#------------------------------------------------------------------------------
#$Date: 2018-06-19 15:12:59 +0300 (Tue, 19 Jun 2018) $
#$Revision: 208504 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/23/09/7230918.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7230918
loop_
_publ_author_name
'Yue, Qi'
'Liu, Xu'
'Guo, Wei-Xiao'
'Gao, En-Qing'
_publ_section_title
;
 Structural diversity and magnetic properties of Co(II)/Mn(II)/Ni(II)
 coordination polymers constructed from an unsymmetrical tetracarboxylic
 acid and varying N-donor ligands
;
_journal_name_full               CrystEngComm
_journal_paper_doi               10.1039/C8CE00692J
_journal_year                    2018
_chemical_formula_sum            'C2.8 H3.4 Co0.2 N0.2 O1.6'
_chemical_formula_weight         77.24
_chemical_name_systematic
;
 ?
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   mixed
_audit_creation_method           SHELXL-2014
_audit_update_record
;
2018-04-20 deposited with the CCDC.
2018-06-19 downloaded from the CCDC.
;
_cell_angle_alpha                74.175(5)
_cell_angle_beta                 81.702(5)
_cell_angle_gamma                74.789(5)
_cell_formula_units_Z            20
_cell_length_a                   11.0005(16)
_cell_length_b                   11.3676(17)
_cell_length_c                   13.521(2)
_cell_measurement_reflns_used    4166
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      24.5
_cell_measurement_theta_min      2.39
_cell_volume                     1564.9(4)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_refinement  'SHELXL-2014 (Sheldrick, 2014)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.984
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0699
_diffrn_reflns_av_unetI/netI     0.0773
_diffrn_reflns_Laue_measured_fraction_full 0.992
_diffrn_reflns_Laue_measured_fraction_max 0.984
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            19291
_diffrn_reflns_point_group_measured_fraction_full 0.992
_diffrn_reflns_point_group_measured_fraction_max 0.984
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         25.997
_diffrn_reflns_theta_min         1.570
_exptl_absorpt_coefficient_mu    1.140
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.639
_exptl_crystal_description       block
_exptl_crystal_F_000             796
_refine_diff_density_max         0.797
_refine_diff_density_min         -0.594
_refine_diff_density_rms         0.084
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.042
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     497
_refine_ls_number_reflns         6054
_refine_ls_number_restraints     16
_refine_ls_restrained_S_all      1.041
_refine_ls_R_factor_all          0.0782
_refine_ls_R_factor_gt           0.0514
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0604P)²+0.0839P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1214
_refine_ls_wR_factor_ref         0.1339
_reflns_Friedel_coverage         0.000
_reflns_number_gt                4257
_reflns_number_total             6054
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c8ce00692j2.cif
_cod_data_source_block           3
_cod_original_formula_sum        'C2.80 H3.40 Co0.20 N0.20 O1.60'
_cod_database_code               7230918
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelxl_version_number           2014-3
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
Co1 Co 0.89241(5) 0.08125(5) 0.20719(4) 0.02661(16) Uani 1 1 d . .
Co2 Co 0.73888(5) -0.28886(5) 0.91639(4) 0.03244(17) Uani 1 1 d . .
O1 O 1.0402(3) -0.0727(2) 0.2554(2) 0.0310(6) Uani 1 1 d . .
O2 O 1.0011(3) -0.1984(3) 0.1688(2) 0.0375(7) Uani 1 1 d . .
O3 O 1.2440(3) -0.1122(3) 0.0598(2) 0.0484(8) Uani 1 1 d . .
O4 O 1.3521(3) -0.2898(3) 0.0175(2) 0.0427(8) Uani 1 1 d . .
O5 O 1.0965(3) -0.3772(3) 0.7790(2) 0.0372(7) Uani 1 1 d . .
O6 O 1.0025(2) -0.1731(2) 0.7323(2) 0.0289(6) Uani 1 1 d . .
O7 O 0.8139(2) -0.3213(3) 0.7777(2) 0.0357(7) Uani 1 1 d . .
O8 O 0.6618(3) -0.2517(3) 0.6699(2) 0.0469(8) Uani 1 1 d . .
O9 O 0.9946(3) 0.1127(3) 0.0572(2) 0.0425(8) Uani 1 1 d D .
H9A H 0.957(4) 0.125(5) 0.004(3) 0.054(16) Uiso 1 1 d D .
H9B H 0.938(9) 0.115(12) 0.106(7) 0.27(6) Uiso 1 1 d D .
O10 O 0.7595(3) 0.2523(3) 0.1573(3) 0.0420(8) Uani 1 1 d D .
H10B H 0.798(5) 0.306(4) 0.164(5) 0.08(2) Uiso 1 1 d D .
H10C H 0.738(5) 0.266(5) 0.096(2) 0.08(2) Uiso 1 1 d D .
O11 O 0.7886(3) -0.0080(3) 0.1451(2) 0.0366(7) Uani 1 1 d D .
H11A H 0.847(5) -0.074(4) 0.146(5) 0.12(3) Uiso 1 1 d D .
H11B H 0.757(6) 0.025(6) 0.087(3) 0.10(2) Uiso 1 1 d D .
O12 O 0.7373(4) -0.4832(3) 0.9725(3) 0.0522(9) Uani 1 1 d D .
H12A H 0.798(5) -0.519(6) 0.936(5) 0.11(3) Uiso 1 1 d D .
H12B H 0.664(3) -0.497(5) 0.975(5) 0.08(2) Uiso 1 1 d D .
O13 O 0.5568(3) -0.2307(4) 0.8646(3) 0.0523(9) Uani 1 1 d D .
H13A H 0.491(5) -0.253(7) 0.899(6) 0.15(3) Uiso 1 1 d D .
H13B H 0.561(7) -0.247(7) 0.806(3) 0.11(3) Uiso 1 1 d D .
O14 O 0.7646(3) -0.0981(3) 0.8513(2) 0.0403(8) Uani 1 1 d D .
H14A H 0.777(6) -0.034(4) 0.865(5) 0.09(2) Uiso 1 1 d D .
H14B H 0.826(3) -0.110(4) 0.808(3) 0.041(14) Uiso 1 1 d D .
O15 O 0.9299(3) -0.3420(3) 0.9544(2) 0.0370(7) Uani 1 1 d D .
H15B H 0.960(4) -0.383(4) 1.011(2) 0.059(16) Uiso 1 1 d D .
H15C H 0.984(4) -0.354(5) 0.907(3) 0.052(15) Uiso 1 1 d D .
O16 O 1.0437(3) -0.4203(3) 0.1293(2) 0.0442(8) Uani 1 1 d D .
H16B H 1.032(6) -0.476(4) 0.182(3) 0.09(2) Uiso 1 1 d D .
H16C H 1.032(6) -0.349(3) 0.142(5) 0.09(2) Uiso 1 1 d D .
N1 N 0.7901(3) 0.0536(3) 0.3521(2) 0.0332(8) Uani 1 1 d . .
N2 N 0.3241(3) 0.2576(3) 0.9384(3) 0.0353(9) Uani 1 1 d . .
C1 C 1.0667(4) -0.1728(4) 0.2253(3) 0.0282(9) Uani 1 1 d . .
C2 C 1.1830(3) -0.2715(3) 0.2637(3) 0.0259(8) Uani 1 1 d . .
C3 C 1.2879(4) -0.2993(4) 0.1941(3) 0.0308(9) Uani 1 1 d . .
C4 C 1.2941(4) -0.2279(4) 0.0820(3) 0.0356(10) Uani 1 1 d . .
C5 C 1.3919(4) -0.3954(4) 0.2281(3) 0.0423(11) Uani 1 1 d . .
H5A H 1.4602 -0.4155 0.1816 0.051 Uiso 1 1 calc R U
C6 C 1.3946(4) -0.4608(5) 0.3297(3) 0.0479(13) Uani 1 1 d . .
H6A H 1.4651 -0.5239 0.3521 0.057 Uiso 1 1 calc R U
C7 C 1.2925(4) -0.4327(4) 0.3982(3) 0.0420(11) Uani 1 1 d . .
H7A H 1.2955 -0.4769 0.4671 0.050 Uiso 1 1 calc R U
C8 C 1.1847(4) -0.3397(4) 0.3671(3) 0.0291(9) Uani 1 1 d . .
C9 C 1.0748(4) -0.3198(4) 0.4452(3) 0.0280(9) Uani 1 1 d . .
C10 C 1.0965(4) -0.3108(4) 0.5417(3) 0.0296(9) Uani 1 1 d . .
H10A H 1.1781 -0.3124 0.5539 0.036 Uiso 1 1 calc R U
C11 C 1.0012(4) -0.2995(3) 0.6203(3) 0.0275(9) Uani 1 1 d . .
C12 C 1.0343(3) -0.2827(4) 0.7188(3) 0.0269(9) Uani 1 1 d . .
C13 C 0.8781(4) -0.2979(4) 0.6030(3) 0.0279(9) Uani 1 1 d . .
C14 C 0.7746(4) -0.2881(4) 0.6883(3) 0.0297(9) Uani 1 1 d . .
C15 C 0.8549(4) -0.3056(4) 0.5073(3) 0.0347(10) Uani 1 1 d . .
H15A H 0.7731 -0.3023 0.4947 0.042 Uiso 1 1 calc R U
C16 C 0.9523(4) -0.3181(4) 0.4291(3) 0.0347(10) Uani 1 1 d . .
H16A H 0.9349 -0.3253 0.3660 0.042 Uiso 1 1 calc R U
C17 C 0.6647(4) 0.0994(5) 0.3594(3) 0.0450(12) Uani 1 1 d . .
H17A H 0.6219 0.1237 0.2999 0.054 Uiso 1 1 calc R U
C18 C 0.8476(4) 0.0147(4) 0.4391(3) 0.0332(10) Uani 1 1 d . .
H18A H 0.9340 -0.0210 0.4360 0.040 Uiso 1 1 calc R U
C19 C 0.5964(4) 0.1122(5) 0.4511(3) 0.0465(13) Uani 1 1 d . .
H19A H 0.5095 0.1450 0.4527 0.056 Uiso 1 1 calc R U
C20 C 0.7864(4) 0.0244(4) 0.5328(3) 0.0352(10) Uani 1 1 d . .
H20A H 0.8314 -0.0037 0.5913 0.042 Uiso 1 1 calc R U
C21 C 0.6577(4) 0.0758(4) 0.5412(3) 0.0370(10) Uani 1 1 d . .
C22 C 0.5928(4) 0.0895(5) 0.6439(3) 0.0476(13) Uani 1 1 d . .
H22A H 0.5811 0.0077 0.6837 0.057 Uiso 1 1 calc R U
H22B H 0.6486 0.1140 0.6799 0.057 Uiso 1 1 calc R U
C23 C 0.4680(4) 0.1811(5) 0.6432(3) 0.0497(13) Uani 1 1 d . .
H23A H 0.4078 0.1501 0.6175 0.060 Uiso 1 1 calc R U
H23B H 0.4762 0.2603 0.5958 0.060 Uiso 1 1 calc R U
C24 C 0.4163(4) 0.2049(4) 0.7472(3) 0.0355(10) Uani 1 1 d . .
C25 C 0.3254(4) 0.3139(4) 0.7556(3) 0.0401(11) Uani 1 1 d . .
H25A H 0.2934 0.3715 0.6965 0.048 Uiso 1 1 calc R U
C26 C 0.4593(4) 0.1244(4) 0.8375(3) 0.0420(12) Uani 1 1 d . .
H26A H 0.5202 0.0505 0.8362 0.050 Uiso 1 1 calc R U
C27 C 0.2830(4) 0.3365(4) 0.8503(3) 0.0419(11) Uani 1 1 d . .
H27A H 0.2228 0.4103 0.8536 0.050 Uiso 1 1 calc R U
C28 C 0.4119(4) 0.1535(4) 0.9298(3) 0.0415(11) Uani 1 1 d . .
H28A H 0.4426 0.0975 0.9899 0.050 Uiso 1 1 calc R U
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 Co1 O11 98.20(12) . .
O1 Co1 N1 93.35(12) . .
O11 Co1 N1 93.96(13) . .
O1 Co1 O10 172.39(13) . .
O11 Co1 O10 88.71(14) . .
N1 Co1 O10 89.31(13) . .
O1 Co1 O6 82.18(11) . 2_756
O11 Co1 O6 179.19(11) . 2_756
N1 Co1 O6 86.72(12) . 2_756
O10 Co1 O6 90.86(12) . 2_756
O1 Co1 O9 87.75(12) . .
O11 Co1 O9 85.88(12) . .
N1 Co1 O9 178.90(13) . .
O10 Co1 O9 89.60(13) . .
O6 Co1 O9 93.43(12) 2_756 .
O1 Co1 H9B 97(5) . .
O11 Co1 H9B 82(6) . .
N1 Co1 H9B 169(5) . .
O10 Co1 H9B 80(5) . .
O6 Co1 H9B 97(6) 2_756 .
O9 Co1 H9B 10(5) . .
O7 Co2 N2 175.62(13) . 2_657
O7 Co2 O13 90.77(14) . .
N2 Co2 O13 93.54(14) 2_657 .
O7 Co2 O15 84.53(11) . .
N2 Co2 O15 91.13(13) 2_657 .
O13 Co2 O15 174.66(14) . .
O7 Co2 O12 89.34(14) . .
N2 Co2 O12 90.95(14) 2_657 .
O13 Co2 O12 95.88(16) . .
O15 Co2 O12 86.63(14) . .
O7 Co2 O14 85.81(12) . .
N2 Co2 O14 93.49(13) 2_657 .
O13 Co2 O14 89.43(14) . .
O15 Co2 O14 87.69(12) . .
O12 Co2 O14 172.86(13) . .
C1 O1 Co1 125.0(3) . .
C12 O6 Co1 128.2(2) . 2_756
C14 O7 Co2 134.3(3) . .
Co1 O9 H9A 120(3) . .
Co1 O9 H9B 16(9) . .
H9A O9 H9B 106(9) . .
Co1 O10 H10B 102(4) . .
Co1 O10 H10C 115(4) . .
H10B O10 H10C 113(6) . .
Co1 O11 H11A 95(5) . .
Co1 O11 H11B 122(5) . .
H11A O11 H11B 114(6) . .
Co2 O12 H12A 103(5) . .
Co2 O12 H12B 113(4) . .
H12A O12 H12B 119(7) . .
Co2 O13 H13A 125(5) . .
Co2 O13 H13B 108(5) . .
H13A O13 H13B 106(7) . .
Co2 O14 H14A 145(4) . .
Co2 O14 H14B 101(3) . .
H14A O14 H14B 99(5) . .
Co2 O15 H15B 129(3) . .
Co2 O15 H15C 116(3) . .
H15B O15 H15C 110(5) . .
H16B O16 H16C 112(6) . .
C18 N1 C17 117.1(4) . .
C18 N1 Co1 121.6(3) . .
C17 N1 Co1 119.9(3) . .
C28 N2 C27 116.4(4) . .
C28 N2 Co2 119.6(3) . 2_657
C27 N2 Co2 124.0(3) . 2_657
O2 C1 O1 124.8(4) . .
O2 C1 C2 117.6(4) . .
O1 C1 C2 117.5(4) . .
C8 C2 C3 119.7(3) . .
C8 C2 C1 120.5(3) . .
C3 C2 C1 119.7(3) . .
C5 C3 C2 119.7(4) . .
C5 C3 C4 117.6(3) . .
C2 C3 C4 122.7(3) . .
O3 C4 O4 124.8(4) . .
O3 C4 C3 118.2(4) . .
O4 C4 C3 116.9(4) . .
C6 C5 C3 120.6(4) . .
C6 C5 H5A 119.7 . .
C3 C5 H5A 119.7 . .
C5 C6 C7 119.7(4) . .
C5 C6 H6A 120.1 . .
C7 C6 H6A 120.1 . .
C6 C7 C8 121.7(4) . .
C6 C7 H7A 119.1 . .
C8 C7 H7A 119.1 . .
C7 C8 C2 118.4(4) . .
C7 C8 C9 118.4(3) . .
C2 C8 C9 123.2(3) . .
C16 C9 C10 117.6(4) . .
C16 C9 C8 123.2(4) . .
C10 C9 C8 119.0(4) . .
C11 C10 C9 122.6(4) . .
C11 C10 H10A 118.7 . .
C9 C10 H10A 118.7 . .
C10 C11 C13 119.2(4) . .
C10 C11 C12 117.8(3) . .
C13 C11 C12 122.9(3) . .
O5 C12 O6 124.9(4) . .
O5 C12 C11 118.0(4) . .
O6 C12 C11 117.0(3) . .
C15 C13 C11 118.8(4) . .
C15 C13 C14 121.5(4) . .
C11 C13 C14 119.6(3) . .
O8 C14 O7 124.7(4) . .
O8 C14 C13 121.3(4) . .
O7 C14 C13 114.0(3) . .
C13 C15 C16 121.3(4) . .
C13 C15 H15A 119.3 . .
C16 C15 H15A 119.3 . .
C9 C16 C15 120.4(4) . .
C9 C16 H16A 119.8 . .
C15 C16 H16A 119.8 . .
N1 C17 C19 122.8(4) . .
N1 C17 H17A 118.6 . .
C19 C17 H17A 118.6 . .
N1 C18 C20 123.4(4) . .
N1 C18 H18A 118.3 . .
C20 C18 H18A 118.3 . .
C17 C19 C21 119.8(4) . .
C17 C19 H19A 120.1 . .
C21 C19 H19A 120.1 . .
C18 C20 C21 120.3(4) . .
C18 C20 H20A 119.8 . .
C21 C20 H20A 119.8 . .
C20 C21 C19 116.5(4) . .
C20 C21 C22 119.6(4) . .
C19 C21 C22 123.9(4) . .
C23 C22 C21 116.6(4) . .
C23 C22 H22A 108.1 . .
C21 C22 H22A 108.1 . .
C23 C22 H22B 108.1 . .
C21 C22 H22B 108.1 . .
H22A C22 H22B 107.3 . .
C22 C23 C24 114.2(4) . .
C22 C23 H23A 108.7 . .
C24 C23 H23A 108.7 . .
C22 C23 H23B 108.7 . .
C24 C23 H23B 108.7 . .
H23A C23 H23B 107.6 . .
C26 C24 C25 116.7(4) . .
C26 C24 C23 122.3(4) . .
C25 C24 C23 120.9(4) . .
C27 C25 C24 120.2(4) . .
C27 C25 H25A 119.9 . .
C24 C25 H25A 119.9 . .
C24 C26 C28 119.7(4) . .
C24 C26 H26A 120.2 . .
C28 C26 H26A 120.2 . .
N2 C27 C25 123.1(4) . .
N2 C27 H27A 118.4 . .
C25 C27 H27A 118.4 . .
N2 C28 C26 123.9(4) . .
N2 C28 H28A 118.0 . .
C26 C28 H28A 118.0 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Co1 O1 2.079(3) .
Co1 O11 2.094(3) .
Co1 N1 2.102(3) .
Co1 O10 2.110(3) .
Co1 O6 2.114(3) 2_756
Co1 O9 2.159(3) .
Co1 H9B 1.37(6) .
Co2 O7 2.025(3) .
Co2 N2 2.079(3) 2_657
Co2 O13 2.097(3) .
Co2 O15 2.126(3) .
Co2 O12 2.135(4) .
Co2 O14 2.183(3) .
O1 C1 1.261(5) .
O2 C1 1.257(5) .
O3 C4 1.255(5) .
O4 C4 1.265(5) .
O5 C12 1.258(4) .
O6 C12 1.260(5) .
O6 Co1 2.114(3) 2_756
O7 C14 1.268(5) .
O8 C14 1.239(5) .
O9 H9A 0.844(19) .
O9 H9B 0.84(2) .
O10 H10B 0.85(2) .
O10 H10C 0.86(2) .
O11 H11A 0.85(2) .
O11 H11B 0.85(2) .
O12 H12A 0.85(2) .
O12 H12B 0.85(2) .
O13 H13A 0.86(2) .
O13 H13B 0.85(2) .
O14 H14A 0.85(2) .
O14 H14B 0.842(19) .
O15 H15B 0.844(19) .
O15 H15C 0.824(19) .
O16 H16B 0.83(2) .
O16 H16C 0.84(2) .
N1 C18 1.327(5) .
N1 C17 1.341(5) .
N2 C28 1.337(5) .
N2 C27 1.337(5) .
N2 Co2 2.079(3) 2_657
C1 C2 1.512(5) .
C2 C8 1.402(5) .
C2 C3 1.405(5) .
C3 C5 1.391(5) .
C3 C4 1.513(5) .
C5 C6 1.372(6) .
C5 H5A 0.9300 .
C6 C7 1.376(6) .
C6 H6A 0.9300 .
C7 C8 1.395(6) .
C7 H7A 0.9300 .
C8 C9 1.498(5) .
C9 C16 1.390(6) .
C9 C10 1.394(5) .
C10 C11 1.388(5) .
C10 H10A 0.9300 .
C11 C13 1.402(5) .
C11 C12 1.502(5) .
C13 C15 1.384(5) .
C13 C14 1.505(5) .
C15 C16 1.400(6) .
C15 H15A 0.9300 .
C16 H16A 0.9300 .
C17 C19 1.377(6) .
C17 H17A 0.9300 .
C18 C20 1.365(5) .
C18 H18A 0.9300 .
C19 C21 1.388(6) .
C19 H19A 0.9300 .
C20 C21 1.384(5) .
C20 H20A 0.9300 .
C21 C22 1.495(6) .
C22 C23 1.489(6) .
C22 H22A 0.9700 .
C22 H22B 0.9700 .
C23 C24 1.505(6) .
C23 H23A 0.9700 .
C23 H23B 0.9700 .
C24 C26 1.372(6) .
C24 C25 1.394(6) .
C25 C27 1.366(6) .
C25 H25A 0.9300 .
C26 C28 1.374(6) .
C26 H26A 0.9300 .
C27 H27A 0.9300 .
C28 H28A 0.9300 .
