#------------------------------------------------------------------------------
#$Date: 2019-11-07 23:16:53 +0200 (Thu, 07 Nov 2019) $
#$Revision: 223977 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/70/07/7700724.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7700724
loop_
_publ_author_name
'Ma, Xiufang'
'Chen, Bingbing'
'Zhang, Yi-Quan'
'Yang, Jinhui'
'Shi, Quan'
'Ma, Yulong'
'Liu, Xiangyu'
_publ_section_title
;
 Enhancing single-molecule magnet behaviour through decorating terminal
 ligands in Dy₂ compounds.
;
_journal_issue                   33
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              12622
_journal_page_last               12631
_journal_paper_doi               10.1039/c9dt02758k
_journal_volume                  48
_journal_year                    2019
_chemical_formula_moiety         'C56 H56 Cl4 Dy2 N8 O6, 2I, 0.48(H2 O)'
_chemical_formula_sum            'C56 H56.97 Cl4 Dy2 I2 N8 O6.48'
_chemical_formula_weight         1666.42
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   mixed
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2018-11-12 deposited with the CCDC.    2019-07-31 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 107.506(2)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   11.8909(8)
_cell_length_b                   17.0320(9)
_cell_length_c                   15.4647(10)
_cell_measurement_reflns_used    4411
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      25.27
_cell_measurement_theta_min      2.99
_cell_volume                     2986.9(3)
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.991
_diffrn_measurement_device_type  'PHOTON 100 CMOS detector'
_diffrn_measurement_method       'omega scan'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0790
_diffrn_reflns_av_unetI/netI     0.0809
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.991
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            17392
_diffrn_reflns_point_group_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.991
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         25.431
_diffrn_reflns_theta_min         3.010
_diffrn_source                   'fine-focus sealed tube'
_exptl_absorpt_coefficient_mu    3.751
_exptl_absorpt_correction_T_max  0.7452
_exptl_absorpt_correction_T_min  0.5537
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS (Bruker, 2014)'
_exptl_crystal_density_diffrn    1.853
_exptl_crystal_description       plate
_exptl_crystal_F_000             1614
_exptl_crystal_size_max          0.180
_exptl_crystal_size_mid          0.150
_exptl_crystal_size_min          0.070
_refine_diff_density_max         1.406
_refine_diff_density_min         -1.223
_refine_diff_density_rms         0.152
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.027
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     363
_refine_ls_number_reflns         5483
_refine_ls_number_restraints     2
_refine_ls_restrained_S_all      1.027
_refine_ls_R_factor_all          0.0968
_refine_ls_R_factor_gt           0.0495
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0396P)²+1.8199P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0846
_refine_ls_wR_factor_ref         0.0998
_reflns_Friedel_coverage         0.000
_reflns_number_gt                3679
_reflns_number_total             5483
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c9dt02758k2.cif
_cod_data_source_block           1_CCDC1
_cod_depositor_comments
'Adding full bibliography for 7700723--7700724.cif.'
_cod_database_code               7700724
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.552
_shelx_estimated_absorpt_t_max   0.779
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
C1 C 0.2800(8) 0.1766(5) 0.2421(6) 0.050(2) Uani 1 1 d . . .
H1A H 0.2767 0.1633 0.3023 0.060 Uiso 1 1 calc R U .
H1B H 0.3277 0.2235 0.2474 0.060 Uiso 1 1 calc R U .
C2 C 0.3391(7) 0.1102(5) 0.2075(6) 0.046(2) Uani 1 1 d . . .
H2A H 0.3493 0.1259 0.1500 0.055 Uiso 1 1 calc R U .
H2B H 0.4170 0.1022 0.2498 0.055 Uiso 1 1 calc R U .
C3 C 0.0870(8) 0.2281(5) 0.2373(6) 0.048(2) Uani 1 1 d . . .
H3A H 0.1121 0.2817 0.2537 0.058 Uiso 1 1 calc R U .
H3B H 0.0994 0.1981 0.2927 0.058 Uiso 1 1 calc R U .
C4 C -0.0415(8) 0.2273(5) 0.1847(6) 0.046(2) Uani 1 1 d . . .
C5 C -0.1129(10) 0.2909(6) 0.1840(7) 0.066(3) Uani 1 1 d . . .
H5 H -0.0819 0.3373 0.2132 0.079 Uiso 1 1 calc R U .
C6 C -0.2297(11) 0.2842(7) 0.1398(8) 0.088(4) Uani 1 1 d . . .
H6 H -0.2793 0.3269 0.1372 0.106 Uiso 1 1 calc R U .
C7 C -0.2755(9) 0.2143(7) 0.0983(7) 0.074(3) Uani 1 1 d . . .
H7 H -0.3560 0.2084 0.0701 0.089 Uiso 1 1 calc R U .
C8 C -0.1985(8) 0.1539(5) 0.1002(5) 0.048(2) Uani 1 1 d . . .
H8 H -0.2283 0.1070 0.0717 0.058 Uiso 1 1 calc R U .
C9 C 0.1605(8) 0.2554(4) 0.1142(6) 0.045(2) Uani 1 1 d . . .
H9A H 0.0807 0.2621 0.0743 0.054 Uiso 1 1 calc R U .
H9B H 0.1840 0.3048 0.1459 0.054 Uiso 1 1 calc R U .
C10 C 0.3925(7) 0.2852(5) -0.0017(6) 0.044(2) Uani 1 1 d . . .
C11 C 0.3227(7) 0.2969(5) 0.0528(5) 0.041(2) Uani 1 1 d . . .
H11 H 0.3309 0.3425 0.0874 0.049 Uiso 1 1 calc R U .
C12 C 0.2390(7) 0.2407(4) 0.0569(5) 0.038(2) Uani 1 1 d . . .
C13 C 0.2281(7) 0.1717(4) 0.0064(5) 0.0322(18) Uani 1 1 d . . .
C14 C 0.3033(7) 0.1611(5) -0.0464(5) 0.040(2) Uani 1 1 d . . .
H14 H 0.2981 0.1153 -0.0801 0.048 Uiso 1 1 calc R U .
C15 C 0.3857(7) 0.2178(5) -0.0495(6) 0.049(2) Uani 1 1 d . . .
H15 H 0.4362 0.2095 -0.0844 0.058 Uiso 1 1 calc R U .
C16 C 0.2918(8) -0.0036(5) 0.2834(5) 0.048(2) Uani 1 1 d . . .
H16A H 0.3708 0.0081 0.3220 0.058 Uiso 1 1 calc R U .
H16B H 0.2861 -0.0600 0.2747 0.058 Uiso 1 1 calc R U .
C17 C 0.2058(8) 0.0212(5) 0.3309(6) 0.045(2) Uani 1 1 d . . .
C18 C 0.2362(10) 0.0161(6) 0.4246(6) 0.061(3) Uani 1 1 d . . .
H18 H 0.3118 0.0010 0.4584 0.073 Uiso 1 1 calc R U .
C19 C 0.1522(10) 0.0339(6) 0.4667(6) 0.070(3) Uani 1 1 d . . .
H19 H 0.1703 0.0314 0.5295 0.084 Uiso 1 1 calc R U .
C20 C 0.0415(10) 0.0553(6) 0.4143(6) 0.064(3) Uani 1 1 d . . .
H20 H -0.0165 0.0678 0.4412 0.077 Uiso 1 1 calc R U .
C21 C 0.0177(8) 0.0579(5) 0.3234(6) 0.052(2) Uani 1 1 d . . .
H21 H -0.0585 0.0706 0.2885 0.063 Uiso 1 1 calc R U .
C22 C 0.3255(7) -0.0167(5) 0.1363(5) 0.039(2) Uani 1 1 d . . .
H22A H 0.3092 0.0069 0.0767 0.047 Uiso 1 1 calc R U .
H22B H 0.4105 -0.0191 0.1629 0.047 Uiso 1 1 calc R U .
C23 C 0.3023(9) -0.2355(6) 0.1617(7) 0.063(3) Uani 1 1 d . . .
C24 C 0.3473(8) -0.1606(5) 0.1652(6) 0.052(2) Uani 1 1 d . . .
H24 H 0.4270 -0.1521 0.1942 0.063 Uiso 1 1 calc R U .
C25 C 0.2765(7) -0.0980(5) 0.1266(5) 0.0379(19) Uani 1 1 d . . .
C26 C 0.1574(7) -0.1112(4) 0.0822(5) 0.0319(18) Uani 1 1 d . . .
C27 C 0.1127(8) -0.1872(4) 0.0828(5) 0.042(2) Uani 1 1 d . . .
H27 H 0.0326 -0.1965 0.0565 0.051 Uiso 1 1 calc R U .
C28 C 0.1864(9) -0.2485(5) 0.1218(7) 0.057(3) Uani 1 1 d . . .
H28 H 0.1561 -0.2989 0.1206 0.069 Uiso 1 1 calc R U .
Cl1 Cl 0.4929(2) 0.35808(15) -0.0097(2) 0.0733(8) Uani 1 1 d . . .
Cl2 Cl 0.3931(3) -0.31160(19) 0.2133(3) 0.1148(13) Uani 1 1 d . . .
Dy1 Dy 0.06031(3) 0.06373(2) 0.10723(2) 0.02914(12) Uani 1 1 d . . .
I1 I 0.29344(6) 0.03446(4) 0.74226(4) 0.0608(2) Uani 1 1 d . . .
N1 N 0.1582(6) 0.1940(4) 0.1830(4) 0.0407(17) Uani 1 1 d . . .
N2 N 0.2744(6) 0.0344(4) 0.1945(4) 0.0383(16) Uani 1 1 d . . .
N3 N -0.0823(6) 0.1597(4) 0.1413(4) 0.0390(16) Uani 1 1 d . . .
N4 N 0.0988(6) 0.0431(4) 0.2804(4) 0.0451(18) Uani 1 1 d . . .
O1 O 0.1498(4) 0.1172(3) 0.0124(3) 0.0354(13) Uani 1 1 d . . .
O2 O 0.0860(4) -0.0524(3) 0.0382(3) 0.0304(12) Uani 1 1 d . . .
O3 O -0.0794(6) -0.0260(4) 0.1337(4) 0.0496(16) Uani 1 1 d D . .
H3C H -0.109(7) -0.053(4) 0.087(4) 0.060 Uiso 1 1 d D U .
H3D H -0.130(6) -0.031(5) 0.162(5) 0.060 Uiso 1 1 d D U .
O4 O -0.434(3) 0.055(2) 0.038(3) 0.12(2) Uiso 0.24(2) 1 d . . P
H4C H -0.4810 0.0194 0.0086 0.145 Uiso 0.24(2) 1 d R U P
H4D H -0.3986 0.0367 0.0903 0.145 Uiso 0.24(2) 1 d R U P
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N1 C1 C2 113.6(6) . .
N1 C1 H1A 108.8 . .
C2 C1 H1A 108.8 . .
N1 C1 H1B 108.8 . .
C2 C1 H1B 108.8 . .
H1A C1 H1B 107.7 . .
N2 C2 C1 114.8(7) . .
N2 C2 H2A 108.6 . .
C1 C2 H2A 108.6 . .
N2 C2 H2B 108.6 . .
C1 C2 H2B 108.6 . .
H2A C2 H2B 107.5 . .
N1 C3 C4 110.6(7) . .
N1 C3 H3A 109.5 . .
C4 C3 H3A 109.5 . .
N1 C3 H3B 109.5 . .
C4 C3 H3B 109.5 . .
H3A C3 H3B 108.1 . .
N3 C4 C5 122.8(9) . .
N3 C4 C3 115.7(8) . .
C5 C4 C3 121.5(8) . .
C6 C5 C4 118.3(10) . .
C6 C5 H5 120.8 . .
C4 C5 H5 120.8 . .
C5 C6 C7 120.5(10) . .
C5 C6 H6 119.8 . .
C7 C6 H6 119.8 . .
C8 C7 C6 117.9(10) . .
C8 C7 H7 121.0 . .
C6 C7 H7 121.0 . .
N3 C8 C7 122.8(9) . .
N3 C8 H8 118.6 . .
C7 C8 H8 118.6 . .
C12 C9 N1 117.0(7) . .
C12 C9 H9A 108.0 . .
N1 C9 H9A 108.0 . .
C12 C9 H9B 108.0 . .
N1 C9 H9B 108.0 . .
H9A C9 H9B 107.3 . .
C15 C10 C11 120.9(8) . .
C15 C10 Cl1 119.4(7) . .
C11 C10 Cl1 119.7(7) . .
C10 C11 C12 120.2(8) . .
C10 C11 H11 119.9 . .
C12 C11 H11 119.9 . .
C13 C12 C11 120.0(8) . .
C13 C12 C9 120.4(7) . .
C11 C12 C9 119.6(7) . .
O1 C13 C14 122.2(7) . .
O1 C13 C12 119.7(7) . .
C14 C13 C12 118.1(7) . .
C15 C14 C13 121.0(8) . .
C15 C14 H14 119.5 . .
C13 C14 H14 119.5 . .
C10 C15 C14 119.8(9) . .
C10 C15 H15 120.1 . .
C14 C15 H15 120.1 . .
N2 C16 C17 114.2(7) . .
N2 C16 H16A 108.7 . .
C17 C16 H16A 108.7 . .
N2 C16 H16B 108.7 . .
C17 C16 H16B 108.7 . .
H16A C16 H16B 107.6 . .
N4 C17 C18 122.3(9) . .
N4 C17 C16 117.9(7) . .
C18 C17 C16 119.7(9) . .
C19 C18 C17 118.7(10) . .
C19 C18 H18 120.6 . .
C17 C18 H18 120.6 . .
C20 C19 C18 118.8(9) . .
C20 C19 H19 120.6 . .
C18 C19 H19 120.6 . .
C21 C20 C19 119.2(10) . .
C21 C20 H20 120.4 . .
C19 C20 H20 120.4 . .
N4 C21 C20 123.4(9) . .
N4 C21 H21 118.3 . .
C20 C21 H21 118.3 . .
C25 C22 N2 112.4(6) . .
C25 C22 H22A 109.1 . .
N2 C22 H22A 109.1 . .
C25 C22 H22B 109.1 . .
N2 C22 H22B 109.1 . .
H22A C22 H22B 107.9 . .
C28 C23 C24 120.1(8) . .
C28 C23 Cl2 120.0(8) . .
C24 C23 Cl2 119.8(8) . .
C23 C24 C25 121.4(9) . .
C23 C24 H24 119.3 . .
C25 C24 H24 119.3 . .
C24 C25 C26 119.0(8) . .
C24 C25 C22 120.4(7) . .
C26 C25 C22 120.5(7) . .
O2 C26 C25 121.1(7) . .
O2 C26 C27 120.3(7) . .
C25 C26 C27 118.5(7) . .
C28 C27 C26 120.7(8) . .
C28 C27 H27 119.7 . .
C26 C27 H27 119.7 . .
C23 C28 C27 120.2(9) . .
C23 C28 H28 119.9 . .
C27 C28 H28 119.9 . .
O1 Dy1 O2 83.74(17) . .
O1 Dy1 O3 149.74(18) . .
O2 Dy1 O3 74.10(19) . .
O1 Dy1 O2 76.89(17) . 3
O2 Dy1 O2 69.99(18) . 3
O3 Dy1 O2 76.31(18) . 3
O1 Dy1 N3 110.73(19) . .
O2 Dy1 N3 147.31(19) . .
O3 Dy1 N3 80.4(2) . .
O2 Dy1 N3 84.52(18) 3 .
O1 Dy1 N2 80.29(19) . .
O2 Dy1 N2 80.05(18) . .
O3 Dy1 N2 114.9(2) . .
O2 Dy1 N2 143.88(19) 3 .
N3 Dy1 N2 130.1(2) . .
O1 Dy1 N4 139.1(2) . .
O2 Dy1 N4 110.69(19) . .
O3 Dy1 N4 69.6(2) . .
O2 Dy1 N4 143.8(2) 3 .
N3 Dy1 N4 78.1(2) . .
N2 Dy1 N4 65.8(2) . .
O1 Dy1 N1 73.39(19) . .
O2 Dy1 N1 146.2(2) . .
O3 Dy1 N1 135.0(2) . .
O2 Dy1 N1 125.97(18) 3 .
N3 Dy1 N1 66.0(2) . .
N2 Dy1 N1 71.9(2) . .
N4 Dy1 N1 74.7(2) . .
O1 Dy1 Dy1 78.09(12) . 3
O2 Dy1 Dy1 35.76(11) . 3
O3 Dy1 Dy1 71.86(14) . 3
O2 Dy1 Dy1 34.23(11) 3 3
N3 Dy1 Dy1 116.39(15) . 3
N2 Dy1 Dy1 113.51(15) . 3
N4 Dy1 Dy1 135.50(14) . 3
N1 Dy1 Dy1 149.62(14) . 3
C3 N1 C1 110.3(6) . .
C3 N1 C9 105.4(6) . .
C1 N1 C9 110.7(6) . .
C3 N1 Dy1 109.5(5) . .
C1 N1 Dy1 109.0(5) . .
C9 N1 Dy1 112.0(5) . .
C16 N2 C2 109.5(6) . .
C16 N2 C22 109.6(6) . .
C2 N2 C22 107.3(6) . .
C16 N2 Dy1 114.6(5) . .
C2 N2 Dy1 107.2(4) . .
C22 N2 Dy1 108.4(4) . .
C8 N3 C4 117.6(7) . .
C8 N3 Dy1 121.1(5) . .
C4 N3 Dy1 119.6(6) . .
C17 N4 C21 117.6(8) . .
C17 N4 Dy1 118.9(6) . .
C21 N4 Dy1 123.4(6) . .
C13 O1 Dy1 143.3(4) . .
C26 O2 Dy1 123.4(4) . .
C26 O2 Dy1 125.3(4) . 3
Dy1 O2 Dy1 110.01(18) . 3
Dy1 O3 H3C 109(6) . .
Dy1 O3 H3D 143(6) . .
H3C O3 H3D 103(8) . .
H4C O4 H4D 108.3 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 N1 1.492(10) .
C1 C2 1.512(12) .
C1 H1A 0.9700 .
C1 H1B 0.9700 .
C2 N2 1.486(10) .
C2 H2A 0.9700 .
C2 H2B 0.9700 .
C3 N1 1.479(10) .
C3 C4 1.500(12) .
C3 H3A 0.9700 .
C3 H3B 0.9700 .
C4 N3 1.348(10) .
C4 C5 1.375(12) .
C5 C6 1.356(14) .
C5 H5 0.9300 .
C6 C7 1.384(15) .
C6 H6 0.9300 .
C7 C8 1.371(12) .
C7 H7 0.9300 .
C8 N3 1.341(10) .
C8 H8 0.9300 .
C9 C12 1.488(11) .
C9 N1 1.498(10) .
C9 H9A 0.9700 .
C9 H9B 0.9700 .
C10 C15 1.356(12) .
C10 C11 1.364(11) .
C10 Cl1 1.752(8) .
C11 C12 1.396(10) .
C11 H11 0.9300 .
C12 C13 1.395(10) .
C13 O1 1.338(8) .
C13 C14 1.392(11) .
C14 C15 1.387(11) .
C14 H14 0.9300 .
C15 H15 0.9300 .
C16 N2 1.477(9) .
C16 C17 1.488(12) .
C16 H16A 0.9700 .
C16 H16B 0.9700 .
C17 N4 1.330(10) .
C17 C18 1.386(11) .
C18 C19 1.381(14) .
C18 H18 0.9300 .
C19 C20 1.371(14) .
C19 H19 0.9300 .
C20 C21 1.350(12) .
C20 H20 0.9300 .
C21 N4 1.349(11) .
C21 H21 0.9300 .
C22 C25 1.492(11) .
C22 N2 1.506(10) .
C22 H22A 0.9700 .
C22 H22B 0.9700 .
C23 C28 1.348(13) .
C23 C24 1.378(13) .
C23 Cl2 1.722(9) .
C24 C25 1.379(11) .
C24 H24 0.9300 .
C25 C26 1.395(10) .
C26 O2 1.356(8) .
C26 C27 1.400(10) .
C27 C28 1.380(11) .
C27 H27 0.9300 .
C28 H28 0.9300 .
Dy1 O1 2.247(5) .
Dy1 O2 2.311(5) .
Dy1 O3 2.382(6) .
Dy1 O2 2.401(4) 3
Dy1 N3 2.521(6) .
Dy1 N2 2.547(6) .
Dy1 N4 2.602(7) .
Dy1 N1 2.614(6) .
Dy1 Dy1 3.8610(7) 3
O2 Dy1 2.401(4) 3
O3 H3C 0.84(2) .
O3 H3D 0.85(2) .
O4 H4C 0.8500 .
O4 H4D 0.8500 .
