#------------------------------------------------------------------------------
#$Date: 2024-07-05 18:18:10 +0300 (Fri, 05 Jul 2024) $
#$Revision: 292939 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/24/87/7248763.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7248763
loop_
_publ_author_name
'Shen, Meng'
'Zhang, Yulin'
'Cheng, Bingliang'
'Ma, Wenjuan'
'Huang, Xiaole'
'Zhang, Lei'
'Chai, Zhifang'
'Lin, Wenwen'
_publ_section_title
;
 Spontaneous phase transition from 3D perovskite to 1D non-perovskite in
 CsPbBr2.7I0.3
;
_journal_issue                   24
_journal_name_full               CrystEngComm
_journal_page_first              3162
_journal_page_last               3166
_journal_paper_doi               10.1039/D4CE00235K
_journal_volume                  26
_journal_year                    2024
_chemical_formula_moiety         '0.25(Br10.8 Cs4 I1.2 Pb4)'
_chemical_formula_sum            'Br2.7 Cs I0.3 Pb'
_chemical_formula_weight         593.93
_space_group_crystal_system      orthorhombic
_space_group_IT_number           62
_space_group_name_Hall           '-P 2ac 2n'
_space_group_name_H-M_alt        'P n m a'
_atom_sites_solution_primary     dual
_audit_creation_date             2024-05-07
_audit_creation_method
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_audit_update_record
;
2024-05-07 deposited with the CCDC.	2024-05-31 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   8.2876(17)
_cell_length_b                   11.814(3)
_cell_length_c                   8.2579(18)
_cell_measurement_reflns_used    1188
_cell_measurement_temperature    300(2)
_cell_measurement_theta_max      24.30
_cell_measurement_theta_min      3.45
_cell_volume                     808.5(3)
_computing_cell_refinement       'SAINT V8.40B (?, 2016)'
_computing_data_reduction        'SAINT V8.40B (?, 2016)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_diffrn_ambient_temperature      300
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.989
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0707
_diffrn_reflns_av_unetI/netI     0.0465
_diffrn_reflns_Laue_measured_fraction_full 0.995
_diffrn_reflns_Laue_measured_fraction_max 0.989
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       10
_diffrn_reflns_limit_l_min       -10
_diffrn_reflns_number            6178
_diffrn_reflns_point_group_measured_fraction_full 0.995
_diffrn_reflns_point_group_measured_fraction_max 0.989
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.578
_diffrn_reflns_theta_min         3.010
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    39.676
_exptl_absorpt_correction_T_max  0.7456
_exptl_absorpt_correction_T_min  0.5032
_exptl_absorpt_correction_type   none
_exptl_absorpt_process_details
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1331 before and 0.0758 after correction.
The Ratio of minimum to maximum transmission is 0.6749.
The λ/2 correction factor is Not present.
;
_exptl_crystal_colour            'clear orangish orange'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_modifier   orangish
_exptl_crystal_colour_primary    orange
_exptl_crystal_density_diffrn    4.879
_exptl_crystal_description       block
_exptl_crystal_F_000             990
_exptl_crystal_size_max          0.02
_exptl_crystal_size_mid          0.01
_exptl_crystal_size_min          0.01
_refine_diff_density_max         1.805
_refine_diff_density_min         -1.692
_refine_diff_density_rms         0.318
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.020
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     28
_refine_ls_number_reflns         971
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.020
_refine_ls_R_factor_all          0.0787
_refine_ls_R_factor_gt           0.0437
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0190P)²+28.7997P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0893
_refine_ls_wR_factor_ref         0.1069
_reflns_Friedel_coverage         0.000
_reflns_number_gt                563
_reflns_number_total             971
_reflns_threshold_expression     'I > 2σ(I)'
_iucr_refine_instructions_details
;
TITL 5_a.res in Pnma
    5.res
    created by SHELXL-2018/3 at 11:02:06 on 07-May-2024
REM Old TITL 5 in Pnma #62
REM SHELXT solution in Pnma: R1 0.189, Rweak 0.002, Alpha 0.032
REM <I/s> 0.672 for 127 systematic absences, Orientation as input
REM Formula found by SHELXT: Br4 Pb
CELL 0.71073 8.2876 11.8141 8.2579 90 90 90
ZERR 4 0.0017 0.0029 0.0018 0 0 0
LATT 1
SYMM 0.5-X,-Y,0.5+Z
SYMM -X,0.5+Y,-Z
SYMM 0.5+X,0.5-Y,0.5-Z
SFAC Br Cs I Pb
UNIT 10.8 4 1.2 4
EADP I1 Br1
EADP Br2 I2
EXYZ I1 Br1
EXYZ Br2 I2

L.S. 20
PLAN  5
SIZE 0.01 0.01 0.02
TEMP 26.85
list 4
fmap 2 53
acta
OMIT 4 1 1
OMIT 4 14 0
OMIT 2 14 0
OMIT 6 1 1
OMIT 2 3 4
REM <olex2.extras>
REM <HklSrc "%.\\5.hkl">
REM </olex2.extras>

WGHT    0.019000   28.799702
FVAR       0.14682
PB1   4    1.000000    0.500000    0.500000    10.50000    0.03023    0.02784 =
         0.03141   -0.00076   -0.00026    0.00112
CS1   2    0.970879    0.750000    0.992636    10.50000    0.09842    0.07835 =
         0.10216    0.00000    0.02985    0.00000
PART 5
BR2   1    0.708768    0.524506    0.707849    10.90000    0.06304    0.10074 =
         0.06451    0.00529    0.03370    0.00902
PART 0
PART 3
I1    3    1.003658    0.750000    0.453253    10.05000    0.13907    0.02646 =
         0.10718    0.00000   -0.01360    0.00000
PART 0
PART 6
I2    3    0.708768    0.524506    0.707849    10.10000    0.06304    0.10074 =
         0.06451    0.00529    0.03370    0.00902
PART 0
PART 4
BR1   1    1.003658    0.750000    0.453253    10.45000    0.13907    0.02646 =
         0.10718    0.00000   -0.01360    0.00000
HKLF 4

#
# h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared), status flag
#
data_5_CCDC1
_shelx_title ' 5_a.res in Pnma'
_shelx_refln_list_code          4
_shelx_F_calc_maximum      686.17
_exptl_crystal_F_000       989.60
_reflns_d_resolution_high  0.7676

loop_
 _space_group_symop_operation_xyz
 'x, y, z'
 '-x+1/2, -y, z+1/2'
 '-x, y+1/2, -z'
 'x+1/2, -y+1/2, -z+1/2'
 '-x, -y, -z'
 'x-1/2, y, -z-1/2'
 'x, -y-1/2, z'
 '-x-1/2, y-1/2, z-1/2'

_cell_length_a     8.2876
_cell_length_b    11.8141
_cell_length_c     8.2579
_cell_angle_alpha  90.000
_cell_angle_beta   90.000
_cell_angle_gamma  90.000

_shelx_F_squared_multiplier     1.000

loop_
 _refln_index_h
 _refln_index_k
 _refln_index_l
 _refln_F_squared_calc
 _refln_F_squared_meas
 _refln_F_squared_sigma
 _refln_observed_status
   2   0   0     119409.16     119611.09      3010.25 o
   4   0   0     192190.95     191879.31      4983.61 o
   6   0   0      41278.39      39447.58      1994.86 o
   2   1   0       1543.93       1353.12       101.75 o
   4   1   0       6838.98       5344.82       222.88 o
   6   1   0        681.97        501.73       106.23 o
   8   1   0        612.97        282.99       204.12 o
  10   1   0          8.10        120.62       171.65 o
   0   2   0      47095.95      48235.25      1664.48 o
   2   2   0      29219.99      30504.08       769.17 o
   4   2   0      25282.60      26225.55       636.86 o
   6   2   0      12966.22      11207.38       765.47 o
   8   2   0       5948.22       6911.94       603.10 o
  10   2   0       7328.61       7259.42       640.21 o
   2   3   0       7874.72       6725.87       404.36 o
   4   3   0         48.56        -42.67        59.01 o
   6   3   0       5471.64       5222.52       479.02 o
   8   3   0          1.57        -23.20       190.21 o
   0   4   0     470831.09     434428.31     11604.95 o
   2   4   0     110909.12     115165.10      3991.89 o
   4   4   0     122919.21     118865.19      4013.23 o
   6   4   0      33881.65      32393.25       819.64 o
   8   4   0       7961.80       8372.83       723.72 o
  10   4   0       5859.91       4940.28       705.16 o
   2   5   0        120.12        140.43       101.94 o
   4   5   0       9890.28       8669.88       438.23 o
   6   5   0        272.22        297.45       113.12 o
   8   5   0       1080.01       1322.17       398.97 o
  10   5   0         19.11        134.54       218.04 o
   0   6   0       9017.88       8738.01      1159.80 o
   2   6   0        656.37       1018.57       211.60 o
   4   6   0      10451.49      10802.33      1131.29 o
   6   6   0      10186.35       9860.38       488.75 o
   8   6   0       5057.57       4994.70       583.93 o
   2   7   0       3908.25       4297.67       318.49 o
   4   7   0        306.53        329.66       173.80 o
   6   7   0       3537.84       3903.22       385.03 o
   8   7   0         47.29        129.59       236.60 o
   0   8   0     119153.95     115595.15      4213.36 o
   2   8   0      70540.00      67548.54      1646.10 o
   4   8   0      43358.14      40803.81      1229.39 o
   6   8   0      18313.81      17571.50      1483.60 o
   8   8   0       5532.56       4994.62       484.80 o
   2   9   0        122.11        120.63       111.04 o
   4   9   0       2387.96       3019.89       320.30 o
   6   9   0        188.34         79.45       206.40 o
   8   9   0        245.30        402.15       218.30 o
   0  10   0       1625.36       1591.30       667.81 o
   2  10   0       2390.52       2477.79       268.88 o
   4  10   0       3849.21       3965.05       331.39 o
   6  10   0       5358.30       5939.09       564.56 o
   8  10   0       3105.94       3262.60       405.84 o
   2  11   0        492.54        625.79       204.18 o
   4  11   0         26.17         13.01       103.79 o
   6  11   0        507.07        620.08       281.11 o
   0  12   0      27844.96      26628.79      2880.71 o
   2  12   0      25773.96      24939.62      1034.22 o
   4  12   0      12985.69      13659.69      1759.95 o
   6  12   0       6771.66       7278.00       776.90 o
   2  13   0          8.65         -8.67       102.12 o
   4  13   0        116.39         28.61        97.96 o
   0  14   0        903.98        547.45       318.64 o
   2  15   0         19.56         67.17       137.08 o
   1   0   1      44154.26      42977.37      1428.62 o
   2   0   1       9840.58       9616.59       392.00 o
   3   0   1      64753.58      62539.20      2099.13 o
   4   0   1      19978.17      20322.48      1122.69 o
   5   0   1      20453.20      20056.04       811.90 o
   6   0   1       7110.18       6359.88       528.87 o
   7   0   1      22094.57      19352.89      1159.80 o
   8   0   1       1931.99       2356.25       398.97 o
   9   0   1       7709.65       8544.48       681.96 o
  10   0   1        134.42        139.18       194.85 o
   0   1   1        104.64         47.06        16.63 o
   1   1   1        748.48        768.31        64.71 o
   2   1   1       3125.36       3691.52       122.11 o
   3   1   1       5997.05       4801.10       171.96 o
   5   1   1       3508.92       3810.49       231.22 o
   7   1   1        889.13        871.99       155.79 o
   8   1   1         36.69         90.40       123.49 o
   9   1   1        168.05         91.55       128.06 o
  10   1   1          0.69        171.65       194.85 o
   1   2   1     103580.38     108500.32      1567.28 o
   2   2   1      11364.05      10588.77       272.51 o
   3   2   1      96174.84     101359.38      2826.32 o
   4   2   1      10943.85      10181.65       326.05 o
   5   2   1      25489.62      28302.72       875.31 o
   6   2   1       7420.29       7077.03       280.99 o
   7   2   1      19474.63      20330.35       603.91 o
   8   2   1       1264.92       1869.86       206.26 o
   9   2   1       6357.80       6714.28       464.29 o
  10   2   1        106.80        114.83       139.16 o
   0   3   1      14831.66      12650.94       400.18 o
   1   3   1       2840.49       2744.86       122.56 o
   2   3   1       2593.18       2801.20       140.50 o
   3   3   1       2632.83       2586.81       155.63 o
   4   3   1       2490.34       2984.57       186.10 o
   5   3   1       2681.13       2671.69       160.27 o
   6   3   1          5.14        202.29        79.46 o
   7   3   1        942.46       1225.78       241.73 o
   8   3   1          2.65        109.00        97.80 o
   9   3   1         31.53        129.75       146.10 o
  10   3   1         47.38       -148.45       148.45 o
   1   4   1      39492.51      40201.55       761.89 o
   2   4   1       3203.16       3652.74       166.68 o
   3   4   1      48776.52      46195.68      1091.96 o
   4   4   1       8005.65       7357.19       265.07 o
   5   4   1      19798.85      19151.92       634.55 o
   6   4   1       2618.14       2820.98       182.90 o
   7   4   1      17078.20      17048.19       449.62 o
   8   4   1        728.74       1145.97       149.37 o
   9   4   1       6611.00       7047.06       385.56 o
  10   4   1         38.15        -18.07       103.69 o
   0   5   1       6518.37       6521.65       649.27 o
   1   5   1          1.53          1.21        45.04 o
   2   5   1      10559.06       9367.64       298.85 o
   3   5   1       4003.77       4241.19       191.92 o
   4   5   1        661.41        656.77        85.26 o
   5   5   1       1897.94       1982.59       171.09 o
   6   5   1        199.25        275.02        88.62 o
   7   5   1        375.94        237.95       131.05 o
   8   5   1        102.66        152.21       124.27 o
   9   5   1        200.43         39.88        96.56 o
  10   5   1         36.06         53.89       149.02 o
   1   6   1      48047.88      46838.51       926.40 o
   2   6   1       1671.94       2350.55       183.31 o
   3   6   1      42822.62      43667.22       811.59 o
   4   6   1       1311.38       1457.33       144.32 o
   5   6   1      17897.89      18985.93       731.99 o
   6   6   1       1132.98       1035.62       159.41 o
   7   6   1      11383.30      12102.16       915.67 o
   8   6   1        129.27         92.05        92.67 o
   9   6   1       4689.32       4246.14       458.45 o
   0   7   1      10344.69       9417.65       553.48 o
   1   7   1       1283.94       1561.60       166.14 o
   2   7   1       2480.92       2390.91       185.39 o
   3   7   1        530.71        843.22       107.08 o
   4   7   1       1845.64       2049.18       184.74 o
   5   7   1        807.43       1423.34       165.69 o
   6   7   1          1.69        189.89       129.63 o
   7   7   1        357.71        224.00       123.13 o
   8   7   1         17.98        120.25       119.69 o
   9   7   1          0.50        -91.41        91.41 o
   1   8   1      28590.34      27682.05       630.52 o
   2   8   1         78.14        -33.84        62.10 o
   3   8   1      25643.58      24792.04       567.17 o
   4   8   1        468.31        639.66       122.90 o
   5   8   1      14674.04      15342.81       543.33 o
   6   8   1         54.47         52.94        98.43 o
   7   8   1       8877.50       9215.08       643.82 o
   8   8   1         19.13         47.03       120.47 o
   9   8   1       4058.54       3885.71       528.43 o
   0   9   1       1287.43       1438.28       267.79 o
   1   9   1          3.69         34.26        69.79 o
   2   9   1       3149.88       3759.57       252.04 o
   3   9   1        964.43       1299.94       153.34 o
   4   9   1        106.59         36.11        81.69 o
   5   9   1        515.40        803.97       161.09 o
   6   9   1         46.51        122.97       136.06 o
   7   9   1        105.18       -129.09       198.20 o
   8   9   1         50.59         95.00       135.31 o
   1  10   1      14502.26      14062.59       430.68 o
   2  10   1         31.93        -21.10        69.87 o
   3  10   1      12410.60      12458.59       593.35 o
   4  10   1          0.75         36.58        72.34 o
   5  10   1       8258.16       7998.87       424.16 o
   6  10   1          6.72        -90.76        90.76 o
   7  10   1       4808.54       4084.36       557.04 o
   8  10   1          2.47       -113.75       113.75 o
   0  11   1       1528.75       1418.06       239.65 o
   1  11   1        156.48         81.26        86.07 o
   2  11   1        112.57        117.37        96.83 o
   3  11   1         79.23         90.30       106.74 o
   4  11   1        266.12        -53.84        71.94 o
   5  11   1         97.71         48.58       135.39 o
   6  11   1          8.87         21.74       140.27 o
   7  11   1         41.54        129.90       412.89 o
   1  12   1      14387.99      13518.22       575.71 o
   2  12   1          9.47        -59.13        81.48 o
   3  12   1      11038.35      10933.02       572.90 o
   4  12   1          0.13        -58.87        79.95 o
   5  12   1       7081.24       8392.10       689.24 o
   6  12   1         13.65       -126.29       126.29 o
   0  13   1          0.61        -40.24       122.05 o
   1  13   1          1.36        -72.86        85.48 o
   2  13   1        301.97        148.39        83.65 o
   3  13   1        111.45          2.64        93.23 o
   4  13   1          4.02         13.75        91.13 o
   5  13   1         84.63        -36.85       136.55 o
   1  14   1       3446.36       2536.93       396.47 o
   2  14   1          0.05          3.83        83.28 o
   3  14   1       3143.19       2232.76       561.00 o
   4  14   1         12.86        -84.08        84.08 o
   0  15   1        112.03        -28.54       120.96 o
   1  15   1          5.98        -59.58        87.82 o
   2  15   1         10.20          7.91       245.26 o
   0   0   2     116590.66     123980.12      3488.94 o
   1   0   2      11490.03      10735.14       216.07 o
   2   0   2     397564.31     404527.97      7467.53 o
   3   0   2       3872.74       3731.01       158.85 o
   4   0   2      57219.68      62007.68      2149.98 o
   5   0   2         93.39        226.19       120.84 o
   6   0   2      39591.05      40050.43      1511.88 o
   7   0   2        409.96        745.39       199.38 o
   8   0   2      15196.72      15841.48      1076.29 o
   9   0   2        321.07        231.96       250.52 o
  10   0   2       2791.60       2551.10       487.12 o
   1   1   2       6190.34       5510.82       111.80 o
   2   1   2       3509.99       3031.62       109.27 o
   3   1   2        929.03       1142.20        89.53 o
   4   1   2       1654.01       1552.52       123.34 o
   5   1   2        442.29        622.39       125.80 o
   6   1   2       2318.93       2571.78       232.89 o
   7   1   2         22.10        225.43       140.60 o
   8   1   2        101.45        128.91       114.79 o
   9   1   2          0.25         35.32       117.57 o
  10   1   2         55.37       -111.53       111.53 o
   0   2   2      27092.98      28114.66       642.48 o
   1   2   2      10628.03       9855.19       192.69 o
   2   2   2      36518.79      35940.48       651.24 o
   3   2   2       1260.82       1231.71        87.14 o
   4   2   2       1354.18       1620.15       123.61 o
   5   2   2         18.83        -34.96        60.71 o
   6   2   2      14848.84      15155.30       516.68 o
   7   2   2        539.67        761.82       285.31 o
   8   2   2      11431.70      11627.71       509.17 o
   9   2   2        252.28        312.10       348.02 o
  10   2   2       2837.53       2571.80       341.38 o
   1   3   2       2796.62       3021.92       133.66 o
   2   3   2        187.84        149.07        55.81 o
   3   3   2       4017.03       4357.07       193.72 o
   4   3   2       7608.41       6788.76       252.05 o
   5   3   2        128.49        104.98        79.07 o
   6   3   2         28.57        -25.08        65.64 o
   7   3   2        136.94         13.94       109.29 o
   8   3   2       1028.83       1242.41       385.78 o
   9   3   2         24.02       -124.61       124.61 o
  10   3   2          0.40        459.28       352.58 o
   0   4   2     107487.18     113875.70      3182.52 o
   1   4   2       3792.49       4362.73       170.64 o
   2   4   2     231172.22     226162.30      7513.08 o
   3   4   2       1431.33       1702.98       161.54 o
   4   4   2      51914.31      52169.23      1134.40 o
   5   4   2         70.38        112.33        78.40 o
   6   4   2      29186.07      28409.37       720.49 o
   7   4   2        188.87         33.77        90.41 o
   8   4   2      12131.47      12619.12       445.13 o
   9   4   2        135.85        133.01       131.95 o
  10   4   2       2669.06       1988.49       320.50 o
   1   5   2       4838.71       5962.49       324.87 o
   2   5   2       3996.73       4892.97       259.52 o
   3   5   2          7.70         30.90        54.19 o
   4   5   2         48.97        138.14        81.78 o
   5   5   2       1453.13       1773.76       239.25 o
   6   5   2       3535.83       3737.48       304.96 o
   7   5   2        168.88        156.01       107.06 o
   8   5   2         75.13         86.71       111.72 o
   9   5   2          7.69        -84.99        84.99 o
   0   6   2        519.47        847.00       150.34 o
   1   6   2       1317.01       1854.03       178.68 o
   2   6   2      11652.50      10543.81       364.32 o
   3   6   2         97.87         55.95        59.74 o
   4   6   2       4881.94       6015.36       289.96 o
   5   6   2          0.60        -34.34        91.80 o
   6   6   2       8939.45       9441.43       429.70 o
   7   6   2        119.23        158.45       100.36 o
   8   6   2       7440.31       8334.01       484.91 o
   9   6   2         43.33        -59.16       151.00 o
   1   7   2        986.61       1202.74       149.47 o
   2   7   2         18.79         37.60        76.06 o
   3   7   2       2713.45       3924.92       315.51 o
   4   7   2       4349.48       5632.68       405.95 o
   5   7   2        187.42        -59.17        95.68 o
   6   7   2         72.80         48.43        97.73 o
   7   7   2        156.55         25.90       115.07 o
   8   7   2        728.32        636.88       154.69 o
   9   7   2         15.26         42.35       136.50 o
   0   8   2      67481.96      68716.80      1878.78 o
   1   8   2        118.63        227.81        99.91 o
   2   8   2      69006.98      68288.57      1428.34 o
   3   8   2         53.60         62.10       105.90 o
   4   8   2      32137.98      30491.77       685.66 o
   5   8   2         20.45         64.78       117.01 o
   6   8   2      13769.36      14093.53       593.59 o
   7   8   2         16.68         47.75       149.79 o
   8   8   2       6437.29       5160.84       466.53 o
   1   9   2       1807.46       2507.26       245.42 o
   2   9   2        917.73       1316.65       221.91 o
   3   9   2         29.40        -74.20       101.14 o
   4   9   2         82.72         -9.70        81.32 o
   5   9   2        579.59        813.11       160.26 o
   6   9   2        878.84       1524.44       293.08 o
   7   9   2         34.03        -92.14       128.09 o
   8   9   2         48.82        -74.89        98.78 o
   0  10   2       2762.51       3074.33       363.16 o
   1  10   2          4.92        -67.45        67.45 o
   2  10   2       3404.75       3926.23       317.76 o
   3  10   2          2.27        -43.77       100.46 o
   4  10   2       5096.66       5241.18       318.46 o
   5  10   2          0.74        -91.74        91.74 o
   6  10   2       4314.06       4301.53       945.40 o
   7  10   2          3.63        -43.03       157.36 o
   1  11   2        428.51        505.54       179.38 o
   2  11   2          0.56        -72.88        72.88 o
   3  11   2        634.80       1035.79       203.12 o
   4  11   2        617.45       1258.62       212.81 o
   5  11   2          3.05       -104.19       104.19 o
   6  11   2          1.14        -35.23       109.18 o
   7  11   2         25.66        -70.27       163.37 o
   0  12   2      24382.73      23352.29       955.81 o
   1  12   2          2.91         18.72       132.63 o
   2  12   2      17868.39      17584.99       650.44 o
   3  12   2          2.16        119.83        76.89 o
   4  12   2      12083.05      12346.50       607.07 o
   5  12   2          0.75         36.23       122.89 o
   6  12   2       5222.84       6027.91       451.65 o
   1  13   2        448.98        363.87       163.81 o
   2  13   2         51.10        -39.73        67.87 o
   3  13   2         82.14          7.51        76.62 o
   4  13   2          5.03        -55.10        73.44 o
   5  13   2         89.25         29.00        99.59 o
   0  14   2       2000.82       1005.63       398.28 o
   1  14   2          3.52        -79.59        79.59 o
   2  14   2       1584.08       1539.84       443.89 o
   3  14   2          0.66         -3.13        93.04 o
   4  14   2       2279.44       1223.46       470.20 o
   1  15   2        143.98          8.17       107.43 o
   1   0   3      46974.91      46954.77      1044.82 o
   2   0   3       5027.08       4370.97       182.10 o
   3   0   3       5954.08       6040.34       226.42 o
   4   0   3       1900.12       2247.17       188.50 o
   5   0   3      50241.07      47552.57      1425.40 o
   6   0   3       4863.01       5877.36       450.00 o
   7   0   3       5950.64       6777.41       658.77 o
   8   0   3        865.71       1183.00       403.61 o
   9   0   3       7896.56       8284.68       751.55 o
  10   0   3        222.84        436.08       269.07 o
   0   1   3       5271.25       5022.88       150.48 o
   1   1   3       1719.62       2349.78        81.02 o
   2   1   3        705.84       1226.44        70.61 o
   3   1   3       1343.31       1489.52        94.63 o
   4   1   3       1894.50       2577.48       135.48 o
   5   1   3       1787.20       1955.70       149.97 o
   6   1   3        233.04        392.19        97.50 o
   7   1   3        692.70        385.12       139.97 o
   8   1   3         88.32        141.30       144.08 o
   9   1   3         37.70        -49.77       107.66 o
  10   1   3         16.39        231.79       218.04 o
   1   2   3     117828.88     117316.67      2491.25 o
   2   2   3        538.28        782.38        66.51 o
   3   2   3      28090.57      30227.86       547.19 o
   4   2   3       6643.95       6306.87       294.50 o
   5   2   3      60105.55      60949.77      1193.54 o
   6   2   3       1478.05       1830.37       176.50 o
   7   2   3       6932.48       7564.55       469.63 o
   8   2   3       1114.91       1592.71       371.43 o
   9   2   3       6870.47       7086.76       744.36 o
  10   2   3        156.97        -32.38       137.75 o
   0   3   3         59.43        -37.23        48.70 o
   1   3   3        816.67       1117.62        82.73 o
   2   3   3       7542.06       7073.09       191.48 o
   3   3   3       4334.76       4460.38       265.27 o
   4   3   3          8.84         92.81        56.15 o
   5   3   3       1058.38        873.40       135.55 o
   6   3   3        777.97        727.08       134.02 o
   7   3   3        132.65        196.93        99.96 o
   8   3   3         52.24        -28.05       133.88 o
   9   3   3        228.78        324.74       236.60 o
  10   3   3          0.20       -105.64       105.64 o
   1   4   3      36218.27      36676.98       731.95 o
   2   4   3       2221.28       2425.92       143.83 o
   3   4   3       9845.43       9761.78       251.29 o
   4   4   3        514.39        527.18        87.40 o
   5   4   3      33706.23      32231.47       874.80 o
   6   4   3       2146.00       2304.42       217.41 o
   7   4   3       6730.76       7676.76       322.61 o
   8   4   3        296.49        243.08       131.73 o
   9   4   3       6056.64       6258.88       693.34 o
   0   5   3      10932.92       9094.74       331.57 o
   1   5   3       4878.76       5113.02       197.20 o
   2   5   3        183.10         37.72        47.73 o
   3   5   3         14.51         11.87        55.60 o
   4   5   3       3485.23       3867.00       210.43 o
   5   5   3       1119.76       1316.87       191.57 o
   6   5   3         17.38          3.45       119.11 o
   7   5   3        788.89        712.19       165.12 o
   8   5   3         62.62        169.07       117.01 o
   9   5   3          3.65        322.01       152.47 o
   1   6   3      52954.95      52157.80      1072.32 o
   2   6   3          9.00        -49.16        49.16 o
   3   6   3      23101.63      22777.93       545.52 o
   4   6   3       1365.50       1493.16       171.14 o
   5   6   3      26680.84      26446.48       717.72 o
   6   6   3        114.45         91.29       102.33 o
   7   6   3       6990.05       7170.97       501.15 o
   8   6   3        173.01        374.25       143.77 o
   9   6   3       4196.53       3951.74       395.25 o
   0   7   3        200.01          2.51       103.61 o
   1   7   3       1251.17       1756.43       224.46 o
   2   7   3       5467.76       5614.37       276.28 o
   3   7   3       2114.62       2758.41       224.39 o
   4   7   3         14.26         20.34        73.83 o
   5   7   3        292.67        483.68       130.88 o
   6   7   3        457.10        414.99       153.32 o
   7   7   3          2.02       -108.71       108.71 o
   8   7   3         25.62        166.55       126.45 o
   9   7   3        138.78        131.24       133.24 o
   1   8   3      20006.37      21021.99       540.29 o
   2   8   3        236.59         87.55        81.51 o
   3   8   3      12741.90      12935.93       450.89 o
   4   8   3          6.69         40.83        87.12 o
   5   8   3      13333.70      13540.58       770.72 o
   6   8   3        172.07        144.89       201.91 o
   7   8   3       6038.53       6440.27       524.02 o
   8   8   3          1.39         94.51       134.21 o
   0   9   3       4052.93       3632.67       353.50 o
   1   9   3       1327.16       1843.06       185.93 o
   2   9   3          1.87         37.67        78.96 o
   3   9   3          0.45         94.56        89.04 o
   4   9   3       1250.95       1320.07       145.12 o
   5   9   3        264.33        330.99       139.24 o
   6   9   3         23.48        245.69       148.01 o
   7   9   3        271.00        468.06       206.94 o
   8   9   3         16.61        -70.71       177.37 o
   1  10   3      15510.45      15376.28       525.79 o
   2  10   3         27.80        117.88        91.05 o
   3  10   3      11519.29      10988.31       480.36 o
   4  10   3         65.02        -38.28       108.82 o
   5  10   3       8020.00       7783.13       722.08 o
   6  10   3         12.93       -149.39       149.99 o
   7  10   3       4352.46       2885.12       988.15 o
   0  11   3         66.32        -82.65       238.17 o
   1  11   3        147.29         65.98        98.37 o
   2  11   3       1176.59        995.56       192.00 o
   3  11   3        231.26         29.38       130.05 o
   4  11   3         29.75          6.27        61.29 o
   5  11   3         37.52        -88.92       104.77 o
   6  11   3         80.64        234.80       328.61 o
   1  12   3       9068.91       9182.84       441.70 o
   2  12   3         10.55        -65.15        65.15 o
   3  12   3       7628.67       7374.04       880.29 o
   4  12   3         36.23        -42.23        79.65 o
   5  12   3       4843.74       5781.27       583.69 o
   6  12   3          2.26        -74.23       269.07 o
   0  13   3        728.37        469.62       299.53 o
   1  13   3         81.42         22.96       101.93 o
   2  13   3        152.10        -38.99        79.65 o
   3  13   3          6.20          3.56        74.51 o
   4  13   3        211.05         48.47       114.22 o
   1  14   3       3906.32       3802.45       523.75 o
   2  14   3         10.23        -98.78        98.78 o
   3  14   3       3588.62       2626.45       586.45 o
   0   0   4     179513.84     182483.19      6021.85 o
   1   0   4      19124.82      17418.82       368.21 o
   2   0   4      55614.56      56031.50      1148.33 o
   3   0   4       3004.29       3429.50       349.54 o
   4   0   4      77209.98      78246.66      1954.89 o
   5   0   4        285.81        342.89        97.20 o
   6   0   4      14414.83      14630.38       615.69 o
   7   0   4        816.82       1511.27       621.65 o
   8   0   4      10019.34      11369.75       932.48 o
   9   0   4        544.92        291.66       248.20 o
   1   1   4       4671.41       4287.07       120.52 o
   2   1   4        759.94        921.34        67.46 o
   3   1   4       3043.48       3563.54       155.91 o
   4   1   4       1812.20       2357.49       135.12 o
   5   1   4          0.27         28.59        55.39 o
   6   1   4        464.88        696.65       105.79 o
   7   1   4         31.35        -47.25        82.83 o
   8   1   4        279.60        104.26       139.06 o
   9   1   4         26.80        -86.78       194.96 o
   0   2   4      26769.17      26525.02       555.35 o
   1   2   4      11720.62      10322.84       191.32 o
   2   2   4       1810.02       2142.86       111.76 o
   3   2   4       5856.70       6079.78       172.34 o
   4   2   4      24606.68      24862.91       612.79 o
   5   2   4         48.88        176.02        77.81 o
   6   2   4       6432.65       6665.78       262.53 o
   7   2   4        305.78        367.25       111.17 o
   8   2   4       7936.70       8080.10       413.32 o
   9   2   4        495.47        529.65       185.56 o
   1   3   4       6591.23       5611.18       148.98 o
   3   3   4         58.40          7.48        45.60 o
   4   3   4        524.73        826.40        94.60 o
   5   3   4       1666.50       2095.52       167.28 o
   6   3   4       1473.07       2112.67       232.98 o
   7   3   4        349.93        305.00       123.23 o
   8   3   4          5.72        -16.98       115.02 o
   9   3   4         11.96        -93.88        93.88 o
   0   4   4     114329.73     112319.63      2417.43 o
   1   4   4       7293.01       7525.47       203.91 o
   2   4   4      49204.60      49256.64       871.88 o
   3   4   4        939.16        847.99        94.81 o
   4   4   4      52119.98      50150.82       853.44 o
   5   4   4        105.40         -5.54        68.82 o
   6   4   4      13455.44      12654.92       468.50 o
   7   4   4        406.81        561.13       158.78 o
   8   4   4       7743.51       7884.48       476.69 o
   9   4   4        240.51        157.83       128.54 o
   1   5   4       1850.02       1907.90       129.31 o
   2   5   4        156.04        160.61        65.06 o
   3   5   4       5404.53       5787.71       214.54 o
   4   5   4       1639.83       2219.94       174.51 o
   5   5   4        563.43        629.65       110.18 o
   6   5   4          7.68        -58.54        93.68 o
   7   5   4        448.81        414.41       167.05 o
   8   5   4        425.48        500.76       190.32 o
   9   5   4         76.18         75.34       124.17 o
   0   6   4      12621.02      11760.51       427.20 o
   1   6   4       1426.62       1590.60       117.87 o
   2   6   4       5592.13       6292.66       241.16 o
   3   6   4        900.36       1201.75       115.32 o
   4   6   4      12442.01      12085.67       307.65 o
   5   6   4         61.66        160.64        92.91 o
   6   6   4       6563.80       7649.82       343.85 o
   7   6   4         59.28        -27.47        96.13 o
   8   6   4       4987.92       5329.29       333.66 o
   9   6   4         93.92         45.51       139.18 o
   1   7   4       3664.05       4411.61       214.22 o
   2   7   4        551.00       1078.60       116.59 o
   3   7   4         12.34        -47.23        67.35 o
   4   7   4         89.36        154.28        76.31 o
   5   7   4       1564.62       2521.88       201.43 o
   6   7   4        885.67       1141.22       269.07 o
   7   7   4        315.56        282.55       144.34 o
   8   7   4          3.68        250.71       154.88 o
   0   8   4      39214.28      38495.97      1048.60 o
   1   8   4        307.44        612.23       106.24 o
   2   8   4      29245.43      29428.08       719.03 o
   3   8   4          2.69        -65.13        65.13 o
   4   8   4      20013.22      19530.47       486.42 o
   5   8   4          2.77         20.53        88.86 o
   6   8   4       9063.13       9281.88       427.55 o
   7   8   4         44.79        -32.36       137.33 o
   8   8   4       4062.89       4032.51       357.86 o
   1   9   4        869.42       1430.58       180.57 o
   2   9   4         23.75        188.36       105.73 o
   3   9   4       2140.82       2891.86       237.85 o
   4   9   4        388.84        138.48       126.91 o
   5   9   4        107.55         58.08       109.98 o
   6   9   4          1.80        -69.03       107.68 o
   7   9   4        182.48        160.39       380.94 o
   0  10   4       5287.08       5498.20       599.89 o
   1  10   4          0.06        -25.82        90.63 o
   2  10   4       5789.75       6463.02       337.65 o
   3  10   4          6.46        116.46       111.60 o
   4  10   4       5120.67       5669.43       331.75 o
   5  10   4         19.72        -33.22        68.02 o
   6  10   4       4248.29       5158.37       499.47 o
   7  10   4          0.94        119.41       183.39 o
   1  11   4       1025.78       1267.90       164.86 o
   2  11   4         91.82        247.59       118.04 o
   3  11   4         33.49        -53.26        61.75 o
   4  11   4         30.88        -48.60        75.54 o
   5  11   4        299.41        205.29       193.34 o
   6  11   4        160.47       -130.43       237.04 o
   0  12   4      11105.78      12980.51       813.62 o
   1  12   4          4.17        -36.03        94.33 o
   2  12   4      10678.20      10394.90       688.05 o
   3  12   4          9.76        -14.81        85.53 o
   4  12   4       6383.56       7501.52      1016.40 o
   5  12   4          0.48          1.49       111.85 o
   1  13   4        384.50        316.74       120.86 o
   2  13   4          3.28        -70.04       112.03 o
   3  13   4        396.17        302.22       128.75 o
   4  13   4         25.32         51.98       110.68 o
   0  14   4       2346.23       3274.81      1039.18 o
   1  14   4          6.37         -6.59        98.41 o
   2  14   4       2667.59       2449.03       876.81 o
   1   0   5       8299.98       8889.98       258.95 o
   2   0   5        477.61        368.04        74.09 o
   3   0   5      38495.62      38463.05      1136.62 o
   4   0   5        491.05        509.24       172.01 o
   5   0   5       1528.63       1430.06       175.78 o
   6   0   5          7.20         50.07        90.71 o
   7   0   5      17565.56      15824.52       713.91 o
   8   0   5        517.46       1035.90       244.17 o
   9   0   5       2404.76       2282.49       514.95 o
   0   1   5        552.55        623.46        91.62 o
   1   1   5         58.90        203.97        46.71 o
   2   1   5       1174.51       1330.57        81.69 o
   3   1   5        996.03       1370.93       111.86 o
   4   1   5        299.15        332.68        81.80 o
   5   1   5        328.80        292.20        76.55 o
   6   1   5        439.76        652.13       106.97 o
   7   1   5        131.53        163.31        99.05 o
   8   1   5         31.92        -20.35       124.14 o
   9   1   5         77.87        -59.42       145.73 o
   1   2   5      43315.46      42343.09       622.51 o
   2   2   5        130.15         73.36        39.60 o
   3   2   5      70955.70      67239.97      1157.63 o
   4   2   5        251.14        237.04        77.91 o
   5   2   5       6595.68       7269.56       332.18 o
   6   2   5        529.64        556.62       150.42 o
   7   2   5      18636.25      17753.41       795.84 o
   8   2   5        191.90         51.87        96.13 o
   9   2   5       2505.86       2348.09       288.42 o
   0   3   5       1752.75       1856.56       198.79 o
   1   3   5       2538.23       2960.96       150.03 o
   2   3   5        111.37        143.89        57.28 o
   3   3   5         70.84         72.34        57.11 o
   4   3   5       1384.59       1510.41       121.77 o
   5   3   5        582.20        457.76       108.86 o
   6   3   5          2.99         24.72        84.32 o
   7   3   5        246.59        196.09       119.33 o
   8   3   5        195.03        256.74       120.48 o
   9   3   5          7.28        -19.90       137.53 o
   1   4   5       9237.72       9812.00       229.15 o
   2   4   5        300.17        301.83        69.22 o
   3   4   5      25822.10      25385.34       529.90 o
   4   4   5        294.05        231.98        75.31 o
   5   4   5       3202.05       3608.39       258.48 o
   6   4   5          0.46        -96.06        96.06 o
   7   4   5      11845.97      11941.51       624.72 o
   8   4   5        238.51        -13.89       111.30 o
   9   4   5       2529.62       2318.28       309.46 o
   0   5   5        125.57        243.94       108.16 o
   1   5   5       1908.98       2035.87       200.20 o
   2   5   5       1913.60       2161.13       136.95 o
   3   5   5       2153.63       2555.34       164.86 o
   4   5   5          4.17        172.19        72.62 o
   5   5   5         65.43        172.76        78.63 o
   6   5   5        801.37        759.69       145.22 o
   7   5   5         19.68        102.69       113.71 o
   8   5   5          1.34          5.95       107.26 o
   1   6   5      28265.45      26952.35       597.52 o
   2   6   5         62.37         92.66        60.64 o
   3   6   5      32376.59      30452.56       610.79 o
   4   6   5        137.30        120.39        92.57 o
   5   6   5       8358.15       8940.81       316.61 o
   6   6   5        137.65        129.27       107.99 o
   7   6   5       8951.62       8874.76       604.92 o
   8   6   5         22.57       -130.63       142.87 o
   0   7   5       1288.39        722.48       153.45 o
   1   7   5       2133.82       2618.59       172.55 o
   2   7   5         39.04        234.10        82.01 o
   3   7   5        289.93        262.82       107.53 o
   4   7   5        963.08       1091.29       160.05 o
   5   7   5        217.50         94.90        85.88 o
   6   7   5          9.69         -7.29        79.78 o
   7   7   5        119.37         82.02       123.85 o
   8   7   5        121.88        219.89       138.09 o
   1   8   5       8434.66      10031.59       324.51 o
   2   8   5         81.30         61.12        91.10 o
   3   8   5      10329.29      11425.12       341.04 o
   4   8   5         73.09         67.35        83.01 o
   5   8   5       5100.74       5776.99       355.19 o
   6   8   5         13.90          2.69       117.04 o
   7   8   5       4704.50       4774.78       597.90 o
   0   9   5        214.21        178.27       123.64 o
   1   9   5        610.19        581.12       140.84 o
   2   9   5        855.88        723.00       130.52 o
   3   9   5        585.25        803.58       171.25 o
   4   9   5         24.90        -18.75        56.49 o
   5   9   5         20.25         28.78        95.72 o
   6   9   5        287.75         67.95        83.33 o
   7   9   5          2.86        -57.90       148.07 o
   1  10   5      12141.82      12827.83       491.12 o
   2  10   5         15.89         71.49       100.89 o
   3  10   5       9894.35       9718.43       444.88 o
   4  10   5         35.97          4.83        64.41 o
   5  10   5       5802.41       6343.27       486.88 o
   6  10   5         11.25         58.54        92.41 o
   0  11   5        390.61         70.45       160.33 o
   1  11   5        240.30        450.98       149.30 o
   2  11   5         96.31         35.46       108.09 o
   3  11   5         43.14        -65.68        65.68 o
   4  11   5        207.67         22.66       123.62 o
   5  11   5         11.88       -114.37       114.37 o
   1  12   5       4684.84       4644.97       352.25 o
   2  12   5         11.27        -66.40        74.96 o
   3  12   5       3886.03       4164.29       408.88 o
   4  12   5         10.76         21.59        80.99 o
   0  13   5        198.65         -7.96       132.26 o
   1  13   5         27.25        -34.66        94.15 o
   2  13   5        223.67        237.15       129.55 o
   0   0   6      39834.20      38936.80      1078.06 o
   1   0   6       6817.64       6637.72       263.50 o
   2   0   6      36695.95      37909.15       799.46 o
   3   0   6       4938.19       5350.00       400.93 o
   4   0   6      14682.35      14112.38       556.22 o
   5   0   6         45.07        197.66       237.95 o
   6   0   6      18497.58      17604.59      1386.89 o
   7   0   6         24.22        -96.88        96.88 o
   8   0   6       2581.89       1904.30       593.59 o
   1   1   6       1849.71       1951.12       101.90 o
   2   1   6        151.66        256.32        60.62 o
   3   1   6        216.17        196.25        67.38 o
   4   1   6        461.44        429.11        95.27 o
   5   1   6        193.15        168.17       108.84 o
   6   1   6        212.44        200.61       108.65 o
   7   1   6         69.73        -17.74        93.82 o
   8   1   6         40.68        -20.39       107.18 o
   0   2   6      14072.53      12684.20       353.43 o
   1   2   6       7247.83       7346.13       200.39 o
   2   2   6      14459.03      14797.43       277.66 o
   3   2   6       1417.30       1402.62       112.36 o
   4   2   6       6483.17       6424.40       331.89 o
   5   2   6        653.59        733.99       145.55 o
   6   2   6      12852.44      12128.56       488.19 o
   7   2   6        186.66        283.25       117.18 o
   8   2   6       2270.73       2119.50       280.98 o
   1   3   6        750.12        702.48        75.62 o
   2   3   6        377.59        437.53        75.49 o
   3   3   6       1670.06       1915.86       129.14 o
   4   3   6        165.61        393.39       104.20 o
   5   3   6        301.34        349.23       124.93 o
   6   3   6        224.00        343.65       128.06 o
   7   3   6        170.15         49.97       108.69 o
   8   3   6        130.60       -136.60       136.60 o
   0   4   6      31037.96      31489.67       788.68 o
   1   4   6       2497.70       2802.21       156.61 o
   2   4   6      27083.81      26421.46       499.25 o
   3   4   6       2054.41       2972.83       191.54 o
   4   4   6      13227.75      13156.00       399.63 o
   5   4   6          1.82        -60.73        86.33 o
   6   4   6      13072.71      13821.61       467.05 o
   7   4   6         12.77        -85.47        97.61 o
   8   4   6       2743.85       2397.20       319.63 o
   1   5   6       1878.98       2114.42       141.46 o
   2   5   6         11.08        262.63        78.02 o
   3   5   6         21.06         31.20        82.38 o
   4   5   6        410.55        814.79       147.88 o
   5   5   6       1037.85       1531.12       164.84 o
   6   5   6         88.86         63.62       120.09 o
   7   5   6        371.11        668.18       204.74 o
   8   5   6          0.54        110.30       174.99 o
   0   6   6      11074.97      11361.42       437.94 o
   1   6   6       1071.72       1511.30       169.39 o
   2   6   6       9775.25       9823.69       287.70 o
   3   6   6         89.50        -60.78        71.76 o
   4   6   6       6544.61       7072.66       323.03 o
   5   6   6        119.06        127.86        96.12 o
   6   6   6       7003.61       7530.87       375.37 o
   7   6   6         67.85        -69.20       124.47 o
   1   7   6        261.97        194.72        83.39 o
   2   7   6        225.10        285.26        96.46 o
   3   7   6       1270.56       1339.15       151.60 o
   4   7   6         38.99        143.20       102.46 o
   5   7   6        356.29        187.18        89.73 o
   6   7   6        108.03         43.84        87.07 o
   7   7   6        211.56         66.83       153.65 o
   0   8   6      15216.33      17549.35       626.50 o
   1   8   6         54.18        -38.19        75.00 o
   2   8   6      12457.96      12540.94       384.17 o
   3   8   6        116.68        176.58        94.64 o
   4   8   6       8448.04       8015.32       385.31 o
   5   8   6         15.73        110.36        99.51 o
   6   8   6       5594.27       5748.09       420.91 o
   1   9   6        784.70        802.09       133.07 o
   2   9   6          0.55        -12.33        76.34 o
   3   9   6          0.06        -60.06        60.06 o
   4   9   6        107.10       -102.02       142.81 o
   5   9   6        425.68        167.91       137.23 o
   6   9   6         15.83         74.57       122.44 o
   0  10   6       6198.52       7032.45       553.02 o
   1  10   6          4.07        -71.48        86.06 o
   2  10   6       5195.54       6072.87       430.55 o
   3  10   6         15.26         60.49       121.91 o
   4  10   6       4330.11       3970.18       443.44 o
   5  10   6          3.33        -23.90        83.06 o
   1  11   6        119.09        146.38       125.33 o
   2  11   6         45.90         -0.68        91.49 o
   3  11   6        262.48        112.66        89.83 o
   4  11   6         14.68         45.47       109.58 o
   0  12   6       5241.13       4904.49       574.24 o
   1  12   6          9.62        -82.67        82.67 o
   2  12   6       4426.54       4659.45       470.16 o
   3  12   6          0.07        173.03       216.83 o
   1   0   7      11513.44      12063.09       388.53 o
   2   0   7        201.41        131.15        80.92 o
   3   0   7       2987.27       2967.73       217.46 o
   4   0   7       1342.22       2103.76       298.51 o
   5   0   7      14766.84      14444.86      1487.68 o
   6   0   7         22.41         30.06       120.86 o
   7   0   7       1121.05        882.01       355.24 o
   8   0   7          0.30        203.57       216.21 o
   0   1   7         27.36        -68.65        68.65 o
   1   1   7        159.55        248.40        65.51 o
   2   1   7         74.30         56.90        54.74 o
   3   1   7          0.24         16.49        63.54 o
   4   1   7        133.28        115.31        90.52 o
   5   1   7        138.53        -54.33       159.49 o
   6   1   7         18.05        -72.80        72.80 o
   7   1   7         36.47         13.29       119.09 o
   8   1   7         65.47        118.84       131.72 o
   1   2   7      29507.96      28616.20       470.47 o
   2   2   7        817.99        968.76        87.85 o
   3   2   7      11236.83      11525.04       331.16 o
   4   2   7        198.55        204.10        89.29 o
   5   2   7      20124.25      18001.32      1068.94 o
   6   2   7        251.80         95.66       104.04 o
   7   2   7       2004.52       1602.76       235.12 o
   8   2   7         21.16        -91.58        91.58 o
   0   3   7        125.54         73.42        80.22 o
   1   3   7        498.22        527.33        80.91 o
   2   3   7         32.77        -28.83        60.52 o
   3   3   7        575.91        454.59        96.69 o
   4   3   7          4.69        -79.12        79.12 o
   5   3   7          3.99        -69.26        69.26 o
   6   3   7        264.87        252.20       145.45 o
   7   3   7         30.27        283.45       203.09 o
   1   4   7       9198.30      10041.82       262.19 o
   2   4   7         64.06         29.85        65.07 o
   3   4   7       3754.56       3853.53       248.45 o
   4   4   7        655.05        915.05       148.01 o
   5   4   7      10072.48      10096.21       570.06 o
   6   4   7          2.97        -91.94       122.56 o
   7   4   7       1624.76       1114.95       249.74 o
   0   5   7          4.14         41.82        94.69 o
   1   5   7        994.10       1121.67       118.47 o
   2   5   7        111.83         50.68        72.84 o
   3   5   7        255.50         42.29        75.08 o
   4   5   7        239.50        401.96       109.48 o
   5   5   7        280.51        141.42        99.78 o
   6   5   7         20.75        -49.75       105.01 o
   7   5   7         22.39       -102.01       102.01 o
   1   6   7      17189.42      16792.32       398.37 o
   2   6   7        190.21        248.23        87.56 o
   3   6   7       9669.27       9996.41       348.13 o
   4   6   7         13.65        -64.53        64.53 o
   5   6   7       9939.63       9634.99       471.08 o
   6   6   7         56.19        141.50       130.82 o
   7   6   7       2546.47       1728.94       388.83 o
   0   7   7        134.51         61.74       124.91 o
   1   7   7        569.78        519.84       141.38 o
   2   7   7         13.97         51.90        83.11 o
   3   7   7        429.06        543.35       117.22 o
   4   7   7          0.11         48.36        66.47 o
   5   7   7         31.12        -73.46        73.46 o
   6   7   7        194.13        374.43       226.26 o
   1   8   7       5218.10       5649.77       275.83 o
   2   8   7          0.04        -84.00        84.00 o
   3   8   7       3924.33       4833.38       490.54 o
   4   8   7         76.26         89.17        74.23 o
   5   8   7       4110.96       4069.24       326.48 o
   0   9   7         14.56        -88.03        88.03 o
   1   9   7        299.26        311.45       121.98 o
   2   9   7         91.73         17.00        82.62 o
   3   9   7         82.52         89.41       103.02 o
   4   9   7        106.66        -71.16        71.16 o
   5   9   7         80.83        -22.35        77.16 o
   1  10   7       6976.44       7356.16       444.75 o
   2  10   7          9.75        -21.72        75.03 o
   3  10   7       5398.93       5132.27       621.31 o
   4  10   7          2.52         38.38       101.66 o
   0  11   7         51.57         65.26       153.91 o
   1  11   7         72.30         20.78        90.78 o
   2  11   7          7.97         -6.20        91.35 o
   0   0   8       8209.36       9668.50       621.41 o
   1   0   8       1853.04       2384.08       235.69 o
   2   0   8      15325.06      16436.01       523.07 o
   3   0   8        641.54        431.87       134.48 o
   4   0   8       9690.31       9423.89       721.19 o
   5   0   8        671.70        687.64       253.93 o
   6   0   8       2771.19       1871.00       415.62 o
   7   0   8          5.71         63.66       197.69 o
   1   1   8        148.78         96.35        69.70 o
   2   1   8         61.79         73.68        66.32 o
   3   1   8        100.94        141.04        81.06 o
   4   1   8         10.65        108.93        91.08 o
   5   1   8         10.23         33.04       119.18 o
   6   1   8         71.28         41.00       139.57 o
   7   1   8          3.01        -99.28        99.28 o
   0   2   8       5346.40       5533.35       300.82 o
   1   2   8        991.59       1308.09       158.65 o
   2   2   8      10834.72      11251.55       336.88 o
   3   2   8       1358.87       1658.52       173.48 o
   4   2   8       7033.01       6771.76       376.83 o
   5   2   8        113.84        -25.01       113.40 o
   6   2   8       2187.32       1506.21       536.05 o
   7   2   8         64.27        211.21       151.74 o
   1   3   8        196.92        292.15        78.64 o
   2   3   8          7.87         39.87        67.82 o
   3   3   8          2.58        185.83       103.67 o
   4   3   8        277.69        184.86       114.87 o
   5   3   8        101.59        -73.66       110.72 o
   6   3   8          0.07         59.81       148.61 o
   0   4   8       7470.61       8105.46       517.51 o
   1   4   8        725.36        846.61       117.53 o
   2   4   8      11653.10      11425.04       339.60 o
   3   4   8        195.68         59.62        95.67 o
   4   4   8       7600.89       6828.75       578.40 o
   5   4   8        289.64        397.42       172.48 o
   6   4   8       2805.50       2426.48       303.18 o
   1   5   8         69.71         28.42        72.58 o
   2   5   8        159.28         65.23        84.30 o
   3   5   8        245.08        252.89       114.50 o
   4   5   8         49.20        172.81        85.70 o
   5   5   8        109.42        135.35       131.45 o
   6   5   8        129.65         85.55       130.86 o
   0   6   8       5152.92       4911.67       368.59 o
   1   6   8         94.86        -71.84        71.84 o
   2   6   8       7060.83       7756.01       375.39 o
   3   6   8        238.90         90.13       149.48 o
   4   6   8       4806.45       5549.97       379.13 o
   5   6   8          1.80        -95.01        95.01 o
   1   7   8         97.50         27.99       109.49 o
   2   7   8         21.93        -56.42        86.11 o
   3   7   8         16.04        -19.51        71.99 o
   4   7   8        231.38        121.08        82.35 o
   5   7   8        104.11         -3.78        85.94 o
   0   8   8       5016.03       5042.81       440.00 o
   1   8   8         26.22        -75.93        85.33 o
   2   8   8       5642.09       4807.06       361.87 o
   3   8   8          0.11        -67.73        67.73 o
   4   8   8       3990.79       3895.55       365.48 o
   1   9   8         38.63        -66.44       105.16 o
   2   9   8         49.71         19.30        92.98 o
   3   9   8        104.52          3.95        96.65 o
   0  10   8       3442.90       3008.87       451.19 o
   1  10   8          2.81        -35.57       104.17 o
   1   0   9       4703.86       4689.85       381.07 o
   2   0   9        428.31        401.36       137.89 o
   3   0   9       5249.36       5501.99       723.18 o
   4   0   9        355.35        219.27       245.94 o
   5   0   9       1904.48       1123.61       370.56 o
   0   1   9          4.36        -73.20        87.81 o
   1   1   9          8.75         32.76        66.44 o
   2   1   9          4.29         34.51        68.93 o
   3   1   9         32.16         69.20        88.54 o
   4   1   9          3.72        -38.74       118.46 o
   5   1   9          0.07       -122.95       130.05 o
   1   2   9       8806.03       8045.76       435.90 o
   2   2   9        161.47        111.12        76.19 o
   3   2   9       8246.96       7361.67       350.40 o
   4   2   9        593.39        988.33       287.65 o
   5   2   9       3125.12       2398.61       320.41 o
   0   3   9         90.91        127.66       103.01 o
   1   3   9         98.84        173.18        85.38 o
   2   3   9         22.67        -28.10        68.43 o
   3   3   9         54.72        116.87       121.47 o
   4   3   9          1.15        -34.37       108.27 o
   5   3   9         81.14         21.13       140.77 o
   1   4   9       4128.35       4370.50       224.78 o
   2   4   9        194.59          8.05        85.47 o
   3   4   9       4200.94       4454.94       292.64 o
   4   4   9        130.82        303.30       150.02 o
   5   4   9       1977.82       1377.87       247.63 o
   0   5   9        103.99         32.18       163.56 o
   1   5   9        110.84         37.02        96.42 o
   2   5   9         30.51        -60.96        84.81 o
   3   5   9        156.64        105.61       108.69 o
   4   5   9          5.72        -24.12       116.32 o
   1   6   9       6077.01       5690.75       427.12 o
   2   6   9         20.75        -82.61        82.61 o
   3   6   9       5155.69       4667.36       363.51 o
   4   6   9        110.85        192.50       105.66 o
   0   7   9         97.72        272.81       315.57 o
   1   7   9         90.28        -76.29       135.40 o
   2   7   9         26.61        -87.97        96.02 o
   3   7   9         73.76         17.26        87.16 o
   1   8   9       2698.81       3077.15       297.80 o
   0   0  10       7559.93       9059.09       761.23 o
   1   0  10         79.68        170.07       135.05 o
   2   0  10       2739.23       2500.62       441.90 o
   3   0  10        253.85        206.57       199.51 o
   1   1  10          8.26        -72.51        72.51 o
   2   1  10          0.48        -43.71        80.02 o
   3   1  10          1.32       -116.11       122.82 o
   0   2  10       6442.45       6056.29       607.44 o
   1   2  10        108.02         74.79        94.01 o
   2   2  10       2373.11       2361.56       290.99 o
   3   2  10         68.89        -59.90       122.39 o
   1   3  10          3.98        -69.07        69.07 o
   2   3  10         30.85       -105.10       105.10 o
   3   3  10          1.04        -60.76       105.92 o
   0   4  10       5550.36       5531.03       485.24 o
   1   4  10         22.50        -28.48        88.61 o
   2   4  10       2621.01       2035.68       243.23 o
   1   5  10          7.90        -94.79       233.02 o
                                                



REM  5_a.res in Pnma
REM wR2 = 0.1069, GooF = S = 1.020, Restrained GooF = 1.020 for all data
REM R1 = 0.0437 for 563 Fo > 4sig(Fo) and 0.0787 for all 971 data
REM 28 parameters refined using 0 restraints

END  
     
WGHT      0.0225     23.7715 

REM Highest difference peak  1.805,  deepest hole -1.692,  1-sigma level  0.318
Q1    1   1.0157  0.8022  1.0330  11.00000  0.05    1.80
Q2    1   0.9658  0.7500  0.9450  10.50000  0.05    1.55
Q3    1   1.1111  0.7278  0.5167  11.00000  0.05    1.22
Q4    1   0.9954  0.5429  0.4317  11.00000  0.05    1.17
Q5    1   0.7002  0.4601  0.8248  11.00000  0.05    1.13

  REM The information below was added by Olex2.
  REM
  REM R1 = 0.0437 for 563 Fo > 4sig(Fo) and 0.0787 for all 6706 data
  REM n/a parameters refined using n/a restraints
  REM Highest difference peak 1.80, deepest hole -1.69
  REM Mean Shift 0, Max Shift 0.000.

  REM +++ Tabular Listing of Refinement Information +++
  REM R1_all = 0.0787
  REM R1_gt = 0.0437
  REM wR_ref = 0.1069
  REM GOOF = 1.020
  REM Shift_max = 0.000
  REM Shift_mean = 0
  REM Reflections_all = 6706
  REM Reflections_gt = 563
  REM Parameters = n/a
  REM Hole = -1.69
  REM Peak = 1.80
  REM Flack = n/a

  
;
_cod_data_source_file            d4ce00235k2.cif
_cod_data_source_block           5
_cod_depositor_comments          'Adding full bibliography for 7248763.cif.'
_cod_original_formula_sum        'Br2.70 Cs I0.30 Pb'
_cod_database_code               7248763
_shelx_shelxl_version_number     2018/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_max   0.692
_shelx_estimated_absorpt_t_min   0.504
_olex2_refinement_description
;
1. Shared sites
{I1, Br1}
{Br2, I2}
2. Uiso/Uaniso restraints and constraints
Uanis(I1) = Uanis(Br1)
Uanis(Br2) = Uanis(I2)
3. Others
 Fixed Sof: Br2(0.9) I1(0.05) I2(0.1) Br1(0.45)
;
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, y, -z-1/2'
'x, -y-1/2, z'
'-x-1/2, y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pb1 Pb 1.000000 0.500000 0.500000 0.0298(2) Uani 1 2 d S T P . .
Cs1 Cs 0.9709(3) 0.750000 0.9926(3) 0.0930(8) Uani 1 2 d S T P . .
Br2 Br 0.7088(3) 0.5245(2) 0.7078(2) 0.0761(7) Uani 0.9 1 d . . . A 5
I1 I 1.0037(5) 0.750000 0.4533(4) 0.0909(12) Uani 0.1 2 d S T P A 3
I2 I 0.7088(3) 0.5245(2) 0.7078(2) 0.0761(7) Uani 0.1 1 d . . . A 6
Br1 Br 1.0037(5) 0.750000 0.4533(4) 0.0909(12) Uani 0.9 2 d S T P A 4
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
Pb1 0.0302(4) 0.0278(4) 0.0314(4) -0.0008(3) -0.0003(3) 0.0011(4)
Cs1 0.0984(18) 0.0783(15) 0.1022(16) 0.000 0.0298(14) 0.000
Br2 0.0630(12) 0.1007(17) 0.0645(11) 0.0053(11) 0.0337(10) 0.0090(12)
I1 0.139(3) 0.0265(12) 0.107(2) 0.000 -0.014(2) 0.000
I2 0.0630(12) 0.1007(17) 0.0645(11) 0.0053(11) 0.0337(10) 0.0090(12)
Br1 0.139(3) 0.0265(12) 0.107(2) 0.000 -0.014(2) 0.000
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cs Cs -0.3680 2.1192 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pb Pb -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Br2 Cs1 Br2 119.02(7) 4_566 . ?
Br2 Cs1 Br2 125.26(7) 8_766 . ?
Br2 Cs1 Br2 62.39(3) 2_665 . ?
Br2 Cs1 Br2 64.23(4) 6_657 . ?
Br2 Cs1 Br2 79.53(8) 7_575 . ?
Br2 Cs1 I1 61.02(5) 4_566 6_657 ?
Br2 Cs1 I1 125.15(6) . 6_657 ?
Br2 Cs1 I1 125.15(6) 7_575 6_657 ?
Br2 Cs1 I1 109.07(6) 8_766 6_657 ?
Br2 Cs1 I1 109.07(6) 2_665 6_657 ?
Br2 Cs1 I1 61.02(5) 6_657 6_657 ?
I1 Cs1 I1 92.29(9) 6_657 . ?
I1 Cs1 I1 100.07(10) 6_557 . ?
I1 Cs1 I1 172.42(14) 1_556 . ?
I1 Cs1 I1 80.14(9) 1_556 6_657 ?
I1 Cs1 I1 167.64(12) 6_557 6_657 ?
I2 Cs1 I1 125.15(6) . 6_657 ?
Pb1 Br2 Pb1 158.05(9) . 2_665 ?
Pb1 Br2 Cs1 104.11(7) . 6_557 ?
Pb1 Br2 Cs1 84.72(6) 2_665 . ?
Pb1 Br2 Cs1 87.99(6) . . ?
Pb1 Br2 Cs1 97.04(7) 2_665 6_557 ?
Pb1 Br2 Cs1 88.09(6) . 2_664 ?
Pb1 Br2 Cs1 93.73(7) 2_665 2_664 ?
Cs1 Br2 Cs1 100.78(6) 6_557 2_664 ?
Cs1 Br2 Cs1 94.01(7) 6_557 . ?
Cs1 Br2 Cs1 165.21(7) 2_664 . ?
Pb1 I1 Pb1 165.06(14) 3_756 . ?
Pb1 I1 Cs1 88.67(8) 3_756 6_557 ?
Pb1 I1 Cs1 82.53(7) 3_756 . ?
Pb1 I1 Cs1 97.39(7) . 1_554 ?
Pb1 I1 Cs1 88.67(8) . 6_557 ?
Pb1 I1 Cs1 89.73(8) 3_756 6_657 ?
Pb1 I1 Cs1 82.53(7) . . ?
Pb1 I1 Cs1 89.73(8) . 6_657 ?
Pb1 I1 Cs1 97.39(7) 3_756 1_554 ?
Cs1 I1 Cs1 167.64(12) 6_657 6_557 ?
Cs1 I1 Cs1 80.73(8) 6_557 . ?
Cs1 I1 Cs1 86.91(8) 6_657 . ?
Cs1 I1 Cs1 100.67(11) 1_554 6_657 ?
Cs1 I1 Cs1 91.69(9) 1_554 6_557 ?
Cs1 I1 Cs1 172.42(14) 1_554 . ?
Pb1 I2 Pb1 158.05(9) . 2_665 ?
Pb1 I2 Cs1 97.04(7) 2_665 6_557 ?
Pb1 I2 Cs1 104.11(7) . 6_557 ?
Pb1 I2 Cs1 87.99(6) . . ?
Pb1 I2 Cs1 88.09(6) . 2_664 ?
Pb1 I2 Cs1 84.72(6) 2_665 . ?
Pb1 I2 Cs1 93.73(7) 2_665 2_664 ?
Cs1 I2 Cs1 100.78(6) 6_557 2_664 ?
Cs1 I2 Cs1 165.21(7) 2_664 . ?
Cs1 I2 Cs1 94.01(7) 6_557 . ?
Pb1 Br1 Pb1 165.06(14) 3_756 . ?
Pb1 Br1 Cs1 97.39(7) . 1_554 ?
Pb1 Br1 Cs1 89.73(8) . 6_657 ?
Pb1 Br1 Cs1 89.73(8) 3_756 6_657 ?
Pb1 Br1 Cs1 97.39(7) 3_756 1_554 ?
Cs1 Br1 Cs1 100.67(11) 1_554 6_657 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pb1 Br2 2.9758(18) . ?
Pb1 Br2 2.9829(18) 6_657 ?
Pb1 Br2 2.9758(18) 5_766 ?
Pb1 Br2 2.9829(18) 2_664 ?
Pb1 I1 2.9788(9) 5_766 ?
Pb1 I1 2.9788(9) . ?
Pb1 I2 2.9758(18) . ?
Pb1 Br1 2.9788(9) . ?
Cs1 Cs1 5.765(3) 6_657 ?
Cs1 Br2 4.165(3) 7_575 ?
Cs1 Br2 3.987(3) 2_665 ?
Cs1 Br2 3.987(3) 8_766 ?
Cs1 Br2 4.165(3) . ?
Cs1 Br2 3.705(3) 4_566 ?
Cs1 Br2 3.705(3) 6_657 ?
Cs1 I1 3.898(5) 6_557 ?
Cs1 I1 4.462(4) . ?
Cs1 I1 3.813(4) 1_556 ?
Cs1 I1 4.438(5) 6_657 ?
Cs1 I2 4.165(3) . ?
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_meas
_refln_F_squared_sigma
0 0 -1 0.1 0.5
0 0 1 1 0.7
0 0 -1 0.2 0.9
0 0 1 0.2 0.8
0 0 2 2773.42 132.39
0 0 -2 2617.84 130.99
0 0 -2 2551.64 179.58
0 0 2 2695.73 181.18
0 0 3 1.2 2.6
0 0 3 -1 1.4
0 0 -3 1.7 1.8
0 0 -3 1.7 2.5
0 0 4 4025.7 184.68
0 0 -4 3839.12 182.48
0 0 -5 -1.2 3.4
0 0 -5 4.2 3.8
0 0 5 -1.7 3.1
0 0 5 0.7 2.5
0 0 6 821.92 43.9
0 0 6 865.71 50.59
0 0 -6 810.92 44.6
0 0 -6 865.71 47.7
0 0 7 -2.3 5.4
0 0 -7 -5.7 2.5
0 0 7 1.5 4
0 0 -7 -0.7 5
0 0 -8 227.38 17.5
0 0 8 199.48 16.6
0 0 8 179.48 26.1
0 0 9 -1.4 7
0 0 -9 2.8 5.6
0 0 9 1.8 4.5
0 0 10 190.78 31.6
0 0 -10 196.88 19.2
1 0 0 0.3 0.6
-1 0 0 -0.3 0.4
1 0 1 933.31 43.6
-1 0 -1 919.41 43.5
1 0 -2 227.38 13.3
-1 0 2 222.48 14
1 0 -2 227.98 13.7
-1 0 -2 229.08 11.9
-1 0 -2 218.68 13.7
-1 0 2 256.27 13.5
1 0 2 226.28 14.2
1 0 2 236.58 11.8
1 0 -3 999.4 50.39
-1 0 -3 997.9 50.69
-1 0 3 1029.3 49.5
1 0 -3 1029.1 49.8
1 0 3 1002.3 51.49
-1 0 -4 367.56 20.6
1 0 4 376.76 24.7
-1 0 4 357.06 24.2
-1 0 4 400.56 22.2
1 0 4 389.16 20.3
1 0 -4 371.06 23.3
-1 0 -4 367.66 23.4
1 0 -4 365.06 22.1
1 0 -5 192.28 14.8
-1 0 5 196.08 17
1 0 5 188.08 12.7
-1 0 -5 189.78 13.3
1 0 5 199.78 17.1
-1 0 5 191.08 14.3
-1 0 -5 188.18 16
1 0 -6 136.09 13.3
1 0 6 129.39 11.2
-1 0 6 146.69 12.9
1 0 6 122.69 17.4
-1 0 -6 143.99 11.9
-1 0 -6 170.98 18.3
-1 0 6 166.98 20.6
1 0 7 264.17 24.3
1 0 7 247.78 17.9
-1 0 7 303.87 25.6
-1 0 7 244.38 19
-1 0 -7 269.17 18.5
-1 0 -7 242.78 21.2
-1 0 8 30.2 13.2
1 0 8 47.4 13.8
1 0 8 67.09 10.3
1 0 -8 47.4 9.2
-1 0 8 66.39 17.7
-1 0 -8 43.1 8.4
1 0 9 102.29 20.5
1 0 -9 82.69 13.1
-1 0 9 119.29 23.2
1 0 9 109.79 14.5
-1 0 10 11.1 10.4
1 0 -10 -3.9 6.9
1 0 10 -1.7 8.8
1 0 10 8 6.4
-1 0 10 4.3 6.4
-1 0 -10 5 6.2
2 0 0 2538.55 120.89
-2 0 0 2466.85 120.29
-2 0 0 2707.13 141.59
2 0 0 2642.44 141.29
2 0 -1 206.48 12
-2 0 1 208.08 11.9
2 0 -2 8922.61 403.66
2 0 2 8751.22 402.46
2 0 2 8628.04 461.45
-2 0 2 9165.98 405.26
-2 0 -2 8847.42 472.55
-2 0 -2 8238.68 400.86
-2 0 2 8361.26 456.55
2 0 -3 100.79 8.8
-2 0 3 92.59 9.1
2 0 3 99.29 9.5
-2 0 -3 93.69 8.7
-2 0 3 85.49 8
-2 0 4 1249.77 60.29
2 0 4 1213.48 62.69
2 0 -4 1195.28 60.49
2 0 4 1199.68 56.79
-2 0 -4 1179.78 61.09
-2 0 4 1206.98 63.09
-2 0 5 1.3 3.3
-2 0 5 4.6 4.6
2 0 5 6.8 5.3
2 0 5 10.8 3.4
-2 0 -5 10.5 5.8
2 0 -5 15.1 5.6
-2 0 -5 9.2 3.8
2 0 6 786.62 41.2
-2 0 -6 839.62 46.7
-2 0 6 821.62 49.5
-2 0 -6 854.51 42.2
2 0 -6 779.52 45.1
2 0 6 867.31 53.19
-2 0 6 779.32 44.5
-2 0 7 3.9 4.3
2 0 7 7.8 4.5
-2 0 -7 -2.5 4.8
-2 0 -7 6 4.4
-2 0 7 3.7 6.9
2 0 7 -1.9 3.9
2 0 -7 3.4 4.8
2 0 8 354.46 22.3
-2 0 8 349.87 25.5
-2 0 -8 354.86 31
-2 0 -8 360.56 28.2
2 0 8 331.17 30.7
-2 0 8 374.66 32.3
-2 0 9 9.9 9.7
-2 0 9 7.7 7
2 0 9 2.3 10.1
2 0 9 4.6 5.4
-2 0 -9 14.2 6.8
2 0 -9 13.1 7.8
2 0 10 77.39 12.1
-2 0 -10 38.4 9.9
-2 0 10 49.1 12.2
-2 0 10 31.7 14
3 0 0 0.7 1.5
-3 0 0 1.3 1.7
3 0 -1 1364.16 64.09
-3 0 1 1331.67 63.89
3 0 -2 75.99 7.3
3 0 2 89.79 7.8
-3 0 2 79.69 7.4
-3 0 2 78.99 7.6
-3 0 -2 76.39 8.3
3 0 -3 118.89 10.6
-3 0 3 148.69 11.8
-3 0 -3 126.79 10.7
3 0 3 124.39 11
-3 0 3 131.89 10.6
-3 0 -4 60.19 9.7
3 0 -4 87.89 12.1
-3 0 4 63.19 9.3
-3 0 4 87.69 12.1
-3 0 5 830.82 47.8
-3 0 -5 848.92 46.3
3 0 5 822.72 61.09
-3 0 5 811.42 45
-3 0 6 110.19 14.6
3 0 -6 95.19 12.5
3 0 6 102.49 15.8
-3 0 6 154.08 19.9
-3 0 -6 124.89 15.3
-3 0 -7 71.49 14.1
-3 0 7 51.89 11
-3 0 7 74.29 15.6
3 0 7 58.89 8
3 0 7 55.49 13.3
3 0 -7 76.69 12.1
-3 0 -8 2.6 7.1
-3 0 -8 14.8 5.6
-3 0 8 4.3 8.2
-3 0 8 16.5 8.3
3 0 -8 13.2 8
3 0 8 4.1 6.7
3 0 -9 88.09 16.8
-3 0 9 137.59 18.5
-3 0 -9 131.59 15.9
-3 0 9 73.09 28
-3 0 10 0.3 8
3 0 10 7.1 5.1
4 0 0 4005.1 194.78
-4 0 0 4070.99 192.48
4 0 0 4292.37 228.08
-4 0 0 4270.27 266.47
4 0 -1 438.06 24.2
-4 0 2 1346.07 65.49
4 0 -2 1326.97 65.59
-4 0 -3 52.69 7.8
-4 0 3 60.39 9.3
4 0 -3 40.2 7.7
4 0 3 36.2 6.9
-4 0 3 52.39 8.5
4 0 -4 1679.13 83.69
-4 0 4 1745.23 83.39
4 0 4 1667.83 85.59
-4 0 4 1649.33 84.49
-4 0 -5 12.9 6.2
4 0 5 6.6 5.5
-4 0 5 9 5.4
4 0 -5 2.5 4.8
-4 0 5 31.3 9
-4 0 6 286.57 25
4 0 6 307.07 25.1
-4 0 -6 340.37 24.1
-4 0 6 278.77 22.1
4 0 7 24.9 9.4
-4 0 -7 42.7 10
-4 0 7 58.99 14.7
-4 0 7 53.19 10.3
-4 0 -8 190.08 32.2
-4 0 8 234.68 19.5
4 0 8 149.59 23.4
-4 0 8 193.58 27.5
-4 0 9 6.6 6.6
-4 0 9 2.2 8.9
-5 0 0 0.8 2.2
5 0 -1 418.66 24.8
-5 0 1 445.06 24.7
-5 0 2 7.3 3.9
5 0 -2 2.7 3.5
-5 0 3 990.1 52.59
-5 0 3 1083.19 53.49
5 0 -3 997.6 53.59
5 0 -4 13.2 4.8
-5 0 -4 9 5.2
-5 0 4 8.3 5
5 0 4 2.5 3.9
-5 0 4 5.2 4.9
-5 0 5 24.9 8.7
-5 0 -5 35.5 8.7
5 0 5 37.1 9.1
-5 0 5 25.3 8.5
5 0 -5 28.8 7.6
-5 0 -6 4 5.6
-5 0 6 -2.1 3.8
-5 0 6 19.4 8.8
-5 0 7 380.16 29.1
-5 0 -7 304.57 27.6
5 0 7 193.98 31.4
-5 0 7 282.17 40.3
-5 0 8 11.7 7.7
-5 0 8 7.3 7.2
-5 0 -8 27.4 8.9
-5 0 9 20.7 9.6
-5 0 9 29.5 14.4
-6 0 0 850.31 43
-6 0 1 137.09 11.4
-6 0 2 843.52 45.5
6 0 -2 883.21 46.7
-6 0 3 115.09 14.1
6 0 -3 134.49 12.5
-6 0 4 286.47 22
-6 0 4 330.17 22.7
6 0 -4 327.97 23.3
-6 0 5 0.2 4
-6 0 -5 6.5 5.9
-6 0 5 0.4 4.3
6 0 -5 2 5.8
6 0 5 -1.3 3.4
-6 0 6 346.27 29
-6 0 6 406.06 28.1
6 0 -7 14.4 10.7
-6 0 7 -2.2 5.3
6 0 7 -4.3 3.3
-6 0 -7 2.8 6.1
-6 0 7 3 5.9
-6 0 8 42.9 11.3
-6 0 8 36.1 14.7
-7 0 0 0.7 3
-7 0 1 417.16 25
-7 0 2 13.5 5.8
7 0 -2 18.9 6.4
7 0 -3 146.09 14.2
7 0 -4 18.6 8.4
-7 0 4 45.4 10.8
7 0 -5 341.87 28.8
-7 0 5 362.06 26
-7 0 5 317.47 25.5
-7 0 -6 -5.7 3.7
-7 0 6 -7.1 3.3
7 0 -6 -2.4 6.4
-7 0 6 0.7 5
-7 0 -7 22.2 8.8
-7 0 7 32.8 9.4
-7 0 7 3.5 7.5
-7 0 8 -1.2 4.7
-7 0 8 6.9 10.1
-8 0 1 50.79 8.6
-8 0 2 341.47 23.2
8 0 -3 25.5 8.7
-8 0 4 245.08 20.1
-8 0 5 29.1 12.3
8 0 -5 14.5 8.9
-8 0 5 24.7 7.7
-8 0 6 55.49 13.8
-8 0 6 29.9 8.9
-8 0 7 6 6
-8 0 7 2.4 7.4
-9 0 1 184.18 14.7
-9 0 2 5 5.4
-9 0 3 178.58 16.2
9 0 -4 0.9 7.3
-9 0 4 11.6 7.2
-9 0 5 49.2 11.1
-10 0 1 3 4.2
-10 0 2 54.99 10.5
-10 0 3 9.4 5.8
0 -1 1 0.5 1.2
0 1 1 1.3 0.8
0 -1 1 2.2 1
0 1 -1 0.9 0.9
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2 -3 -2 2.9 2.5
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3 -12 0 -6.1 5.7
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3 -12 -1 244.38 20.5
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3 -12 -2 8.4 6.2
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6 -12 -1 -5.6 4.1
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1 -13 -2 30.9 12.1
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2 15 1 0.4 4.2
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