#------------------------------------------------------------------------------
#$Date: 2019-11-07 21:24:17 +0200 (Thu, 07 Nov 2019) $
#$Revision: 223499 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/23/33/7233350.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7233350
loop_
_publ_author_name
'Wang, Yue'
'Shi, Yongfang'
'Zou, Xiaochuan'
'He, Yucen'
'Wang, Xia'
_publ_section_title
;
 Pyridylphosphine supported Ag(i) and Cu(i) complexes for detection of
 alcohols and nitriles via structural transformations from 1D to 0D
;
_journal_issue                   37
_journal_name_full               CrystEngComm
_journal_page_first              5595
_journal_paper_doi               10.1039/C9CE00943D
_journal_volume                  21
_journal_year                    2019
_chemical_formula_sum            'C34 H28 Cl2 Cu2 N2 O8 P2'
_chemical_formula_weight         852.50
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2016/6
_audit_update_record
;
2019-06-16 deposited with the CCDC.    2019-08-06 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 101.679(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   9.1529(5)
_cell_length_b                   18.4467(10)
_cell_length_c                   20.8604(13)
_cell_measurement_reflns_used    9869
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      27.10
_cell_measurement_theta_min      2.54
_cell_volume                     3449.2(3)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2016/6 (Sheldrick, 2016)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0347
_diffrn_reflns_av_unetI/netI     0.0184
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.998
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            59958
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.998
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.145
_diffrn_reflns_theta_min         2.208
_exptl_absorpt_coefficient_mu    1.536
_exptl_absorpt_correction_T_max  0.650
_exptl_absorpt_correction_T_min  0.563
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            'Light Yellow'
_exptl_crystal_density_diffrn    1.642
_exptl_crystal_description       Bloc
_exptl_crystal_F_000             1728
_exptl_crystal_size_max          0.38
_exptl_crystal_size_mid          0.34
_exptl_crystal_size_min          0.28
_refine_diff_density_max         0.685
_refine_diff_density_min         -0.854
_refine_diff_density_rms         0.218
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.021
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     451
_refine_ls_number_reflns         7641
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.021
_refine_ls_R_factor_all          0.0308
_refine_ls_R_factor_gt           0.0246
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0522P)²+4.3631P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0726
_refine_ls_wR_factor_ref         0.0916
_reflns_Friedel_coverage         0.000
_reflns_number_gt                6947
_reflns_number_total             7641
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c9ce00943d2.cif
_cod_data_source_block           Cu2
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4973 2017-02-22 13:04:09Z antanas 

 Adding full bibliography for 7233348--7233351.cif.
;
_cod_database_code               7233350
_shelx_shelxl_version_number     2016/6
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
Cu1 Cu 0.61869(3) 0.70855(2) 0.34800(2) 0.01365(7) Uani 1 1 d . .
Cu2 Cu 0.25346(3) 0.71246(2) 0.31338(2) 0.01660(8) Uani 1 1 d . .
P1 P 0.50365(5) 0.60184(3) 0.32301(2) 0.01231(11) Uani 1 1 d . .
P2 P 0.51227(6) 0.81564(3) 0.36309(3) 0.01348(11) Uani 1 1 d . .
Cl1 Cl 0.80959(6) 0.68972(3) 0.48655(2) 0.01859(11) Uani 1 1 d . .
Cl2 Cl 0.86984(6) 0.69749(3) 0.25578(2) 0.01740(11) Uani 1 1 d . .
O1 O 0.82666(17) 0.69295(9) 0.41830(7) 0.0200(3) Uani 1 1 d . .
O2 O 0.67420(19) 0.65076(9) 0.48887(8) 0.0258(3) Uani 1 1 d . .
O3 O 0.9359(2) 0.65256(13) 0.52380(9) 0.0410(5) Uani 1 1 d . .
O4 O 0.8006(2) 0.76178(10) 0.51054(10) 0.0364(4) Uani 1 1 d . .
O5 O 0.73771(17) 0.73386(9) 0.26980(8) 0.0211(3) Uani 1 1 d . .
O6 O 0.8733(2) 0.62346(9) 0.27643(9) 0.0305(4) Uani 1 1 d . .
O7 O 0.99945(18) 0.73574(10) 0.29245(9) 0.0290(4) Uani 1 1 d . .
O8 O 0.8674(2) 0.70337(10) 0.18730(9) 0.0311(4) Uani 1 1 d . .
N1 N 0.26451(19) 0.63445(9) 0.37447(9) 0.0160(3) Uani 1 1 d . .
N2 N 0.2954(2) 0.78913(9) 0.25825(9) 0.0164(4) Uani 1 1 d . .
C1 C 0.3822(2) 0.59997(11) 0.24174(10) 0.0158(4) Uani 1 1 d . .
C2 C 0.2328(3) 0.57812(13) 0.22975(11) 0.0225(4) Uani 1 1 d . .
H2B H 0.189905 0.561121 0.264776 0.027 Uiso 1 1 calc R U
C3 C 0.1469(3) 0.58125(15) 0.16665(12) 0.0302(5) Uani 1 1 d . .
H3B H 0.044983 0.567179 0.158727 0.036 Uiso 1 1 calc R U
C4 C 0.2099(3) 0.60484(15) 0.11544(12) 0.0319(6) Uani 1 1 d . .
H4B H 0.151133 0.606973 0.072378 0.038 Uiso 1 1 calc R U
C5 C 0.3583(3) 0.62533(14) 0.12670(12) 0.0295(5) Uani 1 1 d . .
H5A H 0.401574 0.640532 0.091216 0.035 Uiso 1 1 calc R U
C6 C 0.4439(3) 0.62376(12) 0.18956(11) 0.0223(4) Uani 1 1 d . .
H6B H 0.545118 0.638960 0.197162 0.027 Uiso 1 1 calc R U
C7 C 0.6072(2) 0.51736(11) 0.32727(10) 0.0148(4) Uani 1 1 d . .
C8 C 0.7504(2) 0.51432(11) 0.36647(10) 0.0169(4) Uani 1 1 d . .
H8B H 0.794516 0.556685 0.388034 0.020 Uiso 1 1 calc R U
C9 C 0.8281(3) 0.44904(12) 0.37379(11) 0.0217(4) Uani 1 1 d . .
H9A H 0.924939 0.446846 0.400759 0.026 Uiso 1 1 calc R U
C10 C 0.7650(3) 0.38715(12) 0.34197(13) 0.0255(5) Uani 1 1 d . .
H10A H 0.818531 0.342704 0.347242 0.031 Uiso 1 1 calc R U
C11 C 0.6236(3) 0.39016(12) 0.30241(13) 0.0271(5) Uani 1 1 d . .
H11A H 0.580721 0.347848 0.280315 0.033 Uiso 1 1 calc R U
C12 C 0.5445(2) 0.45511(12) 0.29507(12) 0.0215(4) Uani 1 1 d . .
H12A H 0.447637 0.457009 0.268076 0.026 Uiso 1 1 calc R U
C13 C 0.3734(2) 0.58401(11) 0.37748(10) 0.0139(4) Uani 1 1 d . .
C14 C 0.3853(2) 0.52596(11) 0.42059(10) 0.0175(4) Uani 1 1 d . .
H14A H 0.462420 0.491111 0.422254 0.021 Uiso 1 1 calc R U
C15 C 0.2829(3) 0.51940(12) 0.46135(11) 0.0215(4) Uani 1 1 d . .
H15A H 0.289917 0.480432 0.491596 0.026 Uiso 1 1 calc R U
C16 C 0.1712(3) 0.57042(13) 0.45708(11) 0.0221(4) Uani 1 1 d . .
H16A H 0.099277 0.566672 0.483998 0.027 Uiso 1 1 calc R U
C17 C 0.1649(2) 0.62719(12) 0.41310(11) 0.0191(4) Uani 1 1 d . .
H17A H 0.087524 0.662091 0.410249 0.023 Uiso 1 1 calc R U
C18 C 0.3788(2) 0.81561(11) 0.41737(10) 0.0164(4) Uani 1 1 d . .
C19 C 0.4252(3) 0.78384(13) 0.47893(12) 0.0263(5) Uani 1 1 d . .
H19A H 0.524292 0.765999 0.491372 0.032 Uiso 1 1 calc R U
C20 C 0.3288(3) 0.77796(15) 0.52218(13) 0.0322(6) Uani 1 1 d . .
H20A H 0.362502 0.757277 0.564285 0.039 Uiso 1 1 calc R U
C21 C 0.1835(3) 0.80232(14) 0.50374(13) 0.0288(5) Uani 1 1 d . .
H21A H 0.116182 0.796931 0.532633 0.035 Uiso 1 1 calc R U
C22 C 0.1365(3) 0.83420(16) 0.44384(13) 0.0327(6) Uani 1 1 d . .
H22A H 0.036806 0.851212 0.431626 0.039 Uiso 1 1 calc R U
C23 C 0.2332(3) 0.84201(14) 0.40054(12) 0.0255(5) Uani 1 1 d . .
H23A H 0.200008 0.865323 0.359571 0.031 Uiso 1 1 calc R U
C24 C 0.6289(2) 0.89515(11) 0.38572(10) 0.0171(4) Uani 1 1 d . .
C25 C 0.5991(3) 0.94728(12) 0.42974(11) 0.0222(4) Uani 1 1 d . .
H25A H 0.514674 0.942065 0.449370 0.027 Uiso 1 1 calc R U
C26 C 0.6929(3) 1.00700(14) 0.44503(13) 0.0298(5) Uani 1 1 d . .
H26A H 0.673633 1.041803 0.475853 0.036 Uiso 1 1 calc R U
C27 C 0.8138(3) 1.01569(14) 0.41545(14) 0.0314(6) Uani 1 1 d . .
H27A H 0.877004 1.056688 0.425650 0.038 Uiso 1 1 calc R U
C28 C 0.8430(3) 0.96472(14) 0.37092(15) 0.0343(6) Uani 1 1 d . .
H28A H 0.924826 0.971435 0.349892 0.041 Uiso 1 1 calc R U
C29 C 0.7529(3) 0.90377(13) 0.35692(13) 0.0281(5) Uani 1 1 d . .
H29A H 0.775638 0.867941 0.327725 0.034 Uiso 1 1 calc R U
C30 C 0.4007(2) 0.83953(11) 0.28236(10) 0.0160(4) Uani 1 1 d . .
C31 C 0.4278(2) 0.89851(12) 0.24544(12) 0.0226(5) Uani 1 1 d . .
H31A H 0.499720 0.933995 0.263410 0.027 Uiso 1 1 calc R U
C32 C 0.3478(3) 0.90479(14) 0.18166(12) 0.0269(5) Uani 1 1 d . .
H32A H 0.365014 0.944713 0.155380 0.032 Uiso 1 1 calc R U
C33 C 0.2430(3) 0.85282(14) 0.15642(11) 0.0255(5) Uani 1 1 d . .
H33A H 0.188970 0.855917 0.112539 0.031 Uiso 1 1 calc R U
C34 C 0.2185(3) 0.79615(12) 0.19652(11) 0.0212(4) Uani 1 1 d . .
H34A H 0.144725 0.761019 0.179763 0.025 Uiso 1 1 calc R U
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_3
O1 Cu1 O5 91.78(6) .
O1 Cu1 P1 110.26(5) .
O5 Cu1 P1 107.16(5) .
O1 Cu1 P2 111.47(5) .
O5 Cu1 P2 102.22(4) .
P1 Cu1 P2 127.31(2) .
N2 Cu2 N1 165.69(8) .
N2 Cu2 O7 93.76(7) 1_455
N1 Cu2 O7 100.42(7) 1_455
C7 P1 C1 104.03(9) .
C7 P1 C13 102.35(9) .
C1 P1 C13 102.80(9) .
C7 P1 Cu1 121.70(7) .
C1 P1 Cu1 113.60(7) .
C13 P1 Cu1 110.27(7) .
C24 P2 C18 105.69(10) .
C24 P2 C30 103.44(10) .
C18 P2 C30 104.53(10) .
C24 P2 Cu1 119.72(7) .
C18 P2 Cu1 116.67(7) .
C30 P2 Cu1 104.95(7) .
O4 Cl1 O3 110.68(13) .
O4 Cl1 O2 109.94(11) .
O3 Cl1 O2 110.40(12) .
O4 Cl1 O1 109.13(11) .
O3 Cl1 O1 108.29(10) .
O2 Cl1 O1 108.33(10) .
O8 Cl2 O6 111.64(11) .
O8 Cl2 O7 109.55(11) .
O6 Cl2 O7 109.78(11) .
O8 Cl2 O5 108.58(10) .
O6 Cl2 O5 110.26(10) .
O7 Cl2 O5 106.92(10) .
Cl1 O1 Cu1 114.20(9) .
Cl2 O5 Cu1 127.41(9) .
Cl2 O7 Cu2 133.50(11) 1_655
C17 N1 C13 119.14(18) .
C17 N1 Cu2 121.71(15) .
C13 N1 Cu2 119.13(14) .
C34 N2 C30 118.90(19) .
C34 N2 Cu2 121.24(15) .
C30 N2 Cu2 119.80(14) .
C6 C1 C2 119.1(2) .
C6 C1 P1 116.83(16) .
C2 C1 P1 124.03(17) .
C3 C2 C1 120.1(2) .
C3 C2 H2B 119.9 .
C1 C2 H2B 119.9 .
C4 C3 C2 120.0(2) .
C4 C3 H3B 120.0 .
C2 C3 H3B 120.0 .
C3 C4 C5 120.2(2) .
C3 C4 H4B 119.9 .
C5 C4 H4B 119.9 .
C4 C5 C6 120.2(2) .
C4 C5 H5A 119.9 .
C6 C5 H5A 119.9 .
C5 C6 C1 120.3(2) .
C5 C6 H6B 119.8 .
C1 C6 H6B 119.8 .
C12 C7 C8 119.64(19) .
C12 C7 P1 121.53(16) .
C8 C7 P1 118.76(15) .
C9 C8 C7 119.8(2) .
C9 C8 H8B 120.1 .
C7 C8 H8B 120.1 .
C10 C9 C8 120.4(2) .
C10 C9 H9A 119.8 .
C8 C9 H9A 119.8 .
C9 C10 C11 120.0(2) .
C9 C10 H10A 120.0 .
C11 C10 H10A 120.0 .
C10 C11 C12 120.1(2) .
C10 C11 H11A 120.0 .
C12 C11 H11A 120.0 .
C11 C12 C7 120.1(2) .
C11 C12 H12A 119.9 .
C7 C12 H12A 119.9 .
N1 C13 C14 121.31(19) .
N1 C13 P1 114.33(15) .
C14 C13 P1 124.32(16) .
C13 C14 C15 119.2(2) .
C13 C14 H14A 120.4 .
C15 C14 H14A 120.4 .
C16 C15 C14 118.9(2) .
C16 C15 H15A 120.5 .
C14 C15 H15A 120.5 .
C15 C16 C17 119.3(2) .
C15 C16 H16A 120.4 .
C17 C16 H16A 120.4 .
N1 C17 C16 122.1(2) .
N1 C17 H17A 118.9 .
C16 C17 H17A 118.9 .
C23 C18 C19 118.4(2) .
C23 C18 P2 124.65(17) .
C19 C18 P2 116.91(16) .
C20 C19 C18 121.0(2) .
C20 C19 H19A 119.5 .
C18 C19 H19A 119.5 .
C21 C20 C19 119.7(2) .
C21 C20 H20A 120.1 .
C19 C20 H20A 120.1 .
C22 C21 C20 120.0(2) .
C22 C21 H21A 120.0 .
C20 C21 H21A 120.0 .
C21 C22 C23 120.8(2) .
C21 C22 H22A 119.6 .
C23 C22 H22A 119.6 .
C22 C23 C18 120.0(2) .
C22 C23 H23A 120.0 .
C18 C23 H23A 120.0 .
C25 C24 C29 119.3(2) .
C25 C24 P2 122.99(17) .
C29 C24 P2 117.73(17) .
C26 C25 C24 120.2(2) .
C26 C25 H25A 119.9 .
C24 C25 H25A 119.9 .
C27 C26 C25 120.1(2) .
C27 C26 H26A 119.9 .
C25 C26 H26A 119.9 .
C26 C27 C28 120.1(2) .
C26 C27 H27A 119.9 .
C28 C27 H27A 119.9 .
C27 C28 C29 120.2(2) .
C27 C28 H28A 119.9 .
C29 C28 H28A 119.9 .
C28 C29 C24 120.1(2) .
C28 C29 H29A 120.0 .
C24 C29 H29A 120.0 .
N2 C30 C31 121.7(2) .
N2 C30 P2 113.31(15) .
C31 C30 P2 124.73(17) .
C30 C31 C32 118.7(2) .
C30 C31 H31A 120.7 .
C32 C31 H31A 120.7 .
C33 C32 C31 119.9(2) .
C33 C32 H32A 120.1 .
C31 C32 H32A 120.1 .
C32 C33 C34 118.6(2) .
C32 C33 H33A 120.7 .
C34 C33 H33A 120.7 .
N2 C34 C33 122.3(2) .
N2 C34 H34A 118.9 .
C33 C34 H34A 118.9 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Cu1 O1 2.1742(15) .
Cu1 O5 2.1876(15) .
Cu1 P1 2.2435(6) .
Cu1 P2 2.2527(6) .
Cu2 N2 1.9103(18) .
Cu2 N1 1.9111(18) .
Cu2 O7 2.3172(16) 1_455
P1 C7 1.817(2) .
P1 C1 1.829(2) .
P1 C13 1.835(2) .
P2 C24 1.819(2) .
P2 C18 1.826(2) .
P2 C30 1.838(2) .
Cl1 O4 1.4286(18) .
Cl1 O3 1.4307(17) .
Cl1 O2 1.4418(17) .
Cl1 O1 1.4645(16) .
Cl2 O8 1.4283(18) .
Cl2 O6 1.4303(16) .
Cl2 O7 1.4570(17) .
Cl2 O5 1.4634(16) .
N1 C17 1.340(3) .
N1 C13 1.356(3) .
N2 C34 1.343(3) .
N2 C30 1.360(3) .
C1 C6 1.395(3) .
C1 C2 1.399(3) .
C2 C3 1.391(3) .
C2 H2B 0.9500 .
C3 C4 1.383(4) .
C3 H3B 0.9500 .
C4 C5 1.383(4) .
C4 H4B 0.9500 .
C5 C6 1.385(3) .
C5 H5A 0.9500 .
C6 H6B 0.9500 .
C7 C12 1.394(3) .
C7 C8 1.398(3) .
C8 C9 1.391(3) .
C8 H8B 0.9500 .
C9 C10 1.386(3) .
C9 H9A 0.9500 .
C10 C11 1.388(4) .
C10 H10A 0.9500 .
C11 C12 1.392(3) .
C11 H11A 0.9500 .
C12 H12A 0.9500 .
C13 C14 1.388(3) .
C14 C15 1.392(3) .
C14 H14A 0.9500 .
C15 C16 1.380(3) .
C15 H15A 0.9500 .
C16 C17 1.386(3) .
C16 H16A 0.9500 .
C17 H17A 0.9500 .
C18 C23 1.395(3) .
C18 C19 1.397(3) .
C19 C20 1.388(3) .
C19 H19A 0.9500 .
C20 C21 1.383(4) .
C20 H20A 0.9500 .
C21 C22 1.369(4) .
C21 H21A 0.9500 .
C22 C23 1.394(3) .
C22 H22A 0.9500 .
C23 H23A 0.9500 .
C24 C25 1.394(3) .
C24 C29 1.396(3) .
C25 C26 1.393(3) .
C25 H25A 0.9500 .
C26 C27 1.381(4) .
C26 H26A 0.9500 .
C27 C28 1.385(4) .
C27 H27A 0.9500 .
C28 C29 1.390(3) .
C28 H28A 0.9500 .
C29 H29A 0.9500 .
C30 C31 1.384(3) .
C31 C32 1.388(3) .
C31 H31A 0.9500 .
C32 C33 1.383(4) .
C32 H32A 0.9500 .
C33 C34 1.385(3) .
C33 H33A 0.9500 .
C34 H34A 0.9500 .
