#------------------------------------------------------------------------------
#$Date: 2019-11-16 05:02:29 +0200 (Sat, 16 Nov 2019) $
#$Revision: 227930 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/70/19/7701952.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7701952
loop_
_publ_author_name
'Kan, Wei-Qiu'
'He, Yuan-Chun'
'Wen, Shizheng'
'Zhao, Pu Su'
_publ_section_title
;
 A series of host-guest coordination polymers containing viologens:
 syntheses, crystal Structures, thermo/photochromism and influence factors
 of the thermo/photochromic behaviors
;
_journal_name_full               'Dalton Transactions'
_journal_paper_doi               10.1039/C9DT03929E
_journal_year                    2019
_chemical_formula_moiety         'C28 H20 Co N O7,(H2 O)'
_chemical_formula_sum            'C28 H22 Co N O8'
_chemical_formula_weight         559.40
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2019-07-03 deposited with the CCDC.	2019-11-15 downloaded from the CCDC.
;
_cell_angle_alpha                72.491(3)
_cell_angle_beta                 83.489(3)
_cell_angle_gamma                80.575(3)
_cell_formula_units_Z            2
_cell_length_a                   9.5637(17)
_cell_length_b                   10.988(2)
_cell_length_c                   11.922(2)
_cell_measurement_reflns_used    2053
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      23.0143
_cell_measurement_theta_min      2.2458
_cell_volume                     1175.9(4)
_computing_cell_refinement
'CrysAlisPro(1.171.35.21) (Agilent Tech., 2012)'
_computing_data_collection
'CrysAlisPro(1.171.35.21) (Agilent Tech., 2012)'
_computing_data_reduction
'CrysAlisPro(1.171.35.21) (Agilent Tech., 2012)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXL-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 10.0
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_measurement_method       'ω scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0411
_diffrn_reflns_av_sigmaI/netI    0.0630
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            9717
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.34
_diffrn_reflns_theta_min         1.80
_exptl_absorpt_coefficient_mu    0.787
_exptl_absorpt_correction_T_max  0.875
_exptl_absorpt_correction_T_min  0.815
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlis (Oxford Diffraction, 2006)
;
_exptl_crystal_colour            green
_exptl_crystal_density_diffrn    1.580
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             576
_exptl_crystal_size_max          0.26
_exptl_crystal_size_mid          0.23
_exptl_crystal_size_min          0.17
_refine_diff_density_max         0.251
_refine_diff_density_min         -0.464
_refine_diff_density_rms         0.068
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.043
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     349
_refine_ls_number_reflns         4303
_refine_ls_number_restraints     5
_refine_ls_restrained_S_all      1.043
_refine_ls_R_factor_all          0.0652
_refine_ls_R_factor_gt           0.0433
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0449P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0917
_refine_ls_wR_factor_ref         0.1008
_reflns_number_gt                3269
_reflns_number_total             4303
_reflns_threshold_expression     >2σ(I)
_cod_data_source_file            c9dt03929e2.cif
_cod_data_source_block           compound-1
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_symmetry_cell_setting' value 'Triclinic' was changed to
'triclinic' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 6909 2019-04-08 15:41:33Z antanas 
;
_cod_original_cell_volume        1176.0(4)
_cod_database_code               7701952
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Co1 Co 0.88704(4) 0.05465(4) 0.91106(3) 0.02355(14) Uani 1 1 d .
C1 C 0.6849(3) 0.1865(3) 0.7284(3) 0.0282(7) Uani 1 1 d .
C2 C 0.1754(3) 0.1319(3) 0.8477(2) 0.0260(7) Uani 1 1 d .
C3 C 0.5309(3) 0.2204(3) 0.7009(2) 0.0244(7) Uani 1 1 d .
C4 C 0.4254(3) 0.1733(3) 0.7846(2) 0.0234(7) Uani 1 1 d .
H4 H 0.4494 0.1260 0.8604 0.028 Uiso 1 1 calc R
C5 C 0.2844(3) 0.1955(3) 0.7576(2) 0.0233(6) Uani 1 1 d .
C6 C 0.2467(3) 0.2684(3) 0.6445(2) 0.0273(7) Uani 1 1 d .
H6 H 0.1525 0.2844 0.6256 0.033 Uiso 1 1 calc R
C7 C 0.3526(3) 0.3164(3) 0.5609(2) 0.0296(7) Uani 1 1 d .
C8 C 0.4934(3) 0.2928(3) 0.5881(2) 0.0278(7) Uani 1 1 d .
H8 H 0.5631 0.3254 0.5310 0.033 Uiso 1 1 calc R
C9 C 0.1903(3) 0.4264(4) 0.4105(3) 0.0419(9) Uani 1 1 d .
H9A H 0.1426 0.4914 0.4468 0.050 Uiso 1 1 calc R
H9B H 0.1372 0.3536 0.4348 0.050 Uiso 1 1 calc R
C10 C 0.1967(3) 0.4807(3) 0.2781(2) 0.0307(7) Uani 1 1 d .
C11 C 0.0719(3) 0.5254(3) 0.2214(2) 0.0323(8) Uani 1 1 d .
H11 H -0.0147 0.5254 0.2657 0.039 Uiso 1 1 calc R
C12 C 0.0742(3) 0.5699(3) 0.1000(2) 0.0311(7) Uani 1 1 d .
H12 H -0.0112 0.5986 0.0639 0.037 Uiso 1 1 calc R
C13 C 0.2006(3) 0.5727(3) 0.0308(2) 0.0269(7) Uani 1 1 d .
C14 C 0.3241(3) 0.5320(4) 0.0892(3) 0.0486(10) Uani 1 1 d .
H14 H 0.4109 0.5356 0.0453 0.058 Uiso 1 1 calc R
C15 C 0.3231(3) 0.4861(4) 0.2104(3) 0.0491(10) Uani 1 1 d .
H15 H 0.4085 0.4586 0.2465 0.059 Uiso 1 1 calc R
C16 C 0.2041(3) 0.6124(3) -0.1003(2) 0.0245(7) Uani 1 1 d .
C17 C 0.2845(3) 0.5334(3) -0.1626(3) 0.0328(8) Uani 1 1 d .
H17 H 0.3391 0.4586 -0.1213 0.039 Uiso 1 1 calc R
C18 C 0.2858(3) 0.5628(3) -0.2841(3) 0.0362(8) Uani 1 1 d .
H18 H 0.3434 0.5097 -0.3235 0.043 Uiso 1 1 calc R
C19 C 0.2017(3) 0.6708(3) -0.3467(3) 0.0354(8) Uani 1 1 d .
H19 H 0.1999 0.6898 -0.4281 0.042 Uiso 1 1 calc R
C20 C 0.1205(3) 0.7501(3) -0.2871(3) 0.0318(7) Uani 1 1 d .
H20 H 0.0621 0.8221 -0.3287 0.038 Uiso 1 1 calc R
C21 C 0.1239(3) 0.7249(3) -0.1658(2) 0.0243(7) Uani 1 1 d .
C22 C 0.0551(3) 0.8290(3) -0.1117(3) 0.0291(7) Uani 1 1 d .
C23 C 0.3523(4) 0.0639(4) 0.3965(3) 0.0490(10) Uani 1 1 d .
H23 H 0.2741 0.0487 0.4502 0.059 Uiso 1 1 calc R
C24 C 0.3318(4) 0.1170(4) 0.2795(3) 0.0522(10) Uani 1 1 d .
H24 H 0.2403 0.1364 0.2539 0.063 Uiso 1 1 calc R
C25 C 0.5746(4) 0.1153(4) 0.2365(3) 0.0523(10) Uani 1 1 d .
H25 H 0.6505 0.1347 0.1812 0.063 Uiso 1 1 calc R
C26 C 0.5999(4) 0.0602(3) 0.3533(3) 0.0448(9) Uani 1 1 d .
H26 H 0.6926 0.0414 0.3764 0.054 Uiso 1 1 calc R
C27 C 0.4875(3) 0.0324(3) 0.4369(3) 0.0328(7) Uani 1 1 d .
C28 C 0.4183(5) 0.1929(4) 0.0746(3) 0.0706(13) Uani 1 1 d .
H28A H 0.5074 0.2054 0.0297 0.106 Uiso 1 1 calc R
H28B H 0.3572 0.2737 0.0609 0.106 Uiso 1 1 calc R
H28C H 0.3743 0.1329 0.0508 0.106 Uiso 1 1 calc R
N1 N 0.4431(3) 0.1413(3) 0.2015(2) 0.0439(7) Uani 1 1 d .
O1 O 0.7061(2) 0.1285(2) 0.83608(17) 0.0341(5) Uani 1 1 d .
O2 O 0.7778(2) 0.2125(3) 0.64863(19) 0.0566(8) Uani 1 1 d .
O3 O 0.2161(2) 0.0722(2) 0.94856(16) 0.0371(6) Uani 1 1 d .
O4 O 0.0530(2) 0.1381(2) 0.81467(17) 0.0336(5) Uani 1 1 d .
O5 O 0.3297(2) 0.3869(2) 0.44640(18) 0.0504(7) Uani 1 1 d .
O6 O 0.1191(2) 0.8452(2) -0.03206(18) 0.0398(6) Uani 1 1 d .
O7 O -0.0559(2) 0.8981(2) -0.1537(2) 0.0410(6) Uani 1 1 d .
O1W O 1.0366(3) 0.0860(3) 0.5693(3) 0.0698(8) Uani 1 1 d D
H1A H 0.9509(18) 0.096(3) 0.593(4) 0.105 Uiso 1 1 d D
H1B H 1.0735(12) 0.0185(8) 0.5554(11) 0.105 Uiso 1 1 d D
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 Co1 O4 111.77(8) . 1_655
O1 Co1 O6 101.88(9) . 2_666
O4 Co1 O6 92.49(9) 1_655 2_666
O1 Co1 O7 100.18(9) . 1_646
O4 Co1 O7 90.24(9) 1_655 1_646
O6 Co1 O7 154.95(9) 2_666 1_646
O1 Co1 O3 91.42(8) . 2_657
O4 Co1 O3 156.81(8) 1_655 2_657
O6 Co1 O3 82.63(9) 2_666 2_657
O7 Co1 O3 85.12(9) 1_646 2_657
O2 C1 O1 125.5(3) . .
O2 C1 C3 119.6(3) . .
O1 C1 C3 114.9(3) . .
O3 C2 O4 125.4(3) . .
O3 C2 C5 116.8(2) . .
O4 C2 C5 117.7(2) . .
C4 C3 C8 118.9(3) . .
C4 C3 C1 120.7(2) . .
C8 C3 C1 120.4(3) . .
C3 C4 C5 121.2(2) . .
C3 C4 H4 119.4 . .
C5 C4 H4 119.4 . .
C4 C5 C6 119.9(3) . .
C4 C5 C2 119.4(2) . .
C6 C5 C2 120.6(2) . .
C7 C6 C5 118.8(3) . .
C7 C6 H6 120.6 . .
C5 C6 H6 120.6 . .
O5 C7 C8 114.6(3) . .
O5 C7 C6 124.4(3) . .
C8 C7 C6 121.0(3) . .
C7 C8 C3 120.2(3) . .
C7 C8 H8 119.9 . .
C3 C8 H8 119.9 . .
O5 C9 C10 108.7(2) . .
O5 C9 H9A 110.0 . .
C10 C9 H9A 110.0 . .
O5 C9 H9B 110.0 . .
C10 C9 H9B 110.0 . .
H9A C9 H9B 108.3 . .
C15 C10 C11 118.1(3) . .
C15 C10 C9 122.3(3) . .
C11 C10 C9 119.5(3) . .
C12 C11 C10 120.8(3) . .
C12 C11 H11 119.6 . .
C10 C11 H11 119.6 . .
C11 C12 C13 121.5(3) . .
C11 C12 H12 119.2 . .
C13 C12 H12 119.2 . .
C14 C13 C12 116.7(3) . .
C14 C13 C16 121.3(3) . .
C12 C13 C16 122.0(3) . .
C15 C14 C13 122.3(3) . .
C15 C14 H14 118.9 . .
C13 C14 H14 118.9 . .
C10 C15 C14 120.5(3) . .
C10 C15 H15 119.8 . .
C14 C15 H15 119.8 . .
C17 C16 C21 117.3(3) . .
C17 C16 C13 119.7(3) . .
C21 C16 C13 122.9(3) . .
C18 C17 C16 122.0(3) . .
C18 C17 H17 119.0 . .
C16 C17 H17 119.0 . .
C19 C18 C17 120.0(3) . .
C19 C18 H18 120.0 . .
C17 C18 H18 120.0 . .
C20 C19 C18 119.0(3) . .
C20 C19 H19 120.5 . .
C18 C19 H19 120.5 . .
C19 C20 C21 121.4(3) . .
C19 C20 H20 119.3 . .
C21 C20 H20 119.3 . .
C20 C21 C16 120.2(3) . .
C20 C21 C22 117.6(3) . .
C16 C21 C22 121.8(2) . .
O6 C22 O7 124.9(3) . .
O6 C22 C21 116.6(3) . .
O7 C22 C21 118.3(3) . .
C24 C23 C27 121.2(3) . .
C24 C23 H23 119.4 . .
C27 C23 H23 119.4 . .
N1 C24 C23 120.1(3) . .
N1 C24 H24 120.0 . .
C23 C24 H24 120.0 . .
N1 C25 C26 120.9(3) . .
N1 C25 H25 119.5 . .
C26 C25 H25 119.5 . .
C25 C26 C27 120.1(3) . .
C25 C26 H26 119.9 . .
C27 C26 H26 119.9 . .
C23 C27 C26 116.9(3) . .
C23 C27 C27 122.0(4) . 2_656
C26 C27 C27 121.1(4) . 2_656
N1 C28 H28A 109.5 . .
N1 C28 H28B 109.5 . .
H28A C28 H28B 109.5 . .
N1 C28 H28C 109.5 . .
H28A C28 H28C 109.5 . .
H28B C28 H28C 109.5 . .
C25 N1 C24 120.8(3) . .
C25 N1 C28 120.2(3) . .
C24 N1 C28 118.9(3) . .
C1 O1 Co1 129.40(19) . .
C2 O3 Co1 129.31(19) . 2_657
C2 O4 Co1 127.34(18) . 1_455
C7 O5 C9 120.0(2) . .
C22 O6 Co1 145.5(2) . 2_666
C22 O7 Co1 112.4(2) . 1_464
H1A O1W H1B 121.0(19) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Co1 O1 1.9762(19) .
Co1 O4 2.027(2) 1_655
Co1 O6 2.052(2) 2_666
Co1 O7 2.061(2) 1_646
Co1 O3 2.0947(19) 2_657
C1 O2 1.226(3) .
C1 O1 1.273(3) .
C1 C3 1.507(4) .
C2 O3 1.255(3) .
C2 O4 1.262(3) .
C2 C5 1.504(4) .
C3 C4 1.384(4) .
C3 C8 1.393(4) .
C4 C5 1.387(4) .
C4 H4 0.9300 .
C5 C6 1.399(4) .
C6 C7 1.388(4) .
C6 H6 0.9300 .
C7 O5 1.373(3) .
C7 C8 1.386(4) .
C8 H8 0.9300 .
C9 O5 1.406(3) .
C9 C10 1.508(4) .
C9 H9A 0.9700 .
C9 H9B 0.9700 .
C10 C15 1.374(4) .
C10 C11 1.384(4) .
C11 C12 1.380(4) .
C11 H11 0.9300 .
C12 C13 1.384(4) .
C12 H12 0.9300 .
C13 C14 1.380(4) .
C13 C16 1.489(4) .
C14 C15 1.380(4) .
C14 H14 0.9300 .
C15 H15 0.9300 .
C16 C17 1.391(4) .
C16 C21 1.403(4) .
C17 C18 1.386(4) .
C17 H17 0.9300 .
C18 C19 1.380(4) .
C18 H18 0.9300 .
C19 C20 1.376(4) .
C19 H19 0.9300 .
C20 C21 1.391(4) .
C20 H20 0.9300 .
C21 C22 1.503(4) .
C22 O6 1.256(3) .
C22 O7 1.258(3) .
C23 C24 1.364(5) .
C23 C27 1.385(5) .
C23 H23 0.9300 .
C24 N1 1.337(4) .
C24 H24 0.9300 .
C25 N1 1.329(4) .
C25 C26 1.373(5) .
C25 H25 0.9300 .
C26 C27 1.388(4) .
C26 H26 0.9300 .
C27 C27 1.485(6) 2_656
C28 N1 1.479(4) .
C28 H28A 0.9600 .
C28 H28B 0.9600 .
C28 H28C 0.9600 .
O3 Co1 2.0947(19) 2_657
O4 Co1 2.027(2) 1_455
O6 Co1 2.052(2) 2_666
O7 Co1 2.061(2) 1_464
O1W H1A 0.838(10) .
O1W H1B 0.823(9) .
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
O1W H1A O2 0.838(10) 2.093(15) 2.844(4) 149(3) .
O1W H1B O1W 0.823(9) 2.533(6) 3.061(6) 123.0(6) 2_756
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O2 C1 C3 C4 169.1(3) . .
O1 C1 C3 C4 -9.2(4) . .
O2 C1 C3 C8 -6.8(5) . .
O1 C1 C3 C8 175.0(3) . .
C8 C3 C4 C5 0.9(4) . .
C1 C3 C4 C5 -175.0(3) . .
C3 C4 C5 C6 -1.0(4) . .
C3 C4 C5 C2 174.1(3) . .
O3 C2 C5 C4 7.5(4) . .
O4 C2 C5 C4 -169.5(3) . .
O3 C2 C5 C6 -177.4(3) . .
O4 C2 C5 C6 5.5(4) . .
C4 C5 C6 C7 0.5(4) . .
C2 C5 C6 C7 -174.6(3) . .
C5 C6 C7 O5 178.7(3) . .
C5 C6 C7 C8 0.1(5) . .
O5 C7 C8 C3 -178.9(3) . .
C6 C7 C8 C3 -0.2(5) . .
C4 C3 C8 C7 -0.3(5) . .
C1 C3 C8 C7 175.6(3) . .
O5 C9 C10 C15 0.5(5) . .
O5 C9 C10 C11 179.5(3) . .
C15 C10 C11 C12 2.2(5) . .
C9 C10 C11 C12 -176.8(3) . .
C10 C11 C12 C13 -0.6(5) . .
C11 C12 C13 C14 -1.6(5) . .
C11 C12 C13 C16 176.0(3) . .
C12 C13 C14 C15 2.3(6) . .
C16 C13 C14 C15 -175.3(3) . .
C11 C10 C15 C14 -1.5(6) . .
C9 C10 C15 C14 177.5(4) . .
C13 C14 C15 C10 -0.8(6) . .
C14 C13 C16 C17 49.3(4) . .
C12 C13 C16 C17 -128.2(3) . .
C14 C13 C16 C21 -133.7(3) . .
C12 C13 C16 C21 48.8(4) . .
C21 C16 C17 C18 -0.4(4) . .
C13 C16 C17 C18 176.7(3) . .
C16 C17 C18 C19 -2.4(5) . .
C17 C18 C19 C20 1.9(5) . .
C18 C19 C20 C21 1.3(5) . .
C19 C20 C21 C16 -4.2(5) . .
C19 C20 C21 C22 168.2(3) . .
C17 C16 C21 C20 3.6(4) . .
C13 C16 C21 C20 -173.4(3) . .
C17 C16 C21 C22 -168.5(3) . .
C13 C16 C21 C22 14.5(4) . .
C20 C21 C22 O6 -139.7(3) . .
C16 C21 C22 O6 32.6(4) . .
C20 C21 C22 O7 35.8(4) . .
C16 C21 C22 O7 -151.9(3) . .
C27 C23 C24 N1 -1.0(6) . .
N1 C25 C26 C27 -0.9(6) . .
C24 C23 C27 C26 1.5(6) . .
C24 C23 C27 C27 -176.4(4) . 2_656
C25 C26 C27 C23 -0.6(5) . .
C25 C26 C27 C27 177.3(4) . 2_656
C26 C25 N1 C24 1.5(6) . .
C26 C25 N1 C28 -176.0(3) . .
C23 C24 N1 C25 -0.6(6) . .
C23 C24 N1 C28 177.0(4) . .
O2 C1 O1 Co1 -3.1(5) . .
C3 C1 O1 Co1 175.05(18) . .
O4 Co1 O1 C1 23.3(3) 1_655 .
O6 Co1 O1 C1 120.9(3) 2_666 .
O7 Co1 O1 C1 -71.1(3) 1_646 .
O3 Co1 O1 C1 -156.4(3) 2_657 .
O4 C2 O3 Co1 8.6(5) . 2_657
C5 C2 O3 Co1 -168.19(19) . 2_657
O3 C2 O4 Co1 -0.5(5) . 1_455
C5 C2 O4 Co1 176.29(19) . 1_455
C8 C7 O5 C9 -174.7(3) . .
C6 C7 O5 C9 6.7(5) . .
C10 C9 O5 C7 -170.2(3) . .
O7 C22 O6 Co1 7.9(5) . 2_666
C21 C22 O6 Co1 -176.9(2) . 2_666
O6 C22 O7 Co1 5.6(4) . 1_464
C21 C22 O7 Co1 -169.53(19) . 1_464
