#------------------------------------------------------------------------------
#$Date: 2019-11-07 22:01:48 +0200 (Thu, 07 Nov 2019) $
#$Revision: 223684 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/23/25/7232572.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7232572
loop_
_publ_author_name
'Shemchuk, O.'
'André, V.'
'Duarte, M. T.'
'Braga, D.'
'Grepioni, F.'
_publ_section_title
;
 Mechanochemical preparation of molecular and ionic co-crystals of the
 hormone melatonin
;
_journal_issue                   18
_journal_name_full               CrystEngComm
_journal_page_first              2949
_journal_paper_doi               10.1039/C9CE00316A
_journal_volume                  21
_journal_year                    2019
_chemical_formula_moiety         'C26 H32 Ca Cl2 N4 O6'
_chemical_formula_sum            'C26 H32 Ca Cl2 N4 O6'
_chemical_formula_weight         611.57
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_audit_update_record
;
2019-03-04 deposited with the CCDC.    2019-04-08 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 99.6349(17)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   18.9658(4)
_cell_length_b                   8.93532(14)
_cell_length_c                   8.98702(18)
_cell_measurement_temperature    298
_cell_volume                     1501.51(5)
_diffrn_ambient_temperature      298
_diffrn_measurement_device_type  'Panalytical XPert PRO'
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.5418
_exptl_crystal_density_diffrn    1.299
_pd_char_colour                  white
_pd_proc_ls_prof_R_factor        0.0374
_pd_proc_ls_prof_wR_expected     0.0217
_pd_proc_ls_prof_wR_factor       0.0483
_refine_ls_goodness_of_fit_all   2.22789
_refine_ls_number_parameters     0.000000
_refine_ls_R_I_factor            0.0178
_refine_ls_shift/su_max          1.65330873e-017
_cod_data_source_file            c9ce00316a2.cif
_cod_data_source_block           CaCl2_Mehatonin_hydrate
_cod_depositor_comments
'Adding full bibliography for 7232572--7232574.cif.'
_cod_original_cell_volume        1501.50(5)
_cod_original_sg_symbol_Hall     -P2ybc
_cod_original_sg_symbol_H-M      P21/c
_cod_database_code               7232572
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z '
'-x, y+1/2, -z+1/2 '
'x, -y+1/2, z+1/2 '
'-x, -y, -z '
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_symmetry_multiplicity
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_B_iso_or_equiv
OW O 4 0.5139(5) 0.5273(14) 0.2391(12) 1 3
Cl1 Cl 4 0.5678(3) 0.2272(7) 0.5260(6) 1 2.3387
C1M C 4 0.2468(6) 0.3974(9) 0.3202(7) 1 2.87307
C2M C 4 0.2704(4) 0.6005(13) 0.6013(6) 1 2.87307
C3M C 4 -0.0170(12) 0.287(4) 0.7281(13) 1 2.87307
C4M C 4 0.3545(12) 0.280(3) 0.4554(13) 1 2.87307
C5M C 4 0.388(2) 0.136(4) 0.5149(19) 1 2.87307
C6M C 4 0.1874(3) 0.4639(8) 0.3901(5) 1 2.87307
C7M C 4 0.21080(12) 0.5216(4) 0.5463(5) 1 2.87307
C8M C 4 0.17350(19) 0.5009(7) 0.6696(5) 1 2.87307
C9M C 4 0.1092(5) 0.4280(18) 0.6831(7) 1 2.87307
C10M C 4 0.0885(5) 0.424(2) 0.8217(8) 1 2.87307
C11M C 4 0.1297(4) 0.4920(12) 0.9470(6) 1 2.87307
C12M C 4 0.1923(4) 0.5649(7) 0.9375(5) 1 2.87307
C13M C 4 0.2136(3) 0.5688(7) 0.7968(5) 1 2.87307
H1M H 4 0.2556(16) 0.2058(12) 0.4537(16) 1 3.447684
H2M H 4 0.3090(7) 0.673(2) 0.8127(8) 1 3.447684
H3M H 4 0.3106(6) 0.646(2) 0.5459(7) 1 3.447684
H4M H 4 -0.0371(9) 0.366(5) 0.6340(13) 1 3.447684
H5M H 4 -0.0572(14) 0.239(5) 0.7774(15) 1 3.447684
H6M H 4 0.0121(17) 0.209(4) 0.663(2) 1 3.447684
H7M H 4 0.349(2) 0.055(3) 0.542(2) 1 3.447684
H8M H 4 0.413(2) 0.086(5) 0.430(2) 1 3.447684
H9M H 4 0.423(2) 0.151(5) 0.6166(19) 1 3.447684
H10M H 4 0.2269(8) 0.3497(11) 0.2088(9) 1 3.447684
H11M H 4 0.2871(3) 0.4816(16) 0.3049(9) 1 3.447684
H12M H 4 0.1464(7) 0.3810(16) 0.3866(7) 1 3.447684
H13M H 4 0.1634(3) 0.5505(14) 0.3205(5) 1 3.447684
H14M H 4 0.0772(7) 0.377(3) 0.5897(8) 1 3.447684
H15M H 4 0.1104(5) 0.4888(15) 1.0496(7) 1 3.447684
H16M H 4 0.2227(6) 0.6187(13) 1.0344(6) 1 3.447684
N1M N 4 0.2839(12) 0.2820(17) 0.4161(11) 1 2.87307
N2M N 4 0.2721(5) 0.6317(16) 0.7511(6) 1 2.87307
O1M O 4 0.0274(9) 0.354(3) 0.8512(10) 1 2.87307
O2M O 4 0.3908(6) 0.392(4) 0.4422(16) 1 2.87307
Ca Ca 2 0.5 0.5 0.5 1 2.41464
loop_
_pd_proc_point_id
_pd_meas_2theta_scan
_pd_proc_intensity_total
_pd_calc_intensity_total
_pd_proc_ls_weight
1 3.00007 1896.27028 1936.00000 0.00052
2 3.01307 1893.62983 1962.48999 0.00051
3 3.02607 1891.00403 1866.24011 0.00054
4 3.03907 1888.41056 1980.25000 0.00050
5 3.05207 1885.84881 2007.03992 0.00050
6 3.06507 1883.31003 1971.36011 0.00051
7 3.07807 1880.58258 1892.25000 0.00053
8 3.09107 1877.84833 1831.83997 0.00055
9 3.10407 1875.10752 1900.95984 0.00053
10 3.11707 1872.36041 1797.76013 0.00056
11 3.13007 1869.60740 1892.25000 0.00053
12 3.14307 1866.84878 1892.25000 0.00053
13 3.15607 1864.08496 1883.56018 0.00053
14 3.16907 1861.31632 1936.00000 0.00052
15 3.18207 1858.54340 1892.25000 0.00053
16 3.19507 1855.76663 1918.43994 0.00052
17 3.20807 1852.98600 1849.00000 0.00054
18 3.22107 1850.20180 1823.29004 0.00055
19 3.23407 1847.41439 1892.25000 0.00053
20 3.24707 1844.62460 1892.25000 0.00053
21 3.26007 1841.83219 1831.83997 0.00055
22 3.27307 1839.03747 1823.29004 0.00055
23 3.28607 1836.24072 1900.95984 0.00053
24 3.29907 1833.44311 1814.75989 0.00055
25 3.31207 1830.64433 1722.25000 0.00058
26 3.32507 1827.84466 1772.40991 0.00056
27 3.33807 1825.04441 1780.84009 0.00056
28 3.35107 1822.24478 1797.76013 0.00056
29 3.36407 1819.44597 1814.75989 0.00055
30 3.37707 1816.64801 1806.25000 0.00055
31 3.39007 1813.85131 1789.28992 0.00056
32 3.40307 1811.05712 1797.76013 0.00056
33 3.41607 1808.26673 1806.25000 0.00055
34 3.42907 1805.47983 1730.55981 0.00058
35 3.44207 1802.69721 1755.61011 0.00057
36 3.45507 1799.92021 1780.84009 0.00056
37 3.46807 1797.15352 1780.84009 0.00056
38 3.48107 1794.39730 1780.84009 0.00056
39 3.49407 1791.65575 1789.28992 0.00056
40 3.50707 1788.93419 1764.00000 0.00057
41 3.52007 1786.27530 1772.40991 0.00056
42 3.53307 1783.65794 1797.76013 0.00056
43 3.54607 1780.98305 1789.28992 0.00056
44 3.55907 1778.20604 1755.61011 0.00057
45 3.57207 1775.43518 1713.96008 0.00058
46 3.58507 1772.67088 1722.25000 0.00058
47 3.59807 1769.91288 1764.00000 0.00057
48 3.61107 1767.16164 1755.61011 0.00057
49 3.62407 1764.41881 1772.40991 0.00056
50 3.63707 1761.68593 1772.40991 0.00056
51 3.65007 1758.96185 1705.68994 0.00059
52 3.66307 1756.24715 1722.25000 0.00058
53 3.67607 1753.54299 1738.89001 0.00058
54 3.68907 1750.85342 1705.68994 0.00059
55 3.70207 1748.17603 1697.44006 0.00059
56 3.71507 1745.51162 1705.68994 0.00059
57 3.72807 1742.86102 1705.68994 0.00059
58 3.74107 1740.23083 1672.81018 0.00060
59 3.75407 1737.61855 1713.96008 0.00058
60 3.76707 1735.02487 1755.61011 0.00057
61 3.78007 1732.45123 1705.68994 0.00059
62 3.79307 1729.90555 1648.35986 0.00061
63 3.80607 1727.38995 1672.81018 0.00060
64 3.81907 1724.90480 1681.00000 0.00059
65 3.83207 1722.45467 1689.20984 0.00059
66 3.84507 1720.05398 1730.55981 0.00058
67 3.85807 1717.74455 1697.44006 0.00059
68 3.87107 1715.50892 1705.68994 0.00059
69 3.88407 1713.29017 1738.89001 0.00058
70 3.89707 1710.99281 1755.61011 0.00057
71 3.91007 1708.80547 1697.44006 0.00059
72 3.92307 1706.70426 1656.49011 0.00060
73 3.93607 1704.62339 1648.35986 0.00061
74 3.94907 1702.50301 1689.20984 0.00059
75 3.96207 1700.48964 1730.55981 0.00058
76 3.97507 1698.40133 1713.96008 0.00058
77 3.98807 1696.31898 1656.49011 0.00060
78 4.00107 1694.29304 1705.68994 0.00059
79 4.01407 1692.34682 1722.25000 0.00058
80 4.02707 1690.48571 1713.96008 0.00058
81 4.04007 1688.70723 1672.81018 0.00060
82 4.05307 1687.01902 1730.55981 0.00058
83 4.06607 1685.44771 1747.23999 0.00057
84 4.07907 1684.02739 1747.23999 0.00057
85 4.09207 1682.74505 1664.63989 0.00060
86 4.10507 1681.61531 1722.25000 0.00058
87 4.11807 1680.66383 1722.25000 0.00058
88 4.13107 1679.99450 1713.96008 0.00058
89 4.14407 1679.57253 1747.23999 0.00057
90 4.15707 1679.43059 1780.84009 0.00056
91 4.17007 1679.60358 1900.95984 0.00053
92 4.18307 1680.31955 1831.83997 0.00055
93 4.19607 1681.58578 1874.88989 0.00053
94 4.20907 1683.51836 1892.25000 0.00053
95 4.22207 1686.35027 1883.56018 0.00053
96 4.23507 1691.19741 1823.29004 0.00055
97 4.24807 1702.32469 1874.88989 0.00053
98 4.26107 1726.36135 2052.08984 0.00049
99 4.27407 1769.08680 1989.15991 0.00050
100 4.28707 1842.16600 2079.35986 0.00048
101 4.30007 1944.44454 2106.81006 0.00047
102 4.31307 2062.12626 2237.29004 0.00045
103 4.32607 2192.08725 2294.41016 0.00044
104 4.33907 2332.17365 2313.60986 0.00043
105 4.35207 2484.86816 2440.36011 0.00041
106 4.36507 2647.33891 2631.68994 0.00038
107 4.37807 2820.27924 2590.81006 0.00039
108 4.39107 3004.43170 2766.75977 0.00036
109 4.40407 3206.21908 3080.25000 0.00032
110 4.41707 3423.84042 3192.25000 0.00031
111 4.43007 3658.01787 3306.25000 0.00030
112 4.44307 3910.38584 3516.48999 0.00028
113 4.45607 4189.45986 3893.76025 0.00026
114 4.46907 4498.68131 4225.00000 0.00024
115 4.48207 4838.08298 4395.69043 0.00023
116 4.49507 5211.80937 4970.25000 0.00020
117 4.50807 5632.32132 5285.28955 0.00019
118 4.52107 6120.96027 5867.55957 0.00017
119 4.53407 6678.36242 6400.00000 0.00016
120 4.54707 7319.55858 7208.01025 0.00014
121 4.56007 8067.19052 8190.25000 0.00012
122 4.57307 9032.57221 9235.20996 0.00011
123 4.58607 10259.52821 10588.41016 0.00009
124 4.59907 11890.53878 12343.20996 0.00008
125 4.61207 14090.13199 14762.25000 0.00007
126 4.62507 17700.80922 18306.09180 0.00005
127 4.63807 21944.20196 22861.43945 0.00004
128 4.65107 24481.32784 25728.15820 0.00004
129 4.66407 23553.29731 23104.00000 0.00004
130 4.67707 16092.22818 16078.24121 0.00006
131 4.69007 9414.20750 9331.55957 0.00011
132 4.70307 4985.80786 5241.76025 0.00019
133 4.71607 2914.38941 3283.28979 0.00030
134 4.72907 2273.12107 2430.48999 0.00041
135 4.74207 2039.99705 2070.25000 0.00048
136 4.75507 1912.40065 1823.29004 0.00055
137 4.76807 1833.98152 1780.84009 0.00056
138 4.78107 1777.93237 1738.89001 0.00058
139 4.79407 1737.43552 1689.20984 0.00059
140 4.80707 1703.95064 1648.35986 0.00061
141 4.82007 1676.13191 1608.00989 0.00062
142 4.83307 1652.77772 1544.48999 0.00065
143 4.84607 1633.81877 1536.64001 0.00065
144 4.85907 1617.38186 1536.64001 0.00065
145 4.87207 1602.93782 1521.00000 0.00066
146 4.88507 1590.20104 1568.15991 0.00064
147 4.89807 1579.20183 1552.36011 0.00064
148 4.91107 1569.49392 1521.00000 0.00066
149 4.92407 1560.71514 1560.25000 0.00064
150 4.93707 1552.75848 1544.48999 0.00065
151 4.95007 1545.60681 1513.21008 0.00066
152 4.96307 1539.19125 1497.69006 0.00067
153 4.97607 1533.25480 1489.95984 0.00067
154 4.98907 1527.74689 1474.56006 0.00068
155 5.00207 1522.62984 1444.00000 0.00069
156 5.01507 1517.94491 1459.24011 0.00069
157 5.02807 1513.51633 1474.56006 0.00068
158 5.04107 1509.31896 1482.25000 0.00067
159 5.05407 1505.32870 1489.95984 0.00067
160 5.06707 1501.57272 1489.95984 0.00067
161 5.08007 1497.97290 1513.21008 0.00066
162 5.09307 1494.50436 1513.21008 0.00066
163 5.10607 1491.15535 1444.00000 0.00069
164 5.11907 1487.93515 1406.25000 0.00071
165 5.13207 1484.82014 1451.60986 0.00069
166 5.14507 1481.78625 1505.43994 0.00066
167 5.15807 1478.82752 1489.95984 0.00067
168 5.17107 1475.94541 1421.29004 0.00070
169 5.18407 1473.13865 1406.25000 0.00071
170 5.19707 1470.38629 1459.24011 0.00069
171 5.21007 1467.68497 1466.88989 0.00068
172 5.22307 1465.03242 1436.41016 0.00070
173 5.23607 1462.43584 1451.60986 0.00069
174 5.24907 1459.87744 1474.56006 0.00068
175 5.26207 1457.35486 1459.24011 0.00069
176 5.27507 1454.86577 1459.24011 0.00069
177 5.28807 1452.41339 1436.41016 0.00070
178 5.30107 1449.98745 1391.28992 0.00072
179 5.31407 1447.58318 1383.84009 0.00072
180 5.32707 1445.19672 1444.00000 0.00069
181 5.34007 1442.82047 1459.24011 0.00069
182 5.35307 1440.42317 1376.40991 0.00073
183 5.36607 1438.01171 1406.25000 0.00071
184 5.37907 1435.63010 1383.84009 0.00072
185 5.39207 1433.39297 1383.84009 0.00072
186 5.40507 1431.11664 1451.60986 0.00069
187 5.41807 1428.79898 1421.29004 0.00070
188 5.43107 1426.50555 1428.83997 0.00070
189 5.44407 1424.33330 1466.88989 0.00068
190 5.45707 1422.36076 1361.61011 0.00073
191 5.47007 1420.40794 1398.76013 0.00071
192 5.48307 1418.47129 1444.00000 0.00069
193 5.49607 1416.55051 1406.25000 0.00071
194 5.50907 1414.64698 1391.28992 0.00072
195 5.52207 1412.75879 1436.41016 0.00070
196 5.53507 1410.88526 1421.29004 0.00070
197 5.54807 1409.02616 1428.83997 0.00070
198 5.56107 1407.18209 1376.40991 0.00073
199 5.57407 1405.35240 1421.29004 0.00070
200 5.58707 1403.53612 1376.40991 0.00073
201 5.60007 1401.73304 1428.83997 0.00070
202 5.61307 1399.94325 1361.61011 0.00073
203 5.62607 1398.16673 1317.68994 0.00076
204 5.63907 1396.40241 1436.41016 0.00070
205 5.65207 1394.65007 1428.83997 0.00070
206 5.66507 1392.90948 1383.84009 0.00072
207 5.67807 1391.18054 1428.83997 0.00070
208 5.69107 1389.46227 1369.00000 0.00073
209 5.70407 1387.75425 1421.29004 0.00070
210 5.71707 1386.05604 1361.61011 0.00073
211 5.73007 1384.36625 1339.55994 0.00075
212 5.74307 1382.68349 1398.76013 0.00071
213 5.75607 1381.00619 1428.83997 0.00070
214 5.76907 1379.33195 1383.84009 0.00072
215 5.78207 1377.65236 1369.00000 0.00073
216 5.79507 1375.93881 1421.29004 0.00070
217 5.80807 1374.20454 1406.25000 0.00071
218 5.82107 1372.50237 1398.76013 0.00071
219 5.83407 1370.95994 1413.75989 0.00071
220 5.84707 1369.42895 1413.75989 0.00071
221 5.86007 1367.90901 1383.84009 0.00072
222 5.87307 1366.40004 1428.83997 0.00070
223 5.88607 1364.90197 1376.40991 0.00073
224 5.89907 1363.41457 1346.89001 0.00074
225 5.91207 1361.93749 1376.40991 0.00073
226 5.92507 1360.47069 1303.20984 0.00077
227 5.93807 1359.01411 1339.55994 0.00075
228 5.95107 1357.56772 1310.44006 0.00076
229 5.96407 1356.13138 1324.96008 0.00075
230 5.97707 1354.70501 1332.25000 0.00075
231 5.99007 1353.28856 1361.61011 0.00073
232 6.00307 1351.88192 1361.61011 0.00073
233 6.01607 1350.48495 1332.25000 0.00075
234 6.02907 1349.09760 1346.89001 0.00074
235 6.04207 1347.71979 1332.25000 0.00075
236 6.05507 1346.35136 1339.55994 0.00075
237 6.06807 1344.99204 1354.23999 0.00074
238 6.08107 1343.64184 1332.25000 0.00075
239 6.09407 1342.30062 1310.44006 0.00076
240 6.10707 1340.96826 1317.68994 0.00076
241 6.12007 1339.64398 1281.63989 0.00078
242 6.13307 1338.32795 1303.20984 0.00077
243 6.14607 1337.01991 1317.68994 0.00076
244 6.15907 1335.71957 1339.55994 0.00075
245 6.17207 1334.42551 1332.25000 0.00075
246 6.18507 1333.13731 1317.68994 0.00076
247 6.19807 1331.85432 1339.55994 0.00075
248 6.21107 1330.57540 1339.55994 0.00075
249 6.22407 1329.29655 1303.20984 0.00077
250 6.23707 1328.00965 1317.68994 0.00076
251 6.25007 1326.69898 1317.68994 0.00076
252 6.26307 1325.40410 1310.44006 0.00076
253 6.27607 1324.23105 1303.20984 0.00077
254 6.28907 1322.81856 1324.96008 0.00075
255 6.30207 1321.66437 1369.00000 0.00073
256 6.31507 1320.51957 1369.00000 0.00073
257 6.32807 1319.38414 1361.61011 0.00073
258 6.34107 1318.25805 1376.40991 0.00073
259 6.35407 1317.14128 1361.61011 0.00073
260 6.36707 1316.03380 1317.68994 0.00076
261 6.38007 1314.93559 1324.96008 0.00075
262 6.39307 1313.84661 1324.96008 0.00075
263 6.40607 1312.76684 1317.68994 0.00076
264 6.41907 1311.69626 1288.81006 0.00078
265 6.43207 1310.63483 1324.96008 0.00075
266 6.44507 1309.58254 1339.55994 0.00075
267 6.45807 1308.53935 1310.44006 0.00076
268 6.47107 1307.50523 1324.96008 0.00075
269 6.48407 1306.48016 1339.55994 0.00075
270 6.49707 1305.46411 1369.00000 0.00073
271 6.51007 1304.45705 1346.89001 0.00074
272 6.52307 1303.45895 1296.00000 0.00077
273 6.53607 1302.46978 1225.00000 0.00082
274 6.54907 1301.48952 1239.04004 0.00081
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1791 26.27007 1889.90063 1936.00000 0.00052
1792 26.28307 1888.13565 1944.80981 0.00051
1793 26.29607 1886.51433 1883.56018 0.00053
1794 26.30907 1885.02075 1849.00000 0.00054
1795 26.32207 1883.65012 1806.25000 0.00055
1796 26.33507 1882.38919 1900.95984 0.00053
1797 26.34807 1881.24043 1857.60986 0.00054
1798 26.36107 1880.21101 1849.00000 0.00054
1799 26.37407 1879.22220 1764.00000 0.00057
1800 26.38707 1878.30866 1797.76013 0.00056
1801 26.40007 1877.51470 1918.43994 0.00052
1802 26.41307 1877.08963 1971.36011 0.00051
1803 26.42607 1876.87221 1823.29004 0.00055
1804 26.43907 1877.46546 1755.61011 0.00057
1805 26.45207 1878.44701 1857.60986 0.00054
1806 26.46507 1879.50766 1849.00000 0.00054
1807 26.47807 1879.42046 1849.00000 0.00054
1808 26.49107 1878.17134 1849.00000 0.00054
1809 26.50407 1876.15092 1840.41016 0.00054
1810 26.51707 1874.24514 1874.88989 0.00053
1811 26.53007 1873.03081 1831.83997 0.00055
1812 26.54307 1871.75692 1840.41016 0.00054
1813 26.55607 1870.17914 1789.28992 0.00056
1814 26.56907 1868.77249 1814.75989 0.00055
1815 26.58207 1867.71182 1814.75989 0.00055
1816 26.59507 1866.99306 1831.83997 0.00055
1817 26.60807 1866.41967 1789.28992 0.00056
1818 26.62107 1866.13665 1900.95984 0.00053
1819 26.63407 1866.07388 1806.25000 0.00055
1820 26.64707 1866.19698 1831.83997 0.00055
1821 26.66007 1866.47620 1814.75989 0.00055
1822 26.67307 1866.92531 1857.60986 0.00054
1823 26.68607 1867.52423 1730.55981 0.00058
1824 26.69907 1868.28244 1823.29004 0.00055
1825 26.71207 1869.27315 1874.88989 0.00053
1826 26.72507 1870.46038 1789.28992 0.00056
1827 26.73807 1871.87207 1874.88989 0.00053
1828 26.75107 1873.53276 1823.29004 0.00055
1829 26.76407 1875.56992 1814.75989 0.00055
1830 26.77707 1877.94904 1857.60986 0.00054
1831 26.79007 1880.54722 1840.41016 0.00054
1832 26.80307 1883.50821 1814.75989 0.00055
1833 26.81607 1886.99815 1789.28992 0.00056
1834 26.82907 1891.09522 1840.41016 0.00054
1835 26.84207 1895.79981 1814.75989 0.00055
1836 26.85507 1901.18230 1806.25000 0.00055
1837 26.86807 1907.48341 1857.60986 0.00054
1838 26.88107 1915.10123 1866.24011 0.00054
1839 26.89407 1923.99046 1823.29004 0.00055
1840 26.90707 1934.37004 1857.60986 0.00054
1841 26.92007 1946.56215 1849.00000 0.00054
1842 26.93307 1962.14310 1874.88989 0.00053
1843 26.94607 1981.10341 1909.69006 0.00052
1844 26.95907 2004.60032 1927.21008 0.00052
1845 26.97207 2033.44992 2007.03992 0.00050
1846 26.98507 2073.23413 2070.25000 0.00048
1847 26.99807 2127.28823 2190.23999 0.00046
1848 27.01107 2201.42043 2284.83984 0.00044
1849 27.02407 2304.32900 2460.15991 0.00041
1850 27.03707 2469.69487 2693.61011 0.00037
1851 27.05007 2757.19014 3069.16016 0.00033
1852 27.06307 3205.04340 3576.03979 0.00028
1853 27.07607 3841.64513 4199.04053 0.00024
1854 27.08907 4717.81570 4733.44043 0.00021
1855 27.10207 5636.66898 5112.25000 0.00020
1856 27.11507 6164.79707 5461.21045 0.00018
1857 27.12807 6143.54758 5550.25000 0.00018
1858 27.14107 5424.14825 5329.00000 0.00019
1859 27.15407 4817.39867 5083.69043 0.00020
1860 27.16707 4483.21598 4802.49023 0.00021
1861 27.18007 4283.38845 4435.55957 0.00023
1862 27.19307 4069.41015 4070.43994 0.00025
1863 27.20607 3620.74639 3696.63989 0.00027
1864 27.21907 3164.54757 3283.28979 0.00030
1865 27.23207 2773.37083 2862.25000 0.00035
1866 27.24507 2486.17509 2580.63989 0.00039
1867 27.25807 2310.83272 2371.69019 0.00042
1868 27.27107 2196.85283 2180.89014 0.00046
1869 27.28407 2117.13957 2106.81006 0.00047
1870 27.29707 2061.86686 2070.25000 0.00048
1871 27.31007 2024.41125 1962.48999 0.00051
1872 27.32307 1998.91494 1936.00000 0.00052
1873 27.33607 1979.84092 1918.43994 0.00052
1874 27.34907 1961.56328 1900.95984 0.00053
1875 27.36207 1944.13625 1909.69006 0.00052
1876 27.37507 1927.02239 1883.56018 0.00053
1877 27.38807 1912.75440 1849.00000 0.00054
1878 27.40107 1902.61628 1831.83997 0.00055
1879 27.41407 1894.92665 1892.25000 0.00053
1880 27.42707 1889.24064 1874.88989 0.00053
1881 27.44007 1884.56303 1849.00000 0.00054
1882 27.45307 1882.58145 1857.60986 0.00054
1883 27.46607 1886.29282 1953.64001 0.00051
1884 27.47907 1899.13161 1953.64001 0.00051
1885 27.49207 1920.56722 2052.08984 0.00049
1886 27.50507 1948.74822 2070.25000 0.00048
1887 27.51807 1979.37711 2034.00989 0.00049
1888 27.53107 1987.99670 2143.68994 0.00047
1889 27.54407 1972.52435 2116.00000 0.00047
1890 27.55707 1944.18269 2134.44019 0.00047
1891 27.57007 1919.89466 2097.63989 0.00048
1892 27.58307 1911.57649 1962.48999 0.00051
1893 27.59607 1903.90763 1971.36011 0.00051
1894 27.60907 1892.80044 1953.64001 0.00051
1895 27.62207 1875.54371 1962.48999 0.00051
1896 27.63507 1857.46635 1892.25000 0.00053
1897 27.64807 1844.01237 1780.84009 0.00056
1898 27.66107 1834.31925 1780.84009 0.00056
1899 27.67407 1827.86500 1747.23999 0.00057
1900 27.68707 1823.94155 1755.61011 0.00057
1901 27.70007 1821.37523 1722.25000 0.00058
1902 27.71307 1819.62970 1722.25000 0.00058
1903 27.72607 1818.70164 1755.61011 0.00057
1904 27.73907 1818.14443 1755.61011 0.00057
1905 27.75207 1818.36611 1681.00000 0.00059
1906 27.76507 1818.98186 1713.96008 0.00058
1907 27.77807 1820.00949 1689.20984 0.00059
1908 27.79107 1821.52241 1823.29004 0.00055
1909 27.80407 1823.48120 1780.84009 0.00056
1910 27.81707 1825.89127 1755.61011 0.00057
1911 27.83007 1828.86972 1689.20984 0.00059
1912 27.84307 1832.63910 1689.20984 0.00059
1913 27.85607 1837.15487 1831.83997 0.00055
1914 27.86907 1842.42335 1780.84009 0.00056
1915 27.88207 1848.63792 1772.40991 0.00056
1916 27.89507 1856.21087 1722.25000 0.00058
1917 27.90807 1865.32978 1789.28992 0.00056
1918 27.92107 1876.19414 1866.24011 0.00054
1919 27.93407 1889.17113 1823.29004 0.00055
1920 27.94707 1905.32568 1962.48999 0.00051
1921 27.96007 1926.16820 1953.64001 0.00051
1922 27.97307 1952.35063 1998.09009 0.00050
1923 27.98607 1985.58244 2025.00000 0.00049
1924 27.99907 2029.03923 2070.25000 0.00048
1925 28.01207 2094.45280 2227.84009 0.00045
1926 28.02507 2190.29578 2440.36011 0.00041
1927 28.03807 2334.25499 2580.63989 0.00039
1928 28.05107 2546.01135 2937.64014 0.00034
1929 28.06407 2936.04696 3192.25000 0.00031
1930 28.07707 3485.84013 3588.01025 0.00028
1931 28.09007 4132.59224 3994.23999 0.00025
1932 28.10307 4782.63990 4160.25000 0.00024
1933 28.11607 4992.48971 4290.25000 0.00023
1934 28.12907 4604.95674 4435.55957 0.00023
1935 28.14207 4116.00792 4356.00000 0.00023
1936 28.15507 3765.46944 4160.25000 0.00024
1937 28.16807 3711.82749 3918.75977 0.00026
1938 28.18107 3683.25902 3856.40991 0.00026
1939 28.19407 3547.57588 3636.08984 0.00028
1940 28.20707 3305.55686 3552.15991 0.00028
1941 28.22007 3039.76484 3398.88989 0.00029
1942 28.23307 2929.68572 3294.76025 0.00030
1943 28.24607 2950.78880 3329.29004 0.00030
1944 28.25907 3131.06641 3504.64014 0.00029
1945 28.27207 3472.84980 3806.89014 0.00026
1946 28.28507 3880.51155 4057.69019 0.00025
1947 28.29807 4302.35369 4316.48975 0.00023
1948 28.31107 4760.14733 4475.61035 0.00022
1949 28.32407 4895.10039 4475.61035 0.00022
1950 28.33707 4661.87939 4382.43945 0.00023
1951 28.35007 4156.07510 4212.01025 0.00024
1952 28.36307 3734.19340 3918.75977 0.00026
1953 28.37607 3575.97987 3660.25000 0.00027
1954 28.38907 3448.06397 3469.21021 0.00029
1955 28.40207 3291.77785 3237.61011 0.00031
1956 28.41507 3018.97792 3014.01025 0.00033
1957 28.42807 2719.23996 2756.25000 0.00036
1958 28.44107 2504.27664 2520.04004 0.00040
1959 28.45407 2342.46072 2371.69019 0.00042
1960 28.46707 2217.04274 2171.55981 0.00046
1961 28.48007 2123.45667 1998.09009 0.00050
1962 28.49307 2057.14784 1989.15991 0.00050
1963 28.50607 2022.64990 1944.80981 0.00051
1964 28.51907 2002.92763 1849.00000 0.00054
1965 28.53207 1990.43392 1806.25000 0.00055
1966 28.54507 1976.85948 1797.76013 0.00056
1967 28.55807 1952.84658 1806.25000 0.00055
1968 28.57107 1920.70334 1831.83997 0.00055
1969 28.58407 1890.70982 1789.28992 0.00056
1970 28.59707 1868.97298 1705.68994 0.00059
1971 28.61007 1859.21909 1713.96008 0.00058
1972 28.62307 1852.97875 1764.00000 0.00057
1973 28.63607 1846.71733 1814.75989 0.00055
1974 28.64907 1840.42955 1789.28992 0.00056
1975 28.66207 1837.13444 1772.40991 0.00056
1976 28.67507 1843.77335 1840.41016 0.00054
1977 28.68807 1862.47267 1900.95984 0.00053
1978 28.70107 1897.61523 1936.00000 0.00052
1979 28.71407 1956.79397 1989.15991 0.00050
1980 28.72707 2055.21973 2043.04004 0.00049
1981 28.74007 2167.00657 2061.16016 0.00049
1982 28.75307 2257.84325 2134.44019 0.00047
1983 28.76607 2289.83238 2162.25000 0.00046
1984 28.77907 2179.61645 2125.20996 0.00047
1985 28.79207 2091.91555 2088.48999 0.00048
1986 28.80507 2039.73742 2088.48999 0.00048
1987 28.81807 2027.21812 2079.35986 0.00048
1988 28.83107 2020.36284 2034.00989 0.00049
1989 28.84407 1980.00457 2016.01013 0.00050
1990 28.85707 1924.59811 1892.25000 0.00053
1991 28.87007 1866.65276 1849.00000 0.00054
1992 28.88307 1827.49409 1764.00000 0.00057
1993 28.89607 1803.89241 1747.23999 0.00057
1994 28.90907 1788.37815 1764.00000 0.00057
1995 28.92207 1778.96650 1747.23999 0.00057
1996 28.93507 1774.40542 1738.89001 0.00058
1997 28.94807 1773.60484 1713.96008 0.00058
1998 28.96107 1775.47790 1764.00000 0.00057
1999 28.97407 1780.30061 1689.20984 0.00059
2000 28.98707 1789.90554 1738.89001 0.00058
2001 29.00007 1805.15982 1747.23999 0.00057
2002 29.01307 1828.06329 1789.28992 0.00056
2003 29.02607 1861.31016 1823.29004 0.00055
2004 29.03907 1922.61725 1780.84009 0.00056
2005 29.05207 2023.03297 1874.88989 0.00053
2006 29.06507 2167.87971 2052.08984 0.00049
2007 29.07807 2357.12561 2209.00000 0.00045
2008 29.09107 2567.78656 2265.75977 0.00044
2009 29.10407 2663.40684 2371.69019 0.00042
2010 29.11707 2615.09332 2371.69019 0.00042
2011 29.13007 2453.82129 2294.41016 0.00044
2012 29.14307 2329.27008 2199.61011 0.00045
2013 29.15607 2305.68560 2218.40991 0.00045
2014 29.16907 2314.88895 2256.25000 0.00044
2015 29.18207 2329.45625 2180.89014 0.00046
2016 29.19507 2316.07425 2256.25000 0.00044
2017 29.20807 2321.66015 2294.41016 0.00044
2018 29.22107 2401.14427 2246.76025 0.00045
2019 29.23407 2525.07612 2246.76025 0.00045
2020 29.24707 2651.70274 2361.95996 0.00042
2021 29.26007 2682.46866 2284.83984 0.00044
2022 29.27307 2521.97931 2361.95996 0.00042
2023 29.28607 2362.06544 2275.29004 0.00044
2024 29.29907 2248.03232 2143.68994 0.00047
2025 29.31207 2211.04507 2106.81006 0.00047
2026 29.32507 2191.88126 2152.96021 0.00046
2027 29.33807 2134.27287 2034.00989 0.00049
2028 29.35107 2046.66823 2007.03992 0.00050
2029 29.36407 1942.46375 1936.00000 0.00052
2030 29.37707 1867.05881 1831.83997 0.00055
2031 29.39007 1813.90454 1764.00000 0.00057
2032 29.40307 1776.51484 1730.55981 0.00058
2033 29.41607 1750.73475 1697.44006 0.00059
2034 29.42907 1733.68813 1713.96008 0.00058
2035 29.44207 1721.05977 1697.44006 0.00059
2036 29.45507 1711.00585 1697.44006 0.00059
2037 29.46807 1702.98981 1681.00000 0.00059
2038 29.48107 1696.82230 1656.49011 0.00060
2039 29.49407 1691.95928 1648.35986 0.00061
2040 29.50707 1687.91443 1648.35986 0.00061
2041 29.52007 1684.57344 1747.23999 0.00057
2042 29.53307 1681.86162 1664.63989 0.00060
2043 29.54607 1679.76535 1640.25000 0.00061
2044 29.55907 1678.09171 1648.35986 0.00061
2045 29.57207 1676.79069 1664.63989 0.00060
2046 29.58507 1675.84150 1648.35986 0.00061
2047 29.59807 1675.28602 1632.16016 0.00061
2048 29.61107 1675.10921 1681.00000 0.00059
2049 29.62407 1675.26538 1689.20984 0.00059
2050 29.63707 1675.87279 1640.25000 0.00061
2051 29.65007 1676.84902 1648.35986 0.00061
2052 29.66307 1678.33343 1664.63989 0.00060
2053 29.67607 1680.31115 1689.20984 0.00059
2054 29.68907 1682.82373 1664.63989 0.00060
2055 29.70207 1685.93676 1664.63989 0.00060
2056 29.71507 1689.86412 1672.81018 0.00060
2057 29.72807 1694.78872 1640.25000 0.00061
2058 29.74107 1700.77421 1664.63989 0.00060
2059 29.75407 1708.00908 1730.55981 0.00058
2060 29.76707 1717.02805 1697.44006 0.00059
2061 29.78007 1728.92095 1672.81018 0.00060
2062 29.79307 1744.01136 1755.61011 0.00057
2063 29.80607 1763.29862 1823.29004 0.00055
2064 29.81907 1788.15523 1823.29004 0.00055
2065 29.83207 1826.32798 1883.56018 0.00053
2066 29.84507 1882.39842 1989.15991 0.00050
2067 29.85807 1966.98878 2143.68994 0.00047
2068 29.87107 2091.24086 2284.83984 0.00044
2069 29.88407 2306.87875 2440.36011 0.00041
2070 29.89707 2609.39996 2693.61011 0.00037
2071 29.91007 2949.42404 2883.69019 0.00035
2072 29.92307 3266.58479 2970.25000 0.00034
2073 29.93607 3364.25598 3003.03979 0.00033
2074 29.94907 3163.56084 3025.00000 0.00033
2075 29.96207 2913.94226 2992.09009 0.00033
2076 29.97507 2713.58855 2872.95972 0.00035
2077 29.98807 2647.29038 2735.29004 0.00037
2078 30.00107 2622.88489 2672.89014 0.00037
2079 30.01407 2553.47053 2590.81006 0.00039
2080 30.02707 2433.40580 2401.00000 0.00042
2081 30.04007 2272.85445 2294.41016 0.00044
2082 30.05307 2151.87690 2171.55981 0.00046
2083 30.06607 2072.80234 2134.44019 0.00047
2084 30.07907 2032.16697 2152.96021 0.00046
2085 30.09207 2028.61782 2106.81006 0.00047
2086 30.10507 2073.13955 2218.40991 0.00045
2087 30.11807 2167.35716 2440.36011 0.00041
2088 30.13107 2325.56026 2530.08984 0.00040
2089 30.14407 2568.81104 2840.88989 0.00035
2090 30.15707 2944.02761 3124.81006 0.00032
2091 30.17007 3337.46416 3306.25000 0.00030
2092 30.18307 3641.32080 3552.15991 0.00028
2093 30.19607 3752.07226 3588.01025 0.00028
2094 30.20907 3495.36231 3576.03979 0.00028
2095 30.22207 3278.22646 3516.48999 0.00028
2096 30.23507 3192.59891 3588.01025 0.00028
2097 30.24807 3260.03156 3504.64014 0.00029
2098 30.26107 3405.09917 3422.25000 0.00029
2099 30.27407 3484.41460 3457.43994 0.00029
2100 30.28707 3387.22281 3410.56006 0.00029
2101 30.30007 3139.78613 3058.08984 0.00033
2102 30.31307 2861.26262 2948.48999 0.00034
2103 30.32607 2649.03067 2798.41016 0.00036
2104 30.33907 2562.53627 2693.61011 0.00037
2105 30.35207 2533.05665 2601.00000 0.00038
2106 30.36507 2540.87925 2704.00000 0.00037
2107 30.37807 2591.39820 2601.00000 0.00038
2108 30.39107 2688.62103 2862.25000 0.00035
2109 30.40407 2884.61337 3058.08984 0.00033
2110 30.41707 3194.85046 3340.83984 0.00030
2111 30.43007 3532.72604 3469.21021 0.00029
2112 30.44307 3701.69666 3636.08984 0.00028
2113 30.45607 3643.51695 3528.36011 0.00028
2114 30.46907 3329.61795 3445.69019 0.00029
2115 30.48207 3030.13293 3294.76025 0.00030
2116 30.49507 2864.31585 3058.08984 0.00033
2117 30.50807 2776.50748 2959.36011 0.00034
2118 30.52107 2717.88623 2756.25000 0.00036
2119 30.53407 2586.99928 2560.35986 0.00039
2120 30.54707 2397.47207 2430.48999 0.00041
2121 30.56007 2207.17758 2237.29004 0.00045
2122 30.57307 2041.96376 2007.03992 0.00050
2123 30.58607 1924.51378 1953.64001 0.00051
2124 30.59907 1846.28574 1755.61011 0.00057
2125 30.61207 1789.35575 1705.68994 0.00059
2126 30.62507 1748.37481 1722.25000 0.00058
2127 30.63807 1718.98762 1730.55981 0.00058
2128 30.65107 1698.13747 1713.96008 0.00058
2129 30.66407 1681.27431 1681.00000 0.00059
2130 30.67707 1667.50204 1681.00000 0.00059
2131 30.69007 1656.24968 1656.49011 0.00060
2132 30.70307 1647.45932 1689.20984 0.00059
2133 30.71607 1640.17411 1681.00000 0.00059
2134 30.72907 1633.93575 1689.20984 0.00059
2135 30.74207 1628.96782 1697.44006 0.00059
2136 30.75507 1625.13758 1664.63989 0.00060
2137 30.76807 1622.22340 1689.20984 0.00059
2138 30.78107 1620.09170 1681.00000 0.00059
2139 30.79407 1618.90943 1624.08997 0.00062
2140 30.80707 1618.69438 1640.25000 0.00061
2141 30.82007 1619.48115 1697.44006 0.00059
2142 30.83307 1621.33047 1664.63989 0.00060
2143 30.84607 1625.09872 1656.49011 0.00060
2144 30.85907 1631.27779 1681.00000 0.00059
2145 30.87207 1640.82583 1697.44006 0.00059
2146 30.88507 1654.85672 1632.16016 0.00061
2147 30.89807 1678.74281 1697.44006 0.00059
2148 30.91107 1716.56094 1705.68994 0.00059
2149 30.92407 1767.23629 1764.00000 0.00057
2150 30.93707 1828.45753 1797.76013 0.00056
2151 30.95007 1890.58010 1823.29004 0.00055
2152 30.96307 1920.54291 1806.25000 0.00055
2153 30.97607 1918.45496 1849.00000 0.00054
2154 30.98907 1896.51199 1857.60986 0.00054
2155 31.00207 1879.84067 1866.24011 0.00054
2156 31.01507 1902.36648 1909.69006 0.00052
2157 31.02807 1956.80397 2052.08984 0.00049
2158 31.04107 2043.88790 2162.25000 0.00046
2159 31.05407 2163.18502 2304.00000 0.00043
2160 31.06707 2327.40851 2450.25000 0.00041
2161 31.08007 2491.35536 2601.00000 0.00038
2162 31.09307 2597.46031 2756.25000 0.00036
2163 31.10607 2608.41515 2724.84009 0.00037
2164 31.11907 2464.83620 2601.00000 0.00038
2165 31.13207 2320.91453 2510.00977 0.00040
2166 31.14507 2217.45047 2440.36011 0.00041
2167 31.15807 2162.65322 2430.48999 0.00041
2168 31.17107 2137.65371 2332.88989 0.00043
2169 31.18407 2086.35915 2218.40991 0.00045
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