 3.4010 no 3_565
H29A C9 3.5772 no 4_775
H29A C10 2.9155 no 4_775
H29A C11 3.4100 no 4_775
H29A C21 3.3539 no 3_566
H29A H10 2.6472 no 4_775
H29A H11 3.4882 no 4_775
H29A H21 2.9086 no 3_566
H29A H22 3.4511 no 3_566
H29B O2 3.0102 no 3_565
H29B O3 3.4530 no 2_645
H29B C20 3.2570 no 2_645
H29B C21 3.4811 no 3_566
H29B H19 3.3373 no 2_645
H29B H20 2.5666 no 2_645
H29B H21 2.6741 no 3_566
H29B H33A 3.3648 no 1_545
H30A C25 3.4959 no 1_556
H30A C26 3.2224 no 1_556
H30A C32 3.5226 no 4_774
H30A H2 3.2447 no .
H30A H25 3.2969 no 1_556
H30A H26 2.7707 no 1_556
H30A H32A 2.9742 no 4_774
H30A H32B 3.2799 no 4_774
H30B O2 3.5134 no 3_565
H30B C1 3.1648 no .
H30B C2 3.0578 no .
H30B C20 3.3073 no 2_645
H30B C32 3.1783 no 4_774
H30B H1 2.9005 no .
H30B H2 2.7050 no .
H30B H20 3.0781 no 2_645
H30B H32A 2.4368 no 4_774
H30B H32B 3.0640 no 4_774
H31A N2 3.1519 no 1_556
H31A C15 3.0481 no 1_556
H31A C16 2.7363 no 1_556
H31A C23 3.5838 no 1_556
H31A C25 3.5197 no 1_556
H31A C26 3.0207 no 1_556
H31A H9 3.0272 no 1_556
H31A H26 3.3923 no 1_556
H31B Cl1 3.3765 no 2_655
H31B O3 2.9249 no 2_655
H31B O4 2.9468 no 2_655
H31B C1 3.2396 no 2_655
H31B C2 3.4129 no 2_655
H31B C5 3.5382 no 2_655
H31B C6 3.3048 no 2_655
H32A Cl1 3.3915 no 2_655
H32A O2 2.8140 no 2_655
H32A O3 3.4862 no 2_655
H32A O4 3.3959 no 2_655
H32A C30 3.0990 no 4_775
H32A H21 3.4375 no 3_576
H32A H30A 2.9742 no 4_775
H32A H30B 2.4368 no 4_775
H32B C1 3.4623 no 4_775
H32B C2 3.4310 no 4_775
H32B C3 3.5425 no 4_775
H32B C25 3.4599 no 1_556
H32B H23 3.4911 no 4_775
H32B H25 3.5267 no 1_556
H32B H30A 3.2799 no 4_775
H32B H30B 3.0640 no 4_775
H33A O2 3.4158 no 2_655
H33A O3 2.8735 no 2_655
H33A C19 3.5380 no 2_655
H33A C20 3.3322 no 2_655
H33A H19 3.1365 no 2_655
H33A H20 2.7282 no 2_655
H33A H21 2.9579 no 3_576
H33A H29B 3.3648 no 1_565
H33B O1 3.5042 no 3_575
H33B C1 3.5734 no 4_775
H33B C5 3.3251 no 4_775
H33B C6 3.0079 no 4_775
H33B H5 3.4764 no 4_775
H33B H6 2.9462 no 4_775
H33B H20 3.5712 no 2_655
H33B H21 3.2588 no 3_576
H33B H28B 3.5232 no 4_774
H34A C11 3.2093 no .
H34A C12 3.3517 no .
H34A C19 3.2053 no 2_655
H34A C20 3.0014 no 2_655
H34A H11 2.6392 no .
H34A H12 2.9292 no .
H34A H19 3.2257 no 2_655
H34A H20 2.8782 no 2_655
H34A H28A 3.2614 no 4_774
H34A H28B 3.4743 no 4_774
H34B C23 3.0432 no 4_775
H34B C24 2.9239 no 4_775
H34B C28 3.4734 no 4_774
H34B H12 3.2639 no .
H34B H23 2.9016 no 4_775
H34B H24 2.6909 no 4_775
H34B H28A 2.7299 no 4_774
H34B H28B 3.3551 no 4_774
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_publ_flag
_geom_torsion_site_symmetry_1
C27 O5 C30 C29 -1.7(9) no .
C30 O5 C27 C28 23.0(8) no .
C31 O6 C34 C33 11.1(18) no .
C34 O6 C31 C32 -32.0(12) no .
Ag1 N1 C3 C2 -10.4(7) no .
Ag1 N1 C3 C4 169.2(3) no .
Ag1 N1 C13 C8 -170.0(3) no .
Ag1 N1 C13 C12 13.0(7) no .
C3 N1 C13 C8 -0.5(8) no .
C3 N1 C13 C12 -177.5(5) no .
C13 N1 C3 C2 -179.9(5) no .
C13 N1 C3 C4 -0.4(8) no .
Ag1 N2 C16 C15 -178.5(4) no 1_554
Ag1 N2 C16 C26 1.6(9) no 1_554
Ag1 N2 C17 C18 179.6(4) no 1_554
Ag1 N2 C17 C22 -2.7(9) no 1_554
C16 N2 C17 C18 3.5(11) no .
C16 N2 C17 C22 -178.8(6) no .
C17 N2 C16 C15 -2.3(11) no .
C17 N2 C16 C26 177.8(6) no .
C2 C1 C6 C5 0.2(13) no .
C6 C1 C2 C3 -0.4(12) no .
C1 C2 C3 N1 -179.8(6) no .
C1 C2 C3 C4 0.6(9) no .
N1 C3 C4 C5 179.9(5) no .
N1 C3 C4 C7 0.4(8) no .
C2 C3 C4 C5 -0.5(8) no .
C2 C3 C4 C7 180.0(5) no .
C3 C4 C5 C6 0.3(9) no .
C3 C4 C7 C8 0.5(9) no .
C3 C4 C7 C14 -179.1(5) no .
C5 C4 C7 C8 -179.0(6) no .
C5 C4 C7 C14 1.5(10) no .
C7 C4 C5 C6 179.8(6) no .
C4 C5 C6 C1 -0.1(11) no .
C4 C7 C8 C9 178.5(5) no .
C4 C7 C8 C13 -1.2(9) no .
C4 C7 C14 C15 -91.0(9) no .
C4 C7 C14 C18 93.7(9) no .
C8 C7 C14 C15 89.4(9) no .
C8 C7 C14 C18 -85.9(9) no .
C14 C7 C8 C9 -2.0(10) no .
C14 C7 C8 C13 178.3(6) no .
C7 C8 C9 C10 -178.2(6) no .
C7 C8 C13 N1 1.3(8) no .
C7 C8 C13 C12 178.4(5) no .
C9 C8 C13 N1 -178.4(5) no .
C9 C8 C13 C12 -1.4(8) no .
C13 C8 C9 C10 1.5(9) no .
C8 C9 C10 C11 -0.9(10) no .
C9 C10 C11 C12 0.3(11) no .
C10 C11 C12 C13 -0.2(10) no .
C11 C12 C13 N1 177.9(6) no .
C11 C12 C13 C8 0.8(9) no .
C7 C14 C15 C16 -177.5(7) no .
C7 C14 C15 C23 5.8(12) no .
C7 C14 C18 C17 178.6(7) no .
C7 C14 C18 C19 -3.5(12) no .
C15 C14 C18 C17 3.2(11) no .
C15 C14 C18 C19 -178.9(6) no .
C18 C14 C15 C16 -2.1(11) no .
C18 C14 C15 C23 -178.8(6) no .
C14 C15 C16 N2 1.6(11) no .
C14 C15 C16 C26 -178.5(6) no .
C14 C15 C23 C24 178.3(7) no .
C16 C15 C23 C24 1.6(11) no .
C23 C15 C16 N2 178.5(6) no .
C23 C15 C16 C26 -1.6(10) no .
N2 C16 C26 C25 -179.8(7) no .
C15 C16 C26 C25 0.3(11) no .
N2 C17 C18 C14 -4.0(10) no .
N2 C17 C18 C19 178.0(6) no .
N2 C17 C22 C21 -177.7(6) no .
C18 C17 C22 C21 0.1(10) no .
C22 C17 C18 C14 178.3(6) no .
C22 C17 C18 C19 0.3(9) no .
C14 C18 C19 C20 -178.4(6) no .
C17 C18 C19 C20 -0.5(10) no .
C18 C19 C20 C21 0.4(10) no .
C19 C20 C21 C22 -0.1(10) no .
C20 C21 C22 C17 -0.2(10) no .
C15 C23 C24 C25 -0.2(12) no .
C23 C24 C25 C26 -1.2(13) no .
C24 C25 C26 C16 1.2(13) no .
O5 C27 C28 C29 -34.4(9) no .
C27 C28 C29 C30 32.9(11) no .
C28 C29 C30 O5 -20.6(11) no .
O6 C31 C32 C33 42.0(12) no .
C31 C32 C33 C34 -35.6(15) no .
C32 C33 C34 O6 19(2) no .
