#------------------------------------------------------------------------------
#$Date: 2019-11-08 01:33:54 +0200 (Fri, 08 Nov 2019) $
#$Revision: 224517 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/70/05/7700534.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7700534
loop_
_publ_author_name
'Naito, Toshio'
'Watanabe, Naoki'
'Sakamoto, Yuuka'
'Miyaji, Yuuko'
'Shirahata, Takashi'
'Misaki, Yohji'
'Kitou, Shunsuke'
'Sawa, Hiroshi'
_publ_section_title
;
 A molecular crystal with an unprecedentedly long-lived photoexcited
 state.
;
_journal_issue                   34
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              12858
_journal_page_last               12866
_journal_paper_doi               10.1039/c9dt02377a
_journal_volume                  48
_journal_year                    2019
_chemical_formula_moiety         'C24 H12 Au2 N2 S20'
_chemical_formula_sum            'C24 H12 Au2 N2 S20'
_chemical_formula_weight         1363.51
_chemical_name_systematic        BPY[Au(dmit)2]2
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_update_record
;
2019-01-07 deposited with the CCDC.    2019-07-04 downloaded from the CCDC.
;
_cell_angle_alpha                90.0000
_cell_angle_beta                 100.156(3)
_cell_angle_gamma                90.0000
_cell_formula_units_Z            4
_cell_length_a                   11.272(3)
_cell_length_b                   14.442(4)
_cell_length_c                   23.582(7)
_cell_measurement_reflns_used    7316
_cell_measurement_temperature    300
_cell_measurement_theta_max      31.15
_cell_measurement_theta_min      2.31
_cell_volume                     3778.8(18)
_computing_cell_refinement       CrystalClear
_computing_data_collection       'CrystalClear (Rigaku Inc., 2008)'
_computing_data_reduction        CrystalClear
_computing_molecular_graphics    'CrystalStructure 4.2.2'
_computing_publication_material  'CrystalStructure 4.2.2 (Rigaku, 2016)'
_computing_structure_refinement  'SHELXL Version 2014/6 (Sheldrick, 2008)'
_computing_structure_solution    'SIR2011 (Burla, et al., 2012)'
_diffrn_ambient_temperature      300
_diffrn_detector_area_resol_mean 7.111
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.913
_diffrn_measurement_device_type  'Rigaku Saturn724'
_diffrn_measurement_method       ω
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71075
_diffrn_reflns_av_R_equivalents  0.1365
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.913
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       33
_diffrn_reflns_limit_l_min       -32
_diffrn_reflns_number            65090
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.913
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         31.309
_diffrn_reflns_theta_min         2.251
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    8.915
_exptl_absorpt_correction_T_max  0.915
_exptl_absorpt_correction_T_min  0.472
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'REQAB (Rigaku, 1998)'
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    2.397
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       platelet
_exptl_crystal_F_000             2592.00
_exptl_crystal_preparation       'photo-responsive molecular structure'
_exptl_crystal_recrystallization_method
'Re-crystallisation from solvent: CH3CN'
_exptl_crystal_size_max          0.300
_exptl_crystal_size_mid          0.140
_exptl_crystal_size_min          0.010
_refine_diff_density_max         1.37
_refine_diff_density_min         -2.63
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.183
_refine_ls_hydrogen_treatment    constr
_refine_ls_number_parameters     443
_refine_ls_number_reflns         11302
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.1563
_refine_ls_R_factor_gt           0.1007
_refine_ls_shift/su_max          0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[σ²(Fo²)+(0.0724P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1977
_refine_ls_wR_factor_ref         0.2224
_reflns_Friedel_coverage         0.000
_reflns_number_gt                7527
_reflns_number_total             11302
_reflns_threshold_expression     F²>2.0σ(F²)
_cod_data_source_file            c9dt02377a2.cif
_cod_data_source_block           300K_irr_2nd
_cod_depositor_comments
'Adding full bibliography for 7700531--7700563.cif.'
_cod_database_code               7700534
_shelxl_version_number           2014/6
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 +X,+Y,+Z
2 -X,1/2+Y,1/2-Z
3 -X,-Y,-Z
4 +X,-1/2-Y,-1/2+Z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au2A Au 0.0056(2) 0.1447(2) 0.75751(8) 0.0364(5) Uani 0.912(13) 1 d . . P A 1
Au2B Au -0.0093(10) 0.113(2) 0.7486(7) 0.050(3) Uani 0.088(13) 1 d . . P A 2
Au1 Au 0.50734(4) 0.12720(3) 0.74736(2) 0.03657(17) Uani 1 1 d . . . . .
S1 S 0.6805(5) 0.1144(4) 0.4676(2) 0.0964(17) Uani 1 1 d . . . . .
S2 S 0.6122(3) 0.2186(3) 0.56514(14) 0.0648(10) Uani 1 1 d . . . . .
S3 S 0.5933(3) 0.0201(3) 0.56485(14) 0.0600(9) Uani 1 1 d . . . . .
S4 S 0.5389(3) 0.2405(2) 0.68119(13) 0.0516(8) Uani 1 1 d . . . . .
S5 S 0.5129(3) 0.0116(2) 0.67955(13) 0.0501(8) Uani 1 1 d . . . . .
S6 S 0.5029(3) 0.2422(2) 0.81572(13) 0.0490(8) Uani 1 1 d . . . . .
S7 S 0.4762(3) 0.0141(2) 0.81290(14) 0.0528(8) Uani 1 1 d . . . . .
S8 S 0.4258(3) 0.2311(3) 0.93146(14) 0.0613(10) Uani 1 1 d . . . . .
S9 S 0.4072(3) 0.0323(3) 0.92986(15) 0.0624(10) Uani 1 1 d . . . . .
S10 S 0.3469(5) 0.1338(3) 1.0301(2) 0.0953(17) Uani 1 1 d . . . . .
S11 S 0.1824(5) 0.1512(4) 0.4789(2) 0.1084(19) Uani 1 1 d . . . . .
S12 S 0.2419(3) 0.1394(3) 0.60490(16) 0.0625(10) Uani 1 1 d . . . . .
S13 S -0.0064(3) 0.1655(3) 0.55147(16) 0.0746(12) Uani 1 1 d . . . . .
S14 S 0.1884(3) 0.1385(2) 0.72529(15) 0.0517(8) Uani 1 1 d . . . . .
S15 S -0.0979(3) 0.1722(3) 0.66424(14) 0.0599(10) Uani 1 1 d . . . . .
S16 S 0.1068(3) 0.1259(2) 0.85117(15) 0.0552(9) Uani 1 1 d . . . . .
S17 S -0.1796(3) 0.1390(2) 0.78723(15) 0.0539(9) Uani 1 1 d . . . . .
S18 S 0.0089(3) 0.1159(3) 0.96196(15) 0.0636(11) Uani 1 1 d . . . . .
S19 S -0.2390(3) 0.1294(2) 0.90622(15) 0.0536(9) Uani 1 1 d . . . . .
S20 S -0.1863(4) 0.1109(3) 1.03235(18) 0.0714(12) Uani 1 1 d . . . . .
N1 N -0.0061(11) -0.0919(8) 0.6830(5) 0.065(3) Uani 1 1 d . . . . .
N2 N -0.1796(10) -0.1183(6) 0.7518(4) 0.046(3) Uani 1 1 d . . . . .
C1 C 0.6361(12) 0.1169(10) 0.5297(6) 0.060(4) Uani 1 1 d . . . . .
C2 C 0.5656(10) 0.1691(8) 0.6244(4) 0.039(3) Uani 1 1 d . . . . .
C3 C 0.5567(10) 0.0760(8) 0.6237(5) 0.044(3) Uani 1 1 d . . . . .
C4 C 0.4573(10) 0.1779(9) 0.8701(5) 0.047(3) Uani 1 1 d . . . . .
C5 C 0.4497(10) 0.0852(9) 0.8697(5) 0.047(3) Uani 1 1 d . . . . .
C6 C 0.3867(11) 0.1352(10) 0.9655(6) 0.058(4) Uani 1 1 d . . . . .
C7 C 0.1406(13) 0.1523(11) 0.5422(7) 0.073(5) Uani 1 1 d . . . . .
C8 C 0.1373(10) 0.1465(8) 0.6516(5) 0.047(3) Uani 1 1 d . . . . .
C9 C 0.0221(11) 0.1609(9) 0.6268(5) 0.049(3) Uani 1 1 d . . . . .
C10 C -0.0165(11) 0.1266(8) 0.8880(6) 0.046(3) Uani 1 1 d . . . . .
C11 C -0.1319(11) 0.1346(8) 0.8621(6) 0.049(3) Uani 1 1 d . . . . .
C12 C -0.1410(13) 0.1177(9) 0.9702(7) 0.059(4) Uani 1 1 d . . . . .
C13 C 0.0714(15) -0.0921(11) 0.6443(7) 0.083(5) Uani 1 1 d . . . . .
H13 H 0.0421 -0.0839 0.6052 0.099 Uiso 1 1 calc R U . . .
C14 C 0.1933(15) -0.1045(10) 0.6637(8) 0.080(5) Uani 1 1 d . . . . .
H14 H 0.2473 -0.1048 0.6381 0.096 Uiso 1 1 calc R U . . .
C15 C 0.2330(13) -0.1164(8) 0.7221(7) 0.060(4) Uani 1 1 d . . . . .
H15 H 0.3148 -0.1247 0.7361 0.072 Uiso 1 1 calc R U . . .
C16 C 0.1507(12) -0.1162(8) 0.7604(6) 0.057(4) Uani 1 1 d . . . . .
H16 H 0.1775 -0.1243 0.7997 0.068 Uiso 1 1 calc R U . . .
C17 C 0.0327(13) -0.1042(8) 0.7397(5) 0.050(3) Uani 1 1 d . . . . .
C18 C -0.0628(11) -0.1053(8) 0.7762(5) 0.047(3) Uani 1 1 d . . . . .
C19 C -0.0346(12) -0.0989(9) 0.8346(5) 0.058(4) Uani 1 1 d . . . . .
H19 H 0.0452 -0.0919 0.8527 0.069 Uiso 1 1 calc R U . . .
C20 C -0.1238(14) -0.1028(9) 0.8659(6) 0.063(4) Uani 1 1 d . . . . .
H20 H -0.1038 -0.0965 0.9057 0.075 Uiso 1 1 calc R U . . .
C21 C -0.2433(13) -0.1158(9) 0.8417(7) 0.069(4) Uani 1 1 d . . . . .
H21 H -0.3035 -0.1194 0.8640 0.083 Uiso 1 1 calc R U . . .
C22 C -0.2674(13) -0.1230(8) 0.7841(6) 0.056(4) Uani 1 1 d . . . . .
H22 H -0.3468 -0.1314 0.7659 0.068 Uiso 1 1 calc R U . . .
C23 C -0.2078(13) -0.1334(9) 0.6892(6) 0.065(4) Uani 1 1 d . . . . .
H23A H -0.1899 -0.1970 0.6805 0.077 Uiso 1 1 calc R U . . .
H23B H -0.2930 -0.1227 0.6755 0.077 Uiso 1 1 calc R U . . .
C24 C -0.1382(13) -0.0716(10) 0.6601(6) 0.078(5) Uani 1 1 d . . . . .
H24A H -0.1568 -0.0077 0.6676 0.093 Uiso 1 1 calc R U . . .
H24B H -0.1562 -0.0820 0.6188 0.093 Uiso 1 1 calc R U . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016
;
International Tables for Crystallography
(Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
H H 0.0000 0.0000
;
International Tables for Crystallography
(Vol. C, Table 6.1.1.4)
;
Au Au -2.0133 8.8022
;
International Tables for Crystallography
(Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
N N 0.0061 0.0033
;
International Tables for Crystallography
(Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
S S 0.1246 0.1234
;
International Tables for Crystallography
(Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
S16 Au2A S17 91.50(12)
S16 Au2A S14 89.50(14)
S17 Au2A S14 175.5(2)
S16 Au2A S15 176.83(19)
S17 Au2A S15 87.93(14)
S14 Au2A S15 91.31(12)
S15 Au2B S17 90.9(7)
S15 Au2B S14 91.3(4)
S17 Au2B S14 159.0(17)
S15 Au2B S16 153.0(17)
S17 Au2B S16 86.4(7)
S14 Au2B S16 82.2(4)
S7 Au1 S5 88.74(12)
S7 Au1 S6 90.97(12)
S5 Au1 S6 179.55(12)
S7 Au1 S4 179.77(11)
S5 Au1 S4 91.03(12)
S6 Au1 S4 89.25(12)
C2 S2 C1 97.7(6)
C3 S3 C1 97.7(6)
C2 S4 Au1 99.5(4)
C3 S5 Au1 100.4(4)
C4 S6 Au1 100.1(4)
C5 S7 Au1 99.3(4)
C6 S8 C4 98.2(7)
C6 S9 C5 95.5(7)
C7 S12 C8 96.7(6)
C7 S13 C9 96.7(7)
C8 S14 Au2A 99.7(4)
C8 S14 Au2B 94.7(5)
C9 S15 Au2B 98.7(6)
C9 S15 Au2A 99.1(4)
C10 S16 Au2A 99.8(4)
C10 S16 Au2B 98.7(5)
C11 S17 Au2B 105.3(5)
C11 S17 Au2A 99.9(4)
C10 S18 C12 96.9(7)
C12 S19 C11 97.1(7)
C17 N1 C13 121.9(13)
C17 N1 C24 120.5(12)
C13 N1 C24 117.5(12)
C18 N2 C22 121.3(11)
C18 N2 C23 118.0(11)
C22 N2 C23 120.6(11)
S1 C1 S2 123.4(9)
S1 C1 S3 124.5(9)
S2 C1 S3 111.8(7)
C3 C2 S2 115.7(8)
C3 C2 S4 124.9(8)
S2 C2 S4 119.3(7)
C2 C3 S3 116.8(9)
C2 C3 S5 123.4(9)
S3 C3 S5 119.8(7)
C5 C4 S8 115.3(9)
C5 C4 S6 123.8(9)
S8 C4 S6 120.8(7)
C4 C5 S9 117.2(9)
C4 C5 S7 124.8(9)
S9 C5 S7 118.0(8)
S10 C6 S8 125.3(9)
S10 C6 S9 120.8(8)
S8 C6 S9 113.6(8)
S11 C7 S12 122.0(9)
S11 C7 S13 123.6(10)
S12 C7 S13 114.4(9)
C9 C8 S14 124.8(9)
C9 C8 S12 116.2(10)
S14 C8 S12 119.0(6)
C8 C9 S15 124.7(10)
C8 C9 S13 116.0(10)
S15 C9 S13 119.3(7)
C11 C10 S18 116.4(10)
C11 C10 S16 124.1(11)
S18 C10 S16 119.6(7)
C10 C11 S19 116.5(10)
C10 C11 S17 124.3(11)
S19 C11 S17 119.0(7)
S20 C12 S19 122.7(9)
S20 C12 S18 124.2(9)
S19 C12 S18 113.1(9)
N1 C13 C14 119.6(15)
N1 C13 H13 120.2
C14 C13 H13 120.2
C13 C14 C15 118.3(16)
C13 C14 H14 120.8
C15 C14 H14 120.8
C14 C15 C16 120.4(15)
C14 C15 H15 119.8
C16 C15 H15 119.8
C17 C16 C15 119.3(14)
C17 C16 H16 120.3
C15 C16 H16 120.3
N1 C17 C16 120.4(13)
N1 C17 C18 115.7(12)
C16 C17 C18 123.8(12)
N2 C18 C19 118.5(13)
N2 C18 C17 120.2(11)
C19 C18 C17 121.3(12)
C20 C19 C18 119.1(13)
C20 C19 H19 120.4
C18 C19 H19 120.4
C19 C20 C21 123.1(14)
C19 C20 H20 118.4
C21 C20 H20 118.4
C22 C21 C20 116.0(14)
C22 C21 H21 122.0
C20 C21 H21 122.0
C21 C22 N2 121.9(14)
C21 C22 H22 119.0
N2 C22 H22 119.0
C24 C23 N2 110.4(11)
C24 C23 H23A 109.6
N2 C23 H23A 109.6
C24 C23 H23B 109.6
N2 C23 H23B 109.6
H23A C23 H23B 108.1
C23 C24 N1 107.0(12)
C23 C24 H24A 110.3
N1 C24 H24A 110.3
C23 C24 H24B 110.3
N1 C24 H24B 110.3
H24A C24 H24B 108.6
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
Au2A S16 2.316(4)
Au2A S17 2.318(4)
Au2A S14 2.320(4)
Au2A S15 2.335(4)
Au2B S15 2.234(14)
Au2B S17 2.297(19)
Au2B S14 2.417(11)
Au2B S16 2.546(16)
Au1 S7 2.318(3)
Au1 S5 2.320(3)
Au1 S6 2.322(3)
Au1 S4 2.331(3)
S1 C1 1.629(13)
S2 C2 1.732(11)
S2 C1 1.735(14)
S3 C3 1.718(12)
S3 C1 1.737(14)
S4 C2 1.758(11)
S5 C3 1.753(12)
S6 C4 1.733(12)
S7 C5 1.755(13)
S8 C6 1.696(14)
S8 C4 1.729(11)
S9 C6 1.743(14)
S9 C5 1.751(12)
S10 C6 1.664(14)
S11 C7 1.644(15)
S12 C7 1.711(16)
S12 C8 1.752(12)
S13 C7 1.721(14)
S13 C9 1.749(13)
S14 C8 1.736(13)
S15 C9 1.748(12)
S16 C10 1.765(13)
S17 C11 1.754(13)
S18 C10 1.723(13)
S18 C12 1.734(14)
S19 C12 1.714(16)
S19 C11 1.729(13)
S20 C12 1.638(16)
N1 C17 1.343(14)
N1 C13 1.372(17)
N1 C24 1.520(16)
N2 C18 1.354(15)
N2 C22 1.353(17)
N2 C23 1.471(15)
C2 C3 1.347(16)
C4 C5 1.341(17)
C8 C9 1.344(15)
C10 C11 1.341(16)
C13 C14 1.38(2)
C13 H13 0.9300
C14 C15 1.38(2)
C14 H14 0.9300
C15 C16 1.405(18)
C15 H15 0.9300
C16 C17 1.344(17)
C16 H16 0.9300
C17 C18 1.493(18)
C18 C19 1.359(16)
C19 C20 1.351(17)
C19 H19 0.9300
C20 C21 1.380(18)
C20 H20 0.9300
C21 C22 1.340(19)
C21 H21 0.9300
C22 H22 0.9300
C23 C24 1.440(17)
C23 H23A 0.9700
C23 H23B 0.9700
C24 H24A 0.9700
C24 H24B 0.9700
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
C2 S2 C1 S1 178.8(10)
C2 S2 C1 S3 4.6(9)
C3 S3 C1 S1 -178.6(10)
C3 S3 C1 S2 -4.4(9)
C1 S2 C2 C3 -3.1(10)
C1 S2 C2 S4 174.7(7)
Au1 S4 C2 C3 4.9(10)
Au1 S4 C2 S2 -172.7(6)
S2 C2 C3 S3 0.4(12)
S4 C2 C3 S3 -177.3(7)
S2 C2 C3 S5 179.3(6)
S4 C2 C3 S5 1.6(15)
C1 S3 C3 C2 2.6(10)
C1 S3 C3 S5 -176.4(7)
Au1 S5 C3 C2 -7.1(10)
Au1 S5 C3 S3 171.8(6)
C6 S8 C4 C5 -3.8(10)
C6 S8 C4 S6 179.4(8)
Au1 S6 C4 C5 9.0(11)
Au1 S6 C4 S8 -174.5(6)
S8 C4 C5 S9 1.0(12)
S6 C4 C5 S9 177.6(7)
S8 C4 C5 S7 179.7(7)
S6 C4 C5 S7 -3.7(15)
C6 S9 C5 C4 2.3(10)
C6 S9 C5 S7 -176.5(7)
Au1 S7 C5 C4 -4.1(11)
Au1 S7 C5 S9 174.6(6)
C4 S8 C6 S10 178.6(9)
C4 S8 C6 S9 5.2(8)
C5 S9 C6 S10 -178.4(8)
C5 S9 C6 S8 -4.7(8)
C8 S12 C7 S11 -179.6(10)
C8 S12 C7 S13 0.0(10)
C9 S13 C7 S11 -179.4(10)
C9 S13 C7 S12 1.1(10)
Au2A S14 C8 C9 5.4(12)
Au2B S14 C8 C9 16.9(15)
Au2A S14 C8 S12 -176.9(6)
Au2B S14 C8 S12 -165.4(11)
C7 S12 C8 C9 -1.6(12)
C7 S12 C8 S14 -179.5(8)
S14 C8 C9 S15 -1.3(18)
S12 C8 C9 S15 -179.0(7)
S14 C8 C9 S13 -179.6(7)
S12 C8 C9 S13 2.6(14)
Au2B S15 C9 C8 -16.7(15)
Au2A S15 C9 C8 -3.6(12)
Au2B S15 C9 S13 161.6(11)
Au2A S15 C9 S13 174.7(7)
C7 S13 C9 C8 -2.2(12)
C7 S13 C9 S15 179.3(8)
C12 S18 C10 C11 1.5(11)
C12 S18 C10 S16 -178.2(7)
Au2A S16 C10 C11 1.1(11)
Au2B S16 C10 C11 -10.1(14)
Au2A S16 C10 S18 -179.2(6)
Au2B S16 C10 S18 169.6(10)
S18 C10 C11 S19 -2.0(13)
S16 C10 C11 S19 177.7(6)
S18 C10 C11 S17 -175.9(6)
S16 C10 C11 S17 3.8(16)
C12 S19 C11 C10 1.4(11)
C12 S19 C11 S17 175.6(7)
Au2B S17 C11 C10 5.9(14)
Au2A S17 C11 C10 -6.3(11)
Au2B S17 C11 S19 -167.9(11)
Au2A S17 C11 S19 -180.0(6)
C11 S19 C12 S20 178.7(9)
C11 S19 C12 S18 -0.3(8)
C10 S18 C12 S20 -179.5(9)
C10 S18 C12 S19 -0.5(8)
C17 N1 C13 C14 -1(2)
C24 N1 C13 C14 176.0(13)
N1 C13 C14 C15 0(2)
C13 C14 C15 C16 0(2)
C14 C15 C16 C17 0(2)
C13 N1 C17 C16 1(2)
C24 N1 C17 C16 -175.7(12)
C13 N1 C17 C18 -178.1(12)
C24 N1 C17 C18 5.5(17)
C15 C16 C17 N1 -0.5(19)
C15 C16 C17 C18 178.2(11)
C22 N2 C18 C19 1.3(17)
C23 N2 C18 C19 -174.7(10)
C22 N2 C18 C17 177.6(10)
C23 N2 C18 C17 1.5(15)
N1 C17 C18 N2 17.0(16)
C16 C17 C18 N2 -161.8(12)
N1 C17 C18 C19 -166.9(12)
C16 C17 C18 C19 14.3(19)
N2 C18 C19 C20 -2.0(19)
C17 C18 C19 C20 -178.2(12)
C18 C19 C20 C21 2(2)
C19 C20 C21 C22 -1(2)
C20 C21 C22 N2 0(2)
C18 N2 C22 C21 -0.5(18)
C23 N2 C22 C21 175.4(12)
C18 N2 C23 C24 -41.8(16)
C22 N2 C23 C24 142.1(12)
N2 C23 C24 N1 59.4(15)
C17 N1 C24 C23 -43.7(18)
C13 N1 C24 C23 139.7(14)
